name: junyong zhu (updated on june 1, 2016) junyong (j.y.) zhu › pdf › 1192553.pdf · name:...

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Name: Junyong ZHU (updated on June 1, 2016) 1 JunYong (J.Y.) ZHU Phone: 050 567 9974 E-Mail: [email protected], [email protected], [email protected] ________________________________________________________ PERSONAL PROFILE Dr. J.Y. Zhu is a scientific team leader in woody biomass utilization for sugar/biofuel, chemicals, fiber, and cellulose nanomaterials production at the US Forest Service, Forest Products Laboratory (the only U.S. National Lab in Wood Utilization), Madison, Wisconsin. He holds an Adjunct Professorship at the Dept. of Biological Systems Engineering, University of Wisconsin-Madison. Currently, he is the Fulbright-Aalto University Distinguished Chair in Energy and Sustainable Use Natural Resources, Aalto University, Helsinki, Finland. His research is well recognized by the scientific community around the world and was selected as an Exemplary R&D by US Dept. Agriculture in 2011. Dr. Zhu’s achievements were honored with US Forest Service Deputy Chief for R&D Distinguished Science Award in 2013 and TAPPI R&D Technical Award and William H. Aiken Prize in 2014. Dr. Zhu served on various international panels including the Canadian National Science and Engineering Research Council (NSERC) research program (2006), the Austrian Science Fund (FWF)’s Special long term (8 year) Research Program on biobased resources (2014). He was also invited as an International Expert to speak at the Workshop on Second Generation Ethanol at the Brazilian National Ethanol Science and Technology Laboratory (CTBE), Campinas, Brazil, in 2014. Dr. Zhu serves on the editorial boards of several technical journals, including TAPPI Journal (also a Technical Editor), BioEnergy Research (also an Associate Editor), BioResources, China Pulp and Paper. Dr. Zhu is an elected fellow of the International Academy of Wood Science (IAWS), and Fellow of TAPPI. He is also the Vice Chair of Forest Plant and Bioproducts Division of the American Institute of Chemical Engineers (AIChE). EXPERIENCES and RESEARECHG PROJECTS USDA Forest Service, Forest Products Laboratory, Madison, Wisconsin Scientific Leader, Project Leader February, 2003 Present Direct a group of scientists and engineers in key areas of research related to advancing the science and engineering supporting forest biorefinery for biofuel production, and conservation in wood and fiber utilization. Active Research Programs: Biological and chemical deconstruction of woody biomass cell wall for the productions of sugar/biofuel and bioproducts (including nanocellulose) through enzymatic hydrolysis and fermentation. Biorefinery process integration to achieve low inputs of water and energy and high economic output. Production of cellulose nanocrystals (CNC) and nanofibrills (CNF) through chemical, biological and mechanical means. Characterization of optical, mechanical, and chemical properties of CNC and CNF. Fundamentals of nano-scale structure and activities associated with enzyme access to lignocelluloses. Fundamental properties of wood fibers and biomass resources. Fundamentals of chemical and biological reaction flows of bubbles, particles, and fibers suspensions Key accomplishments: Led a group of scientists and staff to develop a biomass fractionation program for biorethanol production with significant government and industrial funding. Co-Invented a sulfite pretreatment process (SPORL) for robust and bioconversion of forest biomass, demonstrated at pre-commercial-scale to produce 10000 gallon bio-jet. Developed a process to reduce size-reduction energy consumption for biomass substrate production by a factor of 10. Effectively removed barriers for woody biomass to compete with agricultural biomass. Developed a wet image technique for accurately characterize biomass substrate size. Led a group of scientist to develop an environmental friendly and energy efficient process for integrated production of cellulose nanofibrills (CNF) with sugar/biofuel with major funding.

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Page 1: Name: Junyong ZHU (updated on June 1, 2016) JunYong (J.Y.) ZHU › pdf › 1192553.pdf · Name: Junyong ZHU (updated on June 1, 2016) 2 Developed a process to integrate the production

Name: Junyong ZHU (updated on June 1, 2016)

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JunYong (J.Y.) ZHU

Phone: 050 567 9974 E-Mail: [email protected], [email protected], [email protected]

________________________________________________________ PERSONAL PROFILE

Dr. J.Y. Zhu is a scientific team leader in woody biomass utilization for sugar/biofuel, chemicals, fiber, and

cellulose nanomaterials production at the US Forest Service, Forest Products Laboratory (the only U.S. National Lab

in Wood Utilization), Madison, Wisconsin. He holds an Adjunct Professorship at the Dept. of Biological Systems

Engineering, University of Wisconsin-Madison. Currently, he is the Fulbright-Aalto University Distinguished Chair

in Energy and Sustainable Use Natural Resources, Aalto University, Helsinki, Finland. His research is well

recognized by the scientific community around the world and was selected as an Exemplary R&D by US Dept.

Agriculture in 2011. Dr. Zhu’s achievements were honored with US Forest Service Deputy Chief for R&D

Distinguished Science Award in 2013 and TAPPI R&D Technical Award and William H. Aiken Prize in 2014.

Dr. Zhu served on various international panels including the Canadian National Science and Engineering Research

Council (NSERC) research program (2006), the Austrian Science Fund (FWF)’s Special long term (8 year) Research

Program on biobased resources (2014). He was also invited as an International Expert to speak at the Workshop on

Second Generation Ethanol at the Brazilian National Ethanol Science and Technology Laboratory (CTBE),

Campinas, Brazil, in 2014. Dr. Zhu serves on the editorial boards of several technical journals, including TAPPI

Journal (also a Technical Editor), BioEnergy Research (also an Associate Editor), BioResources, China Pulp and

Paper. Dr. Zhu is an elected fellow of the International Academy of Wood Science (IAWS), and Fellow of TAPPI. He

is also the Vice Chair of Forest Plant and Bioproducts Division of the American Institute of Chemical Engineers

(AIChE).

EXPERIENCES and RESEARECHG PROJECTS

USDA Forest Service, Forest Products Laboratory, Madison, Wisconsin

Scientific Leader, Project Leader February, 2003 – Present

Direct a group of scientists and engineers in key areas of research related to advancing the science and engineering supporting forest biorefinery for biofuel production, and conservation in wood and fiber utilization.

Active Research Programs:

Biological and chemical deconstruction of woody biomass cell wall for the productions of sugar/biofuel and bioproducts (including nanocellulose) through enzymatic hydrolysis and fermentation.

Biorefinery process integration to achieve low inputs of water and energy and high economic output.

Production of cellulose nanocrystals (CNC) and nanofibrills (CNF) through chemical, biological and mechanical means. Characterization of optical, mechanical, and chemical properties of CNC and CNF.

Fundamentals of nano-scale structure and activities associated with enzyme access to lignocelluloses.

Fundamental properties of wood fibers and biomass resources.

Fundamentals of chemical and biological reaction flows of bubbles, particles, and fibers suspensions

Key accomplishments:

Led a group of scientists and staff to develop a biomass fractionation program for biorethanol production with significant government and industrial funding. Co-Invented a sulfite pretreatment process (SPORL) for robust and bioconversion of forest biomass, demonstrated at pre-commercial-scale to produce 10000 gallon bio-jet.

Developed a process to reduce size-reduction energy consumption for biomass substrate production by a factor of 10. Effectively removed barriers for woody biomass to compete with agricultural biomass. Developed a wet image technique for accurately characterize biomass substrate size.

Led a group of scientist to develop an environmental friendly and energy efficient process for integrated production of cellulose nanofibrills (CNF) with sugar/biofuel with major funding.

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Name: Junyong ZHU (updated on June 1, 2016)

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Developed a process to integrate the production of cellulose nanocrystalls (CNC) with CNF to significantly reduce CNC production cost through increased yield, full chemical recovery, and enhanced functionality and mechanical thermal properties.

Identified the unique uniformity in anatomical properties of wood trachieds of suppressed growth trees.

Led a team of a university, a pulp mill (800 ton pulp/day), a logging company, two US Forest Service Research Stations, and a National Forest and carried out thinning operation, pulp mill commercial demonstration. The project proved the benefits of the unique uniformity of small diameters in National Forests for thermomechanical pulp production.

Developed fundamental understanding of the drainage of fiber laden froth and fiber fractionation with the froth during froth flotation to reduce fiber loss in flotation deinking. Invented a conductivity probe for solid and liquid content measurements in a solid laden froth to monitor fiber loss in flotation deinking.

Demonstrated a novel flotation deinking technology (co-invented during previous employment) for significant reduction of fiber loss and brightness gain in a commercial paper recycling mill.

Institute of Paper Science and Technology (IPST, Now Georgia Institute of Technology), Atlanta, Georgia

Associate Professor July 1999 – February, 2003

Assistant Professor November 1993 – June, 1999

Main responsibilities: research, teaching, and academic service.

Key accomplishments:

Developed a research program for chemical processing of wood with focus on process monitoring and analysis of pulp properties and process liquor compositions. Several of our headspace gas chromatographic techniques are now widely used by international peers in chemical science.

