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The Sheraton Centre Toronto Hotel 223rd ECS Meeting l May 12-16, 2013 l Toronto, ON, Canada

Special Meeting Section

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223rd ECS Meeting

May 12-16, 2013 l Toronto, ON, Canada

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18 TheElectrochemicalSocietyInterface•Spring2013

Featured SpeakersPlenary SeSSion and The eCS leCTure

The Frontier of Electronics Researchby Michael Mayberry

Monday, May 131700hGrand Ballroom East

The current era of semiconductor researchis heavily dependent on the incorporation ofnew materials into structures measured innanometers. For the next decade, these trendsare expected to continue and will suffice to

improve the traditional metrics of performance-power and costs.Neverthelessthereareinflectionpointscoming,bothfortechnologyand for products, which will require advanced research to deliversolutions in time. Traditional computation is morphing and noveltechnologiesunderinvestigationwillrequireamoreinterdisciplinaryapproach.Therearemanychoicestobemadebutarichfutureliesaheadofus.

MiChael C. Mayberry is Director of Components Research,which is the research arm for the Technology andManufacturingGroupofIntel.Heisresponsibleforongoingresearchtoenablefutureprocess options for Intel’s technology development organizations.This scope includes internal research, external university research,andotherexternalcollaborations.

Since joining Intel in 1984 as a process integration engineer,Mayberryhasheldavarietyofpositions.Aspartof theCaliforniaTechnologyDevelopment team, he developed EPROM, flash, and

logic wafer fabrication processes. In 1994 he moved to Sort TestTechnologyDevelopment,mostrecentlyasDirector,responsibleforroadmapsanddevelopmentoftestprocessesforIntelmicroprocessors.In2005,hemovedtoComponentsResearch.

Mayberry received his PhD in physical chemistry from theUniversityofCalifornia,Berkeleyin1983andhisBachelor’sdegreeinchemistryandmathematicsfromMidlandCollegein1978.

2013 eCS Gordon e. Moore Medal for ouTSTandinG aChieveMenT in

Solid STaTe SCienCe and TeChnoloGy award leCTure

Wide Bandgap Semiconductors for Sensing Applications

by Fan Ren

Monday, May 131400hGrand Ballroom East

The biosensor market is forecasted to reach$4.4 billion by 2014 in the U.S. This growthwillbesustainedespeciallybyahighdemandfor biosensors that can be used for medicalapplications such as glucose monitoring,

biomarkerdetectionforinfectiousdiseases,andcancerdiagnosis.Inaddition,therewillbestrongdemandforbiosensorswithapplicationsinbiodefense,environmentalmonitoring,food,andpharmaceuticalindustries.Thereiscurrentlygreatinterestindevelopingsensorsthatcouldbeusedinpoint-of-careapplicationsoron-fieldmeasurementstoreducemedicalcostsandemergencyroomvisits.Transistorbasedsensors are promising for these applications. These sensors need

Welcome to Toronto!Wearepleasedtobebackinthisexcitingcityforthe223rdECSMeeting.Thismajorinternational conferencewill be held at the Sheraton CentreTorontoHotel andwill include 45 topicalsymposiaconsistingof1,514technicalpresentations.Youareinvitedtoparticipateinthetechnicalprogramaswellasmanyothersocialeventsplannedforthemeeting.

223rd ECS Meeting

May 12-16, 2013 l Toronto, ON, Canada

TheElectrochemicalSocietyInterface•Spring2013 19

to have high precision, compact size, fast response time, and besensitivetosmallamountsofbiologicalmaterial.

Semiconductor properties include current, potential, andimpedance characteristics that can be used to directly measurechemical or physical stimuli on the semiconductor surface. Thewideenergybandgapsemiconductorgalliumnitride(GaN)materialsystem is attracting much interest for commercial applications ofgreen,blue,andUV lightemittingdiodes (LEDs), laserdiodes,aswell as high speed and high frequency power devices.Due to thewide-bandgapnatureofthematerial(3.2eVforGaNascomparedto1.12eVforSi),itisverythermallystable,andelectronicdevicescanbeoperatedattemperaturesupto500ºC.TheGaNbasedmaterialsarealsochemicallystable,andnoknownwetchemicaletchantcanetch these materials; this makes them very suitable for operationin chemically harsh environments.GaNbased sensors for gas andchemicaldetectionaswellasmedicalapplicationswillbepresented.

fan ren receivedaBSdegree in appliedchemistry fromFengChiaUniversityin1975;anMSdegreeinchemicalengineeringfromNationalChengKungUniversityin1978,anMSdegreeinpolymerscience and engineering, and a PhD in inorganic chemistry fromBrooklynPolytechnic in1991.He joined theUniversityofFlorida(UF)in1998whereheisaDistinguishedProfessorintheDepartmentof Chemical Engineering and an ExxonMobil Gator ChemicalEngineeringAlumniChairProfessor.PriortojoiningUF,RenworkedatBellLabswherehewasakeyfigure indevelopingGaAsmetalsemiconductor field effect transistors grown on silicon substrate,carbon-doped InGaP/GaAs heterojunction bipolar transistors, andenhancementmodeGaAs and InGaAsmetal oxide semiconductor(MOS)fieldeffecttransistors.AtUF,Dr.Renhasprimarilyfocusedon fabrication processes for high breakdown voltage GaN basedSchottky and MOS diodes, as well asAlGaN/GaN high electronmobilitytransistorbasedsensors.

Dr.Ren’spublicationshavebeencitedover13,500 times in theliterature.HeisaFellowofECS,APS,AVS,IEEE,MRS,andSPIE.He is the co-authorofmore than820 journalpublications andco-inventorof31issuedpatents.Hereceivedthe2008ElectronicsandPhotonicsDivisionAwardfromECS,the2010AlbertNerkenAwardfromAVS,andthe2010NASATechBriefInitialAward.

Short Courses and WorkshopsFourShortCourseswill be offered inToronto.These courseswillbe held on Sunday, May 12, 2013, from 0900h to 1630h. TheregistrationfeefortheShortCoursesis$425forECSMembersand$520fornonmembers.Studentsareoffereda50%discount:$212.50forECSStudentMembersand$260forNonmemberStudents.Theregistration fee for the course covers the course, text materials,continentalbreakfast,luncheon,andrefreshmentbreaks;it does not cover the meeting registration,anditisnotapplicabletoanyotheractivitiesofthemeeting.

