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We’re here for you. Orange County Sanitation District Biosolids Management Compliance Report Year 2011 EPA 40 CFR Part 503 Leyla Perez Biosolids Inspector

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We’re here for you.

Orange County Sanitation District

Biosolids ManagementCompliance Report

Year 2011EPA 40 CFR Part 503

Leyla PerezBiosolids Inspector

TABLE OF CONTENTS ACKNOWLEDGEMENTS

CERTIFICATION STATEMENT

2011 BIOSOLIDS MANAGEMENT COMPLIANCE REPORT Introduction ......................................................................................................... 1 Organization and Function .................................................................................. 1 Biosolids Program Policies and Guidance .......................................................... 1 OCSD’s Biosolids Management System ............................................................. 2 Long Range Biosolids Management Plan ........................................................... 4 Goals and Targets .............................................................................................. 5 Program History .................................................................................................. 8 OCSD’s Treatment Plants ................................................................................... 9 Biosolids Management – Contractors .............................................................. 11 Biosolids Distribution ......................................................................................... 13 Summary of Pollutants ...................................................................................... 13 Determination of Hazardousness ...................................................................... 14

APPENDIX A Table 1: Biosolids Monitoring and Reporting for 2011, Plant 1 Table 2: Biosolids Monitoring and Reporting for 2011, Plant 2 Table 3: Digester Cleaning Material – Beneficial Reuse for 2011 Table 4: Digester Cleaning Material – Disposal for 2011 Notice and Necessary Information Certification Forms

APPENDIX B Chapter 9 - FY 2010-2011 Solids Management Program of OCSD’s Source Control Program Annual Report

APPENDIX C Summary of Priority Pollutants and Trace Constituents Analysis

ACKNOWLEDGEMENTS

The Orange County Sanitation District wishes to acknowledge the following individuals for their valuable contribution to this report: Leyla Perez .......................................................... Editor, Senior Environmental Specialist Rachel Van Exel ............................................ Reviewer, Senior Environmental Specialist Deirdre Bingman ......................................... Reviewer, Principal Environmental Specialist Michelle Hetherington ..................................................... Reviewer, Regulatory Specialist Tom Meregillano ............................................................. Reviewer, Regulatory Specialist Lisa Rothbart ........................................................... Reviewer, Environmental Supervisor James Colston ............................. Final Reviewer, Environmental Compliance Manager

CERTIFICATION STATEMENTS

2011 BIOSOLIDS MANAGEMENT COMPLIANCE REPORT

Introduction Organization and Function

Biosolids Program Policies and Guidance OCSD’s Biosolids Management System

Long Range Biosolids Management Plan Goals and Targets

Program History OCSD’S Treatment Plants

Biosolids Management - Contractors Biosolids Distribution

Summary of Pollutants Determination of Hazardousness

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Introduction The Orange County Sanitation District’s (OCSD) nationally-certified Biosolids Program is responsible for the management of biosolids and related residuals. OCSD strives to recycle biosolids by using sustainable options while protecting public health and the environment. OCSD recognizes the importance of building strong relationships throughout its biosolids value chain, including with interested parties and regulators, and continuously improving in all areas of its Biosolids Program. Organization and Function OCSD is responsible for safely collecting, treating, recycling, and disposing of wastewater generated by 2.5 million people living in central and northwest Orange County, California, encompassing 21 cities and three (3) special districts. Operating under its National Pollutant Discharge Elimination System (NPDES) Permit No. CA0110604, OCSD owns facilities that include 580 miles of sewer pipes and two wastewater treatment plants – one in Fountain Valley and the other in Huntington Beach. During 2011, OCSD treated an average daily sewage influent flow of 204 million gallons per day (MGD), and produced approximately 270,000 wet tons of biosolids. This is an average of 735 wet tons per day of biosolids. Biosolids Program Policies and Guidance Originally adopted in 2000 and amended in 2006, OCSD’s Resolution 06-10, established a policy that commits the agency to support biosolids beneficial reuses (organics recycling). The resolution states:

• OCSD declares its full support for the recycling of biosolids, including land application, composting, and energy production.

• OCSD will use on its site, and encourage its member agencies to use

at their facilities, compost made using OCSD’s biosolids.

• OCSD supports the proper management and oversight of practices in accordance with the United States Environmental Protection Agency's Code of Federal Regulations Title 40, Part 503 and the California Water Environment Association’s Manual of Good Practice.

• OCSD is committed to the National Biosolids Partnership’s (NBP) Code of Good Practice and to implementing a biosolids environmental management system (now referred to as Biosolids Management System).

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OCSD’s biosolids policy statement, which summarizes the Board’s Biosolids Resolution above, is:

“Orange County Sanitation District strives to recycle its biosolids using sustainable options while protecting public health and the environment.”

In December 2007, OCSD’s Board of Directors adopted a 5-Year Strategic Plan (search “Strategic Plan” at www.ocsd.com) that guides OCSD’s priorities, goals, and level of service targets. The Strategic Plan includes OCSD’s commitment to recycling biosolids and ensuring a sustainable Biosolids Program. In November 2011 the Board adopted a change in OCSD’s strategic level of service to allow local landfill disposal for up to 12% of biosolids (increased from 5%) during peak solids production through 2017. This is a potential reduction in OCSD’s level of recycling to 88%. This further diversifies OCSD’s management options portfolio while using in-county options. The Strategic Plan and its annual updates (November 2011 Strategic Plan) are available online. The biosolids goals and targets that come from this Plan are reported in the Goals and Targets section below. OCSD’s Biosolids Management System In July 2000, OCSD signed a Letter of Understanding with the National Biosolids Partnership (NBP) and became one of 27 charter demonstration agencies committed to developing a Biosolids Management System (BMS). The NBP is a nonprofit coalition between the United States Environmental Protection Agency, the National Association of Clean Water Agencies, and the Water Environment Federation. The goal of this partnership is to promote and assist agencies in developing environmentally-sound biosolids management practices. The NBP biosolids management program is based on ISO 14001 Environmental Management concepts and is customized for biosolids processes. It incorporates biosolids-related issues by focusing on outcomes and encouraging public participation. The purpose for developing a BMS is to evaluate and improve current biosolids management practices to create a sustainable biosolids program. The BMS will continue to improve efficiency and environmental protective management practices, thereby building credibility with the public. By committing to the NBP’s certification program, OCSD pledges to uphold the following principles of conduct (Code of Good Practice) (also recognized in its Board-adopted Biosolids Policy referenced above):

1. Comply with all applicable federal, state, and local requirements.

2. Provide biosolids that meet the applicable standards for their intended use.

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3. Develop a management system for biosolids that includes a method of independent third-party verification to ensure effective ongoing biosolids operations.

4. Enhance the monitoring of biosolids production and management

practices.

5. Require good housekeeping practices for biosolids production, processing, transport, storage, and end-use.

6. Develop response plans for unanticipated events, such as inclement

weather, spills, and equipment malfunctions.

7. Enhance the environment by committing to sustainable, environmentally acceptable biosolids management practices and operations.

8. Prepare and implement a plan for preventive maintenance for equipment

used to manage biosolids. 9. Seek continual improvement in all aspects of biosolids management.

10. Provide methods of effective communication with gatekeepers,

stakeholders, and interested citizens. In order to implement the Code of Good Practice, OCSD improved its documentation and recordkeeping procedures, and proactively sought to engage interested parties in biosolids issues. In 2010, OCSD also required its contractors to officially agree to adhere to the Code of Good Practice. OCSD underwent a biosolids management system assessment in January 2001, followed by a series of internal audits. In February 2002, OCSD announced the official launch of its Biosolids Management System. An independent third-party verification audit was conducted in March and June of 2003. In July 2003, the NBP announced that OCSD was the first agency in the nation to obtain certification for its biosolids management system. In 2004, OCSD received the EPA’s National Clean Water Act Recognition Award for Special Recognition in the Biosolids Exemplary Management Awards Program category for its outstanding biosolids program. In 2006, OCSD was recognized with a Platinum Level Certificate by the NBP for reaching NBP's highest achievement in biosolids management and environmental stewardship. The Platinum Level applies to NBP agencies that were previously certified by NBP and have successfully met the third-party audit requirements to maintain ongoing certification for the NBP Biosolids Management Program. OCSD entered its second five-year cycle in June 2008 with a re-certification audit of its BMS by KEMA, an independent third-party auditor. The second interim

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audit of the cycle, conducted in January 2011, found no nonconformances, and noted the following as strengths:

• OCSD has an excellent contractor oversight program and has driven EMS principles down to the contractor level

• BMS has helped to maintain focus on contractor issues which might otherwise have been overlooked

The next interim audit is scheduled for April 2012. Long Range Biosolids Management Plan OCSD’s 2003 Long-Range Biosolids Management Plan (search “Long Range Plan” at www.ocsd.com) set forth recommendations to ensure a sustainable biosolids program. Overall, OCSD has followed this guidance. Exceptions are noted in the individual status notes below.

Table 1 - Implementation of the Long Range Biosolids Management Plan Long Range Biosolids Management

Plan Recommendation Implementation/Status

1. Optimize capital and operations and maintenance (O&M) costs at OCSD’s treatment plants as part of implementation of the long-range plan.

Secondary treatment flows are managed to the lowest cost alternative when flows allow. In addition, digester detention times were managed between both plants by using the sludge diversion line. This allowed the plants to operate at optimal detention times improving volatile solids reductions. Belt filter press operation receives continuous oversight from operations to maintain highest biosolids solids concentrations achievable with the presses. Maintenance staff are proactive at maintaining the belt presses to assure highest performance.

2 Maintain at least three different product-manufacturing options at any given time.

In 2011, OCSD maintained three different products: compost, energy, and land application. See Table 5.

3. Limit maximum participation for any market to one-half of the total biosolids production.

In 2011, OCSD slightly exceeded this guidance with 53% of its solids going to Land Application due to the diversion from EnerTech-Rialto’s material. See Table 5.

4. Limit biosolids management In 2011, OCSD slightly exceeded this

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contracts to a maximum of one-third of total biosolids production per merchant facility, and one-half per contractor (for contractors with multiple product manufacturing facilities).

guidance with 38% of its solids going to compost. See Table 5.

5. Explore funding options for in-county facilities (private capital, OCSD capital, or both).

In 2011, the OCSD Board of Directors modified the biosolids recycling level of service to allow up to 12% of our biosolids to be used in local landfills. In early 2012, OCSD released a request for proposals for landfill and land application to replace a contract expiring at the end of 2012

6. Allocate up to 10 percent of biosolids for participation in emerging markets.

In 2011, OCSD sent about one-third of its biosolids to EnerTech to create a cement kiln alternative fuel pellet.

7. Pursue Orange County-based product manufacturing facilities and maximize the use of horticultural products within the OCSD service area by member agencies and through developing public-private partnerships.

Synagro re-entered the local compost market. OCSD will be partnering with Synagro as opportunities arise.

8. Maintain capacity and options at OCSD’s Central Valley Ranch.

OCSD’s Kings County property, which was sold in late 2011, has not received biosolids since 2004 due to a Kings County Ordinance banning the land application of biosolids. In late 2008, OCSD stopped using Tule Ranch’s Kern County farm.

9. Pursue failsafe backup options (landfilling, alternative daily cover [ADC] for landfills, and dedicated landfilling) to acquire a 100 percent contingency capacity.

In 2011, OCSD maintained approximately fourteen times (1400%) our daily production in contracted contingency capacity for our biosolids. These alternatives include landfilling, land application, and compost.

Goals and Targets The Strategic Planning process described above translated into the following goals and level of service targets updated for 2011 (see November 2011 Strategic Plan).

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Table 2 2011 Biosolids-Related Goals

and Levels of Service (LOS) from Updated Strategic Plan

2011 Accomplishments

Sustainable Biosolids Program (Wastewater Management Goal) Conduct research to reduce the

amount of biosolids produced.

Ongoing goal to be completed annually. See OpenCEL research project in the 2011

Research Report (search for “research” at www.ocsd.com).

Sustainable Biosolids Program (LOS) Maintain NBP Certification for

Biosolids Environmental Management System.

After obtaining the 5-year NBP re-certification in 2008, in 2011 OCSD successfully completed an interim external audit. See section “OCSD’s Biosolids Management System” above for more information on audit outcomes.

See 2011 Biosolids Program Performance Report (search “BMPP” at www.ocsd.com).

Sustainable Biosolids Program (LOS) The percent of biosolids beneficially

reused annually (95% beneficial reuse; 5% landfill), with an exception allowing for an increased 12 % landfill use for peak solids production through 2017

Achieved target: 100% beneficial reuse (0% landfill) (excluding digester cleanings).

See Table 5 in Biosolids Distribution section below.

Sustainable Biosolids Program (LOS) Respond to all biosolids contractor

violations within a week of violation notice

Achieved target

OCSD will protect public health and the environment (Environmental Stewardship LOS) Permit compliance (air, land, and

water). Goal of no Notices of Violation (NOVs).

Target achieved for land, with no NOV’s received.

The Environmental Compliance and Awareness Program (ECAP) was implemented in 2008 to provide all OCSD staff with an efficient method of obtaining compliance information and documentation, streamlining communication between divisions regarding compliance, and tracking compliance and performance targets (listed below). The table below notes which biosolids key performance indicators (KPI) are related to compliance (permit and regulatory requirements), and which are conformance-related (self-imposed requirements that ensure high-quality performance and biosolids processing). Any non-compliance or non-conformance issues that arise, whether internal to OCSD or with its Biosolids Management Contractors, are addressed through OCSD’s corrective and preventive action process.

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Table 3 ECAP Biosolids Key

Performance Indicators 2011 Accomplishments

Class B Certification – contains measurements associated with the production of biosolids to meet time and temperature regulatory requirements in order to certify OCSD biosolids as Class B per 40CFR part 503. Failure to meet Class B standards is a non-conformance issue.

All analytical data for biosolids reporting was completed. All constituents were measured below 40 CFR Part 503 Tables 1 and 3 limits. See compliance data contained in Appendix A.

All biosolids produced met the 15-day minimum detention time average, the minimum average temperature of 95° F, and the average volatile solids reduction of greater than 38%. See Appendix A of this report for digester performance data.

Contractor Oversight – contains items that seek to improve the day-to-day operations in handling biosolids more efficiently, while ensuring optimal biosolids program performance. Failure to meet these performance indicators is a non-conformance issue. Includes: • Biosolids hauler inspections • Contractor Notices of Violation

(NOVs) • Quarterly site inspections • Significant contractor issues, and

inspection findings • Biosolids management options

capacity • Releases • Quarterly reports • Offsite complaints

As an additional check on biosolids haulers, the OCSD biosolids inspector aims to inspect a minimum of 20 biosolids haulers’ trucks per quarter and interview drivers on safety and release response protocols to ensure optimal preparedness. OCSD performed 86 hauler inspections with an average of 21.5 inspections per quarter. This goal was met each quarter with the exception of the 4th quarter (18 inspections) due to limited resources.

Contractor NOVs and other significant contractor issues were monitored for proper resolution. The year started with two (2) unresolved NOVs from 2010. A total of two (2) new NOVs were documented, with one (1) remaining open as of 12/31/11. The contractor is actively working on resolving the NOV.

Twenty one (21) site inspections were performed by OCSD’s inspector with a combined total of 20 findings. All the findings were successfully resolved by the contractor.

Two (2) regulatory issued areas of concern were documented and resolved during the 2011 calendar year.

In 2011, OCSD maintained approximately fourteen times (1400%) its daily production in contracted contingency capacity for its biosolids. OCSD’s target is 200% of maximum daily biosolids production.

Two (2) offsite and two (2) onsite biosolids releases occurred in 2011. None of them adversely impacted the environment. Each was promptly cleaned and addressed through OCSD’s corrective and preventive action process.

Quarterly reports were received from all biosolids management contractors.

Offsite Complaints (odor/flies) South Kern Composting: 13 Arizona Soils Composting: 14 Tule Ranch Arizona: 0 EnerTech: 0

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Table 3 ECAP Biosolids Key

Performance Indicators 2011 Accomplishments

Terra Renewal (Failsafe for EnerTech): 0 Budget – tracks the portion of the budget

spent each month. Also tracks the amount of dollars spent fiscal year-to-date for each month, and compares it with the proportional part of the budget allocated up to that month. Failure to meet cumulative monthly budget could result in failure to meet the annual budget.

• During calendar year 2011, expenditures averaged 94% of the monthly budgeted amounts.

Program History A comprehensive history of OCSD’s Biosolids Program may be found in the 2010 Biosolids Compliance Report. The following are the developments during calendar year 2011:

• OCSD recycled 100% of its biosolids (not including digester cleanings) from 2006 to 2011.

• In January 2011, Tule Ranch subcontracted their land application operations to AgTech, and managed OCSD biosolids at 2 sites in Yuma.

• During 2011, EnerTech Environmental continued implementation of their Single Train Technical Plan. March 2012 is the plan’s deadline to finish commissioning process. During the start-up process, biosolids not processed at the Rialto facility were land-applied in Yuma County, Arizona.

• In June 2011 OCSD completed start-up of the new trickling filters at Plant No. 2. Biosolids production increased by an average 90 tons/day with the start-up of these trickling filters.

• OCSD is planning to replace the belt filter presses with new dewatering centrifuge facilities at both plants. Plant No 1 is scheduled to operate centrifuges by 2015 and Plant No. 2 by 2017. In that same timeframe, the Irvine Ranch Water District, which currently discharges solids to OCSD, plans to build and operate their own solids treatment facilities. As a result, OCSD anticipates an increase in the production of biosolids peaking at about 790 tons per day in 2013, and then decreasing to less than 710 tons per day by 2017.

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Figure 1 presents OCSD’s historical trends of biosolids production in tons per year.

Figure 1: Biosolids Production History from July 1985 – December 2011 See Biosolids Distribution section below for information on where OCSD’s biosolids were utilized in 2011. OCSD’s Treatment Plants Reclamation Plant No. 1, located in the city of Fountain Valley, treated an average of 96 MGD during the year 2011. Treatment Plant No. 2, located in the City of Huntington Beach, treated an average of 108 MGD of wastewater during that same period. A diversion structure, located after the flow meters at Reclamation Plant 1, allows the wastewater from any of six sewer trunks tributary to Plant No. 1, to be diverted to Plant No. 2 to match wastewater flow with the plants’ treatment capacities. The headworks at both facilities include mechanically-cleaned bar screens, main sewage pumps and aerated grit chambers where heavier particles and debris are removed. Following the grit and screening process, the wastewater undergoes advanced primary treatment. The advanced primary treatment process (amended with ferric chloride and anionic polymers) includes the primary sedimentation basins (clarifiers) where the organic solids settle and are separated from the

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wastewater. The covered primary clarifiers capture potentially-odorous air that is scrubbed to meet OCSD’s odor control policy requirements. All dry-weather flow of primary treated wastewater is routed for secondary treatment to the nitrification activated sludge process at Plant 1, an oxygen-activated sludge process at Plant 2, and the trickling filters at both plants. The Orange County Water District (OCWD) Ground Water Replenishment System (GWRS) utilizes OCSD’s secondary treated water from Plant 1 to purify and meet drinking water standards. The GWRS uses advanced treatment processes including microfiltration and reverse osmosis. GWRS water is used as a barrier for salt water intrusion and to recharge groundwater basins. In 2011, the GWRS treated an average of 80 MGD of secondary effluent to produce purified water for reuse. The Steve Anderson Lift Station diverts influent water from Plant No. 2 to Plant No. 1 to stabilize the diurnal nature of reclamation Plant No. 1 to provide a more steady flow for GWRS. Secondary effluent not sent to GWRS flows to Plant No. 2 and blends with treated wastewater from Plant No. 2 prior to ocean discharge through OCSD’s 120-inch diameter, five-mile long ocean outfall. The settled solids from the primary and secondary treatment processes from both plants are pumped into anaerobic digesters for stabilization. These solids are treated according to 40 CFR Part 503, section 503.32(b)(3) for class B classification with respect to pathogens and section 503.33 (b)(1) for vector attraction reduction by anaerobic digestion. This rule requires a minimum average retention time of 15 days at an average temperature of greater than 95 degrees Fahrenheit and a volatile solids reduction greater than 38 percent. The stabilization process produces biogas (primarily methane gas), which OCSD captures to fuel internal combustion engines that provide power to three 2,500-kilowatt and five 3,000 kilowatt electric generators. Electricity produced from the digester gas produces the majority of the power needed to operate the treatment plants. The anaerobically-digested biosolids are dewatered to 16-22 percent total solids utilizing belt filter presses. The dewatered solids are loaded into trucks for transport to beneficial reuse sites. OCSD’s loading facilities allows for rapid loading of biosolids into trucks stationed on scales within a building using odor control. Plant No. 1 is limited to the amount of solids they can anaerobically digest and dewater until the thickening and dewatering centrifuge facility is completed. Primary sludge can be diverted to the influent of Plant No. 2 when digestion detention times exceed 19 days or if a belt filter press is out of service. The additional wastewater treated at Plant No. 1 for the GWRS causes a relative increase in sludge production. Until two solids-handling projects are completed (scheduled for 2014), the capacity of Plant No. 1 solids treatment systems is inadequate to handle the increased sludge production. A portion of the primary

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sludge produced at Plant No. 1 is diverted and conveyed to Plant 2 through the interplant line for treatment at Plant No. 2. Reclamation Plant No. 1 – 2011 Biosolids Production and Processes Reclamation Plant No. 1 produced 22,939 dry metric tons of biosolids from January 1, 2011 through December 31, 2011. These biosolids were anaerobically digested for an average of 19 days at 37 degrees Celsius (98 degrees Fahrenheit) resulting in an average volatile solids reduction of 57 percent over this reporting period. This process provides compliance with the “Class B Pathogen Reduction” and “Vector Attraction Reduction” definition for “Class B” biosolids as defined in 40 CFR Part 503.32(b)(3) and 503.33(b)(1), respectively. No digester cleanings were removed from Plant No. 1 digesters in 2011. Treatment Plant No. 2 – 2011 Biosolids Production and Processes Treatment Plant No. 2 produced 24,069 dry metric tons of biosolids from January 1, 2011 through December 31, 2011. The process at Plant No. 2 is similar to Plant No. 1 in that the biosolids were anaerobically digested for an average of 21 days at 37 degrees Celsius (98 degrees Fahrenheit). Biosolids from Plant No. 2 had an average volatile solids reduction of 65 percent. This process provides compliance with the “Class B Pathogen Reduction” and “Vector Attraction Reduction” definition for “Class B” biosolids as defined in 40 CFR Part 503.32(b)(3) and 503.33(b)(1), respectively. Additionally, 24 dry metric tons of digester cleaning material (screened overs) were removed from digester M at Plant No. 2 and taken to South Yuma County Landfill. The removed digester cleaning material was tested and passed all the landfill analytical requirements for this landfill. Biosolids Management - Contractors Biosolids produced in 2011 at OCSD’s two treatment facilities were managed by three biosolids management contractors:

Table 4 Tule Ranch 4324 E. Ashlan Ave. Fresno, CA 93726 Contact: Shaen Magan Phone: (559) 970-9432 Synagro P.O. Box 265 Taft, CA 93268 Contact: Lorrie Loder Phone: (909) 322-0388

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EnerTech 503 E. Santa Ana Avenue Bloomington, California 92316 Contact: Rus Miller Phone: (949) 276-2344 Terra Renewal – subcontractor to EnerTech and reporting for EnerTech 12340 Seal Beach Blvd., Ste. B-383 Seal Beach, CA 90740 Contact: Chris Marks Phone: (760) 434-0003 Ag Tech, LLC – subcontractor to Tule Ranch and reporting for Tule Ranch and Synagro (digester cleanings) PO Box 2854 Yuma, Arizona 85366 Contact: Susan Pemberton Phone: (928) 341-9625

These biosolids management contractors and subcontractors provide OCSD with diversification and reliability and are thereby important partners in OCSD’s biosolids management team. Contractor’s compliance annual reports are available at www.ocsd.com (search for “503”) when submitted.

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Biosolids Distribution For this reporting period, OCSD’s biosolids were beneficially reused in the following areas:

Table 5 - Biosolids Distribution by Vendor and Biosolids Management Options for 2011 Summary of Pollutants OCSD’s Pretreatment Program has been very effective in lowering the content of metals in both the influent wastewater and, therefore, the biosolids. OCSD’s influent wastewater meets drinking water standards for metals. Please see Appendix B to review the biosolids chapter of OCSD’s Source Control Annual Report. Tables 1 and 2 in the compliance data section (Appendix A) compare the concentration limits of the pollutants listed in 40 CFR 503 to OCSD’s average biosolids concentrations for each plant. The maximum concentrations of all pollutants in OCSD’s biosolids are well below the conservative Table-1 Ceiling Limits and Table-3 Exceptional Quality Limits found in 40 CFR Part 503. In accordance with OCSD’s Ocean Discharge NPDES permit, biosolids are also tested semi-annually for all pollutants listed under Section 307(a) of the Clean Water Act. Appendix C contains the summary of all the priority pollutants analyzed in the plants’ influents, effluent, and biosolids.

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Determination of Hazardousness Legal Definition OCSD’s 2004 Ocean Discharge NPDES permit requires OCSD to test annually for hazardousness in accordance with California law. Hazardous waste is defined under the provisions of California Code of Regulations, Title 22, Chapter 11, Article 5. Determination OCSD’s biosolids are tested at least annually for the determination of hazardousness. OCSD does not produce biosolids with the listed substances in amounts deemed as hazardous in Title 22 above (see OCSD’s Biosolids Monitoring data in Appendix C, Summary of Priority Pollutants and Trace Constituents Analysis – 2010). As a result of this determination, OCSD’s biosolids are non-hazardous.