Developed a research program in environmental air emission control in pulp mills with major research funding from the US Dept of Energy and the State of Georgia. Conducted several pulp mill trails.

Co-invented a novel flotation deinking technology (US patented) and received US Dept of Energy support to develop the technology.

Collaborated with Georgia Tech faculty members and developed an ink jet printing research program that received funding and Technical Excellence Award from the US National Textile Center.

Raised about $3 MM research grants in 12 different projects from industry and government agencies to support the research team.

Advised 11 graduate, and 3 undergraduate students to successful completion of their Masters (9), Ph.D degrees (2), and summer intern program in pulp and paper engineering. Directed and financially supported (through external grants) 10 postdoctoral research fellows.

Developed a new course: Optical technique for wood fiber science research. Taught Engineering Mathematics (2 years) and Transport Process (5 years).

Raised fund from several local companies, e.g., RockTenn, Callaway Chemicals, to sponsor a Distinguished Speaker’s Lecture Series of half dozen world-renowned speakers.

Consulted dozens of industry problems for Georgia Pacific, Weyerhaeuser and resulted in savings over $10M for the two companies.

CURRENT ACADEMIC APPOINTMENT

Fulbright-Aalto University Chair, Dept. of Forest Products Technologies, Aalto University, Espoo, Finland

Adjunct Professor, Dept. Biological Systems Eng., University of Wisconsin-Madison, WI

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AWARDS and HONORS

TAPPI J. 2015 Best Research Paper Award, Technical Association of the Pulp and Paper Industry (TAPPI), 2016

Fulbright-Aalto University Distinguished Chair (2015-2016) and Scholarship, The J. William Fulbright Foreign Scholarship Board, 2015

Employee of the Year –Technical, 2014, Greater Madison Area of Federal Agency Association (GMAFAA)

TAPPI International Research and Development Technical Award and William H. Aiken Prize, 2014, Technical Association of the Pulp and Paper Industry (TAPPI)

US Forest Service Deputy Chief for R&D’s Distinguished Science Award, 2013

USDA Exemplary R&D in Agriculture, Food, Nutrition, and Natural Resources, 2011

Scientific Excellence Award, National Textile Center, A University Research Consortium, 2002

President’s Award for Innovating and Engineering a Successful Surfactant Spray Deinking Technology, Institute of Paper Science and Technology, 1999.

Successful Story Project, US Dept. of Energy and American Forest and Paper Association, 1998.

PROFESSIONAL ACTIVITIES

Editorship: Technical Editor: TAPPI Journal 2009 – present Associate Editor: Frontiers in Bioenergy and Biofuels 2014 – present

Editorial Board: BioEnergy Research (also an Associate Editor) 2011 – present Editorial Board: J. Biobased Materials and Bioenergy 2010 – present Editorial Board: BioResources 2006 – present Editorial Board: China Pulp and Paper 2010 – present (Official scientific publication of the China Technical Association of the Paper Industry)

Societies: Fellow: IAWS (International Academy of Wood Science)

Fellow: TAPPI (Technical Association of the Pulp and Paper Industry)

Sr. Member: AIChE (American Institute of Chemical Engineers), Vice Chair of Forest Products Division

Member: ACS (American Chemical Society)

Member: MRS (Materials Research Society)

International Activities

1. Reviewer: Swiss National Science Foundation, 2015

2. Invited Panel Speaker at the Workshop on Second Generation Bioethanol-2014, Brazilian National Ethanol Science and Technology Laboratory (CTBE), Campinas, Brazil, Nov., 2014.

3. Member of the International Innovation Team at Dalian Institute of Chemical Physics, Chinese of Academy of Sciences, Oct, 2014 – present.

4. Opponent of a Ph.D dissertation defense at School of Chemical Technology, Aalto University, Espoo, Finland, Sep, 2014.

5. Expert Team Member for the International Organization for Standardization (ISO) TC 229 Nanotechnologies –Cellulose Nanomaterials Standard, June 2014 - present

6. Invited Inaugural Speaker: George Tsao Renewable Resource Forum, Tsinghua University, Beijing, China, June, 2014.

7. Reviewer: Austrian Science Fund (FWF), 2014

8. Invited Panel Speaker at NSERC Bioconversion Network Pretreatment Workshop, the Natural Science and Engineering Research Council (NSERC) of Canada, University of British Columbia, Vancouver, Canada, June, 2012

9. Member of an International Proposal Review Committee for International Center of Excellence in Biorefinery, Chilen Economic Development Agency (InnovaChile-CORFO), June, 2011

10. Panel Member of an International Site Visiting and Proposal Review Committee, the Natural Science and Engineering Research Council (NSERC) of Canada, University of British Columbia, Vancouver, Canada, November, 2006

11. Member of International Doctoral Dissertation Examination Committees

Monash University, Dept. of Chemical Engineering, Victoria, Australia,

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August, 2006; March, 2008

Aalto University, School of Chemical Technology, Espoo, Finland March, 2014; November, 2014

South China University of Technology, School Chemistry Chem. Eng., Guangzhou, China May 2014

Abo Academy University, School of Chemical Technology, Finland July 2016

University of Oulu, Faculty of Technology, Finland October 2014; September 2016

12. Conference Organizing Committee and Chairs

Co-Chair: Symposium on Nanocellulose Materials and Beyond—Nanoscience, Structures, Nanomanufacturing and Devices, MRS Fall Annual Meeting, Boston, 2015

Chair: Symposium on Cell Wall Deconstruction, ACS Spring 245 Annual Meeting, New Orleans, 2013

Chair: Symposium on Bioconversion of Lignocellulose to Fuel Ethanol, Chemicals and Materials, Pacifichem 2010, Hawaii, December, 2010

Chair: 6th Int. Symp. Moisture and Creep Effect on Paper, Board, and Containers, Madison, 2009 16th Int. Symp. Wood, Fiber, Pulping Chemistry (ISWFPC), TianJin, China, 2011

Referee for the Following Journals/Publications (total of 75+):

Advanced Materials Appl. Microbiology Biotechnol. J. Chromatography A

Scientific Report – Nature Fuel Int. J. Serv Technol. Manag.

Energy Environ. Sci. – RSC Process Biochemistry TAPPI J.

Green Chemistry – RSC Biomass and Bioenergy Forest Products Journal

RSC advances – RSC BioEnergy Research J. Polym Environ.

Soft Matters – RSC Biotechnology for Biofuels J. Biobased Materials Bioenergy

Progress Energy Combustion Sci. Colloids and Surfaces A Energies

ChemSusChem J. Colloid and Interface Sci Energy

Enzymes Microbial Technology Applied Energy The Combustion Symposiums

Bioresource Technology Appl. Biochemistry Biotechnology J. Biobased Materials Bioenergy

Biotechnol. Bioengineering Biotechnology Progress Annals of Forest Science

Critical Rev. Biotechnol. J. Ind. Microbiology Biotechnol. Wood and Fiber Science

Cellulose Chem. Eng. J. African Journal of Forestry

Biofuels, Bioproducts &

Biorefining – Biofpr

ASME Tran. J. Manufacturing

Science and Engineering

ASME Tran. J. Eng. Gas Turbine Power

Nano Letters – ACS Chemical Eng. Sci. African J. of Biotechnology

Environ Sci. and Technol.– ACS J. Chem. Technol Biotechnol Chemical Eng and Technology

J. Agri. Food Chemistry – ACS Biofuel Prog. Paper Recycling

Langmuir – ACS Holtzforschung BioResources

Analytical Chemistry – ACS Carbohydrate Polymers China Pulp and Paper

Ind. Eng. Chem. Res – ACS Environ. Prog. Sustainable Energy Pulp and Paper Canada

Energy and Fuel – ACS Ind. Crops Products J. Chilean Chemical Society

Biomacromolecules – ACS Powder Technology J Wood Chemistry Technology

ACS Applied Materials & Interfaces Separation Sci. and Technol. Cellulose Chemistry Technology

ACS Sustainable Chem. & Eng. Separation and Purification Tech J. Pulp Paper Sci.

Biotechnology Journal ASABE J. ASME Tran. J. Fluids Eng.

