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Table of Contents
Larger Cover
September 1, 2009
Volume 81, Issue 17
Pages 7127-7514
In this issue:
● Editorial
● Research Profile
● AC Detective
● Features
● Accelerated Articles
● Articles
● Technical Notes
● Correspondence
About the Cover:
The field of nanofluidics is maturing, and nanoscale lab-on-a-chip analyses are becoming more routine. Michelle L. Kovarik and
Stephen C. Jacobsen of Indiana University describe how the unique behavior of matter at the nanoscale adds new functionality
to devices that integrate nanopores or nanochannels. The cover shows a schematic of single-molecule fluorescence in a
nanochannel, a schematic of resistive-pulse sensing using a nanopore, and a histogram of photon bursts for single-molecule
fluorescence measurements of a DNA mixture. View the article.
indicates the article is freely available through sponsorship by the author or related funding agency. More about this program.
Editorial
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Soft and Molecular Surfaces
Royce Murray
p 7127
Publication Date (Web): August 10, 2009 (Editorial)
DOI: 10.1021/ac901752x
Abstract
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Research Profile
SERS enters the art scene
Katie Cottingham
p 7128
Publication Date (Web): August 10, 2009 (Research Profile)
DOI: 10.1021/ac901678f
Abstract
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A simple grating-based instrument for spectral microscopy
Nancy D. Lamontagne
p 7129
Publication Date (Web): August 4, 2009 (Research Profile)
DOI: 10.1021/ac9016665
Abstract
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Molecule counting made easy
Erika Gebel
pp 7130–7131
Publication Date (Web): August 11, 2009 (Research Profile)
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (2 of 17) [3/10/2552 11:49:08]
DOI: 10.1021/ac901633n● PDF w/ Links[87K]
Sponsored Access
AC Detective
The mercury mystery of South America
Rajendrani Mukhopadhyay
p 7132
Publication Date (Web): July 15, 2009 (AC Detective)
DOI: 10.1021/ac901452h
Abstract
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● PDF w/ Links[134K]
Sponsored Access
Features
Nanofluidics in Lab-on-a-Chip Devices
Michelle L. Kovarik and Stephen C. Jacobson
pp 7133–7140
Publication Date (Web): August 10, 2009 (Feature)
DOI: 10.1021/ac900614k
Abstract
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● Hi-Res PDF[2418K]
● PDF w/ Links[341K]
Sponsored Access
Accelerated Articles
Protein Quantification in Complex Mixtures by Solid Phase Single-Molecule Counting
Lee A. Tessler, Jeffrey G. Reifenberger and Robi D. Mitra
Abstract | Supporting Info
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (3 of 17) [3/10/2552 11:49:08]
pp 7141–7148
Publication Date (Web): July 14, 2009 (Accelerated Article)
DOI: 10.1021/ac901068x
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● PDF w/ Links[225K]
Articles
Nonprotein Based Enrichment Method to Analyze Peptide Cross-Linking in Protein
Complexes
Funing Yan, Fa-Yun Che, Dmitry Rykunov, Edward Nieves, Andras Fiser, Louis M. Weiss and Ruth Hogue Angeletti
pp 7149–7159
Publication Date (Web): July 30, 2009 (Article)
DOI: 10.1021/ac900360b
Abstract
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● PDF w/ Links[381K]
Automated Principal Component-Based Orthogonal Signal Correction Applied to Fused Near
Infrared−Mid-Infrared Spectra of French Olive Oils
Peter de B. Harrington, Jacky Kister, Jacques Artaud and Nathalie Dupuy
pp 7160–7169
Publication Date (Web): August 5, 2009 (Article)
DOI: 10.1021/ac900538n
Abstract
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● Hi-Res PDF[2474K]
● PDF w/ Links[329K]
Evaluation of Several MS/MS Search Algorithms for Analysis of Spectra Derived from
Electron Transfer Dissociation Experiments
Kumaran Kandasamy, Akhilesh Pandey and Henrik Molina
pp 7170–7180
Publication Date (Web): July 29, 2009 (Article)
DOI: 10.1021/ac9006107
Abstract | Supporting Info
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (4 of 17) [3/10/2552 11:49:08]
