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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 1 Study & Evaluation Scheme Of Master of Sciences Chemistry [Applicable w.e.f. Academic Year 2012-13] TEERTHANKER MAHAVEER UNIVERSITY N.H. 24, Delhi Road, Moradabad, Uttar Pradesh-244001 Website: www.tmu.ac.in [With changes in MHM301 wide approval of V.C dated 26-10-2013]

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Page 1: M.Sc. Chemistry Syllabus of Teerthanker Mahaveer ... …tmu.ac.in/.../uploads/sites/4/2016/05/syllabusmscchemistry1213.pdfSyllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session

Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 1

Study & Evaluation Scheme

Of

Master of Sciences

Chemistry

[Applicable w.e.f. Academic Year 2012-13]

TEERTHANKER MAHAVEER UNIVERSITY

N.H. 24, Delhi Road, Moradabad, Uttar Pradesh-244001

Website: www.tmu.ac.in

[With changes in MHM301 wide approval of V.C dated 26-10-2013]

Page 2: M.Sc. Chemistry Syllabus of Teerthanker Mahaveer ... …tmu.ac.in/.../uploads/sites/4/2016/05/syllabusmscchemistry1213.pdfSyllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session

Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 2

TEERTHANKER MAHAVEER UNIVERSITY (Established under Govt. of U.P. Act No. 30,2008)

Delhi Road, Bagarpur, Moradabad, U.P.-244001

Study & Evaluation Scheme

Of

Master of Sciences - Chemistry

SUMMARY Programme : M.Sc. Chemistry

Duration : Two year full time (Four Semesters)

Medium : English

Minimum Required Attendance : 75 percent

Credit :

Maximum Credit : 90

Minimum Credit required for the degree : 86

Assessment- theory :

Internal Evaluation

(Theory papers)

:

Evaluation of Practical :

Evaluation of Project /Seminar

Reports :

Duration of Examination : To qualify the course a student is required to secure a minimum of 40 % marks in aggregate including the

semester end examination and teachers continuous evaluation.(i.e. both internal and external).

A candidate who secures less than 40% of marks in a course shall be deemed to have failed in that course.

The student should have at least 50% marks in aggregate to clear the semester. In case a student has more

than 40% in each course, but less than 50% overall in a semester, he/she shall re-appear in courses where

the marks are less than 50% to achieve the required aggregate percentage (of 50%) in the semester.

Question Paper Structure

1. The question paper shall consist of eight questions. Out of which first question shall be of short answer

type (not exceeding 50 words) and will be compulsory. Question No. 1 shall contain 8 parts representing

all units of the syllabus and students shall have to answer any five (weightage 4 marks each).

2. Out of the remaining seven questions, students shall be required to attempt any five questions. There will

be minimum one and maximum two questions from each unit of the syllabus. The weightage of Question

No. 2 to 8 shall be 10 marks each.

Internal External Total

30% 70% 100%

1st

Class

Test

2nd

Class

Test

3rd

Class

Test

Assignment(s)

Other

Activity

(including

attendance)

Total

Best two shall be

taken

10 10 10 5 05 30

Internal External Total

50 50 100

Internal External Total

50 50 100

External Internal

3 hrs 1 ½ hrs

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 3

Study and Evaluation Scheme

Course: M.Sc. Chemistry

Semester I (Chemistry)

S.

No

Course

Code

Subject Periods Credit Evaluation Scheme

L T P Internal External Total

1. MCH101 Thermodynamics &

Chemical Equilibrium

3 1 - 4 30 70

100

2. MCH102 Organic Reaction

Mechanism & Stereo

chemistry

3 1 - 4

30 70

100

3. MCH103 Inorganic Chemistry I 3 1 - 4 30 70 100

4. MCH104 Advanced Bioorganic

Chemistry

3 1 - 4 30 70

100

5. MCH105 Environmental Chemistry 3 1 - 4 30 70 100

6. MHM 101 Industrial Management 2 - - 2 30 70 100

7. MCH151 Organic Chemistry Lab - - 4 2 50 50 100

Total 17 5 4 24 230 470 700

Semester II (Chemistry)

S.

No

Course

Code

Subject Periods Credit Evaluation Scheme

L T P Internal External Total

1. MCH201 Chemical kinetics &

Reaction Dynamics

3 1 - 4 30 70

100

2. MCH202 Inorganic Chemistry-II 3 1 - 4 30 70 100

3. MCH203 Coordination Chemistry 3 1 - 4 30 70 100

4. MCH204 Bio-Inorganic Chemistry

3 1 - 4 30 70

100

5. MCH205 Analytical Chemistry 3 1 - 4 30 70 100

6. MHM201 Organization Behavior 2 - - 2 30 70 100

7. MCH251 Inorganic lab - - 4 2 50 50 100

Total 17 5 4 24 230 470 700

L – Lecture T- Tutorial P- Practical C-Credits

1L = 1Hr 1T= 1 Hr 1P=1Hr C=1Hr of theory

1C= 2 Hrs of Practical

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 4

Semester III (Chemistry)

S.

No

Course

Code

Subject Periods Credit Evaluation Scheme

L T P Internal External Total

1. MCH301 Organic Chemistry II

3 1 - 4 30 70 100

2. MCH302 Advances in Inorganic

Chemistry & Spectroscopy

3 1 - 4 30 70 100

3. MCH303 Physical Chemistry 3 1 - 4 30 70 100

4. MCH304 Chemistry of Natural

Products

3 1 - 4 30 70 100

MCH351 Physical Chemistry lab - - 4 2 50 50 100

8.

MCH391 Minor Research Project and

Seminar - - 4 2 50 50 100

Total 14 4 12 24 280 520 800

Semester IV (Chemistry)

(Minor Research Project may be carried out from III semester to IV semester with some

additional applications.)

L – Lecture T- Tutorial P- Practical C-Credits

1L = 1Hr 1T= 1 Hr 1P=1Hr C=1Hr of theory

1C= 2 Hrs of Practical

S.

No

Course

Code Subject

Periods Credit

Evaluation Scheme

L T P Internal External Total

1 MCH 401 Materials Chemistry 3 1 - 4 30 70 100

2 MCH 402 Computer applications in

Chemistry 3 1 - 4 30 70 100

3 MCH 491 Project work, Seminar & Viva - - 20 10 50 50 100

Total 6 2 20 18 110 190 300

5. MCH 305 Quantum Chemistry - - 4 2 30 70 100

6. MHM302 Project Management 2 - - 2 30 70 100

7.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 5

M.Sc. Chemistry Ist Year : Ist Semester

THERMODYNAMICS& CHEMICAL EQUILIBRIUM

Course code MCH101 L T P C

3 1 0 4

Unit I-First Law of Thermodynamics (Lectures 08)

Work and heat, Internal energy, Conservation of energy, The First Law and its universal

applications, System and surroundings, Exact and inexact differential, Heat capacities, Isolated

systems, Adiabatic versus isothermal processes; First thermodynamic functions, Enthalpy and its

calculations, Thermodynamic relationships; Temperature, pressure, and volume variations of

enthalpy and internal energy, Isoenthalpic process, Joule–Thompson effect; Chemical

applications of the First Law, Thermo chemistry, Standard quantities of formation, Zeroth law of

thermodynamics.

Unit II-Thermo chemistry (Lectures 08)

Change of internal energy in a chemical reaction; Relation between heat of reaction at const

volume and const pressure; bond energies, Application of bond energy; Hess law of const heat

summation and application of Hess Law, Determination of enthalpies of reactions and standard

enthalpy change; The Kirchh off equation.

Unit III - Second Laws of Thermodynamics. (Lectures 08)

Concept of spontaneity; Conversions of heat to work and vice versa; Carnot cycle;

Thermodynamic formulation of absolute temperature; Carnot, Clausius and Kelvin formulation

of entropy; Reversibility; Criteria of spontaneity and entropy increase in isolated systems,

Entropy calculations for specific processes, Trouton's rule. The Nernst heat theorem,

Unit IV -Third Laws of Thermodynamics (Lectures 08) The Third Law; Unification of the First and Second Laws: the fundamental equation, Real gases:

the fugacity, Fugacity versus pressure.

Unit V -Chemical Equilibrium (Lectures 08)

Spontaneity of chemical reactions; Gibbs energy minimum; Perfect gas equilibria; Gibbs free

energy change for the reaction and chemical quotient; Expression for thermodynamic

equilibrium constant; Equilibrium Calculations, Response of equilibrium to pressure, volume and

temperature. The van't Hoff equation.

Books Recommended

1) Iila Prigofine, Thermodynamics of Irreversible Processes .

2) S. N. Blinder, Advanced physical Chemistry, The Macmilan Company.

3) R. C. Srivatsava, S. Saha and A. K. Jain, Thermodynamics , Prentice-hall, India

.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 6

M.Sc. Chemistry Ist Year : Ist Semester

Organic Reaction Mechanism & Stereo-chemistry

Course code MCH102 L T P C

3 1 0 4

Unit I-Stereochemistry (Lectures 08)

Configuration nomenclature; Axial and planar chirality and helicity; Topicity and

prostereoisomerism; Racemic modification and optical purity; Conformational analysis of

acyclic, cyclic, heterocyclic and steroidal systems; Effects of conformation on reactivity;

Regioselectivity, stereospecificity and stereoselectivity; Asymmetric synthesis (including

enzymatic and catalytic nexus); Enantio- and diastereoselective synthesis.

Unit II-Nucleophilic Substitution Reactions (Lectures 08)

Nucleophilic substitution at saturated carbon – SN1, SN2 and related mechanisms; Parameters

influencing reaction rates; Neighboring group participation by π and σ bonds; Anchimeric

assistance; Synthetic applications of nucleophilic substitution involving alcohols, thiols, amines

and hydrides; Aromatic nucleophilic substitutions.

Structure and Reactivity:

Linear free energy relationships; Hammett and Taft equations; σ and ρ parameters; Aromaticity

in benzenoid and non-benzenoid compounds, antiaromaticity and homoaromaticity; Huckel rule,

n-annulenes, heteroannulenes, fullerenes, cryptates.

