monday, march 25, 2019...vt lab registration #vt11301 this laboratory is in compliance with the...

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CC70132 - CC70142 Monday, March 25, 2019 Sample ID#s: Attn: Kevin McCarthy Tighe & Bond 213 Court St, Suite 1100 Middletown, CT 06457 SDG ID: GCC70132 Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL Sincerely yours, Laboratory Director Phyllis Shiller If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. NELAC - #NY11301 CT Lab Registration #PH-0618 MA Lab Registration #M-CT007 ME Lab Registration #CT-007 NH Lab Registration #213693-A,B NJ Lab Registration #CT-003 NY Lab Registration #11301 PA Lab Registration #68-03530 RI Lab Registration #63 UT Lab Registration #CT00007 VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. This report is incomplete unless all pages indicated in the pagination at the bottom of the page are included. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original. 587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040 Telephone (860) 645-1102 Fax (860) 645-0823 Page 1 of 29

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Page 1: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

CC70132 - CC70142

Monday, March 25, 2019

Sample ID#s:

Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

SDG ID: GCC70132Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #M-CT007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63UT Lab Registration #CT00007VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. This report is incomplete unless all pages indicated in the pagination at the bottom of the page are included.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

Page 1 of 29

Page 2: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Id Cross ReferenceMarch 25, 2019

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GCC70132

Client Id Lab Id Matrix

Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

0315BS-01 CC70132 BULK0315BS-02 CC70133 BULK0315BS-03 CC70134 BULK0315BS-04 CC70135 BULK0315BS-05 CC70136 BULK0315BS-06 CC70137 BULK0315BS-07 CC70138 BULK0315BS-08 CC70139 BULK0315BS-09 CC70140 BULK0315BS-10 CC70141 BULK0315BS-11 CC70142 BULK

Page 2 of 29

Page 3: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-01

Phoenix ID: CC70132

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1221 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1232 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1242 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1248 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1254 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1260 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1262 490 03/20/19 SC SW8082Aug/Kg 2NDPCB-1268 490 03/20/19 SC SW8082Aug/Kg 2

QA/QC Surrogates56% DCBP 03/20/19 SC 30 - 150 %% 262% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 245% TCMX 03/20/19 SC 30 - 150 %% 265% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 2

Ver 1

Page 3 of 29

Page 4: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-01Phoenix I.D.: CC70132

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 4 of 29

Page 5: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-02

Phoenix ID: CC70133

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1221 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1232 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1242 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1248 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1254 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1260 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1262 430 03/20/19 SC SW8082Aug/Kg 2NDPCB-1268 430 03/20/19 SC SW8082Aug/Kg 2

QA/QC Surrogates45% DCBP 03/20/19 SC 30 - 150 %% 255% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 249% TCMX 03/20/19 SC 30 - 150 %% 255% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 2

Ver 1

Page 5 of 29

Page 6: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-02Phoenix I.D.: CC70133

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 6 of 29

Page 7: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-03

Phoenix ID: CC70134

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1221 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1232 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1242 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1248 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1254 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1260 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1262 650 03/20/19 SC SW8082Aug/Kg 2NDPCB-1268 650 03/20/19 SC SW8082Aug/Kg 2

QA/QC Surrogates43% DCBP 03/20/19 SC 30 - 150 %% 255% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 247% TCMX 03/20/19 SC 30 - 150 %% 253% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 2

Ver 1

Page 7 of 29

Page 8: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-03Phoenix I.D.: CC70134

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 8 of 29

Page 9: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-04

Phoenix ID: CC70135

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1221 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1232 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1242 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1248 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1254 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1260 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1262 790 03/20/19 SC SW8082Aug/Kg 5NDPCB-1268 790 03/20/19 SC SW8082Aug/Kg 5

QA/QC Surrogates88% DCBP 03/20/19 SC 30 - 150 %% 584% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 578% TCMX 03/20/19 SC 30 - 150 %% 575% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 5

Ver 1

Page 9 of 29

Page 10: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-04Phoenix I.D.: CC70135

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 10 of 29

Page 11: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-05

Phoenix ID: CC70136

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1221 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1232 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1242 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1248 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1254 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1260 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1262 620 03/20/19 SC SW8082Aug/Kg 2NDPCB-1268 620 03/20/19 SC SW8082Aug/Kg 2