Self-Assembly Approach to Multiplexed Surface-Enhanced Raman Spectral-Encoder Beads
Christina I. Brady, Nathan H. Mack, Leif O. Brown and Stephen K. Doorn
pp 7181–7188
Publication Date (Web): August 11, 2009 (Article)
DOI: 10.1021/ac900619h
Abstract | Supporting Info
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● PDF w/ Links[415K]
A NIST Standard Reference Material (SRM) to Support the Detection of Trace Explosives
William A. MacCrehan
pp 7189–7196
Publication Date (Web): July 28, 2009 (Article)
DOI: 10.1021/ac900641v
Abstract | Supporting Info
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Fixation and Drying Protocols for the Preparation of Cell Samples for Time-of-Flight
Secondary Ion Mass Spectrometry Analysis
Jakob Malm, Dimitrios Giannaras, Mathis O Riehle, Nikolaj Gadegaard and Peter Sj vall
pp 7197–7205
Publication Date (Web): July 29, 2009 (Article)
DOI: 10.1021/ac900636v
Abstract | Supporting Info
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● PDF w/ Links[648K]
Macroporous Thermosensitive Imprinted Hydrogel for Recognition of Protein by Metal
Coordinate Interaction
Lei Qin, Xi-Wen He, Wei Zhang, Wen-You Li and Yu-Kui Zhang
pp 7206–7216
Publication Date (Web): August 5, 2009 (Article)
DOI: 10.1021/ac900676t
Abstract | Supporting Info
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● Hi-Res PDF[1874K]
● PDF w/ Links[473K]
Recipe for Uncovering the Bioactive Components in Herbal Medicine Abstract
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (5 of 17) [3/10/2552 11:49:08]
Foo-Tim Chau, Hoi-Yan Chan, Chui-Yee Cheung, Cheng-Jian Xu, Yizeng Liang and Olav M. Kvalheim
pp 7217–7225
Publication Date (Web): July 27, 2009 (Article)
DOI: 10.1021/ac900731z
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Membrane-Based Electrochemical Nanobiosensor for the Detection of Virus
Binh T.T. Nguyen, Guiwan Koh, Hui Si Lim, Anthony J. S. Chua, Mary M. L. Ng and Chee-Seng Toh
pp 7226–7234
Publication Date (Web): August 7, 2009 (Article)
DOI: 10.1021/ac900761a
Abstract
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Cold Chemical Oxidation of Proteins
David M. Hambly and Michael L. Gross
pp 7235–7242
Publication Date (Web): July 30, 2009 (Article)
DOI: 10.1021/ac900855f
Abstract
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Plasmon-Induced Enhancement in Analytical Performance Based on Gold Nanoparticles
Deposited on TiO2 Film
Anwei Zhu, Yongping Luo and Yang Tian
pp 7243–7247
Publication Date (Web): August 5, 2009 (Article)
DOI: 10.1021/ac900894p
Abstract
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Enhanced Flow Cytometry-Based Bead Immunoassays Using Metal Nanostructures
Wei Deng, Krystyna Drozdowicz-Tomsia, Dayong Jin and Ewa M. Goldys
Abstract | Supporting Info
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (6 of 17) [3/10/2552 11:49:08]
pp 7248–7255
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac900947h
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Spray Performance of Microfluidic Glass Devices with Integrated Pulled Nanoelectrospray
Emitters
Peter Hoffmann, Markus Eschner, Stefanie Fritzsche and Detlev Belder
pp 7256–7261
Publication Date (Web): July 29, 2009 (Article)
DOI: 10.1021/ac9015038
Abstract
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Subnanomolar Ion Detection by Stripping Voltammetry with Solid-Supported Thin Polymeric
Membrane
Yushin Kim, Patrick J. Rodgers, Ryoichi Ishimatsu and Shigeru Amemiya
pp 7262–7270
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac900995a
Abstract | Supporting Info
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Nonenzymatic Electrochemical Detection of Glucose Based on Palladium−Single-Walled
Carbon Nanotube Hybrid Nanostructures
Ling Meng, Juan Jin, Gaixiu Yang, Tianhong Lu, Hui Zhang and Chenxin Cai
pp 7271–7280
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac901005p
Abstract
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Microstructured Photonic Fibers as Multichannel Electrospray Emitters