Unit III-Elimination Reactions (Lectures 08)

Mechanism and stereochemistry of different types of elimination reactions; Effects of substrate

structure, attacking base, leaving group and medium; Formation of other double bonds (C=N,

C=O) and triple bonds by elimination reactions; Mechanism and orientation in pyrolytic

elimination.

Addition to Carbon-Carbon Multiple Bonds

Mechanistic and stereochemical aspects of addition reactions involving electrophiles,

nucleophiles and free radicals; Regio- and chemoselectivity; Orientation and reactivity; Addition

to cyclopropane and carbon-heteroatom multiple bonds; Hydroboration, alkylation, epoxidation

and hydroxylation.

Unit IV-Carbonyl and Related Groups (Lectures 08)

Reactivity of carbonyl group, 1,3-dithiane reactivity, Umpolung effect; Ring expansions;

Homologation and dehomologation of carbonyl compounds; Nucleophilic addition of hetero-

atoms (N,O,S); Conjugate addition reactions, Acylation of carbonyl carbon; Carbonyl

cyclizations and cleavages; Carboxylic acids and derivatives, decarboxylation reactions.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 7

Unit V- Pericyclic Reactions (Lectures 08)

Main features of pericyclic reactions; Woodward-Hoffman rules, correlation diagram and FMO

approaches; Electro-cyclic reactions – conrotatory and disrotatory motions for 4n and 4n+2

systems; Cycloadditions – antarafacial and suprafacial additions, [2+2] and [4+2] reactions (hν

and Δ), 1,3-dipolar cycloadditions and chelotropic reactions; Sigmatropic [i,j] shifts of C-H and

C-C bonds; Sommelet-Hauser, Claisen, thio-Claisen, Cope and aza-Cope rearrangements.

Books recommended

1. S. H. Pine., Organic Chemistry, McGraw-Hill Bool.

2. J. March. Advanced Organic Chemistry: Reactions, Mechanisms and Structure.

3. Wiley Student Edition, John Wiley & Sons Asia Pte. Ltd.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 8

M.Sc. Chemistry IstYear :Ist Semester

Inorganic Chemistry I

Course code MCH 103 L T P C

3 1 0 4

UnitI -Chemistry of transition elements (Lectures 08)

General characteristic properties of transition elements; Co-ordination chemistry of transition

metal ions; stereochemistry of coordination compounds; Interpretation of electronic spectra

including charge transfer spectra; Metal clusters.

Unit II Metal – Ligand bonding (Lectures 08)

Crystal field theory; CFT for octahedral, tetrahedral and square planner complexes; John-Teller

effect,,spectro chemical series, limitation of crystal field theory; Molecular orbital theory for

octahedral, tetrahedral complexes, Ligand field theory.

Unit III-Hard & Soft Acid Base (Lectures 08)

Hard and soft acid base, Principle, theoretical basis of hardness and softness; Lewis-acid Base

reactivity approximately; Donor acceptor number, applications of HSAB Concept.

Unit IV-Inorganic Polymers (Lectures 08)

Homo and hetero catenated inorganic polymers; Polyphosphazenes: synthetic routes and bonding

features, polymerization of organo/organo-metallic substituted phosphazenes and their

applications, synthesis and characterization of polysilanes. Polysiloxanes: synthetic routes via

anionic and cationic polymerization and properties.

Unit V-Nuclear Chemistry (Lectures 08)

Nuclear reaction; Types of reaction, fission & fusion; Fission products & fission yield,

Radioactive’ tracer techniques.

Books recommended

1) A. F. Wells, Structural Inorganic Chemistry – 5th edition (1984).

2) J H Huheey, Inorganic Chemisry - Principles, structure and reactivity, Harper

and Row Publisher, Inc. New York (1972).

3) J. D. Lee, Concise Inorganic Chemistry, Elbs with Chapman and Hall, London.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 9

M.Sc. Chemistry Ist Year : Ist Semester

Advanced Bioorganic chemistry

Course Code: MCH104 L T P C

3 1 0 4

UNIT I-Cell Structure and Functions (Lectures 08)

Structure of prokaryotic and eukaryotic cells; Intracellular organelles and their functions;

Comparison of plant and animal cells; Overview of metabolic process catabolism and anabolism;

ATP – the biological energy currency; Enzymes, Structure activity and reactions; Catalyzed

determination of active site; Inhibition mechanism chemical transformations using enzyme.

UNIT II-Carbohydrates (Lectures 08)

Conformation of monosaccharide’s; Structure and functions of important derivatives of

monosaccharides like glycosides; Deoxy sugars, myoinositol, amino sugars; N aceyl muramic

acid, sialic acid and disaccharides polysaccharides, Structural polysaccharides- cellulose and

chitin; Storage polysaccharides - starch and glycogen; Ascorbic acid,

UNIT III

Carbohydrate metabolism Kreb’s cycle; Glycolysis, Glycogenesis and Glycogenolysis, Pentose phosphate pathway.

UNIT IV Lipids (Lectures 08)

Fatty acids, Essential fatty acids; Structures and function of triglycerides; Glycerophspholipids;

Sphingolipids, Cholesterol, Bile acids, Prostaglandins; Lipoproteins composition and function;

Properties of lipid aggregates– micelles, Bilayers, Liposomes and their possible biological

functions; Biological members; Fluid mosaic model of membrane structure.

UNIT V-Nucleic Acids (Lectures 08)

Purine and Pyrimidine of nucleic acids; Base pairing via H – bonding; Structure of ribonucleic

acids (RNA) and deoxyribonucleic acid (DNA); Double helix model of DNA and forces

responsible for holding it; Chemical and enzymatic hydrolysis of nucleic acids; The chemical

basis for heredity, An overview of replication of DNA; Transcription, Translation and genetic

code; Chemical synthesis of mono and poly nucleosides.

Books recommended

1. A. L. Lehinger, Principles of Biochemistry, Worth Publications.

2. L. Stryer, W. H. Freeman Biochemistry.

3. J. David Rawn, Neil Patterson Biochemistry.

4. Voet and Voet, John Wiley Biochemistry.

5. E. E. Conn and P. K. Stumpt, John Wiley. Outlines of Biochemistry.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 10

M.Sc. Chemistry Ist Year : Ist Semester

Environmental Chemistry

Course Code: MCH105 L T P C

3 1 0 4

Unit I-Air Pollution & Water pollution (Lectures 08)

Sources and sinks of gases pollutants; Classification & effects of air pollutants on living and

nonliving things; Air pollution problems in India; Pollution problems in industrial area; Global

air pollution problems, green house effect, acid rain, ozone depletion and their consequences on

Environment, Major air pollution disasters, Types, sources and classification of water pollutants,

Industrial water pollution; Constituents of aquatic Environment; Oxygen contents of water and

aquatic life; Oxygen electrode and its use; Mercury pollution and estimation of organo-

mercurials; Industrial water; Effects of water pollutants on life and Environment.

UNIT II -Method of control of air pollution & water pollution (Lectures 08)

Method of control of air pollution; Electrostatic precipitation wet & dries scrubber; Filters,

gravity and cyclonic separation; Adsorption, absorption and condensation of gaseous effluent;

Method of control of water pollution; Water and waste water treatment; Aerobic and anaerobic;

aeration of water; Principle of coagulation, flocculation, softening, disinfection, demineralization

and fluoridation.

UNIT III-Sampling & analysis of air and water pollutants (Lectures 08)

Methods of sampling gaseous; Liquid and solid pollutants; Analysis of - CO, CO2, NO2, SO2,

H2S, CO2; Analysis of toxic heavy metals - Cd, Cr, As, Pb, Cu; Separation of Co, Cu, Mg, Mn,

Fe; Analysis of total cationic and anionic burdens of water; Pesticide, residue analysis soil

pollution; Sources of pesticides residue in the Environment; Pesticides degradation by natural

forces; Effect of pesticide residue on life; Analytical techniques for pesticides residue analysis.

UNIT-IV-Radiation pollution (Lectures 08)

Classification & effects of radiation; Effects of ionizing radiation on man; Effects of non

ionizing radiation on life; Radioactivity and Nuclear fallout; Protection and control from

radiation.

UNIT V-Environmental toxicology (Lectures 08)

Chemical solutions to environmental problems biodegradability; Principles of decomposition

better industrial processes; Bhopal gas tragedy, Chernobyl, Three Mile Island, Sewozo and

Minamata disasters.

Books recommended

1. A.K. De ,Environmental Pollution.

2. Wark & Werner Air Pollution.

3. S.P. Mahajan Environmental Pollution Control in Process Industries

4. B.K. Sharma & H.Kaur Environmental Pollution.

5. P.K. Trivedi Introduction to Air Pollution.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 11

M.Sc. Chemistry Ist Year : Ist Semester

Industrial Management

Course Code: MHM 101 L T P C

2 0 0 2

Unit I (Lectures 06)

General Management: Principles of scientific management; Brief description of managerial

functions.

Business Organizations: Salient features of sole Proprietorship, Partnership, Joint stock

Company – private and public limited.

Unit II (Lectures 06)

Financial Management: Concept of interest; Compound interest; Present worth method, Future

worth method.

Depreciation – purpose, Types of Depreciation; Common methods of depreciation - Straight line

method, Declining balance method, Sum of the years digits method.

Unit III (Lectures 06)

Personnel Management: Leadership and motivation; Staff role of the personnel department;

Personnel functions; Organizational structure.

Human Resource Planning: Reasons for human resource planning; Planning process; Goals

and plans of the organizations; Implementation programs; Brief description of recruitment,

selection, placement, performance appraisal, career development, promotion, transfer,

retirement, training and development, motivation and compensation.

Unit IV (Lectures 06)

Material Management: Importance; Definition; Source selection, Vendor rating and Value

analysis; Scope of MRP.

Inventory Control: Definition, objectives, reasons, and requirements for inventory management;

Inventory methods - ABC Analysis, VED.

Economic Order Quantity models - Basic EOQ, Economic production run size and Quantity

discounts.

Unit V (Lectures 06)

Marketing Management: Product life cycle; Channels of distribution; Advertising & sales

promotion; Market Research.

