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Luminescence dating of fluvial deposits: applications to geomorphic, palaeoseismic and archaeological research TAMMY M. RITTENOUR BOREAS Rittenour, T. M. 2008 (November): Luminescence dating of fluvial deposits: applications to geomorphic, palaeo- seismic and archaeological research. Boreas, Vol. 37, pp. 613–635. 10.1111/j.1502-3885.2008.00056.x. ISSN 0300-9483. Fluvial deposits and landforms are important archives of river response to climate, tectonics and base level change and are commonly associated with archaeological sites. Unlike radiocarbon dating, the target material for opti- cally stimulated luminescence (OSL) dating (sands and silts) is nearly ubiquitous in fluvial deposits and the age range for OSL spans the last glacial–interglacial cycle, a time period of interest to many Quaternary scientists. Recent advances in OSL techniques and the development of single-grain dating capabilities have now allowed fluvial deposits, and other deposits commonly afflicted with incomplete zeroing of the luminescence signal, to be dated. The application of OSL dating to fluvial deposits is discussed with respect to its potential to provide im- portant contributions to research in the fields of geomorphology, palaeoseismology and archaeology. Examples are given from each research field. Tammy M. Rittenour (e-mail: [email protected]), Department of Geology, Utah State University, 4505 Old Main Hill, Logan UT, 84322, USA; received 25th February 2008, accepted 18th July 2008. River systems are important geomorphic agents in sculpting the Earth’s surface and are excellent monitors of environmental change because they integrate signals related to the geology, geomorphology, climate, hy- drology, vegetation and tectonics from within their catchments (e.g. Schumm 1977). As such, fluvial deposits and landforms provide important archives of river re- sponse to changes in climate, tectonics and base level. Additionally, fluvial deposits are commonly associated with archaeological sites. Obtaining age control from fluvial deposits, however, has been difficult due to limited organic material for radiocarbon dating and problems with reworking of old carbon in many fluvial sediments (e.g. Blong & Gillespie 1978; Gillespie et al. 1992; Stanley & Hait 2000). Other techniques, such as cosmogenic nuclide dating of terrace surfaces and U-series dating of pedogenic carbonate, provide mini- mum ages on sediment deposition and landform aban- donment (e.g. Gosse & Phillips 2001; Sharp et al. 2003). Optically stimulated luminescence (OSL) dating has the benefit of directly dating the time of sediment deposition and is a rapidly growing technique in the fields of sedi- mentology, geomorphology and archaeology (see reviews by Stokes 1999; Feathers 2003; Lian & Roberts 2006). This paper provides a review of new applications of OSL dating to fluvial deposits. Technical descriptions of OSL techniques are given elsewhere (e.g. Aitken 1998; Btter-Jensen et al. 2003). Wintle (2008a) pro- vides a general introduction to the minerals used for dating (quartz and feldspars) and dating methodolo- gies. Wallinga (2002) and Jain et al. (2004a) have pro- vided excellent reviews of the applications and problems of OSL dating in fluvial settings. The goal of this article is to provide an updated review of in- novative applications of OSL dating to fluvial deposits to solve questions related to fluvial response to climate and base level change, palaeoseismic studies and ar- chaeological applications. Luminescence dating of fluvial sediments OSL dating provides an age estimate for the last time sediments were exposed to sunlight, which resets the luminescence signal (Huntley et al. 1985). After burial, this signal grows with time due to exposure to ambient radiation in the surrounding sediments and from in- coming cosmic rays. The longer the sample is buried, the longer it is exposed to this low-level radiation and the greater the intensity of the luminescence signal subsequently measured. In the laboratory, the age of a sample is calculated by dividing the amount of ionizing radiation the sample absorbed during burial (called the equivalent dose, D e ) by the dose rate derived from the environment surrounding the sample. A number of techniques for D e determination have been developed (e.g. Wintle 1997; Aitken 1998; Lian & Roberts 2006). This article focuses on applications using the most re- cent single-aliquot regenerative dose (SAR) technique for quartz sand (blue and green light stimulated OSL) (Murray & Wintle 2000), feldspar (infrared stimulated luminescence, IRSL) (Wallinga et al. 2000a) and fine- grained (silt) IRSL dating (Banerjee et al. 2001). In this paper, quartz SAR OSL ages are referred to as quartz OSL ages, while luminescence ages obtained from other methods and minerals are identified differently. All methods of OSL dating rely on the luminescence signal acquired during the preceding burial history to have been removed by light exposure prior to deposi- tion. Incomplete solar resetting of the luminescence DOI 10.1111/j.1502-3885.2008.00056.x r 2008 The Author, Journal compilation r 2008 The Boreas Collegium

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Page 1: palaeoseismic and archaeological research · OSL dating to fluvial deposits. Technical descriptions of OSL techniques are given elsewhere (e.g. Aitken 1998; B tter-Jensen et al

Luminescence dating of fluvial deposits: applications to geomorphic,palaeoseismic and archaeological research

TAMMYM. RITTENOUR

BOREAS Rittenour, T. M. 2008 (November): Luminescence dating of fluvial deposits: applications to geomorphic, palaeo-seismic and archaeological research.Boreas, Vol. 37, pp. 613–635. 10.1111/j.1502-3885.2008.00056.x. ISSN 0300-9483.

Fluvial deposits and landforms are important archives of river response to climate, tectonics and base level changeand are commonly associated with archaeological sites. Unlike radiocarbon dating, the target material for opti-cally stimulated luminescence (OSL) dating (sands and silts) is nearly ubiquitous in fluvial deposits and the agerange for OSL spans the last glacial–interglacial cycle, a time period of interest to many Quaternary scientists.Recent advances in OSL techniques and the development of single-grain dating capabilities have now allowedfluvial deposits, and other deposits commonly afflicted with incomplete zeroing of the luminescence signal, to bedated. The application of OSL dating to fluvial deposits is discussed with respect to its potential to provide im-portant contributions to research in the fields of geomorphology, palaeoseismology and archaeology. Examplesare given from each research field.

TammyM. Rittenour (e-mail: [email protected]), Department of Geology, Utah State University, 4505 OldMain Hill, Logan UT, 84322, USA; received 25th February 2008, accepted 18th July 2008.

River systems are important geomorphic agents insculpting the Earth’s surface and are excellent monitorsof environmental change because they integrate signalsrelated to the geology, geomorphology, climate, hy-drology, vegetation and tectonics from within theircatchments (e.g. Schumm 1977). As such, fluvial depositsand landforms provide important archives of river re-sponse to changes in climate, tectonics and base level.Additionally, fluvial deposits are commonly associatedwith archaeological sites. Obtaining age control fromfluvial deposits, however, has been difficult due tolimited organic material for radiocarbon dating andproblems with reworking of old carbon in many fluvialsediments (e.g. Blong & Gillespie 1978; Gillespie et al.1992; Stanley & Hait 2000). Other techniques, such ascosmogenic nuclide dating of terrace surfaces andU-series dating of pedogenic carbonate, provide mini-mum ages on sediment deposition and landform aban-donment (e.g. Gosse & Phillips 2001; Sharp et al. 2003).Optically stimulated luminescence (OSL) dating has thebenefit of directly dating the time of sediment depositionand is a rapidly growing technique in the fields of sedi-mentology, geomorphology and archaeology (see reviewsby Stokes 1999; Feathers 2003; Lian & Roberts 2006).

This paper provides a review of new applications ofOSL dating to fluvial deposits. Technical descriptionsof OSL techniques are given elsewhere (e.g. Aitken1998; B�tter-Jensen et al. 2003). Wintle (2008a) pro-vides a general introduction to the minerals used fordating (quartz and feldspars) and dating methodolo-gies. Wallinga (2002) and Jain et al. (2004a) have pro-vided excellent reviews of the applications andproblems of OSL dating in fluvial settings. The goal ofthis article is to provide an updated review of in-novative applications of OSL dating to fluvial deposits

to solve questions related to fluvial response to climateand base level change, palaeoseismic studies and ar-chaeological applications.

Luminescence dating of fluvial sediments

OSL dating provides an age estimate for the last timesediments were exposed to sunlight, which resets theluminescence signal (Huntley et al. 1985). After burial,this signal grows with time due to exposure to ambientradiation in the surrounding sediments and from in-coming cosmic rays. The longer the sample is buried,the longer it is exposed to this low-level radiation andthe greater the intensity of the luminescence signalsubsequently measured. In the laboratory, the age of asample is calculated by dividing the amount of ionizingradiation the sample absorbed during burial (called theequivalent dose, De) by the dose rate derived from theenvironment surrounding the sample. A number oftechniques for De determination have been developed(e.g. Wintle 1997; Aitken 1998; Lian & Roberts 2006).This article focuses on applications using the most re-cent single-aliquot regenerative dose (SAR) techniquefor quartz sand (blue and green light stimulated OSL)(Murray & Wintle 2000), feldspar (infrared stimulatedluminescence, IRSL) (Wallinga et al. 2000a) and fine-grained (silt) IRSL dating (Banerjee et al. 2001). In thispaper, quartz SAR OSL ages are referred to as quartzOSL ages, while luminescence ages obtained from othermethods and minerals are identified differently.

