mr tom wallace, office of environmental elllorcement, … · mr tom wallace, office of...

Mr Tom Wallace, Office of Environmental Elllorcement, Envircmmmtal Pro t cction A gcnc y,

Inniscarra, Co. Cork

R~giol~aX Inspectorate,

Yol"1.rs sincerely,

ENCL: Air monitoring F C S I I I ~ ~ S for Novcmhcr 2018.

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTL1131118 / 2018700 Visit No; 11 Year: 2018 Office: Trim

EPA licence No.: WLOO41-01 licence Holder: Envn Shannon, X2

Facility location: Smithstown Facility Rev.No: 1

Report Titlo

Company addross

Air Emissions Compliance Monitoring Emission$ Rapori Air Scientific Ltd., 32 DeGranville Court, Dublin road,

Trim, Co. Meath

Smithstown Facility

Contact Porson Thomas Kelleher w L004.I-01

Enva 5hannon. X2

13/11/2018 Stack Reforonce Number x2

Uater of h e Monitoring Campaign Job Refermm Numbor

Report Approve0 by

---- ENSHTL11311X8 / 20lX700

Verstan I I

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EPA Export 20-03-2019:03:51:01

Document No . . ENTHTLI131118 / 201.8700 Visit No: 11 Year: 2018 Office: Trim

EPA IICEIXX NO . . WLO04l-tTl Licance Ilolder: Enva Shannon. X 2

Facility Locallon; Smithstown Facllity Rev.No: 3.

Gonteaats 1 . Executive 5u mmary ............................................................................................................................

I . Monitoring Objectives ....................................................................................................................... Overall Aim of the monitoring Campaign ....................................................................................... Special Requirements ........................................................................................................................ Target Parameters .............................................................................................................................. Emissiun Limit Values ........................................................................................................................ Reference Conditions ........................................................................................................................ O v m H Results .................................................................................................................................... Accreditation details .......................................................................................................................... Monitoring Dates & Times ................................................................................................................ Monitoring, Equipment & Analytical Melt i~ds ............................................................................... Sampling Devtations ........................................................................................................................... Reference Documents ........................................................................................................................ Suitability of sampling location ......................................................................................................... Process details ..................................................................................................................................... Stack diagram ......................................................................................................................................

2 . APPENDttES ......................................................................................................................................... II . Appendix 1 - Monltorlng Personnd & Equipment ........................................................................

Stack hmissions Monitoring Personnel ............................................................................................ I I I . Appendix I t -Stack Details &flow charmerlstlcs ........................................................................

Preliminary stark survey calculations .............................................................................................. IV . Appendix I t i .. Individual parameter sampling details and rerulcs .............................................

Oxides of Nitrogen Quality Assurance ............................................................................................ Oxldes of Nitrogen Results & Sampling detaits ............................................................................. Oxides of Nitrogen Trend .................................................................................................................. Oxides of Nitrogen Measurement Uncertainty ............................................................................. Hydrogen Chloride Sampting Details & Results .............................................................................. Hydrogen t h loride Quality A w ra ncc ............................................................................................. Hydrogen Chloride Results & Measurement Uncertainty ............................................................ Sulphur Dioxide Qudity Assurance ................................................................................................. Sulphur Dioxide Sampling Details & Results .................................................................................. Sulphur Dioxide Trend ....................................................................................................................... Sulphur Dioxide Results & Measurement Uncertajnty ................................................................. 'I A Luft Organics ................................................................................................................................. Ammonia Sampling Dalalls & Results ........................................................................................... Ammonia Quality Assurance .......................................................................................................... Ammonia Results & Measurement. Uncertainty .........................................................................

3 3 3 3 3 4 4 5 6 7 13 9 11 1. 3. 12 13 14 14 14 IS 15 23 23 24 2% 30 32 33 40 41 42 48 56 58 60 Elf 62

Page 2 of40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTL2131118 / 2018700 Visit No: If Year: 2018 Office: Trim

EPA L ~ C W I C ~ NO.: WLOO63.1-01 licence Holder: Enva Shannon, X 2

Facility Locatlan: Smithstown Facility Rev.Na: 1

1. Executiva Summary

Overall Aim of the monitoring Campaign Tha aim gf th@ mor$[orlng campaign was to deinbrritrate compliance with a set of emission limit values as specified in tho Situ Ilcence.