APPENDIX A

Table 1: Biosolids Monitoring and Reporting for 2011, Plant 1 Table 2: Biosolids Monitoring and Reporting for 2011, Plant 2

Table 3: Digester Cleaning Material - Beneficial Reuse for 2011 Table 4: Digester Cleaning Material - Disposal for 2011 Notice and Necessary Information Certification Forms

Constituent (mg/Kg) Dry Jan Feb Mar April May June July Aug Sep Oct Nov Dec Ceiling EQ

Arsenic 8.6 9.7 8.6 8.8 8.4 9.2 6.2 7.6 9.8 10 11 7.6 8.8 75 41Cadmium 3.2 3.6 3.5 3.4 <2.1 2.9 4.2 4.1 4.0 3.6 6.0 1.8 3.7 85 39Copper 560 560 600 600 520 580 580 480 560 520 670 440 556 4300 1500Lead <23 <24 <22 <24 <21 <22 <22 <22 <23 <22 <21 <38 <38 840 300Mercury 1.1 1.1 1 1.2 1.1 2.1 1.3 1.3 0.95 1 1.4 1.3 1.2 57.0 17.0Molybdenum 14 15 14 15 14 14 12 7 16 16 18 7 13 75 N/ANickel 36 37 38 36 34 34 40 32 34 36 48 20 35 420 420Selenium 17 26 10 6.5 7 16 8.5 5.5 11 6.5 6 26 12.2 100 100Zinc 680 720 740 730 690 740 780 650 840 740 880 580 731 7500 2800Total Kjeldahl Nitrogen * 43,000 55,000 63,000 57,000 55,000 60,000 58,000 55,000 54,000 49,000 54,000 48,000 54,250

Digester Detention Time (days) 22 21 19 19 18 19 19 20 19 18 17 17 19Digester Temperature (º F) 98 97 97 98 98 98 98 98 98 98 98 98 98Digester Temperature (ºC) 37 36 36 37 37 37 37 37 37 37 37 37 37Volatile Solids Reduction (%) 60 58 59 52 54 54 54 59 54 54 64 60 57Biosolids Cake Solids (%) 19 17 18 18 19 18 18 18 18 18 20 19 18

EnerTech CA (Wet tons) 3,649 2,244 2,569 2,021 1,816 893 1,084 1,770 1,133 1,479 252 600 19,512EnerTech Failsafe backup AZ (wet tons) 1,419 2,840 3,596 3,486 3,498 4,769 3,536 2,944 4,030 3,700 5,097 4,785 43,699

Synagro CA (wet tons) 5,823 4,864 5,869 5,461 2,896 0 4,211 5,120 5,068 5,149 5,611 5,828 55,901Synagro AZ (wet tons) 149 125 151 428 3,476 5,465 1,801 1,086 957 1,243 637 735 16,253Tule Ranch AZ (wet tons) 463 0 132 79 238 0 0 608 315 97 369 97 2,398Dry Metric Tons 1,982 1,553 2,011 1,874 2,055 1,817 1,736 1,882 1,878 1,905 2,171 2,076 22,939* No ceiling or EQ limit

137,763

DRY METRIC TONS 22,939

15 days minimum detention95 - 131 oF 35 - 55 oC

38% or higher

Quantity Generated Total Total Biosolids Generated

WET TONS

Process Assessment Pathogen and vector reduction requirements (Class B, Option 1)

Table 1 - Orange County Sanitation District503 Analyses Biosolids Monitoring and Reporting for 2011 503 Criteria

Reclamation Plant #1, Fountain Valley, CAAnnual Mean

Constituent Dry Weight (mg/Kg)

Constituent (mg/Kg) Dry Jan Feb Mar April May June July Aug Sep Oct Nov Dec Ceiling EQ

Arsenic 12.0 12.0 10.0 10.0 11.0 12.0 8.2 12.0 10.0 8.6 12.0 6.6 10.2 75 41Cadmium 3.0 3.2 2.4 2.5 <3 3.0 3.7 3.4 3.6 3.3 4.4 2.6 3.2 85 39Copper 500 530 520 580 570 540 540 520 590 520 720 380 546 4300 1500Lead <19 <20 <19 <20 <30 <21 <22 <21 <20 26 <21 <21 <30 840 300Mercury 0.8 1.0 1.0 1.0 1.0 1.2 1.0 1.3 0.8 2.6 1.6 1.4 1.2 57 17Molybdenum 14 14 15 14 16 18 16 18 19 17 20 12 16 75 N/ANickel 35 33 34 26 <30 30 39 28 32 32 38 20 32 420 420Selenium 14 26 11 11 9 12 12 8 16 10 8 19 13 100 100Zinc 720 700 700 720 790 750 790 780 870 740 910 560 753 7500 2800Total Kjeldahl Nitrogen * 42000 57000 42000 54000 74000 56000 53000 59000 47000 54000 55000 55000 54000

Digester Detention Time (days) 25 23 23 23 26 21 18 18 19 20 19 21 21Digester Temperature (º F) 98 98 98 98 98 98 99 98 98 98 98 98 98Digester Temperature (ºC) 37 37 37 37 37 37 37 37 37 37 37 37 37Volatile Solids Reduction (%) 71 66 65 63 66 66 60 67 64 58 64 65 65Biosolids Cake Solids (%) 22 20 21 20 18 20 19 20 20 20 20 19 20

EnerTech CA (Wet tons) 196 121 124 48 256 1,180 1,111 741 331 202 0 205 4,513EnerTech Failsafe backup AZ (wet tons) 1,149 1,228 1,002 1,290 1,093 964 1,208 1,687 1,364 1,318 1,337 1,721 15,363Synagro CA (wet tons) 1,830 2,529 2,666 1,962 727 0 2,223 3,153 2,487 2,674 2,022 2,483 24,756

Synagro AZ (wet tons) 0 0 0 0 574 2,898 906 0 151 0 0 50 4,579Tule Ranch AZ (wet tons) 4,683 5,202 5,959 5,600 6,138 7,411 7,589 8,020 7,602 8,225 7,284 7,659 81,372Dry Metric Tons 1,568 1,647 1,857 1,614 1,435 2,259 2,247 2,467 2,165 2,253 1,931 2,088 23,531NA - Data not available* No ceiling or EQ limit

130,583

DRY METRIC TONS 23,531

15 days minimum detention95 - 131 oF35 - 55 oC

38% or higher

TotalQuantity Generated Total Biosolids Generated

WET TONS

Process Assessment Pathogen and vector reduction requirements (Class B, Option 1)

Table 2 - Orange County Sanitation District503 Analyses Biosolids Monitoring and Reporting for 2011 503 Criteria

Wastewater Treatment Plant #2, Huntington Beach, CAAnnual Mean

Constituent Dry Weight (mg/Kg)

Constituent (mg/Kg) Dry Jan Feb Mar April May June July Aug Sep Oct Nov Dec Annual Mean

Arsenic - - - - 10 - - - - - - - 10 75 41Cadmium - - - - 6.9 - - - - - - - 6.9 85 39Copper - - - - 450 - - - - - - - 450.0 4300 1500Lead - - - - 69 - - - - - - - 69.0 840 300Mercury - - - - 1 - - - - - - - 1 57 17Molybdenum - - - - 34 - - - - - - - 34.0 75 N/ANickel - - - - 69 - - - - - - - 69.0 420 420Selenium - - - - 17 - - - - - - - 17 100 100Zinc - - - - 570 - - - - - - - 570.0 7500 2800Digester Cleaning Total Solids(%) - - - - 54 - - - - - - - 54.1

Quantity Generated TotalLand Application AZ (Digester Cleanings) (wet tons) - - - - 1,096 - - - - - - - 1,096 Dry Metric Tons - - - - 538 - - - - - - - 538

Constituent (mg/Kg) Dry Jan Feb Mar April May June July Aug Sep Oct Nov Dec Annual Mean

Digester Cleaning Total Solids(%) - - - - 54 - - - - - - - 54

Quantity Generated TotalLandfill AZ (Digester Cleanings) (wet tons)** - - - - 49 - - - - - - - 49 Dry Metric Tons - - - - 24 - - - - - - - 24 **South Yuma County Landfill

Wet Tons 49

Dry Metric Tons 24

Table 4 - Orange County Sanitation DistrictDigester Cleaning Material - Disposal for 2011

Wastewater Treatment Plant #2, Huntington Beach, CATotal Biosolids Generated

Total Biosolids Generated

Wet Tons 1,096

Dry Metric Tons 538

Table 3 - Orange County Sanitation DistrictDigester Cleaning Material - Beneficial Reuse for 2011

Wastewater Treatment Plant #2, Huntington Beach, CA

3/24/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

3/25/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

3/16/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: January 1- 31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 1/5/11, 1/12/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 8.6 3.2 560 <23 1.1 14 36 17 680 34,700 8,300 42 19

Table 3

41

39

1,500

300 17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840 57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 21.5 to 22.2 days at a mean minimum temperature of 98 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.15 %VSout = 1.25 %VSR = 60.4

3/24/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

3/25/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

3/16/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: January 1- 31, 2010 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 1/5/10, 1/12/10

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 12 3.0 500 <19 0.82 14 35 14 720 33,800 8,200 58 22

Table 3

41

39

1,500

300

17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840

57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 24.5 to 25.7 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 4.07 %VSout = 1.2 %VSR = 70.5

4/26/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

4/26/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

4/13/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: February 1- 28, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 2/2/11, 2/9/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 9.7 3.6 560 <24 1.1 15 37 26 720 45,800 9,200 49 17

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 21.3 to 22.1 days at a mean minimum temperature of 97 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.07 %VSout = 1.3 %VSR = 57.7

4/26/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

4/26/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

4/13/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: February 1- 28, 2010 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 2/2/11, 2/9/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 12 3.2 530 <20 1.0 14 33 26 700 49,800 7,200 50 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 22.6 to 25.1 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.87 %VSout = 1.3 %VSR = 66.4

6/16/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

6/21/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

6/13/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: March 1- 31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 3/2/11, 3/9/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 8.6 3.5 600 <22 1.0 14 38 10 740 54,200 8,800 53 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 19.4 to 21.1 days at a mean minimum temperature of 97 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.06 %VSout = 1.25 %VSR = 59.2

6/16/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

6/21/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

6/13/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: March 1- 31, 2010 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 3/2/11, 3/9/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 10 2.4 520 <19 1.0 15 34 11 700 32,900 9,100 60 21

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 23.2 to 24.5 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 4.04 %VSout = 1.4 %VSR = 65.3

7/11/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

7/11/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

6/29/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: April 1- 30, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 4/6/11, 4/13/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 8.8 3.4 600 <24 1.2 15 36 6.5 730 48,100 8,900 58 18

Table 3

41

39

1,500

300 17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840 57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 18.6 to 19.6 days at a mean minimum temperature of 98 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.13 %VSout = 1.5 %VSR = 52.0

7/11/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

7/11/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

6/29/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: April 1- 30, 2010 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 4/6/11, 4/13/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 10 2.5 580 <20 1.0 14 26 11 720 45,900 8,100 54 20

Table 3

41

39

1,500

300

17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840

57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 23.0 to 34.9 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.82 %VSout = 1.4 %VSR = 63.4

8/3/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

8/4/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

7/14/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: May 1- 31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 5/4/11, 5/11/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 8.4 <2.1 520 <21 1.1 14 34 7.0 690 48,400 6,600 48 19

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 18.0 to 18.7 days at a mean minimum temperature of 98 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 2.84 %VSout = 1.3 %VSR = 54.2

8/3/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

8/4/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colston, Jim

7/14/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: May 1- 31, 2010 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 5/4/11, 5/11/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 11 <3.0 570 <30 0.96 16 <30 9 790 66,300 7,700 62 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 25.7 to 28.1 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 4.02 %VSout = 1.35 %VSR = 66.4

9/8/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

9/12/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

9/8/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: June 1- 30, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 6/1/11, 6/8/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 9.2 2.9 580 <22 2.1 14 34 16 740 53,800 6,200 56 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 18.5 to 19.3 days at a mean minimum temperature of 98 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 2.84 %VSout = 1.3 %VSR = 54.2

9/8/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

9/12/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

9/8/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: June 1- 30, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 6/1/11, 6/8/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 12 3.0 540 <21 1.2 18 30 12 750 47,900 8,100 64 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 20.5 to 25.5 days at a mean minimum temperature of 98° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 4.02 %VSout = 1.35 %VSR = 66.4

10/11/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

10/17/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

9/29/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: July 1-31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 07/06/11, 07/13/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 6.2 4.2 580 <22 1.3 12 8.5 9.0 780 51,100 6,900 <11 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 18.5 to 20 days at a mean minimum temperature of 98 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 2.70 %VSout = 1.25 %VSR = 53.6

10/11/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

10/17/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

9/29/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: July 1-31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 07/06/11, 07/13/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 8.2 3.7 540 <22 1.0 16 39 12 790 46,400 6,600 66 19

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 18.3 to 20.7 days at a mean minimum temperature of 99 ° F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.27 %VSout = 1.30 %VSR = 60.2

10/31/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

10/31/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

10/26/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: August 1-31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 08/03/11, 08/10/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 7.6 4.1 480 <22 1.3 7.0 32 5.5 650 40,000 15,000 42 18

Table 3

41

39

1,500

300 17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840 57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 19.8 to 20.2 days at a mean minimum temperature of 98°F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 2.9 %VSout = 1.2 %VSR = 58.6

10/31/2011

XDavid R. Heinz [email protected] Operations Manager (714)593-7383Signed by: Heinz, Dave

10/31/2011

XJames E. Colston [email protected]. Compliance Manager (714) 593-7450Signed by: Colstonj

10/26/2011

XRonald Coss [email protected] Manager (714)593-7508Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: August 1-31, 2011 Pollutant and Nitrogen concentrations (report results on 100% dry weight basis).

Sampling date(s): 08/03/11, 08/10/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg) Cr

(mg/kg)%

solids

Result 12 3.4 520 <21 1.3 18 28 8.0 780 45,000 14,000 66 20

Table 3

41

39

1,500

300

17 N/A 420 100 2,800

N/A

N/A N/A N/A

Table 1

75

85

4,300

840

57 75 420 100 7,500

N/A

N/A 3,000 N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. 503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment. Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids requirements have been met. I am aware that there are significant penalties for false certification including the possibility of fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR part 503 have been met via anaerobic digestion by digesting solids for a mean residence time of 17.8 to 19.0 days at a mean minimum temperature of 98°F

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR part 503 and Arizona Administrative Code R18-9-1010.A have been met using data analyzed by an Arizona certified laboratory to comply with Option 1: %VSin = 3.96 %VSout = 1.3 %VSR = 67.2

11/30/2011

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

12/1/2011

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

11/29/2011

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: September 1-30, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 09/07/11, 09/14/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 9.8 4.0 560 <23 0.95 16 34 11 840 47,400 6,600 52 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 18.6 to

20.2 days at a mean minimum temperature of 98 ° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 2.61

%VSout = 1.2 %VSR = 54.1

11/30/2011

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

12/1/2011

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

11/29/2011

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: September 1-30, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 09/07/11, 09/14/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 10 3.6 590 <20 0.84 19 32 16 870 40,200 6,800 58 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 18.8 to

20.2 days at a mean minimum temperature of 98 ° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 3.56

%VSout = 1.3 %VSR = 63.5

12/20/2011

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

12/20/2011

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

12/13/2011

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: October 1-31, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 10/05/11, 10/12/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 10 3.6 520 <22 1.0 16 36 6.5 740 40,100 8,900 55 18

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 18.0 to

18.7 days at a mean minimum temperature of 98 ° F

...degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 2.71

%VSout = 1.25 %VSR = 53.9

12/20/2011

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

12/20/2011

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

12/13/2011

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: October 1-31, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 10/05/11, 10/12/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 8.6 3.3 520 26 2.6 17 32 10 740 44,000 10,000 54 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 19.5 to

20.1 days at a mean minimum temperature of 98 ° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 3.32

%VSout = 1.40 %VSR = 57.8

1/26/2012

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

1/26/2012

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

1/16/2012

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: November 1-30,2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 11/02/11, 11/09/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 11 6.0 670 <21 1.4 18 48 6.0 880 47,800 6,200 74 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 17.4 to

18.5 days at a mean minimum temperature of 98° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 3.17

%VSout = 1.15 %VSR = 63.7

1/26/2012

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

1/26/2012

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

1/16/2012

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: November 1-30,2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 11/02/11, 11/09/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 12 4.4 720 <21 1.6 20 38 8.0 910 47,700 7,300 70 20

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 19.3 to

20.9 days at a mean minimum temperature of 98° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 3.58

%VSout = 1.3 %VSR = 63.7

1/31/2012

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

1/31/2012

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

1/26/2012

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Reclamation Plant #1, Fountain Valley, CA

Monitoring Period: December 1 - 31, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 12/7/11, 12/14/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 7.6 1.8 440 <38 1.3 6.5 20 26 580 43,300 4,700 44 19

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 17.4 to

19.1 days at a mean minimum temperature of 98° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 2.84

%VSout = 1.15 %VSR = 59.5

1/31/2012

XDavid R. Heinz [email protected]

OM Operations Manager (714)593-7383

Signed by: Heinz, Dave

1/31/2012

XJames E. Colston [email protected]

Env. Compliance Manager (714) 593-7450

Signed by: Colston, Jim

1/26/2012

XRonald Coss [email protected]

Laboratory Manager (714)593-7508

Signed by: Coss, Ronald

Notice and Necessary Information To be Completed by Preparers of Class B Biosolids

Facility Name: Orange County Sanitation District Treatment Plant #2, Huntington Beach, CA

Monitoring Period: December 1 - 31, 2011

Pollutant and Nitrogen concentrations (report results on 100% dry weight basis). Sampling date(s): 12/07/11, 12/14/11

As

(mg/kg)

Cd

(mg/kg)

Cu

(mg/kg)

Pb

(mg/kg)

Hg

(mg/kg)

Mo

(mg/kg)

Ni

(mg/kg)

Se

(mg/kg)

Zn

(mg/kg)

Org-N (mg/kg)

Ammonia

(mg/kg)

Cr

(mg/kg)

%

solids

Result 6.6 2.6 380 <20 1.4 12 20 19 560 48,400 6,600 40 19

Table 3

41

39

1,500

300

17

N/A

420

100

2,800

N/A

N/A

N/A

N/A

Table 1

75

85

4,300

840

57

75

420

100

7,500

N/A

N/A

3,000

N/A

Certifications:

NPDES permit: I certify, under penalty of law, that this document and all attachments were prepared under my direction or

supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the

information submitted. Based on my inquiry of the person or persons who manage the system or the persons directly

responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine

and imprisonment for knowing violations.

503 Class B: I certify, under penalty of law, that the Class B pathogen requirements in 503.32(b) and the vector attraction

reduction requirement in 503.33(b)(1) have been met. This determination has been made under my direction and supervision in

accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to

determine that the pathogen requirements and vector attraction requirements have been met. I am aware that there are

significant penalties for false certification including the possibility of fine and imprisonment.

Arizona Class B: I certify, under penalty of law, that the pollutant analyses and the description of pathogen treatment and

vector attraction reduction activities have been made under my direction and supervision and under a system designed to ensure

that qualified personnel properly gather and evaluate the information used to determine whether the applicable biosolids

requirements have been met. I am aware that there are significant penalties for false certification including the possibility of

fine and imprisonment

Class B Pathogen Reduction Class B pathogen reduction requirements from 40 CFR

part 503 have been met via anaerobic digestion by

digesting solids for a mean residence time of 20.7 to

21.6 days at a mean minimum temperature of 98° F

degrees F.

Vector Attraction Reduction The vector attraction reduction requirements of 40 CFR

part 503 and Arizona Administrative Code R18-9-1010.A

have been met using data analyzed by an Arizona certified

laboratory to comply with Option 1: %VSin = 3.99

%VSout = 1.4 %VSR = 64.9

APPENDIX B

OCSD’s Source Control Program Annual Report (Chapter 9) FY 2010-2011 Solids Management Program

9.1

chapter 9

SOLIDS MANAGEMENT PROGRAM

9.1 INTRODUCTION

This section provides an overview of the Biosolids Management Program for the Orange County Sanitation District (OCSD) focusing on the quality with respect to metals. Biosolids are the treated solids resulting from the process of separating solids from water in the wastewater treatment process.

OCSD’s biosolids management program has maintained certification with the National Biosolids Partnership (www.biosolids.org) since 2003. The pretreatment program program is a key element in maintaining this certification as well as maintaining our continued goal of recycling our biosolids through their minimization of negative constituents into the collection system and ultimately the solids.

OCSD’s annual biosolids compliance report is completed and posted online in February. Visit OCSD.com’s Document Center and search for “503” to access the most recent document that contains our Biosolids Management Program history, certifications, regulations, quantities, and how and where biosolids are recycled. OCSD also produced an annual biosolids brochure summarizing our program accomplishments and future goals (search the Document Center for “bmpp”).

9.2 BIOSOLIDS QUALITY

Biosolids quality plays an important role in determining the feasibility of recycling versus disposal options. OCSD's pretreatment program has been very effective in reducing and maintaining levels of pollutants. The ceiling concentrations and EQ (exceptional quality) concentrations promulgated by the EPA's sludge regulations (40 CFR 503) are presented in the figures as a reference. For FY 2010/11, OCSD's biosolids met the EQ limits for all the regulated parameters.

The levels in trace metals, shown in Figures 9.1 - 9.10, have provided opportunity for beneficial recycling of biosolids including direct application to agricultural land and composting for use as a soil amendment.

TABLE 9.1 Trends in Trace Metal Content of Biosolids, Fiscal Years 2000–2011

(Concentration in mg/kg, dry weight) Orange County Sanitation District, Environmental Compliance Division

Metal

Fiscal Year

Exceptional Quality Limits

Plant No. 1 Plant No. 2

Min. Max. Avg. Min. Max. Avg.

Arsenic 41 1999-00 5.5 9.7 8.5 6.9 12 8.5 2000-01 1.4 8.1 6.3 3.1 9.7 7.8 2001-02 3.7 6.5 4.9 4 7.5 6.4 2002-03 4.2 6.4 5.4 5.3 9 7 2003-04 3.5 5 4.3 4 6.7 5.7 2004-05 3.3 6.7 5 5.8 9.1 7 2005-06 0.9 7.7 4.4 4.6 9.8 6.9 2006-07 2.7 7.2 5.3 5.1 11 7.3 2007-08 2.9 9.0 6.2 4.1 14 7.9 2008-09 4.3 12 7.1 3.5 13 9.0 2009-10 2.0 10.0 5.2 4.4 10.0 7.2 2010-11 7.2 9.7 8.4 8.6 12 10.4

9.2

TABLE 9.1 Trends in Trace Metal Content of Biosolids, Fiscal Years 2000–2011 (Concentration in mg/kg, dry weight) Orange County Sanitation District, Environmental Compliance Division

Metal

Fiscal Year

Exceptional Quality Limits

Plant No. 1 Plant No. 2

Min. Max. Avg. Min. Max. Avg.

Cadmium 39 1999-00 14 24 20 8 11 10 2000-01 15 37 22 7 13 10 2001-02 9 16 12 8 14 10 2002-03 8 11 9 6 8 7 2003-04 7 19 13 3 9 6 2004-05 11 22 17 6 10 8 2005-06 5 11 7 3 8 6 2006-07 3.7 6.1 5 2 4 3.3 2007-08 3.2 11 5.5 2.6 6.4 3.8 2008-09 2.5 6.20 4.1 1.7 4.4 3.0 2009-10 1.1 4.4 2.9 1.0 4.8 2.81 2010-11 1.2 3.8 2.6 1.4 5.0 2.5 Chromium ** 1999-00 86 110 100 84 120 100 2000-01 99 227 149 82 140 101 2001-02 90 217 120 92 163 120 2002-03 71 120 97 76 110 90 2003-04 71 260 113 38 100 78 2004-05 75 140 99 59 75 66 2005-06 55 78 63 47 60 54 2006-07 51 77 62 47 86 60 2007-08 50 62 54 46 77 60 2008-09 44 65 55 42 88 62.3 2009-10 29 56 44 30 54 47 2010-11 41 58 47 50 66 59 Copper 1,500 1999-00 750 920 851 783 900 838 2000-01 810 1,100 938 670 960 885 2001-02 540 820 710 650 720 690 2002-03 660 830 710 560 810 660 2003-04 620 790 680 490 700 600 2004-05 570 690 623 500 680 593 2005-06 600 710 641 520 680 603 2006-07 600 800 686 540 620 576 2007-08 500 650 570 460 630 538 2008-09 500 590 560 500 540 523 2009-10 420 620 543 370 560 497 2010-11 520 600 567 500 720 574 Lead 300 1999-00 48 57 53 40 53 47 2000-01 51 86 63 38 64 51 2001-02 35 57 44 30 69 42 2002-03 30 46 36 28 38 32 2003-04 27 47 35 22 29 26 2004-05 27 41 32 16 26 22

9.3

TABLE 9.1 Trends in Trace Metal Content of Biosolids, Fiscal Years 2000–2011 (Concentration in mg/kg, dry weight) Orange County Sanitation District, Environmental Compliance Division

Metal

Fiscal Year

Exceptional Quality Limits

Plant No. 1 Plant No. 2

Min. Max. Avg. Min. Max. Avg.

2005-06 18 32 27 14 29 22 2006-07 23 30 26 14 24 21 2007-08 6 30 20 6 24 14 2008-09 11 25 21 6 21 15 2009-10 9 44 23 9 20 17 2010-11 21 24 23 9 30 20 Mercury 17 1999-00 1.5 2.4 1.9 1.3 2.7 2 2000-01 1.5 2.3 1.9 1 2.7 1.8 2001-02 1.7 2.6 2.2 1.6 2.4 2 2002-03 1.7 2.6 2.2 1.6 2.4 2 2002-04 1.4 2.2 1.7 1.4 2.3 1.7 2004-05 1 2.4 1.8 1.1 2.2 1.4 2005-06 1.5 2 1.7 1.2 6.4 2.1 2006-07 1.1 2.4 1.6 1.3 2.5 1.7 2007-08 1.1 4.2 1.9 1.3 2.6 1.6 2008-09 1.0 1.9 1.4 1.0 2.6 1.4 2009-10 1.0 3.2 1.4 0.9 1.6 1.3 2010-11 0.8 2.2 1.3 0.8 2.3 1.2 Molybdenum ** 1999-00 18 26 21 17 22 20 2000-01 15 22 18 11 23 16 2001-02 15 21 18 12 18 14 2002-03 16 26 20 10 18 13 2003-04 17 24 20 12 17 14 2004-05 14 19 17 10 18 15 2005-06 9 18 15 12 18 15 2006-07 13 22 18 14 18 16 2007-08 12 17 13 12 18 15 2008-09 12 16 15 8 16 14 2009-10 6 16 13 6 14 10 2010-11 12 19 15 4.8 18 14 Nickel 420 1999-00 105 180 130 102 180 126 2000-01 140 240 203 71 217 121 2001-02 100 237 150 83 123 100 2002-03 95 160 120 58 97 77 2003-04 90 300 170 54 83 72 2004-05 69 150 114 36 62 48 2005-06 58 87 66 32 60 39 2006-07 44 60 54 28 44 34 2007-08 34 58 45 24 56 31 2008-09 30 41 35 22 37 29 2009-10 12 36 28 9 27 21 2010-11 28 46 37 14 38 32

9.4

TABLE 9.1 Trends in Trace Metal Content of Biosolids, Fiscal Years 2000–2011 (Concentration in mg/kg, dry weight) Orange County Sanitation District, Environmental Compliance Division

Metal

Fiscal Year

Exceptional Quality Limits

Plant No. 1 Plant No. 2

Min. Max. Avg. Min. Max. Avg.

Selenium 100 1999-00 4.7 15 10 3.2 9.3 7.5 2000-01 4.4 22 9.7 4.2 12 8.4 2001-02 4.1 17 8.2 2.8 16 8.3 2002-03 4 10 8 5 12 7 2003-04 3.2 14 8 2.1 12 6 2004-05 3.6 11 7.2 1.3 10 4.7 2005-06 5.5 12 7.8 3 9.5 6 2006-07 4.7 13 8.2 1.8 14 5.8 2007-08 3.0 14 8 1.4 11 5.6 2008-09 2.5 14.0 9.7 2.8 13 7.5 2009-10 2.7 18 7.3 2.8 16 5.6 2010-11 2.8 26 10.6 3.7 26 9.8 Silver ** 1999-00 41 72 59 23 74 41 2000-01 8 76 49 36 42 39 2001-02 37 61 45 33 43 36 2002-03 40 53 44 29 39 32 2003-04 34 43 38 25 27 26 2004-05 38 52 43 17 25 23 2005-06 ND ND ND ND ND ND 2006-07 28 36 31 ND ND ND 2007-08 19 25 22 10 15 13 2008-09 19 24 20.8 9.5 13 11.6 2009-10 10 18 15 7.4 13 10 2010-11 10 17 13 5.2 12 9.57 Zinc 2,800 1999-00 640 798 736 752 900 827 2000-01 760 1,100 865 710 925 810 2001-02 630 817 730 750 893 830 2002-03 650 790 710 640 830 760 2003-04 660 820 750 630 760 690 2004-05 640 800 720 600 720 663 2005-06 700 910 801 680 900 760 2006-07 820 1100 900 720 930 790 2007-08 740 890 806 680 790 716 2008-09 720 870 785 700 800 749 2009-10 560 810 741 520 790 710 2010-11 630 740 696 700 830 740

** No 40 CFR Part 503 Exceptional Quality Criteria. ND = Non-detectable

9.5

Figure 9-1 Trends in Concentrations of Arsenic in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

Figure 9-2 Trends in Concentrations of Cadmium in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

0

10

20

30

40

50

60

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2 Series3

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 39 mg/kg (Feb. 1993), 41 mg/kg (1998)

Concentration less than method detection limit of 59 mg/kg limit in 1993

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 39 mg/kg (Feb. 1993), 41 mg/kg (1998)

Concentration less than method detection limit of 59 mg/kg limit in 1993

0

5

10

15

20

25

30

35

40

45

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 39 mg/kg (Feb. 1993)

9.6

Figure 9-3 Trends in Concentrations of Chromium in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

Figure 9-4 Trends in Concentrations of Copper in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

0

200

400

600

800

1000

1200

1400

1600

1800

2000

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 1500 mg/kg (Feb. 1993)

0

150

300

450

600

750

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

There are no biosolids limits for chromium

9.7

Figure 9-5 Trends of Concentrations of Lead in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

Figure 9-6 Trends in Concentrations of Mercury in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

0

5

10

15

20

25

30

35

40

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 17 mg/kg (Feb. 1993)

0

100

200

300

400

500

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 300 mg/kg (Feb. 1993)

9.8

Figure 9-7 Trends in Concentrations of Molybdenum in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

Figure 9-8 Trends in Concentrations of Nickel in Biosolids, Fiscal Years, 1990-2011 Orange County Sanitation District

0

10

20

30

40

50

60

70

80

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

No Exceptional Quality EPA Biosolids Pollutant Concentration Limit

Ceiling Concentration 75 mg/kg (Feb. 1993)

0

50

100

150

200

250

300

350

400

450

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2 Exceptional Quality EPA Biosolids Pollutant Concentration Limit and Ceiling Limit 420 mg/kg (Feb. 1993)

9.9

Figure 9-9 Trends in Concentrations of Selenium in Biosolids, Fiscal Years 1990-2011

Orange County Sanitation District

Figure 9-10 Trends in Concentrations of Zinc in Biosolids, Fiscal Years 1990-2011 Orange County Sanitation District

0

500

1000

1500

2000

2500

3000

3500

4000

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2

Exceptional Quality EPA Biosolids Pollutant Concentration Limit 2800 mg/kg (Feb. 1993)

0

10

20

30

40

50

60

70

80

90

100

110

1990 1992 1994 1996 1998 2000 2002 2004 2006 2008 2010

mg/kg

Plant No. 1 Plant No. 2Exceptional Quality EPA Biosolids Pollutant Concentration Limit & Ceiling Concentration 100 mg/kg

Concentration less than method detection limit of 63 mg/kg limit in 1993

APPENDIX C

Summary of Priority Pollutants and Trace Constituents Analysis 2011

Appendix C

Summary of Priority Pollutants and

Trace Constituents Analyses

From January 2011 to December 2011

1) An Annual Mean is reported for all compounds that are detected at a frequency of 50% or greaterduring the 12-month period or when the Annual Mean exceeds the highest detection limit for the 12-monthperiod. Monthly results are reported as the mean of all analytical determinations for the compoundperformed during the month. If the Annual Mean is reported as <x, then x equals the highest detectionlimit for that analysis during the 12-month period. For the mean calculation, ND=0.

2) Organochlorine Pesticides and PCB's in wastewater were analyzed by the Districts' Laboratory usingMethod 608. Organochlorine Pesticides and PCB's in biosolids were analyzed by contract lab(s) usingMethod 8081.

3) Organophosphorous Pesticides in biosolids were analyzed by contract lab(s) using Method 8141.

4) Herbicides in biosolids were analyzed by contract lab(s) using Method 8151.

5) Volatile Organics in wastewater were analyzed by the Districts' Laboratory using Method 624. Theinfluent and the final effluent are sampled at least once a quarter. Volatile Organics in biosolids wereanalyzed by contract lab(s) using Method 8260.

6) B/N/A extractables in wastewater were analyzed by the Districts' Laboratory using Method 625. B/N/Aextractables in biosolids were analyzed by contract lab(s) using Method 8270.

7) Dioxins and Furans in the final effluent were analyzed by contract lab(s) using Method 1613.

8) All biosolids results are reported in mg/kg dry weight.