The deadline for registration for a course is April 12, 2013. Pre-registration is required for the Short Courses. YoumayregisterusingtheEarly-BirdRegistrationFormontheECSwebsite.Writtenrequests forShortCourse refundswillbehonoredonly if receivedatECSheadquartersbyApril19,2013.Allrefundsaresubjecttoa10%processingfeeandrequestsforrefundsmustbemadeinwritingand e-mailed to, [email protected]. Refunds willnotbeprocesseduntilAFTERthemeeting.Allcoursesaresubjecttocancellationpendinganappropriatenumberofadvanceregistrants.Before making any flight or hotel reservations, please check to make sure the course is running!

Visit the ECS website for full course descriptions and instructor biographies.

Short CourSe #1Basic Impedance SpectroscopyMark E Orazem, Instructor

Thiscourseisintendedforchemists,physicists,materialsscientists,andengineerswithaninterestinapplyingelectrochemicalimpedancetechniquestostudyabroadvarietyofelectrochemicalprocesses.Theattendee will develop a basic understanding of the technique, thesourcesoferrorsinimpedancemeasurements,themannerinwhichexperimentscanbeoptimizedtoreducetheseerrors,andtheuseofgraphicalmethodstointerpretmeasurementsintermsofmeaningfulphysicalproperties.Thetopicstobecoveredinclude:

1. Themotivationforusingimpedancespectroscopyadvantagesascomparedtoothertransienttechniquesandtheconditionsunderwhichitsuseisideallysuited,

2. Thebasicconceptsofhowimpedanceismeasured,3. Properselectionofexperimentalparameters,4. Graphicalrepresentationofimpedancedata,including

methodstoextractsomephysicallymeaningfulparameters,5. Constant-phaseelements,6. Applicationofelectricalcircuitanalogues,and7. ThemeaningoftheKramers-Kronigrelations.

Short CourSe #2Advanced Microscopy Methods for Studying PEM Fuel Cell MaterialsKarren L. More, Instructor

The μm- to sub-Å-scale structural and chemical characterizationoffuelcellmaterialconstituentsviaadvancedelectronmicroscopytechniquesplaysanintegralroleinelucidatingthecriticalmaterial’sdegradationmechanismscontributingtofuelcellperformanceloss.Suchtechniquesincludeatomic-scaleimagingviaaberration-correctedscanningtransmissionelectronmicroscopy(STEM)coupledwiththeabilitytoresolvecompositional/chemicalchangesattheatomicscaleusingenergydispersivespectroscopy(EDS)and/orelectronenergylossspectroscopy(EELS).Recently,thedevelopmentofspecializedholders forconductingnovel in situmicroscopyexperiments(suchasliquidSTEM,electrochemistry,gas-flowreactions,biasing,etc.)combined with high-resolution imaging and microanalysis hasenhancedtheabilitytostudycriticalstructuralchangestoindividualmaterials constituents comprising fuel cell membrane electrodeassembliesunderrelevantenvironmentalconditions.

The primarymicroscopy and spectroscopy techniques availabletoday,whichareusedtostudyfuelcellmaterials,willbesummarizedand described in detail. Advanced methodologies for quantifyingcritical structural changes related to particular fuel cell testingprotocols and materials degradation phenomena will be describedand are supported with specific materials-specific characterizationstudies.

Short CourSe #3Fundamentals of Electrochemistry: Basic Theory and Thermodynamic MethodsJamie Noël, Instructor

Thiscoursecoversthebasictheoryandapplicationofelectrochemicalscience. It is targeted toward people with a physical sciences orengineeringbackgroundwhohavenotbeentrainedaselectrochemists,butwhowanttoaddelectrochemicalmethodstotheirrepertoireofresearch approaches. There are many fields in which researchersoriginally approach their work from another discipline but then


discoverthatitwouldbeadvantageoustounderstandandusesomeelectrochemicalmethodstocomplementtheworkthattheyaredoing.Thetopicstobecoveredinclude:

1. IntroductionandOverviewofElectrodeProcesses2. Chemicalvs.ElectrochemicalThermodynamics

• referenceelectrodes,standardpotentials,cellpotentials,Nernstequations,electrode-solutioninterfaces,anddouble-layerstructures

• ion-selectiveelectrodes,applicationsinanalyticalelectrochemistryandsensors,aqueousandnon-aqueoussystems

3. ChemicalStoichiometryvs.Faraday’sLaw

• coulometry,bulkelectrolysis4. TheoreticalBasisforMethods

• surfacetension,adsorptionandadsorptionisotherms,electrocapillarity,potentialofzerocharge,Lippmannequations

5. Methodology

• potentiometry,differentialcapacity,coulometry,cyclicvoltammetry,polarography

6. ElectrochemicalInstrumentation

• voltmeters,ammeters,potentiostats,galvanostats,designofelectrochemicalcells

7. CoupledCharacterizationMethods(timepermitting)

• modifiedelectrodes,spectroelectrochemistry,in situneutronscattering,surfaceanalysis,etc.

Short CourSe #4Atomic Force Microscopy for Energy Research Applications & ElectrochemistryKeith Jones, Instructor

Thiscourseisintendedforchemists,physicists,andmaterialsscientiststhatwanttounderstandhowAtomicForceMicroscopy(AFM)canbeusedtocharacterizematerialsandtoprobeelectrochemicalprocessesand ionic transport in solids for a broad range of applications forenergygenerationandstoragerangingfrombatteriestofuelcells.AnewtechniquecalledElectrochemicalStrainMicroscopy(ESM)willbeintroduced.ESM,developedbyOakRidgeNationalLaboratory,isaninnovativenewAFM/SPMtechniquethatiscapableofprobingelectrochemical reactivityand ionicflows insolidson thesub-ten-nanometerlevel.Studentswilllearnthesciencebehindthetechnique,how it works, and the advantages of this technique over othermethods. Current ESM results will also be presented and generalAFMtipsandtricksforelectrochemistryapplications.

• IntroductiontoAFM• Instrumentationandscanningmodes• Challengesinbattery/energyresearchcharacterization• IntroductiontotheESMtechnique

• Advantagesofthetechniqueoverothers• Currentresearchandimageexamples• TipsandtricksforAFMelectrochemistrymeasurements

ProfeSSional DeveloPment WorkShoPS

The following are available at no additional cost; but space is limited, so please arrive early!