All methods of OSL dating rely on the luminescencesignal acquired during the preceding burial history tohave been removed by light exposure prior to deposi-tion. Incomplete solar resetting of the luminescence

DOI 10.1111/j.1502-3885.2008.00056.x r 2008 The Author, Journal compilation r 2008 The Boreas Collegium

Page 2: palaeoseismic and archaeological research · OSL dating to fluvial deposits. Technical descriptions of OSL techniques are given elsewhere (e.g. Aitken 1998; B tter-Jensen et al

signal at deposition (partial bleaching) results in ageoverestimation and can be a problem in some fluvialsettings (e.g. Murray et al. 1995; Gemmell 1997; Olleyet al. 1999, 2004b; Stokes et al. 2001).

Partial bleaching (zeroing) of the luminescence signalprior to deposition is likely in fluvial environments for anumber of reasons. Solar resetting of water-transportedsediment is limited by the attenuation of light throughthe water column (e.g. Berger 1990). This effect is en-hanced by increased suspended sediment concentra-tions (e.g. Berger & Luternauer 1987). Water depth, themode of sediment transport (suspension, saltation orbedload) and transport distance are also importantcontrols on the bleaching of fluvial sediments. The di-rect input of non-bleached sediment from the erosion ofolder deposits and river banks is common in fluvialsystems and also contributes to scatter in results. Ad-ditionally, floods, storms and other high-dischargeevents cause rapid erosion and transport of sediments,limiting solar exposure.

A number of methods have been proposed to combatthe influence of partial bleaching on De values and re-sulting age calculations. One group of methods utilizesthe multiple components of the quartz OSL signal toisolate and date the most light-sensitive OSL traps(e.g. Tsukamoto et al. 2003; Jain et al. 2005a; Li & Li2006). A second group of methods takes advantage ofrecent advances in the OSL technique that have led tothe measurement of smaller and smaller aliquot sizes(Olley et al. 1998), culminating in the development ofsingle-grain dating techniques (Duller et al. 1999;Duller 2000, 2008) and instrumentation (B�tter-Jensenet al. 2000).

In partially bleached samples, analysis of large ali-quots of sand may produce age overestimates from thecontribution of non-bleached grains to the total signalmeasured (e.g. Jacobs et al. 2003; Thomas et al. 2005;Porat et al. 2008). Small-aliquot (o100 grains) andsingle-grain dating may allow the true burial age of asample to be isolated by allowing the population ofgrains not bleached at deposition to be identified. Single-grain results commonly show positively skewed De dis-tributions, with the youngest population representingthe grains fully bleached at deposition (Fig. 1).

Owing to the large distribution of De results in single-grain analysis, a number of statistical methods havebeen produced to isolate grains representative of thetrue burial dose. These include methods that calculatethe mean of the lowest 5% of the De values (Olley et al.1998), methods that fit a Gaussian distribution to theleading edge (youngest values) of a De distribution his-togram (Lepper et al. 2000) and the central age model(CAM), minimum age model (MAM) and finite mix-ture model (FMM) (Galbraith et al. 1999; Galbraith2005). The optimum choice of statistical methods maybe different for each sample and is dependent on thedominant mechanisms affecting De scatter (e.g. partial

bleaching, post-depositional mixing or dose-rate het-erogeneity) (Bailey & Arnold 2006).

Considerable success has been achieved using single-grain dating from some of the most challengingdepositional environments, including fluvial deposits(Olley et al. 2004b; Thomsen et al. 2007; see also reviewby Duller 2008). Single-grain dating is most importantfor, and applicable to, younger samples (less than a fewthousand years old) (Jain et al. 2004a). Collection ofmodern samples from a number of depositional en-vironments has indicated residual luminescence signalin some settings. This level of non-bleached signalwill contribute a large proportion of the measured De

in young samples and can produce large age over-estimates (e.g. Murray et al. 1995). This effect is ex-pected to be reduced in older samples that have higherburial doses. As an example, DeLong & Arnold (2007)report large overestimates (up to 50% and greater) ofsingle-aliquot measurements as compared to single-grain measurements from samples under 1000 yearsold. Negligible differences were found in late Pleisto-cene samples. Similar overestimates in age have beenseen in other analyses of large aliquots from partiallybleached samples (e.g. Thomas et al. 2005; Porat et al.2008).

Figure 1 gives examples of single-grain and large ali-quot results from young fluvial samples collected froman ephemeral stream in western Nebraska (Hanson2006). It is clear from the dose distributions of the sin-gle-grain results that these samples have high De scatterthat is skewed toward higher doses, indicative of partialbleaching. However, results from the large aliquot(5mm) analyses do not show this same skewness andhave much higher mean and minimum De values.Averaging of thousands of grains has masked signs ofpartial bleaching and the true burial age of the sample.For these reasons, single-grain and small-aliquot ana-lysis is preferred for identification and potential miti-gation of problems associated with partial bleaching inyoung fluvial samples.

Despite potential pitfalls, many studies have hadconsiderable success in dating fluvial deposits usingsingle-aliquot (multi-grain) techniques (e.g. Tornqvistet al. 2000; Cheong et al. 2003; Rittenour et al. 2005;Rodnight et al. 2005, 2006; Tooth et al. 2007). As withsingle-grain dating, samples with evidence of partialbleaching may require statistical methods to isolate thetrue burial dose (e.g. Olley et al. 1998; Galbraith et al.1999, 2005; Lepper et al. 2000; Roberts et al. 2000;Fuchs & Lang 2001), but, overall, most sediments haveproved datable by OSL with only a few exceptions(Wallinga 2002; Jain et al. 2004a).

Research by a number of groups over the last coupleof decades has identified interesting results regardingthe bleaching of sediments in fluvial environments. Thefirst is related to the observation that modern and re-cently deposited sediment in fluvial systems is

614 Tammy M. Rittenour BOREAS

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commonly less well bleached than samples collectedfrom older deposits from the same river system (see Jainet al. 2004a). The large influence of small residual lu-minescence signals on ‘modern age’ deposits com-pounds this difference but does not completely explainit. Collection of modern analogue samples has beenproposed to identify the bleaching efficiency of differ-ent depositional environments (Murray et al. 1995).However, not all modern samples are good analoguesfor bleaching of older deposits. It is likely that sedi-ments in terrace deposits and older floodplain and

channel deposits have undergone considerably longerand more numerous transport and deposition cyclesprior to final deposition (allowing for greater bleach-ing) than the transient sediment found in modernchannel and bar deposits (Jain et al. 2004a).

A second unexpected result in the bleaching of fluvialsediment is related to the difference between coarserand finer grain sizes. It might be expected that fine-grained sediment (silt to very fine sand) would be betterbleached due to the greater potential for these sedi-ments to be transported in suspension in the water

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Age Results

SG = 150±20 yrMG = 1400±180 yrLowest MG De = 430±530 yr

SG = 550±40 yrMG = 1400±140 yrLowest MG De = 630±50 yr

SG = 500±50 yrMG = 1270±140 yrLowest MG De = 340±30 yr

Rocky Hollow 7–1n = 21

00 1.5 3 4.5 6 7.5 9 10.5

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Rocky Hollow 8–3n = 247

–3 0 3 6 9 12 15182124273033 363942454851

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Rocky Hollow 14–1n = 20

Rocky Hollow 14–1n = 204

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–2 0 2 4 6 8 1012 14 1618 20 22 24 26 28 3032

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Large aliquot(multi-grain, MG) Single grain (SG)

Fig. 1. Comparison of large-aliquot and single-grain results from three young fluvial samples from an ephemeral stream in western Nebraska(Hanson 2006). Results from the large-aliquot analysis (5mm, thousands of grains) show some signs of equivalent dose (De) scatter, such asbimodal distributions (sample 7-1) and skew toward younger values (sample 14-1). Multi-grain results from sample 8-3 are normally dis-tributed, which may be interpreted to indicate a well-bleached sample. However, single-grain results show skewed distributions toward higherDe values and provide a clearer image of the partial bleaching within these samples. Averaging of thousands of grains within the large aliquotshas masked these signs of partial bleaching and the true burial age of the sample. Under the age results column: SG=single-grain results usinga minimum age model; MG=multi-grain (large-aliquot) results. Data kindly provided by P. R. Hanson, University of Nebraska.

BOREAS Luminescence dating of fluvial deposits 615

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column. Coarser sediment (medium-coarse sand) ismore likely to have been transported as bedload bysaltation or tractive forces at the base of the water col-umn. However, many studies have found that thecoarser grain sizes have lower De values and are betterbleached at deposition (Olley et al. 1998; Colls et al.2001; Truelsen & Wallinga 2003; Alexanderson 2007;Vandenberghe et al. 2007).

The reasons for the difference in bleaching betweenfiner and coarser grain sizes are not fully understoodbut are probably related to the mode of transport.Coarser grained sediments are transported at a slowerrate through a fluvial system than silts and very finesand in suspension, allowing more time for sunlightexposure between initial erosion from an older depositand final deposition. Coarser sediment is also morelikely to be deposited on channel bars and exposed tolight numerous times during transport. In addition tomud coatings on fine grains, the cohesive properties ofsilts and very fine sand may cause these grains to betransported as aggregates and hinder solar bleaching.Regardless of the cause of the difference in bleachingbetween grain sizes, it is recommended that coarsergrain sizes are dated in fluvial deposits where partialbleaching is a problem.