Shuqin Su, Graham T. T. Gibson, Samuel M. Mugo, Dale M. Marecak and Richard D. Oleschuk
Abstract
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (7 of 17) [3/10/2552 11:49:08]
pp 7281–7287
Publication Date (Web): August 11, 2009 (Article)
DOI: 10.1021/ac901026t
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● PDF w/ Links[286K]
Direct Analysis of Volatile Methylsiloxanes in Gaseous Matrixes Using Atmospheric Pressure
Chemical Ionization-Tandem Mass Spectrometry
Koffi Badjagbo, Alexandra Furtos, Mehran Alaee, Serge Moore and S bastien Sauv
pp 7288–7293
Publication Date (Web): July 28, 2009 (Article)
DOI: 10.1021/ac901088f
Abstract
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Accurate Measurement of DNA Methylation That Is Traceable to the International System of
Units
Daniel G. Burke, Kate Griffiths, Zena Kassir and Kerry Emslie
pp 7294–7301
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac901116f
Abstract | Supporting Info
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In situ Studies of Soft- and Reactive Landing of Mass-Selected Ions Using Infrared Reflection
Absorption Spectroscopy
Qichi Hu, Peng Wang, Paul L. Gassman and Julia Laskin
pp 7302–7308
Publication Date (Web): July 10, 2009 (Article)
DOI: 10.1021/ac901149s
Abstract
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● PDF w/ Links[212K]
Chromatically Resolved Optical Microscope (CROMoscope): A Grating-Based Instrument for
Spectral Imaging
Michael R. Webb, Christopher N. LaFratta and David R. Walt
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (8 of 17) [3/10/2552 11:49:08]
pp 7309–7313
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac9011655
● Hi-Res PDF[2364K]
● PDF w/ Links[289K]
Methodology for Determining Disulfide Linkage Patterns of Closely Spaced Cysteine
Residues
Bing Zhang and Steven L. Cockrill
pp 7314–7320
Publication Date (Web): July 23, 2009 (Article)
DOI: 10.1021/ac901161e
Abstract | Supporting Info
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● Hi-Res PDF[1395K]
● PDF w/ Links[248K]
Electro-Coalescence of Digitally Controlled Droplets
Xize Niu, Fabrice Gielen, Andrew J. deMello and Joshua B. Edel
pp 7321–7325
Publication Date (Web): July 21, 2009 (Article)
DOI: 10.1021/ac901188n
Abstract | Supporting Info
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Gradient Elution Moving Boundary Electrophoresis with Channel Current Detection
David Ross and Eugenia F. Romantseva
pp 7326–7335
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac901189y
Abstract | Supporting Info
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● PDF w/ Links[261K]
An Analytical System for Single Nanomaterials: Combination of Capillary Electrophoresis
with Raman Spectroscopy or with Scanning Probe Microscopy for Individual Single-Walled
Carbon Nanotube Analysis
Tatsuhiro Yamamoto, Yoichi Murakami, Jin Motoyanagi, Takanori Fukushima, Shigeo Maruyama and Masaru Kato
Abstract | Supporting Info
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (9 of 17) [3/10/2552 11:49:08]
pp 7336–7341
Publication Date (Web): August 6, 2009 (Article)
DOI: 10.1021/ac901197v
● PDF w/ Links[306K]
Characterization of Route Specific Impurities Found in Methamphetamine Synthesized by the
Leuckart and Reductive Amination Methods
Vanitha Kunalan, Niamh Nic Da id, William J. Kerr, Hilary A. S. Buchanan and Allan R. McPherson
pp 7342–7348
Publication Date (Web): July 28, 2009 (Article)
DOI: 10.1021/ac9005588
Abstract | Supporting Info
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Development of the Space-Resolved Solid-Phase Microextraction Technique and Its
Application to Biological Matrices
Xu Zhang, Jibao Cai, Ken D. Oakes, Fran ois Breton, Mark R. Servos and Janusz Pawliszyn
pp 7349–7356
Publication Date (Web): July 30, 2009 (Article)
DOI: 10.1021/ac900718q
Abstract
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Proteomic Profiling of a High-Producing Chinese Hamster Ovary Cell Culture
Tyler Carlage, Marina Hincapie, Li Zang, Yelena Lyubarskaya, Helena Madden, Rohin Mhatre and William S.