John R. Susko, Instructor

SeveralkeyprofessionaldevelopmentworkshopswillbepresentedMay13-15,2013.Theseimportantworkshopswillprovideattendeeswithup-to-date informationon enhancing career opportunities andgrowth and are a great lead into theCareer Fair.The professionaldevelopment workshops are open to all registered attendees at noadditionalcost.

Professional Development Series – Essential Elements for Employ-ment Success:Landingyournextjobrequiresselectiveandeffectivenetworking,developingandsubmittingspecificallytargetedresumesandcover letters, locating relevant jobopportunitiesandpreparingforandparticipatinginthejobinterview.Thisworkshopwillprovideup-to-dateinformationandtipsforemploymentsuccess.

Monday......................... 1230-1430hTuesday........................ 1230-1430h

Professional Development Series – Résumé Review:Atalossforwords?Bringyourrésuméforaone-on-onesessionwithanindustryleaderandexpertonrésumédevelopment.Youwillwalkawaywitharésuméthatissuretolandyouyournextinterview.

Tuesday........................ 0800-1200hWednesday.................... 0800-1200h

eCS Career fair

SponsoredbyRedcat™,theECSCareerFair isagreatwaytoconnectwithpotentialemployeesatevery levelofexperience—fromveterans in thescience to newcomers entering research,development, and academia—and one of themosteffectivewaystorecruitqualifiedcandidatesfromthe223rdECSMeeting.

With the purchase of any exhibit booth, your organizationautomaticallyhas theopportunity toparticipate in theECSCareerFair. Career Fair participants will receive two customized Career

Fair booth signs, additionaladvertisingontheECSwebsite,andalistinginthemeetingprogramandour newly-designed mobile app.Plus,yourorganizationwillreceiveone free job posting on RedcatTM(redcatresearch.org), the online

communitycreatedforeveryoneinelectrochemistryandsolidstatescience and technology. ECSwill also have a Career Fair Board,locatedintheexhibithall,whereyoucanpostavailablejobsonsiteonacomplimentarybasis.

TheCareer Fairwill take place duringExhibit hours,Tuesday-Thursdayduringthemeeting.

Pre-registrationbyexhibitorsisrequiredtoparticipateintheECSCareerFair—spaceislimited.FormoreinformationabouthowyourorganizationcantakeadvantageoftheseopportunitiespleasecontactDavidHarkness at [email protected] or visit http://www.electrochem.org/meetings/career_fair/.TheCareerFairisopentoallattendees.


Award WinnersNOTE: For complete biographies of the award recipients, and the schedule of their presentations, please see the General Meeting Program on the ECS website: www.electrochem.org/meetings/biannual/223/223.htm.

Dielectric Science & Technology Division Thomas D. Callinan Award

and theElectronics and Photonics Division Award

durGaMadhab (durGa) MiSra, professor andAssociateChair forGraduatePrograms in theDepartment of Electrical and ComputerEngineeringatNewJerseyInstofTechnology(NJIT),hascontributedsignificantlytoresearchinlowpowerMOSFETs,especiallyinthefieldofgatedielectricreliability.Hisrecentworkonhigh-k gate stack reliability, especially thecontributionofvariouslayerstotheentiregate

stackbreakdown, receivedconsiderable recognition.He is anECSFellow.

Dr. Misra has edited and co-edited more than 30 books andconference proceedings, authored more than 250 publications inpeer-reviewed journals and international conference proceedings,anddeliveredmore than30 invited talksworldwide.He served asanAssociateEditorofIEEE Circuits and Devices MagazineandontheadvisoryboardsofInterfacemagazineandECS Transactions.Heis on the program committee ofmany nanoelectronic conferencesandservedastrackchairoftheICTechnologyDivisionoftheIEEEInternationalVLSIDesignConference.HereceivedtheDistinguishedLecturerAward in 2010 from IEEE ElectronDevices Society. HeservedastheDirectorofMicroelectronicsResearchCenteratNJITandasvisitingprofessoratBellLaboratories.

Dr.Misra is also an advisor andmentor tomany graduate andundergraduate students. He has graduated ten PhD students, 40MSstudents,andmorethan50undergraduatestudents.In2005hereceived NJIT’s Excellence in TeachingAward for demonstratingexcellenceintheclassroomandforencouragingandguidingstudentstoworkattheirhighestacademiclevel.

Dr. Misra received his MASc and PhD degrees in electricalengineering from theUniversity ofWaterloo,Canada in 1985 and1988respectively.HealsohasanMTechinsolidstatematerialsfromtheIndianInstituteofTechnology,NewDelhi.

Energy Technology Division Research Award

PioTr Zelenay received his PhD and DSc(“habilitation”) degrees in chemistry fromWarsawUniversity,Warsaw,Poland.Hewasapostdoctoral research fellow at Texas A&MUniversity, College Station (1983-1986), avisiting professor at the University of IllinoisUrbana-Champaign (1988, 1989, 1990-92),University of Alicante, Spain (1994), andColorado State University (1996-1997). Dr.

Zelenay was appointed a faculty member in the Department ofChemistry,WarsawUniversityin1983andremainedattheUniversityuntil1997,whenheacceptedpermanentresearchpositionwithLosAlamosNationalLaboratory(LANL).HehasbeenassociatedwithMaterials Physics and Applications Division (formerly MaterialsScienceandTechnologyDivision)atLosAlamosNationalLaboratoryfor the past 15 years. He is currently a Project Leader and TeamLeader at LANL focusing primarily on fundamental and appliedaspects of polymer electrolyte fuel cell science and technology,electrocatalysis,andelectrodekinetics.

Dr. Zelenay has published more than 100 research articles inrenowned scientific journals, including Nature and Science, co-authorednearly300presentations,ofwhichapproximately100havebeeninvited/keynote/plenarylectures.Tohiscredit,Dr.Zelenayhas16patentsandpatentapplicationsintheareaofpolymerelectrolytefuel cells. Since becoming Project Leader for LANL Fuel CellProgram in 2000,Dr. Zelenay has led numerous research projectsand received more than 20 awards and other recognition.Amongothers,inJune2010,hewasawardedtheDOEHydrogenProgramR&DAward in Recognition of Outstanding Contributions to FuelCellTechnologiesforresearchonnon-preciousmetalelectrocatalystsfor oxygen reduction reaction. Dr. Zelenay is a member of ECS,InternationalSocietyofElectrochemistry,andontheEditorialBoardofElectrocatalysis.