Comparison between dating techniques

A number of studies have compared OSL ages withother dating techniques. Murray & Olley (2002) com-pared quartz OSL ages from known age deposits from a

number of depositional settings and found a good cor-relation, with accurate OSL ages obtained to at least350 kyr. Figure 2 is an updated version of the figureproduced by Murray & Olley (2002) with additionalsamples included. Note that despite potential problemswith partial bleaching in fluvial settings, there is nosystematic offset for fluvial samples as compared toother depositional environments.

Most studies have compared OSL with radiocarbondue to its wide application and acceptance in the Qua-ternary research community and have found good cor-respondence in many cases (e.g. Wallinga et al. 2001;Jain et al. 2004a; Olley et al. 2004a; Rittenour et al.2005), but not all (e.g. Folz et al. 2001; Kolstrup et al.2007; Owen et al. 2007). However, while inconsistenciesbetween these chronometers may indicate errors in theOSL chronology (e.g. due to partial bleaching or doserate uncertainty), it is also likely that they reflect pro-blems with radiocarbon ages due to contamination orreworking of organic material (e.g. Goble et al. 2004;Cupper 2006; DeLong & Arnold 2007). Additionally,there is added uncertainty when comparing OSL andradiocarbon due to problems with calibrating radio-carbon ages to calendar years beyond 15 kyr (Reimeret al. 2004).

Despite potential problems with both techniques,there is good agreement in samples collected from fluvialdeposits from throughout the radiocarbon age range(0–40kyr) (Fig. 2). Fewer comparisons are available forolder samples, but there is no evidence of systematic de-parture between OSL and independent ages over the last

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Aeolian (n = 43)

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Marine (n = 33)

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over

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tial b

leach

ing)

Fig. 2. Comparison of quartz SAR OSL agesfrom fluvial (filled squares) and other depositionsettings to independent age control. Modifiedand updated fromMurray & Olley (2002) withmore recently published results. Age data andreferences provided in Appendix Table 1.

616 Tammy M. Rittenour BOREAS

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several hundred thousand years (e.g. Murray &Olley 2002; Murray & Funder 2003; Watanuki et al.2005; Murray et al. 2007, 2008).

Applications and examples

Fluvial deposits and environments are important ar-chives of past changes in climate, base level and tec-tonics, and commonly contain archaeological horizons.Therefore, accurate age control from fluvial deposits isimportant for a number of research fields. OSL datingof fluvial deposits has become increasingly widely usedand accepted over the past decade. Examples of theapplication of OSL dating to a number of fluvial set-tings and research questions are discussed below.

Fluvial response to glaciation and sea-level change

River channel morphology, longitudinal valley profile,sedimentary architecture and dynamic state (aggrad-ing/incising/stable) are controlled by complex interac-tions between external controls such as climate,tectonics and base level (e.g. Blum & Tornqvist 2000).Although fluvial deposits and landforms do not providea direct record of past base level and climate change,they can provide information about the response of theriver system to these external variables.

Large river systems such as the lower MississippiRiver in the United States, the Rhine–Meuse River

system in The Netherlands, and the River Thames andformer Solent River in southern England have beenextensively studied with respect to fluvial response toglaciation and sea-level change (e.g. Bridgland 1994,2000; Maddy et al. 1998; Tornqvist 1998; Blum et al.2000; Tornqvist et al. 2000, 2004; Rittenour et al. 2007).These rivers have also been extensively dated withradiocarbon, although most of these ages are limited toHolocene deposits due to the lack of organic material inthe Pleistocene strata and the upper age limit forradiocarbon dating. OSL dating has been applied tothese river systems to extend the fluvial chronologiesover the past several glacial–interglacial cycles.

Mississippi River, USA. – An OSL chronology basedon over 80 quartz OSL ages has been developed forPleistocene and Holocene fluvial deposits in the lowerMississippi valley (Rittenour et al. 2003, 2005, 2007;Holbrook et al. 2006). OSL ages were collected fromoutcrops and shallow surface cores from late Pleisto-cene braid belts and last interglacial and Holocenemeander belts and range from 0 to 85 kyr (Fig. 3) (Rit-tenour et al. 2005, 2007). These ages agree with theavailable radiocarbon chronology and relative ageconstraints from loess stratigraphy and cross-cuttingrelationships. Additionally, OSL results show onlyminimal influence of partial bleaching despite sedimenttransport under high suspended sediment load condi-tions and late Pleistocene glacial meltwater discharge.

Fig. 3. Generalized cross-section of fluvial landforms and deposits in the northern lower Mississippi valley with the OSL chronology plottedgraphically above each terrace surface. Modified from Rittenour et al. (2005) with the addition of Holocene meander belt ages.

BOREAS Luminescence dating of fluvial deposits 617

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Adequate bleaching prior to deposition was likely dueto long transport distances. Insights gained from thisnew OSL chronology and field relationships suggestthat braid belt formation and abandonment was con-trolled by fluctuations in glacial sediment and melt-water discharge, while sea level controlled the elevationto which the river was graded (Rittenour et al. 2007).

Rhine–Meuse River, The Netherlands. – OSL datinghas also been conducted on the Rhine–Meuse Riversystem in The Netherlands (Tornqvist 1998; Tornqvistet al. 2000, 2003; Wallinga 2001; Wallinga et al. 2001,2004; Busschers et al. 2005, 2007). Over 90 lumines-cence samples have been collected from a number ofdeep cores collected within the Rhine–Meuse valley(Busschers et al. 2005, 2007). A majority of the sampleswere processed to extract quartz for luminescencemeasurements, while some were processed for bothquartz and feldspar dating. Where comparisons weremade, feldspar IRSL ages consistently underestimatedboth quartz OSL ages and constraints from known-agedeposits (Wallinga et al. 2000b, 2001). This may be dueto anomalous fading of the luminescence signal in feld-spars and problems with its correction (e.g. Wintle1973; Wallinga et al. 2007). Quartz OSL ages rangefrom Holocene to over 200 kyr, and are strati-graphically consistent with the available radiocarbonand pollen biostratigraphic age control (Busschers et al.2005, 2007). OSL results and core descriptions havebeen used to reconstruct river response to sea level andhave helped to refine the subsurface fluvial stratigraphyof the Rhine–Meuse River system (Tornqvist et al.2000, 2003; Busschers et al. 2005, 2007). Additionally,hundreds of cores and stratigraphic descriptions fromthe Rhine–Meuse Delta have been used to reconstructchannel patterns and fluvial response to ice advance,sea level and climate change during the last glacial cycle(Busschers et al. 2005, 2007, 2008).

Thames and Solent River systems, southern Eng-land. – The large river systems south of the Anglian(marine oxygen isotope stage, MIS 12) and Late De-vensian (MIS 2) ice limits in southern England containextensive fluvial records that extend back to the MiddlePleistocene and roughly correlate to glacial–interglacialclimate, sea-level and isostacy changes in the region(e.g. Sandford 1924; Bridgland 1994, 2000; Maddyet al. 1998; Lewis et al. 2001; Briant et al. 2006). Fluvialdeposits and terraces of the River Thames, and to alesser extent those in the Solent basin, have been datedby pollen and mammalian biostratigraphy, aminoacidgeochronology and Palaeolithic artifact assemblages(e.g. Briggs et al. 1985; Bridgland 1994). New quartzOSL chronologies have been developed to refine thechronostratigraphies in these river systems (e.g. Maddyet al. 1998; Lewis et al. 2001; Briant et al. 2006). TheseOSL chronologies for the most part match previous age

models; however, there are some inconsistencies andscatter in age results for deposits older than 300 kyr inthe Solent basin, possibly due to samples nearing themaximum limit for OSL dating and saturation of theluminescence signal (Briant et al. 2006).

Fluvial response to climate change

River systems and climate are intimately linkedthrough the hydrological cycle and climate-mediatedchanges in sediment yield within catchments (e.g.Schumm 1977; Bull 1991). Despite potential problemswith partial bleaching, considerable success has beenobtained applying OSL dating to a number of differentfluvial settings for the reconstruction of fluvial responseto climate change (e.g. Leigh et al. 2004; Schokker et al.2005; Briant et al. 2006; Brook et al. 2006; Williamset al. 2006; Sohn et al. 2007; Thomas et al. 2007b). Stu-dies from a number of regions and climate settings arediscussed below.

Hillslope and fluvial response to climate, Australia. –Luminescence dating has played a key role in Quaternarystudies and climate reconstruction from fluvial sequencesin Australia (e.g. Page et al. 1991, 1996; Page & Nanson1996; English et al. 2001; Ogden et al. 2001; Banerjee et al.2002; Kemp & Spooner 2007). Thomas et al. (2007a)provide an excellent example of the application of OSLdating to hillslope and fluvial deposits along the north-eastern coast of Queensland, Australia to decipher fluvialresponse to climate change. Ages were obtained usingradiocarbon (n=6), thermoluminescence (TL) (n=16)and quartz OSL methods (n=36). Owing to scarcity oforganic material for radiocarbon dating, age control wasonly possible through luminescence dating techniques atmost locations. Results indicate marked differences in al-luvial/colluvial systems between coarse-grained fanglo-merate deposition in MIS 3 (64–28kyr), fine-grainedalluviation and vertical fan accretion inMIS 2 (28–24kyr)and incision at �14–15kyr. Correlation to the regionalpollen stratigraphy (Kershaw et al. 2007) suggests thatthese changes in hillslope and fluvial processes were asso-ciated with climate and vegetation shifts.

