official test results for laboratory sample # 7111625
TRANSCRIPT
THCmax (a.k.a. Total THC) = d9-THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = Not Examined
Unk = Unknown
2020-11-22 12:32
Analytical Methods UsedCannabinoids: HPLC-UV
Microbial: Plate CountingTerpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 1 of 2
Official Test Results for Laboratory Sample # 7111625Origination: Apothecary Rx UBI #: N/A Inventory #: 20201120RB003
Strain: Galactic Haze CBD License #: N/A QA #: 20201120RB003Type: Flower Harvest Date: Unknown
Approved By: T. Sasaki, Ph.D., CSOAddress:4920 Atlanta Highway Date of Receipt: 2020-11-20
Alpharetta, GA 30004 Date of Testing: 2020-11-22 S. Stevens, LDR
PASS/FAIL
[This section intentionally leftblank.]
Cannabinoid Profile (units of measure are by weight)THC max0.738%
7.38mg/g
CBD max17.4%
174mg/g% mg/g % mg/g
THCA 0.764 7.64 d9-THC 0.0678 0.678CBDA 19.4 194 CBD 0.361 3.61CBGA 0.417 4.17 CBG 0.0708 0.708CBC 0.0619 0.619 CBN ND NDTHCVA ND ND THCV ND NDCBDVA 0.164 1.64 CBDV ND NDCBT ND ND d8-THC ND ND
Total Cannabinoids (raw sum): 21.3%, 213mg/g
100
10
1
0.1
0.01d9-THC
CBD CBG CBC CBN THCV d8-THC
CBDV CBT
Shelf Stability
Loss-On-Drying NEWater Activity: NE
Terpene Fingerprint (units in percent by weight)10
1
0.1
0.01
0.0011 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 T
ref# Name %5 Myrcene 0.6536 Caryophyllene 0.5737 Humulene 0.222 a-Pinene 0.1450 Bisabolol 0.112 Limonene 0.07640* a-Bulnesene 0.0721 Linalool 0.0676 b-Pinene 0.05543* b-Maaliene 0.055
ref# Name %45* a-Maaliene 0.03315 b-Ocimene 0.03249* Eudesmol 0.02844* Selinadiene 0.02734* trans-a-Bergamotene 0.02651 trans-Nerolidol 0.02335 Farnesene 0.02128 Terpineol 0.01823 Fenchol 0.01330* Geraniol 0.011
ref# Name %24* trans-2-Pinanol 0.0113 Camphene 0.003842 cis-Nerolidol 0.003747* Guaiol 0.003322 Fenchone 0.00237 a-Phellandrene 0.0028 Carene 0.001919 Terpinolene 0.001320* p-Cymenene 0.001117 Eucalyptol 0.00082
ref# Name %11 a-Ocimene 0.000791* Thujene 0.0005418 g-Terpinene 0.0004810 a-Terpinene 0.0003T Total 2.3
Most Volatile Least Volatile *Semi-quantitative results.
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn for
specific analyses. This report is supplemental to any other reports with the same analytic sample number. Pass/Fail criteria are defined in WAC 314-55-102.
.738
17.4
.437
.0619
.164
43%MONO
TERPENES
6%MONO
TERPENOIDS
44%SESQUI
TERPENES
7%SESQUI
TERPENOIDS
THCmax (a.k.a. Total THC) = d9-THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = Not Examined
Unk = Unknown
2020-11-22 12:32
Analytical Methods UsedCannabinoids: HPLC-UV
Microbial: Plate CountingTerpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 2 of 2
Official Test Results for Laboratory Sample # 7111625Origination: Apothecary Rx UBI #: N/A Inventory #: 20201120RB003
Strain: Galactic Haze CBD License #: N/A QA #: 20201120RB003Type: Flower Harvest Date: Unknown
Approved By: T. Sasaki, Ph.D., CSOAddress:4920 Atlanta Highway Date of Receipt: 2020-11-20
Alpharetta, GA 30004 Date of Testing: 2020-11-22 S. Stevens, LDR
Quantitative Impurities Report
Concentrations of analytes used to determine pass/fail status of individual tests.