There wwa no spacial ruquironrenk. Spet;ial Requirements

Target Pa 1-8 meto m

Oxitkb: 01 Nitrogen (PIOX) as NO2

Hydrogen Chloride (MCL)

T A Lurt organics Sulphur Dioxide (Sod

Stack Gas T@mpra\uro

Ammonia (NH3)

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTL1131~18 / 2018700 Visit No: XI Year: 2018 Office: Trim

Emission Limit Values

EPA Licence NO.: WLOO41-01 Licence Haider: Enva Shannon, X2

Facility lOC3tion: Smithstown facility Rev.No: 1.

Emlssloir Limit Valuos I Mars Ernlsslons Llrnft Values; t ms.rn" I ko,h-' I

Reference Conditions

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EPA Export 20-03-2019:03:51:01

Document No.: ENSMT1113llb8 / 2018700 Visit No: 11 Year: 2018 Office: Trim

EVA Licence No.: WL0041-01 licence Holder: ERW Shannon, X2

Facility Location: Smithstown Facility Rev.No: 1,

Page G of 41)

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EPA Export 20-03-2019:03:51:01

Clxaoutlve Sumniny

Monlkaxing, Equipment & A n s l y t h l Methpdrr l_____l. . . . . . . . . . _...................... . . . .

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EPA Export 20-03-2019:03:51:01

Lfst bf Equtprnmt

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTLl131118 / 2018700 Visit No: 11 Year: 2013 Office: Prim

EPA Licence No.: WLOO41-01 licence Holder: Enva Shannon, X2

Facility Location: Smithstawn Facility Rev.No: 1

Sampling Deviations

-+ , , ... , , , , . , , , . . . , , , , , , , ..,. , , ~ . ,, . , . , .. ,. , , . , . , , ,

Standard ID Mt.13 - Tho absorber sffiriclency of the fir$! absorber must be betier than 95% I ( EN 34791: 2009 section 2) ----

Page 9 of 40

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EPA Export 20-03-2019:03:51:01

Oucummt No.: ENSHTI.11.3I,3.28 / 2018700 Visit No: 11 Year: 203.8 DfFice: Trim

EPA licenca No.: WLI)D41-01 Licence Holder: Enva Shannon, X2

Facility location: Smithstown Facility Rev,No: I

VdUO Cornrnenf Irish EPATaclinical Oirldancts Noto A01 I ES EN 16259 Platform

I Safe Access Available I Yes I I

Pracars details

Process Air

Abatement Systems Runnhg Status Normal Fuol NIA

e NQW

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTtlI31118 1 21118700 Visit No: 11 Year; 2Q18 Office: Trim

EPA licence No.: Wt0041-01 Llctnce Holder; Enva Sharrnon, X2

Facility location: Smithstown Facility Rev,No: 1

Signature 1

Page I1 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTL1131113 / 2018700 Visit; No: 11 Year: 2018 Office; Trim

Exacutlue Summary

Stack diagram

EPA Licence No.: WLOO41-01 I,icencs Mddrr : Enva Shannon, X2

Facility location: Smithstown Facility Rev,No: 1

Page 12 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSIJTL1131118 / 2018700 Vtslt No: 11. Year: 2018 OFfice; Trim

EPA Licence No.: WFLI041-01 Licence Holder; Enva Shannon, X 2

Facility Location: Smithstown Facility Rev.No: 1

2. APPENDICES

Stack Emissions Monitoring Pamsnnol

Qualifications PhD. (Eng.), MSC. (Agr.), B. A y . Sc.

Page 13 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHT1.12311,38 / 2018700 Visit No: 11 Year: 2QJ8 Office: Trim

EPA t.lcence No.: W10041-01 Licence Holder: Enva $hanilon, X2

Facility Location: Smithstawn Facility Rev.No: f

Pre!iminary stat;k survey calculations

Gsnraral Stack D ~ t a l l s -- Suck details Units Vatu€! Date of survey 1Y1 f1.2018 -- 'I'itne of survey 1320

I- -- I

Type Circular

Stack Dlamstor I Depth. D

I StdCk Widlh. w I m I I Average Stack Gas Temp., Ta C 8 i ,, , , , , , , ,

Average Stalk Prassura. P static kPa 0. t -- I

kPa I 100.8

lnltial Pitot teak Check

t Number of Lines Used t I 1 I

Page 14 of 40

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EPA Export 20-03-2019:03:51:01

Dwrurtiet>t No.; ENSHTtli3lli8 / 2018700 visit. NO: 51. Year: 2038 Office; Trlm

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ot 40

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EPA Export 20-03-2019:03:51:01

FPA LiCellCCI NO.; WLOO41-01 Lkencs: tlnldsr: Lnva Sharriian, x7

Facility Locatian: Smithstown Facitity Rev.Na: 1

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EPA Export 20-03-2019:03:51:01

EPA Licence No.: Wt004.1-01 Licente Holder; Enva Shannon, X2

fixllity location: smithtorn Facliity R ~ v . N Q : 1

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTl113Il lX / X118700 Visit No: 11 Year: 2m.8 Office: Trim

EPA Licence NO.: Wt11041-01. Licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev.lVo: 1

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTI.11.31118 / 2013700 Visit No: 11 Year; 2018 Office: Trim

EPA Licence No.: WLOO41-01 Licence Holder: Enva Shannon, X2

Facility location: Smithstown Facility Rev.Ne: 3.