Srinivasan Young Investigator Award of the Energy Technology Division

STefan freunberGer studied chemistry atViennaUniversityofTechnology,Austria.Hisgeneralresearchinterestisfundamentalsciencein electrochemical energy storage andconversion, both with theoretical andexperimentalapproaches.Forhismaster’sandPhD thesis, he moved to the Swiss FederalInstitute ofTechnology (ETH)Zurich and thePaulScherrerInstitute,Switzerland.Thework,

under theguidanceofAlexanderWokaunandFelixBüchi,wasonpolymerelectrolytefuelcells.Toinvestigatetransportprocessesonawide range of relevant scales, he developed advancedmodels andnovel experimental techniques, e.g., the first method to measureresistance and current densitywith sub-mm resolution. Part of themodelingeffortswerecompletedwithNedDjilaliattheUniversityofVictoria,Canada.

Forpostdoctoralwork,hejoinedthegroupofPeterG.Bruce,FRS,attheUniversityofSt.Andrews,Scotland,toworkonfundamentalaspectsof thenonaqueousLiO2battery.For thisworkheearnedaEPSRC early career fellowship. His contributions to this rapidlyevolving field embrace the development of in situ spectroscopictechniques, elucidation of the reactionmechanism, electrocatalysisand the important roleofelectrolyteandelectrodesubstrate.He isauthorofover27peerreviewedpublications,includinginScienceandNature Materials, furthermore fourpatentsand twobookchapters.Hisworkwaspresentedinnumerouslecturesatmajorconferences,many ofwhichwere invited.Dr. Freunberger nowbuilds his ownresearchgroupatGrazUniversityofTechnology,Austria.

Fullerenes, Nanotubes, and Carbon Nanostructures Division

Richard E. Smalley Research Award

naZario MarTínisafullprofessoroforganicchemistry at the University Complutense ofMadrid and Vice-Director of the Institute forAdvanced Studies in Nanoscience of Madrid(IMDEA-Nanoscience). Recently he has beenappointedasDr.h.c.byLaHavanaUniversity.Professor Martín’s research interests span arangeoftargetswithemphasisonthemolecularand supramolecular chemistry of carbon

nanostructuressuchasfullerenes,carbonnanotubes,andgraphenes,π-conjugatedsystemsasmolecularwiresandelectroactivemolecules,in the context of electron transfer processes, photovoltaicsapplications,andnanoscience.Hehaspublishedover420papersinpeerreviewedjournals,givenover260lecturesinscientificmeetingsandresearchinstitutions,andsupervised25theses.Hehasco-editedsixbooksrelatedwithcarbonnanostructuresandhehasbeeninvitedasguest editor for eight special issues inwell-known internationaljournals.

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Professor Martín has been visiting professor at UCSB andUCLA (California, USA) and Angers and Strasbourg (France)universities.Hehas served as amember of theEditorialBoardofChemical Communications, and he has served as General Editorof the Spanish journal Anales de Química (2000-2005) and as amemberoftheInternationalEditorialAdvisoryBoardofThe Journal of Materials Chemistry (2000-2006).He is currently theRegionalEditorforEuropeofthejournalFullerenes, Nanotubes, and Carbon NanostructuresandamemberoftheInternationalAdvisoryBoardofThe Journal of Organic Chemistry (ACS),ChemSusChem (Wiley-VCH), ChemPlusChem (Wiley-VCH), Chemical Society Reviews(RSC), andChemical Communications (RSC).He is amember oftheRoyalAcademyofDoctorsofSpainaswellasaFellowofTheRoyalSocietyofChemistry. In2006-2012hewas thePresidentoftheSpanishRoyalSocietyofChemistry.HewastherecipientoftheDupontPrizeofSciencein2007;andtheGoldMedalandResearchAward in2012, thehighestdistinctiongivenby theSpanishRoyalSociety of Chemistry. He recently received the national Jaime IAwardforBasicResearch2012.HeisthelastchemistdistinguishedwiththeEuCheMSLectureAwardin2012.

Industrial Electrochemistry & Electrochemical Engineering Division New Electrochemical

Technology (NET) Award

UTC Power is a proven leader in designing, manufacturing, anddeploying fuel cells that generate clean and reliable power forbuildingsand transportationapplications.Thecompany,withmorethan50yearsofexperience,isbasedinSouthWindsor,Connecticut,where it conducts research, development, and manufacturing oftransportationandstationaryfuelcells.UTCPoweristheonlyfuelcellcompany in theworld tohaveworkedwithallfivemajor fuelcell technologies and to produce fuel cells for both stationary andtransportationapplications.

AteamofsixengineersfromUTCPowerareawardedthe2012New Electrochemical Technology (NET) award for outstandingwork in electrochemistry and electrochemical engineering that hasenabledfuel-cellpoweredvehiclestoachievecommerciallevelsofreliabilityanddurabilityinreal-worldtransitbusservice.Theteam,withtheassistanceofmanyothersatUTCPower,hassystematicallyidentifiedthephysiochemicalmechanismsthatsubstantiallyimpactthedurabilityofPolymerElectrolyteFuelCells(PEFCs),developedand validated associatedmathematicalmodels and accelerated testprotocols, and successfully implementedmultipledecay-mitigationtechnologies intoUTC Power’s fleet of PEFC-based power plantsin transit bus applications to achieve world-record performance.The fleet leader with the UTC Power designed andmanufacturedPureMotion® 120 fuel cell powerplant has run for over 12,000operating hours in real-world servicewith original cell stacks andno cell replacements. The PureMotion® has also consistentlymaintained90%fleetaverageavailabilityover thepast threeyearswhileconcurrentlyimprovingmilesbetweenroadcallsfrom6,000tomorethan15,000milesontheoriginalfleetofsixbuses.

roberT M. darlinGisanauthorityintheareaofelectrochemicalmodeling.Hehaspublishedover 60 papers and patents in areas rangingfrom basic electrochemical engineering toelectrochemical power sources. Dr. Darling’smodeling work in the area of platinumdissolution and carbon corrosion were keycontributors to understanding transientdurabilityofPEMfuelcells.

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SaThya MoTuPally is the head of fuel cellR&DatUTCPowerandisaworldexpertintheareaoffuelcelldesignandcomponents.Hehaspublishedover50papersandpatentsintheareaof fuel cells and batteries.Dr.Motupallywasresponsible for the development of nextgeneration cell stackmaterials with improveddurabilityandperformance.