* Greater than lower limit of detection (>LLOD) and less than lower limit of quantification (<LLOQ) . Applies to instances when theanalyte has been detected and positively identified, but the concentration is lower than we can accurately quantify. Literally: signalto noise ratio greater than 3 and signal less than calibration. LLOD is ~0.001 ppm for most analytes, LLOQ is ~0.01 for mostanalytes. Number shown is lower end of calibration (LLOQ).
** Greater than upper limit of quantification (>ULOQ). Applies to instances when the analyte concentration in the sample is greaterthan we can accurately measure without additional testing. Number shown is upper end of calibration (ULOQ).
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn for
specific analyses. This report is supplemental to any other reports with the same analytic sample number. Pass/Fail criteria are defined in WAC 314-55-102.
THCmax(a.k.a.TotalTHC)=d9-THC+(THC-A*0.877)CBDmax(a.k.a.TotalCBD)=CBD+(CBD-A*0.877)
TotalCannabinoidisarawsumofallmeasuredcannabinoidsInTraceability,TotalCannabinoidisasumofTHCmaxandCBDmax
Figuresmaydifferslightlyfromtraceabilityduetorounding
ND=NotDetectedNE=NotExamined
Unk=Unknown
AnalyticalMethodsUsedCannabinoids:HPLC-UVMicrobial:PlateCountingTerpenes:HS-GC-FIDSolvents:HS-GC-MS
TraceResidue:UHPLC-MSMS
WaterActivity:HYGROMER®Page1of4
OfficialTestResultsforLaboratorySample#8012382Origination:Apothecary Rx UBI#: Inventory#: 210123BS001
Strain: GalacticHaze License#: QA#: 210123BS001Type: Flower HarvestDate: Unknown
ApprovedBy: N.Mosely,CEOAddress:4920 Atlanta Highway DateofReceipt: 2021-01-23
Alpharetta, GA 30004 DateofTesting: 2021-01-23 S. Stevens,LDR
PASS/FAILForeignMatter+Seeds PASS
LossOnDrying(Moisture) NEWaterActivity NE
Microbiological NEMycotoxins PASSPesticides PASS
ChemicalProfile(unitsinpercentbyweight)
CANNABINOIDSNOTEXAMINED
CANNABINOIDSNOTEXAMINED
ShelfStability
Loss-On-Drying NEWaterActivity: NE
ThesetestingresultsarecertifiedbyscientificexaminationofasinglesampleprovidedbytheProducer/Processor.ConfidenceAnalyticsanditsagentsdidnotobserveorparticipateinthesampleselectionprocess,andcannotconfirmtheauthenticityofthesampleoritsrepresentativenessoftheassociatedlot/batch.Thesample,asreceived,washomogenizedbeforesubsamples
weredrawnforspecificanalyses.Thisreportissupplementaltoanyotherreportswiththesameanalyticsamplenumber.Pass/FailcriteriaaredefinedinWAC314-55-102.
THCmax(a.k.a.TotalTHC)=d9-THC+(THC-A*0.877)CBDmax(a.k.a.TotalCBD)=CBD+(CBD-A*0.877)
TotalCannabinoidisarawsumofallmeasuredcannabinoidsInTraceability,TotalCannabinoidisasumofTHCmaxandCBDmax
Figuresmaydifferslightlyfromtraceabilityduetorounding
ND=NotDetectedNE=NotExamined
Unk=Unknown
AnalyticalMethodsUsedCannabinoids:HPLC-UVMicrobial:PlateCountingTerpenes:HS-GC-FIDSolvents:HS-GC-MS
TraceResidue:UHPLC-MSMS
WaterActivity:HYGROMER®Page2of4
OfficialTestResultsforLaboratorySample#8012382Origination:Apothecary Rx UBI#: Inventory#: 210123BS001
Strain: GalacticHaze License#: QA#: 210123BS001Type: Flower HarvestDate: Unknown
ApprovedBy: N.Mosely,CEOAddress:4920 Atlanta Highway DateofReceipt: 2021-01-23
Alpharetta, GA 30004 DateofTesting: 2021-01-23 S. Stevens,LDR
QuantitativeImpuritiesReport
Concentrationsofanalytesusedtodeterminepass/failstatusofindividualtests.
