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MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE LAMINATES UNDER FOUR POINT BENDING FOR DAMAGE DETECTION AND SENSOR PLACEMENT OPTIMIZATION by STEPHEN ABOAGYE ADU SAMIT ROY, COMMITTEE CHAIR MARK BARKEY EDWARD SAZONOV A THESIS Submitted in partial fulfillment of the requirements for the degree of Master of Science in the Department of Aerospace Engineering and Mechanics in the Graduate School of The University of Alabama TUSCALOOSA, ALABAMA 2013

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MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE LAMINATES

UNDER FOUR POINT BENDING FOR DAMAGE DETECTION AND SENSOR

PLACEMENT OPTIMIZATION

by

STEPHEN ABOAGYE ADU

SAMIT ROY, COMMITTEE CHAIR

MARK BARKEY

EDWARD SAZONOV

A THESIS

Submitted in partial fulfillment of the requirements

for the degree of Master of Science

in the Department of Aerospace Engineering and Mechanics

in the Graduate School of

The University of Alabama

TUSCALOOSA, ALABAMA

2013

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Copyright Stephen Aboagye Adu 2013

ALL RIGHTS RESERVED

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ABSTRACT

Laminated carbon fiber-reinforced polymer composites (CFRPs) possess very high

specific strength and stiffness and this has accounted for their wide use in structural applications,

most especially in the aerospace industry, where the trade-off between weight and strength is

critical. Even though they possess much larger strength ratio as compared to metals like

aluminum and lithium, damage in the metals mentioned is rather localized. However, CFRPs

generate complex damage zones at stress concentration, with damage progression in the form of

matrix cracking, delamination and fiber fracture or fiber/matrix de-bonding.

This thesis is aimed at performing; stiffness degradation analysis on composite coupons,

containing embedded delamination using the Four-Point Bend Test. The Lamb wave-based

approach as a structural health monitoring (SHM) technique is used for damage detection in the

composite coupons.

Tests were carried-out on unidirectional composite coupons, obtained from panels

manufactured with pre-existing defect in the form of embedded delamination in a laminate of

stacking sequence [06/904/06]T. Composite coupons were obtained from panels, fabricated using

vacuum assisted resin transfer molding (VARTM), a liquid composite molding (LCM) process.

The discontinuity in the laminate structure due to the de-bonding of the middle plies caused by

the insertion of a 0.3 mm thick wax, in-between the middle four (4) ninety degree (90o) plies, is

detected using lamb waves generated by surface mounted piezoelectric (PZT) actuators. From

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the surface mounted piezoelectric sensors, response for both undamaged (coupon with no defect)

and damaged (delaminated coupon) is obtained.

A numerical study of the embedded crack propagation in the composite coupon under

four-point and three-point bending was carried out using FEM. Model validation was then

carried out comparing the numerical results with the experimental. Here, surface-to-surface

contact property was used to model the composite coupon under simply supported boundary

conditions. Theoretically calculated bending stiffness’s and maximum deflection were compared

with that of the experimental case and the numerical. After the FEA model was properly

benchmarked with test data and exact solution, data obtained from the FEM model were used for

sensor placement optimization.

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DEDICATION

This thesis is dedicated to everyone who prayed, assisted and guided me through the

trials of creating this manuscript. In particular, my family and close friends who stood by me

throughout the time taken to complete this thesis work.

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LIST OF ABBREVIATIONS

ASTM American society for testing and materials

CFRP Carbon fiber reinforced polymer

CLT Classical lamination theory

CZM Cohesive zone method

EPFM Elastic-plastic fracture mechanics

FEA Finite element analysis

FEM Finite element methods

IM7 Intermediate modulus 7

LEFM Linear elastic fracture mechanics

MTS Mechanical testing services

PMC Polymer matrix composites

PZT Lead zirconate titanate

RTM Resin transfer molding

SHM Structural health monitoring

SNOBFIT Stable noisy optimization by branch and fit

SPO Sensor placement optimization

VARTM Vacuum assisted resin transfer molding

VCCT Virtual crack closure technique

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ACKNOWLEDGEMENTS

My sincerest gratitude first and foremost, goes to God Almighty for bringing me this far

in life, to my committee members without who’s guidance this manuscript could not have been

made and then to my family and friends.

I am most indebted to my advisor Dr. Samit Roy, for giving me the opportunity to be part

of the NASA Structural Health Monitoring (SHM) team and for his excellent technical guidance,

encouragement, and academic advice. I would also like to acknowledge my thesis committee

members, Dr. Mark Barkey and Dr. Edward Sazonov for their time, valuable advice and

feedback. Their unsurpassed knowledge in their respective fields made it possible for this thesis

to be completed.

I also appreciate the knowledge and time investment made by Dr. Susan Burkett and Dr.

Sushma Kotru. Their lab and technical guidance played a major role with regard to the structural

health monitoring section of this thesis. The friendly and cheerful nature of the entire SHM

group; Nicholas Hayes, Donald Tyler Paul, Ben Fairbee, Kanchan Trivedi, Michelle Spiegel,

Akshata Nagabhushana, Muhammed Farooq and Hao Zheng made this research work possible. I

am very grateful for the group’s assistance and guidance at the initial stages of the composite

fabrication process, experimental and numerical testing. Special thanks to Priyank Upadhyaya

for his valuable input in the numerical modeling.

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This thesis would not have been possible without the support from the United States

National Aeronautics and Space Administration, grant number: NNX10AJ14G; Technical

monitor, Dr. Curtis E. Banks, NASA MSFC. Their financial support is very much appreciated.

I would like to acknowledge the financial, academic and technical support of The

University of Alabama, Tuscaloosa and its staff, particularly in the award of a Graduate

Teaching Assistantship and giving me an opportunity to realize my dream.

My final thanks go to my family, especially my mum for her prayers and support.

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CONTENTS

ABSTRACT ................................................................................................ ii

DEDICATION ........................................................................................... iv

LIST OF ABBREVIATIONS ......................................................................v

ACKNOWLEDGEMENTS ....................................................................... vi

LIST OF TABLES .......................................................................................x

LIST OF FIGURES ................................................................................... xi

CHAPTER 1: INTRODUCTION ................................................................1

CHAPTER 2: LITERATURE REVIEW .....................................................5

2.1 Introduction ............................................................................................5

2.2 Composite materials...............................................................................5

2.3 Damaged in laminated composites ........................................................8

2.4 Modeling damage in laminated composites .........................................15

2.5 Four-point bend test .............................................................................16

2.6 Modeling techniques used in delamination..........................................18

CHAPTER 3: FABRICATION OF COMPOSITE LAMINATE ..............22

CHAPTER 4: STRUCTURAL HEALTH MONITORING ......................27

4.1 Damage detection.................................................................................28

4.2 Lamb wave methods ............................................................................29

4.3 Sensing methods ..................................................................................29

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4.4 Piezoelectric transducers and principle of operation ...........................30

4.5 Actuation parameters ...........................................................................30

4.6 Delamination detection ........................................................................31

4.7 Test for damage detection ....................................................................34

4.8 Experimental analysis of damage evolution in delaminated coupon ...36

CHAPTER 5: FINITE ELEMENT ANALYSIS .......................................41

CHAPTER 6: FINITE ELEMENT MODEL FOR OPTIMIZATION ......50

6.1 Interfaces between MATLAB and Abaqus ..........................................50

6.2 Embedded delamination test ................................................................51

CHAPTER 7: CONCLUSIONS AND FUTURE WORK .........................55

7.1 Conclusion ...........................................................................................55

7.2 Suggestions for future work .................................................................57

REFERENCES ..........................................................................................59

APPENDIX A: LabVIEW program...........................................................66

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LIST OF TABLES

Table 4.1: Comparison of Slope (Structural stiffness) of the Load-Deflection data obtained

from the Four-Point Bend Test of tested specimens of dimension (10 in. x 1 in. x 0.14 in).........38

Table 4.2 Comparison of Slope (Structural stiffness) of the Load-Deflection data obtained

from the Four-Point Bend Test of tested specimens of dimension (254mm x25.4mm x3.6mm)

(Presented in SI units)…………………………............................................................................38

Table 4.3 Comparison of the peak load and peak stress of the tested specimens..........................39

Table 4.4 Comparison of the peak load and peak stress of the tested specimens (Presented in

SI units)..........................................................................................................................................39

Table 5.1 Material properties of IM7/PET15 composite used for numerical simulation

(Presented in SI units)....................................................................................................................41

Table 5.2: Comparison of the maximum deflections, for damaged and undamaged specimens

of stacking sequence [06/904/06]T under three-point and four-point load conditions..................49

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LIST OF FIGURES

Figure 2.1 Schematic of modes of failure in CFRP laminates [5].................................................14

Figure 2.2 Schematic of laminate configuration (16 plies) with wax insert in-between the

middle ply......................................................................................................................................14

Figure 2.3 Schematic of a beam cross-section under four-point bending.....................................17

Figure 3.1 Schematic of the VARTM Process [65].......................................................................22

Figure 3.2 Photograph showing wax on resin inlet side and cladded aluminum sheet on the

vacuum outlet side of the laid carbon fiber plies...........................................................................24

Figure 3.3 VARTM materials stacking sequence (release fabric, carbon fibers, release fabric,

distribution mesh) and taping process............................................................................................25

Figure 3.4, (a) Vacuum Pulled on system and (b) Vacuum Gauge on the Resin Catch reading

about 95kPa....................................................................................................................................25

Figure 3.5 Photograph of setup being de-bulked, showing inlet-outlet lines, resin catch and

vacuum pump.................................................................................................................................26

Figure 3.6 Photograph of VARTM manufactured laminate [06/904/06]T with embedded

delamination...................................................................................................................................26

Figure 4.1 A typical PZT excitation input signal for the testing scheme used in this study.........31

Figure 4.2 Data acquisition system using PZT actuators and sensors...........................................33

Figure 4.3 Pictorial representation of composite coupon with delamination (wax insert)

demonstrating the actuator and sensor placement relative to delamination..................................35

Figure 4.4 Experimental results comparing the Lamb wave response of a [06/904/06]T

orientation undamaged coupon and a coupon with embedded delamination in the middle

four plies........................................................................................................................................35

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Figure 4.5 Photographs of the Four-Point Bend Fixtures mounted in the MTS QTest 25

machine..........................................................................................................................................36

Figure 4.6 Photographs showing damaged specimen, (a) under load; (b) Delamination

Extension in specimen; (c) and (d) Transition from Matrix Crack, Delamination to Fiber

Fracture..........................................................................................................................................37

Figure 4.7 Crack initiation and evolution in the undamaged coupon............................................37

Figure 4.8 Schematic of the support and load spans of the Four-Point Bend Fixtures.................38

Figure 4.9 Load (F)-Deflection plots for Damaged and Undamaged specimen under Four-Point

Bending .........................................................................................................................................40

Figure 5.1 Illustration of damaged coupon with partial delamination in-between two

sub-laminates (1) and (2), with stacking sequence of [06/902]T and [902/06]T respectively...........43

Figure 5.2 FE model of a composite coupon with stacking sequence of [06/904/06]T

Representing the loading and boundary conditions for Four-Point Bending................................43

Figure 5.3 Abaqus results showing the deflection contour plot and legend for undamaged

composite coupon undergoing Four-Point Bending in millimeters...............................................44

Figure 5.4 (a) and (b), FE model showing top and bottom sub-laminates of stacking sequence

[06/902]T and [902/06]T respectively.............................................................................................45

Figure 5.5 (a) and (b), FE model showing constraint and interaction property for damaged

composite coupon..........................................................................................................................45

Figure 5.6 Abaqus results showing the deflection contour plot and legend for damaged

composite coupon undergoing Four-Point Bending in millimeters...............................................46

Figure 5.7 FE model of undamaged composite coupon with stacking sequence of

[06/904/06]T representing the load and boundary conditions for Three-Point Bending.............47

Figure 5.8 Abaqus results showing the deflection contour plot and legend for undamaged

composite coupon undergoing Three-Point Bending in millimeters.............................................47

Figure 5.9 (a) and (b), FE model showing constraint and interaction property for damaged

composite coupon..........................................................................................................................48

Figure 5.10 Abaqus results showing the deflection contour plot and legend for damaged

composite coupon undergoing Three-Point Bending in millimeters.............................................48

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Figure 6.1 A flow chart demonstrating MATLAB, Abaqus interface used for generating data

set for sensor placement optimization (where count is the iteration number)...............................51

Figure 6.2 A FE representation of longitudinal strain component contour plot observed on the

top surface of a composite coupon with embedded delamination (in the middle) and subjected

to four point bending......................................................................................................................52

Figure 6.3 A Flow chart demonstrating the sensor placement optimization process....................53

Figure 6.4 Displacement surface plot comparison between damaged and undamaged coupon....54

Figure 6.5 Initial and final placement of sensors after completion of optimization algorithm

(dots represent sensors)..................................................................................................................54

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CHAPTER 1

INTRODUCTION

Due to their low density, high specific strength and modulus to weight ratios that are markedly

superior to those of metallic materials, carbon fiber reinforced materials are being substituted for

metals in many weight critical components in aerospace, automotive and offshore structures.