Tributary and trunk channel response to climate, GrandCanyon and southwestern USA. – Studies of arid flu-vial systems have suggested that they are sensitive in-dicators of climate-related changes in sediment supplyand discharge (e.g. Bull 1991). The Colorado River andits tributaries in the Grand Canyon and Grand WashTrough, just downstream of the Grand Canyon, havebeen the focus of research efforts to understand the re-sponse of different scale fluvial systems to local and re-gional climate (Anders et al. 2005; DeJong et al. 2006;Pederson et al. 2006; Rittenour et al. 2006; DeJong2007). Fluvial deposits and terrace landforms have beendated by a number of methods. The time of fluvial

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aggradation and sediment deposition has beendetermined by quartz OSL dating of sediment andU-series dating of interbedded travertine that wasdeposited contemporaneously with fluvial deposition.Terrestrial cosmogenic nuclide (TCN) surface dating ofdesert pavements and sediment profiles provides mini-mum age estimates for river incision and terrace surfaceabandonment (Gosse & Phillips 2001).

Geochronologic and stratigraphic results from fourstudy areas within and adjoining the Grand Canyon arepresented in Fig. 4. Age results are consistent betweenthe different dating methods and are coherent withstratigraphic relationships. OSL results are roughlyequivalent to U-series ages of fluvial aggradation inTravertine Grotto in western Grand Canyon (Fig. 4C).In eastern Grand Canyon, OSL and TCN samples werecollected from a number of terraces from the ColoradoRiver and its tributaries. As expected, TCN ages ofterrace surface abandonment and landform stabiliza-tion are younger than OSL ages of fluvial aggradationof the underlying terrace fill (Fig. 4A, B). Equivalentdose distributions from samples collected from quartz-rich, long-transported deposits of the mainstem Color-ado River showed very little evidence for partialbleaching, while samples of short-transported and lo-

cally sourced sediments from tributary catchmentscontained much greater scatter and evidence for partialbleaching (DeJong et al. 2006; Rittenour et al. 2006;DeJong 2007).

OSL ages from deposits of the Colorado River andits tributaries in eastern and western Grand Canyonand Grand Wash Trough have provided important in-formation about incision rates (Pederson et al. 2006)and the timing of the response of these arid fluvial sys-tems to regional and extra-regional climate (Anderset al. 2005; DeJong et al. 2006; Rittenour et al. 2006;DeJong 2007). OSL and other chronostratigraphicresults from terrace deposits of the main stem ColoradoRiver indicate that aggradation and incision werepredominantly controlled by MIS 4 glaciation in itsheadwaters. In contrast, tributary chronologiesindicate a local response to climate-related sedimentsupply and have very few similarities with con-temporaneous dynamics in the main stem river (Anderset al. 2005; DeJong et al. 2006; DeJong 2007) (Fig. 4B,C). Terrace stratigraphies from Grand Wash indicatelower late Pleistocene incision rates and record adifferent sequence of fluvial terraces in this much largerand more arid drainage basin (Rittenour et al. 2006)(Fig. 4D).

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Fig. 4. Schematic cross-sections and age constraints from terrace sequences from (A) the Colorado River in eastern Grand Canyon (modifiedfrom Pederson et al. 2006), (B) tributary valleys in eastern Grand Canyon (modified from Anders et al. 2005), (C) Travertine Grotto, a smalltributary in western Grand Canyon, and (D) Grand Wash in the Grand Wash Trough, just downstream of Grand Canyon. Age control hasbeen provided by OSL ages on fluvial sediment, U-series ages on travertine interbedded within fluvial and colluvial sediments and terrestrialcosmogenic nuclide (TCN) dating of terrace surfaces. As expected, OSL and U-series age from the same terrace fills provide similar ages whileTCN ages of terrace surface abandonment and landform stabilization are younger than OSL ages of fluvial aggradation of the underlyingterrace fill.

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Climate and tectonic record from fluvial systems on theGangetic Plains, India. – The broad Gangetic Plains inthe Himalayan Foreland Basin of northern India con-tain a rich archive of fluvial response to climate changeand regional tectonic activity. Radiocarbon, quartzOSL and feldspar IRSL ages have been obtained fromfluvial deposits of the Ganga River and its tributaries(Srivastava et al. 2003a; Gibling et al. 2005; Williamset al. 2006; Sinha et al. 2007). Despite potential partialbleaching problems in these fluvial settings, lumines-cence ages are in close agreement with radiocarbon agecontrol where present. Gibling et al. (2005) identifieddisconformity-bounded floodplain sequences on nowdissected interfluves on the southern Gangetic Plain.Interpretations of these and other stratigraphies fromthe Gangetic Plains suggest that the Ganga River sys-tem has switched between modes of aggradation andincision several times during the last glacial cycle, mostlikely due to changes in the monsoonal precipitationregime (Gibling et al. 2005; Williams et al. 2006; Sinhaet al. 2007). Superimposed on these climate-drivenchanges in fluvial dynamics, geomorphic evidence sug-gests that some incision events were driven by tectonicactivity (Srivastava et al. 2003a, b).

Indian monsoon variability, Thar Desert, India. – Adetailed palaeoclimate record of Indian monsoonvariability is emerging from luminescence-dated fluvialdeposits from the Thar Desert in western India. Juyalet al. (2006) combined quartz OSL ages and strati-graphic descriptions from the Mahi and Orsang Riversto reveal sub-Milankovitch-scale changes in fluvial re-gime related to variations in monsoonal precipitation

over the last 130kyr (see also Tandon et al. 1997) (Fig. 5).This OSL-dated fluvial record shows similar changes inpalaeomonsoon intensity as a marine productivity re-cord from the Arabian Sea (Leuschner & Sirocko 2003)(Fig. 5). Luminescence-dated chronologies from theLuni River and other fluvial systems in the Thar Desertalso suggest a regional fluvial response to climatechange (Jain & Tandon 2003; Jain et al. 2005b).

Equivalent dose distributions from fluvial samplesdisplayed asymmetrical distributions skewed towardhigher values. In order to mitigate partial bleachingproblems and remove the contribution of aliquots con-taining non-bleached grains from the final age calcula-tion, Juyal et al. (2006) used a subset of the youngest De

values (defined as the minimum De value to the mini-mum De value1(2�error)) to calculate their OSL ages.This method is similar to other methods proposed toisolate the youngest population of De values, assumedto be representative of the true burial age.

Slackwater flood sequences from the Thar Deserthave also been analysed to reconstruct monsoon-related large flood frequency over the last millennium.Kale et al. (2000) described several slackwater flooddeposits along the Luni River and used OSL dating toprovide age control. OSL was chosen over radiocarbondating due to the ability to systematically sample de-sired flood units. Because of the possibility of partialbleaching in sediment transported during floods withhigh suspended sediment loads, multiple OSL datingtechniques and different mineral fractions were ana-lysed. The primary age control for the sections was ob-tained by OSL dating quartz using a multiple aliquot(MA) additive-dose technique. Duplicate analyses of

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formation

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weak monsoon

weak monsoon

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enhanced monsoonwith seasonality

Southern Thar Desert Fluvial Record(Juyal et al. 2006)

enhanced monsoon

grain size

Fig. 5. Synthesis diagram from the research ofJuyal et al. (2006) on fluvial deposits in thesouthern Thar Desert, India. OSL ages werecollected from fluvial channel and floodplaindeposits, depositional environments describedand monsoonal activity interpreted. This fluvialrecord of palaeomonsoon activity correlates ni-cely with marine Ba/Al productivity records ofmonsoon strength from the Arabian Sea (right-most panel, Leuschner & Sirocko 2003).

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each sample followed SAR (quartz) and MA differ-ential partial bleach (feldspar) (Singhvi & Lang 1998)techniques. SAR results indicate that the samples werefairly well bleached at deposition. Results from thestudy indicate variability in flood frequency over thelast 1000 years that match records of changes in re-gional monsoon precipitation (Bryson & Swain 1981)and other palaeoflood reconstructions from central In-dia (Ely et al. 1996; Kale 1999).

Summary. – Fluvial deposits contain valuable recordsof river response to changes in sea level, climate andglaciation. Systematic collection of OSL samples fromsilty and sandy material within fluvial sequences canprovide valuable age control on deposits that areotherwise difficult to date due to limited organic mate-rial for radiocarbon dating. Additionally, the age rangefor OSL dating is sufficiently long, up to �300 kyr insome cases (e.g. Murray & Olley 2002), to allow for thereconstruction of fluvial response to climate and sea-level change over the last glacial cycle. Moreover, re-cent statistical and technical advances in OSL datinghave reduced or mitigated partial bleaching problemsfound in some fluvial settings (e.g. Duller et al. 1999;Galbraith et al. 1999; Murray &Wintle 2000; Galbraith2005). These advances and developments allow fluvialdeposits to be accurately dated with OSL and recordsof fluvial response to climate and sea-level change to beconstructed.