Hancock
pp 7357–7362
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac900792z
Abstract
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● Hi-Res PDF[229K]
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Membrane Solid-Phase Microextraction—A New Concept of Sorbent Preparation
Adam Kloskowski and Michał Pilarczyk , Jacek Namie nik
pp 7363–7367
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (10 of 17) [3/10/2552 11:49:08]
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac9007978
● Hi-Res PDF[604K]
● PDF w/ Links[149K]
Quantification of Ferritin-Bound Iron in Plant Samples by Isotope Tagging and Species-
Specific Isotope Dilution Mass Spectrometry
Matthias Hoppler, Christophe Zeder and Thomas Walczyk
pp 7368–7372
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac900885j
Abstract
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● PDF w/ Links[130K]
Single-Step LC/MS Method for the Simultaneous Determination of GC-Amenable
Organochlorine and LC-Amenable Phenoxy Acidic Pesticides
G. Famiglini, P. Palma, V. Termopoli, H. Trufelli and A. Cappiello
pp 7373–7378
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac9008995
Abstract
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● Hi-Res PDF[171K]
● PDF w/ Links[115K]
Quantitative Evaluation of Intracellular Metabolite Extraction Techniques for Yeast
Metabolomics
Andr B. Canelas, Angela ten Pierick, Cor Ras, Reza M. Seifar, Jan C. van Dam, Walter M. van Gulik and Joseph
J. Heijnen
pp 7379–7389
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac900999t
Abstract
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● Hi-Res PDF[644K]
● PDF w/ Links[327K]
Downscaling Limits and Confinement Effects in the Miniaturization of Porous Polymer
Monoliths in Narrow Bore Capillaries
Ivo Nischang, Frantisek Svec and Jean M. J. Fr chet
Abstract | Supporting Info
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (11 of 17) [3/10/2552 11:49:08]
pp 7390–7396
Publication Date (Web): July 30, 2009 (Article)
DOI: 10.1021/ac901162x
● Hi-Res PDF[812K]
● PDF w/ Links[286K]
Gold Electrode Incorporating Corrole as an Ion-Channel Mimetic Sensor for Determination of
Dopamine
Katarzyna Kurzatkowska, Eduard Dolusic, Wim Dehaen, Karolina Siero -Stołtny, Aleksander Siero and Hanna
Radecka
pp 7397–7405
Publication Date (Web): July 28, 2009 (Article)
DOI: 10.1021/ac901213h
Abstract | Supporting Info
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Insights into the Capillary Electrophoresis Separation of Heparin Disaccharides from Nuclear
Magnetic Resonance, pKa, and Electrophoretic Mobility Measurements
Stacie L. Eldridge, Layne A. Higgins, Bailey J. Dickey and Cynthia K. Larive
pp 7406–7415
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac901218q
Abstract | Supporting Info
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Surface Area Effects on the Response Mechanism of Ion Optodes: A Preliminary Study
Valeriya Bychkova and Alexey Shvarev
pp 7416–7419
Publication Date (Web): August 5, 2009 (Article)
DOI: 10.1021/ac901220d
Abstract | Supporting Info
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Fractionation Correction Methodology for Precise and Accurate Isotopic Analysis of Boron
by Negative Thermal Ionization Mass Spectrometry Based on BO2− Ions and Using the
Abstract
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (12 of 17) [3/10/2552 11:49:08]
18O/16O Ratio from ReO4− for Internal Normalization
Suresh K. Aggarwal, Bo-Shian Wang, Chen-Feng You and Chuan-Hsiung Chung
pp 7420–7427
Publication Date (Web): August 3, 2009 (Article)
DOI: 10.1021/ac901224m
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Nanocapillaries for Open Tubular Chromatographic Separations of Proteins in Femtoliter to
Picoliter Samples
Xiayan Wang, Chang Cheng, Shili Wang, Meiping Zhao, Purnendu K. Dasgupta and Shaorong Liu
pp 7428–7435
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac901265t
Abstract | Supporting Info
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Aptamer-Based Microfluidic Device for Enrichment, Sorting, and Detection of Multiple
Cancer Cells
Ye Xu, Joseph A. Phillips, Jilin Yan, Qingge Li, Z. Hugh Fan and Weihong Tan
pp 7436–7442
Publication Date (Web): July 30, 2009 (Article)
DOI: 10.1021/ac9012072
Abstract | Supporting Info
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Surface-Enhanced Raman Spectroscopy: A Direct Method to Identify Colorants in Various
Artist Media
Christa L. Brosseau, Kari S. Rayner, Francesca Casadio, Cecily M. Grzywacz and Richard P. Van Duyne
pp 7443–7447
Publication Date (Web): July 28, 2009 (Article)