9) Abbreviations:ND = Not DetectedDL = Detection LimitRes = Analysis ResultNA = Not Available at time of publicationNR = Not Reportable due to unacceptable quality controlSL = Sample Lost

ENDNOTES

1

Trace Elements Aluminum Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 6,600 48 -- -- -- -- 7,000 52 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 7,700 45 -- -- -- -- 6,600 51 -- -- -- --

Antimony Plant 1 Influent, µg/L (Dist. Lab) 1.14 0.23 1.09 0.23 1.22 0.23 1.20 0.23 1.43 0.23 1.69 0.23 Plant 2 Influent, µg/L (Dist. Lab) 0.99 0.23 1.25 0.23 1.07 0.23 1.07 0.23 1.12 0.23 1.17 0.23 Final Effluent, µg/L (Dist. Lab) 1.05 0.23 1.14 0.23 1.04 0.23 1.08 0.23 1.23 0.23 1.48 0.23 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 19 -- -- -- -- ND 21 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 18 -- -- -- -- ND 20 -- -- -- --

Arsenic Plant 1 Influent, µg/L (Dist. Lab) 2.43 0.47 2.48 0.47 2.38 0.47 2.53 0.47 2.73 0.47 2.38 0.47 Plant 2 Influent, µg/L (Dist. Lab) 4.80 0.47 4.65 0.47 4.79 0.47 5.34 0.47 5.94 0.47 5.53 0.47 Final Effluent, µg/L (Dist. Lab) 3.91 0.47 3.45 0.47 3.75 0.47 4.40 0.47 4.36 0.47 4.18 0.47 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 8.6 3.5 9.7 3.6 8.6 3.2 8.8 3.2 8.4 3.1 9.2 3.3 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 12 2.8 12 2.9 10.0 2.9 10 3.1 11 4.4 12 3.1

Barium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 440 9.6 -- -- -- -- 460 10 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 910 9.1 -- -- -- -- 1,100 10 -- -- -- --

Beryllium Plant 1 Influent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 Plant 2 Influent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 Final Effluent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 0.96 -- -- -- -- ND 1.0 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 0.91 -- -- -- -- ND 1.0 -- -- -- --

Cadmium Plant 1 Influent, µg/L (Dist. Lab) 0.26 0.07 0.41 0.07 0.52 0.07 0.34 0.07 0.44 0.07 0.28 0.07 Plant 2 Influent, µg/L (Dist. Lab) 0.01 0.07 0.28 0.07 0.08 0.07 0.02 0.07 ND 0.07 ND 0.07 Final Effluent, µg/L (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 3.2 2.3 3.6 2.4 3.5 2.2 3.4 2.1 1.4 2.1 2.9 2.2 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 3.0 1.9 3.2 1.9 2.4 1.9 2.5 2.0 1.4 3.0 3.0 2.1

Chromium Plant 1 Influent, µg/L (Dist. Lab) 5.85 0.21 6.20 0.21 6.16 0.21 6.55 0.21 7.07 0.21 14.9 0.21 Plant 2 Influent, µg/L (Dist. Lab) 8.37 0.21 6.32 0.21 9.56 0.21 6.75 0.21 6.99 0.21 9.98 0.21 Final Effluent, µg/L (Dist. Lab) 2.00 0.21 1.37 0.21 1.82 0.21 1.45 0.21 1.36 0.21 0.92 0.21 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 42 9.3 49 9.5 53 8.7 58 8.3 48 8.3 56 8.9 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 58 7.4 50 7.8 60 7.6 54 8.2 62 12 64 8.2

Cobalt Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 9.6 -- -- -- -- ND 10 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 9.1 -- -- -- -- ND 10 -- -- -- --

Copper Plant 1 Influent, µg/L (Dist. Lab) 105 0.26 112 0.26 101 0.26 103 0.26 110 0.26 104 0.26 Plant 2 Influent, µg/L (Dist. Lab) 74.7 0.26 97.0 0.26 88.7 0.26 95 0.26 83.8 0.26 104 0.26 Final Effluent, µg/L (Dist. Lab) 19.8 0.26 21.3 0.26 19.5 0.26 22.2 0.26 29.2 0.26 9.56 0.26 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 560 5.8 560 6.0 600 5.4 600 5.2 520 5.2 580 5.6 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 500 4.6 530 4.9 520 4.8 580 5.1 570 7.4 540 5.1

Iron Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 73,000 70 64,000 71 60,000 65 67,000 62 57,000 62 58,000 67 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 68,000 140 65,000 58 64,000 57 67,000 61 80,000 89 74,000 62

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

2

Annual

Mean

Trace Elements Aluminum Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 5,000 54 -- -- -- -- 5,200 54 -- -- -- -- 6,000

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 5,300 50 -- -- -- -- 4,900 50 -- -- -- -- 6,100

Antimony Plant 1 Influent, µg/L (Dist. Lab) 1.39 0.23 1.68 0.23 1.33 0.23 1.30 0.23 1.18 0.23 1.41 0.23 1.3

Plant 2 Influent, µg/L (Dist. Lab) 1.01 0.23 1.08 0.23 1.16 0.23 0.95 0.23 1.20 0.23 0.96 0.23 1.1

Final Effluent, µg/L (Dist. Lab) 1.15 0.23 1.37 0.23 1.06 0.23 1.13 0.23 1.35 0.23 1.18 0.23 1.2

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 22 -- -- -- -- ND 22 -- -- -- -- <22

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 20 -- -- -- -- ND 20 -- -- -- -- <20

Arsenic Plant 1 Influent, µg/L (Dist. Lab) 2.53 0.47 2.27 0.47 2.72 0.47 2.65 0.47 2.65 0.47 2.16 0.47 2.5

Plant 2 Influent, µg/L (Dist. Lab) 8.08 0.47 7.79 0.47 4.77 0.47 5.96 0.47 5.98 0.47 5.72 0.47 5.8

Final Effluent, µg/L (Dist. Lab) 5.23 0.47 5.17 0.47 3.36 0.47 3.71 0.47 4.22 0.47 3.52 0.47 4.1

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 6.2 3.3 7.6 2.8 9.8 3.3 10.0 3.2 11 3.2 7.6 5.7 8.8

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 8.2 3.3 12 2.7 10 3.0 8.6 3.0 12 3.1 6.6 3.0 10

Barium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 460 11 -- -- -- -- 450 11 -- -- -- -- 450

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 1,100 10 -- -- -- -- 930 10 -- -- -- -- 1,000

Beryllium Plant 1 Influent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 <0.06

Plant 2 Influent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 <0.06

Final Effluent, µg/L (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 <0.06

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 1.1 -- -- -- -- ND 1.1 -- -- -- -- <1.1

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 1.0 -- -- -- -- ND 1.0 -- -- -- -- <1.0

Cadmium Plant 1 Influent, µg/L (Dist. Lab) 0.74 0.07 0.55 0.07 0.59 0.07 0.39 0.07 0.35 0.07 0.25 0.07 0.43

Plant 2 Influent, µg/L (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 <0.07

Final Effluent, µg/L (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 <0.07

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 4.2 2.2 4.1 0.86 4.0 2.2 3.6 2.2 6.0 2.1 1.8 3.8 <3.8

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 3.7 2.2 3.4 0.84 3.6 2.0 3.3 2.0 4.4 2.1 2.6 2.0 3.0

Chromium Plant 1 Influent, µg/L (Dist. Lab) 6.35 0.21 5.72 0.21 6.48 0.21 9.7 0.21 6.76 0.21 6.72 0.21 7.4

Plant 2 Influent, µg/L (Dist. Lab) 7.6 0.21 13.2 0.21 5.79 0.21 8.2 0.21 7.39 0.21 6.10 0.21 8.0

Final Effluent, µg/L (Dist. Lab) 0.79 0.21 0.84 0.21 1.00 0.21 0.80 0.21 0.97 0.21 0.62 0.21 1.2

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 54 8.7 42 0.86 52 8.8 55 8.6 74 8.4 44 15 52

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 60 8.9 66 0.84 58 8.1 54 8.1 70 8.3 40 8.0 58

Cobalt Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 11 -- -- -- -- ND 11 -- -- -- -- <11

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- -- <10

Copper Plant 1 Influent, µg/L (Dist. Lab) 91.7 0.26 95.9 0.26 120 0.26 108 0.26 125 0.26 97.7 0.26 110

Plant 2 Influent, µg/L (Dist. Lab) 77.1 0.26 86.9 0.26 142 0.26 91 0.26 95.7 0.26 77.4 0.26 93

Final Effluent, µg/L (Dist. Lab) 10.4 0.26 14.2 0.26 12.9 0.26 9.2 0.26 8.84 0.26 9.66 0.26 16

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 580 5.4 480 1.3 560 5.5 520 5.4 670 5.3 440 9.4 560

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 540 5.5 520 1.3 590 5.1 520 5.1 720 5.2 380 5.0 540

Iron Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 58,000 65 62,000 5.4 69,000 66 72,000 65 77,000 150 76,000 110 66,000

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 69,000 66 80,000 5.3 70,000 120 70,000 61 86,000 150 54,000 60 71,000

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

3

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Trace Elements Lead Plant 1 Influent, µg/L (Dist. Lab) 2.54 0.43 2.38 0.43 2.60 0.43 2.97 0.43 3.71 0.43 3.01 0.43 Plant 2 Influent, µg/L (Dist. Lab) 1.94 0.43 2.10 0.43 2.02 0.43 2.32 0.43 2.88 0.43 3.68 0.43 Final Effluent, µg/L (Dist. Lab) ND 0.43 0.46 0.43 ND 0.43 0.23 0.43 0.49 0.43 ND 0.43 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 23 ND 24 ND 22 ND 21 ND 21 ND 22 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 19 ND 19 ND 19 ND 20 ND 30 ND 21

Manganese Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 290 3.8 -- -- -- -- 190 4.1 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 240 3.6 -- -- -- -- 220 4.1 -- -- -- --

Magnesium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 6,200 47 5,800 48 5,400 43 5,800 41 4,800 42 7,300 44 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 8,200 37 7,200 39 8,600 38 8,700 41 8,200 59 6,900 41

Mercury Plant 1 Influent, µg/L (Dist. Lab) 0.260 0.006 0.164 0.006 0.196 0.006 0.197 0.006 0.231 0.006 0.22 0.006 Plant 2 Influent, µg/L (Dist. Lab) 0.143 0.006 0.193 0.006 0.088 0.006 0.132 0.006 0.168 0.006 0.109 0.006 Final Effluent, µg/L (Dist. Lab) 0.016 0.006 0.017 0.006 ND 0.006 0.005 0.006 0.024 0.006 0.007 0.006 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 1.1 0.12 1.1 0.12 1.0 0.11 1.2 0.10 1.1 0.11 2.1 0.11 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 0.82 0.093 1.0 0.097 1.0 0.096 1.0 0.10 0.96 0.15 1.2 0.10

Molybdenum Plant 1 Influent, µg/L (Dist. Lab) 20.5 0.12 24.4 0.12 17.0 0.12 18.3 0.12 23.0 0.12 19.3 0.12 Plant 2 Influent, µg/L (Dist. Lab) 23.1 0.12 21.4 0.12 20.6 0.12 21.3 0.12 18.3 0.12 20.1 0.12 Final Effluent, µg/L (Dist. Lab) 27.5 0.12 24.3 0.12 20.6 0.12 23.8 0.12 24.9 0.12 24.2 0.12 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 14 12 15 12 14 11 15 10 14 10 14 11 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 14 9.3 14 9.7 15 9.5 14 10 16 15 18 10

Nickel Plant 1 Influent, µg/L (Dist. Lab) 12.9 0.81 15.2 0.81 14.0 0.81 14.0 0.81 15.1 0.81 12.1 0.81 Plant 2 Influent, µg/L (Dist. Lab) 16.7 0.81 13.1 0.81 18.9 0.81 12.7 0.81 13.4 0.81 14.5 0.81 Final Effluent, µg/L (Dist. Lab) 14.7 0.81 13.7 0.81 13.6 0.81 13.0 0.81 13.4 0.81 14.3 0.81 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 36 23 37 24 38 22 36 21 34 21 34 22 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 35 19 33 19 34 19 26 20 14 30 30 21

Selenium Plant 1 Influent, µgL (Dist. Lab) 4.05 0.32 3.80 0.32 3.41 0.32 3.68 0.32 3.89 0.32 3.14 0.32 Plant 2 Influent, µg/L (Dist. Lab) 10.6 0.32 8.46 0.32 9.43 0.32 11.8 0.32 13.6 0.32 12.7 0.32 Final Effluent, µg/L (Dist. Lab) 11.5 0.32 8.99 0.32 10.8 0.32 12.6 0.32 12.3 0.32 11.9 0.32 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 17 5.8 26 6.0 10.0 5.4 6.5 5.2 7.0 5.2 16 5.6 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 14 4.6 26 4.9 11 4.8 11 5.1 9.0 7.4 12 5.1

Silver Plant 1 Influent, µgL (Dist. Lab) 2.50 0.05 4.26 0.05 2.74 0.05 2.21 0.05 2.81 0.05 2.08 0.05 Plant 2 Influent, µg/L (Dist. Lab) 1.29 0.05 1.76 0.05 1.68 0.05 1.55 0.05 1.26 0.05 2.74 0.05 Final Effluent, µg/L (Dist. Lab) 0.20 0.05 0.25 0.05 0.22 0.05 0.23 0.05 0.22 0.05 0.05 0.05 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 13 3.5 12 3.6 14 3.2 12 3.1 13 3.1 10 3.3 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 8.2 2.8 10 2.9 9.0 2.9 8.4 3.1 12 4.4 9.6 3.1

Sodium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 1,400 480 -- -- -- -- 1,600 520 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 2,500 450 -- -- -- -- 3,000 510 -- -- -- --

4

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Trace Elements Lead Plant 1 Influent, µg/L (Dist. Lab) 3.9 0.43 3.52 0.43 3.43 0.43 4.24 0.43 3.02 0.43 3.34 0.43 3.2

Plant 2 Influent, µg/L (Dist. Lab) 1.97 0.43 2.35 0.43 3.97 0.43 2.50 0.43 2.50 0.43 2.37 0.43 2.6

Final Effluent, µg/L (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 22 ND 1.7 ND 22 ND 22 10 21 ND 38 <38

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 22 ND 1.7 10 20 26 20 12 21 ND 20 <30

Manganese Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 280 4.3 -- -- -- -- 290 4.3 -- -- -- -- 260

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 220 4.0 -- -- -- -- 210 4.0 -- -- -- -- 220

Magnesium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 8,000 43 7,200 4.3 6,300 44 7,300 43 7,400 42 5,800 76 6,400

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 8,000 44 8,400 4.2 8,600 41 8,200 41 10,000 42 5,600 40 8,000

Mercury Plant 1 Influent, µg/L (Dist. Lab) 0.172 0.006 0.281 0.006 0.345 0.006 0.18 0.006 0.12 0.006 0.172 0.006 0.21

Plant 2 Influent, µg/L (Dist. Lab) 0.10 0.006 0.281 0.006 0.119 0.006 0.114 0.006 0.193 0.006 0.131 0.006 0.15

Final Effluent, µg/L (Dist. Lab) 0.001 0.006 0.013 0.006 0.019 0.006 0.01 0.006 ND 0.006 0.009 0.006 0.010

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 1.3 0.11 1.3 0.064 0.95 0.11 1.00 0.11 1.4 0.11 1.3 0.12 1.2

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 1.0 0.11 1.3 0.062 0.84 0.10 2.6 0.10 1.6 0.10 1.4 0.11 1.2

Molybdenum Plant 1 Influent, µg/L (Dist. Lab) 16.1 0.12 17.8 0.12 19.9 0.12 20.3 0.12 23.3 0.12 19.1 0.12 20

Plant 2 Influent, µg/L (Dist. Lab) 16.6 0.12 18.8 0.12 16.6 0.12 20.5 0.12 16.2 0.12 14.6 0.12 19

Final Effluent, µg/L (Dist. Lab) 22.9 0.12 23.3 0.12 18.2 0.12 25.2 0.12 21.7 0.12 21.7 0.12 23

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 12 11 7.0 0.86 16 11 16 11 18 11 6.5 19 <19

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 16 11 18 0.84 19 10 17 10 20 10 12 10 16

Nickel Plant 1 Influent, µg/L (Dist. Lab) 13.6 0.81 12.9 0.81 13.9 0.81 12.9 0.81 13.3 0.81 11.7 0.81 13

Plant 2 Influent, µg/L (Dist. Lab) 11.0 0.81 12.3 0.81 10.0 0.81 13.6 0.81 12.1 0.81 12.2 0.81 13

Final Effluent, µg/L (Dist. Lab) 12.6 0.81 12.4 0.81 9.83 0.81 12.2 0.81 11.3 0.81 11.3 0.81 13

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 40 22 32 0.86 34 22 36 22 48 21 15 38 <38

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 39 22 28 0.84 32 20 32 20 38 21 20 20 30

Selenium Plant 1 Influent, µgL (Dist. Lab) 3.72 0.32 3.44 0.32 3.03 0.32 3.39 0.32 3.73 0.32 3.95 0.32 3.6

Plant 2 Influent, µg/L (Dist. Lab) 20.2 0.32 18.4 0.32 11.1 0.32 14.4 0.32 14.1 0.32 13.2 0.32 13

Final Effluent, µg/L (Dist. Lab) 14.2 0.32 14.5 0.32 9.40 0.32 10.0 0.32 11.5 0.32 11.0 0.32 12

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 8.5 5.4 5.5 3.4 11 5.5 6.5 5.4 6.5 5.3 26 9.4 12

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 12 5.5 8.0 3.4 16 5.1 10 5.1 7.5 5.2 19 5.0 13

Silver Plant 1 Influent, µgL (Dist. Lab) 1.51 0.05 2.33 0.05 2.34 0.05 2.45 0.05 2.84 0.05 3.63 0.05 2.6

Plant 2 Influent, µg/L (Dist. Lab) 1.16 0.05 2.49 0.05 1.24 0.05 1.91 0.05 1.42 0.05 2.46 0.05 1.7

Final Effluent, µg/L (Dist. Lab) 0.07 0.05 0.15 0.05 ND 0.05 0.03 0.05 ND 0.05 0.06 0.05 0.12

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 9.0 3.3 7.0 2.7 11 3.3 9.6 3.2 14 3.2 12 5.7 11

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 9.6 3.3 8.2 2.6 9.2 3.0 8.6 3.0 12 3.1 8.6 3.0 9.4

Sodium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 1,300 540 -- -- -- -- 1,400 540 -- -- -- -- 1,400

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 3,100 500 -- -- -- -- 2,800 500 -- -- -- -- 2,800

5

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Thallium Plant 1 Influent, µg/L (Dist. Lab) 0.01 0.01 0.02 0.01 0.06 0.01 ND 0.01 0.05 0.01 ND 0.01 Plant 2 Influent, µg/L (Dist. Lab) 0.01 0.01 0.02 0.01 0.03 0.01 ND 0.01 0.02 0.01 ND 0.01 Final Effluent, µg/L (Dist. Lab) 0.04 0.01 0.10 0.01 0.18 0.01 0.02 0.01 0.25 0.01 0.10 0.01 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 29 -- -- -- -- ND 31 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 27 -- -- -- -- ND 31 -- -- -- --

Total Sulfur Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Vanadium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 30 9.6 -- -- -- -- 23 10 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 41 9.1 -- -- -- -- 41 10 -- -- -- --

Zinc Plant 1 Influent, µg/L (Dist. Lab) 158 0.76 168 0.76 143 0.76 179 0.76 166 0.76 155 0.76 Plant 2 Influent, µg/L (Dist. Lab) 115 0.76 129 0.76 121 0.76 135 0.76 128 0.76 156 0.76 Final Effluent, µg/L (Dist. Lab) 47.1 0.76 42.2 0.76 34.9 0.76 43.3 0.76 37.6 0.76 33.2 0.76 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 680 9.3 720 9.5 740 8.7 730 8.3 690 8.3 740 8.9 Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 720 7.4 700 7.8 700 7.6 720 8.2 790 12 750 8.2

Organochlorine Pesticides and PCB's, µg/L (Plant 1 Influent)Aldrin (Dist. Lab) ND 0.0015 ND 0.0013 ND 0.050 ND 0.0050 ND 0.0075 ND 0.03Alpha-BHC (Dist. Lab) ND 0.0025 ND 0.0022 ND 0.050 ND 0.0050 ND 0.012 ND 0.05Beta-BHC (Dist. Lab) ND 0.004 ND 0.0034 ND 0.10 ND 0.010 ND 0.02 ND 0.08Delta-BHC (Dist. Lab) ND 0.0035 ND 0.003 ND 0.050 ND 0.0050 ND 0.018 ND 0.07Gamma-BHC (Dist. Lab) ND 0.003 ND 0.0026 ND 0.10 ND 0.010 ND 0.015 ND 0.06Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --4,4'-DDD (Dist. Lab) ND 0.004 ND 0.0034 ND 0.050 ND 0.0050 ND 0.02 ND 0.084-4'-DDE (Dist. Lab) ND 0.003 ND 0.0026 ND 0.050 ND 0.0050 ND 0.015 ND 0.064-4'-DDT (Dist. Lab) ND 0.004 ND 0.0034 ND 0.10 ND 0.010 ND 0.02 ND 0.082,4'-DDD (Dist. Lab) ND 0.02 ND 0.017 ND 1.0 ND 0.10 ND 0.1 ND 0.42,4'-DDE (Dist. Lab) ND 0.02 ND 0.017 ND 1.0 ND 0.10 ND 0.1 ND 0.42,4'-DDT (Dist. Lab) ND 0.02 ND 0.017 ND 1.0 ND 0.10 ND 0.1 ND 0.4Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Dieldrin (Dist. Lab) ND 0.002 ND 0.0017 ND 0.050 ND 0.0050 ND 0.01 ND 0.04Endosulfan I (Dist. Lab) ND 0.002 ND 0.0017 ND 0.050 ND 0.0050 ND 0.01 ND 0.04Endosulfan II (Dist. Lab) ND 0.003 ND 0.0026 ND 0.050 ND 0.0050 ND 0.015 ND 0.06Endosulfan sulfate (Dist. Lab) ND 0.003 ND 0.0026 ND 0.10 ND 0.010 ND 0.015 ND 0.06Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Endrin (Dist. Lab) ND 0.002 ND 0.0017 ND 0.050 ND 0.0050 ND 0.01 ND 0.04Endrin Aldehyde (Dist. Lab) ND 0.002 ND 0.0017 ND 0.10 ND 0.010 ND 0.01 ND 0.04Heptachlor (Dist. Lab) ND 0.003 ND 0.0026 ND 0.10 ND 0.010 ND 0.015 ND 0.06Heptachlor epoxide (Dist. Lab) ND 0.0025 ND 0.0022 ND 0.050 ND 0.0050 ND 0.012 ND 0.05Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Mirex (Dist. Lab) ND 0.002 ND 0.0017 ND 0.10 ND 0.010 ND 0.01 ND 0.04Methoxychlor (Dist. Lab) ND 0.0035 ND 0.003 ND 0.050 ND 0.0050 ND 0.018 ND 0.07Chlordene-alpha (Dist. Lab) ND 1.0 ND 0.86 ND 10 ND 1.0 ND 5.0 ND 20Chlordene-gamma (Dist. Lab) ND 1.0 ND 0.86 ND 10 ND 1.0 ND 5.0 ND 20Oxychlordane (Dist. Lab) ND 1.0 ND 0.86 ND 10 ND 1.0 ND 5.0 ND 20Chlordane-alpha (Dist. Lab) ND 0.03 ND 0.026 ND 2.0 ND 0.20 ND 0.15 ND 0.6Chlordane-gamma (Dist. Lab) ND 0.03 ND 0.026 ND 2.0 ND 0.20 ND 0.15 ND 0.6trans-Nonachlor (Dist. Lab) ND 1.0 ND 0.86 ND 10 ND 1.0 ND 5.0 ND 20cis-Nonachlor (Dist. Lab) ND 1.0 ND 0.86 ND 10 ND 1.0 ND 5.0 ND 20Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --

6

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Thallium Plant 1 Influent, µg/L (Dist. Lab) 0.03 0.01 0.04 0.01 ND 0.01 0.01 0.01 ND 0.01 0.03 0.01 0.021

Plant 2 Influent, µg/L (Dist. Lab) 0.01 0.01 0.02 0.01 ND 0.01 0.02 0.01 ND 0.01 0.02 0.01 0.012

Final Effluent, µg/L (Dist. Lab) 0.01 0.01 0.11 0.01 0.04 0.01 0.03 0.01 0.04 0.01 0.09 0.01 0.084

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 32 -- -- -- -- ND 32 -- -- -- -- <32

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 30 -- -- -- -- ND 30 -- -- -- -- <31

Total Sulfur Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Vanadium Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 19 11 -- -- -- -- 24 11 -- -- -- -- 24

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 37 10 -- -- -- -- 46 10 -- -- -- -- 41

Zinc Plant 1 Influent, µg/L (Dist. Lab) 158 0.76 151 0.76 211 0.76 166 0.76 174 0.76 154 0.76 170

Plant 2 Influent, µg/L (Dist. Lab) 116 0.76 129 0.76 121 0.76 139 0.76 137 0.76 138 0.76 130

Final Effluent, µg/L (Dist. Lab) 28.5 0.76 24.0 0.76 22.7 0.76 24.7 0.76 21.9 0.76 21.6 0.76 32

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) 780 8.7 650 2.6 840 8.8 740 8.6 880 8.4 580 15 730

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) 790 8.9 780 2.5 870 8.1 740 8.1 910 8.3 560 8.0 750

Organochlorine Pesticides and PCB's, µg/L (Plant 1 Influent)Aldrin (Dist. Lab) ND 0.0075 ND 0.015 ND 0.0074 ND 0.015 ND 0.0075 ND 0.0075 <0.050

Alpha-BHC (Dist. Lab) ND 0.012 ND 0.024 ND 0.012 ND 0.025 ND 0.012 ND 0.012 <0.050

Beta-BHC (Dist. Lab) ND 0.02 ND 0.039 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.10

Delta-BHC (Dist. Lab) ND 0.018 ND 0.034 ND 0.017 ND 0.035 ND 0.018 ND 0.018 <0.07

Gamma-BHC (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.10

Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

4,4'-DDD (Dist. Lab) ND 0.02 ND 0.039 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.08

4-4'-DDE (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.06

4-4'-DDT (Dist. Lab) ND 0.02 ND 0.039 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.10

2,4'-DDD (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.1 <1.0

2,4'-DDE (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.1 <1.0

2,4'-DDT (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.1 <1.0

Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Dieldrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.01 <0.050

Endosulfan I (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.01 <0.050

Endosulfan II (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.06

Endosulfan sulfate (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.10

Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Endrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.01 <0.050

Endrin Aldehyde (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.01 <0.10

Heptachlor (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.10

Heptachlor epoxide (Dist. Lab) ND 0.012 ND 0.024 ND 0.012 ND 0.025 ND 0.012 ND 0.012 <0.050

Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Mirex (Dist. Lab) ND 0.01 ND 0.019 0.14 0.0099 ND 0.02 ND 0.01 0.032 0.01 <0.10

Methoxychlor (Dist. Lab) ND 0.018 ND 0.034 ND 0.017 ND 0.035 ND 0.018 ND 0.018 <0.07

Chlordene-alpha (Dist. Lab) ND 5.0 ND 9.7 ND 5 ND 10 ND 5 ND 5 <20

Chlordene-gamma (Dist. Lab) ND 5.0 ND 9.7 ND 5 ND 10 ND 5 ND 5 <20

Oxychlordane (Dist. Lab) ND 5.0 ND 9.7 ND 5 ND 10 ND 5 ND 5 <20

Chlordane-alpha (Dist. Lab) ND 0.15 ND 0.29 ND 0.15 ND 0.3 ND 0.15 ND 0.15 <2.0

Chlordane-gamma (Dist. Lab) ND 0.15 ND 0.29 ND 0.15 ND 0.3 ND 0.15 ND 0.15 <2.0

trans-Nonachlor (Dist. Lab) ND 5.0 ND 9.7 ND 5 ND 10 ND 5 ND 5 <20

cis-Nonachlor (Dist. Lab) ND 5.0 ND 9.7 ND 5 ND 10 ND 5 ND 5 <20

Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

7

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Toxaphene (Dist. Lab) ND 0.25 ND 0.22 ND 5.0 ND 0.50 ND 1.2 ND 5PCB-1016 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1221 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1232 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1242 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1248 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1254 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1260 (Dist. Lab) ND 0.25 ND 0.22 ND 0.50 ND 0.50 ND 0.25 ND 0.25Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --

Organochlorine Pesticides and PCB's, µg/L (Plant 2 Influent)Aldrin (Dist. Lab) ND 0.0015 ND 0.0012 ND 0.051 ND 0.0050 ND 0.015 ND 0.03Alpha-BHC (Dist. Lab) ND 0.0025 ND 0.002 ND 0.051 ND 0.0050 ND 0.025 ND 0.05Beta-BHC (Dist. Lab) ND 0.004 ND 0.0032 ND 0.10 ND 0.010 ND 0.04 ND 0.08Delta-BHC (Dist. Lab) ND 0.0035 ND 0.0028 ND 0.051 ND 0.0050 ND 0.035 ND 0.07Gamma-BHC (Dist. Lab) ND 0.003 ND 0.0024 ND 0.10 ND 0.010 ND 0.03 ND 0.06Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --4,4'-DDD (Dist. Lab) ND 0.004 ND 0.0032 ND 0.051 ND 0.0050 ND 0.04 ND 0.104-4'-DDE (Dist. Lab) ND 0.003 ND 0.0024 ND 0.051 ND 0.0050 ND 0.03 ND 0.064-4'-DDT (Dist. Lab) ND 0.004 ND 0.0032 ND 0.10 ND 0.010 ND 0.04 ND 0.082,4'-DDD (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.1 ND 0.42,4'-DDE (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.1 ND 0.42,4'-DDT (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.2 ND 0.4Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- 0.11 --Dieldrin (Dist. Lab) ND 0.002 ND 0.0016 ND 0.051 ND 0.0050 ND 0.02 ND 0.04Endosulfan I (Dist. Lab) ND 0.002 ND 0.0016 ND 0.051 ND 0.0050 ND 0.02 ND 0.04Endosulfan II (Dist. Lab) ND 0.003 ND 0.0024 ND 0.051 ND 0.0050 ND 0.03 ND 0.06Endosulfan sulfate (Dist. Lab) ND 0.003 ND 0.0024 ND 0.10 ND 0.010 ND 0.03 ND 0.06Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Endrin (Dist. Lab) ND 0.002 ND 0.0016 ND 0.051 ND 0.0050 ND 0.02 ND 0.04Endrin Aldehyde (Dist. Lab) ND 0.002 ND 0.0016 ND 0.10 ND 0.010 ND 0.02 ND 0.04Heptachlor (Dist. Lab) ND 0.003 ND 0.0024 ND 0.10 ND 0.010 ND 0.03 ND 0.06Heptachlor epoxide (Dist. Lab) ND 0.0025 ND 0.002 ND 0.051 ND 0.0050 ND 0.025 ND 0.05Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Mirex (Dist. Lab) ND 0.002 ND 0.0016 ND 0.10 ND 0.010 ND 0.02 ND 0.04Methoxychlor (Dist. Lab) ND 0.0035 ND 0.0028 ND 0.051 ND 0.0050 ND 0.035 ND 0.07Chlordene-alpha (Dist. Lab) ND 1.0 ND 0.80 ND 10 ND 1.0 ND 10 ND 20Chlordene-gamma (Dist. Lab) ND 1.0 ND 0.80 ND 10 ND 1.0 ND 10 ND 20Oxychlordane (Dist. Lab) ND 1.0 ND 0.80 ND 10 ND 1.0 ND 10 ND 20Chlordane-alpha (Dist. Lab) ND 0.03 ND 0.024 ND 2.0 ND 0.20 ND 0.3 ND 0.6Chlordane-gamma (Dist. Lab) ND 0.03 ND 0.024 ND 2.0 ND 0.20 ND 0.3 ND 0.6trans-Nonachlor (Dist. Lab) ND 1.0 ND 0.80 ND 10 ND 1.0 ND 10 ND 20cis-Nonachlor (Dist. Lab) ND 1.0 ND 0.80 ND 10 ND 1.0 ND 10 ND 20Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Toxaphene (Dist. Lab) ND 0.25 ND 0.2 ND 5.1 ND 0.50 ND 2.5 ND 5PCB-1016 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1221 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1232 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1242 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1248 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1254 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25PCB-1260 (Dist. Lab) ND 0.25 ND 0.2 ND 0.51 ND 0.50 ND 0.25 ND 0.25Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --

Organochlorine Pesticides and PCB's, µg/L (Plant 2 Influent D Headworks)Aldrin (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Alpha-BHC (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Beta-BHC (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

8

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Toxaphene (Dist. Lab) ND 1.2 ND 2.4 ND 1.2 ND 2.5 ND 1.2 ND 1.2 <5.0

PCB-1016 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1221 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1232 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1242 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1248 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1254 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1260 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Organochlorine Pesticides and PCB's, µg/L (Plant 2 Influent)Aldrin (Dist. Lab) ND 0.0075 ND 0.014 ND 0.015 ND 0.015 ND 0.0075 ND 0.0075 <0.051

Alpha-BHC (Dist. Lab) ND 0.012 ND 0.024 ND 0.025 ND 0.025 ND 0.012 ND 0.012 <0.051

Beta-BHC (Dist. Lab) ND 0.02 ND 0.038 ND 0.04 ND 0.04 ND 0.02 ND 0.02 <0.10

Delta-BHC (Dist. Lab) ND 0.018 ND 0.034 ND 0.035 ND 0.035 ND 0.018 ND 0.018 <0.07

Gamma-BHC (Dist. Lab) ND 0.015 ND 0.029 ND 0.03 ND 0.03 ND 0.015 ND 0.015 <0.10

Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

4,4'-DDD (Dist. Lab) ND 0.02 ND 0.038 ND 0.04 ND 0.04 ND 0.02 ND 0.02 <0.10

4-4'-DDE (Dist. Lab) ND 0.015 ND 0.029 ND 0.03 ND 0.03 ND 0.015 ND 0.015 <0.06

4-4'-DDT (Dist. Lab) ND 0.02 ND 0.038 ND 0.04 ND 0.04 ND 0.02 ND 0.02 <0.10

2,4'-DDD (Dist. Lab) ND 0.1 ND 0.19 ND 0.2 ND 0.2 ND 0.1 ND 0.1 <1.0

2,4'-DDE (Dist. Lab) ND 0.1 ND 0.19 ND 0.2 ND 0.2 ND 0.1 ND 0.1 <1.0

2,4'-DDT (Dist. Lab) ND 0.1 ND 0.19 ND 0.2 ND 0.2 ND 0.1 ND 0.1 <1.0

Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- 0.0092

Dieldrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.02 ND 0.02 ND 0.01 ND 0.01 <0.051

Endosulfan I (Dist. Lab) ND 0.01 ND 0.019 ND 0.02 ND 0.02 ND 0.01 ND 0.01 <0.051

Endosulfan II (Dist. Lab) ND 0.015 ND 0.029 ND 0.03 ND 0.03 ND 0.015 ND 0.015 <0.06

Endosulfan sulfate (Dist. Lab) ND 0.015 ND 0.029 ND 0.03 ND 0.03 ND 0.015 ND 0.015 <0.10

Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Endrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.02 ND 0.02 ND 0.01 ND 0.01 <0.051

Endrin Aldehyde (Dist. Lab) ND 0.01 ND 0.019 ND 0.02 ND 0.02 ND 0.01 ND 0.01 <0.10

Heptachlor (Dist. Lab) ND 0.015 ND 0.029 ND 0.03 ND 0.03 ND 0.015 ND 0.015 <0.10

Heptachlor epoxide (Dist. Lab) ND 0.012 ND 0.024 ND 0.025 ND 0.025 ND 0.012 ND 0.012 <0.051

Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Mirex (Dist. Lab) ND 0.01 ND 0.019 0.12 0.02 ND 0.02 ND 0.01 0.028 0.01 <0.10

Methoxychlor (Dist. Lab) ND 0.018 ND 0.034 ND 0.035 ND 0.035 ND 0.018 ND 0.018 <0.07

Chlordene-alpha (Dist. Lab) ND 5.0 ND 9.6 ND 10 ND 10 ND 5 ND 5 <20

Chlordene-gamma (Dist. Lab) ND 5.0 ND 9.6 ND 10 ND 10 ND 5 ND 5 <20

Oxychlordane (Dist. Lab) ND 5.0 ND 9.6 ND 10 ND 10 ND 5 ND 5 <20

Chlordane-alpha (Dist. Lab) ND 0.15 ND 0.29 ND 0.3 ND 0.3 ND 0.15 ND 0.15 <2.0

Chlordane-gamma (Dist. Lab) ND 0.15 ND 0.29 ND 0.3 ND 0.3 ND 0.15 ND 0.15 <2.0

trans-Nonachlor (Dist. Lab) ND 5.0 ND 9.6 ND 10 ND 10 ND 5 ND 5 <20

cis-Nonachlor (Dist. Lab) ND 5.0 ND 9.6 ND 10 ND 10 ND 5 ND 5 <20

Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Toxaphene (Dist. Lab) ND 1.2 ND 2.4 ND 2.5 ND 2.5 ND 1.2 ND 1.2 <5.1

PCB-1016 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1221 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1232 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1242 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1248 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1254 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

PCB-1260 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.51

Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Organochlorine Pesticides and PCB's, µg/L (Plant 2 Influent D Headworks)Aldrin (Dist. Lab) ND 0.0075 ND 0.014 ND 0.0074 ND 0.015 ND 0.0075 ND 0.0074 <0.015

Alpha-BHC (Dist. Lab) ND 0.012 ND 0.024 ND 0.012 ND 0.025 ND 0.012 ND 0.012 <0.025

Beta-BHC (Dist. Lab) ND 0.02 ND 0.038 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.04

9

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Delta-BHC (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Gamma-BHC (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total HCH (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4,4'-DDD (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-4'-DDE (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-4'-DDT (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4'-DDD (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4'-DDE (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4'-DDT (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total DDT (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dieldrin (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Endosulfan I (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Endosulfan II (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Endosulfan sulfate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total Endosulfan (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Endrin (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Endrin Aldehyde (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Heptachlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Heptachlor epoxide (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Mirex (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Methoxychlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chlordene-alpha (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chlordene-gamma (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Oxychlordane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chlordane-alpha (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chlordane-gamma (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --trans-Nonachlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --cis-Nonachlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total Chlordane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Toxaphene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1016 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1221 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1232 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1242 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1248 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1254 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PCB-1260 (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total PCB (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Organochlorine Pesticides and PCB's, µg/L (Final Effluent)Aldrin (Dist. Lab) ND 0.0015 ND 0.0012 ND 0.050 ND 0.0050 ND 0.0075 ND 0.0015Alpha-BHC (Dist. Lab) ND 0.0025 ND 0.0021 ND 0.050 ND 0.0050 ND 0.012 ND 0.0025Beta-BHC (Dist. Lab) ND 0.004 ND 0.0033 ND 0.10 ND 0.010 ND 0.02 ND 0.004Delta-BHC (Dist. Lab) ND 0.0035 ND 0.0029 ND 0.050 ND 0.0050 ND 0.018 ND 0.0035Gamma-BHC (Dist. Lab) ND 0.003 ND 0.0025 ND 0.10 ND 0.010 ND 0.015 ND 0.003Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --4,4'-DDD (Dist. Lab) ND 0.004 ND 0.0033 ND 0.050 ND 0.0050 ND 0.02 ND 0.0044-4'-DDE (Dist. Lab) ND 0.003 ND 0.0025 ND 0.050 ND 0.0050 ND 0.015 ND 0.0034-4'-DDT (Dist. Lab) ND 0.004 ND 0.0033 ND 0.10 ND 0.010 ND 0.02 ND 0.0042,4'-DDD (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.1 ND 0.022,4'-DDE (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.1 ND 0.022,4'-DDT (Dist. Lab) ND 0.02 ND 0.016 ND 1.0 ND 0.10 ND 0.1 ND 0.02Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Dieldrin (Dist. Lab) ND 0.002 ND 0.0016 ND 0.050 ND 0.0050 ND 0.01 ND 0.002Endosulfan I (Dist. Lab) ND 0.002 ND 0.0016 ND 0.050 ND 0.0050 ND 0.01 ND 0.002Endosulfan II (Dist. Lab) ND 0.003 ND 0.0025 ND 0.050 ND 0.0050 ND 0.015 ND 0.003Endosulfan sulfate (Dist. Lab) ND 0.003 ND 0.0025 ND 0.10 ND 0.010 ND 0.015 ND 0.003

10

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Delta-BHC (Dist. Lab) ND 0.018 0.12 0.034 ND 0.017 ND 0.035 ND 0.018 ND 0.017 <0.035

Gamma-BHC (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.03

Total HCH (Dist. Lab) ND -- 0.12 -- ND -- ND -- ND -- ND -- 0.020

4,4'-DDD (Dist. Lab) ND 0.02 ND 0.038 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.04

4-4'-DDE (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.03

4-4'-DDT (Dist. Lab) ND 0.02 ND 0.038 ND 0.02 ND 0.04 ND 0.02 ND 0.02 <0.04

2,4'-DDD (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.098 <0.2

2,4'-DDE (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.098 <0.2

2,4'-DDT (Dist. Lab) ND 0.1 ND 0.19 ND 0.099 ND 0.2 ND 0.1 ND 0.098 <0.2

Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Dieldrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.0098 <0.02

Endosulfan I (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.0098 <0.02

Endosulfan II (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.03

Endosulfan sulfate (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.03

Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Endrin (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.0098 <0.02

Endrin Aldehyde (Dist. Lab) ND 0.01 ND 0.019 ND 0.0099 ND 0.02 ND 0.01 ND 0.0098 <0.02

Heptachlor (Dist. Lab) ND 0.015 ND 0.029 ND 0.015 ND 0.03 ND 0.015 ND 0.015 <0.03

Heptachlor epoxide (Dist. Lab) ND 0.012 ND 0.024 ND 0.012 ND 0.025 ND 0.012 ND 0.012 <0.025

Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Mirex (Dist. Lab) ND 0.01 ND 0.019 0.13 0.0099 ND 0.02 ND 0.01 0.031 0.0098 0.027

Methoxychlor (Dist. Lab) ND 0.018 ND 0.034 ND 0.017 ND 0.035 ND 0.018 ND 0.017 <0.035

Chlordene-alpha (Dist. Lab) ND 5.0 ND 9.6 ND 5 ND 10 ND 5 ND 4.9 <10

Chlordene-gamma (Dist. Lab) ND 5.0 ND 9.6 ND 5 ND 10 ND 5 ND 4.9 <10

Oxychlordane (Dist. Lab) ND 5.0 ND 9.6 ND 5 ND 10 ND 5 ND 4.9 <10

Chlordane-alpha (Dist. Lab) ND 0.15 ND 0.29 ND 0.15 ND 0.3 ND 0.15 ND 0.15 <0.3

Chlordane-gamma (Dist. Lab) ND 0.15 ND 0.29 ND 0.15 ND 0.3 ND 0.15 ND 0.15 <0.3

trans-Nonachlor (Dist. Lab) ND 5.0 ND 9.6 ND 5 ND 10 ND 5 ND 4.9 <10

cis-Nonachlor (Dist. Lab) ND 5.0 ND 9.6 ND 5 ND 10 ND 5 ND 4.9 <10

Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Toxaphene (Dist. Lab) ND 1.2 ND 2.4 ND 1.2 ND 2.5 ND 1.2 ND 1.2 <2.5

PCB-1016 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1221 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1232 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1242 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1248 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1254 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

PCB-1260 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.25

Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Organochlorine Pesticides and PCB's, µg/L (Final Effluent)Aldrin (Dist. Lab) ND 0.0015 ND 0.0014 ND 0.0015 ND 0.0015 ND 0.0015 ND 0.0015 <0.050

Alpha-BHC (Dist. Lab) ND 0.0025 ND 0.0024 ND 0.0025 ND 0.0025 ND 0.0025 ND 0.0025 <0.050

Beta-BHC (Dist. Lab) ND 0.004 ND 0.0038 ND 0.004 ND 0.004 ND 0.004 ND 0.004 <0.10

Delta-BHC (Dist. Lab) ND 0.0035 ND 0.0034 ND 0.0035 ND 0.0035 ND 0.0036 ND 0.0035 <0.050

Gamma-BHC (Dist. Lab) ND 0.003 ND 0.0029 ND 0.003 ND 0.003 ND 0.003 ND 0.003 <0.10

Total HCH (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

4,4'-DDD (Dist. Lab) ND 0.004 ND 0.0038 ND 0.004 ND 0.0044 ND 0.004 ND 0.004 <0.050

4-4'-DDE (Dist. Lab) ND 0.003 ND 0.0029 ND 0.003 ND 0.003 ND 0.003 ND 0.003 <0.050

4-4'-DDT (Dist. Lab) ND 0.004 ND 0.0038 ND 0.004 ND 0.004 ND 0.004 ND 0.004 <0.10

2,4'-DDD (Dist. Lab) ND 0.02 ND 0.019 ND 0.02 ND 0.02 ND 0.02 ND 0.02 <1.0

2,4'-DDE (Dist. Lab) ND 0.02 ND 0.019 ND 0.02 ND 0.02 ND 0.02 ND 0.02 <1.0

2,4'-DDT (Dist. Lab) ND 0.02 ND 0.019 ND 0.02 ND 0.02 ND 0.02 ND 0.02 <1.0

Total DDT (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Dieldrin (Dist. Lab) ND 0.002 ND 0.0019 ND 0.002 ND 0.002 ND 0.002 ND 0.002 <0.050

Endosulfan I (Dist. Lab) ND 0.002 ND 0.0019 ND 0.002 ND 0.002 ND 0.002 ND 0.002 <0.050

Endosulfan II (Dist. Lab) ND 0.003 ND 0.0029 ND 0.003 ND 0.003 ND 0.003 ND 0.003 <0.050

Endosulfan sulfate (Dist. Lab) ND 0.003 ND 0.0029 ND 0.003 ND 0.003 ND 0.003 ND 0.003 <0.10

11

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Endrin (Dist. Lab) ND 0.002 ND 0.0016 ND 0.050 ND 0.0050 ND 0.01 ND 0.002Endrin Aldehyde (Dist. Lab) ND 0.002 ND 0.0016 ND 0.10 ND 0.010 ND 0.01 ND 0.002Heptachlor (Dist. Lab) ND 0.003 ND 0.0025 ND 0.10 ND 0.010 ND 0.015 ND 0.003Heptachlor epoxide (Dist. Lab) ND 0.0025 ND 0.0021 ND 0.050 ND 0.0050 ND 0.012 ND 0.0025Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Mirex (Dist. Lab) ND 0.002 ND 0.0016 ND 0.10 ND 0.010 ND 0.01 ND 0.002Methoxychlor (Dist. Lab) ND 0.0035 ND 0.0029 ND 0.050 ND 0.0050 ND 0.018 ND 0.0035Chlordene-alpha (Dist. Lab) ND 1.0 ND 0.82 ND 10 ND 1.0 ND 5.0 ND 1.0Chlordene-gamma (Dist. Lab) ND 1.0 ND 0.82 ND 10 ND 1.0 ND 5.0 ND 0.03Oxychlordane (Dist. Lab) ND 1.0 ND 0.82 ND 10 ND 1.0 ND 5.0 ND 1.0Chlordane-alpha (Dist. Lab) ND 0.03 ND 0.025 ND 2.0 ND 0.20 ND 0.15 ND 0.03Chlordane-gamma (Dist. Lab) ND 0.03 ND 0.025 ND 2.0 ND 0.20 ND 0.15 ND 0.20trans-Nonachlor (Dist. Lab) ND 1.0 ND 0.82 ND 10 ND 1.0 ND 5.0 ND 1.0cis-Nonachlor (Dist. Lab) ND 1.0 ND 0.82 ND 10 ND 1.0 ND 5.0 ND 1.0Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Toxaphene (Dist. Lab) ND 0.25 ND 0.21 ND 5.0 ND 0.50 ND 1.2 ND 0.25PCB-1016 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1221 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1232 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1242 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1248 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1254 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25PCB-1260 (Dist. Lab) ND 0.25 ND 0.21 ND 0.50 ND 0.50 ND 0.25 ND 0.25Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --

Organochlorine Pesticides and PCB's, µg/Kg (Plant 1 BP Cake)Aldrin (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Alpha-BHC (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Beta-BHC (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Delta-BHC (Con. Lab) ND 480 -- -- -- -- ND 1000 -- -- -- --Gamma-BHC (Lindane) (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Chlordane (Con. Lab) ND 2400 -- -- -- -- ND 5200 -- -- -- --4,4'-DDD (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --4-4'-DDE (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --4-4'-DDT (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --2,4'-DDD (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --2-4'-DDE (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --2-4'-DDT (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Dieldrin (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Endosulfan I (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Endosulfan II (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Endosulfan sulfate (Con. Lab) ND 480 -- -- -- -- ND 1000 -- -- -- --Endrin (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Endrin Aldehyde (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Endrin Ketone (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Heptachlor (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Heptachlor epoxide (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Methoxychlor (Con. Lab) ND 240 -- -- -- -- ND 520 -- -- -- --Mirex (Con. Lab) ND 480 -- -- -- -- ND 1000 -- -- -- --Toxaphene (Con. Lab) ND 9600 -- -- -- -- ND 21000 -- -- -- --PCB-1016 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1221 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1232 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1242 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1248 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1254 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --PCB-1260 (Con. Lab) ND 240 -- -- -- -- ND 5200 -- -- -- --

12

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Total Endosulfan (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Endrin (Dist. Lab) ND 0.002 ND 0.0019 ND 0.002 ND 0.002 ND 0.002 ND 0.002 <0.050

Endrin Aldehyde (Dist. Lab) ND 0.002 ND 0.0019 ND 0.002 ND 0.002 ND 0.002 ND 0.002 <0.10

Heptachlor (Dist. Lab) ND 0.003 ND 0.0029 ND 0.003 ND 0.003 ND 0.003 ND 0.003 <0.10

Heptachlor epoxide (Dist. Lab) ND 0.0025 ND 0.0024 ND 0.0025 ND 0.0025 ND 0.0025 ND 0.0025 <0.050

Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Mirex (Dist. Lab) ND 0.002 ND 0.0019 ND 0.002 ND 0.002 ND 0.002 ND 0.002 <0.10

Methoxychlor (Dist. Lab) ND 0.0035 ND 0.0034 ND 0.0035 ND 0.0035 ND 0.0035 ND 0.0035 <0.050

Chlordene-alpha (Dist. Lab) ND 1.0 ND 0.96 ND 1 ND 0.99 ND 1 ND 1 <10

Chlordene-gamma (Dist. Lab) ND 1.0 ND 0.96 ND 1 ND 0.99 ND 1 ND 1 <10

Oxychlordane (Dist. Lab) ND 1.0 ND 0.96 ND 1 ND 0.99 ND 1 ND 1 <10

Chlordane-alpha (Dist. Lab) ND 0.03 ND 0.029 ND 0.03 ND 0.03 ND 0.03 ND 0.03 <2.0

Chlordane-gamma (Dist. Lab) ND 0.03 ND 0.029 ND 0.03 ND 0.03 ND 0.03 ND 0.03 <2.0

trans-Nonachlor (Dist. Lab) ND 1.0 ND 0.96 ND 1 ND 0.99 ND 1 ND 1 <10

cis-Nonachlor (Dist. Lab) ND 1.0 ND 0.96 ND 1 ND 0.99 ND 1 ND 1 <10

Total Chlordane (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Toxaphene (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <5.0

PCB-1016 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1221 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1232 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1242 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1248 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1254 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

PCB-1260 (Dist. Lab) ND 0.25 ND 0.24 ND 0.25 ND 0.25 ND 0.25 ND 0.25 <0.50

Total PCB (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Organochlorine Pesticides and PCB's, µg/Kg (Plant 1 BP Cake)Aldrin (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Alpha-BHC (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Beta-BHC (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Delta-BHC (Con. Lab) ND 540 -- -- -- -- ND 1600 -- -- -- -- <1,600

Gamma-BHC (Lindane) (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Chlordane (Con. Lab) ND 2700 -- -- -- -- ND 8100 -- -- -- -- <8,100

4,4'-DDD (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

4-4'-DDE (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

4-4'-DDT (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

2,4'-DDD (Con. Lab) ND 270 -- -- -- -- 1,100 810 -- -- -- -- <810

2-4'-DDE (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

2-4'-DDT (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Dieldrin (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Endosulfan I (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Endosulfan II (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Endosulfan sulfate (Con. Lab) ND 540 -- -- -- -- ND 1600 -- -- -- -- <1,600

Endrin (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Endrin Aldehyde (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Endrin Ketone (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Heptachlor (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Heptachlor epoxide (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Methoxychlor (Con. Lab) ND 270 -- -- -- -- ND 810 -- -- -- -- <810

Mirex (Con. Lab) ND 540 -- -- -- -- ND 1600 -- -- -- -- <1,600

Toxaphene (Con. Lab) ND 11000 -- -- -- -- ND 32000 -- -- -- -- <32,000

PCB-1016 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1221 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1232 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1242 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1248 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1254 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

PCB-1260 (Con. Lab) ND 5400 -- -- -- -- ND 410 -- -- -- -- <5,400

13

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Organochlorine Pesticides and PCB's, µg/Kg (Plant 2 BP Cake)Aldrin (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Alpha-BHC (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Beta-BHC (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Delta-BHC (Con. Lab) ND 460 -- -- -- -- ND 1000 -- -- -- --Gamma-BHC (Lindane) (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Chlordane (Con. Lab) ND 2300 -- -- -- -- ND 5100 -- -- -- --4,4'-DDD (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --4-4'-DDE (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --4-4'-DDT (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --2,4'-DDD (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --2-4'-DDE (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --2-4'-DDT (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Dieldrin (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Endosulfan I (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Endosulfan II (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Endosulfan sulfate (Con. Lab) ND 230 -- -- -- -- ND 1000 -- -- -- --Endrin (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Endrin Aldehyde (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Endrin Ketone (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Heptachlor (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Heptachlor epoxide (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Methoxychlor (Con. Lab) ND 230 -- -- -- -- ND 510 -- -- -- --Mirex (Con. Lab) ND 460 -- -- -- -- ND 1000 -- -- -- --Toxaphene (Con. Lab) ND 9100 -- -- -- -- ND 20000 -- -- -- --PCB-1016 (Con. Lab) ND 4600 -- -- -- -- ND 5100 -- -- -- --PCB-1221 (Con. Lab) ND 4600 -- -- -- -- ND 5100 -- -- -- --PCB-1232 (Con. Lab) ND 4600 -- -- -- -- ND 5100 -- -- -- --PCB-1242 (Con. Lab) ND 4600 -- -- -- -- ND 5100 -- -- -- --PCB-1248 (Con. Lab) ND 4600 -- -- -- -- ND 5100 -- -- -- --PCB-1254 (Con. Lab) ND 230 -- -- -- -- ND 5100 -- -- -- --PCB-1260 (Con. Lab) ND 230 -- -- -- -- ND 5100 -- -- -- --

Herbicides µg/kg (Plant 1 BP Cake)2,4,5-T (Con. Lab) ND 3110 -- -- -- -- ND 0.173 -- -- -- --2,4-D (Con. Lab) ND 6280 -- -- -- -- ND 0.349 -- -- -- --2,4-DB (Con. Lab) ND 6280 -- -- -- -- ND 0.349 -- -- -- --Dalapon (Con. Lab) ND 15700 -- -- -- -- ND 0.874 -- -- -- --Dicamba (Con. Lab) ND 3110 -- -- -- -- ND 0.173 -- -- -- --Dichlorprop (2,4-DP) (Con. Lab) ND 6280 -- -- -- -- ND 0.349 -- -- -- --Dinoseb (Con. Lab) ND 6280 -- -- -- -- ND 0.349 -- -- -- --MCPA (Con. Lab) ND 313000 -- -- -- -- ND 17.4 -- -- -- --MCPP (Con. Lab) ND 313000 -- -- -- -- ND 17.4 -- -- -- --Pentachlorophenol (Con. Lab) ND 3110 -- -- -- -- ND 0.173 -- -- -- --4-Nitrophenol (Con. Lab) ND 3110 -- -- -- -- ND 0.173 -- -- -- --Silvex (2,4,5-TP) (Con. Lab) ND 1600 -- -- -- -- ND 0.0890 -- -- -- --Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Herbicides µg/kg (Plant 2 BP Cake)2,4,5-T (Con. Lab) ND 2990 -- -- -- -- ND 0.163 -- -- -- --2,4-D (Con. Lab) ND 6040 -- -- -- -- ND 0.329 -- -- -- --2,4-DB (Con. Lab) ND 6040 -- -- -- -- ND 0.329 -- -- -- --Dalapon (Con. Lab) ND 15100 -- -- -- -- ND 0.824 -- -- -- --Dicamba (Con. Lab) ND 2990 -- -- -- -- ND 0.163 -- -- -- --Dichlorprop (2,4-DP) (Con. Lab) ND 6040 -- -- -- -- ND 0.329 -- -- -- --Dinoseb (Con. Lab) ND 6040 -- -- -- -- ND 0.329 -- -- -- --

14

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Organochlorine Pesticides and PCB's, µg/Kg (Plant 2 BP Cake)Aldrin (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Alpha-BHC (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Beta-BHC (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Delta-BHC (Con. Lab) ND 500 -- -- -- -- ND 1500 -- -- -- -- <1,500

Gamma-BHC (Lindane) (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Chlordane (Con. Lab) ND 2500 -- -- -- -- ND 7500 -- -- -- -- <7,500

4,4'-DDD (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

4-4'-DDE (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

4-4'-DDT (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

2,4'-DDD (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

2-4'-DDE (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

2-4'-DDT (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Dieldrin (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Endosulfan I (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Endosulfan II (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Endosulfan sulfate (Con. Lab) ND 500 -- -- -- -- ND 1500 -- -- -- -- <1,500

Endrin (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Endrin Aldehyde (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Endrin Ketone (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Heptachlor (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Heptachlor epoxide (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Methoxychlor (Con. Lab) ND 250 -- -- -- -- ND 750 -- -- -- -- <750

Mirex (Con. Lab) ND 500 -- -- -- -- ND 1500 -- -- -- -- <1,500

Toxaphene (Con. Lab) ND 10000 -- -- -- -- ND 30000 -- -- -- -- <30,000

PCB-1016 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1221 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1232 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1242 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1248 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1254 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

PCB-1260 (Con. Lab) ND 5000 -- -- -- -- ND 380 -- -- -- -- <5,100

Herbicides µg/kg (Plant 1 BP Cake)2,4,5-T (Con. Lab) ND 266 -- -- -- -- ND 0.0325 -- -- -- -- <3,110

2,4-D (Con. Lab) ND 319 -- -- -- -- ND 0.0658 -- -- -- -- <6,280

2,4-DB (Con. Lab) ND 266 -- -- -- -- ND 0.0658 -- -- -- -- <6,280

Dalapon (Con. Lab) ND 319 -- -- -- -- -- -- -- -- -- -- <15,700

Dicamba (Con. Lab) ND 292 -- -- -- -- -- -- -- -- -- -- <3,110

Dichlorprop (2,4-DP) (Con. Lab) ND 372 -- -- -- -- -- -- -- -- -- -- <6,280

Dinoseb (Con. Lab) ND 266 -- -- -- -- -- -- -- -- -- -- <6,280

MCPA (Con. Lab) ND 7280 -- -- -- -- -- -- -- -- -- -- <313,000

MCPP (Con. Lab) ND 13000 -- -- -- -- -- -- -- -- -- -- <313,000

Pentachlorophenol (Con. Lab) ND 266 -- -- -- -- -- -- -- -- -- -- <3,110

4-Nitrophenol (Con. Lab) ND 266 -- -- -- -- -- -- -- -- -- -- <3,110

Silvex (2,4,5-TP) (Con. Lab) ND 292 -- -- -- -- ND 0.0168 -- -- -- -- <1,600

Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Herbicides µg/kg (Plant 2 BP Cake)2,4,5-T (Con. Lab) ND 243 -- -- -- -- ND 0.0325 -- -- -- -- <2,990