J. Biotechnology ASTM J Testing & Evaluation AIAA J. of Propulsion

Waste and Biomass Valorization

No. paper reviewed 40 47 38 51 45 18

Year 2011 2012 2013 2014 2015 2016(YTD)

EDUCATION

Ph.D in Engineering, University of California, Irvine, California

MSc. in Mechanical Engineering, Arizona State University, Tempe, Arizona

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B.Sc. in Thermal Power Engineering, Beijing Institute Aeronautics Astronautics, Beijing, China

PATENTS and REFEREED PUBLICATIONS

Selected Patents (since 2011 only):

1. Vahey, D.W., Zhu, J.Y., Scott, T.C., “Method for Characterizing the Density and Cross-section morphology of trees,” U.S. Patent No. 7, 945, 098 B2 (2011)

2. Zhu, J.Y., Reiner, R., “Methods for Integrating the Production of Cellulose Nanofibrils with the production of Cellulose Nanocrystals” U.S. Patent No. 8, 710,213 B2 (2014)

3. Liu, H., and Zhu, J.Y., “Metal Compounds to Eliminate Nonproductive Enzyme Adsorption and Enhance Enzymatic Saccharification of Lignocelluloses”, Filed by Wisconsin Alumni Research Foundation (WARF) U.S. Patent No. 8, 815,561 B2 (2014)

4. Zhu, J.Y., Sabo, R., and Clemons, C.M., “Methods for Integrated Conversion of Lignocellulosic Material to Sugars/Biofuels and Nanocellulose” U.S. Patent No. 8, 835,141 B2 (2014)

5. Zhu, J.Y., “Reducing Non-specific Enzyme Binding to Enhance Lignocellulose Conversion”, U.S. Patent No. 9,074,231 B2 (2015)

6. Wang, G.S., Pan, X.J., Zhu, J.Y., and Gleisner, R.L.,“Sulfite Pretreatment for Biorefining Biomass,” U.S. Patent No. 9,090,915 B2 (2015)

7. Zhu, J.Y., Gleisner, R., “Methods of Pretreating Lignocellulosic Biomass with Reduced Formation of Fermentation Inhibitors”, U.S. Utility Patent No. 9,243,364 B2 (2016)

8. Zhu, J.Y., Chen, L., Gleisner, R., “Integrating the Production of Carboxylated Cellulose Nanofibrils and Cellulose Nanocrystals Using Recycling Organic acids” U.S. Utility Patent Application No 15/017,229, 02/05/2016

Book:

Zhu JY, Zhang X, Pan XJ (2011) Sustainable Production of Fuels, Chemicals, and Fibers from Forest Biomass, American Chemical Society (ACS) Symposium Series 1067. July 11 2011 (Web), ISBN: 9780841226432, eISBN: 9780841226449

Zhao, X., Liu, W., Deng, Y., Zhu, J.Y., (2015), Lignocellulosic Biomass-Energized Fuel Cells, Momentum Press

Book Chapters:

1. BOOK CHAPTER: Zhang, C., Gleisner, R., Houtman, C.J., Pan, X., Zhu, J.Y. (2016), “Sulfite Pretreatment to Overcome the Recalcitrance of Lignocelluloses (SPORL) for Bioconversion of Woody Biomass”, in Biomass Fractionation Technologies for a Lignocellulosic Feedstock Based Biorefinery (Mussatto Dragone, SI ed.), Elsevier, Chapter 22.

2. BOOK CHAPTER: Rockwood, D.L., Kirst, M., Isebrands, J.G., and Zhu, J.Y. (2012), “Forest Trees” in Handbook of Bioenergy Crop Plants (Kole C, Joshi CP, and Shonnard DR, eds.) CRC Press, Taylor and Francis Group, pp 348-399

3. BOOK CHAPTER: Zhu, J.Y. (2011), “Chapter 4: Physical Pretreatment – Woody Biomass Size-Reduction – for Forest Biorefinery” in Sustainable Production of Fuels, Chemicals, and Fibers from Forest Biomass (Zhu JY, Pan XJ, Zhang X, eds), American Chemical Society (ACS). July 11 2011 (Web). ISBN13: 9780841226432, eISBN: 9780841226449, DOI: 10.1021/bk-2011-1067, pp 89-107

4. BOOK CHAPTER: Beecher, J.F., Hunt, C.G., and Zhu, J.Y. (2009), “Tools for the Characterization of Biomass at the Nanometer Scale,” In: Lucia, L.A. and Rojas, O.J. (Eds), The Nanoscience and Technology of Renewable Biomaterials, Wiley-Blackwell, pp. 61-80

5. BOOK CHAPTER: Chai, X.-S. and Zhu, J.Y. (2001), “Application of Headspace Gas Chromatography in the Pulp and Paper Industry,” in Recent Research Development in Analytical Chemistry, 1, p61. Transworld Research Network

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Trade Journal News Articles and Editorials (non-refereed):

6. Zhu, J.Y., Chai, X.S., (1999), “Automation in Determining Solute Concentration and Henry’s Constant by Multiple Headspace Extraction Gas Chromatography,” American Lab. News, 31(8), p28C.

7. Zhu, J.Y., (2011), “Forest Biorefinery: The Next Century of Innovation,” TAPPI J. (Editorial), 10(5):5

8. Rockwood, D.L., Tamang, B., Kirst, M., Zhu, JY, (2012) “Field performance and bioenergy characteristics of four commercial eucalyptus grandis cultivars in Florida”, Butnor, John R., ed. Proceedings of the 16th biennial southern silvicultural research conference. e-Gen. Tech. Rep. SRS-156. Asheville, NC: U.S. Department of Agriculture Forest Service, Southern Research Station. 267-268

9. Zhu, J.Y., Yuan, Z.-H., Jiang, J.C., (2013), “Bioenergy Special Issue: International Conference on Bioenergy Technologies and Joint Symposium with AIChE Forest Products Division, Nanjing, China, October 2012” Bioenergy Research (Editorial), 6:1127

10. Zhu, J.Y., (2015), “The pulp and paper industry in 2040” TAPPI J. (TAPPI Centennial Editorial), 14(3):S19-S20

Refereed Publications (since 2000 only): Google scholar citation h index = 40 {#C} = Number of Citations

1. Zhu, H., Luo, W., Ciesielski, P. Fang, Z., Zhu, J.Y., Henriksson, G., Himmel, M., Hu, L. (2016), "Wood-Derived Materials for Green Electronics, Biological Devices, and Energy Applications", Chem. Rev. (accepted).

2. Chen, L., Vahey, D.W., Zhu, J.Y., Fu, S., (2016), “Simultaneous Determination of Length and Diameter of Rod-like Cellulose Nanoparticles by Spectral Absorption Measurements Using Rayleigh-Gans Scattering” Langmuir (submitted)

3. Zhao, X., Liu, W., Deng, Y., Zhu, J.Y. (2016), “Low-temperature Microbial and Direct Conversion of Lignocellulosic Biomass to Electricity: Advances and Challenges” Renewable & Sustainable Energy Reviews. (submitted)

4. Qin, Y. Qiu, X., Zhu, J.Y., (2016), “Towards mechanistic control in producing cellulose nanofibrils using disk milling with diluted acid pretreatment” Sci. Rep - Nature (submitted)

5. Xu, X., Zhou, J., Jiang, L., Lubineau, G., Ng, T., Ooi, B.S., Liao, H.-Y., Shen, C., Chen, L., Zhu, J.Y., (2016) “Novel and

Scalable Synthesis of Transparent, Low-haze, Flexible Hybrid Cellulose Nanopaper as Electrodes for Flexible Electronics” Nanoscale DOI: 10.1039/C6NR02245F

6. Chen, L., Zhu, J.Y., Baez, C., Kitin, P., Elder, T., (2016), “Highly Thermal-stable and Functional Cellulose Nanocrystals

and Nanofibrils Produced Using Fully Recyclable Organic Acids”, Green Chem. DOI: 10.1039/C6GC00687F

7. Chen, N., Zhu, J.Y., Tong, Z., (2016), “Fabrication of microfibrillated cellulose gel from waste pulp sludge via mild maceration combined with mechanical shearing”, Cellulose DOI: 10.1007/s10570-016-0959-1

8. Rudie, A.W., Houtman, C.J., Groom, L.H., Nicholls, D.L., Zhu, J.Y., (2016), “A Survey of bioenergy research in Forest Service Research and Development” Bioeng Res. 9:534-547, DOI 10.1007/s12155-016-9731-5

9. Wang, W., Mozuch, M.D., Sabo, R.C., Kersten, P., Zhu, J.Y., Jin, Y. (2016), “Endoglucanase post-milling treatment for producing cellulose nanofibrils from bleached eucalyptus fibers by a SuperMassColloider” Cellulose 23:1859-1870 DOI:

10.1007/s10570-016-0946-6

10. Wang, Q., Zhu, J.Y., (2016), “Effects of Mechanical Fibrillation Time by Disk Grinding on the Properties of Isolated

Cellulose Nanofibrils” TAPPI J. (accepted)

11. Qin, Y., Chang, Y., Wu, R., Yang, D., Qiu, X., Zhu, J.Y., (2016) “Biorefinery Lignosulfonates from Sulfite-Pretreated Softwoods as Dispersant for Graphite”, ACS Sustainable Chem. Eng. 4:2200–2205 DOI:

10.1021/acssuschemeng.5b01664

12. Harde, S.M., Wang, Z., Zhu, J.Y., Pan, X., (2016), “Microbial lipid production from SPORL-Pretreated Douglas fir by Mortierella isabellina”, Fuel 175:64-74 DOI: 10.1016/j.fuel/2016.02.023

13. Qin, Y., Yang, D., Gu, F., Li, X., Xiong, W., Zhu, J.Y., (2016), “Biorefinery Lignosulfonates as a Dispersant for Coal Water Slurry” Sustainable Chemical Processes DOI: 10.1186/s40508-016-0050-0