OxlrJes of Mltmgon Quality Assurance

Unita Run $ Run 2 Run 3 --

Page 22 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTL1131118 / 20187UO EPA Licence No.: WLOO41-01 Visit No: 11 Licence Holder: Enva Shannon, X2 Year; 2018 Facility location: Smithstown Facility Office: Trim Rt?v.FJo: 1

Oxldos of Nitrogen Results & Sampllng D~tzrlls;

Span Gas Starl Prassurs (bar)

160.7 I . . . . . -.

Span Gas Wncartajnty (96) <2 -...,,..., , , , , , , . . . , , . , , . . . , , , , ~~

Nitrogen

1 Refererlce Canclltiona I . . . - . - .. - Temperature (K) 273.15

101.3

Drv

-- P

I. ~~

NO Oxygen Ref

Page 23 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHIL1131118 / 2O187W Visit No; 11 Y f w : 2018 C)ffics: Trim

Run 1

8 a.

I Time

Paee 24 of 40

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EPA Export 20-03-2019:03:51:01

Document No.: ENSI..1TL113111& / 2018700 Visit No: 11 Year: 2018 Office: Trim

EPA Licence No.: WLOO41-03. Licence Holder: Enva Shannon, X2


Oxides of Nitrogen Measurement Uncertainty

-

Nonlinearity % 1.4

Temperature Dependant Zero drlff % -0.04

Tompcralurs Dependent Span drill % -0.25

--- -

Cross-sensif ivlty -.,..., , , , , , , , , , , , , , , , , , , , ..,,,.,,.,- -

Leak % 0 r 2

--....., , , , , , , , , , , , , , ~~

....................._...._....._....__.._...___.._.....,,... . .

Page 25 of 40

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EPA Export 20-03-2019:03:51:01

Document NO.: EMSHTL1131118 / 20187QO Visit No: 12 Year: 2018 Office: Trim

€PA licence No.: WLOt)41-01 l icence Holder: Enva Shannon, X2


Hydrogm Chloride Sampling Datrlls & ResuIts

llrnln

m i r t

Average sample Volume; llmin

- -

1 Sample TW -rims: I 30 I nlln I

Page 26 of 4.0

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EPA Export 20-03-2019:03:51:01

Document No.: EN5HTL1131118 / 2018700 Visit No: 11 Year: 2018 Office: Trim

EPA Licence No.: W1~0042-OJ licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev.No: 3.

Hydrogen Chiorid@ Quality Assurance

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EPA Export 20-03-2019:03:51:01

Document No.: ENSHTLll31118 / 2018700 visit No: 1 , l Year: 2018 Office; Trim

EPA Lic~nct; NO.: W10041-I31 Liceoce Holder: Enva Shannon, X2

Facility location: Smithstown Facllity Rev.No: 1

Hydrogen Chloride Results & Measrxrwtiwnt Uncartalnty

. . . . . . . . . . . . . . . . . . . . . . . . . Flrrlsh T h e

Results

lmpinger final Volume

Concentretion

Sample Volume

Page 28 of 40

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EPA Export 20-03-2019:03:51:02

CIocurncnt No.: ENS1.ITLl131118 / 2018700 Visit No: 11 Year; 2018 Office: Trim

EPA Licence No,; WL0041-01 Licence Holder: Enva Shannon, X2


Sulphur CIIoxide Quality Assurance

Span Gas Value

140

148 ...... - Span Uown Sampling Line (Post)

Span Drift PPT,, , ,, ,, , , , 2 ______I,.,..... , , , , ,, ,,,.,,.. , , ~ ~

Atrowahla Span Drift

Span Gas Eonc.