* Greaterthanlowerlimitofdetection(>LLOD)andlessthanlowerlimitofquantification(<LLOQ).Appliestoinstanceswhentheanalytehasbeendetectedandpositivelyidentified,buttheconcentrationislowerthanwecanaccuratelyquantify.Literally:signaltonoiseratiogreaterthan3andsignallessthancalibration.LLODis~0.001ppmformostanalytes,LLOQis~0.01formostanalytes.Numbershownislowerendofcalibration(LLOQ).
**Greaterthanupperlimitofquantification(>ULOQ).Appliestoinstanceswhentheanalyteconcentrationinthesampleisgreaterthanwecanaccuratelymeasurewithoutadditionaltesting.Numbershownisupperendofcalibration(ULOQ).
Findings
ALKANESNOTEXAMINED
ALCOHOLSNOTEXAMINED
SOLVENTIMPURITIESNOTEXAMINED
MYCOTOXINSAnalyte Concentration ActionLevel*AflatoxinB1 <LLOQ 20ppbAflatoxinB2 <LLOQ 20ppbAflatoxinG1 <LLOQ 20ppbAflatoxinG2 <LLOQ 20ppbOchratoxinA <LLOQ 20ppb*ActionLevelisSumofAflatoxins
MICROBIOLOGICALSNOTEXAMINED
ThesetestingresultsarecertifiedbyscientificexaminationofasinglesampleprovidedbytheProducer/Processor.ConfidenceAnalyticsanditsagentsdidnotobserveorparticipateinthesampleselectionprocess,andcannotconfirmtheauthenticityofthesampleoritsrepresentativenessoftheassociatedlot/batch.Thesample,asreceived,washomogenizedbeforesubsamples
weredrawnforspecificanalyses.Thisreportissupplementaltoanyotherreportswiththesameanalyticsamplenumber.
THCmax(a.k.a.TotalTHC)=d9-THC+(THC-A*0.877)CBDmax(a.k.a.TotalCBD)=CBD+(CBD-A*0.877)
TotalCannabinoidisarawsumofallmeasuredcannabinoidsInTraceability,TotalCannabinoidisasumofTHCmaxandCBDmax
Figuresmaydifferslightlyfromtraceabilityduetorounding
ND=NotDetectedNE=NotExamined
Unk=Unknown
AnalyticalMethodsUsedCannabinoids:HPLC-UVMicrobial:PlateCountingTerpenes:HS-GC-FIDSolvents:HS-GC-MS
TraceResidue:UHPLC-MSMS
WaterActivity:HYGROMER®Page3of4
OfficialTestResultsforLaboratorySample#8012382Origination:Apothecary Rx UBI#: Inventory#: 210123BS001
Strain: GalacticHaze License#: QA#: 210123BS001Type: Flower HarvestDate: Unknown
ApprovedBy: N.Mosely,CEOAddress:4920 Atlanta Highway DateofReceipt: 2021-01-23
Alpharetta, GA 30004 DateofTesting: 2021-01-23 S. Stevens,LDR
ChemicalResidueScreen-TestReport
Cannabissampleswerehomogenizedandextractedusingacustomprotocol.InstrumentalanalysiswasperformedwithUHPLC-MS/MS(tandemquadrupole).TargetcompoundswereidentifiedbymatchingtoCertifiedReferenceMaterials.Ion-selectivedetection(multiplereactionmonitoring,orMRM)wasusedtoensurethatprecursorandproductionsofthecorrectmassesco-elutedandwereobservedinratiosmatchingthoseforthereferencematerials.