However, their use in aerospace structures is still dependent on many difficulties in prediction of

damage tolerance and this has led to over-conservative designs, not fully realizing the promised

economic performance benefits. Delamination, or interfacial cracking between composite layers,

is undoubtedly one of the more common and critical types of damage in laminated fiber-

reinforced composites due to their relatively weak inter-laminar strengths. It is caused by out-of-

plane shear and normal stresses, which may arise under various circumstances such as, impact

loads, free edge effects, ply drop offs, or transverse loading and may be divided into

delamination onset and delamination growth in a laminated composite structure.

For the structural integrity of composite materials to be maintained, delamination as a

failure mode needs to be well understood, since it is difficult to detect under inspection due the

fact that delamination usually occur between plies internal to the laminate.

Tragic incidents that have occurred over the years in structures built with composite

materials have also prompted a significant amount of research in the area of damage detection in

composite materials using an array of actuator-sensor combinations placed at strategic locations.

Structural health monitoring (SHM) therefore has become a vital tool to help engineers improve

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safety and maintainability of critical structures. Here, a variety of sensing technologies with an

embedded controller to capture, log, and analyze real-time data are designed to reliably monitor

and test the health and performance of structures as seen in the case of the Boeing 787 aircraft

health monitoring plan [1].

SHM implementation over the years have helped save unnecessary maintenance

downtime, money and reduced the chances of catastrophic failures. Evolving from non-

destructive evaluation (NDE) techniques in which sensors and actuators are external to a

structure and the sensing probes can be adjusted and manipulated to extract the maximum signal,

tests are conducted at scheduled intervals. Unlike NDE techniques, examples of which include,

laser ultrasound, laser shearography, infrared thermography and X-ray radiography, in SHM, the

locations of sensors and actuators are fixed and remain on the structure continuously and are

therefore not completely unobtrusive. This integrated sensing scheme allows for continuous

monitoring and provides important information on the damage evolution; the structure does not

have to be taken out of service during structural health testing.

The SHM process involves implementation evaluation, data acquisition and damage

feature extraction, and classification. Implementation evaluation includes studying the economic

and human life safety advantages, possible damage types, operational and environmental

conditions, cost and maintenance needs and the time requirement for deploying the SHM system.

The data acquisition portion of the process involved a decision about the number and type of

sensors, placement of sensors, type of actuation, acquisition hardware, and signal transmission

hardware and data storage. A signal processing step is typically performed after data acquisition

to cleanse and remove any noise from the data. In feature extraction, damage sensitive features

such as the natural frequency of vibration, strain, time of flight, displacement, and modal shape,

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are separated out while also compensating for any environmental effects. As a final step, a

statistical analysis of acquired data leads to a classification of the structure as damaged or

undamaged [2].

The four-point bend test has been used over the years to carry out various tests, ranging

from determination of flexural properties and bending stiffness’s of all kinds of materials, to the

investigation and evaluation of the different modes of failure in engineering materials. Unlike the

three point bend test, the four-point bending method allows for uniform load distribution

between the two loading fixtures. Following the testing conventions specified in the American

Society for Testing and Materials (ASTM D6272-00), transverse vertical loads are applied to

horizontal beams such that, a constant bending moment results between the two inner load

locations. With the embedded delamination located mid-way along the length of the coupon and

across the width of the specimen, the four-point bend test serve as an appropriate engineering

procedure for the analysis of stiffness degradation in the composite coupon. Here the specimen

lies on a span and stress is uniformly distributed between the loading fixtures. The horizontal

distance between the two support fixtures and the vertical depth which a specimen can be

displaced are dependent on material type and thickness. The load span to support can also be a

ratio of 1 to 2, or 1 to 3.

Historical data for the experiment was obtained for analyses from data acquisition

software and hardware used with the machine.

In this thesis, a Lamb wave-based approach for damage detection in composite coupon

with embedded delamination is described. A surface mounted piezoelectric actuator was used to

generate Lamb waves in a composite coupon and the response was measured using a surface

mounted piezoelectric sensor. This aspect of the research involves optimization of testing

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parameters, sensor location and the number of sensors. Stiffness degradation under four-point

bend test was also investigated using a universal testing machine (MTS QTest/25) with a pre-

written program (Testworks QT 2.03), and data acquisition software.

The thesis is divided into seven chapters. Chapter 2 is focused on reviewing the available

research in the areas relevant to this project. An introduction to composite materials and a

discussion of damage in laminated composites is provided, followed by a review of analysis

methods employed to study failure, in particular delamination, in laminates. The four-point bend

test (FPBT), as a failure analysis tool in composite materials is also discussed. Some modeling

techniques used in the analysis of delamination is also presented in this chapter. The processing

of composite laminates, with and without delamination is presented in Chapter 3.

A brief background on SHM using different sensors is presented in chapter 4. The damage

detection system used to detect embedded delamination in a composite coupon is also detailed in

this chapter. Mechanical property testing and delamination propagation, in CFRP coupons under

four-point bending using the MTS machine is presented, and corresponding experimental results

are analyzed for both damaged and undamaged coupons. Chapter 5 describes the finite element

simulation of delamination in composite coupons, using the commercially available finite

element code Abaqus. Chapter 6 has details on the sensor optimization process. Here the time

domain information along with finite element analysis was used to characterize the damage. A

brief description of interfacing Abaqus and optimization algorithms that can be used for sensor

placement optimization is provided. Chapter 7, the final chapter, focuses on presenting the major

conclusions deduced from the work carried out in the project. Some suggestions for future

research are presented in this chapter.

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CHAPTER 2

LITERATURE REVIEW

2.1 Introduction

The main objective of this thesis work is damage detection, testing and sensor optimization

analysis in unidirectional intermediate modulus (IM7/epoxy) CFRP laminate coupon with an

embedded delamination using Lamb waves and the study of stiffness degradation in CFRP

laminate coupon subjected to four-point bending. However, before addressing this problem, it is

necessary to provide an introduction to the laminated composite materials and their failure

mechanisms with focus on delamination.

An introduction to composite materials and a discussion of damage in laminated

composites is first introduced in this chapter, followed by a review of the analysis methods

employed to study their failure, in particular delamination. The four-point bend test as a failure

analysis tool in laminated composites is discussed and finally modeling techniques used in the

analysis of delamination and then damage propagation in CFRP is explained.

2.2 Composite materials

The rise in demand of structural materials, with high specific strength, high specific

stiffness, low density, corrosion resistance, wear resistance, fatigue resistance and design

flexibility has led to the development of composite materials. Since it is difficult to achieve all

these desired properties within a single material, it has become necessary, to combine two or

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more materials on a macroscopic scale to form a useful third that would exhibit the best qualities

of the individual components and hence the desired properties for structural applications.

Composites therefore, are types of materials that consist of more than one constituent, where

constituent materials are proportionally distributed and geometry is controlled to obtain optimum

material properties [3]. It normally consists of a matrix and reinforcement. The matrix is used to:

transfer loads into and out of fiber

remove abrasion between fibers

transfer internal loads between fibers in short-fiber composites

provide a barrier against adverse environment

effect in-plane shear and inter-laminar shear properties of composites.

The reinforcement which may be fibrous or particulate provides the composite with high

stiffness and strength properties [3]. The material used in this thesis work consists of SC-780

epoxy matrix, reinforced with plies of unidirectional IM7 carbon fiber with the total stacking

sequence of [06/904/06]T.

2.2.1 Classification of composite materials

Composite materials are classified into two categories, fiber-reinforced composites and

particle-reinforced composites. They are further re-classified based on the kind of matrix

material used in their formation and this leads to four different categories of composites namely;

polymer matrix composites (PMCs), metal-matrix composites (MMCs), ceramic-matrix

composites (CMCs), and carbon-carbon composites (CCCs) [3].

Over the years, polymer matrix composites have become dominant, due their good in-

plane stiffness and strength, low density, ease of fabricability, relatively low cost, corrosion

resistance, fatigue resistance, low coefficient of thermal expansion, creep and creep fracture

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resistance, relatively mature technology and excellent in-service experience compared to MMCs

and CMCs [3]. However, CMCs have special applications in the space industry where they serve

as thermal protection materials in the nose cap and the leading edges of the wing of space

shuttles as well as being applied in rocket nozzles and gas turbines. MMCs have found limited

use due to problems in controlling the chemical reaction between the fibers and the molten

metals at high processing temperatures required for such composites [3].

Polymer matrix composites (PMCs) consist of polymer (resin) matrix combined with

dispersed fibrous reinforcements and are very popular due to their low cost and simple

fabrication methods [4]. According to the reinforcement material, PMCs are grouped as;

Glass fiber reinforced polymers

Carbon fiber reinforced polymer composites

Kevlar (aramid) fiber reinforced polymers

They are used for manufacturing applications such as load-bearing aerospace structures, boat

bodies, automotive parts, radio controlled vehicles and bullet-proof vests and their properties are

determined by;

Properties of the fibers

Orientation of the fibers

Concentration of the fibers

Properties of the matrix

They are typically anisotropic materials and have low stiffness in the transverse fiber direction

where their properties are usually matrix-dominated. For example, the tensile strength and

modulus of a unidirectional oriented fiber-reinforced polymer are maximum when these

properties are measured in the longitudinal direction of fibers, but at any other angle, these

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properties are lower [3]. Lower mechanical properties of fiber-reinforced polymer composites in

directions other than the fiber direction and their generally anisotropic nature goes a long way to

have an effect on all aspects of their design and analysis, and failure modes, making isotropic

analytical methods inapplicable for their design analysis [5].

The design of a fiber-reinforced composite structure is considerably more difficult than

that of a metal structure, principally due to the difference in its properties in different directions.

However, its non-isotropic nature creates a unique opportunity of tailoring its properties

according to the design requirement and this coupled with their high specific strength and

stiffness have attracted many researchers over the years [3]. Compared with monolithic

materials, the damage initiation and propagation behavior of fiber-enforced composites laminates

is a distinct, complicated and a progressive phenomenon. This usually starts with matrix

cracking, which evolve to delamination between the layers and then to fiber breakage. This

adversely degrades the mechanical properties of the structures. It is therefore critical that the

nature and effect of damage in these kinds of materials is investigated for better and safer

structural applications.

2.3 Damage in laminated composites

CFRPs generate complex damage zones at stress concentration, with damage progression

in the form of, matrix cracking, delamination and fiber fracture or fiber/matrix de-bonding.

Research on the failure mechanism of unidirectional composites started in close relation to the

utilization of such composite materials in aerospace industries. Countless efforts have been made

in this area and substantial breakthroughs have been made with constant improvements of

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existing theories still on-going, to lead the way towards a better understanding of the essence

behind the various failure behaviors of lamina/laminate [6].

Since fiber reinforced composites are comprised of two materials with distinct

mechanical and thermal properties, if geometric inhomogeneity is taken into account, fiber and

matrix play different roles under different loading conditions. Fibers are longitudinally

continuous and contribute more to the development of longitudinal modulus and strength,

indicating that the fiber supports almost the entire longitudinal tensile load applied to a ply and

compressive load without consideration of fiber buckling [6]. The matrix on the other hand,

binds fibers together and contributes more to the development of transverse strength and

modulus [3].

With the longitudinal modulus of laminated composites being always greater than the

transverse modulus, minimizing the transverse stresses of laminated composite materials

therefore is a critical design consideration. Load transfer between adjacent layers in a fiber

reinforced laminate takes place by means of inter-laminar stresses which develop due to

mismatch in Poisson’s ratios and coefficients of mutual influence between various layers [3].