14. Gu, F., Gilles, W., Gleisner, R., Zhu, J.Y., (2016), “Fermentative High Titer Ethanol Production from a Douglas-fir Forest Residue without Detoxification Using SPORL: High SO2 Loading at a Low Temperature” Ind. Biotechnol. DOI: 10.1089/ind.2015.0028

15. Dien, B.S., Zhu, J.Y., Slininger, P.J., Kurtzman, C.P., Moser, B., O’Bryan, P.J., Gleisner, R., and Cotta, M.A. (2016)

“Conversion of SPORL pretreated Douglas-fir forest residue into microbial lipids with oleaginous yeasts” RSC Advances 6:20695-20705 DOI: 10.1039/c5ra24430g

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16. Xiang, Z., Gao, W., Chen, L., Lan, W., Zhu, J.Y., Runge, T., (2016) “A comparison of cellulose nanofibrils produced from Cladophora glomerata algae and bleached eucalyptus”, Cellulose 23:493-503 DOI 10.1007/s10570-015-0840-7

17. Zhao, X., Zhu, J.Y., (2016), “Efficient Conversion of Lignin to Electricity Using A Novel Direct Biomass Fuel Cell Mediated by Polyoxometalates at Low Temperatures” ChemSusChem 9:197-207 DOI: 10.1002/cssc.201501446

18. Zhou, H., Yang, D., Zhu, J.Y., (2016), “Molecular Structure of Sodium Lignosulfonate from Different Sources and their Properties as Dispersant of TiO2 Slurry” J. Dispersion Sci. Technol. 37(2):296-303

19. Zhou, H., Zhu, J.Y., Gleisner, R., Qiu, X., Horn, E., Negron, J., (2016) “Pilot-scale demonstration of SPORL for bioconversion of beetle-killed lodgepole pine to bio-ethanol and lignosulfonate” Holzforschung 70(1):21-30

DOI:10.1515/hf-2014-0332

20. Zhu, J.Y., Chandra, M.S., Roland Gleisner, William Gilles, Johnway Gao, Gevan Marrs, Dwight Anderson, John Sessions, (2015) “Case studies on sugar production from underutilized woody biomass using sulfite chemistry”, TAPPI J. 14(9):577-583

21. Wang, W., Sabo, R. C., Mozuch, M.D., Kersten, P., Zhu, J.Y., Jin, Y., (2015) “Properties of film made of cellulose nanofibrils from different endoglucanase treatments of a bleached eucalyptus pulp” J. Polymers Environ. 23:551-558

dx.doi.org/10.1007/s10924-015-0726-7O

22. Hu, C., Zhu, J.Y., Gleisner, R., (2015), “Optimizing Cellulose Fibrillation for Production of Cellulose Nanofibrils (CNF) Using a Disk Grinder” Holzforschung 69(8):993-1000, DOI: 10.1515/hf-2014-0219

23. Chen, L., Wang, Q., Hirth, K., Baez, C., Agarwal, U.P., Zhu, J.Y., (2015) “Tailoring the Yield and Characteristics of Wood Cellulose Nanocrystals (CNC) Using Concentrated Acid Hydrolysis” Cellulose 22:1753-1762 DOI: 10.1007/s10570-015-0615-1 {#C} = 14

24. Zhou, H., Zhu, J.Y., Gleisner, R., Qiu, X., Horn, E., (2015), “High titer ethanol and lignosulfonate productions from SPORL pretreated poplar at pilot-scale”, Front. Energy Res. 3:16. DOI: 10.3389/fenrg.2015.00016

25. Zhang, J., Gu, Feng, Zhu, J.Y., and Zalesny, Jr. R.S. (2015) “Using a Combined Hydrolysis Factor (CHF) to Optimize High Titer Ethanol Production from a SPORL Pretreated Poplar without Detoxification” Bioresource Technology 186:223–

231 DOI: 10.1016/j.biortech.2015.03.080

26. Qing, Y., Sabo, R., Wu, Y., Zhu, J.Y., and Cai, Z. (2015), “Self-Assembled Optically Transparent Cellulose Nanofibril films: Effect of Nanofibril Morphology and Drying Procedure”, Cellulose 22:1091–1102 DOI 10.1007/s10570-015-0563-9

27. Cheng, J., Leu, S.Y., Zhu, J.Y. Gleisner, R., (2015), “High Titer and Yield Ethanol Production from Undetoxified Whole Slurry of Douglas-fir Forest Residue using pH-Profiling in SPORL”, Biotechnol. Biofuels 8:22 DOI:10.1186/s13068-015-

205-3

28. Zhu, J.Y., Chandra, M.S., Gu, F., Gleisner, R., Reiner, R., Sessions, J., Marrs, G., Gao, J., Anderson, D., (2015) “Using

Sulfite Chemistry for Robust Bioconversion of Douglas-fir Forest Residue to High Titer Bioethanol and Lignosulfonate: A Pilot-Scale Demonstration”, Bioresource Technology 179:390-397 DOI: 10.1016/j.biortech.2014.12.052 {#C} = 20

29. Wang, Q., Zhu, J.Y., (2015), “Facile Preparation of Nanofiller-paper Using Mixed Office Paper without Deinking”, TAPPI J. 14(3):167-174.

30. Wang, W., Mozuch, M.D., Sabo, R.C., Kersten, P., Zhu, J.Y., Jin, Y., (2015), “Production of cellulose nanofibrils from

bleached eucalyptus fibers by hyperthermophilic endoglucanase treatment and subsequent microfluidization” Cellulose 22:351-361 DOI: 10.1007/s10570-014-0465-2

31. Zhang, J., Laguna, A., Clemons, C., Wolcott, M.P., Gleisner, R., Zhu, J.Y. (2015), “Effect of Hot-pressing Temperature on the Subsequent Enzymatic Saccharification and Fermentation SPORL of Pretreated Forest Biomass and” BioEnergy Res. 8:464-470 DOI:10.1007/s12155-014-9530-9

32. Cheng, J., Leu, S.-Y., Gleisner , R., Pan, X.J., Zhu, J.Y. (2014) High Solids Simultaneous Enzymatic Saccharification and Fermentation of Un-detoxified Whole Slurry of SPORL Pretreated Douglas-fir Forest Residue” Cellulose Chem. Technol. 48:849-854

33. Nair, S.S., Sharma, S., Pu, Y., Sun, Q., Pan, S., Zhu, J.Y., Deng, Y., Ragauskas, A.J., (2014), “High Shear Homogenization of Lignin to Nanolignin and Thermal Stability of Nanolignin-Poly (Vinyl Alcohol) Blends”, ChemSusChem 7:3513-3520, DOI: 10.1002/cssc.201402314

34. Nair, S. S., Zhu, J.Y., Y. Deng, A.J. Ragauskas, (2014) “High performance green barriers based on nanocellulose”, Sustainable Chemical Processes 2:23 {#C} = 14

35. Zhou, H.F., Lan, T.Q., Dien, B.S., Hector, R.E., Zhu, J.Y. (2014), “Comparisons of Five Saccharomyces cerevisiae strains for Ethanol Production from SPORL Pretreated Lodgepole Pine”, Biotechnology Progress 30:1076-1083, DOI

10.1002/btpr.1937

36. Sharma, S., Zhang, X., Nair, S., Ragauskas, R., Zhu, J.Y., Deng, Y. (2014), “Thermally Enhanced High Performance Cellulose Nano Fibril Barrier Membranes” RSC Advances 4 (85):45136 – 45142. DOI: 10.1039/ c4ra07469f

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8

37. Wang, Q.Q., Zhao, X., Zhu, J.Y., (2014), “Kinetics of Strong Acid Hydrolysis of A Bleached Kraft Pulp for Producing Cellulose Nanocrystals (CNC)”, Ind. Eng. Chem. Res. 53(27):11007-11014, DOI: 10.1021/ie501672m {#C} = 13

38. Zhou, H.F., Leu, S.-Y., Zhu, J.Y., Wu, X., Gleisner, R., Yang, D., Qiu, X., Horn, E., (2014), “Comparisons of high titer

ethanol production and lignosulfonate properties by SPORL pretreatment of lodgepole pine at two temperatures”, RSC Advances 4:27030–27038 DOI: 10.1039/c4ra03608e

39. Xu, X., Wang, H.; Jiang, L.; Wang, X.; Payne, S.; Zhu, J.Y. (2014) “Electrospun Polyethylene Oxide Nanofiber Mats:

Effects of Cellulose Nanocrystals and Cellulose Nanofibrils and Novel Shish-kebab-like Crystalline Structures” Macromolecules 47:3409-3416, DOI: 10.1021/ma402627j {#C} = 18

40. Anderson, S.R., Esposito, D., Gillette, W., Zhu, J.Y., Baxa, U., and McNeil, S.E. (2014), “Enzymatic preparation of nanocrystalline and microcrystalline cellulose”, TAPPI J. 13(5):35-41