Managing Marketing Effort: Marketing implementation and evaluation; Appraisal and

prospects.

Text books:

1. K. K. Ahuja, Industrial Management, Vol. I & II, Khanna Publisher.

2. E.Paul Degarmo, John R.Chanda, William G.Sullivan, Engg Economy, Mac Millan Publishing Co.

Reference Books:

1. Philip Kotler, Principles of Marketing Management, Prentice Hall.

2. P. Gopalakrishnan, M. Sundaresan, Materials Management, Prentice Hall of India Ltd.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 12

M.Sc. Chemistry Ist Year : Ist Semester

Organic Chemistry lab

Course Code MCH151 L T P C

0 0 4 2

List of Experiments

1. To perform Oxidation: Adipic acid by chromic acid oxidation of Cyclohexanol.

2. To perform Aldol condensation: Dibenzal acetone from Benzaldehyde.

3. To perform Sandmeyer reaction: p- Chlorotoulene from p-Toluidine.

4. To perform Aromatic Electrophonic substitutions: Synthesis of p-Nitroaniline and p-

Bromoaniline.

5. Determination of neutralization equivalent of organic acids Separation & identification of

compounds having one or more functional groups.

6. Preparation characterization of two & three steps organic compounds solution of caffeine

from tea leaves.

Evaluation of Practical Examination:

Internal Evaluation (50 marks)

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5

point scale which would include the practical conducted by the students and a Viva voce taken by

the faculty concerned. The marks shall be entered on the index sheet of the practical file.

Evaluation scheme:

PRACTICAL PERFORMANCE & VIVA

DURING THE SEMESTER (30 MARKS)

ATTENDANCE

(5 MARKS)

QUIZ

(5

MARKS)

VIVA

(10

MARKS)

TOTAL

INTERNAL

(50

MARKS)

EXPERIMENT

(10 MARKS)

FILE

WORK

(10

MARKS)

VIVA

(10

MARKS)

External Evaluation (50 marks)

The external evaluation would also be done by the external Examiner based on the experiment

conducted during the examination.

EXPERIMENT

(20 MARKS)

FILE WORK

(10 MARKS) VIVA

(20 MARKS) TOTAL EXTERNAL

(50 MARKS)

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 13

M.Sc. Chemistry Ist Year : IInd Semester

Chemical kinetics & Reaction Dynamics

Course Code MCH201 L T P C

3 1 0 4

UNIT I-Chemical Kinetics (Lectures 08)

Basic concepts: reaction order; Molecularity; Rate laws; Reaction mechanisms: time dependence

of reactance; Intermediates and products; Rate constants: Arrhenius rate law and deviation;

Activation energy versus entrance barriers; Experimental determination of rate constants.

UNIT II-Theories of reaction rates (Lectures 08)

The collision theory of bimolecular gaseous reaction; Activated complex theory; The Lindemann

theory of unimolecular reaction; Kinetics of complex reactions.

UNIT III-Potential energy surfaces (Lectures 08)

Two dimensional representation; Features on potential energy surfaces; Experimental probing of

potential energy surfaces and reaction mechanisms; Molecular dynamics calculations.

UNIT IV-Theories of Unimolecular Gaseous reactions (Lectures 08)

Partition functions and chemical equilibrium; Transition state theory; Application of transition

state theory to unimolecular decomposition; Hinshelwood theory; The RRK Theory; RRKM

theory.

UNIT V (Lectures 08)

Marcus theory of Electron transfer reaction; Statistical mechanical derivation of the rate constant

of a gaseous bimolecular reaction using TST.

Books recommended

1. R.D. Levine, R.B. Bernstein Molecular Reaction Dynamics and Chemical Reactivity (Oxford,

New York).

2. Paul L. Houston Chemical Kinetics and Reaction Dynamics, (Mc Graw Hill, New York).

3. G. Arfken Mathematical Methods for Physicists, , (Academic Press, New York).

4. J.I. Seinfeld, J.S. Francisco, W.L. Hase Chemical Kinetics and Dynamics.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 14

M.Sc. Chemistry Ist Year :IInd Semester

Inorganic Chemistry- II Course Code: MCH202 L T P C

3 1 0 4

Unit I-Chemistry of non – Transition elements (Lectures 08)

General discussion on the properties of the non–transition elements; Special features of

individual elements; Synthesis, properties and structure of halides and oxides of the non–

transition elements; Polymorphism in carbon, phosphorous and sulphur; Synthesis, properties

and structure of boranes, silicates, nitrogen compounds; Structure and bonding in oxy-acid of

nitrogen, phosphorous, sulphur and halogens, inter-halogens, pseudo halides.

UNIT-II-Oregano metallic Chemistry of transition elements (Lectures 08)

Ligand captivity; Electron count for different types of organ metallic compounds;18 and 16

electron rule exceptions; Synthesis, structure and bonding, organ metallic reagents in organic

synthesis and in homogeneous catalytic reactions (Hydrogenation and hydroformylation,

isomerisation).

Unit III-Photochemistry of Metal Complexes and Metal–Metal Multiple Bonds (Lectures 08)

Excited states, ligand field states, charge-transfer states and Thexi states; Phosphoresence and

fluorescence; Photochemical reactions: substitution and redox reactions of Cr(III) andRu(II)

complexes; Applications: synthesis and catalysis, chemical actinometrical and photo-chromism.

Unit IV-Nanomaterials (Lectures 08)

General introduction to nonmaterial’s and emergence of nanotechnology; synthesis of

nanoparticles of gold, palladium, platinum, and silver; Synthesis of nanowires and Nano rods;

electroplating and electrophoresis deposition, Thin films: Chemical vapour deposition and

Atomic layer deposition techniques; Carbon fullerenes and nanotubes. Single walled and

multiwalled carbon nanotubes, Applications of nanoparticles.

Unit V (Lectures 08)

Synthesis, properties and structures of carboranes, silicones, phosphazenes, zeolites and clay;

polymorphism of carbon, phosphorus and sulphur;

Books recommended

1. R. C. Mehrotra& A. Singh. Organometallic Chemistry: A Unified Approach (2nd edn.), New

Age International (2000).

2 F. A. Cotton & G. Wilkinson. Advanced Inorganic Chemistry (5th edn.), John Wiley (1988).

3. D. M. Roundhill. Photochemistry and Photophysics of Metal Complexes, Plenum Press.

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M.Sc. Chemistry Ist Year : IInd Semester

Coordination Chemistry

Course Code: MCH 203 L T P C

3 1 0 4

UNIT I -Theories of Metal - Ligand bonding (Lectures 08) Molecular Orbital treatment; Octahedral (with and without pi bonding) tetrahedral and square

planer complexes in a qualitative manner; Comparison of theories of bonding, VBT, CFT, LFT

and MOT.

UNIT II -Structural studies of coordination compounds (Lectures 08)

Compounds of first transition series elements, with respect to their electronic spectra, magnetic

& thermal properties (DTA, TGA).

UNIT III-Magneto Chemistry (Lectures 08)

Diamagnetic correction, single & multielectron system; Types of the magnetic behavior;

Diamagnetism, Para magnetism, Ferro & Ferri, Antiferro and magnetic interaction; The origin of

Para magnetism, Magnetic behavior of complexes; Simplification of Van Velck equation;

Magnitude of magnetic moments; Determination of magnetic susceptibility by Gouy and

Faraday method.

UNIT IV-Transition metal complexes & catalysis (Lectures 08)

Introduction, General Principle; Catalysis by transition metal complexes; Hydrocarbons

Oxidation by Molecular oxygen, olefin Oxidation, olefin polymerization, olefin hydrogenation;

Arene reactions catalyzed by metal complexes; Catalysis of condensation polymerization

reaction; Current and feature trend in catalysis.

UNIT V-Mixed Ligand complexes (Lectures 08)

Stabilities of ternary complexes; Dynamics of formation of ternary complexes reaction of

Coordination ligand in ternary complexes; Mimicking reactions in biological systems; Enzyme

models; Amino acids ester hydrolysis; Peptide synthesis & hydrolysis; Detarbodylation of β keto

acids.

Books recommended

1. Jones: Elementary Coordination Chemistry. J. Weily.

2. Graddon: Introduction to Coordination Chemistry. J. Weily.

3. Drago: Physical methods of Inorganic Chemistry. J. Weily.

4. Graddon: Introduction to coordination Chemistry, Parasmom.

5. Lewis and Wilkins: Coordination Chemistry. J. Weily.

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M.Sc. Chemistry Ist Year : IInd Semester

Bio Inorganic chemistry

Course Code: MCH 204 L T P C

3 1 0 4

Unit I -Bioinorganic Chemistry of Alkali and Alkaline Earth Metals (Lectures 08)

Essential and trace elements in biological systems; Structure and functions of biological

membranes; mechanism of ion transport across membranes; Sodium pump; Ionophores:

valinomycin and crown ether complexes of Na+ and K+; ATP and ADP; Photosynthesis:

chlorophyll a PS I and PS II; Role of calcium in muscle contraction; Blood clotting mechanism

and biological calcification.

Unit II -Bioinorganic Chemistry of Iron and Copper (Lectures 08)

Iron-sulphur proteins: Rubredoxin and ferredoxins; Metalloporphyrins; Heme proteins:

hemoglobin, Structure and Mechanism of hemoglobin, myoglobin and cytochrome c; Non-heme

proteins: hemerythrin and hemocyanin.

UNIT III-Nitrogen Fixation, Metal poisoning and there treatment (Lectures 08)

Nitrogen in biosphere; Nitrogen cycle; Role of micro-organisms in nitrification; Nitrogen

fixation in soils; Metal poisoning and drug action of Inorganic complexes compounds; Metal

poisoning, treatment by using chelating agent, mercury, lead & cadmium poisoning & treatment;

Platinum complexes in treatment of cancer. metal deficiency.

UNIT IV-Trace Metals in Plant Life (Lectures 08)

Micronutrients present in soil and role in plant life; Biodegradation of minerals by bacteria and

its applications in treatment of soil and water pollution.