Palaeoseismic reconstruction

Fluvial deposits, terraces and alluvial fans can be im-portant archives of tectonic activity (e.g. Schumm 1986;Holbrook & Schumm 1999; Pearce et al. 2004). Anumber of studies have used OSL and other datingmethods on offset fluvial deposits or landforms to de-termine the timing of fault displacement, slip rates andseismic recurrence intervals (e.g. Chen et al. 2003;Cheong et al. 2003; Caputo et al. 2004; Zuchiewicz et al.2004; Mahan et al. 2006; Mason et al. 2006; Mukulet al. 2007). OSL dating has also been directly appliedto fault-scarp colluvium to more directly date seismicevents (e.g. Lu et al. 2002; Fattahi & Walker 2007;Porat et al. 2008). Some examples of the application ofOSL dating of fluvial deposits for palaeoseismic re-constructions are given below.

Offset fluvial deposits and landforms. – One of the mostcommon uses of OSL dating for palaeoseismic studies isdating offset or deformed fluvial landforms or deposits(e.g. Thompson et al. 2002; Cheong et al. 2003; Coxet al. 2006; Amos et al. 2007). Fluvial landforms cancommonly be correlated over long distances and havefairly consistent slopes, allowing crossing faults andstructures to be identified and the displacement of fea-

tures to be calculated. Age control on displaced land-forms and deposits is necessary for the calculation ofslip rates and recurrence intervals on fault movementand earthquake activity. Age control on past seismicevents is especially important for the development ofaccurate hazard assessments of tectonically active re-gions near population centres.

Fattahi et al. (2006, 2007) have studied displaced anddeformed alluvial fans and terraces from the highlyseismically active Alborz-Kopeh Dagh ranges innortheastern Iran. For example, Fattahi et al. (2006)examined folded and faulted alluvial fan deposits asso-ciated with the Sabzevar thrust fault. Quartz OSL agesfrom deformed alluvial sediments indicate fan deposi-tion from �32 to 13 kyr, faulting and graben formationby �9 kyr and additional faulting on the Sabzevarthrust fault in the last 3 kyr (Fig. 6A). Slip rates as highas �1mm/yr and a 3000-year recurrence interval forlarge earthquakes were calculated for this active faultsegment. Reassessment of a young colluvial sample byFattahi & Walker (2007) has produced a SAR IRSLage of 1.7�0.3 kyr on pre-faulting colluvium (Fig. 6A),suggesting that the most recent faulting and displace-ment on the Sabzevar thrust likely represents theearthquake that destroyed the town of Sabzevar in AD1052.

In southern California, DeLong et al. (2007) studieda fluvial terrace that was cross-cut and offset by theeastern Big Pine oblique-reverse fault, one of a numberof faults associated with the broad San Andreastransform fault system. They used quartz OSL ages toconfirm geomorphic evidence that the deposits on ei-ther side of the fault scarp were originally part of thesame terrace surface (Fig 6B). Although there is somescatter in the data, OSL ages from the hanging wall(24.3�2.8 to 14.3�1.9 kyr) and the foot wall (22.0�2.4to 15.9�3.0 kyr) are consistent. From these OSL agesand the amount of vertical displacement on the fault(�10m), a dip-slip rate estimate of �0.9m/kyr wascalculated.

Geomorphic response to tectonic uplift, folding andfaulting. – In addition to dating offset fluvial land-forms, OSL dating has been used by a number ofresearchers to assess tectonic activity by studying thefluvial geomorphic response of rivers to deformation(e.g. Holbrook et al. 2006; Mason et al. 2006; Mathewet al. 2006; Mukul et al. 2007; Srivastava & Misra2008). Localized river incision and/or channel patternchanges near known structures are commonly used cri-teria to identify fault activity or fold deformation (e.g.Schumm, 1986; Holbrook & Schumm, 1999).

Mathew et al. (2006) used OSL to date incisedchannel deposits from a number of rivers along an ac-tive fault-related fold associated with the KachchhMainland Fault in northwestern India. Incision ages onfluvial deposits progressively decreased in age eastward.

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These data, along with geomorphic evidence, were usedto suggest eastward lateral fold migration during theHolocene due to fault length extension and vertical up-lift rates of 10�1mm/yr.

Mukul et al. (2007) and Srivastava & Misra (2008)have dated fluvial deposits related to incision from ac-tive uplift and faulting along the Himalayan front innortheastern India. Mukul et al. (2007) used an in-novative approach of applying both TL ages fromfault-gouge material (see discussion below) and quartzOSL ages from unpaired strath terraces to providedevidence for the timing and response of the Tista Riverto uplift and seismic activity surrounding the SouthKalijhora Thrust and several out-of-sequence, surface-breaking faults. Srivastava & Misra (2008) combinedgeomorphic analysis of strath terraces and quartz OSLdating to examine the uplift history of the Himalayanfront along the Kameng River. Their results indicatethat the greatest river incision occurred at about 7 kyr(11.9mm/yr), with average incision rates during the14 kyr of record of 7.5mm/yr. Geomorphic analysis ofthe ratio between strath height and alluvial coverthickness (Starkel 2003) suggest that the strath terraceswere formed predominantly in response to tectonic up-lift with lesser climate influence.

Holbrook et al. (2006) used quartz OSL and radio-carbon dating to determine the timing of channelstraightening events in Mississippi River meander beltsin the New Madrid Seismic Zone, USA. They inter-preted the switch from a highly sinuous channel to astraightened channel course as a response to periodicclustering of seismic events and decreased gradient dueto fault displacement. Two and possibly three straigh-tening events were identified through mapping cross-

cutting relationships and extensive coring (Holbrooket al. 2006). Age control was provided by radiocarbonages on carefully selected macrofossils from channel filldeposits (n=12) and OSL samples from point bar de-posits (n=14) (Fig. 7). OSL and radiocarbon ageswere consistent, and where paired samples were col-lected, point bar samples were older than their asso-ciated abandoned channel-fill deposits, as expectedbased on geomorphic relationships.

Fault-scarp colluvium. – Direct dating of discrete faultrupture events can be achieved by OSL dating fault-scarp colluvium. Trenching of faults is a routine tech-nique for many palaeoseismic studies (e.g. McCalpin1998). Traditionally, colluvial wedges and fault planesare identified from these trenches, and organic materialfrom buried soils or other organics within the faultedsediments are radiocarbon dated to obtain a fault-rup-ture chronology. However, organic material is com-monly scarce in many arid settings and thereforeradiocarbon sample collection is mostly opportunisticin nature. Luminescence dating, on the other hand,allows more selective sampling and has been usedby a number of researchers (e.g. Forman et al. 1989,1991; Porat et al. 1997; Zilberman et al. 2000;Amit et al. 2002; Lu et al. 2002). Early analyses usingTL dating have been largely replaced by OSL andsingle-grain techniques to allow measurement ofthe most light-sensitive traps and most well-bleachedgrains.

Porat et al. (2008) examined colluvial wedge depositsfrom the base of a normal fault that has displaced amiddle Holocene alluvial fan in the Dead Sea Trans-form, southern Israel. They compared large aliquot

A

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hinge grabeninfilled withaeolian sand

tilted bedslow angle thrusts

horizontal strata colluvial wedge

alluvial fan surface

not to scale

24.3±2.8 – 14.3±1.9 kyr (n=3) 22.0±2.4 – 15.9±3.0 kyr (n=4)

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Fig. 6. Examples of the applications of OSLdating to palaeoseismic research and re-construction of fault slip rates. A. Schematicdrawing of faulting and folding of an alluvialfan along the Sabzevar thrust fault in north-eastern Iran (Fattahi et al. 2006; Fattahi &Walker 2007). OSL ages indicate fan syndepo-sitional folding and faulting from 32 to 13 kyr,graben formation by 9 kyr and a SAR IRSLage from faulted colluvium suggests that themost recent faulting on the Sabzevar thrust oc-curred within the last 1.7 kyr. Modified fromFattahi et al. (2006). B. OSL age ranges col-lected from a fluvial terrace that has been offsetby the eastern Big Pine fault in southern Cali-fornia, USA. OSL ages were used to confirmthat the now displaced fluvial landforms wereonce the same terrace surface and to calculatedipslip rates on the fault. Modified from De-Long et al. (2007).

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(1000’s grains), small-aliquot (100’s grains) and single-grain results from samples collected from proximal (lessthan 1m from the fault) and distal (�2m from thefault) parts of a stack of colluvial wedges (Fig. 8).Results indicate partial bleaching in all samples, withgreater partial bleaching in proximal colluvial wedgesamples (Table 1). Age reversals in SAR multi-grainanalyses were attributed to progressive exposure anderosion of older sediments with continual faultdisplacement. Large aliquot ages substantially over-estimated the time of faulting, providing additionalsupport for the use of small-aliquot or single-graindating for environments where partial bleaching maybe a problem. Single-grain results analysed using theminimum age model of Galbraith et al. (1999)produced the most reasonable ages (Table 1).