41. Cheng, J., Leu, S.-Y., Zhu, J.Y., Jeffries, T.W., (2014), “Ethanol Production from Non-detoxified Whole Slurry of SPORL-pretreated Empty Fruit Bunches at a Low Cellulase Loading” Bioresource Technology 164:331-337 DOI:10.1016/j.biortech.2014.04.102 {#C} = 11

42. Nair, S.S., Zhu, J. Y., Deng, Y. Ragauskas, A.J., (2014), “Characterization of cellulose nanofibrillation by micro grinding”, J. Nanoparticle Research 16:2349, DOI:10.1007/s11051-014-2349-7. {#C} = 10

43. Lou, H, Zhou, H, Li, X., Wang, M., Zhu, J.Y., and Qiu, X., (2014), “Understanding the Effects of Lignosulfonate on Enzymatic Saccharification of Pure Cellulose”, Cellulose 21:1351-1359, DOI: 10.1007/s10570-014-0237-z {#C} = 20

44. Zhang, C., Houtman, C.J., Zhu, J.Y. (2014), “Using Low Temperature to Balance Enzymatic Saccharification and Furan Formation during SPORL Pretreatment of Douglas-fir”, Process Biochemistry 49:466-473, DOI: 10.1016/j.procbio.2013.12.017 {#C} = 24

45. Zeng, J. Tong, Z., Wang, L., Zhu, J.Y., L. O. Ingram (2014), “Isolation and Structural Characterization of Sugarcane

Bagasse Lignin after Dilute Phosphoric acid Plus Steam Explosion Pretreatment and its Effect on Cellulose Hydrolysis”, Bioresource Technology 154:274-281. DOI:10.1016/j.biortech.2013.12.072 {#C} = 17

46. Nair, S.S., Zhu, J. Y., Deng, Y. Ragauskas, A.J., (2014) “Hydrogels Prepared from Cross-Linked Nanofibrillated Cellulose”, ACS Sustainable Chem. Eng. 2:772-780. dx.doi.org/10.1021/sc400445t {#C} = 14

47. Zhang, C., Lei, X., Scott, C.T., Zhu, J.Y., K. Li, (2014), “Comparison of Dilute Acid and Sulfite Pretreatment for Enzymatic Saccharification of Earlywood and Latewood of Douglas-fir”, BioEnergy Research 7:362-370 DOI:

10.1007/s12155-013-9376-6

48. Hoeger, I.C., Gleisner, R., Negron, J., Rojas, O.J., Zhu, J.Y., (2014) “Bark Beetle-killed Lodgepole Pine for the Production of submicron Lignocellulose Fibrils”, Forest Science 60(3):502-511 DOI: dx.doi.org/10.5849/forsci.13-012

49. Zhu, J.Y., Zhou, H.F., Chai, X.S., Johannes, D., Pope, R., Valls, C., Roncero, M.B., (2014) “Inter-Laboratory Comparisons of HexA Measurements in Kraft Eucalyptus Pulps using a UV-Vis Spectroscopic Method” TAPPI J. 13(1):57-61

50. Zhou, H.F., Zhu, J.Y., Luo, X., Leu, S.-Y., Wu, X., Gleisner, R., Dien, B.S., Hector, R.E., Yang, D., Qiu, X., Horn, E.,

Negron, J. (2013), “Bioconversion of Beetle-Killed Lodgepole Pine Using SPORL: Process Scale-up Design, Lignin Co-product, and High Solids Fermentation without Detoxification”, Ind. Eng. Chem. Res 52(45):16057-16065 DOI: 10.1021/ie402873y {#C} = 30

51. Wang, Z.J., Zhu, J.Y., Fu, Y., Qin, M., Shao, Z., Jiang, J., Yang, F., (2013) “Lignosulfonate-mediated cellulase

adsorption: enhanced enzymatic saccharification of lignocellulose through weakening nonproductive binding to lignin.” Biotechnol. Biofuels, 6:156 DOI:10.1186/1754-6834-6-156 {#C} = 22

52. Leu, S.-Y., Gleisner, R., Zhu, J.Y., Sessions, J., Marrs, G., (2013) “Robust Enzymatic Saccharification of a Douglas-fir Forest Harvest Residue by SPORL”, Biomass Bioenergy 59:393-401 DOI:10.1016/j.biombioe.2013.08.014 {#C} = 22

53. Qing Y., Sabo, R., Zhu, J.Y, Agarwal, U., Cai, Z., Wu, Y., (2013) “A Comparative Study on Cellulose Nanofibrils Disintegrated via Multiple Processing Approaches” Carbohydrate Polymer 97(1): 226-234 DOI:10.1016/j.carbpol.2013.04.086 {#C} = 35

54. Zhou, H.F., Lou, H., Yang, D., Zhu, J.Y., Qiu, X., (2013) “Lignosulfonate to Enhance Enzymatic Saccharification of Lignocelluloses: The Role of Molecular Weight and Substrate Lignin”, Ind. Eng. Chem. Res. 52(25):8464-8470 DOI: 10.1021/ie401085k {#C} = 40

55. Zhang, C., Zhuang, X.S., Wang, Z.J., Matt, F.J., St. John, F., Zhu, J.Y. (2013), “Xylanase Supplementation on Enzymatic Saccharification of Dilute Acid Pretreated Poplars at Different Severities” Cellulose 20(4):1937-1946 DOI:

10.1007/s10570-013-9934-2

56. Lou, H., Zhu, J.Y., Lan, T.Q., Lai, H., and Qiu, X., (2013) “pH-Induced Lignin Surface Modification to Reduce Nonspecific Cellulase Binding and Enhance Enzymatic Saccharification of Lignocelluloses”, ChemSusChem 6(5):919-927 DOI: 10.1002/cssc.201200859 {#C} = 61

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57. Cheng, Q., Tong, Z., Dempere, L., Ingram, L., Wang, L., Zhu, J.Y., (2013) "Disk refining and ultrasonication sugar bagasse residues for poly(vinyl alcohol) composites" J. Polymer. Environ. 21(3):648-657 DOI: 10.1007/s10924-012-

0562-y

58. Lan, T.Q. Lou, H., Zhu, J.Y., (2013), "Enzymatic Saccharification of Lignocelluloses Should Be Conducted at Elevated pH 5.2 to 6.2" BioEnergy Research 6(2):476-485 DOI: 10.1007/s12155-012-9273-4 {#C} = 60

59. Leu, S-Y. and Zhu, J.Y., (2013) “Substrate-Related Factors Affecting Enzymatic Saccharification of Lignocelluloses: Our Recent Understanding” BioEnergy Research 6(2):405-415 DOI: 10.1007/s12155-012-9276-1 {#C} = 107

60. Xu, X., Liu, F., Jiang, L. and Zhu, J.Y. (2013) “Cellulose Nanocrystals vs. Cellulose Nanofibrils: A Comparative Study on Their Microstructures and Effects as Polymer Reinforcing Agents”, ACS Applied Materials & Interfaces 5(8):2999-3009 DOI:10.1021/am302624t {#C} = 87

61. Wang, Q.Q., Zhu, J.Y., Considine, J.M., (2013) “Strong and Optically Transparent Film Prepared Using Cellulosic Solid

Residue (CSR) Recovered from Cellulose Nanocrystals (CNC) Production Waste Stream” ACS Applied Materials & Interfaces 5(7):2527-2534 DOI:10.1021/am302967m {#C} = 16

62. Wang, Z.J., Qin, M., Zhu, J.Y., Tian, G., Li., Z. (2013) “Evaluation energy efficiency of bioconversion knot rejects to ethanol in comparison to other thermos-chemically pretreated biomass”, Bioresource Technology,130:783-788

63. Agarwal, U.P., Zhu, J.Y., Ralph, S. (2013) “Enzymatic Hydrolysis of Loblolly Pine: Effects of Cellulose Crystallinity and Delignification” Holtzforchung 67(4): 371-377. DOI: 10.1515/hf-2012-0116 {#C} = 18

64. Hoeger, I.C., Nair, S.S., Ragauskas, A.J., Deng, Y., Rojas, O.J., Zhu, J.Y., (2013) “Mechanical Deconstruction of Lignocellulose Cell Walls and their Enzymatic Saccharification”, Cellulose 20(2):807-818 DOI: 10.1007/s10570-013-9867-9 {#C} = 38

65. Zhang, D.S., Yang, Q., Zhu, J.Y., Pan, X.J., (2013) “Sulfite (SPORL) Pretreatment of Switchgrass for Enzymatic Saccharification”, Bioresource Technology 129:127-134 {#C} = 24

66. Wang, Z.J., Lan, T.Q., Zhu, J.Y., (2013) “Lignosulfonate and Elevated pH Can Enhance Enzymatic Saccharification of Lignocelluloses”, Biotechnol. Biofuels 6:9. DOI:10.1186/1754-6834-6-9 {#C} = 49