QA/QC Surrogates61% DCBP 03/20/19 SC 30 - 150 %% 264% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 244% TCMX 03/20/19 SC 30 - 150 %% 264% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 2

Ver 1

Page 11 of 29

Page 12: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-05Phoenix I.D.: CC70136

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 12 of 29

Page 13: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-06

Phoenix ID: CC70137

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1221 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1232 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1242 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1248 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1254 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1260 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1262 410 03/20/19 SC SW8082Aug/Kg 1NDPCB-1268 410 03/20/19 SC SW8082Aug/Kg 1

QA/QC Surrogates43% DCBP 03/20/19 SC 30 - 150 %% 148% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 130% TCMX 03/20/19 SC 30 - 150 %% 145% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 1

Ver 1

Page 13 of 29

Page 14: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-06Phoenix I.D.: CC70137

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 14 of 29

Page 15: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-07

Phoenix ID: CC70138

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1221 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1232 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1242 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1248 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1254 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1260 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1262 800 03/20/19 SC SW8082Aug/Kg 5NDPCB-1268 800 03/20/19 SC SW8082Aug/Kg 5

QA/QC Surrogates86% DCBP 03/20/19 SC 30 - 150 %% 587% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 563% TCMX 03/20/19 SC 30 - 150 %% 563% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 5

Ver 1

Page 15 of 29

Page 16: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-07Phoenix I.D.: CC70138

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 16 of 29

Page 17: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-08

Phoenix ID: CC70139

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1221 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1232 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1242 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1248 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1254 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1260 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1262 780 03/20/19 SC SW8082Aug/Kg 5NDPCB-1268 780 03/20/19 SC SW8082Aug/Kg 5

QA/QC Surrogates76% DCBP 03/20/19 SC 30 - 150 %% 573% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 564% TCMX 03/20/19 SC 30 - 150 %% 559% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 5

Ver 1

Page 17 of 29

Page 18: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-08Phoenix I.D.: CC70139

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

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Page 19: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-09

Phoenix ID: CC70140

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/20/19 XX/ML SW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1221 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1232 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1242 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1248 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1254 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1260 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1262 750 03/21/19 SC SW8082Aug/Kg 5NDPCB-1268 750 03/21/19 SC SW8082Aug/Kg 5

QA/QC Surrogates88% DCBP 03/21/19 SC 30 - 150 %% 587% DCBP (Confirmation) 03/21/19 SC 30 - 150 %% 573% TCMX 03/21/19 SC 30 - 150 %% 576% TCMX (Confirmation) 03/21/19 SC 30 - 150 %% 5

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Page 19 of 29

Page 20: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-09Phoenix I.D.: CC70140

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 20 of 29

Page 21: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-10

Phoenix ID: CC70141

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1221 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1232 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1242 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1248 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1254 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1260 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1262 330 03/20/19 SC SW8082Aug/Kg 2NDPCB-1268 330 03/20/19 SC SW8082Aug/Kg 2

QA/QC Surrogates35% DCBP 03/20/19 SC 30 - 150 %% 233% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 240% TCMX 03/20/19 SC 30 - 150 %% 253% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 2

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Page 22: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-10Phoenix I.D.: CC70141

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

Page 22 of 29

Page 23: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

BULKTIGHEStandard28-2087-0331

03/15/19SWsee "By" below

BS/BH

Laboratory Data

0315BS-11

Phoenix ID: CC70142

03/19/19 10:56

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Kevin McCarthyTighe & Bond213 Court St, Suite 1100Middletown, CT 06457

Analysis ReportMarch 25, 2019

Date Time

SDG ID: GCC70132

Client ID:Project ID: SMTF-ROXBURY ELEMENTARY SCHOOL

Dilution

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

CompletedCaulk Extraction for PCB 03/19/19 XX/AK/MLSW3540C

PCB (Soxhlet SW3540C)NDPCB-1016 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1221 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1232 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1242 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1248 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1254 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1260 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1262 730 03/20/19 SC SW8082Aug/Kg 5NDPCB-1268 730 03/20/19 SC SW8082Aug/Kg 5

QA/QC Surrogates85% DCBP 03/20/19 SC 30 - 150 %% 584% DCBP (Confirmation) 03/20/19 SC 30 - 150 %% 563% TCMX 03/20/19 SC 30 - 150 %% 562% TCMX (Confirmation) 03/20/19 SC 30 - 150 %% 5

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Page 24: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

0315BS-11Phoenix I.D.: CC70142

Client ID:SMTF-ROXBURY ELEMENTARY SCHOOLProject ID:

Parameter ResultRL/PQL Units Date/Time By ReferenceDilution

Comments:

Results are reported on an ``as received`` basis, and are not corrected for dry weight.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMarch 25, 2019

If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent.