TiMoThy w. PaTTerSon is a world expert infailure mode analysis with over 15 years ofexperience in the area of fuel cells.When thealpha design of the PureMotion® 120 wasfailing in less than 2,000 hours,Mr. Pattersonled a Root Cause team that systematicallyidentifiedtheimpactofoperatingconditionsandcomponentdesignondurability.TheresultsofMr. Patterson’s work led to a key piece ofintellectual property critical to the properoperationofPEMfuelcells.

ToM Skiba is a fuel cell component engineerwithover15yearsoffuelcelldesignandtestexperience.Mr.Skibawas responsible for thedevelopment of accelerated test protocols toscreen components for PEM fuel cells. Mr.Skiba’seffortsalso led to theverificationofasuiteofmathematicalmodelsthathaveproveninvaluablefornextgenerationdesigns.

MiChael l. Perryisrenownedforhisworkinthe area of fuel cell degradationmechanisms.Hewasapartof the team thatdiscovered thereverse-currentmechanismduringthestart/stopof transportation fuel cells. Mr. Perry’s workhas ranged from carbon corrosion, platinumdissolution,tocontamination.

MaThew P. wilSon is the lead SystemsEngineeronthePureMotion®seriesofproducts.He was responsible for the incorporation ofseveral durability-advancing technologies intothePureMotion®Model120system.Thecyclicdurability and start/stop system technologiesareakeyreasonfortheworldclassdurabilityoftheUTCPowerbuspowerplant.

Physical and Analytical Division David C. Grahame Award

riChard l. MCCreery is currentlyProfessorof Chemistry at the University of Alberta(UofA), with a joint appointment as a SeniorResearch Officer at the National Institute forNanotechnology (NINT). Until 2006, he wasDowProfessorofChemistryat theOhioStateUniversity. He received his BS in chemistryfromtheUniversityofCalifornia,Riverside,in1970, and PhD under Ralph Adams at the

UniversityofKansas in1974.His research involves spectroscopicprobes of electrochemical processes, the electronic andelectrochemical properties of carbon materials, and carbon-basedmolecularelectronics.Muchofhisresearchinvolvescollaborationswithmaterialsscientistsandengineers,aswellassurfacescientists

Exhibitors as of Press-TimeALS Co., Ltd.

Booth 123Katsunobu [email protected] www.als-japan.com

Asylum Research, an Oxford Instruments company

Booth 121Nushaw [email protected] www.asylumreserach.com

Bio-Logic USA

Booths 133, 134, 135David [email protected] www.bio-logic.us

ECS

Booth [email protected] www.electrochem.org

Gamry Instruments

Booths 130, 131Chris [email protected] www.gamry.com

Ivium Technologies

Booth 117Pete [email protected] www.ivium.us

Maccor, Inc.

Booths 100, 101Mark [email protected] www.maccor.com

Metrohm USA

Booth 122Karen [email protected] www.metrohmusa.com

MTI Corporation

Booth 125Mel [email protected] www.mtixtl.com

Pine Research Instrumentation

Booths 116, 109Jenny [email protected] www.pineinst.com/echem

Princeton Applied Research

Booths 102, 103, 104Ari [email protected] www.princetonappliedresearch.com www.solartronanalytical.com

Redcat

Booth [email protected] www.redcatresearch.org

Scribner Associates, Inc.

Booth 108Jason [email protected] www.scribner.com

and electrochemists. He leads an effort at NINT and UofA toinvestigatehybriddevicesformolecularelectronics,whichcombineexistingCMOS technologywithnewelectronicandoptoelectronicdevices containing active molecular components. McCreery haswrittenover200refereedpublications, includingonebookandtenU.S.patents,withthreeofthoseextendedtoEuropeandJapan.

Europe Section Allesandro Volta Medal

Jean-noël ChaZalvielreceivedhiseducationinsolidstatephysics.In1976,histhesisworkon the “spin-dependent Hall effect” wasawardedthebronzemedaloftheCNRSPhysicsDepartment.AfterapostdocstayatBellLabs,he settled at CNRS-Ecole Polytechnique andswitched to semiconductor electrochemistry.He addressed the ubiquitous surface orinterfacial states, formulating an important

model of electron transfer via surface states. He subsequentlydevelopedin situinfraredspectroscopyandbecamealeadingexpertofusingthistechniqueatsemiconductorelectrodes.

In1989Dr.ChazalvielestablishedthatduringanodicdissolutioninHF, the silicon surface remains hydrogenated and fluoride-free.His subsequent studies of the silicon/fluoride system led him toelaboratingporoussilica.Hiscontributionstothespectacularfieldofporoussiliconincludeadetailedtheoreticalmodeloftheformationofporoussemiconductors.Thesestudiespromptedhimtoundertakesiliconsurfacemodificationbyorganicgrafting.Hewasamongthepioneersofthisdomain,whichhassinceblossomedintoaveryactivefield.

Dr.Chazalvielalsore-addressedtheproblemofthegenerationoframifiedmetal electrodeposits, and formulated amodel explainingthe instability of the deposition, based on an analytical/numericalapproach and providing quantitative predictions subsequentlyverifiedbyexperiment.

Inrecognitionofhisachievements,Dr.Chazalvielwasawardedseveral distinctions: the silver medal of the CNRS ChemistryDepartment (1994), theAncelPrizeof theFrenchPhysicsSociety(1994), and the Ivan Peychès Prize of the French Academy ofSciences(2006).Hiselectrochemicalstudieshavebenefitedfromhisstrongbackgroundinphysicsandoriginalideasthatoftenledhimtodesigningnoveltechniques.

Technical ExhibitThe complimentaryTechnical Session coffee breaks are scheduledonWednesdayandThursdayat0930hintheExhibitHall(Osgoode&SheratonBallroom,LowerConcourseLevel).Gatherwith yourcolleagues,browsethroughexhibits,andchatwithECSCareerFaircompanies.Theexhibitwillfeatureinstruments,materials,systems,publications,andsoftwareofinteresttoattendees.