2,4-D (Con. Lab) ND -- -- -- -- -- ND 0.0657 -- -- -- -- <6,040

2,4-DB (Con. Lab) ND 243 -- -- -- -- ND 0.0657 -- -- -- -- <6,040

Dalapon (Con. Lab) ND 292 -- -- -- -- -- -- -- -- -- -- <15,100

Dicamba (Con. Lab) ND 268 -- -- -- -- -- -- -- -- -- -- <2,990

Dichlorprop (2,4-DP) (Con. Lab) ND 341 -- -- -- -- -- -- -- -- -- -- <6,040

Dinoseb (Con. Lab) ND 243 -- -- -- -- -- -- -- -- -- -- <6,040

15

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

MCPA (Con. Lab) ND 302000 -- -- -- -- ND 16.4 -- -- -- --MCPP (Con. Lab) ND 302000 -- -- -- -- ND 16.4 -- -- -- --Pentachlorophenol (Con. Lab) ND 2990 -- -- -- -- ND 0.163 -- -- -- --4-Nitrophenol (Con. Lab) ND 2990 -- -- -- -- ND 0.163 -- -- -- --Silvex (2,4,5-TP) (Con. Lab) ND 1540 -- -- -- -- ND 0.0839 -- -- -- --Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Volatile Organic Compounds (Method 624), µg/L (Plant 1 Influent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.211,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.31,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.11,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 ND 2 ND 21,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.081,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.721,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.21,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.171,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,2,4-Trimethylbenzene (Dist. Lab) 0.21 0.09 0.33 0.09 0.50 0.09 0.64 0.09 0.99 0.09 0.40 0.091,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.331,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.361,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.061,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.41,3,5-Trimethylbenzene (Dist. Lab) ND 0.08 ND 0.08 0.13 0.08 0.18 0.08 0.37 0.08 ND 0.081,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.421,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.911,4-Dichlorobenzene (Dist. Lab) 0.25 0.1 0.28 0.1 0.30 0.1 1.82 0.1 0.40 0.1 ND 0.12,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.42-Butanone (Dist. Lab) 1.69 0.79 ND 0.79 2.75 0.79 1.23 0.79 3.66 0.79 ND 0.792-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.112-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 ND 0.05 ND 0.05 ND 0.052-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.234-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.044-Isopropyltoluene (Dist. Lab) 9.21 0.07 8.12 0.07 1.33 0.07 3.54 0.07 3.52 0.07 1.03 0.074-Methyl-2-pentanone (Dist. Lab) 0.59 0.19 2.99 0.19 1.59 0.19 ND 0.19 ND 0.19 ND 0.19Acetone (Dist. Lab) 441 4.5 1,090 225 800 225 577 4.5 462 4.5 2,630 225Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7Acrylonitrile (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39Benzene (Dist. Lab) ND 0.07 ND 0.07 0.11 0.07 ND 0.07 ND 0.07 ND 0.07Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2Bromochloromethane (Dist. Lab) 0.71 0.2 0.97 0.2 0.63 0.2 0.81 0.2 0.75 0.2 0.92 0.2Bromodichloromethane (Dist. Lab) 0.66 0.11 0.81 0.11 0.41 0.11 0.34 0.11 ND 0.11 0.33 0.11Bromoform (Dist. Lab) 0.57 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66Carbon Disulfide (Dist. Lab) 2.6 2 2.8 2 2.7 2 2.7 2 2.6 2 3.9 2Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38Chloroform (Dist. Lab) 4.99 0.1 7.83 0.1 8.58 0.1 6.23 0.1 6.31 0.1 10.9 0.1Dibromochloromethane (Dist. Lab) 0.60 0.18 0.46 0.18 0.19 0.18 0.21 0.18 ND 0.18 ND 0.18Dibromomethane (Dist. Lab) 0.64 0.36 0.65 0.36 0.64 0.36 0.52 0.36 0.98 0.36 0.45 0.36

16

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

MCPA (Con. Lab) ND 6670 -- -- -- -- -- -- -- -- -- -- <302,000

MCPP (Con. Lab) ND 11900 -- -- -- -- -- -- -- -- -- -- <302,000

Pentachlorophenol (Con. Lab) ND 243 -- -- -- -- -- -- -- -- -- -- <2,990

4-Nitrophenol (Con. Lab) ND 243 -- -- -- -- -- -- -- -- -- -- <2,990

Silvex (2,4,5-TP) (Con. Lab) ND -- -- -- -- -- ND 0.0167 -- -- -- -- <1,540

Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Volatile Organic Compounds (Method 624), µg/L (Plant 1 Influent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 -- -- -- -- <0.21

1,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 <0.3

1,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 <0.12

1,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 <0.1

1,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 -- -- -- -- <2

1,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 <0.08

1,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 <0.72

1,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

1,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

1,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 -- -- -- -- <0.41

1,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

1,2,4-Trimethylbenzene (Dist. Lab) 0.60 0.09 0.27 0.09 ND 0.09 0.35 0.09 -- -- -- -- 0.43

1,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 -- -- -- -- <0.33

1,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 -- -- -- -- <0.36

1,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

1,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 <0.06

cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 -- -- -- -- <0.32

trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

1,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

1,3,5-Trimethylbenzene (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 -- -- -- -- <0.08

1,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

1,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

1,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

1,4-Dichlorobenzene (Dist. Lab) 0.77 0.1 0.45 0.1 0.33 0.1 0.20 0.1 -- -- -- -- 0.48

2,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

2-Butanone (Dist. Lab) ND 0.79 ND 0.79 3.35 0.79 6.30 0.79 -- -- -- -- 1.9

2-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

2-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 ND 0.05 -- -- -- -- <0.05

2-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 -- -- -- -- <0.23

4-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 -- -- -- -- <0.04

4-Isopropyltoluene (Dist. Lab) 2.26 0.07 2.47 0.07 9.04 0.07 1.38 0.07 -- -- -- -- 4.2

4-Methyl-2-pentanone (Dist. Lab) ND 0.19 ND 0.19 ND 0.19 ND 0.19 -- -- -- -- 0.52

Acetone (Dist. Lab) 732 225 1,830 225 676 225 513 4.5 -- -- -- -- 980

Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 <3.7

Acrylonitrile (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 <0.07

Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

Bromochloromethane (Dist. Lab) 0.82 0.2 1.06 0.2 1.39 0.2 0.47 0.2 -- -- -- -- 0.85

Bromodichloromethane (Dist. Lab) 0.49 0.11 0.26 0.11 0.14 0.11 ND 0.11 0.45 0.11 2.72 0.11 0.55

Bromoform (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 0.37 0.17 ND 0.17 <0.17

Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 <0.66

Carbon Disulfide (Dist. Lab) ND 2 6.8 2 2.9 2 ND 2 -- -- -- -- 2.7

Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 <0.28

Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 <0.38

Chloroform (Dist. Lab) 6.52 0.1 8.16 0.1 7.40 0.1 4.56 0.1 7.26 0.1 6.19 0.1 7.1

Dibromochloromethane (Dist. Lab) ND 0.18 ND 0.18 ND 0.18 ND 0.18 0.51 0.18 3.42 0.18 0.45

Dibromomethane (Dist. Lab) ND 0.36 0.61 0.36 0.69 0.36 0.40 0.36 -- -- -- -- 0.56

17

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59Ethylbenzene (Dist. Lab) ND 0.12 0.98 0.12 0.49 0.12 2.81 0.12 0.22 0.12 0.27 0.12Halomethanes (Dist. Lab) 0.570 -- ND -- ND -- ND -- ND -- ND --Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Methyl Chloride (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32Methylene Chloride (Dist. Lab) 6.82 0.61 5.42 0.61 3.06 0.61 5.39 0.61 1.61 0.61 2.32 0.61MTBE (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17Naphthalene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54N-propylbenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 0.09 0.06Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Tetrachloroethene (Dist. Lab) 0.74 0.17 3.33 0.17 2.69 0.17 4.74 0.17 1.77 0.17 1.18 0.17Toluene (Dist. Lab) 0.92 0.07 3.65 0.07 1.65 0.07 1.67 0.07 3.01 0.07 1.13 0.07Trichloroethene (Dist. Lab) ND 0.17 ND 0.17 1.43 0.17 2.90 0.17 0.35 0.17 0.17 0.17Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6m,p-Xylenes (Dist. Lab) 0.28 0.06 2.62 0.06 1.68 0.06 4.59 0.06 0.61 0.06 0.98 0.06o-Xylene (Dist. Lab) ND 0.11 0.98 0.11 0.95 0.11 2.51 0.11 0.30 0.11 0.44 0.11

Volatile Organic Compounds (Method 624), µg/L (Plant 2 Influent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.211,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.31,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.11,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 ND 2 ND 21,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.081,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.721,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.21,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.171,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,2,4-Trimethylbenzene (Dist. Lab) 0.41 0.09 0.53 0.09 1.02 0.09 0.62 0.09 0.68 0.09 0.52 0.091,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.331,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.361,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.061,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 0.99 0.06 ND 0.06cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.41,3,5-Trimethylbenzene (Dist. Lab) ND 0.08 0.10 0.08 0.29 0.08 0.16 0.08 ND 0.08 ND 0.081,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.421,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.911,4-Dichlorobenzene (Dist. Lab) 0.18 0.1 0.18 0.1 0.17 0.1 ND 0.1 ND 0.1 ND 0.12,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.42-Butanone (Dist. Lab) 9.28 0.79 ND 0.79 ND 0.79 ND 0.79 4.20 0.79 26.5 0.792-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.112-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 0.61 0.05 ND 0.05 ND 0.052-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.23

18

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Ethylbenzene (Dist. Lab) 0.39 0.12 0.42 0.12 0.12 0.12 0.36 0.12 1.14 0.12 ND 0.12 0.60

Halomethanes (Dist. Lab) ND -- ND -- ND -- ND -- 0.370 -- ND -- 0.078

Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 -- -- -- -- <0.56

Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Methyl Chloride (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 <0.32

Methylene Chloride (Dist. Lab) 2.06 0.61 2.60 0.61 6.37 0.61 3.41 0.61 4.47 0.61 7.21 0.61 4.2

MTBE (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

Naphthalene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 -- -- -- -- <0.54

N-propylbenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 -- -- -- -- <0.07

Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 -- -- -- -- <3.4

Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Tetrachloroethene (Dist. Lab) 0.92 0.17 0.21 0.17 0.51 0.17 1.16 0.17 0.71 0.17 2.05 0.17 1.7

Toluene (Dist. Lab) 2.13 0.07 1.08 0.07 1.26 0.07 19.1 0.07 1.39 0.07 0.94 0.07 3.2

Trichloroethene (Dist. Lab) ND 0.17 0.18 0.17 0.17 0.17 0.20 0.17 0.24 0.17 ND 0.17 0.47

Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 -- -- -- -- <1.1

Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

m,p-Xylenes (Dist. Lab) 1.84 0.06 1.63 0.06 0.39 0.06 1.10 0.06 -- -- -- -- 1.6

o-Xylene (Dist. Lab) 0.45 0.11 0.78 0.11 0.18 0.11 0.32 0.11 -- -- -- -- 0.69

Volatile Organic Compounds (Method 624), µg/L (Plant 2 Influent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 -- -- -- -- <0.21

1,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 <0.3

1,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 <0.12

1,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 <0.1

1,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 -- -- -- -- <2

1,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 <0.08

1,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 <0.72

1,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

1,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

1,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 -- -- -- -- <0.41

1,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

1,2,4-Trimethylbenzene (Dist. Lab) 2.20 0.09 0.37 0.09 0.19 0.09 0.75 0.09 -- -- -- -- 0.73

1,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 -- -- -- -- <0.33

1,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 -- -- -- -- <0.36

1,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

1,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 0.082

cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 -- -- -- -- <0.32

trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

1,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

1,3,5-Trimethylbenzene (Dist. Lab) 0.66 0.08 0.09 0.08 ND 0.08 0.18 0.08 -- -- -- -- 0.15

1,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

1,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

1,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

1,4-Dichlorobenzene (Dist. Lab) 0.40 0.1 0.14 0.1 ND 0.1 ND 0.1 -- -- -- -- 0.11

2,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

2-Butanone (Dist. Lab) 3.40 0.79 4.55 0.79 7.52 0.79 5.80 0.79 -- -- -- -- 6.1

2-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

2-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 ND 0.05 -- -- -- -- 0.061

2-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 -- -- -- -- <0.23

19

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

4-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.044-Isopropyltoluene (Dist. Lab) 0.53 0.07 0.66 0.07 0.65 0.07 0.91 0.07 1.30 0.07 0.89 0.074-Methyl-2-pentanone (Dist. Lab) 0.21 0.19 ND 0.19 ND 0.19 ND 0.19 ND 0.19 ND 0.19Acetone (Dist. Lab) 104 4.5 142 4.5 145 4.5 102 4.5 155 4.5 316 4.5Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7Acrylonitrile (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39Benzene (Dist. Lab) 0.40 0.07 0.22 0.07 0.60 0.07 1.63 0.07 0.31 0.07 0.31 0.07Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2Bromochloromethane (Dist. Lab) 0.77 0.2 0.80 0.2 0.75 0.2 0.72 0.2 0.62 0.2 1.24 0.2Bromodichloromethane (Dist. Lab) 0.66 0.11 0.45 0.11 0.32 0.11 0.45 0.11 ND 0.11 ND 0.11Bromoform (Dist. Lab) ND 0.17 1.27 0.17 ND 0.17 0.33 0.17 ND 0.17 ND 0.17Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66Carbon Disulfide (Dist. Lab) ND 2 ND 2 ND 2 ND 2 ND 2 ND 2Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38Chloroform (Dist. Lab) 2.87 0.1 4.27 0.1 4.93 0.1 3.83 0.1 3.68 0.1 5.79 0.1Dibromochloromethane (Dist. Lab) 0.89 0.18 0.31 0.18 ND 0.18 0.37 0.18 ND 0.18 ND 0.18Dibromomethane (Dist. Lab) 0.84 0.36 0.88 0.36 0.93 0.36 0.87 0.36 0.77 0.36 0.73 0.36Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59Ethylbenzene (Dist. Lab) 0.20 0.12 0.49 0.12 0.61 0.12 2.39 0.12 0.20 0.12 0.43 0.12Halomethanes (Dist. Lab) ND -- 1.27 -- ND -- 0.330 -- ND -- ND --Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Methyl Chloride (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32Methylene Chloride (Dist. Lab) 2.00 0.61 1.40 0.61 2.04 0.61 1.81 0.61 6.23 0.61 6.30 0.61MTBE (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17Naphthalene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54N-propylbenzene (Dist. Lab) ND 0.06 ND 0.06 0.18 0.06 ND 0.06 ND 0.06 ND 0.06Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Tetrachloroethene (Dist. Lab) 0.88 0.17 3.67 0.17 2.52 0.17 5.16 0.17 1.70 0.17 ND 0.17Toluene (Dist. Lab) 1.03 0.07 2.43 0.07 3.71 0.07 1.29 0.07 1.34 0.07 1.54 0.07Trichloroethene (Dist. Lab) 0.29 0.17 2.47 0.17 1.50 0.17 3.03 0.17 0.18 0.17 ND 0.17Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6m,p-Xylenes (Dist. Lab) 0.50 0.06 0.69 0.06 2.07 0.06 3.13 0.06 0.57 0.06 1.73 0.06o-Xylene (Dist. Lab) 0.27 0.11 0.48 0.11 1.18 0.11 1.96 0.11 0.27 0.11 0.98 0.11

Volatile Organic Compounds (Method 624), µg/L (Plant 2 Influent D Headworks)1,1,1,2-Tetrachloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1,1-Trichloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1,2,2-Tetrachloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1,2-Trichloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1,2-Trichlorotrifluoroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1-Dichloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1-Dichloroethene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,1-Dichloropropene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2,3-Trichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2,3-Trichloropropane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2,4-Trichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2,4-Trimethylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

20

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

4-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 -- -- -- -- <0.04

4-Isopropyltoluene (Dist. Lab) 1.03 0.07 0.65 0.07 0.46 0.07 0.97 0.07 -- -- -- -- 0.80

4-Methyl-2-pentanone (Dist. Lab) ND 0.19 ND 0.19 ND 0.19 ND 0.19 -- -- -- -- <0.19

Acetone (Dist. Lab) 139 4.5 122 4.5 215 4.5 215 4.5 -- -- -- -- 170

Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 <3.7

Acrylonitrile (Dist. Lab) ND 0.39 0.60 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzene (Dist. Lab) 0.48 0.07 0.36 0.07 0.28 0.07 0.60 0.07 0.34 0.07 0.37 0.07 0.49

Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

Bromochloromethane (Dist. Lab) 0.82 0.2 0.63 0.2 0.93 0.2 0.87 0.2 -- -- -- -- 0.81

Bromodichloromethane (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 0.28 0.11 ND 0.11 0.18

Bromoform (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 <0.17

Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 <0.66

Carbon Disulfide (Dist. Lab) ND 2 ND 2 ND 2 ND 2 -- -- -- -- <2

Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 <0.28

Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 <0.38

Chloroform (Dist. Lab) 3.63 0.1 3.03 0.1 3.62 0.1 2.51 0.1 3.49 0.1 2.97 0.1 3.7

Dibromochloromethane (Dist. Lab) ND 0.18 ND 0.18 ND 0.18 ND 0.18 0.30 0.18 ND 0.18 <0.18

Dibromomethane (Dist. Lab) 0.61 0.36 0.37 0.36 0.58 0.36 0.81 0.36 -- -- -- -- 0.74

Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Ethylbenzene (Dist. Lab) 1.13 0.12 0.27 0.12 ND 0.12 0.17 0.12 0.24 0.12 0.22 0.12 0.53

Halomethanes (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- 0.13

Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 -- -- -- -- <0.56

Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Methyl Chloride (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 <0.32

Methylene Chloride (Dist. Lab) 1.95 0.61 0.88 0.61 1.15 0.61 1.24 0.61 7.12 0.61 4.74 0.61 3.1

MTBE (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

Naphthalene (Dist. Lab) 0.40 0.12 0.24 0.12 ND 0.12 0.33 0.12 -- -- -- -- <0.12

N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 -- -- -- -- <0.54

N-propylbenzene (Dist. Lab) 0.30 0.06 ND 0.06 ND 0.06 0.11 0.06 -- -- -- -- <0.06

Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 -- -- -- -- <0.07

Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 -- -- -- -- <3.4

Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Tetrachloroethene (Dist. Lab) 0.71 0.17 0.72 0.17 0.77 0.17 ND 0.17 0.39 0.17 2.38 0.17 1.6

Toluene (Dist. Lab) 6.20 0.07 1.73 0.07 9.78 0.07 2.86 0.07 2.55 0.07 1.63 0.07 3.0

Trichloroethene (Dist. Lab) 0.34 0.17 0.20 0.17 0.24 0.17 ND 0.17 0.37 0.17 ND 0.17 0.72

Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 -- -- -- -- <1.1

Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

m,p-Xylenes (Dist. Lab) 4.80 0.06 0.88 0.06 0.23 0.06 0.37 0.06 -- -- -- -- 1.5

o-Xylene (Dist. Lab) 1.83 0.11 0.47 0.11 ND 0.11 0.27 0.11 -- -- -- -- 0.77

Volatile Organic Compounds (Method 624), µg/L (Plant 2 Influent D Headworks)1,1,1,2-Tetrachloroethane (Dist. Lab) -- -- ND 0.21 ND 0.21 ND 0.21 -- -- -- -- <0.21

1,1,1-Trichloroethane (Dist. Lab) -- -- ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 <0.3

1,1,2,2-Tetrachloroethane (Dist. Lab) -- -- ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 <0.12

1,1,2-Trichloroethane (Dist. Lab) -- -- ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 <0.1

1,1,2-Trichlorotrifluoroethane (Dist. Lab) -- -- ND 2 ND 2 ND 2 -- -- -- -- <2

1,1-Dichloroethane (Dist. Lab) -- -- ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 <0.08

1,1-Dichloroethene (Dist. Lab) -- -- ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 <0.72

1,1-Dichloropropene (Dist. Lab) -- -- ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

1,2,3-Trichlorobenzene (Dist. Lab) -- -- ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

1,2,3-Trichloropropane (Dist. Lab) -- -- ND 0.41 ND 0.41 ND 0.41 -- -- -- -- <0.41

1,2,4-Trichlorobenzene (Dist. Lab) -- -- ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

1,2,4-Trimethylbenzene (Dist. Lab) -- -- ND 0.09 0.14 0.09 0.27 0.09 -- -- -- -- 0.14

21

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

1,2-Dibromo-3-chloropropane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2-Dibromoethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2-Dichloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --cis-1,2-Dichloroethene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --trans-1,2-Dichloroethene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2-Dichloropropane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,3,5-Trimethylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,3-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,3-Dichloropropane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --cis-1,3-Dichloropropene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --trans-1,3-Dichloropropene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,3-Dichloropropene Total (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,4-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,2-Dichloropropane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Butanone (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Chloroethylvinylether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Chlorotoluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Hexanone (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Chlorotoluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Isopropyltoluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Methyl-2-pentanone (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acetone (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acrolein (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acrylonitrile (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Bromobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Bromochloromethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Bromodichloromethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Bromoform (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Bromomethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Carbon Disulfide (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Carbon tetrachloride (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chloroform (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dibromochloromethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dibromomethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dichlorodifluoromethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Ethylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Halomethanes (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachlorobutadiene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Isopropylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Methyl tert-pentyl ether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Methyl Chloride (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Methylene Chloride (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --MTBE (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Naphthalene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --N-butylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --N-propylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Sec-butylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Styrene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Tert-butyl alcohol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Tert-butyl ethyl ether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Tert-butylbenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Tetrachloroethene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Toluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Trichloroethene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

22

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

1,2-Dibromo-3-chloropropane (Dist. Lab) -- -- ND 0.33 ND 0.33 ND 0.33 -- -- -- -- <0.33

1,2-Dibromoethane (Dist. Lab) -- -- ND 0.36 ND 0.36 ND 0.36 -- -- -- -- <0.36

1,2-Dichlorobenzene (Dist. Lab) -- -- ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

1,2-Dichloroethane (Dist. Lab) -- -- ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 <0.06

cis-1,2-Dichloroethene (Dist. Lab) -- -- ND 0.32 ND 0.32 ND 0.32 -- -- -- -- <0.32

trans-1,2-Dichloroethene (Dist. Lab) -- -- ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

1,2-Dichloropropane (Dist. Lab) -- -- ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

1,3,5-Trimethylbenzene (Dist. Lab) -- -- ND 0.08 ND 0.08 ND 0.08 -- -- -- -- <0.08

1,3-Dichlorobenzene (Dist. Lab) -- -- ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

1,3-Dichloropropane (Dist. Lab) -- -- ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

cis-1,3-Dichloropropene (Dist. Lab) -- -- ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

trans-1,3-Dichloropropene (Dist. Lab) -- -- ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

1,3-Dichloropropene Total (Dist. Lab) -- -- ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

1,4-Dichlorobenzene (Dist. Lab) -- -- ND 0.1 0.32 0.1 0.29 0.1 -- -- -- -- 0.20

2,2-Dichloropropane (Dist. Lab) -- -- ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

2-Butanone (Dist. Lab) -- -- ND 0.79 ND 0.79 11.5 0.79 -- -- -- -- 3.8

2-Chloroethylvinylether (Dist. Lab) -- -- ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

2-Chlorotoluene (Dist. Lab) -- -- ND 0.05 ND 0.05 ND 0.05 -- -- -- -- <0.05

2-Hexanone (Dist. Lab) -- -- ND 0.23 ND 0.23 ND 0.23 -- -- -- -- <0.23

4-Chlorotoluene (Dist. Lab) -- -- ND 0.04 ND 0.04 ND 0.04 -- -- -- -- <0.04

4-Isopropyltoluene (Dist. Lab) -- -- 3.61 0.07 23.4 0.07 2.95 0.07 -- -- -- -- 10.0

4-Methyl-2-pentanone (Dist. Lab) -- -- ND 0.19 ND 0.19 ND 0.19 -- -- -- -- <0.19

Acetone (Dist. Lab) -- -- 91.4 4.5 143 4.5 468 4.5 -- -- -- -- 230

Acrolein (Dist. Lab) -- -- ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 <3.7

Acrylonitrile (Dist. Lab) -- -- ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzene (Dist. Lab) -- -- ND 0.07 ND 0.07 ND 0.07 0.14 0.07 ND 0.07 <0.07

Bromobenzene (Dist. Lab) -- -- ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

Bromochloromethane (Dist. Lab) -- -- 0.69 0.2 1.12 0.2 0.81 0.2 -- -- -- -- 0.87

Bromodichloromethane (Dist. Lab) -- -- 0.12 0.11 0.30 0.11 0.11 0.11 0.44 0.11 ND 0.11 0.19

Bromoform (Dist. Lab) -- -- ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 <0.17

Bromomethane (Dist. Lab) -- -- ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 <0.66

Carbon Disulfide (Dist. Lab) -- -- ND 2 ND 2 ND 2 -- -- -- -- <2

Carbon tetrachloride (Dist. Lab) -- -- ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 <0.28

Chlorobenzene (Dist. Lab) -- -- ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

Chloroethane (Dist. Lab) -- -- ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 <0.38

Chloroform (Dist. Lab) -- -- 3.42 0.1 6.27 0.1 4.06 0.1 3.93 0.1 3.25 0.1 4.2

Dibromochloromethane (Dist. Lab) -- -- ND 0.18 ND 0.18 ND 0.18 0.45 0.18 ND 0.18 <0.18

Dibromomethane (Dist. Lab) -- -- 0.49 0.36 0.56 0.36 0.66 0.36 -- -- -- -- 0.57

Dichlorodifluoromethane (Dist. Lab) -- -- ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Ethylbenzene (Dist. Lab) -- -- ND 0.12 ND 0.12 0.25 0.12 0.29 0.12 ND 0.12 <0.12

Halomethanes (Dist. Lab) -- -- ND -- ND -- ND -- ND -- ND -- ND

Hexachlorobutadiene (Dist. Lab) -- -- ND 0.56 ND 0.56 ND 0.56 -- -- -- -- <0.56

Isopropylbenzene (Dist. Lab) -- -- ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

Methyl tert-pentyl ether (Dist. Lab) -- -- ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Methyl Chloride (Dist. Lab) -- -- ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 <0.32

Methylene Chloride (Dist. Lab) -- -- 8.93 0.61 3.42 0.61 2.75 0.61 9.33 0.61 1.25 0.61 5.1

MTBE (Dist. Lab) -- -- ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

Naphthalene (Dist. Lab) -- -- ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

N-butylbenzene (Dist. Lab) -- -- ND 0.54 ND 0.54 ND 0.54 -- -- -- -- <0.54

N-propylbenzene (Dist. Lab) -- -- ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

Sec-butylbenzene (Dist. Lab) -- -- ND 0.07 ND 0.07 ND 0.07 -- -- -- -- <0.07

Styrene (Dist. Lab) -- -- ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butyl alcohol (Dist. Lab) -- -- ND 3.4 ND 3.4 ND 3.4 -- -- -- -- <3.4

Tert-butyl ethyl ether (Dist. Lab) -- -- ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butylbenzene (Dist. Lab) -- -- ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Tetrachloroethene (Dist. Lab) -- -- 0.56 0.17 ND 0.17 0.89 0.17 0.67 0.17 2.41 0.17 0.91

Toluene (Dist. Lab) -- -- 1.04 0.07 1.33 0.07 19.4 0.07 2.22 0.07 1.17 0.07 5.0

Trichloroethene (Dist. Lab) -- -- ND 0.17 ND 0.17 ND 0.17 0.18 0.17 ND 0.17 <0.17

23

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Trichlorofluoromethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Vinyl Acetate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Vinyl Chloride (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --m,p-Xylenes (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --o-Xylene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Volatile Organic Compounds (Method 624), µg/L (Final Effluent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.21 ND 0.211,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.31,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.11,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 ND 2 ND 21,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.081,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.721,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.21,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.171,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.121,2,4-Trimethylbenzene (Dist. Lab) 0.24 0.09 ND 0.09 0.46 0.09 0.36 0.09 0.15 0.09 ND 0.091,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.331,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.361,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.061,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 2.60 0.06 ND 0.06cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.41,3,5-Trimethylbenzene (Dist. Lab) ND 0.08 ND 0.08 0.14 0.08 ND 0.08 ND 0.08 ND 0.081,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.111,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.421,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.911,4-Dichlorobenzene (Dist. Lab) 0.14 0.1 ND 0.1 0.14 0.1 ND 0.1 ND 0.1 ND 0.12,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.42-Butanone (Dist. Lab) 6.51 0.79 5.60 0.79 ND 0.79 1.55 0.79 ND 0.79 ND 0.792-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.112-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 ND 0.05 ND 0.05 ND 0.052-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.23 ND 0.234-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.04 ND 0.044-Isopropyltoluene (Dist. Lab) ND 0.07 ND 0.07 0.22 0.07 0.46 0.07 0.64 0.07 ND 0.074-Methyl-2-pentanone (Dist. Lab) ND 0.19 ND 0.19 ND 0.19 ND 0.19 ND 0.19 ND 0.19Acetone (Dist. Lab) 51.1 4.5 127 4.5 73.1 4.5 72.9 4.5 68.9 4.5 ND 4.5Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7Acrylonitrile (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39Benzene (Dist. Lab) 0.18 0.07 ND 0.07 0.24 0.07 1.59 0.07 ND 0.07 ND 0.07Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2 ND 0.2Bromochloromethane (Dist. Lab) 0.40 0.2 0.37 0.2 ND 0.2 0.37 0.2 0.31 0.2 ND 0.2Bromodichloromethane (Dist. Lab) 2.31 0.11 2.33 0.11 2.01 0.11 2.01 0.11 1.96 0.11 1.93 0.11Bromoform (Dist. Lab) 1.14 0.17 ND 0.17 1.39 0.17 0.59 0.17 ND 0.17 ND 0.17Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66Carbon Disulfide (Dist. Lab) ND 2 ND 2 ND 2 ND 2 ND 2 ND 2Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38Chloroform (Dist. Lab) 7.55 0.1 9.52 0.1 7.67 0.1 7.86 0.1 6.54 0.1 7.01 0.1Dibromochloromethane (Dist. Lab) 1.42 0.18 0.99 0.18 0.78 0.18 0.87 0.18 0.99 0.18 0.64 0.18Dibromomethane (Dist. Lab) 0.60 0.36 0.40 0.36 ND 0.36 ND 0.36 ND 0.36 ND 0.36Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59

24

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Trichlorofluoromethane (Dist. Lab) -- -- ND 1.1 ND 1.1 ND 1.1 -- -- -- -- <1.1