Unit V-Medicinal chemistry (Lectures 08)

Concept of drug; Lead compound and lead modification; Structure activity relationship (SAR);

Quantitative structure-activity relationship (QSAR); Theories of drug activity – occupancy

theory, rate theory, induced fit theory; Concept of drug receptors – elementary treatment of drug-

receptor interactions; Physicochemical parameters – lipophilicity, partition coefficient, electronic

ionization constants, steric; Factors affecting modes of drug administration, absorption,

metabolism and elimination; Significance of drug metabolism in medicinal chemistry.

Recommended Books:

1. Eichhorn: Inorganic Biochemistry : Vol I , 2 Elsevier.

2. Ochiai: Bioinorganic Chemistry: Allyn & Bacon Burton.

3. Williams: an Introduction to Bioinorganic Chemistry, C.C. Thomos Spring III.

4. Wallace: Decade on synthetic chelating agent in Inorganic plant nutrition, Wallace.

5. Williams: Metals in Life.

6. Zagic: Microbial Biogeochemistry, Academic press.

7. Ahuja: Chemical Analysis of the Environment, Plenum press.

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M.Sc. Chemistry Ist Year : IInd Semester

ANALYTICAL CHEMISTRY

Course Code: MCH 205 L T P C

3 1 0 4

UNIT I -Ultraviolet and visible spectrophotometry (UV-VIS) (Lectures 08)

Introduction, Beer Lambert’s law; Instrumentation applications of UV vs, Infrared Spectroscopy

(IR); Introduction, instrumentation, sampling technique, selection rules, types of bonds,

absorption of common functional groups; Factors affecting frequencies & applications.

UNIT II-Nuclear Magnetic Resonance (NMR) (Lectures 08)

Magnetic and nonmagnetic nuclei; Larmor frequency; Absorption of radiofrequency,

Instrumentation (FT-NMR); Sample preparation, chemical shift, spin-spin coupling, coupling

constant, applications to simple structural problems; Mass spectroscopy (MS) - Principle,

working of mass spectrometer (double beam); Formation of different types of ions,

fragmentation of alkanes, alcohols and ketones, simple applications; Simple structural problems

based on IR, UV and MS.

UNITIII-Nephlometry and Turbidometry (Lectures 08)

Introduction, Theory, Instruments, working and Applications, Radiochemical Analysis, NAA:

Scintillation counter and GM counter.

UNITIV-Atomic Absorption Spectroscopy (Lectures 08)

Introduction, Principal, Difference between AAS and FES; Advantages of AASover FES,

Advantages and disadvantages of AAS; Instrumentation; Single and double beam AAS,

Detection limit and sensitivity, Interferences applications.

UNIT V-Inductively coupled Plasma Spectroscopy (Lectures 08)

Introduction, Nebulisation Torch, Plasma; Instrumentation; Interferences; Applications.

Recommended Books:

1. Willard, Merrit, Dean and Settle Instrumental Methods of analysis.

2.R.M. Silverstein and G.C. Bassler Spectroscopic identification of organic compounds.

3.D.H. Williams and I. Fleming Spectroscopic methods in organic chemistry.

4.V.M. Parikh Absorption spectroscopy of organic molecules.

5. P.S. Kalsi Applications of spectroscopic techniques in Organic chemistry.

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M.Sc. Chemistry Ist Year : IInd Semester

ORGANISATIONAL BEHAVIOUR

Course Code MHM 201 L T P C

2 0 0 2

Unit – I (Lecture 08)

Concept, Nature, Characteristics, Models of Organizational Behaviour, Management Challenge,

Organizational Goal. Global challenges and Impact of culture.

Unit – II (Lecture 08)

Perception: Concept, Nature, Process, Importance. Attitudes and Workforce Diversity.

Personality: Concept, Nature, Types and Theories of Personality Shaping, Learning: Concept

and Theories of Learning.

Unit – III (Lecture 08)

Motivation: Concepts and Their Application, Principles, Theories, Motivating a Diverse

Workforce.

Leadership: Concept, Function, Style and Theories of Leadership-Trait, Behavioural and

Situational Theories. Analysis of Interpersonal Relationship.

Unit – IV (Lecture 08)

Organizational Power and Politics: Concept, Sources of Power, Approaches to Power,

Political Implications of Power. Knowledge Management & Emotional Intelligence in

Contemporary Business Organization.

Organizational Change: Concept, Nature, Resistance to change, Managing resistance to

change, Implementing Change.

Unit –V (Lecture 08)

Conflict: Concept, Sources, Types, Functionality and Dysfunctional of Conflict, Classification

of Conflict Intra, Individual, Interpersonal, Intergroup and Organizational, Resolution of

Conflict, Stress: Understanding Stress and Its Consequences, Causes of Stress, Managing Stress.

Text Books:

1. Dwivedi, D. N, Managerial Economics, Vikas Publishing House.

2. Varshney & Maheshwari, Managerial Economics, Sultan Chand & Sons.

Reference Books:

1. Robbins Stephen P., Organizational Behavior Pearson Education

2. Hersey Paul, “Management of Organsational Behavior: Leading Human Resources”

Blanchard, Kenneth H and Johnson Dewey E., Pearson Education

3. Khanka S. S. “Organizational Behavior

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M.Sc. Chemistry Ist Year : IInd Semester

Inorganic Lab Course Code MCH251 L T P C

- - 4 2

List of Experiments.

1.To perform quantitative separation and determination of the following pairs of metal ions using

gravimetric and volumetric methods:

(i) Ag+ (gravimetrically) and Cu2+(Volumetrically)

(ii) Cu2+

(gravimetrically) and Zn2+(Volumetrically)

(iii) Fe3+

(gravimetrically) and Ca2+(Volumetrically)

(iv) Mg2+

(gravimetrically) and Ca2+(Volumetrically)

2.To determine separation of a mixture of cations/anions by paper chromatographic technique

using aqueous/nonaqueous media.

(i) Pb2+

and Ag+ (aqueous and non-aqueous media)

(ii) Co2+

and Cu2+

(non-aqueous medium)

(iii) Cl– and I

– (aqueous-acetone medium)

(iv) Br– and I

– (aqueous-acetone medium)

Recommended Books:

1) A. I. Vogel ,A text book of Quantitative Inorganic Analysis

2) W. G. Palmer Experimental Inorganic Chemistry

Evaluation of Practical Examination:

Internal Evaluation (50 marks)

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5

point scale which would include the practical conducted by the students and a Viva voce taken by

the faculty concerned. The marks shall be entered on the index sheet of the practical file.

Evaluation scheme:

PRACTICAL PERFORMANCE & VIVA

DURING THE SEMESTER (30 MARKS)

ATTENDANCE

(5 MARKS)

QUIZ

(5

MARKS)

VIVA

(10

MARKS)

TOTAL

INTERNAL

(50

MARKS)

EXPERIMENT

(10 MARKS)

FILE

WORK

(10

MARKS)

VIVA

(10

MARKS)

External Evaluation (50 marks)

The external evaluation would also be done by the external Examiner based on the experiment

conducted during the examination.

EXPERIMENT

(20 MARKS)

FILE WORK

(10 MARKS) VIVA

(20 MARKS) TOTAL EXTERNAL

(50 MARKS)

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M.Sc. Chemistry IInd Year : IIIrd Semester

Organic Chemistry ll

Course Code MCH 301 L T P C

3 1 0 4

Unit I-Reductive Reactions (Lectures 08)

Catalytic hydrogenation: Scope and mechanisms for heterogeneous catalytic hydrogenation of

alkenes and other functional groups; Reduction selectivity; Catalyst poisoning and

desulphurization; Homogeneous catalytic hydrogenation with Wilkinson catalyst; Alkene double

bond isomerisation.

Dissolving metal reductions: Scope and basic mechanisms; Liquid ammonia reduction with alkali

metals, Birch reduction of arenes; Acyloin condensation and related reactions.

Metal hydride reductions

Scope, stereochemistry and mechanism of metal hydride reductions of carbonyl compounds;

Reduction of other functional groups like nitro, nitroso, azo and oxime groups; MPV reduction;

Use of hydroboration in reduction, oxidation and carbonylation, regioselectivity.

Unit 2-Oxidation Reactions (Lectures 08)

Cr and Mn Oxidations:

Oxidation of alcohols & aldehydes with Cr (VI) & Mn (VII) oxidants; Oxidation of C=C and C-

H bonds; Uses of PCC, PDC and Collin’s reagent, Peroxy Oxidations: Alkene epoxidation by

peracids and metal/alkyl hydroperoxides.

Other methods of oxidation: DMSO and Swern oxidations; Oppenauer oxidation; Prevost and

Woodward hydroxylation of alkenes; Oxidative cleavage of C-C single and double bonds;

periodates, LTA, oxidation of organic substrates with mercuric acetate and SeO2.

Unit 3-Reactive Intermediate (Lectures 08)

Carbenes stability, structure and spin states of carbenes; Cyclopropanation spin dependence and

stereochemistry; Carbene insertion to C-H bonds; Rearrangement to alkenes; Wolff

rearrangement of acylcarbenes and its synthetic applications; Carbenoids. Nitrenes: Stability,

structure and spin states of nitrenes; C-H bond insertions and aziridine formation; Rearrangement

of acylnitrenes (Hoffmann, Curtius and Schmidt reactions with applications in organic

synthesis); Nitrenoids.

Unit IV-Free radical reactions (Lectures 08) Types of free radical reactions; Detection by ESR, free radical substitution mechanism,

neighboring group assistance; Reactivity for aliphatic and aromatic substrates at a bridgehead;

Reactivity in attacking radicals; The effect of solvent on reactivity; Allylic hydrogenation (NBS);

Oxidation of aldehydes to carboxylic acids, auto oxidation; Coupling of alkynes and arylation of

aromatic compounds by diazonium salt; Sandmeyers reaction; Free radical rearrangement.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 21

Unit-V-Non benzenoid aromatic Compounds (Lectures 08) Aromaticity in Non- benzenoids compounds Annulenes and hetroannulenes; Fullerence C60 ,

Tropone, tropolone azulene, fulvene, tropylium salts, ferrocene; Three and five membered

systems; Crown ether complexes; Cyclodextrins; Cryptands, catenanes and rotaxanes, bonding in

fullerenes.