Exhibit Hours

Tuesday, May 14............................................................ 1300-1600hRe-opening...................................................................... 1800-2000h Includes the General & Student Poster Session

Wednesday, May 15...................................................... 0900-1400hRe-opening...................................................................... 1800-2000h Includes the General Poster Session

Thursday, May 16......................................................... 0900-1400h



A — General Topics

A0 — Special Lectures (M)

A1 — General Student Poster Session (Tu)-Venkat Subramanian, Kalpathy B. Sundaram, and Vimal Chaitanya

A2 — Nanotechnology General Session (M-Tu)-F. Li, O. Leonte, and W. Mustain

B — Batteries, Fuel Cells, and Energy Conversion

B1 — Energy Technology/Battery - Joint General Session(M-Th)-A. Manthiram, A. Manivannan, and Sanjeev Mukerjee

B2 — Battery Electrolytes(W-Th)-F. Alamgir, W. Henderson, R. Jow, V. Thangadurai, Sanjeev Mukerjee, and P. Trulove

B3 — Alkaline Electrochemical Systems for Energy Conversion and Fuel Production(Tu-W)-S. R. Narayanan, Peter Pintauro, Bor Yann Liaw, Vijay Ramani, and P. Kulesza

B4 — Design and Modeling of Battery Materials(Mo-Tu)-J. T. Vaughey, Marina Yakovleva, and Ayakannu Manivannan

B5 — Hydrogen Production, Conversion, and Storage 4 (Tu-W)-Shirley Meng, Bor Yann Liaw, Scott Calabrese Barton, and Gerbrand Ceder

B6 — Stationary and Large Scale Electrical Energy Storage 2(Tu)-E. Fabbri, E. D. DiBartolomeo, F. Chen, and T. Norby SC

B7 — Nanoarchitectures for Energy Storage 1(M-W)-J. Meyers, B. Y. Liaw, and Bob Savinell

B8 — Next Generation of Supercapacitors (M-Tu)-C. Johnson, Candace Chan, P. Atanasov, and Trung Van Nguyen

B9 — Solar Fuels 2 (M-Tu)-Prashant Kumta, Nick Wu, Mani Manivannan, Jeffrey Long, and Wenjing Zhang

C — Biomedical Applications and Organic Electrochemistry

C1 — Innovations and New Directions in Organic Electrochemistry (W-Th)-A. Fry and R. Mantz

D — Corrosion, Passivation, and Anodic Films

D1 — Corrosion General Session (W-Th)-R. S. Lillard

D2 — Corrosion in Nuclear Energy Systems: From Cradle to Grave (M-Tu)- R. S. Lillard, J. Noel, R. Newman, D Shoesmith, and S. Fujimoto

E — Dielectric and Semiconductor Materials, Devices, and Processing

E1 — Bioelectronics, Biointerfaces, and Biomedical Applications 5 (Tu)-D. Cliffel, Z. Aguilar, J. Burgess, A. Hoff, and A. Suroviec

E2 — Graphene, Ge/III-V, and Emerging Materials for Post CMOS Applications 5 (M-W)-D. Misra, S. Albin, Z. Karim, P. Srinivasan, Yaw Obeng, Stefan DeGendt, and Cor Claeys

E3 — Nanocrystal Embedded Dielectrics for Electronic and Photonic Devices (M-W)-P. Mascher, Pooran Joshi, Mark E. Overberg, and Yue Kuo SC

E4 — Organic Semiconductor Materials, Devices, and Processing 4 (M-W)-J. M. Deen, David Gundlach, B. Iniguez, and Hagen Klauk

E5 — Silicon Compatible Materials, Processes, and Technologies for Advanced Integrated Circuits and Emerging Applications 3 (M-Tu)-F. Roozeboom, E. P. Gusev, H. Iwai, S. J. Koester, D.-L. Kwong, M. Z. Ozturk, and P. I. Timans SC

E6 — Advanced Semiconductor-on-Insulator Technology and Related Physics 16 (M-Tu)-Y. Omura, S. Cristoloveanu, F. Gamiz, amd B.-Y. Nguyen SC

E7 — Symposium on Processes at the Semiconductor Solution Interface 5 (W)- Colm O’Dwyer, D. N.Buckley, A. Hillier, and Maria Salazar Villalpando SC

E9 — Wide-Bandgap Semiconductor Materials and Devices 14(Tu)-Z. Mi, J. Bardwell, R.-H. Horng, G. W. Hunter, Z. Karim, C. O’Dwyer, and E. B. Stokes

F — Electrochemical / Chemical Deposition and Etching

F1 — Green Electrodeposition 3 (Tu)-Sudipta Roy, G. Zangari, D. Barkey, and S. Yoshihara

F2 — Novel Design and Electrodeposition Modalitie (W)-E. Podlaha, S. Djokic, and L. Magagnin

G — Electrochemical Synthesis and Engineering

G1 — Advances in Low Temperature Electrolyzer and Fuel Cell Technology: In Honor of Anthony B. (Tony) LaConti (Tu)-John Staser, Cortney Mittelsteadt, Vijay Ramani, Peter Pintauro, and Brian Pivovar

G3 — Electrochemical Engineering for the 21st Century: 3 (W)-James Fenton, Venkat Subramanian, Richard Alkire, H. Deligianni, and John Harb

G4 — Tutorials in Electrochemical Technology: Impedance Spectroscopy (Tu)- Mark Orazem and Vincent Vivier

H — Fullerenes, Nanotubes, and Carbon Nanostructures

H1 — Tutorials in Nanotechnology (Su)-F. D’SouzaH2 — Fullerenes - Chemical Functionalization, Electron Transfer, and Theory

(W-Th)-F. D’Souza, S. Fukuzumi, D. M. Guldi, N. Martin, J. F. Nierengarten, and V. R. Subramanian

H3 — Endofullerenes and Metallofullerenes (Tu-W)-T. Akasaka, A. Balch, and L. Echegoyen

H4 — Carbon Nanotubes-From Fundamental Processes to Devices(M-Th)- S. Doorn, Y. Gogotsi, R. Martel, S. V. Rotkin, R. B. Weisman, and M. Zheng

H5 — Fundamentals of Graphene Related Structures (Tu)-H. Grebel, R. Haddon, and S. V. Rotkin

H6 — Focus Session: Carbon Nanostructures in Energy Applications and Energy Storage (M, W)-D. M. Guldi and Robert Kostecki

H7 — Carbon Nanostructures in Medicine and Biology (Th)-T. Da Ros, Z. Aguilar, A. Hirsch, A. Simonian, and L. Wilson

H8 — Porphyrin and Supramolecular Assemblies (M-W)-K. Kadish, R. Paolesse, and N. Soladie