Reviewed and Released by: Rashmi Makol, Project Manager

RL/PQL=Reporting/Practical Quantitation Level ND=Not Detected BRL=Below Reporting LevelQA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds.

Ver 1

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Page 25: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

QA/QC Data

Parameter BlkBlank RL

MS%

MSD%

MSRPD

QA/QC ReportMarch 25, 2019

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GCC70132

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 471010 (ug/Kg), QC Sample No: CC69179 10X (CC70140)

Polychlorinated Biphenyls - BulkPCB-1016 ND 90 99 9.5 40 - 140 30170

PCB-1221 ND 40 - 140 30170

PCB-1232 ND 40 - 140 30170

PCB-1242 ND 40 - 140 30170

PCB-1248 ND 40 - 140 30170

PCB-1254 ND 40 - 140 30170

PCB-1260 ND 99 107 7.8 40 - 140 30170

PCB-1262 ND 40 - 140 30170

PCB-1268 ND 40 - 140 30170

% DCBP (Surrogate Rec) 95 102 105 2.9 30 - 150 30%

% DCBP (Surrogate Rec) (Confirm 109 111 97 13.5 30 - 150 30%

% TCMX (Surrogate Rec) 86 96 91 5.3 30 - 150 30%

% TCMX (Surrogate Rec) (Confirm 88 100 96 4.1 30 - 150 30%

A LCS and LCS Duplicate were performed instead of a matrix spike and matrix spike duplicate.

Comment:

QA/QC Batch 470837 (ug/Kg), QC Sample No: CC69919 10X (CC70132, CC70133, CC70134, CC70135, CC70136, CC70137, CC70138, CC70139, CC70141, CC70142)

Polychlorinated Biphenyls - BulkPCB-1016 ND 84 79 6.1 40 - 140 30170

PCB-1221 ND 40 - 140 30170

PCB-1232 ND 40 - 140 30170

PCB-1242 ND 40 - 140 30170

PCB-1248 ND 40 - 140 30170

PCB-1254 ND 40 - 140 30170

PCB-1260 ND 94 97 3.1 40 - 140 30170

PCB-1262 ND 40 - 140 30170

PCB-1268 ND 40 - 140 30170

% DCBP (Surrogate Rec) 101 101 106 4.8 30 - 150 30%

% DCBP (Surrogate Rec) (Confirm 102 95 106 10.9 30 - 150 30%

% TCMX (Surrogate Rec) 95 93 86 7.8 30 - 150 30%

% TCMX (Surrogate Rec) (Confirm 86 85 83 2.4 30 - 150 30%

A LCS and LCS Duplicate were performed instead of a matrix spike and matrix spike duplicate.

Comment:

Page 25 of 29

Page 26: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

QA/QC Data

Parameter BlkBlank RL

MS%

MSD%

MSRPD

SDG I.D.: GCC70132

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 25, 2019MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 26 of 29

Page 27: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Sample Criteria Exceedances ReportMonday, March 25, 2019

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GCC70132 - TIGHECriteria: None

RLCriteria

State: CT

#Error*** No Data to Display ***

Phoenix Laboratories does not assume responsibility for the data contained in this exceedance report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

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Page 28: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

Analysis CommentsMarch 25, 2019

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GCC70132

The following analysis comments are made regarding exceptions to criteria not already noted in the Analysis Report or QA/QC Report:

PCB NarrationCC70133, CC70134AU-ECD5 03/20/19-1:

The following Continuing Calibration compounds did not meet % deviation criteria: Samples: CC70133, CC70134 Preceding CC 320B027 - DCBP SURR 17%L (15%) Succeeding CC 320B040 - None.

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Page 29: Monday, March 25, 2019...VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results

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