Generally, tensile normal stresses applied to an isotropic material cause’s elongation in

the direction of the applied stresses and contraction in the two transverse directions, a more

complex response however, is experienced in laminated composites where a combination of

extensional and shear deformation may be produced. To minimize extension-shear coupling

therefore laminates are designed to be balanced and symmetric about the mid-plane with

examples being unidirectional and cross-ply laminates. In this thesis, a carbon fiber reinforced

symmetric composite laminate was manufactured using 16 plies of unidirectional IM7 carbon

fibers with damage, in the form of delamination, embedded during manufacturing of the

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laminate. Damage mechanisms experienced by such laminates and some previous research

finding in this area are discussed in the next section.

2.3.1 Damage mechanisms in laminated composites

The mechanical separation of engineering materials is normally categorized as ductile or

brittle fractures. While ductile fractures absorb more energy, brittle fractures absorb little energy

and are generally characterized by fracture with smooth surfaces [7]. Laminated polymer matrix

composites however, often exhibit a mixture of ductile and brittle failure processes such as

delamination or inter-laminar fracture, matrix-fiber debonding and fiber breaking [8]. Various

models have been proposed in an effort to simulate in-plane and out-of-plane failure mechanisms

and describe different load distributions associated with damage accumulation [9-12]. In-plane

failure is mostly due to material property degradation and theories such as the classical

lamination theory have been used to determine in-plane stress state and the stresses/strains that

can be used to determine the failure criteria for the various failure mechanisms at locations of

interest in a material. The laminated composite material can be accepted for use in structural

application when its actual strength envelope is in agreement with what is predicted by the

failure criterion.

When external and thermal loadings are applied to carbon fiber reinforced composite

laminates, non-uniform micro-stresses at the constituent level develop due to material and

geometric inhomogeneity arising from the inclusion of fibers. Any point within the composite

belongs to one of three regions namely, the fiber, the matrix, or the fiber-matrix interface. This

leads to the initiation of ply failure which can have dissimilar failure mechanisms based on the

location of critical points [6]. Failure in the form of transverse matrix cracking normally occur in

90o

plies, delamination typically occur between 0o and 90

o plies, longitudinal matrix cracking

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takes place in the fiber direction of 0o plies and fiber fracture in the 0

o plies. All the modes of

failure mentioned above are in-plane with the exception of delamination, which is an out-of-

plane damage mode which evolves with inter-laminar stresses [13].

Matrix cracking as an intra-laminar laminated composite failure mode, can adversely

affect the integrity of the composites by initiating other damage developments such as

delamination and fiber fracture, which leads to stiffness reduction of the composite laminate

[14]. For structural integrity of laminated composites to be maintained therefore, insight into the

matrix cracking phenomenon in composite laminates is required. Over the years, a lot of research

has gone in search of better understanding, and prediction of transverse cracking behavior and its

effects on the modulus reduction of laminated composites [11, 15-24]. Shear-lag analysis was

used by Highsmith and Reifsnider [11] for predicting modulus reduction of cross-ply laminates

due to matrix cracking. A modified version of this was adopted by Lim and Hong [15] where the

concept of inter-laminar shear layer and an energy criterion was used to predict the progressive

matrix cracking and stiffness reduction in cross-ply laminates. Smith and Ogin [22] also

presented a one-dimensional analysis of a cross-ply laminate with embedded transverse crack,

under flexural load, where bending theory was used in conjunction with shear-lag analysis to

calculate the degradation of longitudinal modulus of a cracked transverse ply from which the

laminate flexural modulus is to be determined.

Fiber fracture, the mechanical separation of fibers in fiber reinforced composite laminates

owing to the application of stress can be categorized as ductile or brittle fractures. Brittle

fractures absorb little energy and are mostly characterized by fracture with flat surfaces, while

ductile fractures absorb more energy [25]. It represents the ultimate mode of failure of the

composite since most of the load carrying capabilities of the laminate are achieved by the fibers.

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A fracture in the fibers therefore leads to a severe decrease in modulus of the fibers which is

detectable by conventional failure interrogation. It is usually preceded by the occurrence of other

modes of failure such as matrix cracking and delamination. To predict fiber fracture as the

ultimate failure mode of the fiber therefore, models representing the progressive development of

all modes of damage, from transverse matrix cracking and delamination as well as interactions

between the two need to be modeled. The type of materials, the orientation of the laminate plies,

geometry and type of loading play a major part in the complexity of the interaction between the

different damage modes.

High inter-laminar stresses accounts for delamination, a failure mechanism uniquely

characteristic of composite laminates. The existence of these inter-laminar stresses leads to

delamination around free edges of composite laminates at locations around the edges, around a

hole, or at the ends of tubular configuration. Delamination therefore causes a reduction in

stiffness and strength, which leads to premature failure in laminated composites and therefore

needs to be critically considered in specimen design [26].

The influence of delamination on the structural behavior of fiber-reinforced composite

laminates is well known and has been studied extensively in the literature. This kind of damage

is usually embedded within a composite structure, which makes it invisible to the naked eye and

hence difficult to detect under inspection. Due to the complexity of this kind of damage, a lot of

research still needs to be carried out to overcome the issue of overly conservative design in the

application of fiber reinforced composite laminates. A review of relevant literature on work

carried out by a number of researchers in the area of delamination analysis of CFRP is discussed

in the following paragraph.

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Wang et al. [27] considered two types of delamination, namely, delamination initiating

from the intersection of the transverse cracks and the free edges of the laminate, and

delamination initiating from the intersection of transverse cracks and longitudinal splits in the 0o

layers. Here three dimensional finite element analyses was carried out on CFRP cross-ply

laminates to estimate the energy release during delamination growth which led to results which

agreed qualitatively with the experimental. Analytical methods with a capability of predicting the

stress transfer between 0o and 90

o plies in a [0/90/0] cross-ply laminate containing transverse

cracks were developed by McCartney [24]. Wimmer et al. [28] used a combination of a first ply

failure criterion and a fracture mechanics approach where FEM was used to simulate

delamination in a structure without initial delamination and flaws. To predict the delamination

onset, the failure criterion developed by Puck was used, and starting delamination was created

based on the results obtained from the Puck criterion. It was built on a physically based,

phenomenological model which is suitable for long fiber reinforced polymers. Here difference

between fiber failure and the other several modes of matrix dominated failure was established,

with delamination being one of them. Delamination strengths were estimated by slightly

reducing the transverse ply strengths. Stresses in each Gauss point was evaluated together with

the spatial distribution of the risk of failure and failure mode. Virtual growth of the starting

delamination was simulated using virtual crack closure technique (VCCT), where delamination

growth was modeled based on the Griffith crack growth criterion assuming linear elastic fracture

mechanics (LEFM) which can be applied only when a starting crack exists. LEFM deals with the

occurrence of brittle fracture due to crack growth in the absence of noticeable plastic

deformation at the crack tip [29]. Results obtained were in agreement with simulation using

cohesive zone method (CZM), where cohesive element is used to describe the cohesive forces,

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which occur when material elements are being pulled apart. In CZM, the cohesive elements open

to simulate crack initiation and growth. The procedure allowed for the determination of the

critical size and location of a starting delamination and provided information about the

delamination growth stability. Figure 2.1 below is a schematic of a cross-ply laminate showing

the various failure modes in a composite laminate.

Figure 2.1 Schematic of modes of failure in CFRP laminates [5]

In this thesis however, an embedded delamination was artificially inserted at the mid-plane

between the middle four 90o plies of a composite laminate of stacking sequence [06/904/06]T

made up of unidirectional IM7-SC 780 carbon/epoxy composite laminate using a 0.3 mm thick

wax insert. Delaminated and undamaged coupons of dimension (254 mm x 3.5 mm) cut-out from

the same manufactured panel were analyzed. Here the four-point and three-point bend tests were

employed to investigate stiffness degradation of composite coupons containing embedded

delamination. Figure 2.2 below is a schematic of the laminate cross-sectional configuration with

0.3 mm thick wax insert.

Figure 2.2 Schematic of laminate configuration (16 plies) with Wax insert in-between the middle

Ply

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2.4 Modeling damage in laminated composites

This section reviews some of the methods that have been employed over the years in the

design and analysis of damage in laminated composites.

2.4.1 Fracture mechanics

Failures normally occur for many reasons, including defects in materials, inadequacies in

design, uncertainties in loading or environment, and deficiencies in construction or maintenance.

Design against fracture has a technology of its own, and this has become very active in areas of

current research.

Fracture mechanics therefore, deals with mechanics of solids containing planes of

displacement discontinuities (cracks), with special attention to their growth. The nature of the

manufacturing process of laminated polymer composites provides innumerable sites for the

initiation of all kinds of defects in their interior and surfaces. Not all these defects however

become unstable or grow under service conditions. To determine if a flaw is stable or will

propagate as a crack and cause failure requires the use of fracture mechanics, which is divided

into two sections as discussed next.

2.4.1.1 Linear elastic fracture mechanics

Linear elastic fracture mechanics (LEFM) is the basic theory of fracture that deals with

sharp cracks in linearly elastic bodies. It is applicable to any material as long as the material is

elastic except in a vanishingly small region at the crack tip (assumption of small scale yielding),

brittle or quasi-brittle fracture, and stable or unstable crack growth. Griffith began his pioneering

studies of fracture in the years just prior to 1920 where he considered how it might be used in

developing a fundamental approach in predicting fracture strengths. He employed an energy-

balance approach to investigate fracture in very brittle materials, specifically glass rods [25]. It

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was however realized that, when the materials exhibits more ductility, consideration of the

surface energy alone failed to provide an accurate model for fracture. This deficiency was later

remedied independently, by Irwin and Orowan [30]. They suggested that a majority of the

released strain energy in ductile materials was absorbed not by creating new surfaces, but by

energy dissipation due to plastic flow in the material near the crack tip. They also suggested that

catastrophic fracture occurred when the strain energy was released at a rate sufficient to satisfy

the needs of all these energy “sinks,” and denoted this critical strain energy release rate by the

parameter Gc. Therefore LEFM generally gives an accurate criterion for the establishment of

catastrophic failure in brittle materials but runs into a limitation for brittle materials having blunt

notches, but no cracks, since a finite initial crack size is required for its application. Another

limitation for ductile materials occurs, where the size of the non-linear zone due to plasticity is

not negligible. To overcome these limitations therefore required non-linear fracture mechanics

and is discussed next.

2.4.1.2 Elastic-plastic fracture mechanics

In elastic-plastic fracture mechanics (EPFM), the crack tip undergoes significant plasticity.

Usually applicable in engineering materials that exhibit some nonlinear elastic and inelastic

behavior under operating conditions that involves large loads. It applies to elastic-rate-

independent plastic materials generally in the range of large-scale plastic deformation.

2.5 Four-point bend test

The four-point bend test together with three-point bend test, remain the two most used

methods for the determination of flexural properties of laminates. Flexural tests are usually used

to determine the mechanical properties of resins and laminated fiber composite materials owing

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to their simplicity in terms of procedure, instrumentation and equipment requirement [31]. In the

four-point bend method usually a flat rectangular beam specimen is simply supported close to its

ends and with two loads placed symmetrically between the supports, giving four-point bending

load condition as shown in Figure 2.3 below. Here the bending moments increase linearly from

zero at the supports to a maximum at the loading points and are constant between these points, as

shown in Figure 2.3. The shear force and inter-laminar shear stress are zero between the loading

points, so that, that portion of the beam specimen is subjected to a pure bending moment. The

American Society for Testing and Materials (ASTM) specifications allows a series of different

span-to-thickness (S/h) ratios (16:1, 32:1, 40:1 and 60:1) in four-point bending [31], and also

specifies the appropriate specimen width, length, support spans for four-point bending and rate

of crosshead motion for the full range of specimen thicknesses and span-to-thickness ratios

allowed.

Figure 2.3 Schematic of a beam cross-section under four-point bending

Over the years, fracture characterization of all kinds of bonded joints under the opening

(Mode I dominant fracture) has been extensively studied and documented. The four-point bend

test has also been used to investigate the flexural modulus of various engineering materials as

well as different modes of delamination and mixed-mode fractures. More recently, Mode II

fracture toughness of different end-notched flexural (ENF) specimen has been investigated using

the four-point bend test. Martin and Davidson [31] first proposed the use of four-point bending to

analyze Mode II fracture toughness of end-notched flexure specimen (4-ENF) in (1999).