Dozensofcompoundsrepresentingmanydifferentclassesoffungicides,herbicides,andplantgrowthregulatorswerescreenedfor.ThisdocumentlistsallanalytesdetectedintheChemicalResidueScreen.
Findings
AnalyteName CAS#AmountInSample PASS/FAIL
WAStateActionLevel
(sum)Spinosads NA NOTDETECTED PASS 0.20ppm(sum)Permethrins NA NOTDETECTED PASS 0.20ppmCarbaryl 63-25-2 0.062ppm PASS 0.20ppmAbamectinB1a 71751-41-2 NOTDETECTED PASS 0.50ppmAcephate 30560-19-1 NOTDETECTED PASS 0.40ppmAcetamiprid 135410-20-7 NOTDETECTED PASS 0.20ppmAldicarb 116-06-3 NOTDETECTED PASS 0.40ppmAzoxystrobin 131860-33-8 NOTDETECTED PASS 0.20ppmBifenazate 149877-41-8 NOTDETECTED PASS 0.20ppmBifenthrin 82657-04-3 NOTDETECTED PASS 0.20ppmBoscalid 188425-85-6 NOTDETECTED PASS 0.40ppmCarbofuran 1563-66-2 NOTDETECTED PASS 0.20ppmChlorantraniliprole 500008-45-7 NOTDETECTED PASS 0.20ppmChlormequat 7003-89-6 NOTDETECTED PASS 0.10ppmChlorpyrifos 2921-88-2 NOTDETECTED PASS 0.20ppmcis-Permethrin 52645-53-1 NOTDETECTED PASS 0.20ppmClofentezine 74115-24-5 NOTDETECTED PASS 0.20ppmDaminozide 1596-84-5 NOTDETECTED PASS 1.00ppm
AnalyteName CAS#AmountInSample PASS/FAIL
WAStateActionLevel
Diazinon 333-41-5 NOTDETECTED PASS 0.20ppmDichlorvos 62-73-7 NOTDETECTED PASS 0.10ppmDimethoate 60-51-5 NOTDETECTED PASS 0.20ppmEthoprophos 13194-48-4 NOTDETECTED PASS 0.20ppmEtofenprox 80844-07-1 NOTDETECTED PASS 0.40ppmEtoxazole 153233-91-1 NOTDETECTED PASS 0.20ppmFenoxycarb 72490-01-8 NOTDETECTED PASS 0.20ppmFenpyroximate 134098-61-6 NOTDETECTED PASS 0.40ppmFipronil 120068-37-3 NOTDETECTED PASS 0.40ppmFlonicamid 158062-67-0 NOTDETECTED PASS 1.00ppmFludioxonil 131341-86-1 NOTDETECTED PASS 0.40ppmHexythiazox 78587-05-0 NOTDETECTED PASS 1.00ppmImazalil 35554-44-0 NOTDETECTED PASS 0.20ppmImidacloprid 138261-41-3 NOTDETECTED PASS 0.40ppmKresoxim-methyl 143390-89-0 NOTDETECTED PASS 0.40ppmMalathion 121-75-5 NOTDETECTED PASS 0.20ppmMetalaxyl 57837-19-1 NOTDETECTED PASS 0.20ppmMethiocarb 2032-65-7 NOTDETECTED PASS 0.20ppm
*Greaterthanlowerlimitofdetection(>LLOD)andlessthanlowerlimitofquantification(<LLOQ).Appliestoinstanceswhentheanalytehasbeendetectedandpositivelyidentified,buttheconcentrationislowerthanwecanaccuratelyquantify.Specifically:signaltonoiseratiogreaterthan3andsignallessthancalibration.LLODis~0.001ppmformostanalytes,LLOQis~0.01formostanalytes.Numbershownislowerendofcalibration(LLOQ).
