office of legacy management 2014 status report september 15–18, 2014. stephen donivan laboratory...
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Office of Legacy Management 2014 Status Report
September 15–18, 2014
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Stephen DonivanLaboratory Coordinator
The S.M. Stoller Corporation, A subsidiary of Huntington Ingalls Industries Inc.Contract Number DE-LM0000415
ASP 2014 Workshop
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Office of Legacy ManagementOrganization
Office of Business Operations (LM-10.0)
• Benefits Continuity Team LM-10.1
• Archives and Information Management Team LM 10.2
• Planning, Budget, and Acquisition Team LM 10.3
• HR/Administration Team LM 10.4
Office of Site Operations (LM-20.0)
• UMTRCA/NVOS Team LM-20.1
• RCRA/CERCLA/FUSRAP Team LM-20.2
• Asset Management Team LM-20.3
Office of the Director (LM-1)
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Legacy Management Office Location Map
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Site Count by Regulatory Type and Category
FUSRAP 32%
UMTRCA Title I 24%
UMTRCA Title II 7%
Other 12%
CERCLARCRA 9%
D&D6%
NVOS 10%
Type Site Count
CERCLA/RCRA 8
D&D (Decontamination and Decommissioning ) 5
FUSRAP (Formerly Utilized Sites Remedial Action Program )
29
UMTRCA (Uranium Mill Tailings Radiation Control Act ) Title I
30
UMTRCA Title II 6
Nevada Offsites 9
Other 11
Total 98
Cat-egory
I 44%
Category II
46%
Category III 10%
Category 1: Activities typically include records-related activities and stakeholder support.
Category 2: Activities typically include routine inspection (any site visit needed to verify the integrity of engineered or institutional barriers) and monitoring/maintenance, records-related activities, and stakeholder support.
Category 3: Activities typically include operation and maintenance of active remedial action systems, routine inspection (any site visit needed to verify the integrity of engineered or institutional barriers) and monitoring/maintenance, records-related activities,and stakeholder support.
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Legacy Management Site Location Map
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CERCLA/RCRA Sites
Fernald, OH SiteLaboratory for Energy Related Health Research, CA, SiteMaxey Flats, KYMonticello, UT, Disposal and Processing SitesMound, OH, SitePinellas County, FL, SiteRocky Flats, CO, SiteWeldon Spring, MO, Site
Site Samples per Year
Fernald 1850
Monticello 320
Mound 550
Pinellas 280
Rocky Flats 2100
Weldon Spring 530
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Nevada Offsites
Amchitka, AlaskaChariot, AlaskaRio Blanco, ColoradoRulison, ColoradoSalmon Site, MississippiCentral Nevada Test Area, NevadaShoal Site, NevadaGasbuggy Site, New MexicoGnome-Coach Site, New Mexico
Special Analytical Requirements:
• Actinide isotope analyses of biota samples
• Carbon-14 and tritium in natural gas samples
• Accelerator mass spectrometry: C-14, Cl-36, I-129
• Low-level tritium by the enrichment method
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UMTRCA Disposal and Processing Sites
• There are 36 Uranium Mill Tailings Radiation Control Act (UMTRCA) Title I and Title II processing or disposal sites managed LM.
• Twenty-two inactive uranium ore-processing sites were remediated resulting in the creation of 19 disposal cells.
• These sites are location on or near tribal lands: Mexican Hat, UT; Monument Valley, AZ; Riverton WY; Sherwood, WA; Shiprock, NM.
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UMTRCA Sites Analytical Challenges
Contaminants of Concern:• Ammonia• Chloride• Nitrate• Sulfate• Metals (As, Cd, Se, Mo, U, V, others)
Shiprock Groundwater Sample ResultsAnalyte Action Level Concentration, mg/L
Manganese 2.74 2.7
Nitrate/Nitrite as N 10 0.07
Selenium 0.05 0.002
Sulfate 2000 13,000
Uranium 0.044 0.42
Calcium 480
Chloride 640
Magnesium 2000
Potassium 130
Sodium 2900
TDS 24,000
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Legacy Management Sites
There are 98 sites managed by LM.
There are 44 sites that have analytical support requirements.
There are 40 sites identified for transfer to Legacy Management over the next 10 years.
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Analytical Services Contracts
Analytical services were procured utilizing the ICPT Basic Ordering Agreement along with an LM-specific requirements document.
Contracts were awarded March 2008.
The total dollar amount of the contracts for FY2013 was 758K.
FY2014 estimated total is 770K.
Other contracts for special analytical services and site-specific requirements are established as needed.
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Laboratory Data Errors
Common Laboratory Data Quality Errors Samples switched, improperly labeled at log-in or during extraction / digestion.
Sample results from multiple analyses at different dilutions are not in agreement indicating a dilution error.
Sample analyzed at multiple dilutions. Analyst’s hand-written notes misinterpreted during data entry resulting is a dilution factor error.
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Laboratory Data Errors
Metals, Di-lution
Metals, Sample ID
Colormetric, Dilution
Colormetric, Sample ID
IC Dilution IC sample ID
0
2
4
6
8
10
12
14
16
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Data Errors Since 2010
Data are from multiple laboratories
Data are from multiple sites
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Data Quality and Defensibility
Data QualitySample integrity
Effective procedures and processes
Analyses performed correctly
Results reported correctly
Effective review
Data Defensibility
Logbooks
Procedures
Expired standards / calibrations
Traceability
Qualifications and training
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Opportunities for Improvement
Data QualityCommunicate problem areas to the audit team before the audit.
Review the laboratory’s customer complaints to identify systematic errors.
Prioritize audit areas of review. Data quality first, data defensibility second.
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DOECAP Participation
Legacy Management has three DOECAP auditors, one lead auditor.
• Quality Assurance Management Systems and General Laboratory Practices
• Data Quality for Organic Analyses
• Data Quality for Inorganic and Wet Chemistry Analyses
• Data Quality for Radiochemistry Analyses
• Laboratory Information Management Systems/Electronic Data Deliverables
• Hazardous and Radioactive Materials Management