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Schuecker and Davidson (2000) [32]; Vinciquerrqa and Davidson 2000 [33]; Yoshihara 2004,

2008 [34]; de Morais and de Moura 2006 [35]; and Thouless 2009 [36], have all studied fracture

characterization of 4-ENF with focus on specimens made of symmetric sub-layers with identical

material. Qiao et al. [37] used it to analyze mixed-mode fracture of hybrid material bonded

interfaces where a combined analytical and experimental approach was used to characterize the

mixed-mode fracture. The closed-form solution of the compliance and energy release rate (ERR)

was also obtained. The solutions predicted by the conventional beam theory (CBT) and finite-

element analysis (FEA) were in strong agreement with the analytical solution for both the

compliance and ERR of the mixed mode fracture specimens. It was established that the crack-tip

deformation played an important role in accurately characterizing the mixed-mode fracture

toughness of hybrid material bonded interfaces under four-point bending load. In this thesis

however, the four-point bending was used to analyze flexural stiffness degradation for a

composite laminate with an embedded delamination.

2.6 Modeling techniques used in delamination analysis

Progressive failure in composite structures have been modeled over the years with

different models ranging from, the fairly simple material property/stiffness degradation methods

(MPDM) to much more sophisticated MPDM based on continuum damage mechanics (CDM)

and fracture mechanics. The idea of MPDM is that the damaged material’s post-initial failure

behavior is modeled by reduced stiffness, an example of which is given by Tan et al. [38–40]

who proposed a two-dimensional (2D) progressive damage model for laminates containing

central holes subjected to in-plane tensile or compressive loading. Continuum damage mechanics

(CDM), a more sophisticated form of the material stiffness degradation scheme based on the use

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of an internal state variable has also been used to model general damage as well as delamination,

an example is given by Barbero et al. [41]. MPDM schemes are often implemented in FE codes.

In commercial FE software, the implementation is often achieved through user-defined

subroutines such as UMAT for Abaqus [42–46], Ansys [47] or LS-Dyna [48]. Because damage

in composites is three dimensional (3D) in nature with strong and complex interactions between

various damage modes, it is therefore generally modeled with (3D) elements. Delamination

propagation in composite structures, for example is a 3D phenomenon because, delamination

frequently propagates in a non-self-similar fashion and may extend into other plies and propagate

along another ply interface [49]. The presence of micro-cracks often interferes with the direction

and shape of delamination growth which leads to higher computational time and resource

requirement. Analyses based on 2D plate or shell elements [50, 51, 52, 53, 54, 55–57] are still

used in some studies to save computational effort, although Robbins and Reddy [58] recently

showed that first-order shear deformation elements do not give acceptable results and that

higher-order or 3D elements should be used.

2.6.1 Cohesive zone method

Among various damage models, the cohesive-zone model (CZM) is the most commonly

used to investigate interfacial cracks since it handles both delamination onset and growth. The

CZM approach is based on the assumption that, a cohesive zone or softening plasticity develops

near the crack tip and links the microstructural failure mechanisms to the continuum fields

governing bulk deformations. Thus, a CZM is characterized by the properties of the bulk

material, the crack initiation condition, and the crack evolution function. Cohesive damage zone

models relate traction to displacement jumps at an interface where a crack may occur. Damage

initiation is related to the interfacial strength, i.e., the maximum traction on the traction-

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displacement jump relation. When the area under the traction-displacement jump relation is

equal to the fracture toughness, the traction is reduced to zero, and new crack surfaces are

formed [59-61]. The CZM however, is numerically expensive and requires fine meshes in order

to represent the damage zone adequately.

2.6.2 Finite element method

The simulation of delamination using the finite element method (FEM) is normally

performed using the Virtual Crack Closure Technique (VCCT) [62], or decohesion finite

elements [63-64]. The VCCT is based on the assumption that the energy released during de-

lamination propagation equals the work required to close the crack back to its original position.

Based on this assumption, the single-mode components of the energy release rate are computed

from the nodal forces and nodal relative displacements [62]. Delamination growth is predicted

when a combination of the components of the energy release rate is equal to a critical value.

There are some difficulties when using the VCCT in the simulation of progressive delamination.

The calculation of fracture parameters requires nodal variable and topological information from

the nodes ahead and behind the crack front. Such calculations are tedious to perform and may

require re-meshing for crack propagation. Decohesion finite elements have been used to

overcome some of the above difficulties by being able to predict both the onset and non-self-

similar propagation of delamination. However, the simulation of progressive delamination using

decohesion elements poses numerical difficulties related with the proper definition of the

stiffness of the cohesive layer, the requirement of extremely refined meshes, and the

convergence difficulties associated with problems involving softening constitutive models.

Turon et al, in their paper: (An Engineering Solution for using Coarse Meshes in the Simulation

of Delamination with Cohesive Zone Models) addressed the proper definition of interface

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stiffness and proposed a novel procedure which allowed the use of coarse meshes in the

simulation of delamination.

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CHAPTER 3

FABRICATION OF COMPOSITE LAMINATE

Manufacturing of thermoset composite laminates can be accomplished in one of many

ways including, resin transfer molding (RTM), compression molding, and filament winding. In

this thesis work, vacuum assisted resin transfer molding (VARTM), a variation of RTM is used

in the fabrication of CFRP composite panels. The VARTM process, which is a liquid composite

molding process (LCM), involves the injection of premixed liquid thermoset resin into dry fiber

preform in a closed mold, where the liquid coats the fibers, fills spaces between fibers, expels air

and finally as it cures transforms into matrix [3]. The VARTM process has an advantage of low

tooling costs, low pressure requirements compared to compression molding and has improved

quality and fiber wet-out compared to hand layup process. An idealized schematic of the

VARTM setup is shown in Figure 3.1.

Figure 3.1 Schematic of the VARTM Process [65]

Sized unidirectional IM7 carbon fibers were used for the fabrication of the composite

panels. IM7 fibers possess high tensile and shear strength. The VARTM process involved the

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surface preparation of a one-sided hard surface mold, fiber layup, vacuum creation, resin

preparation, infusion of resin and curing. The fabricated panel used in the thesis work had ply

stacking sequence of [06/904/06]T with and without an wax insert in-between the middle four 90o

plies to simulate damaged (delaminated) and undamaged coupons respectively.

The one-sided hard surface mold in the form of a steel plate was sanded and cleaned to

remove any contaminants that may interfere with the fabrication of the laminate. The plate was

then cleaned using acetone and a release agent (Freekote) to prevent the laminate from adhering

to the plate after resin cure. To further aid in the release of the laminate after curing, a release

film of dimension 330.2 mm x 330.2 mm was placed on the mold surface before laying up the

fabric. Each ply of IM7 carbon fabric was cut into a dimension of 304.8 mm x 304.8 mm square

that form the 16 plies. Six plies were laid in the 0o direction, followed by two plies in the 90

o

direction. To embed the delamination, a 0.03 mm thick, aluminum insert of dimension 50.8 mm,

cladded in peel ply was centered on top of the eight plies at the vacuum outlet section of the

panel and a cast wax of 0.3 mm thickness of dimension of 101.6 mm x 50.8 mm, on the resin

inlet section as shown in Figure (3.2). The reason for using the two different methods above was

to investigate which one of the two would give the desired stiffness reduction outcome. The

middle section of the panel had no form of defect, to enable coupons to be obtained for the

undamaged (section of panel with no delamination - control sample) and damaged cases

respectively, from the same panel. This would allow for proper analysis and comparison of test

results.

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Figure 3.2 Photograph showing wax on resin inlet side and cladded aluminum sheet on the

vacuum outlet side of the laid carbon fiber plies

The remaining two, 90o plies and six, 0

o plies were then placed on top of the inserts in that

order and orientation, making the laminate symmetric about the mid-plane. A second release

fabric, followed by a distribution mesh, both of dimension 330.2 mm x 330.2 mm was then

placed above the stack of fibers. The low flow resistance distribution mesh, helped control the

resin flow and promoted good fiber wet-out by ensuring uniform distribution of resin. The entire

setup was vacuum sealed with the aid of tacky tape, leaving out inlet and outlet point for resin

infusion and excess resin collection respectively. Vacuum pressure was monitored with the aid of

a pressure gauge placed at the outlet which was set at 95 kPa. The vacuum was mainly used for

resin infusion and assisted in consolidating the fibers to achieve the desired fiber volume fraction

[66]. The system was then allowed to debulk for an hour to remove air pockets and promote

adhesion of fibers to resin. Figure 3.5 below shows the system being debulked, and the inlet and

outlet connections.

SC-780 matrix, a two part epoxy, mixed in a ratio of resin to hardener, 4:1 by volume, was

used as the matrix material. After the resin infusion, the setup was left for an additional 1.5 hours

to ensure uniform resin distribution and fiber wet-out by eliminating dry spots within the fiber

stack. Investigations into the flow pattern and fill time of resin distribution using finite element

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models [67, 68] has proved that the release film placed between the carbon fiber fabric and

distribution mesh reduced the resin fill time. The vacuum was removed and the setup was green

cured overnight at room temperature. The process was then followed by oven curing for 6 hours

at 71oC, and then post-curing for an additional 2 hours at 104

oC to ensure complete resin cross-

linking. The final trimmed-out panel was cut into 254 mm (10 in.) x 25.4 mm (1 in) coupons for

damage detection tests and 25.4 mm (1 in.) x 25.4 mm (1 in.) pieces for moisture and acid

digestion testing. The fiber volume fraction of the fabricated composite panel, obtained using

acid digestion experiment, was found to be in the range of 49-50%.

Figure 3.3 VARTM materials stacking sequence (release fabric, carbon fibers, release fabric,

distribution mesh) and taping process

Figure 3.4, (a) Vacuum Pulled on system and (b) Vacuum Gauge on the Resin Catch reading

about 95kPa

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Figure 3.5 Photograph of setup being de-bulked, showing inlet-outlet lines, resin catch and

vacuum pump

Figure 3.6 Photograph of VARTM manufactured laminate [06/904/06]T with embedded

delamination

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CHAPTER 4

STRUCTURAL HEALTH MONITORING

The SHM process involves implementation evaluation, data acquisition and damage

feature extraction, and classification. Implementation evaluation includes studying the economic

and human life safety advantages, possible damage types, operational and environmental

conditions, cost and maintenance needs and the time requirement for deploying the SHM system.

The data acquisition portion of the process involved a decision about the number and type of

sensors, placement of sensors, type of actuation, acquisition hardware, and signal transmission

hardware and data storage. A signal processing step is typically performed after data acquisition

to cleanse and remove any noise from the data. In feature extraction, damage sensitive features

such as the natural frequency of vibration, strain, time of flight, displacement, and modal shape,

are extracted from sensor data while also compensating for any environmental effects. As a final

step, a statistical analysis of acquired data leads to a classification of the structure as damaged or

undamaged [2]. The Boeing 787 for example, has a health monitoring plan in place which

provides real-time data which enables the prediction of remaining useful life of the structure by

detecting the existence of damage, evaluating its nature and severity and localizing the damage

[69]. The SHM process therefore involves limited human intervention with testing structural

elements not being required to be taken out of service for its implementation compared to other

NDE techniques such as laser ultrasound, laser shearography, infrared thermography and X-ray

radiography.

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4.1 Damage detection

Damage detection can be done in one of two forms, the active or passive approach.

Damage detection by the active approach involves the use of actuators such as, piezoelectric

patches to cause perturbations in a structure, while disturbances in the passive approach are

caused by ambient vibrations, damage, or impact [70]. However, in both instances, structural

response is obtained by surface mounted or embedded sensors. Kessler et al. [71] used both

approaches, with the effectiveness of the combination being confirmed later on by Mal et al.

[72]. Passive SHM can be in the form of impact measurements using foil gages or piezoelectric

sensors [72, 73] with examples of active approach being the Lamb wave technique and

impedance method.

In this thesis, damage, in the form of embedded mid-plane delamination is detected using

the Lamb wave technique. The Lamb wave technique has shown great promise among the other

damage detection methods and is capable of detecting existence of damage, its severity, type,

location and size. They were first used in damage detection by Worlton [74].