**Greaterthanupperlimitofquantification(>ULOQ).Appliestoinstanceswhentheanalyteconcentrationinthesampleisgreaterthanwecanaccuratelymeasurewithoutadditionaltesting.Numbershownisupperendofcalibration(ULOQ).
ThesetestingresultsarecertifiedbyscientificexaminationofasinglesampleprovidedbytheProducer/Processor.ConfidenceAnalyticsanditsagentsdidnotobserveorparticipateinthesampleselectionprocess,andcannotconfirmtheauthenticityofthesampleoritsrepresentativenessoftheassociatedlot/batch.Thesample,asreceived,washomogenizedbeforesubsamples
weredrawnforspecificanalyses.Thisreportissupplementaltoanyotherreportswiththesameanalyticsamplenumber.
THCmax(a.k.a.TotalTHC)=d9-THC+(THC-A*0.877)CBDmax(a.k.a.TotalCBD)=CBD+(CBD-A*0.877)
TotalCannabinoidisarawsumofallmeasuredcannabinoidsInTraceability,TotalCannabinoidisasumofTHCmaxandCBDmax
Figuresmaydifferslightlyfromtraceabilityduetorounding
ND=NotDetectedNE=NotExamined
Unk=Unknown
AnalyticalMethodsUsedCannabinoids:HPLC-UVMicrobial:PlateCountingTerpenes:HS-GC-FIDSolvents:HS-GC-MS
TraceResidue:UHPLC-MSMS
WaterActivity:HYGROMER®Page4of4
OfficialTestResultsforLaboratorySample#8012382Origination:Apothecary Rx UBI#: Inventory#: 210123BS001
Strain: GalacticHaze License#: QA#: 210123BS001Type: Flower HarvestDate: Unknown
ApprovedBy: N.Mosely,CEOAddress:4920 Atlanta Highway DateofReceipt: 2021-01-23
Alpharetta, GA 30004 DateofTesting: 2021-01-23 S. Stevens,LDR
ChemicalResidueScreen-TestReport
Cannabissampleswerehomogenizedandextractedusingacustomprotocol.InstrumentalanalysiswasperformedwithUHPLC-MS/MS(tandemquadrupole).TargetcompoundswereidentifiedbymatchingtoCertifiedReferenceMaterials.Ion-selectivedetection(multiplereactionmonitoring,orMRM)wasusedtoensurethatprecursorandproductionsofthecorrectmassesco-elutedandwereobservedinratiosmatchingthoseforthereferencematerials.
Dozensofcompoundsrepresentingmanydifferentclassesoffungicides,herbicides,andplantgrowthregulatorswerescreenedfor.ThisdocumentlistsallanalytesdetectedintheChemicalResidueScreen.
Findings
AnalyteName CAS#AmountInSample PASS/FAIL
WAStateActionLevel
Methomyl 16752-77-5 NOTDETECTED PASS 0.40ppmMyclobutanil 88671-89-0 NOTDETECTED PASS 0.20ppmNaled 300-76-5 NOTDETECTED PASS 0.50ppmOxamyl 23135-22-0 NOTDETECTED PASS 1.00ppmPaclobutrazol 76738-62-0 NOTDETECTED PASS 0.40ppmPhosemet(Imidan) 732-11-6 NOTDETECTED PASS 0.20ppmPiperonylButoxide 51-03-6 NOTDETECTED NA NAPrallethrin 23031-36-9 NOTDETECTED PASS 0.20ppmPropiconazole 60207-90-1 NOTDETECTED PASS 0.40ppmPropoxur 114-26-1 NOTDETECTED PASS 0.20ppmPyrethrinI 8003-34-7 NOTDETECTED NA NAPyridaben 96489-71-3 NOTDETECTED PASS 0.20ppmSpinosadA 168316-95-8 NOTDETECTED PASS 0.20ppmSpinosadD 168316-95-9 NOTDETECTED PASS 0.20ppmSpiromesifen 283594-90-1 NOTDETECTED PASS 0.20ppmSpirotetramat 203313-25-1 NOTDETECTED PASS 0.20ppmSpiroxamine 118134-30-8 NOTDETECTED PASS 0.40ppmTebuconazole 80443-41-0 NOTDETECTED PASS 0.40ppm