67. Lan, T.Q., Gleisner, R., Zhu, J.Y., Dien, B., Hector, R. (2013) “High Titer Ethanol Production from SPORL Pretreated Lodgepole Pine by Simultaneous Enzymatic Saccharification and Combined Fermentation”, Bioresource Technology 127:291-297 {#C} = 32

68. Zhang, C., Zhu J.Y., Gleisner, R., Sessions, J. (2012) “Fractionation of Forest Residues of Douglas-fir for Fermentable Sugar Production by SPORL Pretreatment” BioEnergy Research 5(4):978-988 {#C} = 19

69. Martin-Sampedro, R, Filpponen, I., Hoeger, I., Zhu, J.Y., Laine, J., Rojas, O. (2012) “Rapid and Complete Enzyme Hydrolysis of Ligocellulosic Nanofibrils”, ACS Macro Letters 1(11):1321-1325 {#C} = 14

70. Wang, Q.Q., Zhu, J.Y., Reiner, R.S., Verrill, S.P., Baxa, U., McNeil, S.E. (2012) “Approaching Zero Cellulose Loss in

Cellulose Nanocrystal (CNC) Production: Recovery and Characterization of Cellulosic Solid Residues (CSR) and CNC” Cellulose 19(6):2033-2047 {#C} = 32

71. Li, X., Luo, X., Li, K., Zhu, J.Y., Fougere, D., Clarke, K. (2012), “Comparison SPORL and dilute acid pretreatment of lodgepole pine: Substrate morphology, Cell wall structures, and Enzymatic hydrolysis” Applied Biochemistry and Biotechnology 168:1556-1567

72. Wang, Q.Q., Zhu, J.Y., Gleisner, R., Kuster, T.A., Baxa, U., McNeil, S.E. (2012), “Morphological Development of Cellulose Nanofibrils (CNF) of a Bleached Eucalyptus Pulp by Mechanical Fibrillation.” Cellulose 19(5):1631-1643 {#C} = 52

73. Wang, Q.Q., Zhu, J.Y., Hunt, C.G., Zhan, H.Y. (2012) “Kinetics of Adsorption, Desorption, and Re-adsorption of a Commercial Endoglucanase in Lignocellulosic Suspensions”, Biotechnol. Bioeng. 109(8):1965-1975{#C} = 24

74. Zhu, J.Y., Zhuang, X.S. (2012) "Conceptual net energy output for biofuel production from lignocellulosic biomass through biorefining", Prog. Energy Combust. Sci. 38(4):583-598 {#C} = 74

75. Zhu, W., Houtman, C.J., Zhu, J.Y., Gleisner, R., Chen, K.F. (2012), “Quantitative Predictions of Bioconversion of Aspen by Dilute Acid and SPORL pretreatments using a Unified Combined Hydrolysis Factor” Process Biochemistry 47:785-791 {#C} = 39

76. Wang, Z.J., Zhu, J.Y., Zalesny, Jr. R.S., Chen, K.F., (2012), “Ethanol Production from Poplar Wood Through Enzymatic Saccharification and Fermentation by Dilute Acid and SPORL Pretreatments ” Fuel 95:606-614 {#C} = 56

77. Wang, Q.Q., He, Z.B., Zhu, Z., Zhang, Y.-H. P., Ni, Y.H., Luo, X.L., Zhu, J.Y. (2012) “Evaluations of Cellulose Accessibility of Lignocelluloses by Solute Exclusion and Protein Adsorption Techniques” Biotechnol. Bioeng. 109(2):381-389 {#C} = 67

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78. Zhu, J.Y., Gleisner, R., Scott, C.T., Luo, X.L., Tian, S., (2011), “High Titer Ethanol Production from Simultaneous

Enzymatic Saccharification and Fermentation of Aspen at High Solids: A Comparison between SPORL and Dilute Acid (DA) Pretreatments” Bioresource Technology 102(19):8921-8929 {#C} = 57

79. Lee, J.-W., Zhu, J.Y., Scordiad, D., Jeffries, T.W. (2011) “Fermentative Production of Ethanol from Corncob using Scheffersomyces (Pichia) stipitis CBS 6054”, Appl. Biochem. Biotechnol. 165:814-822 {#C} = 16

80. Zhu, J.Y., Sabo, R., Luo, X.L., (2011), “Integrated Production of Nano-fibrillated Cellulose and Biofuel (Ethanol) by Enzymatic Fractionation of Wood Fibers”, Green Chemistry 13(5):1339-1344 {#C} = 71

81. Li, B., Wang, G.S., Chen, K., Vahey, D.W., Zhu, J.Y., (2011) “On Quantification of Residual Ink Content and Deinking Efficiency in Recycling of Mixed Office Wastepaper,” Ind. Eng. Chem. Res. 50(11):6965-6971

82. Liu, H., Zhu, J.Y., Chai, X.S., (2011) “In-situ, Rapid and Temporally Resolved Measurements of Cellulase Adsorption onto Lignocellulosic Substrates by UV-Vis Spectrophotometry” Langmuir 27(1):272-278 {#C} = 27

83. Luo, X., Zhu, J.Y., Gleisner, R., Zhan, H.Y., (2011) “Effect of Wet Pressing-induced Fiber Hornification on Enzymatic Saccharification of Lignocelluloses,” Cellulose 18(4):1055-1062 {#C} = 40

84. Zhu, J.Y., Luo,X., Tian,S., Gleisner, R., Negrone, J., Horn, E., (2011), “Efficient Ethanol Production from Beetle-Killed Lodgepole Pine Using SPORL Technology and Saccharomyces cerevisiae without Detoxification”, TAPPI Journal 10(5):9-18 {#C} = 16

85. Tian, S., Zhu, J.Y., Yang, X., (2011), “Evaluation of an Adapted Inhibitor-tolerant Yeast Strain for Ethanol Production from Combined Hydrolysate of Softwood”, Applied Energy 88(5):1792-1796 {#C} = 20

86. Zhu, J.Y., Verrill, S.P., Liu, H., Herian, V.L., Pan, X.J., Rockwood, D.L., (2011) “On Polydispersity of Plant Biomass Recalcitrance and Its Effects on Pretreatment Optimization for Sugar Production” BioEnergy Research 4(3):201-210 {#C} = 16

87. Tian, S. , Zhu, W., Gleisner, R., Pan, X.J., Zhu, J.Y., (2011) ”Comparisons of SPORL and Dilute Acid Pretreatments for Sugar and Ethanol Productions from Aspen” Biotechnology Progress 27:419-427 {#C} = 39

88. Wang, G.S., Lee, J.-W., Zhu, J.Y., Jeffries, T.W. (2011) “Dilute Acid Pretreatment of Corncob for Efficient Sugar Production”, Appl. Biochem. Biotechnol. 163:658-668 {#C} = 34

89. Luo, X., Zhu, J.Y., (2011) “Effects of Drying-induced Fiber Hornification on Enzymatic Saccharification of Lignocelluloses,” Enzyme and Microbial Technology 48(1):92-99 {#C} = 91

90. Youngblood, A., Zhu, J.Y., Scott, C.T., (2010), “Integrated Management of Carbon Sequestration and Biomass Utilization Opportunities in a Changing Climate”. USDA Forest Service, Rocky Mountain Research Station, Proceedings RMRS-P-61, December 2010. Presented at the 2009 National Silviculture workshop: Climate Biomass and Carbon Sequestration.

91. Liu, H., Zhu, J.Y., (2010), “Eliminating Inhibition of Enzymatic Hydrolysis of Cellulose by Lignin in an Unwashed Aspen Substrate Using Lignin-Metal Complexation” Bioresource Technology 101:9120-9127 {#C} = 28

92. Luo, X.L., Gleisner, R., Tian, S., Zhu, W.Y., Negron, J., Horn, E., Pan, X.J, Zhu, J.Y., (2010), “Evaluation of Mountain Beetle Killed Lodgepole Pine for Cellulosic Ethanol Production by SPORL” Ind. Eng. Chem. Res. 49(17):8258-8266 {#C} = 50

93. Tian, S., Luo, X.L., Yang, X.S., Zhu, J.Y., (2010), “Robust Cellulosic Ethanol Production from SPORL-Pretreated Lodgepole Pine Using an Adapted Strain S. cerevisiae without Detoxification” Bioresource Technology 101:8678-8685 {#C} = 60

94. Liu, H., Zhu, J.Y., Fu, S.Y., (2010), “Effects of Lignin-Metal Complexation on Enzymatic Hydrolysis of Cellulose”. J. Food and Agricultural Chemistry, 58:7233-7238 {#C} = 35

95. Zhu, J.Y., Pan, X.J., Zalesny, R.S. Jr., (2010), “Pretreatment of Woody Biomass for Biofuel production: Energy Efficiency, Pretreatment Technologies, and Recalcitrance” Applied Microbiology and Biotechnology, 87:847-857 {#C} = 160

96. Zhu, J.Y., Pan, X.J., (2010), “Woody Biomass Pretreatment for Cellulosic Ethanol Production: Technology and Energy Consumption Evaluation” Bioresource Technology, 101:4992-5002. {#C} = 433