Vinyl Acetate (Dist. Lab) -- -- ND 1 ND 1 ND 1 -- -- -- -- <1

Vinyl Chloride (Dist. Lab) -- -- ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

m,p-Xylenes (Dist. Lab) -- -- 0.32 0.06 0.10 0.06 0.77 0.06 -- -- -- -- 0.40

o-Xylene (Dist. Lab) -- -- 0.13 0.11 ND 0.11 0.27 0.11 -- -- -- -- 0.13

Volatile Organic Compounds (Method 624), µg/L (Final Effluent)1,1,1,2-Tetrachloroethane (Dist. Lab) ND 0.21 ND 0.21 ND 0.21 ND 0.21 -- -- -- -- <0.21

1,1,1-Trichloroethane (Dist. Lab) ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 ND 0.3 <0.3

1,1,2,2-Tetrachloroethane (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 <0.12

1,1,2-Trichloroethane (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 <0.1

1,1,2-Trichlorotrifluoroethane (Dist. Lab) ND 2 ND 2 ND 2 ND 2 -- -- -- -- <2

1,1-Dichloroethane (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 ND 0.08 <0.08

1,1-Dichloroethene (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 <0.72

1,1-Dichloropropene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

1,2,3-Trichlorobenzene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

1,2,3-Trichloropropane (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 -- -- -- -- <0.41

1,2,4-Trichlorobenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

1,2,4-Trimethylbenzene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- 0.12

1,2-Dibromo-3-chloropropane (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 -- -- -- -- <0.33

1,2-Dibromoethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 -- -- -- -- <0.36

1,2-Dichlorobenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

1,2-Dichloroethane (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 0.22

cis-1,2-Dichloroethene (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 -- -- -- -- <0.32

trans-1,2-Dichloroethene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

1,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

1,3,5-Trimethylbenzene (Dist. Lab) ND 0.08 ND 0.08 ND 0.08 ND 0.08 -- -- -- -- <0.08

1,3-Dichlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

1,3-Dichloropropane (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

cis-1,3-Dichloropropene (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

trans-1,3-Dichloropropene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

1,3-Dichloropropene Total (Dist. Lab) ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 ND 0.91 <0.91

1,4-Dichlorobenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

2,2-Dichloropropane (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

2-Butanone (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 -- -- -- -- 1.4

2-Chloroethylvinylether (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

2-Chlorotoluene (Dist. Lab) ND 0.05 ND 0.05 ND 0.05 ND 0.05 -- -- -- -- <0.05

2-Hexanone (Dist. Lab) ND 0.23 ND 0.23 ND 0.23 ND 0.23 -- -- -- -- <0.23

4-Chlorotoluene (Dist. Lab) ND 0.04 ND 0.04 ND 0.04 ND 0.04 -- -- -- -- <0.04

4-Isopropyltoluene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 -- -- -- -- 0.13

4-Methyl-2-pentanone (Dist. Lab) ND 0.19 ND 0.19 ND 0.19 ND 0.19 -- -- -- -- <0.19

Acetone (Dist. Lab) ND 4.5 37.5 4.5 ND 4.5 ND 4.5 -- -- -- -- 43

Acrolein (Dist. Lab) ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 ND 3.7 <3.7

Acrylonitrile (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 0.17

Bromobenzene (Dist. Lab) ND 0.2 ND 0.2 ND 0.2 ND 0.2 -- -- -- -- <0.2

Bromochloromethane (Dist. Lab) ND 0.2 0.25 0.2 0.39 0.2 0.37 0.2 -- -- -- -- 0.25

Bromodichloromethane (Dist. Lab) 1.33 0.11 1.25 0.11 0.81 0.11 1.60 0.11 1.62 0.11 3.62 0.11 1.9

Bromoform (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 0.26

Bromomethane (Dist. Lab) ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 ND 0.66 <0.66

Carbon Disulfide (Dist. Lab) ND 2 ND 2 ND 2 ND 2 -- -- -- -- <2

Carbon tetrachloride (Dist. Lab) ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 ND 0.28 <0.28

Chlorobenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 <0.11

Chloroethane (Dist. Lab) ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 ND 0.38 <0.38

Chloroform (Dist. Lab) 4.80 0.1 5.66 0.1 3.77 0.1 5.15 0.1 3.88 0.1 5.31 0.1 6.2

Dibromochloromethane (Dist. Lab) 0.39 0.18 0.50 0.18 0.29 0.18 0.47 0.18 0.89 0.18 3.57 0.18 0.98

Dibromomethane (Dist. Lab) ND 0.36 ND 0.36 ND 0.36 ND 0.36 -- -- -- -- <0.36

Dichlorodifluoromethane (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

25

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Ethylbenzene (Dist. Lab) ND 0.12 ND 0.12 0.27 0.12 ND 0.12 ND 0.12 ND 0.12Halomethanes (Dist. Lab) 1.96 -- 1.13 -- 2.03 -- 3.35 -- 1.07 -- ND --Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11 ND 0.11Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Methyl Chloride (Dist. Lab) 0.82 0.32 1.13 0.32 0.64 0.32 2.76 0.32 1.07 0.32 ND 0.32Methylene Chloride (Dist. Lab) ND 0.61 1.76 0.61 1.09 0.61 1.08 0.61 2.80 0.61 0.80 0.61MTBE (Dist. Lab) ND 0.17 0.19 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17Naphthalene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54N-propylbenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06 ND 0.06Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07 ND 0.07Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4 ND 3.4Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09 ND 0.09Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1 ND 0.1Tetrachloroethene (Dist. Lab) 0.28 0.17 3.19 0.17 2.15 0.17 4.42 0.17 0.17 0.17 ND 0.17Toluene (Dist. Lab) 0.71 0.07 2.07 0.07 1.88 0.07 0.87 0.07 0.80 0.07 0.30 0.07Trichloroethene (Dist. Lab) ND 0.17 1.86 0.17 1.36 0.17 ND 0.17 ND 0.17 ND 0.17Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6m,p-Xylenes (Dist. Lab) 0.30 0.06 0.31 0.06 0.90 0.06 2.50 0.06 0.26 0.06 0.11 0.06o-Xylene (Dist. Lab) 0.16 0.11 ND 0.11 0.79 0.11 1.72 0.11 0.11 0.11 0.12 0.11

Volatile Organic Compounds, µg/kg (Plant 1 BP Cake)1,1,1-Trichloroethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,1,1,2-Tetrachloroethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --1,1,2,2-Tetrachloroethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,1,2-Trichloroethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,1-Dichloroethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,1-Dichloroethene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --1,1-Dichloropropene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,2-Dibromoethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,2-Dibromo-3-chloropropane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --1,2-Dichlorobenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,2-Dichloroethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --cis-1,2-Dichloroethene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --trans-1,2-Dichloroethene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,2-Dichloropropane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,2,3-Trichlorobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --1,2,3-Trichloropropane (Con. Lab) ND 230 -- -- -- -- ND 260 -- -- -- --1,2,4-Trichlorobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --1,2,4-Trimethylbenzene (Con. Lab) 120 47 -- -- -- -- 130 52 -- -- -- --1,3-Dichlorobenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,3-Dichloropropane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --cis-1,3-Dichloropropene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --trans-1,3-Dichloropropene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,3,5-Trimethylbenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --1,4-Dichlorobenzene (Con. Lab) 61 47 -- -- -- -- 71 52 -- -- -- --2,2-Dichloropropane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --2-Butanone (Con. Lab) 1,000 230 -- -- -- -- 1,800 260 -- -- -- --2-Chlorotoluene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --4-Chlorotoluene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Acrolein (Con. Lab) ND 2300 -- -- -- -- ND 2600 -- -- -- --Acrylonitrile (Con. Lab) ND 2300 -- -- -- -- ND 2600 -- -- -- --Benzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Bromobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --

26

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Ethylbenzene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 ND 0.12 <0.12

Halomethanes (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- 0.80

Hexachlorobutadiene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 -- -- -- -- <0.56

Isopropylbenzene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- <0.11

Methyl tert-pentyl ether (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Methyl Chloride (Dist. Lab) ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 ND 0.32 0.54

Methylene Chloride (Dist. Lab) 1.12 0.61 0.88 0.61 0.86 0.61 ND 0.61 1.43 0.61 ND 0.61 0.99

MTBE (Dist. Lab) 0.23 0.17 ND 0.17 ND 0.17 ND 0.17 -- -- -- -- <0.17

Naphthalene (Dist. Lab) ND 0.12 ND 0.12 ND 0.12 ND 0.12 -- -- -- -- <0.12

N-butylbenzene (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 -- -- -- -- <0.54

N-propylbenzene (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- <0.06

Sec-butylbenzene (Dist. Lab) ND 0.07 ND 0.07 ND 0.07 ND 0.07 -- -- -- -- <0.07

Styrene (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butyl alcohol (Dist. Lab) ND 3.4 ND 3.4 ND 3.4 ND 3.4 -- -- -- -- <3.4

Tert-butyl ethyl ether (Dist. Lab) ND 0.09 ND 0.09 ND 0.09 ND 0.09 -- -- -- -- <0.09

Tert-butylbenzene (Dist. Lab) ND 0.1 ND 0.1 ND 0.1 ND 0.1 -- -- -- -- <0.1

Tetrachloroethene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 0.85

Toluene (Dist. Lab) 0.17 0.07 0.48 0.07 0.07 0.07 0.08 0.07 0.09 0.07 ND 0.07 0.63

Trichloroethene (Dist. Lab) ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 ND 0.17 0.27

Trichlorofluoromethane (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 -- -- -- -- <1.1

Vinyl Acetate (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Vinyl Chloride (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

m,p-Xylenes (Dist. Lab) ND 0.06 ND 0.06 ND 0.06 ND 0.06 -- -- -- -- 0.44

o-Xylene (Dist. Lab) ND 0.11 ND 0.11 ND 0.11 ND 0.11 -- -- -- -- 0.29

Volatile Organic Compounds, µg/kg (Plant 1 BP Cake)1,1,1-Trichloroethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,1,1,2-Tetrachloroethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

1,1,2,2-Tetrachloroethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,1,2-Trichloroethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,1-Dichloroethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,1-Dichloroethene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

1,1-Dichloropropene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,2-Dibromoethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,2-Dibromo-3-chloropropane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

1,2-Dichlorobenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,2-Dichloroethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

cis-1,2-Dichloroethene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

trans-1,2-Dichloroethene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,2-Dichloropropane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,2,3-Trichlorobenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

1,2,3-Trichloropropane (Con. Lab) ND 260 -- -- -- -- ND 280 -- -- -- -- <280

1,2,4-Trichlorobenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

1,2,4-Trimethylbenzene (Con. Lab) 180 53 -- -- -- -- ND 55 -- -- -- -- 110

1,3-Dichlorobenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,3-Dichloropropane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

cis-1,3-Dichloropropene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

trans-1,3-Dichloropropene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,3,5-Trimethylbenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

1,4-Dichlorobenzene (Con. Lab) 98 53 -- -- -- -- ND 55 -- -- -- -- 58

2,2-Dichloropropane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

2-Butanone (Con. Lab) 2,700 260 -- -- -- -- 1,300 280 -- -- -- -- 1,700

2-Chlorotoluene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

4-Chlorotoluene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Acrolein (Con. Lab) ND 2600 -- -- -- -- ND 2800 -- -- -- -- <2,800

Acrylonitrile (Con. Lab) ND 2600 -- -- -- -- ND 2800 -- -- -- -- <2,800

Benzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Bromobenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

27

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Bromochloromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Bromodichloromethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Bromoform (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Bromomethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --n-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --sec-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --tert-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Carbon tetrachloride (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Chlorobenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Chloroethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Chloroform (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Chloromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Dibromochloromethane (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Dichlorodifluoromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Ethylbenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Hexachlorobutadiene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Isobutyl alcohol (Con. Lab) ND 940 -- -- -- -- ND 1000 -- -- -- --Isopropylbenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --p-Isopropyltoluene (Con. Lab) 3,100 47 -- -- -- -- 4,000 52 -- -- -- --Methylene Chloride (Con. Lab) ND 470 -- -- -- -- ND 520 -- -- -- --MIBK (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Naphthalene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --n-Propylbenzene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Styrene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Tetrachloroethene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Toluene (Con. Lab) 85 47 -- -- -- -- 110 52 -- -- -- --Trichloroethene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --Trichlorofluoromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --Vinyl Chloride (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- --m,p-Xylenes (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --o-Xylene (Con. Lab) ND 47 -- -- -- -- ND 52 -- -- -- --

Volatile Organic Compounds, µg/kg (Plant 2 BP Cake)1,1,1-Trichloroethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,1,1,2-Tetrachloroethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --1,1,2,2-Tetrachloroethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,1,2-Trichloroethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,1-Dichloroethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,1-Dichloroethene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --1,2-Dibromoethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,2-Dibromo-3-chloropropane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --1,2-Dichlorobenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,2-Dichloroethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --cis-1,2-Dichloroethene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --trans-1,2-Dichloroethene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,2-Dichloropropane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,2,3-Trichlorobenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --1,2,3-Trichloropropane (Con. Lab) ND 230 -- -- -- -- ND 250 -- -- -- --1,2,4-Trichlorobenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --1,2,4-Trimethylbenzene (Con. Lab) 320 45 -- -- -- -- 88 51 -- -- -- --1,3-Dichlorobenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,3-Dichloropropane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --cis-1,3-Dichloropropene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --trans-1,3-Dichloropropene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --1,3,5-Trimethylbenzene (Con. Lab) 120 45 -- -- -- -- ND 51 -- -- -- --1,4-Dichlorobenzene (Con. Lab) 82 38 -- -- -- -- ND 51 -- -- -- --2,2-Dichloropropane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --

28

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Bromochloromethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Bromodichloromethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Bromoform (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Bromomethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

n-Butylbenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

sec-Butylbenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

tert-Butylbenzene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Carbon tetrachloride (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Chlorobenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Chloroethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Chloroform (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Chloromethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Dibromochloromethane (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Dichlorodifluoromethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Ethylbenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Hexachlorobutadiene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Isobutyl alcohol (Con. Lab) ND 1100 -- -- -- -- ND 1100 -- -- -- -- <1,100

Isopropylbenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

p-Isopropyltoluene (Con. Lab) 970 53 -- -- -- -- 230 55 -- -- -- -- 2,100

Methylene Chloride (Con. Lab) ND 530 -- -- -- -- ND 550 -- -- -- -- <550

MIBK (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Naphthalene (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

n-Propylbenzene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Styrene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Tetrachloroethene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Toluene (Con. Lab) 140 53 -- -- -- -- 56 55 -- -- -- -- 98

Trichloroethene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Trichlorofluoromethane (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

Vinyl Chloride (Con. Lab) ND 130 -- -- -- -- ND 140 -- -- -- -- <140

m,p-Xylenes (Con. Lab) 59 53 -- -- -- -- ND 55 -- -- -- -- <55

o-Xylene (Con. Lab) ND 53 -- -- -- -- ND 55 -- -- -- -- <55

Volatile Organic Compounds, µg/kg (Plant 2 BP Cake)1,1,1-Trichloroethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,1,1,2-Tetrachloroethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

1,1,2,2-Tetrachloroethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,1,2-Trichloroethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,1-Dichloroethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,1-Dichloroethene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

1,2-Dibromoethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,2-Dibromo-3-chloropropane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

1,2-Dichlorobenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,2-Dichloroethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

cis-1,2-Dichloroethene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

trans-1,2-Dichloroethene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,2-Dichloropropane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,2,3-Trichlorobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

1,2,3-Trichloropropane (Con. Lab) ND 240 -- -- -- -- ND 250 -- -- -- -- <250

1,2,4-Trichlorobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

1,2,4-Trimethylbenzene (Con. Lab) 260 49 -- -- -- -- 86 50 -- -- -- -- 190

1,3-Dichlorobenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,3-Dichloropropane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

cis-1,3-Dichloropropene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

trans-1,3-Dichloropropene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

1,3,5-Trimethylbenzene (Con. Lab) 67 49 -- -- -- -- ND 50 -- -- -- -- <51

1,4-Dichlorobenzene (Con. Lab) 59 49 -- -- -- -- ND 50 -- -- -- -- <51

2,2-Dichloropropane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

29

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

2-Butanone (Con. Lab) 6,000 230 -- -- -- -- 4,900 250 -- -- -- --2-Chlorotoluene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --4-Chlorotoluene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Acrolein (Con. Lab) ND 2300 -- -- -- -- ND 2500 -- -- -- --Acrylonitrile (Con. Lab) ND 2300 -- -- -- -- ND 2500 -- -- -- --Benzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Bromobenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Bromochloromethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Bromodichloromethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Bromoform (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Bromomethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --n-Butylbenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --sec-Butylbenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --tert-Butylbenzene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Chlorobenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Chloroethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Chloroform (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Chloromethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Dibromochloromethane (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Dichlorodifluoromethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Ethylbenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Hexachlorobutadiene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Isobutyl alcohol (Con. Lab) ND 900 -- -- -- -- ND 1000 -- -- -- --Isopropylbenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --p-Isopropyltoluene (Con. Lab) 4,600 45 -- -- -- -- 520 51 -- -- -- --Methylene Chloride (Con. Lab) ND 450 -- -- -- -- ND 510 -- -- -- --MIBK (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Naphthalene (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --n-Propylbenzene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Styrene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Tetrachloroethene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Toluene (Con. Lab) 63 45 -- -- -- -- ND 51 -- -- -- --Trichloroethene (Con. Lab) ND 45 -- -- -- -- ND 51 -- -- -- --Trichlorofluoromethane (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --Vinyl Chloride (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --m,p-Xylenes (Con. Lab) 110 45 -- -- -- -- ND 51 -- -- -- --o-Xylene (Con. Lab) 50 45 -- -- -- -- ND 51 -- -- -- --

Extractable Organic Compounds B/N/A, µg/L (Plant 1 Influent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.481,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.521,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.692,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.752,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.762,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.842,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.622,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.712-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.642-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.72-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.792-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.812-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.63,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49

30

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

2-Butanone (Con. Lab) 5,100 240 -- -- -- -- 2,300 250 -- -- -- -- 4,600

2-Chlorotoluene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

4-Chlorotoluene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Acrolein (Con. Lab) ND 2400 -- -- -- -- ND 2500 -- -- -- -- <2,500

Acrylonitrile (Con. Lab) ND 2400 -- -- -- -- ND 2500 -- -- -- -- <2,500

Benzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Bromobenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Bromochloromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Bromodichloromethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Bromoform (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Bromomethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

n-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

sec-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

tert-Butylbenzene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Chlorobenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Chloroethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Chloroform (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Chloromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Dibromochloromethane (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Dichlorodifluoromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Ethylbenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Hexachlorobutadiene (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Isobutyl alcohol (Con. Lab) ND 980 -- -- -- -- ND 1000 -- -- -- -- <1,000

Isopropylbenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

p-Isopropyltoluene (Con. Lab) 2,000 49 -- -- -- -- 560 50 -- -- -- -- 1,900

Methylene Chloride (Con. Lab) ND 490 -- -- -- -- ND 500 -- -- -- -- <510

MIBK (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Naphthalene (Con. Lab) 150 120 -- -- -- -- ND 130 -- -- -- -- <130

n-Propylbenzene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Styrene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Tetrachloroethene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Toluene (Con. Lab) 130 49 -- -- -- -- 140 50 -- -- -- -- 83

Trichloroethene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Trichlorofluoromethane (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

Vinyl Chloride (Con. Lab) ND 120 -- -- -- -- ND 130 -- -- -- -- <130

m,p-Xylenes (Con. Lab) 94 49 -- -- -- -- ND 50 -- -- -- -- 51

o-Xylene (Con. Lab) ND 49 -- -- -- -- ND 50 -- -- -- -- <51

Extractable Organic Compounds B/N/A, µg/L (Plant 1 Influent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

1,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

1,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 <0.41

1,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 <0.69

2,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 -- -- -- -- <0.75

2,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

2,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 <0.84

2,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

2,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 <0.71

2-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 <0.64

2-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 -- -- -- -- <0.7

2-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 -- -- -- -- <0.79

2-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

2-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

3,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

31

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

3-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.34,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.634-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.584-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.84-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.524-Methylphenol (Dist. Lab) 93.3 0.88 82.7 0.88 67.9 0.88 96.4 0.88 68.6 0.88 85.7 0.884-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.14-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Benzidine (Dist. Lab) ND 2.5 ND 2.5 -- -- -- -- -- -- -- --Benzoic Acid (Dist. Lab) 381 200 377 200 259 200 687 200 141 20 839 200Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Benzyl Alcohol (Dist. Lab) 26.3 1.7 33.3 1.7 19.9 1.7 49.9 1.7 21.3 1.7 22.8 1.7bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53bis(2-Ethylhexyl)Phthalate (Dist. Lab) 11.1 3.1 24.8 3.1 28.4 3.1 37.6 3.1 32.5 3.1 39.1 3.1Butyl Benzyl Phthalate (Dist. Lab) 1.95 0.47 3.83 0.47 4.01 0.47 3.23 0.47 4.12 0.47 3.29 0.47Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Diethyl Phthalate (Dist. Lab) 5.0 1.3 5.0 1.3 6.3 1.3 3.9 1.3 6.8 1.3 6.5 1.3Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54di-n-Butyl Phthalate (Dist. Lab) ND 0.75 1.09 0.75 2.03 0.75 1.96 0.75 1.81 0.75 1.58 0.75di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65

32

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

3-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 -- -- -- -- <1.3

4,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 <0.63

4-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

4-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 -- -- -- -- <1.8

4-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

4-Methylphenol (Dist. Lab) 67.3 0.88 22.8 0.88 69.9 0.88 77.8 0.88 -- -- -- -- 73

4-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 -- -- -- -- <4.1

4-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 <0.81

Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 <0.56

Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 -- -- -- -- <1.5

Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 -- -- -- -- <0.93

Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 -- -- -- -- <1.7

Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Benzidine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- <2.5

Benzoic Acid (Dist. Lab) 446 200 205 200 400 200 248 200 -- -- -- -- 400

Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 <0.45

Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 <0.44

Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Benzyl Alcohol (Dist. Lab) 16.9 1.7 17.6 1.7 29.9 1.7 23.3 1.7 -- -- -- -- 26

bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 <0.92

bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

bis(2-Ethylhexyl)Phthalate (Dist. Lab) 37.8 3.1 27.4 3.1 39.5 3.1 33.1 3.1 12.3 3.1 12.2 3.1 28

Butyl Benzyl Phthalate (Dist. Lab) 5.05 0.47 3.47 0.47 3.79 0.47 3.82 0.47 3.37 0.47 2.41 0.47 3.5

Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 -- -- -- -- <0.57

Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 -- -- -- -- <0.84

Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 -- -- -- -- <0.61

Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Diethyl Phthalate (Dist. Lab) 6.0 1.3 7.5 1.3 7.3 1.3 6.0 1.3 4.1 1.3 5.1 1.3 5.8

Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 <0.54

di-n-Butyl Phthalate (Dist. Lab) 2.34 0.75 2.19 0.75 2.27 0.75 1.85 0.75 1.32 0.75 2.46 0.75 1.7

di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 -- -- -- -- <0.72

Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 <0.57

Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 <0.33

Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 <1.1

Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 <0.77

Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 -- -- -- -- <0.68

Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 <0.59

n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 <2.7

N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 <0.65

33

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53Phenol (Dist. Lab) 28.8 0.99 35.4 0.99 29.2 0.99 36.1 0.99 34.7 0.99 41.2 0.99Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Total Non-Chlorinated Phenols (Dist. Lab) 28.8 -- 35.4 -- 29.2 -- 36.1 -- 34.7 -- 41.2 --

Extractable Organic Compounds B/N/A, µg/L (Plant 2 Influent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.481,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.521,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.692,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.752,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.762,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.842,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.622,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.712-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.642-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.72-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.792-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.812-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.63,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.493-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.34,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.634-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.584-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.84-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.524-Methylphenol (Dist. Lab) 41.1 0.88 39.2 0.88 27.8 0.88 33.3 0.88 22.9 0.88 28.0 0.884-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.14-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Benzidine (Dist. Lab) ND 2.5 ND 2.5 -- -- -- -- -- -- -- --Benzoic Acid (Dist. Lab) 193 20 187 20 131 20 136 20 93 20 690 200Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39

34

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 <0.85

n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 -- -- -- -- <0.42

PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 <0.83

Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 <0.53

Phenol (Dist. Lab) 33.9 0.99 33.5 0.99 34.7 0.99 36.6 0.99 11.2 0.99 16.5 0.99 31

Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 -- -- -- -- <1.2

Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 -- -- -- -- <0.64

Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Total Non-Chlorinated Phenols (Dist. Lab) 33.9 -- 33.5 -- 34.7 -- 36.6 -- 11.2 -- 16.5 -- 31

Extractable Organic Compounds B/N/A, µg/L (Plant 2 Influent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 0.61 0.48 <0.48

1,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

1,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 <0.41

1,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 <0.69

2,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 -- -- -- -- <0.75

2,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

2,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 <0.84

2,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

2,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 <0.71

2-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 <0.64

2-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 -- -- -- -- <0.7

2-Methylphenol (Dist. Lab) 1.15 0.79 ND 0.79 ND 0.79 1.66 0.79 -- -- -- -- <0.79

2-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

2-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

3,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

3-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 -- -- -- -- <1.3

4,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 <0.63

4-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

4-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 -- -- -- -- <1.8

4-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

4-Methylphenol (Dist. Lab) 42.4 0.88 44.8 0.88 68.7 0.88 27.1 0.88 -- -- -- -- 38

4-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 -- -- -- -- <4.1

4-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 <0.81

Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 <0.56

Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 -- -- -- -- <1.5

Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 -- -- -- -- <0.93

Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 -- -- -- -- <1.7

Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Benzidine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- <2.5

Benzoic Acid (Dist. Lab) 289 200 285 200 355 200 132 20 -- -- -- -- 250

Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 <0.45

Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 <0.44

Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

35

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Benzyl Alcohol (Dist. Lab) 12.5 1.7 18.0 1.7 10.8 1.7 22.0 1.7 10.3 1.7 10.0 1.7bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53bis(2-Ethylhexyl)Phthalate (Dist. Lab) 9.6 3.1 26.4 3.1 26.4 3.1 48.0 3.1 34.0 3.1 41.5 3.1Butyl Benzyl Phthalate (Dist. Lab) 1.91 0.47 1.48 0.47 1.78 0.47 1.78 0.47 2.43 0.47 2.21 0.47Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Diethyl Phthalate (Dist. Lab) 5.0 1.3 4.2 1.3 5.9 1.3 3.7 1.3 5.8 1.3 4.9 1.3Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54di-n-Butyl Phthalate (Dist. Lab) ND 0.75 ND 0.75 1.60 0.75 1.18 0.75 1.85 0.75 1.11 0.75di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53Phenol (Dist. Lab) 17.0 0.99 20.6 0.99 20.3 0.99 14.9 0.99 16.2 0.99 14.3 0.99Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Total Non-Chlorinated Phenols (Dist. Lab) 17.0 -- 20.6 -- 20.3 -- 14.9 -- 16.2 -- 14.3 --

Extractable Organic Compounds B/N/A, µg/L (Plant 2 Influent D Headworks)1,2,4-Trichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,2-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,3-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --1,4-Dichlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

36

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Benzyl Alcohol (Dist. Lab) 13.7 1.7 20.6 1.7 13.6 1.7 11.8 1.7 -- -- -- -- 14

bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 <0.92

bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

bis(2-Ethylhexyl)Phthalate (Dist. Lab) 35.9 3.1 29.8 3.1 43.6 3.1 39.5 3.1 9.5 3.1 11.5 3.1 30

Butyl Benzyl Phthalate (Dist. Lab) 3.79 0.47 3.72 0.47 2.38 0.47 3.26 0.47 1.88 0.47 2.20 0.47 2.4

Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 -- -- -- -- <0.57

Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 -- -- -- -- <0.84

Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 -- -- -- -- <0.61

Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Diethyl Phthalate (Dist. Lab) 5.6 1.3 6.2 1.3 7.1 1.3 5.7 1.3 4.5 1.3 4.5 1.3 5.3

Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 <0.54

di-n-Butyl Phthalate (Dist. Lab) 1.42 0.75 1.58 0.75 2.40 0.75 2.26 0.75 1.06 0.75 1.30 0.75 1.3

di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 -- -- -- -- <0.72

Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 <0.57

Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 <0.33

Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 <1.1

Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 <0.77

Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 -- -- -- -- <0.68

Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 0.73 0.59 <0.59

n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 0.87 0.62 <0.62

N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 <2.7

N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 <0.65

N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 <0.85

n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 -- -- -- -- <0.42

PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 <0.83

Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 <0.53

Phenol (Dist. Lab) 17.3 0.99 22.2 0.99 26.0 0.99 9.84 0.99 4.45 0.99 7.98 0.99 16

Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 -- -- -- -- <1.2

Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 -- -- -- -- <0.64

Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Total Non-Chlorinated Phenols (Dist. Lab) 17.3 -- 22.2 -- 26.0 -- 9.84 -- 4.45 -- 7.98 -- 16

Extractable Organic Compounds B/N/A, µg/L (Plant 2 Influent D Headworks)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

1,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

1,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 <0.41

1,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 <0.69

37

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

2,3-Dichloroaniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4,5-Trichlorophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4,6-Trichlorophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-Dichlorophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-Dimethylphenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-Dinitrophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-Dinitrotoluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,6-Dinitrotoluene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Chloronaphthalene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Chlorophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Methylnaphthalene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Methylphenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Nitroaniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --2-Nitrophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --3,3'-Dichlorobenzidine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --3-Nitroaniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4,6-Dinitro-o-Cresol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Bromophenyl-phenylether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Chloroaniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Chlorophenyl-phenylether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Methylphenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Nitroaniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Nitrophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acenaphthene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acenaphthylene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Acetochlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Alachlor (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Aniline (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Anthracene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Atrazine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Azobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzoic Acid (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzo(a)Anthracene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzo(a)Pyrene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzo(b)Fluoranthene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzo(g,h,i)Perylene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzo(k)Fluoranthene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Benzyl Alcohol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --bis(2-Chloroethoxy)Methane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --bis(2-Chloroethyl)Ether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --bis(2-Chloroisopropyl)Ether (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --bis(2-Ethylhexyl)Adipate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --bis(2-Ethylhexyl)Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Butyl Benzyl Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Captan (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Carbazole (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chloropropham (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Chrysene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --DCPA (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dibenzofuran (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dibenzo(a,h)Anthracene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dichlorobenzene Total (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Diethyl Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dimethyl Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --di-n-Butyl Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --di-n-Octyl Phthalate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Diphenamid (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --EPTC (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