Lamb waves are elastic in nature and are used for both internal and external damage

detection due to their ability to travel through the thicknesses of plates. They respond to different

types of damage with changes in flight time, wave attenuation, phase information and

propagation characteristics [75] and are therefore very useful in investigating structural integrity.

The difference in amplitude for the damaged and undamaged structure, gives information on the

severity of the damage with the difference in time of flight providing information on the damage

location [76]. They are elastic waves confined to a plate surface and can travel long distances. A

surface mounted piezoelectric actuator was used to generate Lamb waves in a composite coupon

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and the response was measured using a surface mounted piezoelectric sensor. This aspect of the

research involved the optimization of sensor location and the number of sensors.

4.2 Lamb wave methods

Damage detection using Lamb waves involves two primary modes of operation namely;

pulse echo and pitch catch [77]. The pitch catch method involves signal transmitted by an

actuator from one end of a structure being received by a sensor placed at the opposite end.

Damage detection here relies on changes in amplitude ratio and time of flight of the transmitted

signal and can cover long distances but requires a dense network of sensors [78]. The pulse echo

uses either the same transducer or a sensor co-located with an actuator to transmit and receive

signals; with damage detection relying on reflections or echoes from any discontinuities such as

cracks or delamination in a structure.

4.3 Sensing methods

Different kinds of sensors ranging from fiber optics, fiber Bragg grating, strain gages and

magnetostrictive sensor have been used to detect various types of structural damages. However,

piezoelectric transducers have an advantage of light weight and high sensitivity to small amounts

of strain, and can generate relatively high amplitude output signals compared to the others. Also,

lead zirconate titanate (PZT) has a major advantage in its ease of use in different detection

techniques such as acoustic emission, ultrasonic Lamb waves, and strain-based methods [71].

The ability of the same PZT transducer to act as either an actuator or a sensor at any time allows

for baseline-free detection and gives the flexibility to monitor proper sensor operations. Given

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these advantages, the piezoelectric transducers coupled with Lamb waves were used for

delamination detection in composite laminate coupon in this thesis work.

4.4 Piezoelectric transducers and principle of operation

PZT actuators are normally mounted on the surfaces of composite materials to generate

Lamb waves [79]. They operate on both principles of piezoelectric and inverse piezoelectric

effect. Due to the crystalline property of piezoelectric materials, electric pulses are able to be

converted into mechanical vibrations in accordance to the inverse piezoelectric effect.

Piezoelectric sensors, on the other hand, convert mechanical vibrations into electrical charge by

the piezoelectric effect.

Examples of piezoelectric materials include lead metaniobate, PZT and polyvinylidene

fluoride. The PZT is the preferred choice when using the Lamb wave detection technique

because of its ability to withstand high operating temperatures (365oC) [78].

4.5 Actuation parameters

Piezoelectric actuators are excited by the application of voltage. To produce strong Lamb waves

with larger signal to noise ratio requires high voltage, which leads to high consumption of power

[80]. SHM systems however, have lower power requirement with an optimum voltage range of

5-10V. Higher energy is associated signals made up of large number of peaks, which

compensates for any attenuation due to damping in long distance signal propagation. Increasing

the number of peaks however, increases the pulse width and in turn, the interference [81, 82].

The use of low frequency for composite damage detection has been studied by Diamanti and

Soutis [83]. Smaller number of modes can be excited using lower frequencies which make them

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more distinguishable. The first order anti-symmetric (A0) mode has a smaller wavelength for a

given frequency compared to the first order symmetric (S0) mode making A0 waves more

sensitive to small levels of damage. S0 modes also undergo higher attenuation during propagation

[76, 82]. Based on these characteristics, a five cycle tone burst of 1 kHz center frequency and

amplitude of 6 V to generate A0 mode Lamb wave was considered in the testing protocol. The

excitation input signal is as shown below in Figure 4.1.

Figure 4.1 A typical PZT excitation input signal for the testing scheme used in this study

4.6 Delamination detection

In this thesis, delamination, a form of inter-laminar damage, prevalent in composite

laminates is detected using the Lamb wave technique. Inter-laminar stresses lead to delamination

in composites at different locations such as, around the edges and holes, which causes a

reduction in the modulus and strength of the laminate leading to premature failure [23]. The

Lamb wave based approach with PZT actuators and sensors has been used by Soni et al. [82] to

study changes in amplitude ratio due to fatigue crack. In this thesis however, the Lamb wave

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based approach was used to study delamination in composite materials. A surface mounted PZT

sensor was used to measure the response of Lamb waves generated using a surface mounted PZT

actuator. The response of Lamb waves to embedded delamination in a composite coupon

containing 16 plies of IM7 carbon fiber was studied.

4.6.1 Experimental analysis of delamination detection

Composite coupons of dimension 254 mm x 25.4 mm machined from 304.8 mm x 304.8 mm

panels were used for the test. Variation in the modulus of elasticity and width was minimized by

cutting each set of test coupon from a single piece of composite panel. Tests were carried out on

both the undamaged (coupons with no delamination) and damaged (delaminated coupons)

obtained from the same panel. A Lamb wave based approach was used for damage detection. A

surface mounted PZT actuator was used to excite Lamb waves in the composite coupon and the

response, received by surface mounted PZT sensor. The response from an undamaged composite

coupon was used as a reference baseline.

4.6.2 Data acquisition setup

The composite coupon was fixed at one end with a PZT actuator surface-mounted on the

free end. An AC signal applied to the terminals of a PZT actuator puts the coupon into vibrations

by the inverse piezoelectric effect. A Hanning modulated five cycle tone burst signal at a center

frequency of 1 kHz was used for Lamb wave excitation. The actuation signal was amplified by a

factor of 20 using a piezo amplifier before sending to the actuator. The Lamb waves, generated

by the actuator were received by the sensor located 60 mm from the clamped end. The sensor

generates a voltage equivalent to the induced strain by the direct piezoelectric effect. The sensor

was connected to a data acquisition (DAQ) card through a connector box with a sampling rate of

100 kHz. National instrument LabView software was used to synchronize the actuation initiation

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and sensor data collection (DAQ). Real time sensor data were collected for further analysis. The

experimental setup is shown in Figure 4.2 below.

Figure 4.2 Data acquisition system using PZT actuators and sensors

Actuation input was generated using an Agilent 33210A arbitrary waveform generator. A

National Instruments LabVIEW program was developed using the Agilent 33XXX driver and

VIs (virtual instruments) to control the waveform generator through the general purpose interface

bus (GPIB) port. A GPIB to USB cable connects the waveform generator to the computer. The

arbitrary waveform generation feature was utilized to generate a Hanning burst. The frequency,

amplitude, burst count and burst rate of actuation input were user configurable in the LabVIEW

program.

The output of the waveform generator was fed to a piezo amplifier AA 301HS that had an

amplification factor of 20. The amplitude of the waveform generator was set to 6 Vp-p to generate

input actuation amplitude of 120 Vp-p after amplification. This was within a safe margin for the

PZT actuator that had an operating range of 180 Vp-p.

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Data from the PZT sensors were read into a LabVIEW program using the NI DAQmx driver

software. The number of sensors to import, and the number of samples to read were configurable

in the LabVIEW program. The program displayed a real time waveform of voltage versus time

for all of the sensors for rapid data analysis. The sensor data was stored in text files for further

analysis. The experimental system was found to generate the desired amplitude and shape A0

mode Lamb waves in a composite coupon required for this study.

4.7 Test for damage detection

4.6.1 Simulated damage using an embedded longitudinal delamination

Tests were performed on 254 mm x 25.4 mm coupons, machined from [06/904/06]T

IM7/SC780 composite laminate to enable both damaged (delaminated) and undamaged coupons

to be obtained from the same panel. The fabrication process outlined in chapter 3 was followed.

Embedded delamination in between the mid-plane of the [06/904/06]T laminate extending through

the width, was used to simulate damage. . The response from an undamaged composite coupon

was used to provide a baseline for reference. The coupon was clamped at one end with a PZT

actuator disk of center frequency 7.3 kHz measured 12.7 mm in diameter and was 0.38 mm

thick. A Hanning modulated five cycle tone burst signal at a center frequency of 1 kHz was used

for Lamb wave excitation. The Lamb waves generated by the actuator were received by a PZT

sensor located 60 mm from the clamped end as shown in Figure 4.3.

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Figure 4.3 Pictorial representation of composite coupon with delamination (wax insert)

demonstrating the actuator and sensor placement relative to delamination

Figure 4.4 below shows the comparison of the Lamb wave response of an undamaged

composite coupon and a coupon with embedded delamination. The difference in amplitude ratio

of the incident wave between the undamaged and damaged coupon on the average, was found to

be 0.05% due to the embedded delamination in the damaged coupon.

Figure 4.4 Experimental results comparing the Lamb wave response of a,

[06/904/06]T orientation, undamaged coupon and a coupon with embedded delamination in the

middle four plies

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4.8 Experimental analysis of damage evolution in delaminated coupon

The four-point bend test as a failure characterization tool was employed to study crack

growth analysis on composite coupons containing embedded delamination. With the embedded

delamination located mid-way along the length of the coupon and spanning the entire width of

the specimen, the four-point bend test served as an appropriate engineering procedure for the

analysis of flexural stiffness degradation in the composite coupon. Variation in the modulus of

elasticity and width was minimized by cutting each set of test coupon from a single piece of

composite panel. The MTS QTest/25 machine with fixtures of 152.4 mm (6 in) supporting span,

and a 76.2 mm (3 in) loading span as shown in Figure 4.5 below was used for the analysis.

Figure 4.5 Photographs of the Four-Point Bend Fixtures mounted in the MTS QTest 25 machine

During the testing process to investigate crack evolution, a transverse vertical load was

applied with a crosshead speed of 2 in/min (5.08 mm/min), which initially led to matrix cracking

for the damaged specimen, then to delamination extension followed by the final state of fiber

fracture. This served as basis for investigating the various modes of failure in the composite

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coupons. Shown below in Figure 4.6, are pictures of the specimen under loading, going through

the damage evolution process in the MTS QTest/25 machine.

Figure 4.6 Photograph showing damaged specimen, (a) under load; (b) Delamination Extension

in specimen; (c) and (d) Transition from Matrix Crack, Delamination to Fiber Fracture

Damage evolution for the undamaged specimen, as shown in Figure 4.7 below, started

with matrix cracking, then delamination at the (0o/90

o) ply interface where there is a change in

stacking sequence. The four-point bend specimens then fractured in a brittle manner with across

the width-fractures, which appeared to have initiated under the central loading rollers causing not

only width-wise fracture but also inter-laminar failures between these central rollers.

Figure 4.7 Crack initiation and evolution in undamaged coupon

From the configurable program used with the Testworks QT 2.03, which enabled all the

coupon dimensions to be configured, historical data for the experiment was obtained for

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analyses. Tabulated below are the load-deflection data obtained from the test. Slopes were

obtained from linear portions of the load-deflection plots and represented the structural stiffness

of the composite coupons given as , where F represented the load and δ the

deflection at load application points as shown on the schematic below.

Figure 4.8 Schematic of the support and load spans of the Four-Point Bend Fixtures

Table 4.1: Comparison of Slope (Structural stiffness) of the Load-Deflection data obtained from

the Four-Point Bend Test of tested specimens of dimension (10 in. x 1 in. x 0.14 in)

SPECIMEN

TYPE

UNDAMAGED

1

UNDAMAGED

2

DAMAGED

1

DAMAGED

2

SLOPE

(lbs./in) 1406 1423 896 1146

Table 4.2: Comparison of Slope (Structural stiffness) of the Load-Deflection data obtained from

the Four-Point Bend Test of tested specimens of dimension

(254 mm x 25.4 mm x 3.6 mm) (Presented in SI units)

SPECIMEN

TYPE

UNDAMAGED

1

UNDAMAGED

2

DAMAGED

1

DAMAGED

2

SLOPE (k N/m) 246 249 157 200

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Table 4.3: Comparison of the peak load and peak stress of the tested specimens

SPECIMEN

NUM. TYPE

PEAK LOAD

(lbs)

PEAK STRESS

(ksi)

1 UNDAMAGED 360.1 36.7

2 UNDAMAGED 365.2 37.3

MEAN 362.65 37

STDEV 2.55 0.3

3 DAMAGED 230.0 23.6

4 DAMAGED 236.5 24.1

MEAN 233.3 23.85

STDEV 3.25 0.25

% CHANGE -36 -36

Table 4.4: Comparison of the peak load and peak stress of the tested specimens

(Presented in SI units)

SPECIMEN

NUM. TYPE PEAK LOAD (N)

PEAK STRESS

(GPa)

1 UNDAMAGED 1609 0.248

2 UNDAMAGED 1624.6 0.251

MEAN

1616.8 0.2495

STDEV

7.8 0.0015

3 DAMAGED 1023.0 0.158

4 DAMAGED 1052.0 0.162

MEAN

1037.5 0.16

STDEV

14.5 0.002

% CHANGE

-36 -36

Figure 4.9 shows a plot of the load against deflection for damaged and undamaged

specimens under the four-point bending. The undamaged specimens exhibited a greater bending

stiffness than the damaged specimens as shown by the slope of the load-deflection curve, due to

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the effect of the embedded delamination in the damaged specimen. Also, the difference in peak

load and peak stress gave information on the stiffness degradation in the damaged specimen as a

result of the embedded delamination with the average peak load for the undamaged specimen

being higher than that of the damaged.