97. Shuai, L., Yang, Q., Zhu, J.Y., Lu, F., Weimer, P., Ralph, J., Pan, X.J., (2010), “Comparative Study of SPORL and Dilute Acid Pretreatments of Softwood Spruce for Cellulose Ethanol Production”. Bioresource Technology 101:3106-3114 {#C} = 132

98. Zhu, J.Y., Zhu, W. OBryan, P., Dien, B.S.,Tian, S., Gleisner, R., Pan, X.J., (2010), “Ethanol Production from SPORL-

Pretreated Lodgepole Pine: Preliminary Evaluation of Mass Balance and Process Energy Efficiency”. Applied Microbiology and Biotechnology, 86(5):1355-1365 {#C} = 90

99. Zhu, W., Zhu, J.Y., Glesiner, R., Pan, X.J., (2010), “On Energy Consumption for Size-Reduction and Yield from Subsequent Enzymatic Hydrolysis of Lodgepole Pine,” Bioresource Technology, 101:2782-2792 {#C} = 96

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100. Liu, H., Fu, S.Y., Zhu, J.Y., Li, H., Zhan, H.Y., (2009) “Visualization of Enzymatic Hydrolysis of Cellulose using AFM Phase Imaging” Enzyme and Microbial Technology, 45:274-281 {#C} = 42

101. Wang, G.S., Pan, X.J., Zhu, J.Y., Gleisner, R., Rockwood, D.R., (2009), “Sulfite Pretreatment to Overcome

Recalcitrance of Lignocellulose (SPORL) for Robust Enzymatic Saccharification of Hardwoods“ Biotechnology Progress, 25(4):1086-1093 {#C} = 102

102. Zhu, J.Y., Pan, X.J., Wang, G.S, Gleisner, R., (2009), “Sulfite Pretreatment (SPORL) for Robust Enzymatic Saccharification of Spruce and Red Pine“ Bioresource Technology, 100(8):2411-2418. {#C} = 302

103. Zhu, J.Y., Wang, G.S., Gleisner, R., Pan, X., (2009), “Specific Surface for Evaluating Wood Size Reduction and Pretreatment Efficiencies” Chemical Engineering Science, 64(3):474-485. {#C} = 151

104. Rockwood, D.R., Rudie, A.W., Ralph, S.A., Zhu, J.Y., Winandy, J.E., (2008), “Energy Product Options for Eucalyptus Species Grown as Short Rotation Woody Crops”, Int. J. Mol. Sci. 9:1361-1378 {#C} = 77

105. Zhao, Y., Wang, Y. Zhu, J.Y., Ragauskas, A.J., Deng, Y. (2008), “Enhanced Enzymatic Hydrolysis of Spruce by Alkaline Pretreatment at Low Temperature,” Biotechnology and Bioengineering, 99(6):1320-1328 {#C} = 209

106. Zhu, J.Y., Vahey, D. W., Scott, C.T., (2008), “Some Observations of Wood Density and Anatomical Properties in a Douglas fir Sample with Suppressed Growth”, Wood Fib. Sci. 40(2):225-232

107. Zhu, J.Y., Vahey, D.W., Scott, T.C., and Myers, G.C., (2008), “ Effect of Tree Growth Rate on Papermaking Fiber Properties, “ APPITA J., 61(2):141-147

108. Rong, X., Qi, D., Zhu, J.Y., and Scott, T.C., (2008) "Single Curved Fiber Sedimentation under Gravity", Computers and Mathematics with Applications, 55(7):1560-1567.

109. Zhu, J.Y., Scott, C.T., Gleisner, R., Mann, D., Vahey, D.W., Dykstra, D.P., Quinn, G.H., Edwards, L.L., (2007), “Forest Thinnings for Integrated Commercial Production of Lumber and Paper” Forest Products J., 57(11):8-13 Feature Article

110. Chai, X-S., Samp, J., Hou, Q.X., Yoon, S-H., and Zhu, J.Y., (2007) “Possible Mechanism for Anthraquinone Species Diffusion in Alkaline Pulping” Ind. Eng. Chem. Res. 46:5245-5249.

111. Zhu, J.Y., Scott, C.T., Gleisner, R., Mann, D.W., Dykstra, D.P., Quinn, G.H., Edwards, L.L., (2007) “Mill Demonstration of TMP Production from Forest Thinnings: Pulp Quality, Refining Energy and Handsheet Properties,” BioResources, 2(4):544-559

112. Zhu, J.Y. Scott, T.C., Scallon, K.L., and Myers, G.C., (2007), “Effect of Plantation Density on Wood Density and Anatomical Properties of Red Pine (Pinus resinosa Ait.)” Wood Fib. Sci. 39(3):502 {#C} = 15

113. Vahey, D. W., Zhu, J.Y., Scott, T.C. (2007), “Wood Density and Anatomical Properties in Suppressed- Growth Trees: Comparison of Two Methods”, Wood Fib. Sci. 39(3):462

114. Vahey, D.W., Zhu, J.Y., Houtman, C.J., (2006), “On Measurements of Effective Residual Ink Concentration (ERIC) of Recycled Papers using Kubelka-Munk Theory,” Prog. Paper Recycling., 16(1):3 {#C} = 14

115. Zhu, J.Y. and Myers, G.C., (2006), “Effect of Plantation Density on Kraft Pulp Production from Red Pine (Pinus resinosa Ait.),” J. Pulp Paper Sci. 32(3):187.

116. Zhu, J.Y. and Myers, G.C., (2006), "Kraft Pulp from Budworm Infested Jack Pine," Holtzforschung, 60(4):383

117. Klungness, J.H., Gleisner, R., Mann, D., Scallon, K.L., Zhu, J.Y., Horn, E., Edwards, L.L., (2006) "Evaluation of Forest Thinning Materials for TMP Production," TAPPI J., 5(4):17.

118. Chai, X.-S., Samp, J.C., Yang, Q.F., Song, H.N., Zhang, D.C., Zhu, J.Y., (2006) “Determination of microstickies in recycled whitewater by headspace gas chromatography.” J. Chromatography A, 1108(1):14. also in Prog. Paper Recycling 16(3):12, 2007 {#C} = 15

119. DeLozier, G., Zhao, Y.L., Deng, Y., White, D., Zhu, J.Y., and Prein, M., (2005), "Laboratory- and Mill-Scale Study of Surfactant Spray Flotation Deinking," TAPPI J., 4(10):25

120. Zhu, J.Y., Tan, F., (2005), "On Fiber Rejection Loss in Flotation Deinking," Canadian J. Chem. Eng., 83:377 {#C} = 12

121. Zhu, J.Y., Tan, F., and Gleisner, R., (2005), "Monitor Liquid and Solid Content in Froth Using Conductivity," Prog. Paper Recycling., 14(4):21

122. Zhu, J.Y., Tan, F., (2005), "Drainage and Fractionation of Wood Fibers in Flotation Froth," Prog. Paper Recycling, 14(4):13

123. Considine, J.M., Scott, C.T., Gleisner, R., and Zhu, J.Y. (2005), "Use of digital imaging correlation to study the local

deformation field of paper and paperboard," Trans. of the 13th Fundamental Research Symposium, Oxford, UK, pp 613-630 {#C} = 17

124. Zhu, J.Y., Tan, F., (2005), "Dynamic Drainage of Froth with Wood Fibers," Ind. Eng. Chem. Res. 44:3336-3342.

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125. Schmidt, E.A. and Zhu, J.Y., (2005), "Flow Regime Effect on the Spreading Rate of a Nylon Fiber Suspension Jet in a Rectangular Channel," TAPPI J., 4(6):9.

126. Zhu, J.Y., Tan, F., Scallon, K.L., Zhao, Y.L., Deng, Y., (2005), "Deinking Selectivity (Z-Factor): A New Parameter to Evaluate the Performance of Flotation Deinking Process, " Separation and Purification Technology, 43(1):33-41. {#C} = 23

127. Zhu, J.Y. and Chai, X.S. (2005), "Some Recent Developments in Headspace Gas Chromatography" Current Analytical Chemistry, 1(1), pp.79-83. {#C} = 25

128. Schmidt, E.A. and Zhu, J.Y., (2004) "Confined Shear Dilution of a Nylon Fiber Suspension," TAPPI J., 3(11):11.

129. Ok, H., Park, H., Carr, W. W., Morris, J.F., Zhu, J.Y. (2004) "Particle-Laden Drop Impacting on Solid Surfaces," J. Dispersion Sci. Tech., 25(4):1.