38

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

2,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 -- -- -- -- <0.75

2,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

2,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 <0.84

2,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

2,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 <0.71

2-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 <0.64

2-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 -- -- -- -- <0.7

2-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 -- -- -- -- <0.79

2-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

2-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

3,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

3-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 -- -- -- -- <1.3

4,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 <0.63

4-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

4-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 -- -- -- -- <1.8

4-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

4-Methylphenol (Dist. Lab) ND 0.88 ND 0.88 2.70 0.88 3.05 0.88 -- -- -- -- 1.4

4-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 -- -- -- -- <4.1

4-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 <0.81

Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 <0.56

Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 -- -- -- -- <1.5

Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 -- -- -- -- <0.93

Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 -- -- -- -- <1.7

Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Benzoic Acid (Dist. Lab) ND 20 24 20 32 20 56 20 -- -- -- -- 28

Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 <0.45

Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 <0.44

Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Benzyl Alcohol (Dist. Lab) 5.1 1.7 8.5 1.7 16.2 1.7 11.0 1.7 -- -- -- -- 10

bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 <0.92

bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

bis(2-Ethylhexyl)Phthalate (Dist. Lab) 27.6 3.1 30.6 3.1 22.3 3.1 31.3 3.1 9.2 3.1 13.6 3.1 22

Butyl Benzyl Phthalate (Dist. Lab) 2.36 0.47 4.38 0.47 2.34 0.47 3.26 0.47 1.46 0.47 2.54 0.47 2.7

Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 -- -- -- -- <0.57

Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 -- -- -- -- <0.84

Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 -- -- -- -- <0.61

Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Diethyl Phthalate (Dist. Lab) 5.4 1.3 4.9 1.3 5.4 1.3 5.6 1.3 4.6 1.3 4.8 1.3 5.1

Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 <0.54

di-n-Butyl Phthalate (Dist. Lab) 1.92 0.75 1.61 0.75 2.42 0.75 2.05 0.75 0.91 0.75 1.52 0.75 1.7

di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 -- -- -- -- <0.72

39

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Fluoranthene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Fluorene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachlorobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachlorobutadiene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachlorocyclopentadiene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Hexachloroethane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Indeno(1,2,3-cd)Pyrene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Isophorone (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Molinate (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Naphthalene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --n-Decane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Nitrobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --N-Nitrosodimethylamine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --N-Nitrosodiphenylamine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --N-Nitroso-di-n-propylamine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --n-Octadecane (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --PAHs (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --p-Chloro-m-Cresol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Pentachloronitrobenzene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Pentachlorophenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Phenanthrene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Phenol (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Pyrene (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Simazine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Terbacil (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Terbufos (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Thiobencarb (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total Chlorinated Phenols (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --Total Non-Chlorinated Phenols (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Extractable Organic Compounds B/N/A, µg/L (Final Effluent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.481,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.521,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.411,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.692,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.752,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.762,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.862,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.842,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.622,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 12-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.712-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.642-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.7 ND 0.72-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.79 ND 0.792-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.812-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.63,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.493-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.34,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.634-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.584-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.8 ND 1.84-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.524-Methylphenol (Dist. Lab) 23.8 0.88 20.1 0.88 ND 0.88 11.6 0.88 11.3 0.88 ND 0.884-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.1 ND 4.1

40

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 <0.57

Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 <0.33

Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 <1.1

Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 <0.77

Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 -- -- -- -- <0.68

Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 <0.59

n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 <2.7

N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 <0.65

N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 <0.85

n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 -- -- -- -- <0.42

PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 <0.83

Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 <0.53

Phenol (Dist. Lab) 1.20 0.99 ND 0.99 3.72 0.99 ND 0.99 2.10 0.99 7.78 0.99 2.5

Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 -- -- -- -- <1.2

Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 -- -- -- -- <0.64

Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Total Non-Chlorinated Phenols (Dist. Lab) 1.20 -- ND -- 3.72 -- ND -- 2.10 -- 7.78 -- 2.5

Extractable Organic Compounds B/N/A, µg/L (Final Effluent)1,2,4-Trichlorobenzene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

1,2-Dichlorobenzene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

1,3-Dichlorobenzene (Dist. Lab) ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 ND 0.41 <0.41

1,4-Dichlorobenzene (Dist. Lab) ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 ND 0.69 <0.69

2,3-Dichloroaniline (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 -- -- -- -- <0.75

2,4,5-Trichlorophenol (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

2,4,6-Trichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dichlorophenol (Dist. Lab) ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 ND 0.86 <0.86

2,4-Dimethylphenol (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2,4-Dinitrophenol (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 <0.84

2,4-Dinitrotoluene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

2,6-Dinitrotoluene (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1 <1

2-Chloronaphthalene (Dist. Lab) ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 ND 0.71 <0.71

2-Chlorophenol (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 <0.64

2-Methylnaphthalene (Dist. Lab) ND 0.7 ND 0.7 ND 0.7 ND 0.7 -- -- -- -- <0.7

2-Methylphenol (Dist. Lab) ND 0.79 ND 0.79 ND 0.79 ND 0.79 -- -- -- -- <0.79

2-Nitroaniline (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

2-Nitrophenol (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

3,3'-Dichlorobenzidine (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

3-Nitroaniline (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 -- -- -- -- <1.3

4,6-Dinitro-o-Cresol (Dist. Lab) ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 ND 0.63 <0.63

4-Bromophenyl-phenylether (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

4-Chloroaniline (Dist. Lab) ND 1.8 ND 1.8 ND 1.8 ND 1.8 -- -- -- -- <1.8

4-Chlorophenyl-phenylether (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

4-Methylphenol (Dist. Lab) 1.32 0.88 ND 0.88 ND 0.88 ND 0.88 -- -- -- -- 6.8

4-Nitroaniline (Dist. Lab) ND 4.1 ND 4.1 ND 4.1 ND 4.1 -- -- -- -- <4.1

41

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

4-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5 ND 1.5Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93 ND 0.93Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7 ND 1.7Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Benzidine (Dist. Lab) ND 2.5 ND 2.5 -- -- -- -- -- -- -- --Benzoic Acid (Dist. Lab) 104 20 82 20 ND 20 69 20 59 20 53 20Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Benzyl Alcohol (Dist. Lab) ND 1.7 6.1 1.7 2.5 1.7 3.6 1.7 2.9 1.7 ND 1.7bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53bis(2-Ethylhexyl)Phthalate (Dist. Lab) ND 3.1 ND 3.1 ND 3.1 ND 3.1 ND 3.1 ND 3.1Butyl Benzyl Phthalate (Dist. Lab) 0.55 0.47 ND 0.47 ND 0.47 ND 0.47 ND 0.47 ND 0.47Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84 ND 0.84Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Diethyl Phthalate (Dist. Lab) 2.5 1.3 2.1 1.3 2.1 1.3 ND 1.3 2.8 1.3 ND 1.3Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54di-n-Butyl Phthalate (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76 ND 0.76EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72 ND 0.72Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68 ND 0.68Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 ND 1 ND 1Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53

42

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

4-Nitrophenol (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 <0.81

Acenaphthene (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Acenaphthylene (Dist. Lab) ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 ND 0.56 <0.56

Acetochlor (Dist. Lab) ND 1.5 ND 1.5 ND 1.5 ND 1.5 -- -- -- -- <1.5

Alachlor (Dist. Lab) ND 0.93 ND 0.93 ND 0.93 ND 0.93 -- -- -- -- <0.93

Aniline (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Anthracene (Dist. Lab) ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 ND 0.52 <0.52

Atrazine (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 -- -- -- -- <1.7

Azobenzene (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Benzidine (Dist. Lab) -- -- -- -- -- -- -- -- -- -- -- -- <2.5

Benzoic Acid (Dist. Lab) ND 20 ND 20 ND 20 ND 20 -- -- -- -- 37

Benzo(a)Anthracene (Dist. Lab) ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 ND 0.48 <0.48

Benzo(a)Pyrene (Dist. Lab) ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 ND 0.45 <0.45

Benzo(b)Fluoranthene (Dist. Lab) ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 ND 0.44 <0.44

Benzo(g,h,i)Perylene (Dist. Lab) ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 ND 0.39 <0.39

Benzo(k)Fluoranthene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Benzyl Alcohol (Dist. Lab) ND 1.7 ND 1.7 ND 1.7 ND 1.7 -- -- -- -- <1.7

bis(2-Chloroethoxy)Methane (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Chloroethyl)Ether (Dist. Lab) ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 ND 0.92 <0.92

bis(2-Chloroisopropyl)Ether (Dist. Lab) ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 ND 0.73 <0.73

bis(2-Ethylhexyl)Adipate (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

bis(2-Ethylhexyl)Phthalate (Dist. Lab) ND 3.1 ND 3.1 ND 3.1 ND 3.1 ND 3.1 ND 3.1 <3.1

Butyl Benzyl Phthalate (Dist. Lab) ND 0.47 ND 0.47 ND 0.47 ND 0.47 ND 0.47 ND 0.47 <0.47

Captan (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 -- -- -- -- <0.4

Carbazole (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 -- -- -- -- <0.57

Chloropropham (Dist. Lab) ND 0.84 ND 0.84 ND 0.84 ND 0.84 -- -- -- -- <0.84

Chrysene (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

DCPA (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 -- -- -- -- <0.61

Dibenzofuran (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 -- -- -- -- <0.59

Dibenzo(a,h)Anthracene (Dist. Lab) ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 ND 0.4 <0.4

Dichlorobenzene Total (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Diethyl Phthalate (Dist. Lab) ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.3 ND 1.3 <1.3

Dimethyl Phthalate (Dist. Lab) ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 ND 0.54 <0.54

di-n-Butyl Phthalate (Dist. Lab) ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 ND 0.75 <0.75

di-n-Octyl Phthalate (Dist. Lab) ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 ND 0.46 <0.46

Diphenamid (Dist. Lab) ND 0.76 ND 0.76 ND 0.76 ND 0.76 -- -- -- -- <0.76

EPTC (Dist. Lab) ND 0.72 ND 0.72 ND 0.72 ND 0.72 -- -- -- -- <0.72

Fluoranthene (Dist. Lab) ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 ND 0.49 <0.49

Fluorene (Dist. Lab) ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 ND 0.57 <0.57

Hexachlorobenzene (Dist. Lab) ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 ND 0.43 <0.43

Hexachlorobutadiene (Dist. Lab) ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 ND 0.33 <0.33

Hexachlorocyclopentadiene (Dist. Lab) ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 ND 1.1 <1.1

Hexachloroethane (Dist. Lab) ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 ND 0.6 <0.6

Indeno(1,2,3-cd)Pyrene (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 ND 0.42 <0.42

Isophorone (Dist. Lab) ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 ND 0.77 <0.77

Molinate (Dist. Lab) ND 0.68 ND 0.68 ND 0.68 ND 0.68 -- -- -- -- <0.68

Naphthalene (Dist. Lab) ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 ND 0.59 <0.59

n-Decane (Dist. Lab) ND 1 ND 1 ND 1 ND 1 -- -- -- -- <1

Nitrobenzene (Dist. Lab) ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 ND 0.62 <0.62

N-Nitrosodimethylamine (Dist. Lab) ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 ND 2.7 <2.7

N-Nitrosodiphenylamine (Dist. Lab) ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 ND 0.65 <0.65

N-Nitroso-di-n-propylamine (Dist. Lab) ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 ND 0.85 <0.85

n-Octadecane (Dist. Lab) ND 0.42 ND 0.42 ND 0.42 ND 0.42 -- -- -- -- <0.42

PAHs (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

p-Chloro-m-Cresol (Dist. Lab) ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 ND 0.83 <0.83

Pentachloronitrobenzene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 -- -- -- -- <0.53

Pentachlorophenol (Dist. Lab) ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 ND 0.61 <0.61

Phenanthrene (Dist. Lab) ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 ND 0.53 <0.53

43

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Phenol (Dist. Lab) 8.56 0.99 7.09 0.99 ND 0.99 4.63 0.99 4.63 0.99 ND 0.99Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3 ND 2.3Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2 ND 1.2Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64 ND 0.64Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81 ND 0.81Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND --Total Non-Chlorinated Phenols (Dist. Lab) 8.56 -- 7.09 -- ND -- 4.63 -- 4.63 -- ND --

Extractable Organic Compounds B/N/A, ug/kg dry weight (Plant 1 BP Cake)1,2,4-Trichlorobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --1,2-Dichlorobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --1,2-Diphenylhydrazine/Azobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --1,3-Dichlorobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --1,4-Dichlorobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,4,5-Trichlorophenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,4,6-Trichlorophenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,4-Dichlorophenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,4-Dimethylphenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,4-Dinitrophenol (Con. Lab) ND 95000 -- -- -- -- ND 69000 -- -- -- --2,4-Dinitrotoluene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2,6-Dinitrotoluene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Chloronaphthalene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Chlorophenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Methylnaphthalene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Methylphenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Nitroaniline (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --2-Nitrophenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --3,3'-Dichlorobenzidine (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --3-Nitroaniline (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4,6-Dinitro-2-methylphenol (Con. Lab) ND 60000 -- -- -- -- ND 43000 -- -- -- --4-Bromophenyl-phenylether (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4-Chloroaniline (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4-Chlorophenyl-phenylether (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4-Chloro-3-methylphenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4-Methylphenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --4-Nitroaniline (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --4-Nitrophenol (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --Acenaphthene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Acenaphthylene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Aniline (Con. Lab) ND 60000 -- -- -- -- ND 43000 -- -- -- --Anthracene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzidine (Con. Lab) ND 95000 -- -- -- -- ND 69000 -- -- -- --Benzoic Acid (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --Benzo(a)Anthracene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzo(a)Pyrene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzo(b)Fluoranthene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzo(g,h,i)Perylene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzo(k)Fluoranthene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Benzyl Alcohol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --bis(2-Chloroethoxy)Methane (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --bis(2-Chloroethyl)Ether (Con. Lab) ND 24000 -- -- -- -- ND 17000 -- -- -- --bis(2-Chloroisopropyl)Ether (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --bis(2-Ethylhexyl)Phthalate (Con. Lab) 57,000 48000 -- -- -- -- 74,000 35000 -- -- -- --Butyl Benzyl Phthalate (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Chrysene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Dibenzofuran (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Dibenzo(a,h)Anthracene (Con. Lab) ND 60000 -- -- -- -- ND 43000 -- -- -- --

44

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Phenol (Dist. Lab) ND 0.99 ND 0.99 ND 0.99 ND 0.99 ND 0.99 ND 0.99 2.1

Pyrene (Dist. Lab) ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 ND 0.58 <0.58

Simazine (Dist. Lab) ND 2.3 ND 2.3 ND 2.3 ND 2.3 -- -- -- -- <2.3

Terbacil (Dist. Lab) ND 1.2 ND 1.2 ND 1.2 ND 1.2 -- -- -- -- <1.2

Terbufos (Dist. Lab) ND 0.64 ND 0.64 ND 0.64 ND 0.64 -- -- -- -- <0.64

Thiobencarb (Dist. Lab) ND 0.81 ND 0.81 ND 0.81 ND 0.81 -- -- -- -- <0.81

Total Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- ND

Total Non-Chlorinated Phenols (Dist. Lab) ND -- ND -- ND -- ND -- ND -- ND -- 2.1

Extractable Organic Compounds B/N/A, ug/kg dry weight (Plant 1 BP Cake)1,2,4-Trichlorobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

1,2-Dichlorobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

1,2-Diphenylhydrazine/Azobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

1,3-Dichlorobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

1,4-Dichlorobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,4,5-Trichlorophenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,4,6-Trichlorophenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,4-Dichlorophenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,4-Dimethylphenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,4-Dinitrophenol (Con. Lab) ND 54000 -- -- -- -- ND 27000 -- -- -- -- <95,000

2,4-Dinitrotoluene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2,6-Dinitrotoluene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Chloronaphthalene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Chlorophenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Methylnaphthalene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Methylphenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Nitroaniline (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

2-Nitrophenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

3,3'-Dichlorobenzidine (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

3-Nitroaniline (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4,6-Dinitro-2-methylphenol (Con. Lab) ND 34000 -- -- -- -- ND 17000 -- -- -- -- <60,000

4-Bromophenyl-phenylether (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4-Chloroaniline (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4-Chlorophenyl-phenylether (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4-Chloro-3-methylphenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4-Methylphenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

4-Nitroaniline (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

4-Nitrophenol (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

Acenaphthene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Acenaphthylene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Aniline (Con. Lab) ND 34000 -- -- -- -- ND 17000 -- -- -- -- <60,000

Anthracene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzidine (Con. Lab) ND 54000 -- -- -- -- ND 27000 -- -- -- -- <95,000

Benzoic Acid (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

Benzo(a)Anthracene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzo(a)Pyrene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzo(b)Fluoranthene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzo(g,h,i)Perylene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzo(k)Fluoranthene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Benzyl Alcohol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

bis(2-Chloroethoxy)Methane (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

bis(2-Chloroethyl)Ether (Con. Lab) ND 14000 -- -- -- -- ND 6800 -- -- -- -- <24,000

bis(2-Chloroisopropyl)Ether (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

bis(2-Ethylhexyl)Phthalate (Con. Lab) 49,000 27000 -- -- -- -- 23,000 14000 -- -- -- -- 51,000

Butyl Benzyl Phthalate (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Chrysene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Dibenzofuran (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Dibenzo(a,h)Anthracene (Con. Lab) ND 34000 -- -- -- -- ND 17000 -- -- -- -- <60,000

45

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Diethyl Phthalate (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Dimethyl Phthalate (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --di-n-Butyl Phthalate (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --di-n-Octyl Phthalate (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Fluoranthene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Fluorene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Hexachlorobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Hexachlorobutadiene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Hexachlorocyclopentadiene (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --Hexachloroethane (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Indeno(1,2,3-cd)Pyrene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Isophorone (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Naphthalene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Nitrobenzene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --N-Nitrosodimethylamine (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --N-Nitrosodiphenylamine (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --N-Nitroso-di-n-propylamine (Con. Lab) ND 36000 -- -- -- -- ND 26000 -- -- -- --Pentachlorophenol (Con. Lab) ND 120000 -- -- -- -- ND 87000 -- -- -- --Phenanthrene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Phenol (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --Pyrene (Con. Lab) ND 48000 -- -- -- -- ND 35000 -- -- -- --

Extractable Organic Compounds B/N/A, ug/kg dry weight (Plant 2 BP Cake)1,2,4-Trichlorobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --1,2-Dichlorobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --1,2-Diphenylhydrazine/Azobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --1,3-Dichlorobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --1,4-Dichlorobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,4,5-Trichlorophenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,4,6-Trichlorophenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,4-Dichlorophenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,4-Dimethylphenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,4-Dinitrophenol (Con. Lab) ND 90000 -- -- -- -- ND 68000 -- -- -- --2,4-Dinitrotoluene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2,6-Dinitrotoluene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Chloronaphthalene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Chlorophenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Methylnaphthalene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Methylphenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Nitroaniline (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --2-Nitrophenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --3,3'-Dichlorobenzidine (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --3-Nitroaniline (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4,6-Dinitro-2-methylphenol (Con. Lab) ND 57000 -- -- -- -- ND 43000 -- -- -- --4-Bromophenyl-phenylether (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4-Chloroaniline (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4-Chlorophenyl-phenylether (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4-Chloro-3-methylphenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4-Methylphenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --4-Nitroaniline (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --4-Nitrophenol (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --Acenaphthene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Acenaphthylene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Aniline (Con. Lab) ND 57000 -- -- -- -- ND 43000 -- -- -- --Anthracene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Benzidine (Con. Lab) ND 90000 -- -- -- -- ND 68000 -- -- -- --Benzoic Acid (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --Benzo(a)Anthracene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --

46

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Diethyl Phthalate (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Dimethyl Phthalate (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

di-n-Butyl Phthalate (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

di-n-Octyl Phthalate (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Fluoranthene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Fluorene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Hexachlorobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Hexachlorobutadiene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Hexachlorocyclopentadiene (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

Hexachloroethane (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Indeno(1,2,3-cd)Pyrene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Isophorone (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Naphthalene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Nitrobenzene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

N-Nitrosodimethylamine (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

N-Nitrosodiphenylamine (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

N-Nitroso-di-n-propylamine (Con. Lab) ND 20000 -- -- -- -- ND 10000 -- -- -- -- <36,000

Pentachlorophenol (Con. Lab) ND 68000 -- -- -- -- ND 34000 -- -- -- -- <120,000

Phenanthrene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Phenol (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Pyrene (Con. Lab) ND 27000 -- -- -- -- ND 14000 -- -- -- -- <48,000

Extractable Organic Compounds B/N/A, ug/kg dry weight (Plant 2 BP Cake)1,2,4-Trichlorobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

1,2-Dichlorobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

1,2-Diphenylhydrazine/Azobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

1,3-Dichlorobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

1,4-Dichlorobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,4,5-Trichlorophenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,4,6-Trichlorophenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,4-Dichlorophenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,4-Dimethylphenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,4-Dinitrophenol (Con. Lab) ND 48000 -- -- -- -- ND 25000 -- -- -- -- <90,000

2,4-Dinitrotoluene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2,6-Dinitrotoluene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Chloronaphthalene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Chlorophenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Methylnaphthalene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Methylphenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Nitroaniline (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

2-Nitrophenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

3,3'-Dichlorobenzidine (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

3-Nitroaniline (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4,6-Dinitro-2-methylphenol (Con. Lab) ND 30000 -- -- -- -- ND 16000 -- -- -- -- <57,000

4-Bromophenyl-phenylether (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4-Chloroaniline (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4-Chlorophenyl-phenylether (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4-Chloro-3-methylphenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4-Methylphenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

4-Nitroaniline (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

4-Nitrophenol (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

Acenaphthene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Acenaphthylene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Aniline (Con. Lab) ND 30000 -- -- -- -- ND 16000 -- -- -- -- <57,000

Anthracene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Benzidine (Con. Lab) ND 48000 -- -- -- -- ND 25000 -- -- -- -- <90,000

Benzoic Acid (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

Benzo(a)Anthracene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

47

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Benzo(a)Pyrene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Benzo(b)Fluoranthene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Benzo(g,h,i)Perylene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Benzo(k)Fluoranthene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Benzyl Alcohol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --bis(2-Chloroethoxy)Methane (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --bis(2-Chloroethyl)Ether (Con. Lab) ND 23000 -- -- -- -- ND 17000 -- -- -- --bis(2-Chloroisopropyl)Ether (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --bis(2-Ethylhexyl)Phthalate (Con. Lab) 83,000 46000 -- -- -- -- 84,000 34000 -- -- -- --Butyl Benzyl Phthalate (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Chrysene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Dibenzofuran (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Dibenzo(a,h)Anthracene (Con. Lab) ND 57000 -- -- -- -- ND 43000 -- -- -- --Diethyl Phthalate (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Dimethyl Phthalate (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --di-n-Butyl Phthalate (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --di-n-Octyl Phthalate (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Fluoranthene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Fluorene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Hexachlorobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Hexachlorobutadiene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Hexachlorocyclopentadiene (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --Hexachloroethane (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Indeno(1,2,3-cd)Pyrene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Isophorone (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Naphthalene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Nitrobenzene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --N-Nitrosodimethylamine (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --N-Nitrosodiphenylamine (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --N-Nitroso-di-n-propylamine (Con. Lab) ND 34000 -- -- -- -- ND 26000 -- -- -- --Pentachlorophenol (Con. Lab) ND 110000 -- -- -- -- ND 85000 -- -- -- --Phenanthrene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Phenol (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --Pyrene (Con. Lab) ND 46000 -- -- -- -- ND 34000 -- -- -- --

Dioxins and Furans, pg/L (Final Effluent)2,3,7,8-TCDD (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- --Total TCDD (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- --1,2,3,7,8-PeCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total PeCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,4,7,8-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,6,7,8-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,7,8,9-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,4,6,7,8-HpCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total HpCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --OCDD (Con. Lab) ND 100 -- -- -- -- ND 100 -- -- -- --2,3,7,8-TCDF (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- --Total TCDF (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- --1,2,3,7,8-PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --2,3,4,7,8-PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,4,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,6,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --2,3,4,6,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,7,8,9-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --

48

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Benzo(a)Pyrene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Benzo(b)Fluoranthene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Benzo(g,h,i)Perylene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Benzo(k)Fluoranthene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Benzyl Alcohol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

bis(2-Chloroethoxy)Methane (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

bis(2-Chloroethyl)Ether (Con. Lab) ND 12000 -- -- -- -- ND 6300 -- -- -- -- <23,000

bis(2-Chloroisopropyl)Ether (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

bis(2-Ethylhexyl)Phthalate (Con. Lab) 39,000 24000 -- -- -- -- 38,000 13000 -- -- -- -- 61,000

Butyl Benzyl Phthalate (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Chrysene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Dibenzofuran (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Dibenzo(a,h)Anthracene (Con. Lab) ND 30000 -- -- -- -- ND 16000 -- -- -- -- <57,000

Diethyl Phthalate (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Dimethyl Phthalate (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

di-n-Butyl Phthalate (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

di-n-Octyl Phthalate (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Fluoranthene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Fluorene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Hexachlorobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Hexachlorobutadiene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Hexachlorocyclopentadiene (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

Hexachloroethane (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Indeno(1,2,3-cd)Pyrene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Isophorone (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Naphthalene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Nitrobenzene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

N-Nitrosodimethylamine (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

N-Nitrosodiphenylamine (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

N-Nitroso-di-n-propylamine (Con. Lab) ND 18000 -- -- -- -- ND 9400 -- -- -- -- <34,000

Pentachlorophenol (Con. Lab) ND 61000 -- -- -- -- ND 31000 -- -- -- -- <110,000

Phenanthrene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Phenol (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Pyrene (Con. Lab) ND 24000 -- -- -- -- ND 13000 -- -- -- -- <46,000

Dioxins and Furans, pg/L (Final Effluent)2,3,7,8-TCDD (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- -- <10

Total TCDD (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- -- <10

1,2,3,7,8-PeCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total PeCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,4,7,8-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,6,7,8-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,7,8,9-HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total HxCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,4,6,7,8-HpCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total HpCDD (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

OCDD (Con. Lab) ND 100 -- -- -- -- ND 100 -- -- -- -- <100

2,3,7,8-TCDF (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- -- <10

Total TCDF (Con. Lab) ND 10 -- -- -- -- ND 10 -- -- -- -- <10

1,2,3,7,8-PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

2,3,4,7,8-PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total PeCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,4,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,6,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

2,3,4,6,7,8-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,7,8,9-HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total HxCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

49

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

1,2,3,4,6,7,8-HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --1,2,3,4,7,8,9-HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --Total HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- --OCDF (Con. Lab) ND 100 -- -- -- -- ND 100 -- -- -- --Total TEQ (TEQ units) (Con. Lab) ND -- -- -- -- -- ND -- -- -- -- --

2,3,7,8-TCDD, ng/kg (dry weight) Plant 1 BP Cake (Con. Lab) 0.96 0.4 -- -- -- -- ND 0.38 -- -- -- -- Plant 2 BP Cake (Con. Lab) ND 0.58 -- -- -- -- ND 0.43 -- -- -- --

Ammonia ,mg/L Plant 1 Influent (Dist. Lab) 28.7 0.82 31.1 0.82 31.0 0.82 31.3 0.82 30.7 0.82 31.0 0.82 Plant 2 Influent (Dist. Lab) 29.6 0.82 30.5 0.82 31.2 0.82 30.8 0.82 33.2 0.82 30.4 0.82 Plant 2 Influent D Headworks 35.8 0.82 -- -- 32.8 0.82 -- -- -- -- 32.5 0.82 Final Effluent (Dist. Lab) 24.7 0.82 26.0 0.82 23.7 0.82 27.4 0.82 29.5 0.82 29.2 0.82

Ammonia Nitrogen (as N), mg/kg(dry weight) Plant 1 BP Cake (Con. Lab) 8,300 950 9,200 1200 8,800 1100 8,900 1000 6,600 1000 6,200 530 Plant 2 BP Cake (Con. Lab) 8,200 900 7,200 960 9,100 950 8,100 1000 7,700 1500 8,100 510

Cyanide, µg/L Plant 1 Influent (Dist. Lab) ND 2.44 ND 2.44 3.02 2.44 2.73 2.44 ND 2.44 2.72 2.44 Plant 2 Influent (Dist. Lab) ND 2.44 ND 2.44 ND 2.44 3.41 2.44 2.78 2.44 3.73 2.44 Plant 2 Influent D Headworks -- -- -- -- -- -- -- -- -- -- -- -- Final Effluent (Dist. Lab) 2.6 2.44 ND 2.44 2.49 2.44 4.1 2.44 2.87 2.44 3.01 2.44 Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 2.4 -- -- -- -- 3.5 2.6 -- -- -- -- Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 2.3 -- -- -- -- ND 2.5 -- -- -- --

Fluoride, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Hexavalent Chromium, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) ND 0.48 -- -- -- -- ND 0.52 -- -- -- -- Plant 2 BP Cake (Con. Lab) ND 0.46 -- -- -- -- ND 0.51 -- -- -- --

Nitrate Nitrogen (as N), mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) ND 5.3 ND 6.6 ND 5.9 ND 5.7 ND 5.8 ND 5.9 Plant 2 BP Cake (Con. Lab) 5.5 5.0 ND 5.3 ND 5.3 6.5 5.6 ND 8.1 ND 5.6

Total Kjeldahl Nitrogen, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) 43,000 4700 55,000 5700 63,000 5300 57,000 5300 55,000 5300 60,000 5300 Plant 2 BP Cake (Con. Lab) 42,000 4600 57,000 4700 42,000 4800 54,000 4800 74,000 7300 56,000 5100

Organic Nitrogen, mg/kg (dry weight) Plant 1 BP Cake (Calc.) 35,000 -- 46,000 -- 54,000 -- -- -- 48,000 -- 54,000 -- Plant 2 BP Cake (Calc.) 34,000 -- 50,000 -- 33,000 -- 46,000 -- 66,000 -- 48,000 --