Figure 4.9 Load (F)-Deflection plots for Damaged and Undamaged specimen under Four-Point

Bending

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CHAPTER 5

FINITE ELEMENT ANALYSIS

Due to their ability to model complex shapes and loading conditions, finite element

methods have become widely used for analyzing damage in different kinds of materials under

different loading and boundary conditions. In this present study, a two dimensional finite

element analysis of delamination in IM7-SC780 carbon/epoxy coupons of dimension

254 mm x 3.5 mm under four-point bending (FPBT) was carried out using Abaqus version 6.11-

1 commercial FEM software. Four node bilinear plane stress quadrilateral elements (CPS4R)

were used to discretize both damaged (simulated embedded delamination) and undamaged

coupons. The two dimensional shell element models for the finite element analysis were

developed using material properties of the composite coupons obtained from mechanical testing

of the specimen. These properties as tabulated in Table 5.1 were used for the numerical

simulation.

Table 5.1: Material properties of IM7/PET15 composite used for numerical simulation

(Presented in SI units)

E11 E22 E33 G12 G13 G23 Ѵ12 Ѵ21 Ѵ23

GPa GPa GPa GPa GPa GPa

113.8 5.24 5.24 31.78 31.78 1.081 0.3 0.014 0.42

The bending stiffness for the 16 plies composite laminate was obtained from the Classical

Lamination Theory (CLT) using the equations (5.1 – 5.9) below. The stiffness matrices of the 0o

and 90o plies of the laminate are given by:

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(5.1)

(5.2)

(5.3)

(5.4)

And the angle-invariant stiffness properties of the laminate , and were calculated from:

(5.5)

(5.6)

(5.7)

From Equations (5.5-5.7), the reduced stiffness matrix, was calculated from:

(5.8)

Where is the ply orientation angle of the laminate [3]. The theoretical bending stiffness for

the laminate with stacking sequence [06/904/06]T was calculated using Equation (5.9) below;

(5.9)

Where N represents the total number of laminas in the laminate and is the distance from

the mid-plane to the top of the lamina and is the distance from the mid-plane to the bottom

of the lamina.

Figure 5.1 shows a schematic of the damaged composite with partial delamination in-

between the two sub-laminates, under four-point bending.

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Figure 5.1 Illustration of damaged coupon with partial delamination in-between two sub-

laminates (1) and (2), with stacking sequence of T and T respectively

The four-point bend test of undamaged specimen was modeled using 2D shell element as

shown in Figure 5.2 below. It was modeled as a four-layered composite laminate corresponding

to the stacking sequence of T and T respectively and meshed using 2400, four

node linear quadrilateral elements (CPS4R). Both ends were fixed. For numerical analysis of the

undamaged coupon under four-point bending a uniform pressure load of 40 N/mm2 was applied

to the model.

Figure 5.2 FE model of a composite coupon with stacking sequence of

[06/904/06]T representing the loading and boundary conditions for Four-Point Bending

The value of the maximum displacement for the four-point bend test was then analyzed

numerically using Abaqus. Below is a plot of how displacement changes along the length of the

specimens for both cases of damaged and undamaged coupons.

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Figure 5.3 Abaqus results showing the deflection contour plot and legend for undamaged

composite coupon undergoing Four-Point Bending in millimeters

The damaged specimen (delaminated specimen) was modeled using two sub-laminates of

2D shell elements with one below and one above the plane of delamination. The top and bottom

sub-laminates had a stacking sequence of [06/902]T and [902/06]T respectively as shown in Figure

5.4. The sub-laminates were modeled by finite elements. The undamaged portion of the sub-

laminates was modeled using a contact element such that, the nodes corresponding to the top and

bottom sub-laminates had contact property with their rotational degrees of freedom (DOF) tied

together. Delamination was explicitly modeled, but with master-slave nodes defined for contact,

thus preventing interpenetration of contact surfaces.

The damaged portion (mid-rectangular section shown in Figure 5.5(b)) was modeled such

that the sub-laminates had just surface-to-surface property, simulating the wax insert used

experimentally. This ensured continuity of displacements and rotation at the plane of

delamination. Figures 5.4 - 5.5 below represent the model for the damaged specimen.

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Figure 5.4 (a) and (b), FE model showing top and bottom sub-laminates of stacking sequence

[06/902]T and [902/06]T respectively

Figure 5.5 (a) and (b), FE model showing constraint and interaction property for damaged

composite coupon

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Figure 5.6 Abaqus results showing the deflection contour plot and legend for damaged composite

coupon undergoing Four-Point Bending in millimeters

From the analytical results it was realized that the location of the delamination at the mid-

section of the composite coupon under four-point bending, showed limited difference in the

maximum deflection between the damaged and undamaged cases, as can be verified from the

Abaqus results, even though experimental results showed otherwise. This was later attributed to

the pure bending in-between the two loading points which led to zero shear forces and inter-

laminar shear stresses being experienced at the mid-section of the composite coupon in both

damaged and undamaged coupons under four-point bending. This situation could be remedied by

relocating the delamination to one end of the specimen or subjecting the damaged specimen to

three-point bending.

Based on this observation, finite element analysis of the composite coupon under three-

point bending was then carried out. The dimensions for both damaged and undamaged specimens

were the same as that used for the four-point bending, with the only differences being the load

and load application point. With the same material properties, finite element analysis of three-

point bending for damaged (delaminated) and undamaged composite coupons were carried out

using a mid-point uniform pressure load of 40 N/mm2. Figure 5.7 shows the load and boundary

conditions of the finite element model for the undamaged case.

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Figure 5.7 FE model of undamaged composite coupon with stacking sequence of

[06/904/06]T representing the load and boundary conditions for Three-Point Bending

The finite element model was meshed using 2400 elements and below is the deflection contour

plot and legend showing the maximum deflection of the undamaged coupon.

Figure 5.8 Abaqus results showing the deflection contour plot and legend for undamaged

composite coupon undergoing Three-Point Bending in millimeters

The delaminated specimen was modeled similar to that used for the four-point bending with the

extreme ends constrained and tied, and the delaminated mid-section with surface-to-surface

interaction property as shown in Figure 5.9.

(a)

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(b)

Figure 5.9 (a) and (b), FE model showing constraint and interaction property for damaged

composite coupon

1200 elements each for the top and bottom sub-laminates were used to discretize the model,

below is the deflection contour plot and legend showing the maximum deflection of the damaged

coupon under three-point bending.

Figure 5.10 Abaqus results showing the deflection contour plot and legend for damaged

composite coupon undergoing Three-Point Bending in millimeters

Analytical results for the maximum deflection of the damaged specimen undergoing three-

point bending showed a significant increase in displacement (28%) compared to that of the

undamaged case. This was due to the presence of delamination and the effect of shear forces and

inter-laminar shear stresses between the sub-laminates of the composite coupon as a result of the

location of the applied uniform pressure load.

The comparison of the numerical solutions for both cases of damaged and undamaged

composite coupons under three-point and four-point bending is as shown in Table 5.2.

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Table 5.2: Comparison of the maximum deflections, for damaged and undamaged specimens of

stacking sequence [06/904/06]T under three-point and four-point load conditions

Four-point bending Pressure load

(N/mm2)

Numerical

Solution

Maximum

deflection

(mm)

% difference

Undamaged specimen

40

Abaqus-CPS4R

(2400 elements) 7.41

0.80 Damaged specimen Abaqus-CPS4R

(2400 elements) 7.47

Three-point bending

Undamaged specimen

40

Abaqus-CPS4R

(2400 elements) 7.30

28.22 Damaged specimen Abaqus-CPS4R

(2400 elements) 9.36

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CHAPTER 6

FINITE ELEMENT MODEL FOR OPTIMIZATION

6.1 Interfaces between MATLAB and Abaqus

Sensing optimization problems usually seek to find a set of sensors that provides the best

possible sensing quality at the minimum possible cost. Genetic and evolutionary algorithms [84]

and stable noisy optimization by branch and fit (SNOBFIT) [85] have both been used

successfully for sensor placement optimization (SPO). Even though large sensor density

generally implies easy damage detection, the negative effect of cost, power and weight cannot be

overemphasized and therefore the need for optimal sensor locations and density. A four step

sensor optimization method was proposed by Guratzsch et al. [86], where a finite element

analysis was performed by modeling the plate thickness and material properties; Young’s

modulus, Poisson’s ratio and density, as a Gaussian random field. Each node of the finite

element model was considered for a probable sensor location and the SNOBFIT algorithm was

used for SPO.

Using an approach similar to what is outlined above; SPO was achieved for damaged and

undamaged finite element models developed using Abaqus. Data obtained from reports

generated on each particular model in Abaqus, was saved as a DAT file and called using

MATLAB to achieve the desired number of data sets for particular damaged and undamaged

cases. Each Abaqus run was called after values of material properties for both the damaged and

undamaged cases were varied within experimentally determined standard deviation to regenerate

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a new input files. A suitable feature set (strain, displacement, and stress) was written to the report

files. The data was recorded only for the top surface nodes for the undamaged model and the also

the top surface nodes of the top layer sub-laminate for the damaged case, with the aim to

optimize sensor placement only on the top surface of the specimen. Embedding the sensors or

placing sensors on the sides or bottom of the coupon were not considered in this research project.

The process flow is presented in Figure 6.1 below.

Figure 6.1 A flow chart demonstrating MATLAB, Abaqus interface used for generating data set

for sensor placement optimization (where count is the iteration number)

6.2 Embedded delamination test

The delaminated coupon of dimensions 254 mm x 25.4mm x 3.6 mm was modeled using

two sub-laminates of 3D solid element, with one below and one above the plane of delamination.

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The top and bottom sub-laminates had a stacking sequence of [06/902]T and [902/06]T

respectively, and the geometry was discretized using 38304 linear brick elements of type

C3D8R. Damage in the form of delamination was introduced into the middle section of the two

sub-laminate using wax insert. The coupon was simply supported by a four-point bend fixture of

supporting span 152.4 mm (6 in) and loading span of 76.2 mm (3 in). The coupon was subjected

to a uniform pressure load at the loading roller sections modeled as an area, with dimensions of

25.4 mm (1 in) x 3 mm (.12 in). For this test, 60 simulations were run, 30 simulations of the

undamaged model and 30 simulations of the damaged model with varying material properties.

The longitudinal strain contour plot for the damaged case is shown in Figure 6.2. The static strain

values measured from 30 undamaged simulation cases at the entire surface nodes was used to

train the classifier.

Figure 6.2 A FE representation of longitudinal strain component contour plot observed on the

top surface of a composite coupon with embedded delamination (in the middle) and subjected to

four-point bending

The aim of the experiment was to find the optimal sensor placement given the damage at a

specific location. The process flow is as summarized below in Figure 6.3.