OSL dating of fault gouge and liquefaction features. –Innovative research is being developed to directly datefaulting by luminescence dating fault gouge and lique-faction features. During seismic activity and fault slip itmay be possible that sediment within the fault gouge

receives enough energy from friction, vibration, crush-ing and heat to zero the luminescence signal. Initialstudies tested the application of thermoluminescence(Fukuchi 1992) and electron-spin resonance (ESR)(Singhvi et al. 1994) to date fault-gouge materials andfound results consistent with radiocarbon ages. Morerecently, Mukul et al. (2007) applied TL dating of fault-gouge deposits in northeastern India and found TLages much younger than the source rock (42–45 kyrcompared to Z2Myr), suggesting the samples werezeroed during fault movement. Owing to uncertaintieswith partial resetting of the TL signal, the ages wereconsidered maximum ages for faulting. Research in-volving OSL analysis of fault-gouge deposits may pro-vide more sensitive indicators of fault movement andluminescence resetting (Rink et al. 1999).

Liquefaction features such as injection dikes and sandblows (deposition from the surface rupture of an injec-tion dike) are commonly produced during earthquakesin sandy fluvial deposits. New research is investigatingthe potential applications of OSL to these liquefactionfeatures in an attempt to directly date seismic events.

Channel Fill

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Fig. 7. OSL and radiocarbon ages collected from point bar and channel fill deposits of the Mississippi River in the NewMadrid Seismic Zone,USA. Meanderbelt abandonment and straightening of channel courses, as dated by OSL and radiocarbon, have been interpreted to haveoccurred in response to clustered seismic activity on the Reelfoot fault. Note that OSL ages from point bar deposits are older than their asso-ciated channel fill deposits, as expected from geomorphic relationships. Modified from Holbrook et al. (2006).

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Porat et al. (2007) investigated the use of OSL todetermine the difference between clastic dikes (filledfrom above) and injection dikes (formed by liquefac-tion during earthquakes) in the southern Dead Sea ba-sin of Israel. It was proposed that injection dikes wouldhave the same OSL age as the late Pleistocene sourcematerial, OSL dated to 43–34 kyr. However, quartz

OSL ages from both the depositional and injectiondikes were dated to 17–15 kyr. These results imply thatthe OSL signals in the injection dikes may have beenreset during liquefaction and that OSL may be used todate earthquake-induced liquefaction features directly.However, a similar study by Thomas et al. (2007c) inNE India has produced indistinguishable quartz OSL

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Fig. 8. Locations of OSL samples collected from fault-scarp colluvial wedges adjacent to a fault that cuts across an alluvial fan in the Dead SeaTransform, Israel (Porat et al. 2008). OSL samples were collected from proximal, medial and distal colluvial wedges to determine relationshipsbetween bleaching and distance from the fault scarp. Samples were analysed for quartz and feldspar using large aliquots, small aliquots andsingle-grain analysis. Results are presented in Table 1. Arabic numerals refer to colluvial wedges and Roman numerals to deposits in the faultedalluvial fan (numbered from oldest to youngest). Modified from Porat et al. (2008).

Table 1. OSL ages from colluvial wedges in Trench-18, Dead Sea Transform, from Porat et al. (2008).

Sample no. and location Feldspar IRSL ages (kyr) Quartz OSL ages (kyr)

Large aliquot SAAD Small aliquot SAR Large aliquot SAR Single-grain SAR

Mean Youngest Mean Youngest MAM Mean Youngest Mean MAM

Distant colluvial wedge5 Upper wedge (X) 3.6�1.3 1.5�0.2 2.6�2.0 0.57�0.04 3.2�2.6 (34) 0.83�0.206 Lower wedge (VII) 3.6�1.3 2.0�0.2 2.1�1.5 0.7�0.1 0.82�0.10 5.2�4.4 1.6�0.10 3.0�2.7 (72) 0.64�0.11

Medial colluvial wedge7 Lowest colluvium 4.2�1.4 2.4�0.3 4.8�3.25 1.4�0.1 2.8�2.3 (30) 1.3�0.2

Proximal colluvial wedge11 Upper wedge (IX) 16.7�2.3 14.2�1.2 12.8�4.4 7.9�0.3 20�25 (35) 0.83�0.2610 Middle wedge (VIII) 10.9�1.4 10.0�0.4 9.2�8.2 1.3�0.1 1.8�0.35 8.3�3.5 4.6�0.6 8.7�11.8 (26) 0.96�0.389 Lowest wedge (VII) 4.5�0.8 3.8�0.4 4.3�2.9 1.8�0.1 2.2�1.6 (23) 0.53�0.11

Mean is the age calculated from the average of all aliquots measured. Youngest is the age calculated from the lowest measured De.

MAM=minimum age model of Galbraith et al. (1999). Numbers of grains included in single-grain age estimates are given in parentheses. See

Fig. 8 for sample locations.

624 Tammy M. Rittenour BOREAS

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ages between injection dikes and their source sediment,suggesting that further research into the applicability ofOSL for dating liquefaction is needed.

Additional age constraint on the timing of liquefac-tion and seismic activity may be obtained by OSL dat-ing sand blows formed by the surface rupture ofliquefaction features and injection dikes. Thomas et al.(2007c) used thin sampling tubes to collect the upper1.5 cm of sediment from a sand blow deposit, hoping tocollect the sediment exposed to sunlight during the de-position of the sand blow, but prior to subsequentfloodplain deposition. Results were scattered suggest-ing that non-bleached sediments were collected and thepossible influence of bioturbation. Future samplingstrategies have been proposed including careful mm-scale excavation of the upper sediment from sand blows(Thomas et al. 2007c). Cox et al. (2007) applied a dif-ferent approach to dating sand blows from the lowerMississippi valley, USA. Instead of sampling the sandblow directly, they collected fine-grained samples fromburied soils and sediment layers underlying the targetsand blows. For the most part, their multiple aliquotIRSL results fit with the radiocarbon ages obtained fromthe underlying deposits and within the sand blows, withsome evidence of partial bleaching resulting from thepresence of reworked older sedimentary grains.

Summary. – OSL dating has great potential forpalaeoseismic reconstruction owing to its versatility todirectly sample targeted features and deposits. OSLsamples from offset or deformed fluvial terraces andalluvial fans provide critical age control for slip-ratecalculations. Dating proximal settings such as fault-scarp colluvium and sand blows is more challenging dueto partial bleaching, but may provide more detailed in-formation of recurrence intervals. New advances in OSLdating techniques (Murray & Wintle 2000), single-graindating (Duller et al. 1999; B�tter-Jensen et al. 2000;Duller 2000) and statistical analyses of De results (e.g.Galbraith et al. 1999; Galbraith 2005) have improvedthe accuracy of OSL dating and have allowed newapplications of OSL dating to palaeoseismic studies.

Archaeological applications

Rivers, lakes and other water sources have always beenimportant human resources and the focal points of pastcultures and occupation sites. As such, archaeologicalsites are commonly associated with, and interleavedwithin, fluvial deposits. Traditionally, archaeologicalsites and occupation horizons have been dated withradiocarbon, commonly from charcoal or wood. Whileradiocarbon ages have been instrumental in placing ar-chaeological features and artefacts in a chronologicalframework, there are several caveats that limit their use.For example, radiocarbon ages may not provide the

desired age of occupation due to reuse of materials orreworking of detrital charcoal and wood, which iscommon in fluvial settings. Radiocarbon dating is fur-ther limited by uncertainties in calibration to calendaryears and is constrained to the last �40 kyr. For thesereasons, luminescence dating may be preferable in somecases and has been increasingly applied to archae-ological settings.

There has been a long-standing connection betweenluminescence dating and archaeological research.Thermoluminescence dating has been the keystonetechnique for dating fired pottery (e.g. Zimmerman1971; Aitken, 1985), with more recent applications ofOSL dating of pottery (see reviews by Roberts 1997;Feathers 2003; Wintle 2008b). Additionally, OSL dat-ing has been applied to sediments associated witharchaeological sites for geoarchaeological and environ-mental studies (e.g. Folz et al. 2001; Sommerville et al.2001; Feathers 2003; Gibling et al. 2008).

Luminescence techniques have been particularlyuseful for dating sites older than 40 kyr (e.g. Bowleret al. 2003; Grine et al. 2007; Mercier et al. 2007), andsites associated with initial colonization of Australia(e.g. Cupper & Duncan 2006; Olley et al. 2006; Davidet al. 2007; Prescott et al. 2007) and the Americas (e.g.Feathers et al. 2006; Gonzalez et al. 2006). The focus ofthis article is on the application of OSL dating to fluvialdeposits, but it should be noted that there are manyapplications of OSL dating that are unique to archae-ological studies. These include dating fired sedimentsand rocks associated with hearths (Tribolo et al. 2003;Lamothe 2004; Lian & Brooks 2004; Fanning et al.2008), single-grain dating mud wasp nests associatedwith rock art (Roberts et al. 1997; Yoshida et al. 2003),single-grain dating grave infills to determine age of hu-man burials (Olley et al. 2006), dating sediment ce-mented within late Pleistocene human remains (Grineet al. 2007), and dating brick and mortar to determinethe timing of building construction (Bailiff & Holland2000; Jain et al. 2004b; Vieillevigne et al. 2006).