Recommended Books:

1. H. O. House. Modern Synthetic Reactions, W. A. Benjamin (1972).

2. J. March. Advanced Organic Chemistry: Reactions, Mechanisms and Structure, John.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 22

M.Sc. Chemistry IInd Year : IIIrd Semester

Advances in Inorganic chemistry & spectroscopy

Course Code MCH 302 L T P C

3 1 0 4

Unit 1

Homogeneous Catalysis (Lectures 08)

Coordinative unsaturation; Oxidative addition reactions, insertion reactions; Reactions of

coordinated ligand and activation of small molecules by complexation; Catalytic reactions of

alkenes: isomerization, hydrogenation, hydroformylation, hydrosilylation and polymerization.

Unit 2

Transition Metal π-acid Complexes and Supramolecular Chemistry (Lectures 08)

Bonding, Synthesis and reactivity of transition metal complexes with CO, NO, O2, N2 and

tertiary phosphine and arsine ligands; Metal carbonyl hydrides and metal carbonyl clusters:

LNCC and HNCC; Wade’s rule and the capping rule; Supramolecular chemistry: Definition,

supramolecular host-guest compounds; Macrocyclic effect; Nature of suparmolecular

interactions.

Unit 3

Kinetics and Mechanism of Inorganic Reactions (Lectures 08)

Labile and inert complexes; mechanisms of ligand-replacement reactions; ligand displacement

reactions in square planar and octahedral complexes; the trans effect; isomerisation and

racemisation of tris-chelate complexes; electron transfer reactions; stereochemical ,nonrigidity

and fluxional molecules.

Unit IV- Infrared and Raman Spectroscopy (Lectures 08)

Structural studies (involving IR and Raman spectroscopy) of coordination compounds containing

the following molecules/ions and ligands - NH3, H2O, OH−, SO4

2−, CN

−, SCN

−, NO, O2 and

halides.

Magnetic Resonance Spectroscopy

Electron spin resonance spectroscopy: ESR of d1 and d9 transition metal ions in cubic and

tetragonal ligand fields; Evaluation of g values and metal hyperfine coupling constants.

Unit V-X-ray Crystallography (Lectures 08)

Lattices, planes and indices; X-ray diffraction and Bragg’s law; Crystal systems and symmetry,

point groups, ; Symmetry elements: isogonal symmetry groups and reciprocal lattice, Crystal

growing .

Mossbauer Spectroscopy: Principles, isomer shift; Quadrupole effect of magnetic field,

applications to iron and tin compounds.

Recommended Books:

1.K. Nakamoto. Infrared and Raman Spectra of Inorganic and Coordination Compounds, (5th

edn.), John Wiley (1997).

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 23

M.Sc. Chemistry IInd Year : IIIrd Semester

Physical chemistry Course Code MCH 303 L T P C

3 1 0 4

UNIT I- Photochemistry (Lectures 08) Absorption of light and nature of electronic spectra; Electronic transition, Beer Lambert Law and

its limitation, The Law Photochemistry, quantum yield; The Photochemical laws, photochemical

reactions: photo-reduction, photo-oxidation, photo dimerization, photochemical substitution,

photo-isomerization, photochemistry of environment: Green house effect.

UNIT II-Photo physical phenomena (Lectures 08) Electronic structure of molecules; Molecular orbital; Electronically excited singlet states,

designation based on multiplicity rule, construction of Jablonski diagram; Fluorescence, delayed

fluorescence and phosphorescence; Chemi-luminescence; Fluorescence quenching: concentration

quenching, quenching by excimer and exciplex emission; Fluorescence resonance energy

transfer between photo-excited donor and acceptor systems; Stern-Volmer relation.

UNIT III-Electrochemistry (Lectures 08) Arrhenius theory of electrolytic dissociation (Evidences and limitations), revision of basic

electrochemistry (Types of electrodes and cells), Electrochemical cells with and without

transference, determination of activity coefficients of an electrolyte, degree of dissociation of

monobasic weak acid (approximate and accurate ), instability constant of silver ammonia

complex, Acid and alkaline storage batteries.

UNIT IV-Kinetic theory of gases (Lectures 08)

Postulates of kinetic theory of gases; P-V-T relations for an ideal gas, non-ideal behavior of

gases; Equation of state, compressibility factor, Virial equation, Van der Waal’s equation;

Excluded volume and molecular diameter; Relations of Van der Waal’s constants with Virial

coefficients and Boyle temperature; Maxwell-Boltzmann law for distribution of molecular

velocities; Physical significance of the distribution law, deviation of expressions for average,

root mean square and most probable velocities; Experimental verification of the distribution law;

Molecular collision in gases, mean free path.

UNIT V-Colloids and Macromolecules (Lectures 08)

Sols, Lyophilic and lyophobic sols, properties of sols, coagulation. Sols of surface active

reagents, surface tension and surfactants, critical micelle concentration, Mechanism of

polymerization, molecular weight of a

polymer (Number and mass average ),viscosity average molecular weight, numerical problems;

Degree of polymerization and molecular weight, methods of determining molecular weights

(Osmometry, viscometry, light scattering, diffusion and ultracentrifugation).

Books Recommended:

1. Vol. 2 A & B, J.O’M. Bockris and A. K. N. Reddy Modern Electrochemistry, , 2nd Ed.

Plenum Press,

2. P. W. Atkins, 7th & 8th Eds. Physical Chemistry, , Oxford University Press, New York.

3. I.N. Levine, 5th Ed., Physical Chemistry, Tata McGraw Hill Pub. Co. Ltd., New Delhi.

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 24

M.Sc. Chemistry IInd Year : IIIrd Semester

Chemistry of Natural Products

Course Code MCH 304 L T P C

3 1 0 4

Unit I- Natural Products and their Biosynthetic Pathways (Lectures 08)

General classification of natural products, their isolation and characterisation and biosynthesis of

common plant products; Biosynthesis pathways for natural products using co-enzymes and

enzymes; Synthesis of selected natural products based on genetic classification – fatty acid

derivatives and related compounds, general biogenesis and synthesis of cis-jasmone, methyl

jasmonate, prostaglandins, exaltone and muscone.

Unit II-Antibiotics (Lectures 08)

Cell wall biosynthesis, inhibitors of β-lactam rings, antibiotics inhibiting protein synthesis;

Isolation, structure elucidation, synthesis, SAR and mode of action of penicillins; Synthesis of

penicillin G, penicillin V, ampicillin, amoxicillin and cephalosporin. Isolation, structure

elucidation, synthesis, SAR and mode of action of following antibiotics: streptomycin,

tetracyclines and chloroamphanicol.

Unit III-Terpenoids and Alkaloids (Lectures 08)

General biosyntheses of mono- and sesquiterpenes, trans-chrysanthemic acid, cyclo- pentato

monoterpene lactones, Synthesis of α-vetinone and total synthesis of β-eudesmol; Synthesis of

hirsutene, abietic acid, cis juvenile hormone; trans annular cyclisation of caryophyllene,

synthesis of caryophyllene and isocaryophyllene; Rearrangements of santonic acid and

thujospene; Synthesis and rearrangement of longifolene.

Unit IV-Steroids (Lectures 08)

Biosynthesis of diterpenes, higher terpenes and steroids; Nomenclature of steroids and synthesis

of squalene; Lanosterol and caretonoids; Synthesis of equlenins; Estrogens and total synthesis of

non-aromatic steroids (progesterones); Corticosteroids; Degradation of diosgenin to progesterone

and its synthesis; Miscellaneous transformations of steroid molecules.

Unit V-Biogenesis (Lectures 08) a)Alkaloids (pyridine, morphine and indole type) terpenoids of classes with examples,

cholesterol, flavones, coumarins, carbohydrates and proteins.

b)Vitamins - Synthesis and structure of biotin and vitamin B2, synthesis of vitamin B1, biological

functions of B6, B12, folic acid and thiamin.

Recommended Books:

1. Burger. Medicinal Chemistry and Drug Discovery, Vol-1, Ed. M. E. Wolff, John Wiley.

2. K. Nakanashi. Natural Products Chemistry, Vols. I and II, Academic Press, New York and

London.

3. M. Harmata. Strategies and Tactics in Organic Synthesis 4 & 5, Academic Press (2004).

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Syllabus M.Sc.-Chemistry Applicable w.e.f. Academic Session 2012-13 Page 25

M.Sc. Chemistry IInd Year : IIIrd Semester

Quantum Chemistry Course Code MCH 305 L T P C

3 1 0 4

Unit I-Brief review of failure of classical mechanics (Lectures 08)

Wave-particle duality; Dynamics of microscopic systems: the Schrodinger equation, the

uncertainty principle, the interpretation of the wave function.

Unit II-Formalism of Quantum Mechanics (Lectures 08) Postulates of Quantum Mechanics, Eigen function and Eigen values Operators; Acceptability of

wave functions; Normalized and orthogonal wave functions; Principles of superposition; Schnidt

Orthogonalisation; Hermition operators; Theorems related to commutator operations; Stern-

Gerlach experiment and spin of electron; Spin eigen function; Concept of angular momentum,

angular momentum operators, Ladder operators.

Unit III-Quantum Mechanics of some simple systems (Lectures 08) a)Parcticle in a box: One dimensional Box - application to spectra of linear conjugated molecular

degeneracy in multidimensional box.

b)Potential well of finite depth (Tunneling effect )

c)Rigid rotator

d)Linear harmonic oscillator, the formal solutions, energy levels, degeneracy, properties of wave

functions and selection rules.

Unit IV Schrodinger equation (Lectures 08)

Schrodinger equation for hydrogen atoms (polar co-ordinates) and its solution; The radial

distribution function and its significance, shape of atom orbitals.

Unit V-A brief introduction to hydrogen like atoms (Lectures 08) Helium atoms, Approximate methods: Perturbation theory and Self-consistent field theory;

Chemical bonding and hybridization; Approximate methods: The variation theorem and

principles, its use to obtain optimum molecular orbital and energies; Secular equation and secular

determinants, Huckel Molecular Orbital Theory; Origin of aromatic stability and calculation of

delocalization energy; Brief introduction to hetero-nuclear systems; Use of symmetry based

linear combination to simplify the problem of Huckel theory calculations for larger aromatic

molecules.