AnalyteName CAS#AmountInSample PASS/FAIL
WAStateActionLevel
Thiacloprid 111988-49-9 NOTDETECTED PASS 0.20ppmThiamethoxam 153719-23-4 NOTDETECTED PASS 0.20ppmtrans-Permethrin 52645-53-2 NOTDETECTED PASS 0.20ppmTrifloxystrobin 141517-21-7 NOTDETECTED PASS 0.20ppmUniconazole 83657-22-1 NOTDETECTED PASS 0.10ppm
*Greaterthanlowerlimitofdetection(>LLOD)andlessthanlowerlimitofquantification(<LLOQ).Appliestoinstanceswhentheanalytehasbeendetectedandpositivelyidentified,buttheconcentrationislowerthanwecanaccuratelyquantify.Specifically:signaltonoiseratiogreaterthan3andsignallessthancalibration.LLODis~0.001ppmformostanalytes,LLOQis~0.01formostanalytes.Numbershownislowerendofcalibration(LLOQ).
**Greaterthanupperlimitofquantification(>ULOQ).Appliestoinstanceswhentheanalyteconcentrationinthesampleisgreaterthanwecanaccuratelymeasurewithoutadditionaltesting.Numbershownisupperendofcalibration(ULOQ).
ThesetestingresultsarecertifiedbyscientificexaminationofasinglesampleprovidedbytheProducer/Processor.ConfidenceAnalyticsanditsagentsdidnotobserveorparticipateinthesampleselectionprocess,andcannotconfirmtheauthenticityofthesampleoritsrepresentativenessoftheassociatedlot/batch.Thesample,asreceived,washomogenizedbeforesubsamples
weredrawnforspecificanalyses.Thisreportissupplementaltoanyotherreportswiththesameanalyticsamplenumber.
R&D
Medicine Creek Analytics Certificate of Analysis
3700 Pacific HWY E, Ste 400, Fife, WA 98424WA State I502 Certification 0018 | ISO 17025 91428 | Accreditation #91428
Sample: 8012382 #COC/INVOICE: 4082
Laboratory ID 210124-006 Matrix Flower Batch ID Inventory ID
Tested for Confidence Analytics Address 14797 NE 95th St Redmond, WA 98052 License 3
Received 01/25/2021 Reported 01/28/2021
Analyses executed MET
MET - Heavy Metals Detection AnalysisAnalyzed Jan 28, 2021 | Instrument ICP-MS
AnalyteLOD
ug/5gLOQ
ug/5gResultug/5g
WRLug/5g
AnalyteLOD
ug/5gLOQ
ug/5gResultug/5g
WRLug/5g
Arsenic (As) 0.02 0.06 10 Cadmium (Cd) 0.01 0.04 ND 4.1
Lead (Pb) 0.01 0.02 ND 6 Mercury (Hg) 0.02 0.07 ND 2
NR Not ReportedND Not Detected<LOD Below Lod NT Not TestedLOD Limit of DetectionLOQ Limit of QuantificationDET Detected below quantitation limitCFU/g Colony Forming Units per 1 gramTNTC Too Numerous to Countmg/g Milligrams per gramppm Parts per million WRL Washington Regulatory Limit
Authorized Signature
Kyle Shelton Lab Manager01/28/2021
*This report shall not be reproduced except in full, without the written approval of the lab. This report is for informational purposesonly and should not be used to diagnose, treat or prevent any disease. Results are only for samples and batches indicated.Measurement uncertainties available upon request. Reporting limits available upon request. Results are valid for 6 months fromdate reported, unless otherwise indicated.
210124-006 page 1 of 1
ND