Dating Palaeolithic sites. – Palaeolithic archaeologicalsites provide important information about the evolu-tion and dispersal routes of Neanderthal and modernhumans. While late Upper Palaeolithic sites(�40–10 kyr) may be dated with radiocarbon, MiddlePalaeolithic and older Upper Palaeolithic sites are nearor beyond the applicable limit for radiocarbon datingand are associated with large calibration uncertaintiesand multiple calibration curves available for this inter-val (e.g. Kitagawa & van der Plicht 1998; Hughen et al.2004; Fairbanks et al. 2005). For these reasons, OSLdating has been increasingly used to provide age con-trol at a number of Palaeolithic sites. Many importantPalaeolithic sites in rock shelters and non-fluvial set-tings have been dated with OSL (e.g. Bowler et al. 2003;Cupper & Duncan 2006; Olley et al. 2006; Rhodes et al.

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2006; David et al. 2007; Mercier et al. 2007; Prescottet al. 2007). Applications of OSL dating to Palaeolithicsites found along river terraces in Russia and India arediscussed here.

The Kostenki Palaeolithic sites, found on the lowterraces of the Don River in westernmost Russia, havebeen the focus of archaeological research since the in-itial discovery of stone artifacts and mammoth bones inthe late 1800s (see Hoffecker et al. 2002, 2004 and re-ferences therein). Initial age control was obtained fromstratigraphic relationships and radiocarbon ages frombone. More recently, Holliday et al. (2007; see also Si-nitsyn & Hoffecker 2006; Anikovich et al. 2007) havedeveloped a more detailed chronostratigraphy of thelocality from fine-grained MA IRSL ages and radio-carbon dating of charcoal (Fig. 9). Additional age con-trol was obtained from identification of the CampanianIgnimbrite Y5 tephra (�40 kyr) and palaeomagneticcorrelation to the Laschamp Excursion (39–45 kyr).Luminescence ages are consistent with the other agecontrol and provide the most reliable ages for the oldestcultural horizons and lowest part of the section.

In a similar study, Gibling et al. (2008) used quartzOSL and radiocarbon dating to provide age control forarchaeological sites from river terraces along the BelanRiver in India. Terrace deposits containing MiddlePalaeolithic artifacts were dated to between 85�11kyrand 72�8kyr and stratigraphically younger aeolian andfluvial channel fills were OSL dated to 13–8kyr. Theseyounger ages are consistent with radiocarbon results andcorrelate with strata containing Neolithic artifacts.

Irrigation canals. – In addition to providing age con-straints beyond the limit of radiocarbon, OSL datingmay, in some cases, provide improved age control inyoung sediments, where there are greater radiocarboncalibration uncertainties and reworking of older organicmaterial is common. Examples of the application of OSLdating to young canal sediments are given below.

Canal networks on the Mekong Delta in southernCambodia have been investigated to determine the uti-lity of OSL dating to date channel use and infilling(Sanderson et al. 2003, 2007; Bishop et al. 2004). Al-though underwater bleaching experiments and subaqu-eous spectral measurements suggest reduced bleachingefficiency in canal settings with high suspended sedimentloads (Sanderson et al. 2007), many quartz OSL ages areconsistent with radiocarbon ages (Sanderson et al. 2003;Bishop et al. 2004). Age overestimates from some sam-ples are interpreted to be due to incorporation of non-bleached grains in multi-grain aliquots. Smaller aliquotsizes or single-grain dating may reduce these problems.

In the American southwest, Berger et al. (2004)examined irrigation canals near Phoenix, Arizona.Samples were collected and analysed for fine-grainedMA IRSL, SAR IRSL and post-IR SAR (analysis ofquartz signal). Results indicate that some sampleswere incompletely zeroed at deposition. However,as with the samples from canals on the MekongDelta, these outliers were easily identified within thestratigraphy and the age range of canal use could bedetermined.

Summary. – OSL dating can provide important agecontrol for fluvial sediments associated with archae-ological sites. While charcoal and other material forradiocarbon dating may be common within culturalfeatures, OSL samples can be collected from horizonsthat lack suitable material for radiocarbon dating andcan provide invaluable environmental informationabout the timing and rate of deposition between cul-tural horizons. Additionally, OSL ages do not need tobe calibrated, reducing age uncertainties. The larger agerange of OSL dating makes this technique particularlyuseful for Palaeolithic sites that are older than or nearthe limit for radiocarbon dating. In addition, OSL dat-ing is important for geoarchaeological investigationsthat relate people to their environment by dating

Fig. 9. IRSL, radiocarbon and other age con-trol obtained for the Kostenki Upper Palaeo-lithic site 12, east wall, along the Don River inwestern Russia. Luminescence dating is espe-cially useful in dating Palaeolithic sites such asthis due to their antiquity (near the upper limitsfor radiocarbon) and the abundant and well-suited target material for luminescence dating inthe fluvial sediments associated with the culturalhorizons. Modified from Anikovich et al. (2007)and Holliday et al. (2007).

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sediments and non-cultural features and landformsassociated with occupation sites.

Conclusions

The study of fluvial deposits and landforms is im-portant for many subdisciplines of geomorphology,palaeoseismology and geoarchaeology. While early TLand OSL applications to fluvial deposits proved diffi-cult due to the incorporation of non-bleached signalswithin the age calculations, recent advances in OSLdating techniques, such as the development of the sin-gle-aliquot regenerative-dose (SAR) method (Murray& Wintle 2000), single-grain dating capabilities (Dulleret al. 1999; Duller 2000; B�tter-Jensen et al. 2000) andstatistical methods for De analysis (e.g. Galbraith et al.1999; Galbraith 2005), have allowed reliable dating offluvial deposits. Target materials for OSL dating (sandsand silts) are nearly ubiquitous in most fluvial depositsand the age range for OSL spans the last glacial–interglacial cycle, with older ages possible in some set-tings. Moreover, fluvial deposits can provide importantarchives of past changes in climate, base level and tec-tonics and commonly contain archaeological horizons.For these reasons, the application of OSL dating tofluvial deposits can provide important contributions tothe geomorphologic, sedimentologic, palaeoseismicand archaeologic research communities.

Acknowledgements. – I thank M. Jain and J. Wallinga for theirhelpful reviews of this manuscript and P. R. Hanson for providing themulti-grain and single-grain data for Fig. 1.

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Appendix Table 1. Quartz SAR OSL and independent age data and references for Fig. 2 in text. Updated from Murray & Olley (2002).

Sediment type Aliquot and grain size OSL age (kyr)� n Independent age (kyr)� Reference

Fluvial s,c 11�5 yr 1 10 yr Jain et al. (2004a)n=61 s,c 29�15 yr 1 42 yr Murray & Olley (2002)��

sg 40�15 yr 1 55 yr Olley et al. (2004a)s,c 67�5 yr 1 70 yr Olley et al. (1998)sg 70�8 yr 1 63�8 yr Murray & Olley (2002)��

sg 70�15 yr 1 55–125 yr Olley et al. (2004a)sg 110�15 yr 1 120–160 yr Olley et al. (2004a)sg 140�20 yr 1 120–160 yr Olley et al. (2004a)l,c 164�13 yr 1 150 yr Thomas et al. (2007b)sg 170�20 yr 1 128�10 yr Murray & Olley (2002)��

l,c 197�16 yr 1 150 yr Thomas et al. (2007b)sg 290�30 yr 1 230�147 DeLong & Arnold (2007)sg 350�90 yr 1 460�92 DeLong & Arnold (2007)l,c 380�40 yr 1 360–500 yr Lang & Mauz (2006)sg 430�110 yr 1 550�98 DeLong & Arnold (2007)l,c 432�43 yr 1 507�40 yr Thomas et al. (2007b)s,c 0.66�0.03 1 0.35–0.53 Rodnight et al. (2006)l,c 0.69�0.06 1 360–500 yr Lang & Mauz (2006)sg 0.7�0.05 1 0.74�0.11 DeLong & Arnold (2007)l,c 0.74�0.07 1 0.51�0.04 Thomas et al. (2007b)s,c 0.92�0.10 1 0.3 Wallinga et al. (2001)l,c 0.99�0.07 1 0.7–0.8 Lang & Mauz (2006)sg 0.99�0.08 1 0.61�0.07 DeLong & Arnold (2007)s,c 1.07�0.06 1 1.01–1.11 Rodnight et al. (2006)sg 1.17�0.09 1 1.09�.11 DeLong & Arnold (2007)sg 1.21�0.12 1 1.64�.09 DeLong & Arnold (2007)sg 1.23�0.09 1 1.65�0.15 DeLong & Arnold (2007)s,c 1.23�0.1 1 0.7–2.4 Wallinga et al. (2001)l,c 1.29�0.17 1 0.3–0.5 Lang & Mauz (2006)l,c 1.3�0.19 1 0.84–1.0 Lang & Mauz (2006)l,c 1.31�0.06 1 0.84–1.0 Lang & Mauz (2006)l,c 1.38�0.24 1 1.0–1.3 Lang & Mauz (2006)sg 1.55�0.3 1 1.42–1.59 Olley et al. (2004a)s,c 1.75�0.1 1 0.7–2.4 Wallinga et al. (2001)l,c 2.87�0.32 1 1.0–1.3 Lang & Mauz (2006)sg 2.9�0.37 1 3.34–3.47 Olley et al. (2004a)s,c 4.6�0.27 1 3.90–4.04 Rodnight et al. (2006)l,c 4.8�0.6 1 1.0–1.3 Lang & Mauz (2006)s,c 5.1�0.4 1 5.2–6.0 Wallinga et al. (2001)s,c 6.1�0.5 1 5.2–6.0 Wallinga et al. (2001)s,c 6.9�0.4 1 7.7�0.1 Busschers et al. (2007)l,c 9.0�0.6 2 12�0.3 Strickertsson & Murray (1999)l,c 9.1�0.4 1 11.2�0.1 Chen et al. (2003)l,c 9.3�0.5 1 12.3�0.3 Chen et al. (2003)l,c 10�0.4 1 12.6�0.1 Chen et al. (2003)l,c 12.6�0.7 1 13.8�0.3 Chen et al. (2003)l,c 13.1�0.6 1 12.6�0.2 Chen et al. (2003)s,c 13.3�0.8 1 13.0–13.3 Wallinga et al. (2001)l,c 13.5�0.9 1 10.7�0.4 Chen et al. (2003)l,c 13.6�1.1 1 14.3�0.1 Strickertsson & Murray (1999)l,c 13.6�1.0 1 13.9�0.5 Murray & Olley (2002)���

l,c 13.7�1.1 1 11.1�0.3 Larsen et al. (1999)l,c 13.8�0.9 1 14�0.5 Murray & Olley (2002)���

s,c 19.7�1.0 1 19.75�0.65 Rittenour et al. (2005)l,c 22.6�3 1 21.3�2.4 Rittenour & Sharp (2007)sg 25.4�2.02 1 21.74�0.54 DeLong & Arnold (2007)s,c 41�2 1 38�1 Busschers et al. (2007)l,c 41.7�1.6 1 43.4�0.4 Chen et al. (2003)s,c 55�9 1 49.8�4 Roberts et al. (2001)l,c 55.6�1.3 1 58�2 Tanaka et al. (2001)l,c 207�14 10 198�7 Murray et al. (2008)

Aeolian l,c 7.4�1.4 yr 3 15�5 yr Nielsen et al. (2006)n=43 l,c 14�2 yr 2 20�3 yr Ballarini et al. (2003)

l,c 16�2 yr 1 32�7 yr Forman et al. (2006)l,c 17�2 yr 5 14�7 yr Madsen et al. (2007b)

BOREAS Luminescence dating of fluvial deposits 633

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Appendix Table 1 (continued)

Sediment type Aliquot and grain size OSL age (kyr)� n Independent age (kyr)� Reference

l,c 19�1 yr 1 31�5 yr Ballarini et al. (2003)l,c 22�3 yr 6 47�9 yr Madsen et al. (2007b)l,c 25�2 yr 1 23�8 yr Ballarini et al. (2003)l,c 26.2�1.4 yr 1 70�4 yr Ballarini et al. (2003)l,c 35�9 yr 1 46�7 yr Forman et al. (2006)l,c 36�6 yr 1 51�5 yr Ballarini et al. (2003)l,c 39�2 yr 2 68�16 yr Nielsen et al. (2006)l,c 62�4 yr 1 89�9 yr Ballarini et al. (2003)l,c 70�6 yr 9 95�15 yr Madsen et al. (2007b)l,c 153�9 yr 2 143�2 yr Ballarini et al. (2003)l,c 160�21 yr 3 190�20 yr Nielsen et al. (2006)l,c 163�10 yr 1 186�11 yr Ballarini et al. (2003)l,c 220�12 yr 1 218�5 yr Ballarini et al. (2003)l,c 225�6 yr 6 259�3 yr Ballarini et al. (2003)l,c 235�10 yr 5 284�38 yr Madsen et al. (2007b)l,c 290�020 yr 1 350�30 yr Strickertsson & Murray (1999)l,c 0.5�0.025 2 0.555�0.025 Aagaard et al. (2007)l,c 0.68�0.14 1 0.669 Bailey et al. (2001)l,c 0.71�0.05 1 0.669 Bailey et al. (2001)l,c 0.92�0.04 4 0.87�0.04 Murray & Clemmensen (2001)l,c 2.0�0.2 1 2.00�0.05 Murray & Clemmensen (2001)l,c 2.7�0.3 1 2.81�0.02 Murray & Clemmensen (2001)l,c 4.23�0.1 6 4.31�0.07 Murray & Clemmensen (2001)l,c 11.2�1.3 1 13.155 Hilgers et al. (2001)l,c 12.6�0.7 1 12.0�0.3 Mangerud et al. (1999)l,c 13.00�0.7 3 13.155 Radtke et al. (2001)l,c 13.1�0.9 2 13.45�0.3 Hilgers et al. (2001)l,c 14.6�1.2 1 14.3�0.5 Mangerud et al. (1999)s,c 25.5�1.4 1 28�2 Turney et al. (2001)s,c 44.1�2.1 1 43�2 Turney et al. (2001)s,c 47.1�2.6 1 48�2 Turney et al. (2001)l,f 53�3 1 51�1 Watanuki et al. (2005)l,f 93�10 1 98�9 Watanuki et al. (2005)l,c 114�12 1 125�5 Schokker et al. (2004)l,f 145�12 1 135�15 Watanuki et al. (2005)l,f 215�22 1 170�20 Watanuki et al. (2005)l,f 296�39 1 290�30 Watanuki et al. (2005)l,f 308�36 1 290�70 Watanuki et al. (2005)l,f 311�33 1 290�60 Watanuki et al. (2005)

Marine l,c 7�2 yr 1 11.8�0.8 yr Madsen et al. (2005)n=33 l,c 15�2 yr 1 20.4�1.4 yr Madsen et al. (2005)

l,c 33�3 yr 1 34.2�2.5 yr Madsen et al. (2005)l,c 40�6 yr 1 28�10 yr Madsen et al. (2007a)l,c 49�3 yr 1 48.9�4.2 yr Madsen et al. (2005)l,c 57�3 yr 1 63�6.3 yr Madsen et al. (2005)l,c 68�6 yr 1 70 yr Madsen et al. (2007a)l,c 76�4 yr 1 17.8�7.7 yr Madsen et al. (2005)l,c 77�9 yr 1 73�25 yr Madsen et al. (2007a)l,c 96�14 yr 1 50�18 yr Madsen et al. (2007a)l,c 108�11 yr 1 118�41 yr Madsen et al. (2007a)l,c 123�6 yr 1 88.3�11 yr Madsen et al. (2005)l,c 157�19 yr 1 95�33 yr Madsen et al. (2007a)l,c 167�8 yr 1 127.9�34.8 yr Madsen et al. (2005)sg 1.78�0.29 1 0.79–1.55 Olley et al. (2004b)sg 6.49�0.73 1 4.5–5.56 Olley et al. (2004b)l,f 7.3�0.3 1 7.50�0.09 Stokes et al. (2003)sg 8.6�1.05 1 7.97–8.87 Olley et al. (2004b)l,c 14.9�0.6 3 17.2�0.4 Strickertsson & Murray (1999)l,c 17.3�1.5 1 16.2�0.7 Strickertsson & Murray (1999)sg 17.9�2.5 1 16.06–17.09 Olley et al. (2004b)sg 18.7�3.9 1 21.36–23.24 Olley et al. (2004b)l,f 22.1�0.8 1 20.0�0.12 Stokes et al. (2003)l,c 25.3�1.8 1 24�2 Strickertsson & Murray (1999)sg 31.9�4.3 1 28.2–34.0 Olley et al. (2004b)l,f 36.3�1.4 1 43�2 Stokes et al. (2003)

634 Tammy M. Rittenour BOREAS

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Appendix Table 1 (continued)

Sediment type Aliquot and grain size OSL age (kyr)� n Independent age (kyr)� Reference

sg 51.1�6.5 1 38.4–48.0 Olley et al. (2004b)l,f 66.9�2.8 1 71�4 Stokes et al. (2003)l,c 101�4 4 122�7 Mangerud et al. (1999)l,c 112�2 16 130�2 Murray et al. (2007)l,f 117.2�4.3 1 128�6 Stokes et al. (2003)l,c 119�7 22 129�4 Murray & Funder (2003)l,c 135�8 2 122�7 Sigaard et al. (unpubl.)

Glacial l,f 26�2 1 32�2 Murray & Olley (2002)���

n=6 l,f 28�2 1 27�1 Murray & Olley (2002)���

l,f 29�2 1 32�3 Murray & Olley (2002)���

l,f 29�2 1 30�2 Murray & Olley (2002)���

l,f 30�2 1 33�2 Murray & Olley (2002)���

l,f 30�3 1 33�1 Murray & Olley (2002)���

�Ageso500 years reported in years (yr) not kyr. ��Originally unpublished data from Olley & Hancock. ���Originally unpublished data from

Houmark-Nielsen.

Aliquot size: l= large aliquot, s= small aliquot, sg=single grain.

Grain size: c=sand, f= silt.

n=number of ages making up reported OSL age.

BOREAS Luminescence dating of fluvial deposits 635