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Figure 6.3 A flow chart demonstrating the sensor placement optimization process

Damage classification was performed using artificial neural network (ANN) and sensor

optimization carried out using the evolutionary strategy. A sample result has been added in this

section for illustration. This result came from the work led by Muhammad Farooq [87]. The

surface plot of one of the feature vectors (displacement) used in the sensor optimization

procedure is as shown in Figure 6.4; the initial and final placement of sensors proposed by the

optimization algorithm is as shown in Figure 6.5. The sensors failed to move during the

optimization process with possible reasons being over-fitting of the classifier to the given data

set since we had close to 20% damage in this case. Also the use of multiple sensors in this

particular case may have accounted for the inability of the sensors to move due to its dependence

on the initial sensor locations with respect to the damage and level of noise.

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Figure 6.4 Displacement surface plot comparison between damaged and undamaged coupon

Figure 6.5 Initial and final placement of sensors after completion of optimization algorithm

(dots represent sensors)

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CHAPTER 7

CONCLUSIONS AND FUTURE WORK

7.1 Conclusion

With their enormous advantages in the manufacturing sector taken into consideration,

damage analysis and its comprehension in CFRP composites has become very critical as a way

to sustain its current and prospective applications, as well as its extension into other areas of

manufacturing. The search for a reliable structural health monitoring system with its added

economic advantage of enabling maintenance of engineering structures to be carried out based

on prevailing condition of a structure, rather than on estimated time has become paramount. This

has become necessary especially in large and expensive structures. This thesis therefore makes a

useful contribution to the detection and analysis of delamination in CFRP laminated composites

by analyzing stiffness degradation using four-point and three point bend test. Here, numerical

modeling was combined with an experimental study using a Lamb wave-based approach to

detect delamination in composite coupons. Damaged and undamaged test specimens were

fabricated using a VARTM process and subjected to four-point bend test to analyze delamination

onset and evolution. Numerical analysis of delaminated and un-delaminated composite coupons,

were also carried out using three point bending. Surface mounted PZT actuators and PZT sensors

were used for actuation of Lamb waves in the composite materials and in sensing the response of

the structure. The actuation parameters and the choice of transducers were made based on a

review of relevant literature. National Instruments LabVIEW software was used to synchronize

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the actuation initiation and response measurement. Embedded delamination using a surface

mounted PZT actuator and a surface mounted sensor was experimentally demonstrated.

Using the MTS QTest equipment, and with the pre-written program Testworks QT 2.03,

the four-point bend test experimental analysis was carried out. This analysis was supported by

finite element models developed using Abaqus version 6.11-1, commercial FEM software.

Numerical results obtained from finite element modeling for both cases of damaged and

undamaged specimens under four-point bend test produced insignificant difference in maximum

deflection due to absence of shear stresses at the delaminated section of the specimen. Further

numerical analysis was then carried out for both cases of damaged and undamaged specimen

using three-point bend test. The effect of shear stresses this time led to differences in maximum

deflection for the two cases. Time constraints however made it impossible to verify this

experimentally.

From the experimental results, it was found out that the A0 mode Lamb waves carried

sufficient information to detect an embedded delamination in a composite coupon. The

amplitude ratio of the incident wave for the undamaged coupon was found to be higher than the

damaged coupon due to the embedded delamination.

A detailed description of a damage detection system, results from finite element models of

four-point and three-point bend test for damaged and undamaged composite coupon, and a

review of the limitations and capabilities of anti-symmetric mode Lamb waves in embedded

delamination detection were discussed in this thesis. This information can serve as a good

reference for four- point and three-point bend tests modeling and help develop a reliable

structural health monitoring system for delamination.

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7.2 Suggestions for future work

The presence of stress concentration zones during the performance of four-point bend test

has a critical influence on the total accuracy of the experimental results. The loading rollers

introduce stress concentration under four-point loading. To mitigate this effect and enable more

accurate results to be obtained in future experiments, the rollers need to be lined with a soft

plastic or rubbery material or even the steel rollers would have to be replaced completely with

plastic ones altogether to avoid influencing damage on the compressive side of the specimen.

Strain gages could also be mounted underneath the mid-section of the specimen to give a more

accurate strain reading of the specimen. Experimental error can also be reduced by carrying out

effective calibration of the testing equipment. Also, three-point bend test for the damaged and

undamaged composite coupons could be carried out experimentally and results compared with

the exact and numerical solutions. This will help provide useful information on the behavior of

CFRP’s.

To efficiently classify the damage (delamination), the wavelength of actuation frequency

needs to be on the order of, or comparable to the damage length. Thus the actuation frequency

plays a very important role in generating the desired mode Lamb waves and also in deciding the

level of damage that can be detected. More careful selection of frequency must therefore be

carried out in future experiments.

The VARTM manufacturing process could also be improved by placing the resin/epoxy

mixture in a vacuum chamber to rid it of air bubbles before infusion into the fibers to ensure

improved fiber wet out, reduce void content to the barest minimum and obtain a more uniform

specimen width. Also more innovative ways to embed delamination in carbon/epoxy composite

laminates should also be explored to assist in obtaining the desired effect without damaging the

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material properties of the laminate. This thesis was focused primarily on detecting delamination,

which in this case was similar to a horizontal crack. Transverse crack damage, which is also

common in composite materials can also be investigated by similar fabrication process and SHM

system setup in future works.

Abaqus 11-1 software should be explored further to improve upon composite coupon

models, to give a more accurate representation of the surface irregularities of the coupons.

This thesis presented a case study showing the result of sensor placement optimization for a

composite coupon with embedded delamination. The percentage of damage and number of

sensors can be reduced and the same algorithm re-applied to check its effectiveness. Also, other

optimization algorithms such as the genetic algorithm can be explored to find out which will

produce the desired results in a case similar to what was undertaken in this thesis work. Tests

considered strain and displacement values as the feature vector set. The existing setup can be

extended to perform dynamic tests and extract frequency domain as well as time domain features

for damage classification and sensor placement optimization.

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REFERENCES

[1] R. Waugh, “Not just a load of hot air: Dream becomes reality as Boeing’s new carbon-fiber

787 Dreamliner heralds a new age of air travel,” 2011.

[2] H. Sohn, C. R. Farrar, F. M. Hemez, and J. J. Czarnecki, A Review of Structural Health

Monitoring Literature 1996-2001, 2002.

[3] P. K. Mallick, “Fiber Reinforced Composites: materials, manufacturing, and design,” Third

Edition

[4] http://www.substech.com/dokuwiki/doku.php?id=polymer_matrix_composites_introduction

[email protected]

[5] Z. R. Khokhar, Finite-element analysis of delamination in CFRP laminates: effect of material

randomness, Doctoral Thesis-Loughborough University. (April, 2010).

[6] Sung Kyu Ha, Kyo Kook Jin and Yuanchen Huang. Micro-Mechanics of Failure (MMF) for

Continuous Fiber Reinforced Composites, DOI: 10.1177/0021998308093911

Journal of Composite Materials 2008 42: 1873 originally published online 17 July 2008

[7] M. S. Sham Prasad, C.S. Venkatesh, T. Jayaraju. Experimental Methods of Determining

Fracture Toughness of Fiber Reinforced Polymer Composites under Various Loading

Conditions. Journal of Minerals & Materials Characterization & Engineering, Vol. 10, No.13,

pp.1263-1275, 2011.

[8] C. K. H. Dharan. (1978). Fracture mechanics of composite materials. Journal of engineering

materials and technology. 100: 223-247.

[9] K.Y. Chang, S. Liu, and F. K. Chang. Damage tolerance of laminated composites containing

an open hole and subjected to tensile loadings. Journal of Composite Materials, (1991), 25: pp.

274-301.

[10] L.R. Dharani and F.S. Ji, Effect of transverse cracking on stiffness reduction of cross-ply

laminates. Applied Composite Materials, (1995), 2(4): pp. 217-231.

[11] A.L. Highsmith and K.L. Reifsnider, Stiffness reduction mechanisms in composite

laminates ASTM digital library, (1982), 775: pp. 103-117.

Page 74: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

60

[12] Y. Qingda and B. Cox, Cohesive models for damage evolution in laminated composites.

International Journal of Fracture, (2005), 133(2): pp. 107-137.

[13] S. Ogiharaa and N. Takedab, Interaction between transverse cracks and delamination during

damage progress in CFRP cross-ply laminates. Composites Science and Technology, (1995),

54(4): pp. 395-404.

[14] K.W. Garrett and J.E. Bailey, Multiple transverse fracture in 90° cross-ply laminates of a

glass fibre-reinforced polyester. Journal Of Materials Science, (1977), 12(1): pp. 157-168.

[15] S.G. Lim and C.S. Hong, Prediction of transverse cracking and stiffness reduction in cross-

ply laminated composites. Journal of Composite Materials, (1989), 23(7): pp. 695-713.

[16] A. Parvizi, K.W. Garrett, and J.E. Bailey, Constrained cracking in glass fiber reinforced

Epoxy cross-ply laminates. Journal of Materials Science, (1978), 13(1): pp. 195-201.

[17] D. Flaggs, Prediction of tensile matrix failure in composite laminates. Journal of Composite

Materials, (1985), 19(1): pp. 29-50.

[18] S.C. Tan and R.J. Nuismer, A theory of progressive matrix cracking in composite laminates.

Journal of Composite Materials, (1989), 23(10): pp. 1029-1047.

[19] Z. Hashin, Analysis of cracked laminates: a variational approach. Journal of Mechanics of

Materials, (1985), 4: pp. 121-136.

[20] R. Talreja, Modeling of damage development in composites using internal variables

concepts. Damage Mechanics in Composites, ASME, (1987), 12.

[21] L. Boniface, P.A. Smith, M.G. Bader, and A.H. Rezaifard, Transverse Ply Cracking in

Cross-Ply CFRP Laminates--Initiation or Propagation Controlled? Journal of Composite

Materials, (1997), 31(11): pp. 1080-1112.

[22] P.A. Smith and S.L. Ogin, On transverse matrix cracking in cross-ply laminates loaded in

simple bending. Composites A, (1999), 30(8): pp. 1003-1008.

[23] Robert M. Jones, Mechanics of Composite Materials-second edition

[24] L.N. McCartney, Theory of stress transfer in a 0°-90°-0° cross-ply laminate containing a

parallel array of transverse cracks. Journal of the Mechanics and Physics of Solids, (1992),

40(1): pp. 27-68.

[25] A.A. Griffith, “The Phenomena of Rupture and Flow in Solids.” Philosophical

Transactions of the Royal Society London (1921), A(221): pp. 163-198.

Page 75: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

61

[26] T.E. Tay, G. Liu, V.B.C. Tan, X.S. Sun and D.C. Pham, Progressive Failure Analysis of

Composites, Journal of Composite Materials 2008 42: 1921 originally published online 17 July

2008, DOI: 10.1177/0021998308093912

[27] A.S.D. Wang, N.N. Kishore, and C.A. Li, Crack development in graphite-epoxy cross-ply

laminates under uniaxial tension. Composites Science and Technology, (1985), 24(1): pp. 1-31.

[28] G. Wimmer, C. Schuecker, H.E. Pettermann, Numerical simulation of delamination onset

and growth in laminated composites. Austrian Aeronautics Research (AAR) / Network for

Materials and Engineering (2006)

[29] V.Z. Parton, Fracture Mechanics-From theory to practice. Gordon and Breach Publisher,

Philadelphia, (1992).

[30] G. R. Irwin, Analysis of stresses and strains near the end of a crack traversing a plate.

Journal of Applied Mechanics, A.S.M.E., New York, (1957).

[31] Martin, R. H., Davidson, B.D. (1999). “Mode II fracture toughness evaluation using four

point bend, end notched flexure test.” Plast., Rubber Compos., 28(8) 401-406.

[32] Shuecker, C., and Davidson, B.D. (2000). “Evaluation of the accuracy of the four-point

bend end-notched flexure test for mode II delamination toughness determination.” Compos. Sci.

Technol., 60,2137-2146

[33] Vinciquerra, A. J., Davidson, D.B. (2004). “ Effect of crack length measurement technique

and data reduction procedures on the perceived toughness from four-point bend end-notched

flexure tests., J. Reinf. Plast. Compos., 23, 1051-1062.

[34] Yoshihara, H. (2004). “Mode II R-curve of wood measured by 4-ENF test.” Eng. Frac.

Mech., 71, 2065-2077.Yoshihara, H. (2008). “Theoretical analysis of 4-ENF test for mode II

fracturing in wood by finite element method.” Eng. Frac. Mech., 75, 290-296.