H9 — Nanostructures for Energy Conversion (W-Th)-H. Imahori and P. V. Kamat

I — Physical and Analytical Electrochemistry

I2 — Computational Chemistry (W-Th)-Steve Paddison

I3 — Ethanol Oxidation (Mo-Th)-Pawel Kulesza and Sanjeev Mukerjee

I4 — Grahame Award Symposium and Physical and Analytical Electrochemistry General Session (M-W)

I5 — Ion Conduction in Polymers (Tu)-Tom Zawodinski, Andrew Herring, and Gao Liu

I6 — State of the Art Tutorial on Membranes and MEAs for Low Temperature Fuel Cells (M)-T. Zawodzinski, N. Garland, D. Jones, and K. Yamada

J — Sensors and Displays: Principles, Materials, and Processing

J1 — Environmental, Water Quality, and Safety Monitorin (Tu)-Gary Hunter, Bryan Chin, Petr Vanýsek, and Rangachary Mukundan

J2 — Nano/Bio Sensors (M-Tu)-Zoraida P. Aguilar, A. Simonian, Larry Nagahara, Ajit Khosla, and H. De Long

J3 — Sensors, Actuators and Microsystems General Session (M-Tu)-M. Carter, N. Wu, R. Mukundan, G. Hunter, and Z. Aguilar

Symposium Topics and Organizers

ECS Transactions (ECST) – Symposia with proceedings available “at” the meeting are labeled with the following icons:

Hard-cover (HC) editions of ECS Transactions will be available forpurchaseandpick-upatthemeeting;oryoumaypre-orderyourhard-coverECST issuewhenregisteringonline.

SC Softcover (SC)editionsofECS Transactionswillbeavailableforpurchaseatthemeetingandwillbeshippedtoyouafterthemeetingends.PleasevisitECSCentralinTorontotoorderyoursoftcoverECSTissue.

Electronic (PDF)editionsofECS TransactionswillbeavailableONLYviatheECSDigitalLibrary(www.ecsdl.org).ElectroniceditionsoftheToronto“at”meetingissueswillbeavailableforpurchasebeginningMay3,2013.PleasevisittheECSwebsiteforallissuepricingandorderinginformationfortheelectroniceditions.

ECS Transactions – Forthcoming IssuesInadditiontothosesymposiathathavecommittedtopublishinganissueofECS Transactions,allothersymposiapotentiallywillbepublishinganissueofECSTapproximately16weeksaftertheTorontomeeting.Ifyouwouldliketoreceiveinformationonanyof these issueswhen theybecomeavailable,[email protected],e-mailaddress,andallissuesinwhichyouareinterested.

Purchase a hardcover copy of ECS Transactions Volume 53, Issues 1 or 2 with your Toronto meeting registration and receive 10% off that issue’s list price!For ECSMembers the 10% discountwill be on top of your regularMemberdiscountfortheseissues.AnydiscountedbookspurchasedmustbepickedupattheTorontomeeting.Thediscountdoesnotapplytoelectroniceditionsoftheseissues.ThisdiscountisnotvalidonanyotherissuesofECST,Monographs,orProceedingsVolumespurchasedatthemeeting.


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Hotel & Travel InformationThe223rdECSMeetingwillbeheldatthe SheratonCentreTorontoHotel(123QueenStreetWest,Toronto,Ontario,M5H2M9,Canada),thedesignatedmeetingheadquarters.Westronglyencourageyoutostay at the Sheraton Centre Toronto Hotel, which offers the mostconvenientandenjoyablemeetingexperience.ReservationscanbemadeonlinefromtheECSwebsiteataspecialdiscountedmeetingratestartingat$199 CADoruntil the block sells out, whichever comes first.SeetheECSwebsiteformoredetailsandtomakeyourreservation.

The deadline for reservations is April 12, 2013.Reservationsattempted after April 12 will be accepted on a space and rateavailabilitybasis.

Registration & General Meeting Information

Meeting Registration—Themeetingregistrationareawillbelocatedin the Sheraton Centre Toronto Hotel, on the Concourse Level,one level directly below the main lobby. Registration will openon Saturday evening and the technical sessionswill be conductedSundaythroughThursday.

Early-Bird Registration—The deadline for Early-Bird registration is April 12, 2013. Early-Bird registration is encouraged. Registeronline at www.electrochem.org or fax your registration form to1.609.737.2743.Attendeespre-payingbycreditcardareencouragedto use our online system or send the form by fax. If you send aregistration formbyfax,pleasedonotsendanothercopybymail,as this may result in duplicate charges. Refunds are subject to a10% processing fee and will only be honored if written requestsarereceivedbyApril29,2013.RefundswillnotbeprocesseduntilAFTER themeeting.Regular registration ratesare ineffectonlineafterApril12,2013andatthemeeting.Allmeetingparticipantsarerequiredtopaytheappropriateregistrationfees.Early-Birdandpost-April12registrationpaymentsmustbemadeinU.S.DollarsviaVisa,MasterCard, American Express, Discover Card, check, or moneyorderpayabletoECS.

Nontechnical Registrant—Travel companions of TechnicalRegistrants are invited to register for the 223rd ECSMeeting as a“NontechnicalRegistrant.”The nontechnical registrant registrationfeeof $25 (Early-Bird) or $30 (afterApril 12) includes admissionto non-ticketed social events; an exclusivemeet-upwith beverageservice and light refreshments, Monday through Thursday, 0800-1000h;andaspecial“WelcometoToronto”orientationpresentedbyTourismTorontoonMonday,May13that0900hintheNontechnicalRegistrant Meet-up. Please note that online registration is notavailableforNontechnicalRegistrants.

Key Locations in the Sheraton Centre Toronto HotelMeetingRegistration..............................................ConcourseLevelInformation/MessageCenter.................................ConcourseLevelECSHeadquartersOffice.....................WentworthRoom,2ndFloorECSCentral............................................................ConcourseLevelAVTechTable................. Locatedoutsideselectsymposiumrooms

Registration and ECS Central HoursSaturday,May11............................................................ 1700-1900hSunday,May12.............................................................. 0700-1900hMonday,May13............................................................. 0700-1900hTuesday,May14............................................................. 0700-1730hWednesday,May15........................................................ 0800-1600hThursday,May16...........................................................0800-1200h

Event HighlightsNote: For a list of Committee Meetings, please visit the Toronto meeting page: www.electrochem.org/meetings/biannual/223.