Organic Lead, Units Plant 1 BP Cake (Con. Lab) ND 120 -- -- -- -- 490 130 -- -- -- -- Plant 2 BP Cake (Con. Lab) ND 110 -- -- -- -- ND 130 -- -- -- --

pH, Units Plant 1 BP Cake (Con. Lab) 8.2 0.100 -- -- -- -- 8.1 0.10 -- -- -- --

50

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

1,2,3,4,6,7,8-HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

1,2,3,4,7,8,9-HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

Total HpCDF (Con. Lab) ND 50 -- -- -- -- ND 51 -- -- -- -- <51

OCDF (Con. Lab) ND 100 -- -- -- -- ND 100 -- -- -- -- <100

Total TEQ (TEQ units) (Con. Lab) ND -- -- -- -- -- ND -- -- -- -- -- ND

2,3,7,8-TCDD, ng/kg (dry weight) Plant 1 BP Cake (Con. Lab) ND 2.8 -- -- -- -- ND 2.2 -- -- -- -- <2.8

Plant 2 BP Cake (Con. Lab) ND 2.4 -- -- -- -- ND 1.5 -- -- -- -- <2.4

Ammonia ,mg/L Plant 1 Influent (Dist. Lab) 29.3 0.82 29.5 0.82 30.2 0.82 30.0 0.82 32.5 0.82 33.6 0.82 31

Plant 2 Influent (Dist. Lab) 28.8 0.82 29.8 0.82 29.9 0.82 29.6 0.82 31.9 0.82 31.2 0.82 31

Plant 2 Influent D Headworks 28.5 0.82 29.6 0.82 31.2 0.82 31.5 0.82 32.8 0.82 32.4 0.82 32

Final Effluent (Dist. Lab) 23.4 0.82 23.8 0.82 26.1 0.82 27.0 0.82 26.0 0.82 29.6 0.82 26

Ammonia Nitrogen (as N), mg/kg(dry weight) Plant 1 BP Cake (Con. Lab) 6,900 540 15,000 540 6,600 560 8,900 540 6,200 420 4,700 470 8,000

Plant 2 BP Cake (Con. Lab) 6,600 500 14,000 510 6,800 500 10,000 500 7,300 420 6,600 500 8,300

Cyanide, µg/L Plant 1 Influent (Dist. Lab) 2.94 2.44 ND 2.44 ND 2.44 ND 2.44 ND 2.44 ND 2.44 <2.44

Plant 2 Influent (Dist. Lab) ND 2.44 ND 2.44 ND 2.44 ND 2.44 ND 2.44 ND 2.44 <2.44

Plant 2 Influent D Headworks 3.38 2.44 ND 2.44 ND 2.44 3.4 2.44 ND 2.44 ND 2.44 <2.44

Final Effluent (Dist. Lab) ND 2.44 7.8 2.44 ND 2.44 2.98 2.44 3.69 2.44 2.68 2.44 2.7

Plant 1 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 2.7 -- -- -- -- ND 2.7 -- -- -- -- <2.7

Plant 2 BP Cake, mg/kg (dry wt.) (Con. Lab) ND 2.5 -- -- -- -- ND 2.5 -- -- -- -- <2.5

Fluoride, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Hexavalent Chromium, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) ND 0.54 -- -- -- -- ND 11 -- -- -- -- <11

Plant 2 BP Cake (Con. Lab) ND 0.50 -- -- -- -- ND 10 -- -- -- -- <10

Nitrate Nitrogen (as N), mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) ND 6.0 ND 3.2 ND 3.4 ND 5.9 ND 5.8 ND 5.2 <6.6

Plant 2 BP Cake (Con. Lab) ND 5.5 ND 3.2 ND 3 ND 5.5 5.9 5.8 ND 5.5 <8.1

Total Kjeldahl Nitrogen, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) 58,000 5400 55,000 1600 54,000 1900 49,000 6700 54,000 5100 48,000 4700 54,000

Plant 2 BP Cake (Con. Lab) 53,000 5000 59,000 1600 47,000 1800 54,000 6200 55,000 5300 55,000 5100 54,000

Organic Nitrogen, mg/kg (dry weight) Plant 1 BP Cake (Calc.) 51,000 -- 40,000 -- 47,000 -- 40,000 -- 48,000 -- 43,000 -- 46,000

Plant 2 BP Cake (Calc.) 46,000 -- 45,000 -- 40,000 -- 44,000 -- 48,000 -- 48,000 -- 46,000

Organic Lead, Units Plant 1 BP Cake (Con. Lab) ND 140 -- -- -- -- ND 140 -- -- -- -- <140

Plant 2 BP Cake (Con. Lab) ND 130 -- -- -- -- ND 130 -- -- -- -- <130

pH, Units Plant 1 BP Cake (Con. Lab) 8.0 0.10 -- -- -- -- 8.0 0.10 -- -- -- -- 8.1

51

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant 2 BP Cake (Con. Lab) 8.2 0.100 -- -- -- -- 8.2 0.10 -- -- -- --

Hydrozable Phosphorus, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Orthophosphate, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Total Phosphorus (as P), mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Radioactivity, pCi/L (Gross Alpha + Gross Beta) Plant 1 Influent (Con. Lab) 11.87 4.29 10.36 3.52 7.14 4.45 6.05 2.89 30.83 4.45 16.04 5.20 Plant 2 Influent (Con. Lab) 16.61 4.48 15.34 4.26 9.99 4.62 26.1 4.9 11.76 4.21 14.58 6.17 Plant 2 Influent D Headworks -- -- -- -- -- -- -- -- -- -- -- -- Final Effluent (Con. Lab) 34 5.07 22.52 4.97 30.9 6.35 16.31 4.34 12.01 6.12 16.119 6.48

Total Solids, % Plant 1 BP Cake (Con. Lab) 19 0.10 17 0.10 18 0.10 18 0.10 19 0.10 18 0.10 Plant 2 BP Cake (Con. Lab) 22 0.10 20 0.10 21 0.10 20 0.10 18 0.10 20 0.10

Elements (California Waste Extract Samples)Antimony Plant 1 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- --

Arsenic Plant 1 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- --

Barium Plant 1 BP Cake, mg/L (Con. Lab) 7.0 2.0 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) 14 2.0 -- -- -- -- -- -- -- -- -- --

Beryllium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.040 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.040 -- -- -- -- -- -- -- -- -- --

Cadmium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- --

Chromium, Total Plant 1 BP Cake, mg/L (Con. Lab) 0.54 0.20 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) 0.87 0.20 -- -- -- -- -- -- -- -- -- --

Cobalt Plant 1 BP Cake, mg/L (Con. Lab) ND 1.6 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 1.6 -- -- -- -- -- -- -- -- -- --

Copper Plant 1 BP Cake, mg/L (Con. Lab) ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.2 -- -- -- -- -- -- -- -- -- --Lead

52

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant 2 BP Cake (Con. Lab) 8.1 0.10 -- -- -- -- 8.2 0.10 -- -- -- -- 8.2

Hydrozable Phosphorus, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Orthophosphate, mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Total Phosphorus (as P), mg/kg (dry weight) Plant 1 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Radioactivity, pCi/L (Gross Alpha + Gross Beta) Plant 1 Influent (Con. Lab) 9.11 3.19 12.35 2.52 7.614 3.90 12.18 2.69 11.05 2.68 26.25 2.56 13

Plant 2 Influent (Con. Lab) 23.82 4.83 11.89 4.93 13.23 5.81 -- -- 13.54 6.13 16.68 3.06 16

Plant 2 Influent D Headworks 24.06 4.49 23.37 3.85 14.58 3.33 16.03 3.92 19.07 4.43 22.8 4.66 20

Final Effluent (Con. Lab) 22.2 4.79 14.45 3.06 17.57 3.40 22.63 5.95 27.5 2.51 28 3.73 22

Total Solids, % Plant 1 BP Cake (Con. Lab) 18 0.10 18 0.1 18 0.1 18 0.10 20 0.10 19 0.10 18

Plant 2 BP Cake (Con. Lab) 19 0.10 20 0.1 20 0.1 20 0.10 20 0.10 19 0.10 20

Elements (California Waste Extract Samples)Antimony Plant 1 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Arsenic Plant 1 BP Cake, mg/L (Con. Lab) 0.23 0.20 -- -- -- -- -- -- -- -- -- -- <0.40

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.40

Barium Plant 1 BP Cake, mg/L (Con. Lab) 7.0 1.0 -- -- -- -- -- -- -- -- -- -- 7.0

Plant 2 BP Cake, mg/L (Con. Lab) 16 1.0 -- -- -- -- -- -- -- -- -- -- 15

Beryllium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.040

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.040

Cadmium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.10

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.10

Chromium, Total Plant 1 BP Cake, mg/L (Con. Lab) 0.63 0.10 -- -- -- -- -- -- -- -- -- -- 0.59

Plant 2 BP Cake, mg/L (Con. Lab) 0.84 0.10 -- -- -- -- -- -- -- -- -- -- 0.86

Cobalt Plant 1 BP Cake, mg/L (Con. Lab) ND 0.80 -- -- -- -- -- -- -- -- -- -- <1.6

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.80 -- -- -- -- -- -- -- -- -- -- <1.6

Copper Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.2

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.2

Lead

53

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant 1 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- --

Mercury Plant 1 BP Cake, mg/L (Con. Lab) ND 0.002 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.002 -- -- -- -- -- -- -- -- -- --

Molybdenum Plant 1 BP Cake, mg/L (Con. Lab) ND 0.80 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.80 -- -- -- -- -- -- -- -- -- --

Nickel Plant 1 BP Cake, mg/L (Con. Lab) ND 0.4 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) 0.40 0.40 -- -- -- -- -- -- -- -- -- --

Selenium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.4 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.4 -- -- -- -- -- -- -- -- -- --

Silver Plant 1 BP Cake, mg/L (Con. Lab) ND 0.4 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.4 -- -- -- -- -- -- -- -- -- --

Thallium Plant 1 BP Cake, mg/L (Con. Lab) ND 1 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 1 -- -- -- -- -- -- -- -- -- --

Vanadium Plant 1 BP Cake, mg/L (Con. Lab) ND 1.0 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 1.0 -- -- -- -- -- -- -- -- -- --

Zinc Plant 1 BP Cake, mg/L (Con. Lab) ND 4 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 4 -- -- -- -- -- -- -- -- -- --

Elements (TCLP Extract Samples)Arsenic Plant 1 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- --

Barium Plant 1 BP Cake, mg/L (Con. Lab) ND 1 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 1.0 -- -- -- -- -- -- -- -- -- --

Cadmium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.05 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.050 -- -- -- -- -- -- -- -- -- --

Chromium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.1 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- --

Lead Plant 1 BP Cake, mg/L (Con. Lab) ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- --

Mercury Plant 1 BP Cake, mg/L (Con. Lab) ND 0.002 -- -- -- -- -- -- -- -- -- --

54

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant 1 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.40

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.40

Mercury Plant 1 BP Cake, mg/L (Con. Lab) ND 0.0020 -- -- -- -- -- -- -- -- -- -- <0.002

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.0020 -- -- -- -- -- -- -- -- -- -- <0.002

Molybdenum Plant 1 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- -- <0.80

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.40 -- -- -- -- -- -- -- -- -- -- <0.80

Nickel Plant 1 BP Cake, mg/L (Con. Lab) 0.39 0.20 -- -- -- -- -- -- -- -- -- -- <0.4

Plant 2 BP Cake, mg/L (Con. Lab) 0.44 0.20 -- -- -- -- -- -- -- -- -- -- 0.42

Selenium Plant 1 BP Cake, mg/L (Con. Lab) 0.30 0.20 -- -- -- -- -- -- -- -- -- -- <0.4

Plant 2 BP Cake, mg/L (Con. Lab) 0.29 0.20 -- -- -- -- -- -- -- -- -- -- <0.4

Silver Plant 1 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.4

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.4

Thallium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- <1

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- <1

Vanadium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.50 -- -- -- -- -- -- -- -- -- -- <1.0

Plant 2 BP Cake, mg/L (Con. Lab) 0.68 0.50 -- -- -- -- -- -- -- -- -- -- <1.0

Zinc Plant 1 BP Cake, mg/L (Con. Lab) 3.9 2.0 -- -- -- -- -- -- -- -- -- -- <4

Plant 2 BP Cake, mg/L (Con. Lab) 2.5 2.0 -- -- -- -- -- -- -- -- -- -- <4

Elements (TCLP Extract Samples)Arsenic Plant 1 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Barium Plant 1 BP Cake, mg/L (Con. Lab) ND 1.0 -- -- -- -- -- -- -- -- -- -- <1

Plant 2 BP Cake, mg/L (Con. Lab) ND 1.0 -- -- -- -- -- -- -- -- -- -- <1.0

Cadmium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.05

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.05 -- -- -- -- -- -- -- -- -- -- <0.050

Chromium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Lead Plant 1 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Mercury Plant 1 BP Cake, mg/L (Con. Lab) ND 0.0020 -- -- -- -- -- -- -- -- -- -- <0.002

55

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.0020 -- -- -- -- -- -- -- -- -- --

Selenium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- --

Silver Plant 1 BP Cake, mg/L (Con. Lab) ND 0.1 -- -- -- -- -- -- -- -- -- -- Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- --

1,2,4-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,2-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,3-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,4-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2,4,5-Trichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

2,4,6-Trichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

2,4-Dichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2,4-Dimethylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

2,4-Dinitrophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- --

2,4-Dinitrotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2,6-Dinitrotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2-Chloronaphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

56

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.0020 -- -- -- -- -- -- -- -- -- -- <0.0020

Selenium Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Silver Plant 1 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

Plant 2 BP Cake, mg/L (Con. Lab) ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

1,2,4-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,2-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,3-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,4-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2,4,5-Trichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

2,4,6-Trichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

2,4-Dichlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2,4-Dimethylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

2,4-Dinitrophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

2,4-Dinitrotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2,6-Dinitrotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2-Chloronaphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

57

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

2-Chlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2-Methylnaphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2-Methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

2-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

2-Nitrophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

3,3-Dichlorobenzidine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- --

3-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

4,6-Dinitro-2-methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- --

4-Bromophenyl phenyl ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

4-Chloro-3-methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

4-Chloroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

4-Chlorophenyl phenyl ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

4-Methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

4-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- --

4-Nitrophenol (TCLP Extract)

58

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

2-Chlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2-Methylnaphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2-Methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

2-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

2-Nitrophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

3,3-Dichlorobenzidine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

3-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

4,6-Dinitro-2-methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

4-Bromophenyl phenyl ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

4-Chloro-3-methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

4-Chloroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

4-Chlorophenyl phenyl ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

4-Methylphenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

4-Nitroaniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

4-Nitrophenol (TCLP Extract)

59

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant1 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- --

Acenaphthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Acenaphthylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Aniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Azobenzene/1,2-Diphenylhydrazine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Benz(a)anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzidine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- --

Benzo(a)pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzo(b)fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzo(g,h,i)perylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzo(k)fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzoic acid (TCLP Extract) Plant1 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.5 -- -- -- -- -- -- -- -- -- --

Benzyl alcohol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Bis(2-chloroethoxy)methane (TCLP Extract)

60

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Acenaphthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Acenaphthylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Aniline (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Azobenzene/1,2-Diphenylhydrazine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Benz(a)anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Benzidine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Benzo(a)pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Benzo(b)fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Benzo(g,h,i)perylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Benzo(k)fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Benzoic acid (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.5

Benzyl alcohol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Bis(2-chloroethoxy)methane (TCLP Extract)

61

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Bis(2-chloroethyl)ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Bis(2-chloroisopropyl)ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Bis(2-ethylhexyl)phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.25 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.25 -- -- -- -- -- -- -- -- -- --

Butyl benzyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Chrysene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Di-n-butyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Di-n-octyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- --

Dibenz(a,h)anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.1 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.1 -- -- -- -- -- -- -- -- -- --

Dibenzofuran (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Diethyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Dimethyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Fluorene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Hexachlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

62

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Bis(2-chloroethyl)ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Bis(2-chloroisopropyl)ether (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Bis(2-ethylhexyl)phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.25 -- -- -- -- -- -- -- -- -- -- <0.25

Plant2 BP Cake, mg/L ND 0.25 -- -- -- -- -- -- -- -- -- -- <0.25

Butyl benzyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Chrysene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Di-n-butyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Di-n-octyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Dibenz(a,h)anthracene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

Dibenzofuran (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Diethyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Dimethyl phthalate (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Fluoranthene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Fluorene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Hexachlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

63

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Hexachlorobutadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Hexachlorocyclopentadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- --

Hexachloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Indeno(1,2,3-cd)pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Isophorone (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

N-Nitroso-di-n-propylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.1 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.1 -- -- -- -- -- -- -- -- -- --

N-Nitrosodimethylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

N-Nitrosodiphenylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Naphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Nitrobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- --

Pentachlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.2 -- -- -- -- -- -- -- -- -- --

Phenanthrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Phenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,1,1,2-Tetrachloroethane (TCLP Extract)

64

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Hexachlorobutadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Hexachlorocyclopentadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Hexachloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Indeno(1,2,3-cd)pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Isophorone (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

N-Nitroso-di-n-propylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.1

N-Nitrosodimethylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

N-Nitrosodiphenylamine (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Naphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Nitrobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Pentachlorophenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.2

Phenanthrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Phenol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Pyrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,1,1,2-Tetrachloroethane (TCLP Extract)

65

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,1,1-Trichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,1,2,2-Tetrachloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,1,2-Trichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,1-Dichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,1-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,1-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,2,3-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,2,3-Trichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

1,2,4-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,2,4-Trimethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,2-Dibromo-3-chloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

1,2-Dibromoethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,2-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,2-Dichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

66

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,1,1-Trichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,1,2,2-Tetrachloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,1,2-Trichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,1-Dichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,1-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,1-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,2,3-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,2,3-Trichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

1,2,4-Trichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

1,2,4-Trimethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,2-Dibromo-3-chloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.050

1,2-Dibromoethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,2-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,2-Dichloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

67

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,2-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,3,5-Trimethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- --

1,3-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,3-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

1,4-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

2,2-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

2-Chlorotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

4-Chlorotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Acetone (TCLP Extract) Plant1 BP Cake, mg/L ND -- -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L 0.44 0.10 -- -- -- -- -- -- -- -- -- --

Acrolein (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Acrylonitrile (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Benzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Bromobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Bromochloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

68

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,2-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,3,5-Trimethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

1,3-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,3-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

1,4-Dichlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

2,2-Dichloropropane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

2-Chlorotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.050

4-Chlorotoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.050

Acetone (TCLP Extract) Plant1 BP Cake, mg/L 0.23 0.10 -- -- -- -- -- -- -- -- -- -- 0.12

Plant2 BP Cake, mg/L 0.26 0.10 -- -- -- -- -- -- -- -- -- -- 0.35

Acrolein (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Acrylonitrile (TCLP Extract) Plant1 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Plant2 BP Cake, mg/L ND 0.50 -- -- -- -- -- -- -- -- -- -- <0.50

Benzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Bromobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Bromochloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

69

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Bromodichloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Bromoform (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Bromomethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Carbon tetrachloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Chlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Chloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Chloroform (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Chloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Dibromochloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Dibromomethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Dichlorodifluoromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Ethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Hexachlorobutadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Isobutyl alcohol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- --

70

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Bromodichloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Bromoform (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Bromomethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Carbon tetrachloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Chlorobenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Chloroethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Chloroform (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Chloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.050

Dibromochloromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Dibromomethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Dichlorodifluoromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Ethylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Hexachlorobutadiene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Isobutyl alcohol (TCLP Extract) Plant1 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

Plant2 BP Cake, mg/L ND 0.20 -- -- -- -- -- -- -- -- -- -- <0.20

71

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Isopropylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

MIBK (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- --

Methyl ethyl ketone (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L 0.15 0.10 -- -- -- -- -- -- -- -- -- --

Methylene Chloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Naphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

Styrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Tetrachloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Toluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Trichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- --

Trichlorofluoromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.05 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.05 -- -- -- -- -- -- -- -- -- --

Vinyl chloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.05 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.05 -- -- -- -- -- -- -- -- -- --

cis-1,2-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

cis-1,3-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

m,p-Xylenes (TCLP Extract) Plant1 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- --

n-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

72

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Isopropylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

MIBK (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Methyl ethyl ketone (TCLP Extract) Plant1 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Plant2 BP Cake, mg/L ND 0.10 -- -- -- -- -- -- -- -- -- -- <0.10

Methylene Chloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Naphthalene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Styrene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Tetrachloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Toluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Trichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

Trichlorofluoromethane (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.05

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.05

Vinyl chloride (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.05

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.05

cis-1,2-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

cis-1,3-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

m,p-Xylenes (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

n-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

73

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

n-Propylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

o-Xylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.02 -- -- -- -- -- -- -- -- -- --

p-Isopropyltoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

sec-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

tert-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- --

trans-1,2-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

trans-1,3-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- --

Herbicides µg/L (Plant 1 BP Cake) (TCLP Extraction)2,4,5-T (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-D (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- --2,4-DB (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dalapon (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dicamba (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dichlorprop (2,4-DP) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dinoseb (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --MCPA (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --MCPP (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Pentachlorophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Nitrophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Silvex (2,4,5-TP) (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- --Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Herbicides µg/kg (Plant 2 BP Cake) (TCLP Extraction)2,4,5-T (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --2,4-D (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- --2,4-DB (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dalapon (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dicamba (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Dichlorprop (2,4-DP) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

74

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

n-Propylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

o-Xylene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.02

p-Isopropyltoluene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

sec-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

tert-Butylbenzene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

Plant2 BP Cake, mg/L ND 0.050 -- -- -- -- -- -- -- -- -- -- <0.050

trans-1,2-Dichloroethene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

trans-1,3-Dichloropropene (TCLP Extract) Plant1 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Plant2 BP Cake, mg/L ND 0.020 -- -- -- -- -- -- -- -- -- -- <0.020

Herbicides µg/L (Plant 1 BP Cake) (TCLP Extraction)2,4,5-T (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

2,4-D (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- -- <0.100

2,4-DB (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dalapon (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dicamba (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dichlorprop (2,4-DP) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dinoseb (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

MCPA (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

MCPP (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Pentachlorophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

4-Nitrophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Silvex (2,4,5-TP) (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- -- <0.100

Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Herbicides µg/L (Plant 2 BP Cake) (TCLP Extraction)2,4,5-T (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

2,4-D (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- -- <0.100

2,4-DB (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dalapon (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dicamba (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Dichlorprop (2,4-DP) (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

75

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Dinoseb (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --MCPA (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --MCPP (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Pentachlorophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --4-Nitrophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --Silvex (2,4,5-TP) (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- --Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- --

Organochlorine Pesticides and PCB's, µg/L (Plant 1 BP Cake) (TCLP Extraction)Aldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Alpha-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Beta-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Delta-BHC (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Gamma-BHC (Lindane) (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Chlordane (Con. Lab) ND 0.0050 -- -- -- -- -- -- -- -- -- --4,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --4-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --4-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Dieldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan I (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan II (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan sulfate (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Endrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endrin Aldehyde (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endrin Ketone (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Heptachlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Heptachlor epoxide (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Methoxychlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Mirex (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Toxaphene (Con. Lab) ND 0.025 -- -- -- -- -- -- -- -- -- --

Organochlorine Pesticides and PCB's, µg/L (Plant 2 BP Cake) (TCLP Extraction)Aldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Alpha-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Beta-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Delta-BHC (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Gamma-BHC (Lindane) (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Chlordane (Con. Lab) ND 0.0050 -- -- -- -- -- -- -- -- -- --4,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --4-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --4-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --2-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Dieldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan I (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan II (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endosulfan sulfate (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Endrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endrin Aldehyde (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Endrin Ketone (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Heptachlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --

76

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Dinoseb (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

MCPA (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

MCPP (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Pentachlorophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

4-Nitrophenol (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Silvex (2,4,5-TP) (Con. Lab) ND 0.100 -- -- -- -- -- -- -- -- -- -- <0.100

Picloram (Con. Lab) -- -- -- -- -- -- -- -- -- -- -- -- --

Organochlorine Pesticides and PCB's, µg/L (Plant 1 BP Cake) (TCLP Extraction)Aldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Alpha-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Beta-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Delta-BHC (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Gamma-BHC (Lindane) (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Chlordane (Con. Lab) ND 0.0050 -- -- -- -- -- -- -- -- -- -- <0.0050

4,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

4-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

4-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Dieldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan I (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan II (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan sulfate (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Endrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endrin Aldehyde (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endrin Ketone (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Heptachlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Heptachlor epoxide (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Methoxychlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Mirex (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Toxaphene (Con. Lab) ND 0.025 -- -- -- -- -- -- -- -- -- -- <0.025

Organochlorine Pesticides and PCB's, µg/L (Plant 2 BP Cake) (TCLP Extraction)Aldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Alpha-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Beta-BHC (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Delta-BHC (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Gamma-BHC (Lindane) (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Chlordane (Con. Lab) ND 0.0050 -- -- -- -- -- -- -- -- -- -- <0.0050

4,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

4-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

4-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2,4'-DDD (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2-4'-DDE (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

2-4'-DDT (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Dieldrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan I (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan II (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endosulfan sulfate (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Endrin (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endrin Aldehyde (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Endrin Ketone (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Heptachlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

77

Jun-11Jan-11 Feb-11 Mar-11 Apr-11 May-11

Heptachlor epoxide (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Methoxychlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- --Mirex (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- --Toxaphene (Con. Lab) ND 0.025 -- -- -- -- -- -- -- -- -- --

78

Annual

Mean

Jul-11 Aug-11 Sep-11 Oct-11 Nov-11 Dec-11

Heptachlor epoxide (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Methoxychlor (Con. Lab) ND 0.00050 -- -- -- -- -- -- -- -- -- -- <0.00050

Mirex (Con. Lab) ND 0.0010 -- -- -- -- -- -- -- -- -- -- <0.0010

Toxaphene (Con. Lab) ND 0.025 -- -- -- -- -- -- -- -- -- -- <0.025

APPENDIX D

Arizona Biosolids Annual Report Form for Reporting Year 2011 Paint Filter Test Results

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

LABORATORY REPORT

Prepared For: Orange County Sanitation District

10844 Ellis Avenue

Fountain Valley, CA 92728-8127

Attention: Yu-Li Tsay Sampled:

Received:

Issued:

01/05/11

01/06/11

01/31/11 12:05

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain(s) of Custody, 8 pages, are

included and are an integral part of this report.

This entire report was reviewed and approved for release.

Project: Quarterly Biosolids

PO# 103620-OA

NELAP #01108CA California ELAP#2706 CSDLAC #10256 AZ #AZ0671 NV #CA01531

SAMPLE CROSS REFERENCE

SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report.

MATRIXCLIENT IDLABORATORY ID

IUA0632-01 1337800 P1 CAKE Solid

IUA0632-02 1337805 P2 CAKE Solid

IUA0632-03 1349404 P1 37 RAW SLUDE Solid

IUA0632-04 1349406 P1 TH SL Solid

IUA0632-05 1349408 P2 BASIN SBF Solid

IUA0632-06 1349410 P2 TH SL Solid

IUA0632-07 1349412 P2 FEED Solid

IUA0632-08 1349414 P1 FEED Solid

Reviewed By:

Project Manager

TestAmerica Irvine

IUA0632

Sushmitha Reddy

<Page 1 of 101>

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Orange County Sanitation District

10844 Ellis Avenue

Fountain Valley, CA 92728-8127

Attention: Yu-Li Tsay

Sampled:

Received:

01/05/11

01/06/11Report Number:

Project ID:

IUA0632

Quarterly Biosolids

PO# 103620-OA

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IUA0632-02 (1337805 P2 CAKE - Solid) Sampled: 01/05/11Reporting Units: mg/kg dry

Total Kjeldahl Nitrogen EPA 351.2 11A1091 420004600 01/11/11 01/11/11200N/A

Ammonia-N SM4500NH3 D 11A1436 8200900 01/13/11 01/13/11198N/A

EPA 7196AChromium VI 11A1428 0.46 ND MC601/13/11 01/14/111N/A

EPA 9014Total Cyanide 11A0743 2.3 ND 01/07/11 01/07/111N/A

Nitrate-N EPA 300.0 11A0894 5.55.0 01/10/11 01/10/110.998N/A

Sample ID: IUA0632-01 (1337800 P1 CAKE - Solid) Sampled: 01/05/11Reporting Units: mV

Redox Potential (Eh) SM 2580B 11A0757 3100.10 01/07/11 01/07/111N/A

Sample ID: IUA0632-02 (1337805 P2 CAKE - Solid) Sampled: 01/05/11Reporting Units: mV

Redox Potential (Eh) SM 2580B 11A0757 2200.10 01/07/11 01/07/111N/A

Sample ID: IUA0632-01 (1337800 P1 CAKE - Solid) Sampled: 01/05/11Reporting Units: N/A

EPA 9095AFree Liquid 11A1466 NA Not Present 01/13/11 01/13/111N/A

Sample ID: IUA0632-02 (1337805 P2 CAKE - Solid) Sampled: 01/05/11Reporting Units: N/A

EPA 9095AFree Liquid 11A1466 NA Not Present 01/13/11 01/13/111N/A

Sample ID: IUA0632-01 (1337800 P1 CAKE - Solid) Sampled: 01/05/11Reporting Units: pH Units

pH EPA 9045C 11A0756 8.250.100 01/07/11 01/07/111N/A

Sample ID: IUA0632-02 (1337805 P2 CAKE - Solid) Sampled: 01/05/11Reporting Units: pH Units

pH EPA 9045C 11A0756 8.240.100 01/07/11 01/07/111N/A

Project Manager

TestAmerica Irvine

IUA0632

Sushmitha Reddy

The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 19 of 101>

ORANGE COUNTY SANITATION DISTRICTEnvironmental Compliance Division

10844 Ellis AvenueFountain Valley, California 92708-7018

714.962.2411

www.ocsd.com

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