DOI: 10.1021/ac901219m
Abstract
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● PDF w/ Links[316K]
A Monolithic Continuous-Flow Microanalyzer with Amperometric Detection Based on the
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (13 of 17) [3/10/2552 11:49:08]
Green Tape Technology
Cynthia S. Mart nez-Cisneros, Zaira da Rocha, Marcos Ferreira, Francisco Vald s, Antonio Seabra, Mario G
ngora-Rubio and Julian Alonso-Chamarro
pp 7448–7453
Publication Date (Web): August 7, 2009 (Article)
DOI: 10.1021/ac9012418
Abstract | Supporting Info
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Detection and Quantitation of IgG 1 Hinge Aspartate Isomerization: A Rapid Degradation in
Stressed Stability Studies
David M. Hambly, Douglas D. Banks, Joanna L. Scavezze, Christine C. Siska and Himanshu S. Gadgil
pp 7454–7459
Publication Date (Web): July 24, 2009 (Article)
DOI: 10.1021/ac901258g
Abstract
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Isotope Dilution Method for Determination of Polybrominated Diphenyl Ethers Using Liquid
Chromatography Coupled to Negative Ionization Atmospheric Pressure Photoionization
Tandem Mass Spectrometry: Validation and Application to House Dust
Mohamed Abou-Elwafa Abdallah, Stuart Harrad and Adrian Covaci
pp 7460–7467
Publication Date (Web): August 4, 2009 (Article)
DOI: 10.1021/ac901305n
Abstract | Supporting Info
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Noncompetitive Fluorescence Polarization Aptamer-based Assay for Small Molecule
Detection
Josephine Ruta, Sandrine Perrier, Corinne Ravelet, Jennifer Fize and Eric Peyrin
pp 7468–7473
Publication Date (Web): July 24, 2009 (Article)
DOI: 10.1021/ac9014512
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (14 of 17) [3/10/2552 11:49:08]
Influence of a Magnetic Nanoparticle As a Drug Carrier on the Activity of Anticancer Drugs:
Interactions of Double Stranded DNA and Doxorubicin Modified with a Carrier
Anna M. Nowicka, Agata Kowalczyk, Mikolaj Donten, Pawel Krysinski and Zbigniew Stojek
pp 7474–7483
Publication Date (Web): August 10, 2009 (Article)
DOI: 10.1021/ac9014534
Abstract
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Technical Notes
Aptamer-Linked Assay for Thrombin Using Gold Nanoparticle Amplification and Inductively
Coupled Plasma−Mass Spectrometry Detection
Qiang Zhao, Xiufen Lu, Chun-Gang Yuan, Xing-Fang Li and X. Chris Le
pp 7484–7489
Publication Date (Web): August 11, 2009 (Technical Note)
DOI: 10.1021/ac900961y
Abstract | Supporting Info
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High-Throughput Profiling of Formalin-Fixed Paraffin-Embedded Tissue Using Parallel
Electrophoresis and Matrix-Assisted Laser Desorption Ionization Mass Spectrometry
Hans-Rudolf Aerni, Dale S. Cornett and Richard M. Caprioli
pp 7490–7495
Publication Date (Web): August 3, 2009 (Technical Note)
DOI: 10.1021/ac900974j
Abstract | Supporting Info
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Fabrication and Characterization of a Dual Submicrometer-Sized Electrode
Chenxi Yang and Peng Sun
pp 7496–7500
Publication Date (Web): July 29, 2009 (Technical Note)
DOI: 10.1021/ac901099n
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (15 of 17) [3/10/2552 11:49:08]
● PDF w/ Links[160K]
Half-Life Mapping of Nitroxyl Radicals with Three-Dimensional Electron Paramagnetic
Resonance Imaging at an Interval of 3.6 Seconds
Hideo Sato-Akaba, Yoko Kuwahara, Hirotada Fujii and Hiroshi Hirata
pp 7501–7506
Publication Date (Web): July 31, 2009 (Technical Note)
DOI: 10.1021/ac901169g
Abstract
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Scattering Imaging of Single Quantum Dots with Dark-Field Microscopy
Xiaobing Bu, Huaping Chen, Hongwei Gai, Ronghua Yang and Edward S Yeung
pp 7507–7509
Publication Date (Web): August 7, 2009 (Technical Note)
DOI: 10.1021/ac901410w
Abstract
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Correspondence
Antibody−Antigen Exchange Equilibria in a Field of an External Force: Design of Reagentless
Biosensors
Christopher F. Monson, Laura N. Driscoll, Eliot Bennion, Cary J. Miller and Marcin Majda
pp 7510–7514
Publication Date (Web): July 29, 2009 (Correspondence)
DOI: 10.1021/ac9010759
Abstract
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Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
http://pubs.acs.org/toc/ancham/81/17 (16 of 17) [3/10/2552 11:49:08]
Analytical Chemistry: Volume 81, Issue 17 (ACS Publications)
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http://pubs.acs.org/toc/ancham/81/17 (17 of 17) [3/10/2552 11:49:08]