Sunday, May 120900h..........Short Courses1400h..........Technical Sessions1730h..........Student Mixer (invitation only; contact

[email protected] for details)

Please note, the Sunday Evening Get Together has been rescheduled to Monday at 1800h and is now called the Opening Reception.

Monday, May 130800h..........Technical Sessions0930h..........Technical Session Coffee Break1230h..........Professional Development Series: Essential Elements for

Employment Success1400h..........2013 ECS Gordon E. Moore Medal for Outstanding

Achievement in Solid State Science and Technology Award Lecture: “Wide Bandgap Semiconductors for Sensing Applications,” by Fan Ren

1700h..........The ECS Lecture: “The Frontier of Electronics Research,” by Michael Mayberry

1800h..........Opening Reception (formally known as the Sunday Evening Get Together)

TueSday, May 140800h..........Technical Sessions0800h..........Professional Development Series: Resume Review0930h..........Technical Session Coffee Break1215h..........ECS Annual Business Meeting & Luncheon;

non-refundable ticketed event1230h..........Professional Development Series: Essential Elements for

Employment Success1300h..........Technical Exhibit1300h..........Professional Development Series: Career Fair1630h..........ECST Tutorial1700h..........ECST Open Forum1800h..........Technical Exhibit & General & Student Poster Session1800h..........Professional Development Series: Career Fair

WedneSday, May 150800h..........Technical Sessions0800h..........Professional Development Series: Resume Review0900h..........Technical Exhibit0900h..........Professional Development Series: Career Fair0930h..........Technical Session Coffee Break located in the Exhibit Hall1800h..........Student Poster Award Presentation in the Exhibit Hall1800h..........Technical Exhibit & General Poster Session1800h..........Professional Development Series: Career Fair

ThurSday, May 160800h..........Technical Sessions0900h..........Technical Exhibit0900h..........Professional Development Series: Career Fair0930h..........Technical Session Coffee Break located in the Exhibit Hall


Registration Fees—ALL PARTICIPANTS AND ATTENDEES ARE REQUIRED TO PAY THE APPROPRIATE REGISTRA-TION FEE LISTED BELOW. Payment can be made by cash,check,ortravelers’checksinU.S.fundsdrawnonaU.S.bank.Visa,MasterCard,AmericanExpress,orDiscoverarealsoaccepted.

ECSMember.........................................................................................$450ECSStudentMember............................................................................$160OneDayECSMember.........................................................................$280Nonmember...........................................................................................$620StudentNonmember..............................................................................$195OneDayNonmember...........................................................................$370

All studentsmust present a current, dated student ID card, or forpostdocs, a letter from a professor stating that you are a full orpart-time student,when you pick up your registrationmaterials atthemeeting.Attendeeswhowish tohavepapercopiesofabstractsin advance of themeeting should download copies from the ECSwebsite,freeofcharge.

Financial Assistance—Financialassistanceislimitedandgenerallygoverned by the symposium organizers. Individuals may inquiredirectly to the symposium organizers of the symposium in whichthey are presenting their paper to see if funding is available.Individuals requiring anofficial letterof invitation shouldwrite totheECSheadquartersoffice;suchletterswillnotimplyanyfinancialresponsibilitiesofECS.

ADA Accessibility—SpecialaccommodationsfordisabledattendeeswillbehandledonanindividualbasisprovidedthatadequatenoticeisgiventotheECSHeadquartersOffice.

No Recording Allowed—Recording meetings events throughaudiovisualorphotographicmethodsisprohibitedatallofficialECSMeetingeventswithoutwrittenconsentfromECS.Theuseofcamerasis not permitted during technical sessions.Attendees or exhibitorsmayphotographtheirownactivity,butpermissionmustbeobtainedfromall involvedpartiesbeforephotographscanbe takenofotherpeopleordisplaysatthemeetingorexposition.Pressrepresentativesmust receivemedia credentials and recording permission from theECSHeadquartersOffice.

ECS l The Electrochemical Society65SouthMainStreet

Pennington,NJ08534-2839,USAPhone:+1609.737.1902Fax:+1609.737.2743

E-mail:[email protected]

www.electrochem.org

Open Forum on the Future of ECS Transactions

In2005,thedistributionofECSmeetingcontentthroughECSProceedingsVolumes(PVs)wasreplacedwiththeestablishmentofECS Transactions(ECST).Currently,ECSTincludesfull-textcontentthathasbeenpresentedatECSmeetingsandECS-sponsoredmeetings,andthepapersappearinginECSTarereviewedtoensurethatsubmissionsmeetgenerally-acceptedscientificstandards.Thetypesofpaperspresentedinthetwopublicationsaresimilar,butECSTwascreatedtotakethePVsonline(intheECSDigitalLibrary)andthusprovideexpandedfeatures:accessibility,enhancedsearchcapabilities,andlinkingtootherECSpublications.

Changesincommunicationandinformationsharingtechnologiesrequirethatscientificpublicationscontinuetoadapttomaintaineffectivenesstomeettheneedsofauthorsandreaders.ECSisevaluatingopportunitiesforusingECSTtoexpanddistributionofECSmeetingtechnicalcontentandpromotescientificdiscourseamongmembersofourcommunity.Toobtainauthoranduserinputandgenerateideas,anopenforumisscheduledattheECSmeetinginTorontotodiscussfutureopportunitiesforECST.

EveryoneiswelcometojoinECSTEditorJeffFergusandtheECSPublicationsstaffforthisfirstopenforum.

open ForuM on The FuTure oF ECS TranSaCTionS

Tuesday,May14,1700-1800ConferenceRoomG,MezzanineLevelTheSheratonCentreTorontoHotel

ECS Transactions Tutorial Session for Authors

Pleasejoinusforaspecialsessionaboutsubmittingyourfull-textmanuscriptofyourTorontopresentationforpublicationinECS Transactions(ECST),theonlineproceedingspublicationofECS.

Thissessionwillcoverhowtoprepareyourmanuscript,whenandwheretosubmitit,andhowtonavigatethemanuscriptsubmissionwebsite.Allpresentingauthorsareencouragedtoattendthisopensession.

ECS TranSaCTionS TuTorial SeSSion For auThorS

Tuesday,May14,1630-1700ConferenceRoomG,MezzanineLevelTheSheratonCentreTorontoHotel

photos by tourism toronto. - electrochemical societyatomic force microscopy for energy research...

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