Books Recommended

1. A. K. Chandra ,Introductory Quantum Chemistry ; Tata McGraw-Hill. 1988.

2. W. J. Moore, Basic Physical Chemistry ;Prentice Hall, 1986.

3. P. W. Atkins, Physical Chemistry, ELBS, 1986.

4. W. Kauzmann ,Quantum Chemistry, , Academic press.

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M.Sc. Chemistry IInd Year : IIIrd Semester

PROJECT MANAGEMENT

Fundamental Topics: Introduction to Project Management and Corporate Planning Process;

Corporate Financial Objectives;; Time Value of Money; Future Value and Present Value of

Multi-period Cash Flow; Interest Rate.

Unit II (Lectures 06)

Concept Stage: Strategic Investment Decisions and Project Ideas; Project Feasibility Study;

Demand Forecasting Techniques; Project Financing; Forms of Business Organization.

Unit III (Lectures 06)

Analysis Stage: Cost-Benefit Analysis; Financial Analysis; Required Rate of Return from

Projects; Economic and Social Cost-Benefit Analysis; Project Portfolio Risk; Project Risk

Analysis; Framework of Project Risk Management.

Unit IV (Lectures 06)

Planning, Execution and Completion Stage: Introduction to PERT & CPM; Allocation of

Limited Capital - Capital Rationing; Project Planning and Control Project Execution and

Control; Post Completion Audit (PCA).

Unit V (Lectures 06)

Special Topics: Inflation and Project Investment; Economic Life of Projects and Replacement

Policy; Infrastructure Projects; International Capital Budgeting.

Text Books:

1. Bhavesh Patel, PROJECT MANAGEMENT: Financial Evaluation with Strategic

Planning, Networking and Control, Vikas Publishing House Pvt Ltd.

Course Code MHM 302 L T P C

2 0 0 2

Unit I (Lectures 06)

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M.Sc. Chemistry IInd Year : IIIrd Semester

Physical Chemistry Lab

Course Code: MCH351 L T P C

0 0 4 2

List of Experiments

1. To perform saponification of ethyl acetate with sodium hydroxide by chemical method.

2. To determine comparison of acid strengths through acid catalyzed methyl acetate hydrolysis.

3. To determine energy of activation of acid catalyzed hydrolysis of methyl acetate.

4. To determine distribution coefficient of I2 between two immiscible solvents.

5. To perform conductometric titration of a weak acid with strong base.

6. To perform conductometric titration of a mixture of weak and strong acids.

7. To perform potentiometric titration of a strong acid with strong base using quinhydrone

electrode.

8. To determine conduct-ometric titration of KCl with AgNO3.

9. To determine molecular weight of a non-electrolyte by cryoscopy method.

Evaluation of Practical Examination:

Internal Evaluation (50 marks)

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5

point scale which would include the practical conducted by the students and a Viva voce taken by

the faculty concerned. The marks shall be entered on the index sheet of the practical file.

Evaluation scheme:

PRACTICAL PERFORMANCE & VIVA

DURING THE SEMESTER (30 MARKS)

ATTENDANCE

(5 MARKS)

QUIZ

(5

MARKS)

VIVA

(10

MARKS)

TOTAL

INTERNAL

(50

MARKS)

EXPERIMENT

(10 MARKS)

FILE

WORK

(10

MARKS)

VIVA

(10

MARKS)

External Evaluation (50 marks)

The external evaluation would also be done by the external Examiner based on the experiment

conducted during the examination.

EXPERIMENT

(20 MARKS)

FILE WORK

(10 MARKS) VIVA

(20 MARKS) TOTAL EXTERNAL

(50 MARKS)

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M.Sc. Chemistry IInd Year : IIIrd Semester

Minor Research Project and Seminar

Course code MCH- 391 L T P C

0 0 4 2

For students to enter into preliminary research field both in theory and experiment the concept of

Project has been introduced in the final Semester. In the Project the student will explore new

developments from the books and journals, collecting literature / data and write a Dissertation

based on his / her work and studies. The Project Work can also be based on experimental work in

industries / research laboratories.

Selection of Topic:

1. Students will make project which should be preferably a working of third thoughts based on

their subject.

2. The student will be assigned a faculty guide who good the supervisor of the students. The

faculty would be identified before the end of the III semester.

3. The assessment of performance of the students should be made at least twice in the

semester. Internal assessment shall be for 250 marks. The students shall present the final

project live using overhead projector PowerPoint presentation on LCD to the internal

committee and the external examiner.

4. The evaluation committee shall consists of faculty members constituted by the college

which would be comprised of at least three members comprising of the department

Coordinator’s Class Coordinator and a nominee of the Dirtier. The students guide would be

special in bitted to the presentation. The seminar session shall be an open house session. The

internal marks would be the average of the marks given by each members of the committee

separately to the director in a sealed envelope.

The Marking shall be as follows.

Internal : 50 marks

By the Faculty Guide – 25 marks

By Committee appointed by the Director – 25 marks

External : 50 marks

By External examiner by the University – 50

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Seminar

Selection of Topic:

1. All students pursuing M.Sc. shall select and propose a topic of the seminar in the first

week of the semester. Care should be taken that the topic selected is not directly related

to the subjects of the course being pursued or thesis work, if any. The proposed topic

should be submitted to the course coordinator.

2. The course coordinator shall forward the list of the topics to the coordinator of concerned

department, who will consolidate the list including some more topics, in consultation

with the faculty of the department. The topics will then be allocated to the students along

with the name of the faculty guide and also forwarded to the director for approval.

3. On approval by the Director, the list shall be displayed on the notice board and the

students will also be accordingly informed by the course coordinator within three weeks

of the commencement of the semester.

Preparation of the Seminar:

1. The student shall meet the guide for the necessary guidance for their preparation for the

seminar.

2. During the next two to four weeks the student will read the primary literature related to

the topic under the guidance of supervisor.

3. After necessary collection of data and literature survey, the students must prepare a

report. The report shall be arranged in the sequence as per following format & lay out

plan :-

a. Top Sheet of transparent plastic.

b. Top cover.

c. Preliminary pages.

(i) Title page

(ii) Certification page.

(iii) Acknowledgment.

(iv) Abstract.

(v) Table of Content.

(vi) List of Figures and Tables.

(vii) Nomenclature.

d. Chapters (Main Material).

e. Appendices, If any.

f. Bibliography/ References.

g. Evaluation Form.

h. Back Cover (Blank sheet).

i. Back Sheet of Plastic (May be opaque or transparent).

a. Top Cover- The sample top cover shall be as Under:

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TITLE OF THE SEMINAR

NAME OF THE STUDENT WITH COURSE, STREAM, SEMESTER & SECTION.

Department of Applied Science

College of Engineering

Teerthanker Mahaveer University

Moradabad-244001

MONTH AND YEAR

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b. Title Page:- The Title Page cover shall be as Under:

Title of the seminar

(Submitted in Partial fulfillment of the requirement for the degree of

BACHELOR OF SCIENCE

in

Chemistry

by

Name of Student in capital Letters

(Roll No.)

College of Engineering

Teerthanker Mahaveer University

Moradabad-244001

MONTH AND YEAR

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c. Certification page:- This shall be as under

Department of Applied Science

College of Engineering

Teerthankar Mahaveer University

Moradabad-244001

The seminar Report and Title “Name of the Topic of the Seminar.” Submitted by Mr./Ms.

(Name of the student) (Roll No.) may be accepted for being evaluated-

Date Signature

Place (Name of guide)

Note:

For Guide: If you choose not to sign the acceptance certificate above, please indicate reasons

for the same from amongst those given below:

i) The amount of time and effort put in by the student is not sufficient;

ii) The amount of work put in by the student is not adequate;

iii) The report does not represent the actual work that was done / expected to be done;

iv) Any other objection (Please elaborate)

d. Abstract:- A portion of the seminar grade will be based on the abstract. The abstract will be

graded according to the adherence to accepted principles of English grammar and according to

the adherence to the format described below.

The seminar abstract is an important record of the coverage of your topic and provides a valuable

source of leading references for students and faculty alike. Accordingly, the abstract must serve

as an introduction to your seminar topic. It will include the key hypotheses, the major scientific

findings and a brief conclusion. The abstract will be limited to 500 words, excluding figures,

tables and references. The abstract will include references to the research articles upon which

the seminar is based as well as research articles that have served as key background material.

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(e). Table of Content:- This shall be as under

SAMPLE SHEET FOR TABLE OF CONTENTS

TABLE OF CONTENTS

Chapter No Title Page No.

Certificate ii

Abstract iii

Acknowledgement iv

List of Figures v

List of Table vi

1 Introduction 1

1.1

1.2

1.3

2 …………………..

3 …………………..

4 References/Bibliography

5 Evaluation sheets ……..

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f. List of Figures and Tables :- This will be as under

List of Figures and Tables - sample entries are given below:

List of Figures

Figure No. Caption / Title Page

No.

2.1 Schematic representation of a double layered droplet . . . 21

…………..

3.2 Variation in rate versus concentration . . . 32

List of Tables - sample entries are given below:

List of Tables

Table No. Caption / Title Page

No.

2.1 Thickness of a double layered droplet . . . 22

…………….

3.2 Variation in rate versus concentration . . . 34

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(g). Main Pages- The Main report should be divided in chapters (1, 2, 3 ….. etc.) and

structured into sections (1.1, 1.2 ……..etc) and subsections (1.2.1, 1.2.2, ….. etc).

Suitable title should be given for sections and subsections, where necessary.

Referencing style- wherever reference is given in the main pages it should have the

following format.

The values of thermal conductivities for a variety of substances have been reported by

Varma (1982). For polymers, however, the information is more limited and some recent

reviews have attempted to fill the gaps (Batchelor and Shah, 1985).

