multiple stress creep recovery (mscr) testing · accumulated strain testing new test procedure to...

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Multiple Stress Creep Recovery (MSCR) testing anand tadas ph.d Malvern Aimil Instruments

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Page 1: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Multiple Stress Creep Recovery (MSCR) testing

anand tadas ph.d

Malvern Aimil Instruments

Page 2: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Multiple Stress Creep Recovery AASHTO TP-70

DSR performing MSCR Identifies beneficial elastic properties.

� Rutting Performance

• Direct measure of Non Recoverable Compliance (Jnr)

• Goal is quantify the non-linear performance of the binder to predict

Rutting Performance.

• 100Pa is in the linear region (expected behavior)

• 3200Pa is in the non-linear region (extreme movement)

Page 3: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Multiple Stress Creep Recovery AASHTO TP-70

DSR performing MSCR Identifies beneficial elastic properties.

� Rutting Performance

• Direct measure of Non Recoverable Compliance (Jnr)

• Goal is quantify the non-linear performance of the binder to predict Rutting Performance.

• Modulus (G*) = Stress/Strain

• Compliance (J*) = Strain/Stress or 1/G*

Page 4: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Multiple Stress Creep Recovery

MSCR Identifies beneficial elastic properties.

� (2 tests in 1)

� Rutting Performance

• Direct measure of Non RecoverableNon Recoverable Compliance

• Goal is quantify the non-linear performance of the binder to predict

Rutting Performance. (Jnr)

� Elastic Recovery Performance

• Direct measure of RecoverableRecoverable Compliance

• Goal is investigate differences in linear & non-linear performance

of the binder (% Recovery)

Page 5: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

What Causes Rutting ?

Tire load applied for a short time; pavement

permitted to recover for a

longer time; over & over & over & over ………….

Page 6: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Simulate pavement loading over many cycles.

Load force applied for 1s and removed to permit binder to relax for 9s for each cycle.

If the binder has any elastic behavior, it can be directly measured in the relaxation part of the cycle.

Accumulated permanent deformation is a measure of the accumulated strain.

� Non recoverable compliance (Jnr)

For Rutting: Accumulated Strain

Page 7: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Accumulated Strain Testing

New test procedure to evaluate binders on a DSR

Loading = Stress On for 1 sec & Stress Off for 9 sec0.0

0.2

0.4

0.6

0.8

1.0

0 2.5 5 7.5 10

time, s

Norm

aliz

ed S

train

γγγγacc Unmodified Binder

γγγγacc Modified Binder

0.0

0.2

0.4

0.6

0.8

1.0

0 2.5 5 7.5 10

time, s

Norm

aliz

ed S

train

γγγγacc Unmodified Binder

γγγγacc Modified Binder

Str

ain

Page 8: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Linear & Non-Linear Applied Stress Loading

Page 9: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Accumulated Strain from Repeated Loading

Page 10: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Accumulated Strain from Repeated Loading on a Modified Binder

Page 11: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Example of a Visco-Elastic Binder

Modified binder PG70-28 tested to MSCR at 70oC

100Pa

3200Pa

Jnr3200

Jnr100

J* Creep Compliance

Page 12: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Example of a Newtonian material

Neat binder PG64-28 tested to MSCR at 64oC

Jnr3200

Jnr100

Page 13: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

MSCR Results

Page 14: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

MSCR Analysis

Page 15: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Passing Jnr Values for MSCR

All testing is at the environmental use temperature

PG 64-28S or PG 64-28H or PG 64-28V

� S: Standard Grade = 4

� H: Heavy Grade = 2

� V: Very Heavy Grade = 1

� E: Extremely Heavy Grade = 0.5 (special applications)

Page 16: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

AASHTO MP-19A New Spec Much Like M-320

Original

DSR G*/sinδ

Min 1.064

RTFOT

64 Standard

MSCR3.2 <4.064

64 Heavy

MSCR 3.2<2.064

64 Very heavy

MSCR3.2 <1.064

PAV

S grade

DSR G*sinδ

Max 5000

28 25 22 19 16

H & V grade DSR G*sinδ Max

6000

28 25 22 19 16

Low temp BBR and DTT remain unchanged

Page 17: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

What’s Really Going On?

Jnr

Jr

J*Creep Compliance

Recoverable Compliance

Non Recoverable Compliance

Page 18: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

How Does It Relate To % Recovery

Total Movement

What you get back

What you loose

Page 19: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

How Does It Relate To % Recovery

20%

80%

100%Total Movement is always 100%

% Recovery

% Non Recoverable

Page 20: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

% Recovery

Tested at Environmental Temp vs. Elastic Recovery (ER) at 25C.

Relates to ‘Good’ Elastic Recovery Performance.

Data is Free. You get it from TP-70

Page 21: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Common Problem

Some report negative (-) Recovery values

� Generally due to low G* samples or samples with very little elastic behavior.

Solution:

� Test at lower temperatures, if possible.

� Increase amount of modification to improve elastic contribution in the measurement.

� Test on an instrument with low instrumental inertia.

Page 22: Multiple Stress Creep Recovery (MSCR) testing · Accumulated Strain Testing New test procedure to evaluate binders on a DSR Loading = Stress On for 1 sec & Stress Off for 9 se 0.0

Thank you for your Time!

Questions ?

[email protected]

(m) +91-9980934852