130. Zhao, Y.L., Deng, Y., and Zhu, J.Y. (2004), "Roles of Surfactants in Flotation Deinking", Prog. Paper Recycling, 14(1), p41. {#C} = 36

131. Chai, X.-S., Hou, Q.X., Luo, Q., Zhu, J.Y., (2004), "Rapid determination of hydrogen peroxide in wood pulp bleaching streams by a dual-wavelength spectroscopic method," Analytica Chimica Acta, 507(2):281. {#C} = 101

132. Park, H., Carr, W.W., Zhu, J.Y., Morris, J.F., (2003) “Single Drop Impaction on a Solid Surface,“ AIChE J., 49(10):2461. {#C} = 86

133. Chai, X.-S. and Zhu, J.Y., (2003), “Erratum to Indirect headspace gas chromatographic method for vapor-liquid phase equilibrium study [J. Chromatography A, 799, (1998) 207-214]" J. Chromatography A, 1020(12), p283.

134. Chai, X.S., Hou, Q.X., Zhu, J.Y., (2003), “Carboxyl Groups in Wood Fibers: Part II. The Fate of Carboxyl Groups during Alkaline Delignification,” Ind. Eng. Chem. Res., 42:5445. {#C} = 11

135. Chai, X.S., Hou, Q.X., Zhu, J.Y., Chen, S.L., Wang, S.F., Lucia, L., (2003), “Carboxyl Groups in Wood Fibers: Part I. Determination of Carboxyl Groups by Headspace Gas Chromatography,” Ind. Eng. Chem. Res., 42:5440. {#C} = 41

136. Yang, X.T., Chai, X.S., Hou, Q., Zhu, J.Y., Danielsson, L.-G., (2003), “Spectroscopic Determination of Anthraquinone in Kraft Pulping Liquors Using A Nafion Membrane Interface,” J. Pulp Paper Sci., 29(9):299.

137. Chai, X.S., Hou, Q., Zhu, J.Y., and W. Ban, (2003) “Online Monitoring of Alkali, Sulfide, and Dissolved Lignin during Wood Pulping by Attenuated Total Reflection UV Spectroscopy and Flow Injection Techniques,” Ind. Eng. Chem. Res., 42:254. {#C} = 12

138. Chai., X.S. Luo, Q., Zhu, J.Y., and Li, J., (2003), “Attentuated Total Reflection UV Spectroscopy for Simultaneous Analysis of Alkali, Sulfide, And Dissolved Lignin in Pulping liquors, “ J. Pulp Paper Sci., 29(6):204

139. Luo, Q., Deng, Y., Zhu, J.Y., and W.-T. Shin (2003), “Foam Control Using Foaming Agent Spray: A Novel Concept for Flotation Deinking of Wastepaper,” Ind. Eng. Chem. Res., 42, p3578. {#C} = 14

140. Yoon, S.-H., Chai, X.-S., Zhu, J.Y., Kim, B.-H., and Song, B.-K., (2003), “Demethylation Kinetics for VOC/TRS Formation during Kraft Wood Pulping,” Korean J. of Industrial and Engineering Chemistry, 9(2):125.

141. Chai, X.-S. and Zhu, J.Y., (2003), “Determination of the Solubility of Inorganic Salts by Headspace Gas Chromatography” J. Chromatography A, 996(1-2), p157. {#C} = 13

142. Chai, X.-S., Zhu, J.Y., and Luo, Q., (2003), “Minor Sources of Carbonate in Kraft Pulping and Oxygen Delignification Processes, “ J. Pulp Paper Sci., 29(2):59. {#C} = 15

143. Zhu, J.Y., Chai, X.-S., Pan, X.J., Luo, Q., and Li, J., (2002), “Quantification and Reduction of Organic Sulfur Compound Formation in a Commercial Wood Pulping Process,” Environ. Sci. Techno. 36(10), p2269.

144. Chai, X.-S., Luo, Q., and Zhu, J.Y., (2002), “A Multiple Headspace Extraction Gas Chromatographic Method for the Study of Process Kinetics,” J. Chromatography A, 946, p177 {#C} = 14

145. Yang, X.T., Chai, X.S., Hou, Q., Zhu, J.Y., Danielsson, L.-G., (2002), “Determination of Anthraquinone-2-Sulfonate in Alkaline Pulping Liquor by Spectrophotometry Using A Nafion Membrane Interface,” Analytica Chimica Acta, 474:69.

146. Chai, X.-S., Li, J., and Zhu, J.Y., (2002), “ATR-UV Spectroscopy for Simultaneous On-Line Analysis of Sulfide, hydroxide, and Carbonate in Kraft Recausticizing Operations,” J. Pulp Paper Sci., 28(4), p110.

147. Chai, X.S., Zhu, J.Y., and J. Li, (2002), "Simultaneous and Rapid Analysis of Sulfide, Hydroxide, and Carbonate in Kraft Liquors by Attenuated Total Reflection-UV Spectroscopy," J. Pulp Paper Sci., 28(4), p105

148. Chai, X.-S. and Zhu, J.Y. (2001), “Analysis of Sulfide, Alkali, and Carbonate by ATR-UV Spectroscopy during Borate Autocausticizing Mill Trials,” Process Control and Quality, 11(6):531.

149. Chai, X.S., Yoon, S.-H., Zhu, J.Y., Li, J., (2001), "The Fate of Hexenuronic Acid Groups during Alkaline Pulping of Loblolly Pine," J. Pulp Paper Sci., 27(12), p407 {#C} = 37

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150. Chai, X.S., Luo, Q., Yoon, S.-H., Zhu, J.Y., (2001), "The Fate of Hexenuronic Acid Groups during Kraft Pulping of Hardwoods," J. Pulp Paper Sci., 27(12), p403 {#C} = 72

151. Yoon, S.-H., Chai, X.S., Zhu, J.Y., Li, J., and Malcolm, E.W., (2001), "In-Digester Odor Reduction in Kraft Pulping," Advances Environ Res., 5(1), p91 {#C} = 18

152. Chai, X.S., Zhu, J.Y., and Li, J., (2001), "A Simple and Rapid Method to Determine Hexenuronic Acid Groups in Chemical Pulps," J. Pulp Paper Sci., 27(5), p165 {#C} = 128

153. Chai, X.S., and Zhu, J.Y., (2001), “Author’s response,” J. Pulp Paper Sci., 27(4) p112.

154. Gu, Y., Edwards, L.L., Zhu, J.Y., Liu, P.H., and Chai, X.S., (2001), "Cluster Rule Simulation: Part 1: Kraft Mill Methanol Equilibrium Calculations," TAPPI J., 84(4), p62

155. Gu, Y., Edwards, L.L., Zhu, J.Y., and Chai, X.S., (2001), "Cluster Rule Simulation: Part 2: Kraft Mill Methanol Generation Models," TAPPI J., 84(4), p62

156. Teja, A.S., Gupta, A.K., Bullock, K. R., Chai, X.-S., and Zhu, J.Y., (2001), “Henry’s Constants of Methanol in Aqueous Systems Containing Salts,” Fluid Phase Equilibria, 185, p265 {#C} = 36

157. Chai, X.-S., Q. Luo, and Zhu, J.Y. (2001), “Analysis of Non-volatile Species in a Complex Matrix by Headspace Gas Chromatography,” J. Chromatography A., 909(2), p249 {#C} = 56

158. Zhu, J.Y., Liu, P.H., and Chai, X.S., Bullock, K.R., Teja, A.S., (2000), "Henry's Law Constant of Methanol in Pulping Spent Liquor," Environ Sci. Techno., 34(9), p1742 {#C} = 28

159. Chai, X.S., Luo, Q., Zhu, J.Y., (2000), "A Simple and Practical Kappa Test Method for Process Control in Pulp Production," Process Control and Quality, 11(5), p407

160. Zhu, J.Y., Yoon, S.-H., Liu, P.-H., and Chai, X.-S., (2000), "Methanol Formation in Alkaline Wood Pulping," TAPPI J., 83(7), p65 {#C} = 27

161. Gupta, A.K., Teja, A., Zhu, J.Y., Chai, X.S., (2000), "Henry's Constants of n-Alkanols in Water at Temperatures between 40oC and 90oC," Fluid Phase Equilibria, 170, p183 {#C} = 42

162. Chai, X.S., Liu, P.H., and Zhu, J.Y., (2000), "Analysis of Volatile Organic Sulfur Compounds in Kraft Liquors by Full Evaporation Headspace Gas Chromatography," J. Pulp Paper Sci., 26(5), p167 {#C} = 29

Recent MAJOR RESEARCH CONTRACTS and GRANTS AWARDED

Note: As a US federal government employee working for a federal government lab, I am not eligible for

applying many government research grants

1. Co-Principal Investigator, Renewable Biomass to Fuels and Value Added Chemicals, USDA National Institute of Food and Agriculture (NIFA), Agricultural Food Research Initiative (AFRI) Competitive Grants - Regional Approaches to Sustainable Bioenergy - Coordinated Agricultural Project (CAP) (2011-68005-30416) 10/2011–9/2016, ~$40,000,000

2. Co-Principal Investigator, High-value Nano-fibrillated Cellulose Polymer Reinforcement as a Biofuel Co-product, USDA National Institute of Food and Agriculture (NIFA), Agricultural Food Research Initiative (AFRI) Competitive Grants - Foundation Program in Sustainable Energy (2011-67009-20056). 01/2011–01/2016, ~$987,000