For two authors - (Batchelor and Kapur, 1985)

For more than two authors - (Batchelor et al., 1986)

By same author/combination of authors in the same year -

(Batchelor, 1978a; Batchelor, 1978b; Batchelor et al., 1978)

(h) Bibliography/References- In the bibliography/ references list standard formats must

be used. The typical formats are given blow-

Journal articles: -

David, A.B., Pandit, M.M. and Sinha, B.K., 1991, "Measurement of surface viscosity by

tensiometric methods", Chem. Engng Sci.47, 931-945.

Books: -

Doraiswamy, L.K. and Sharma, M.M., 1984, "Heterogeneous Reactions-Vol 1", Wiley,

New

York, pp 89-90.

Edited books/Compilations/Handbooks: -

Patel, A.B., 1989, "Liquid -liquid dispersions", in Dispersed Systems

Handbook, Hardy, L.C. and Jameson, P.B. (Eds.), McGraw Hill, Tokyo, pp 165-178.

Lynch, A.B. (Ed.), 1972, "Technical Writing", Prentice Hall, London.

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Theses/Dissertations: -

Pradhan, S.S., 1992, "Hydrodynamic and mass transfer characteristics of packed

extraction columns", Ph.D. Thesis, University of Manchester, Manchester, U.K..

Citations from abstracts: -

Lee, S. and Demlow, B.X., 1985, US Patent 5,657,543, Cf C.A. 56, 845674.

Personal Communications: -

Reddy, A.R., 1993, personal communication at private meeting on 22 October 1992 at

Physics Department, Indian Institute of Technology, Delhi.

Electronic sources (web material and the like)- For citing web pages and electronic

documents, use the APA style given at:

http://www.apastyle.org/elecsource.html

(I) Evaluation Form:- Three sheets of evaluation form should be attached in the

report as under.

a. Evaluation form for guide and other Internal Examiner.

b. Evaluation form for external examiners.

c. Summary Sheet.

(J). Evaluation form for Guide & Internal Examiners:-

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EVALUATION SHEET

(To be filled by the GUIDE & Internal Examiners only)

Name of Candidate:

Roll No:

Class and Section:

Please evaluate out of Five marks each.

S. No. Details Marks (5) Marks (5) Marks (5)

Guide Int. Exam.

1

Int. Exam.

2

1. OBJECTIVE IDENTIFIED &

UNDERSTOOD

2. LITERATURE REVIEW /

BACKGROUND WORK

(Coverage, Organization, Critical

review)

3. DISCUSSION/CONCLUSIONS

(Clarity, Exhaustive)

4. SLIDES/PRESENTATION

SUBMITTED

(Readable, Adequate)

5. FREQUENCY OF

INTERACTION ( Timely

submission, Interest shown, Depth,

Attitude)

Total (Out of 25)

Average out of 50

Signature: Signature: Signature:

Date: Date: Date:

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EVALUATION SHEET FOR EXTERNAL EXAMINER

(To be filled by the External Examiner only)

Name of Candidate:

Roll No:

I. For use by External Examiner ONLY

S.No. Details Marks (5)

1. OBJECTIVE IDENTIFIED & UNDERSTOOD

2. LITERATURE REVIEW / BACKGROUND

WORK

(Coverage, Organization, Critical review)

3. DISCUSSION/CONCLUSIONS

(Clarity, Exhaustive)

4. POWER POINT PRESENTATION

(Clear, Structured)

5. SLIDES

(Readable, Adequate)

Total (Out of 50)

Signature:

Date:

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EVALUATION SUMMARY SHEET

(To be filled by External Examiner)

Name and Roll

No.

Internal

Examiners

(50)

External

Examiner

(50)

Total (100)

Result

(Pass/Fail)

Note:- The summary sheet is to be completed for all students and the same shall also be

Compiled for all students examined by External Examiner. The Format shall be provided

by the course coordinator.

(K). General Points for the Seminar

1. The report should be typed on A4 sheet. The Paper should be of 70-90 GSM.

2. Each page should have minimum margins as under-

(i) Left 1.5 inches

(ii) Right 0.5 Inches

(iii) Top 1 Inch

(iv) Bottom 1 Inch (Excluding Footer, If any)

3. The printing should be only on one side of the paper

4. The font for normal text should Times New Roman, 14 size for text and 16 size for

heading

and should be typed in double space. The references may be printed in Italics or in a

different

fonts.

5. The Total Report should not exceed 50 pages including top cover and blank pages.

6. A CD of the report should be pasted/ attached on the bottom page of the report.

7. Similarly a hard copy of the presentation (Two slides per page) should be attached along

with the report and a soft copy be included in the CD.

8. Three copies completed in all respect as given above is to be submitted to the guide.

One copy will be kept in departmental/University Library, One will be return to the

student and third copy will be for the guide.

9. The power point presentation should not exceed 30 minutes which include 10 minutes

for discussion/Viva.

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M.Sc. Chemistry IInd Year : IVth Semester

Materials Chemistry Course Code MCH 401 L T P C

3 1 0 4

Unit I-Introduction (Lectures 08)

Materials and their classification, Role of Chemistry in Material design.

Unit II-Synthesis and Characterization of Materials (Lectures 08)

Preparative techniques: Ceramic methods; chemical strategies, chemical vapour deposition;

Preparation of nanomaterials; Langmuir-Blodgett Films; Fabrication of ordered nanostructures;

Composition and purity of materials.

Unit III-High- Tc Oxide Superconductors (Lectures 08)

Structural features of cuprate superconductors, 1-2-3 and 2-1-4 cuprates; Structure; Normal state

properties: anisotropy and temperature dependence of electrical resistance; Superconducting

state: heat, capacity, coherence, length, Relation between Tc and hole concentration in cuprates;

mechanism of superconductivity in cuprates; Applications of high Tc-cuprates.

Unit IV-Organic Materials (Lectures 08)

Conducting organics - Metals from molecules; Charge transfer materials and conducting

polymers; Organic superconductors; Fullerenes; Molecular ferromagnets and ferroelectrics;

Liquid crystals: mesomorphic behavior; Optical properties of liquid crystals; Display devices.

Unit V-Non-linear materials (Lectures 08)

Second and third order non-linear effects; molecular rectifiers and frequency doublers;

Unimolecular electronic devices; Photo-chromic materials; Optical data storage; memory and

switches.

Books Recommended

1.A.R. West, Solid State Chemistry and its Applications, John Wiley & Sons, Singapore (1984)

2.C.N R. Rao and J. Gopalkrishnan, New Directions in Solid State Chemistry, Cambridge Univ.

Press (1997).

3.T. V. Ramakrishnan and C.N. Rao, Superconductivity Today, Wiley Eastern Ltd., New Delhi

(1992).

4.P. Ball, Designing the Molecular World: Chemistry at the Frontier, Princeton Univ. Press,

(1994).

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M.Sc. Chemistry IInd Year : IVth Semester

Computer Applications in Chemistry

Course Code MCH 402 L T P C

3 1 0 4

Unit I-Fortran 77 (Lectures 08)

Types of Constants and Variables in Fortran; Dimension; Data; Type; COMMON and

EQUIVALENCE statements; Arithmetic and Logical IF; IF-THEN-ELSE Constructs; DO

statement; Various types of I/O statements; Library functions; Statement functions; Function

Subprograms and subroutine subprograms.

Unit II-Numerical Methods (Lectures 08)

Roots of Polynomials; Solution of Linear simultaneous equations; Matrix multiplication and

inversion; Numerical integration; Statistical treatment of data; Variance and Correlations.

Unit III-Solution of systems of linear equations (Lectures 08)

Direct method; Gauss Jordan and Gauss Elimination methods; Iterative methods – Jacobi and

Gauss Seidel methods; Iterative Methods: Zeros of a single transcendental equation and zeros of

polynomial using Bisection Method; Iteration Method.

Unit IV (Lectures 08)

Regula-Falsi method; Newton Raphson method; Secant method, Rate of convergence of iterative

methods; Runge-Kutta methods; Predictor-corrector method; Automatic error monitoring;

Stability of solution; Euler’s Method; Taylor’s Method.

Unit V (Lectures 08)

Numerical Differentiation and Integration: Introduction, Numerical Differentiation, Numerical

Integration; Trapezoidal rule; Simpson’s rules; Boole’s Rule; Weddle’s Rule Euler- Maclaurin

Formula; Solution of differential equations: Picard’s Method.

Recommended Books

1. V. Rajaraman, Fortran 77, Prentice Hall (India), New Delhi.

2. C. Xavier, Fortran 77 and Numerical Methods, New Age International Pvt. Ltd. Publishers,

New Delhi

3. S. Lipschutz and A. Poe, Schaum’s Outline Series – Theory and Problems of Programming

with Fortran Including structured Fortran, Mc Graw Hill Book Company, Singapore

4. K. V. Raman, Computers in Chemistry, Tata McGraw Hill (1993).

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M.Sc. Chemistry IInd Year : IVth Semester

Project work, Seminar & Viva

Course code: MCH- 491 L T P C

0 0 20 10

For students to enter into preliminary research field both in theory and experiment the concept of

Project has been introduced in the final Semester. In the Project the student will explore new

developments from the books and journals, collecting literature / data and write a Dissertation

based on his / her work and studies. The Project Work can also be based on experimental work in

industries / research laboratories.

Selection of Topic:

5. Students will make project which should be preferably a working of third thoughts based on

their subject.

6. The student will be assigned a faculty guide who good the supervisor of the students. The

faculty would be identified before the end of the III semester.

7. The assessment of performance of the students should be made at least twice in the

semester. Internal assessment shall be for 250 marks. The students shall present the final

project live using overhead projector PowerPoint presentation on LCD to the internal

committee and the external examiner.

8. The evaluation committee shall consists of faculty members constituted by the college

which would be comprised of at least three members comprising of the department

Coordinator’s Class Coordinator and a nominee of the Dirtier. The students guide would be

special in bitted to the presentation. The seminar session shall be an open house session. The

internal marks would be the average of the marks given by each members of the committee

separately to the director in a sealed envelope.

The Marking shall be as follows.