[35] de Morais, A. B., and de Moura, M.F.S.F. (2006). “Evaluation of initiation criteria used in

inter-laminar fracture tests.” Eng. Fract. Mech., 73, 2264-2276.

[36] Thouless, M.D. (2009). ‘’ The effects of transverse shear on the delamination of edge-notch

flexure and 3-point bend geometries.” Composites, Part B, 40, 305-312

[37] P. Qiao, P.E., F. ASCE; F. Chen, C. S. Hamey, and J. Wang. “Mixed-mode fracture of

hybrid material bonded interfaces under four-point bending.”

[38] Tan, S.C. and Nuismer, R.J. (1989). A Theory for Progressive Matrix Cracking in

Composite Laminates, Journal of Composite Materials, 23(10): 1029–1047.

Page 76: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

62

[39] Tan, S.C. and Perez, J. (1993). Progressive Failure of Laminated Composites with a Hole

under Compressive Loading, Journal of Reinforced Plastics and Composites, 12(10): 1043–

1057.

[40] Tan, S.C. (1991). A Progressive Failure Model for Composite Laminates Containing

Openings, Journal of Composite Materials, 25(5): 556–577.

[41] Barbero, E.J. and Lonetti, P. (2002). An Inelastic Damage Model for Fiber Reinforced

Laminates, Journal of Composite Materials, 36(8): 941–962.

[42] Xiao, Y. and Ishikawa, T. (2002). Bearing Failure in Bolted Composite Joints: Analytical

Tools Development, Advanced Composite Materials, 11(4): 375–391.

[43] Chen, J., Crisfield, M., Kinloch, A.J., Busso, E.P., Matthews, F.L. and Qiu, Y. (1999).

Predicting Progressive Delamination of Composite Material Specimens via Interface Elements,

Mechanics of Advanced Materials and Structures, 6(4): 301–317.

[44] McCarthy, C.T., McCarthy, M.A. and Lawlor, V.P. (2005). Progressive Damage Analysis

of Multi-Bolt Composite Joints with Variable Bolt-Hole Clearances, Composites Part B. 36(4):

290–305. 1962 T. E. TAY ET AL. Downloaded from jcm.sagepub.com at UNIV ALABAMA

LIBRARY/SERIALS on June 13, 2012

[45] Basu, S., Waas, A.M. and Ambur, D.R. (2007). Prediction of Progressive Failure in

Multidirectional Composite Laminated Panels, International Journal of Solids and Structures,

44(9): 2648–2676.

[46] Goswami, S. (2005). A Finite Element Investigation on Progressive Failure Analysis of

Composite Bolted Joints Under Thermal Environment, Journal of Reinforced Plastics and

Composites, 24(2): 161–171.

[47] Riccio, A. (2005). Effects of Geometrical and Material Features on Damage Onset and

Propagation in Single-lap Bolted Composite Joints under Tensile Load: Part II – Numerical

Studies, Journal of Composite Materials, 39(23): 2091–2112.

[48] McGregor, C.J., Vaziri, R., Poursartip, A. and Xiao, X. (2007). Simulation of Progressive

Damage Development in Braided Composite Tubes under Axial Compression, Composites Part

A: Applied Science and Manufacturing, 38(11): 2247–2259.

[49] Tao, J. and Sun, C.T. (1998). Influence of Ply Orientation on Delamination in Composite

Laminates, Journal of Composite Materials, 32(21): 1933–1947.

[50] Laurin, F., Carre` re, N. and Maire, J.F. (2007). A Multiscale Progressive Failure Approach

for Composite Laminates Based on Thermodynamical Viscoelastic and Damage Models,

Composites Part A: Applied Science and Manufacturing, 38(1): 198–209.

[51] Reddy, Y.S.N., Moorthy, C.M.D. and Reddy, J.N. (1995). Non-Linear Progressive Failure

Page 77: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

63

Analysis of Laminated Composite Plates, International Journal of Non-Linear Mechanics, 30(5):

629–649.

[52] Pal, P. and Ray, C. (2002). Progressive Failure Analysis of Laminated Composite Plates by

Finite Element Method, Journal of Reinforced Plastics and Composites, 21(16): 1505–1513.

[53] Xiao, Y. and Ishikawa, T. (2002). Bearing Failure in Bolted Composite Joints: Analytical

Tools Development, Advanced Composite Materials, 11(4): 375–391.

[54] Basu, S., Waas, A.M. and Ambur, D.R. (2007). Prediction of Progressive Failure in

Multidirectional Composite Laminated Panels, International Journal of Solids and Structures,

44(9): 2648–2676.

[55] Kweon, J.H., Shin, S.Y. and Choi, J.H. (2007). A Two-Dimensional Progressive Failure

Analysis of Pinned Joints in Unidirectional-Fabric Laminated Composites, Journal of Composite

Materials, 41(17): 2083–2104.

[56] Wolford, G.F. and Hyer, M.W. (2005). Failure Initiation and Progression in Internally-

Pressurized Elliptical Composite Cylinders, Mechanics of Advanced Materials and Structures,

12(6): 437–455.

[57] Reddy, Y.S. and Reddy, J.N. (1993). Three-Dimensional Finite Element Progressive Failure

Analysis of Composite Laminates under Axial Extension, Journal of Composites Technology

and Research, 15(2): 73–87.

[58] Robbins, D.H., Reddy, J.N. and Rostam-Abadi, F. (2005). Layerwise Modeling of

Progressive Damage in Fiber-Reinforced Composite Laminates, International Journal of

Mechanics and Materials in Design, 2(3): 19–36.

[59] Dugdale, D.S., Yielding of steel sheets containing slits. Journal of the Mechanics and

Physics of Solids 8, 100-104. 1960.

[60] Barenblatt, G., The mathematical theory of equilibrium cracks in brittle fracture. Advances

in Applied Mechanics, 7, 55-129. 1962.

[61] Hillerborg, A., Modeer, M., Petersson, P.E., Analysis of crack formation and crack growth

in concrete by means of fracture mechanics and finite elements Cement and Concrete Research.

6, 773-782. 1976.)

[62] Krueger, R., The virtual crack closure technique: history, approach and applications.

NASA/Contractor Report-2002-211628, 2002.

[63] Turon, A., Camanho, P.P., Costa, J. Davila, C.G., An interface damage model for the

simulation of delamination under variable-mode ratio in composite materials. NASA/Technical

Memorandum 213277, 2004.

Page 78: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

64

[64] Turon, A., Camanho, P.P., Costa, J. Davila, C.G., A damage model for the simulation of

delamination in advanced composites under variable-mode loading. Mechanics of Materials,

submitted, 2005.

[65] Jitendra S. Tate, Adekunle T. Akinola, and Dmitri Kabakov, “Bio-based Nanocomposites:

An Alternative to Traditional Composites,” The Journal of Technology Studies, vol. 35 No. 1,

fall 2009.

[66] X. Song, “Vacuum assisted resin transfer molding (VARTM): Model development and

verification.” Ph.D. 3147766, Virginia Polytechnic Institute and State University,

United States – Virginia, 2003.

[67] X. Sun, S. Li, and L. J. Lee, “Mold filling analysis in vacuum-assisted resin transfer

molding. Part I: SCRIMP based on a high-permeable medium,” Polymer Composites, vol. 19,

pp. 807-817, 1998.

[68] R. Chen, C. Dong, Z. Liang, C. Zhang, and B. Wang, “Flow modeling and simulation for

vacuum assisted resin transfer molding process with the equivalent permeability method,”

Polymer Composites, vol. 25, pp. 146-164,2004.

[69] R. Waugh, “Not just a load of hot air: Dream becomes reality as Boeing’s new carbon-fiber

787 Dreamliner heralds a new age of air travel,” 2011.

[70] W. J. Stsaszewski, S. Mahzan, and R. Traynor, “Health monitoring of aerospace composite

structures – Active and passive approach,” Composites Science and Technology, vol. 69, pp.

1678-1685, 2009.

[71] S. S. Kessler and S. M. Spearing, “Design of a piezoelectric-based structural health

monitoring system for damage detection in composite materials,” in Smart Structures and

Materials 2002: Smart Structures and Integrated Systems, 18-21 March 2002, USA, 2002, PP.

86-96.

[72] A. K. Mal, S. Banerjee, and F. Ricci, “Automated structural health monitoring system using

acoustic emission and modal data,” in Health Monitoring and Smart Nondestructive Evaluation

of Structural and Biological Systems III, March 15, 2004 – March 17, 2004, San Diego, CA,

United states, 2004, pp. 1-10.

[73] M. A. Maseras-Gutierrez, W. J. Staszewski, M. S. Found, and K. Worden, “Detection of

impacts in composite materials using piezoceramic sensors and neural networks,” in Smart

Structures and Materials 1998: Smart Structures and Integrated Systems, February 3, 1998 –

February 3, 1998, San Diego, CA, United states, 1998, pp. 491-497.

[74] D. C. Worlton, “Experimental confirmation of lamb waves at megacycle frequencies,”

Journal of Applied Physics, vol. 32, pp. 967-971, 1961.

Page 79: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

65

[75] R. Jha, I. Kim, and D. Widana-Gamage, “Investigation of Incident Lamb Wave Parameters

on Detection of Composite Delamination,” ASME Conference Proceedings, vol. 2010, pp. 675-

683, 2010.

[76] K. Diamanti, J. M. Hodgkinson, and C. Soutis, “Detection of Low-velocity Impact Damage

in Composite Plates using Lamb Waves,” Structural Health Monitoring, Vol. 3, pp. 33-41, 2004.

[77] A. J Croxford, P. D. Wilcox, B. W. Drinkwater, and G. Konstantinidis, “Strategies for

guided-wave structural health monitoring,” Proceedings of the Royal Society A: Mathematical,

Physical and Engineering Science, vol. 463, pp. 2961-2981, 2007.

[78] A. Raghavan and C. E. S. Cesnik, “Review of guided-wave structural health monitoring,”

Shock and Vibration Digest, vol. 39, pp. 91-114, 2007.

[79] V. Giurgiutiu, “Lamb Wave Generation with Piezoelectric Wafer Active Sensors for

Structural Health Monitoring,” in Smart Structures and Materials 2003: Smart Structures and

Integrated Systems, March 3, 2003 – March 6, 2003, San Diego, CA, United states, 2003, pp.

111-122.

[80] J. R. Wait, G. Park, H. Sohn, and C. R. Farrar, “Plate damage identification using wave

propagation and impedance methods,” in Health Monitoring and Smart Nondestructive

Evaluation of Structural and Biological Systems III, March 15, 2004 – March 17, 2004, San

Diego, CA, United states, 2004, pp. 53-65.

[81] A. B. Thien, “Pipeline structural health monitoring using macro-fiber composite active

sensors,” University of Cincinnati, 2006

[82] S. Soni, S. Das, and A. Chattopadhyay, “Simulation of damage-features in a lug joint using

guided waves,” Journal of Intelligent Materials Systems and Structures, vol. 20, pp. 1451-64,

2009.

[83] K. Diamanti and C. Soutis, “Structural health monitoring techniques for aircraft composite

structures,” Progress in Aerospace Science, vol. 46, pp. 342-352, 2010.

[84] H. Gao and J. L. Rose, “Ultrasonic sensor placement optimization in structural health

monitoring using evolutionary strategy” in American Institute of Physics, 2006.

[85] W. Huyer and A. Neumaier, “SNOBFIT – Stable noisy optimization by branch and fit,”

ACM Transactions on Mathematical Software, vol. 35, 2008.

[86] R. F. Guratzsch, S. Mahadevan, C. L. Pettit, and M. M. Derriso, “Sensor placement

optimization for shm systems under uncertainty,” 46th

AIAA/ASME/ASCE/AHS/ASC Structures,

Structural Dynamics and Materials Conference, April 18, 2005 – April 21, 2005, Austin, TX,

United states, 2005, pp. 5182-5188.

[87] “NASA technical report,” The University of Alabama, 2012.

Page 80: MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ...acumen.lib.ua.edu/u0015/0000001/0001262/u0015_0000001_0001262.pdf · MODELING OF DELAMINATION IN CARBON/EPOXY COMPOSITE ... ASTM

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APPENDIX A: LabVIEW program

LabVIEW program developed by my project colleague A. Nagabhushana, and used to write

arbitrary waveform generator, to generate Hanning waveform input.

LabVIEW program developed to read from DAQ