Racordad Cone. down Line

Page 29 of 40

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EPA Export 20-03-2019:03:51:02

Document No.: ENSMTtll31213 / 201870U Visit No: 11 Yaar: 2018 Office: Yrim

EPA Licence MO.; WL0041-0l l.icence Molder: Enva Shannon, XZ

Facility Location: Smithstowti Facility [email protected]: J

Sulphur DioxSdo Results & Sampling Details

Standard Technical Procedure SQP2012 ' -

Fiche material

Heated l h a d Fillnr U3sd

Gas Cylinder Coneenlratiorr (ppni)

Number of SamplinQ tines Used Number of Sampllng Points Used

1

1

Reference Condltians

Page 30 of 40

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EPA Export 20-03-2019:03:51:02

i

'1.2

1

b,a 0.e

0.4

0.2

0 -0.2

-0.4

4.0

4 . B -1

Page 31 uf 40

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of 40

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EPA Export 20-03-2019:03:51:02

Dacurrierrt No.: ENSHTL1131118 / 2018700 Visit No: 11 Year: 2018 Offlca: Trim

EPA licence No.: WL0041-01 Licence Holder; Enva Shannon, X2


Sulphur Dioxide Measurement Uncertainty

Measured Quantities Unlts

I I

Page 33 of 40

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EPA Export 20-03-2019:03:51:02

Docurnant No.: ENSMTlll31218 / 2111871)O Visit NO: 11 Year: 2018 Office: Trim

T A Luft Organics

EPA Licence No.: W10041-Ul Licence Holder: Enva Shannon, X2


Title:

Mothad: Client: Enva Shannon

John Casoy

Test Date; 1311 1EOT8

Laboratory Usod:

IPumn Number; I I I ASLTMI 8EQ509

Actual Sarn~la Volumo:

ITube Tvae; I 226.09 I I Tuba Idantification Number: --

Page 34 of 40

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EPA Export 20-03-2019:03:51:02

Document No.: ENSHTLl131118 / 2018700 Visit No: II. Year: 2018 Office; Trim

EPA licence No,: WFOO41-01 Licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev.Mo: 1

% of value

Expanded uncertainty

EXpanUed rrncahinty % W O

Page 35 of 40

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EPA Export 20-03-2019:03:51:02

Docurnant No.; ENSMTL1231118 / 2018700 Visit No: 11 Year: 2018 Office: Trim

EPA t i c c n ~ e NO.: WLOO41-01 Licence Holder: Enva Shannon, X2


Page 36 of 40

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EPA Export 20-03-2019:03:51:02

Document No.: ENSHTLlI3l,lE3 / 2018700 Visit No; 11 Year: 2018 Office; Trim

EPA Licence No.: WtOO42-01, Licence Holder; Enva Shannon, X2

Factlity Location: Smit hstown Fac Hity Rev.No: 1

Page 37 of 40

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EPA Export 20-03-2019:03:51:02

Document No.: ENSHTL1131118 / 2018700 Visit No: 11 Year: 2018 Office: Trim

EPA licence No.: WL009,1-01 Licence Holder: Enva Shannon, X2

Facility Location: Smithst awn Facility Rev.No: 1

Ammonia Quality Assurance

~

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EPA Export 20-03-2019:03:51:02

Document No.: ENSHTl l13 l I l 8 / 201870c) Visit No: 11 Ycar: 2018 Office: Trim

EPA Licence No.: WLOD41-Ill Licence Holder; Enva Shannon, X2

Facility Location: Smithstown Facility Rev,Na: 1

Arninonia Results & Measurement Unr;ertainty

Stack i l l x2 Run 7

I

0.065

M&ss Emissions 0.002

Page 39 of 40

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EPA Export 20-03-2019:03:51:02

Document No.: ENSWfl113111X / 2018700 Visit No: 11, Year: 2018 Office.: Trim

EPA L~CEVICG NU.: Wt004.1-01 LIcence Holder: Enva Shannon, X2


Combitled Uncertainty Expanded wrrcerrainty as prmnlags of

measured value % of measured value

Expanded uncertainty In units of measurement

Erpsndod unwrtainty as percantage of h i t

Cornblnad uncertainty mg. ln'= -,,, , ., . . .. . ' . ". . ' " . . ' p-.

Expanded w m a i a y as a Expanded uncertainty in units of measurement

% inoasured v a l u ~

' m g . r n . 3

--- Expanded unsertahly as wercentags of lirnlt value % ELV

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EPA Export 20-03-2019:03:51:02

concept Life Sciences Certtificafe of Analysis

Customar: Air Scientific Unit 32 Degranville Court Dublin Road

The result$ reportsd batch. Opinions; and interpretations exgmsse This report should not Be reproduced exci Tests covered by this certificate ware cond All results have been reviewed in accordance with Services Quality Manual

presentative of a whole

t kn approval af the lahoratury

25 of the Concept Life Scisnces, Anatflical

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