Internal : 50 marks

By the Faculty Guide – 25 marks

By Committee appointed by the Director – 25 marks

External : 50 marks

By External examiner by the University – 50

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Seminar

Selection of Topic:

4. All students pursuing M.Sc. shall select and propose a topic of the seminar in the first

week of the semester. Care should be taken that the topic selected is not directly related

to the subjects of the course being pursued or thesis work, if any. The proposed topic

should be submitted to the course coordinator.

5. The course coordinator shall forward the list of the topics to the coordinator of concerned

department, who will consolidate the list including some more topics, in consultation

with the faculty of the department. The topics will then be allocated to the students along

with the name of the faculty guide and also forwarded to the director for approval.

6. On approval by the Director, the list shall be displayed on the notice board and the

students will also be accordingly informed by the course coordinator within three weeks

of the commencement of the semester.

Preparation of the Seminar:

4. The student shall meet the guide for the necessary guidance for their preparation for the

seminar.

5. During the next two to four weeks the student will read the primary literature related to

the topic under the guidance of supervisor.

6. After necessary collection of data and literature survey, the students must prepare a

report. The report shall be arranged in the sequence as per following format & lay out

plan :-

a. Top Sheet of transparent plastic.

b. Top cover.

c. Preliminary pages.

(i) Title page

(ii) Certification page.

(iii) Acknowledgment.

(iv) Abstract.

(v) Table of Content.

(vi) List of Figures and Tables.

(vii) Nomenclature.

d. Chapters (Main Material).

e. Appendices, If any.

f. Bibliography/ References.

g. Evaluation Form.

h. Back Cover (Blank sheet).

i. Back Sheet of Plastic (May be opaque or transparent).

a. Top Cover- The sample top cover shall be as Under:

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TITLE OF THE SEMINAR

NAME OF THE STUDENT WITH COURSE, STREAM, SEMESTER & SECTION.

Department of Applied Science

College of Engineering

Teerthanker Mahaveer University

Moradabad-244001

MONTH AND YEAR

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b. Title Page:- The Title Page cover shall be as Under:

Title of the seminar

(Submitted in Partial fulfillment of the requirement for the degree of

BACHELOR OF SCIENCE

in

Chemistry

by

Name of Student in capital Letters

(Roll No.)

College of Engineering

Teerthanker Mahaveer University

Moradabad-244001

MONTH AND YEAR

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c. Certification page:- This shall be as under

Department of Applied Science

College of Engineering

Teerthankar Mahaveer University

Moradabad-244001

The seminar Report and Title “Name of the Topic of the Seminar.” Submitted by Mr./Ms.

(Name of the student) (Roll No.) may be accepted for being evaluated-

Date Signature

Place (Name of guide)

Note:

For Guide: If you choose not to sign the acceptance certificate above, please indicate reasons

for the same from amongst those given below:

i) The amount of time and effort put in by the student is not sufficient;

ii) The amount of work put in by the student is not adequate;

iii) The report does not represent the actual work that was done / expected to be done;

iv) Any other objection (Please elaborate)

d. Abstract:- A portion of the seminar grade will be based on the abstract. The abstract will be

graded according to the adherence to accepted principles of English grammar and according to

the adherence to the format described below.

The seminar abstract is an important record of the coverage of your topic and provides a valuable

source of leading references for students and faculty alike. Accordingly, the abstract must serve

as an introduction to your seminar topic. It will include the key hypotheses, the major scientific

findings and a brief conclusion. The abstract will be limited to 500 words, excluding figures,

tables and references. The abstract will include references to the research articles upon which

the seminar is based as well as research articles that have served as key background material.

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(e). Table of Content:- This shall be as under

SAMPLE SHEET FOR TABLE OF CONTENTS

TABLE OF CONTENTS

Chapter No Title Page No.

Certificate ii

Abstract iii

Acknowledgement iv

List of Figures v

List of Table vi

1 Introduction 1

1.1

1.2

1.3

2 …………………..

3 …………………..

4 References/Bibliography

5 Evaluation sheets ……..

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f. List of Figures and Tables :- This will be as under

List of Figures and Tables - sample entries are given below:

List of Figures

Figure No. Caption / Title Page

No.

2.1 Schematic representation of a double layered droplet . . . 21

…………..

3.2 Variation in rate versus concentration . . . 32

List of Tables - sample entries are given below:

List of Tables

Table No. Caption / Title Page

No.

2.1 Thickness of a double layered droplet . . . 22

…………….

3.2 Variation in rate versus concentration . . . 34

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(g). Main Pages- The Main report should be divided in chapters (1, 2, 3 ….. etc.) and

structured into sections (1.1, 1.2 ……..etc) and subsections (1.2.1, 1.2.2, ….. etc).

Suitable title should be given for sections and subsections, where necessary.

Referencing style- wherever reference is given in the main pages it should have the

following format.

The values of thermal conductivities for a variety of substances have been reported by

Varma (1982). For polymers, however, the information is more limited and some recent

reviews have attempted to fill the gaps (Batchelor and Shah, 1985).

For two authors - (Batchelor and Kapur, 1985)

For more than two authors - (Batchelor et al., 1986)

By same author/combination of authors in the same year -

(Batchelor, 1978a; Batchelor, 1978b; Batchelor et al., 1978)

(h) Bibliography/References- In the bibliography/ references list standard formats must

be used. The typical formats are given blow-

Journal articles: -

David, A.B., Pandit, M.M. and Sinha, B.K., 1991, "Measurement of surface viscosity by

tensiometric methods", Chem. Engng Sci.47, 931-945.

Books: -

Doraiswamy, L.K. and Sharma, M.M., 1984, "Heterogeneous Reactions-Vol 1", Wiley,

New

York, pp 89-90.

Edited books/Compilations/Handbooks: -

Patel, A.B., 1989, "Liquid -liquid dispersions", in Dispersed Systems

Handbook, Hardy, L.C. and Jameson, P.B. (Eds.), McGraw Hill, Tokyo, pp 165-178.

Lynch, A.B. (Ed.), 1972, "Technical Writing", Prentice Hall, London.

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Theses/Dissertations: -

Pradhan, S.S., 1992, "Hydrodynamic and mass transfer characteristics of packed

extraction columns", Ph.D. Thesis, University of Manchester, Manchester, U.K..

Citations from abstracts: -

Lee, S. and Demlow, B.X., 1985, US Patent 5,657,543, Cf C.A. 56, 845674.

Personal Communications: -

Reddy, A.R., 1993, personal communication at private meeting on 22 October 1992 at

Physics Department, Indian Institute of Technology, Delhi.

Electronic sources (web material and the like)- For citing web pages and electronic

documents, use the APA style given at:

http://www.apastyle.org/elecsource.html

(II) Evaluation Form:- Three sheets of evaluation form should be attached in the

report as under.

a. Evaluation form for guide and other Internal Examiner.

b. Evaluation form for external examiners.

c. Summary Sheet.

(J). Evaluation form for Guide & Internal Examiners:-

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EVALUATION SHEET

(To be filled by the GUIDE & Internal Examiners only)

Name of Candidate:

Roll No:

Class and Section:

Please evaluate out of Five marks each.

S. No. Details Marks (5) Marks (5) Marks (5)

Guide Int. Exam.

1

Int. Exam.

2

1. OBJECTIVE IDENTIFIED &

UNDERSTOOD

2. LITERATURE REVIEW /

BACKGROUND WORK

(Coverage, Organization, Critical

review)

3. DISCUSSION/CONCLUSIONS

(Clarity, Exhaustive)

4. SLIDES/PRESENTATION

SUBMITTED

(Readable, Adequate)

5. FREQUENCY OF

INTERACTION ( Timely

submission, Interest shown, Depth,

Attitude)

Total (Out of 25)

Average out of 50

Signature: Signature: Signature:

Date: Date: Date:

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EVALUATION SHEET FOR EXTERNAL EXAMINER

(To be filled by the External Examiner only)

Name of Candidate:

Roll No:

I. For use by External Examiner ONLY

S.No. Details Marks (5)

1. OBJECTIVE IDENTIFIED & UNDERSTOOD

2. LITERATURE REVIEW / BACKGROUND

WORK

(Coverage, Organization, Critical review)

3. DISCUSSION/CONCLUSIONS

(Clarity, Exhaustive)

4. POWER POINT PRESENTATION

(Clear, Structured)

5. SLIDES

(Readable, Adequate)

Total (Out of 50)

Signature:

Date:

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EVALUATION SUMMARY SHEET

(To be filled by External Examiner)

Name and Roll

No.

Internal

Examiners

(50)

External

Examiner

(50)

Total (100)

Result

(Pass/Fail)

Note:- The summary sheet is to be completed for all students and the same shall also be

Compiled for all students examined by External Examiner. The Format shall be provided

by the course coordinator.

(K). General Points for the Seminar

1. The report should be typed on A4 sheet. The Paper should be of 70-90 GSM.

2. Each page should have minimum margins as under-

(i) Left 1.5 inches

(ii) Right 0.5 Inches

(iii) Top 1 Inch

(iv) Bottom 1 Inch (Excluding Footer, If any)

3. The printing should be only on one side of the paper

4. The font for normal text should Times New Roman, 14 size for text and 16 size for

heading

and should be typed in double space. The references may be printed in Italics or in a

different

fonts.

5. The Total Report should not exceed 50 pages including top cover and blank pages.

6. A CD of the report should be pasted/ attached on the bottom page of the report.

7. Similarly a hard copy of the presentation (Two slides per page) should be attached along

with the report and a soft copy be included in the CD.

8. Three copies completed in all respect as given above is to be submitted to the guide.

One copy will be kept in departmental/University Library, One will be return to the

student and third copy will be for the guide.

9. The power point presentation should not exceed 30 minutes which include 10 minutes

for discussion/Viva.

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Viva- voce

Students will prepare the viva, which should be based on their subject.

The student will be assigned a faculty guide who good the supervisor of the students. The

faculty would be identified before the end of the III semester. The faculty will take the full

responsibility for preparing the viva to the students.

The evaluation committee shall consists of faculty members constituted by the college which

would be comprised of at least three members comprising of the department Coordinator’s

Class Coordinator and a nominee of the Director. The students guide would be special invitee to

the viva. The viva session shall be an open house session. The internal marks would be the

average of the marks given by each members of the committee in a sealed envelope.