programma 2013pag 1 - test veritas · avermectins ivermectin, abamectin, doramectin, eprinomectin,...

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www.testveritas.com [email protected] Highlight 19 years of experiences 65 participating countries Operational Headquarter loc. Padriciano, 99 34149 Trieste (TS) Italy Tel: +39 040 3755560 Via Svizzera, 16 35127 Padova (PD) Italy Tel: +39 049 8256292 Fax: +39 049 21064938 Legal Headquarter FOOD SAFETY ANALYSIS Test Veritas S.r.l. was created to satisfy the increasing international demand for services and products for analysis. scheme Progetto Trieste. The main features of Progetto Trieste are: Screening results are assessed by dedicated criteria Test materials are mainly incurred often provided 2018 beta-lactams in milk List of EN ISO/IEC 17043:2010 accredited scopes available at www.accredia.it 1 in cheese pesticides, nitrate and cadmium in spinach tetracyclines and CAP in shrimps plead, cadmium and mercury in liver ciromazine and macrolides in eggs 2015-2017 Participanting countries avermectins and sulphonamides in liver Details of accredited schemes available at www.testveritas.com MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 1 of 15 (Cert. PTP N. 0008)

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Page 1: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

[email protected]

Highlight

19 years of experiences 65 participating countries

Operational Headquarterloc. Padriciano, 9934149 Trieste (TS)Italy Tel: +39 040 3755560

Via Svizzera, 1635127 Padova (PD)ItalyTel: +39 049 8256292Fax: +39 049 21064938

Legal Headquarter

FOOD SAFETY ANALYSIS

Test Veritas S.r.l. was created to satisfy the increasing international demand for services and products for

analysis.

scheme Progetto Trieste.

The main features of Progetto Trieste are:

Screening results are assessed by dedicatedcriteria

Test materials are mainly incurred

often provided

2018

beta-lactams in milk

List of EN ISO/IEC 17043:2010 accredited scopes

available at

www.accredia.it

1 in cheese

pesticides, nitrate and cadmium in spinach

tetracyclines and CAP in shrimps

plead, cadmium and mercury in liver

ciromazine and macrolides in eggs

2015-2017 Participanting countries

avermectins and sulphonamides in liver

Details of accreditedschemes available at www.testveritas.com

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 1 of 15

(Cert. PTP N. 0008)

Page 2: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

Find out more about

Visit www.testveritas.com

Fumonisins

ZearalenoneOchratoxinDON

Synthetic steroids

RAL (Resorcilic Acid Lactones)Stilbenes!-agonistsRactopamineCorticosteroids

Sulphonamides

Tetracyclines

Quinolones and

ChloramphenicolAvermectins

Nitrofurans (metabolites)

Groups of analytes

fumonisin B1, B2 and/or the sum

zearalenoneochratoxin Adeoxynivalenol

17"-19nortestosterone, 17!-19nortestosterone, 17"-boldenone , 17!-boldenone ,17"-trenbolone, 17!-trenbolone, methyltestosterone, stanozololzeranol, taleranoldiethylstilbestrol (cis-DES & trans-DES), hexestrol, dienestrolclenbuterol, salbutamol, terbutalineractopamine

prednisolone, prednisonesulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine, sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazoloxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers

chloramphenicolivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin

AOZ, AMOZ, AHD, SEM

Tylosin tylosin A, tylosin B

nitrate, pesticides, heavy metals (see page n. 9)Other contaminants

Patulin patulin

betamethasone

Macrolides erythromycin, josamycin, lincomycin, oleandamycin,

1 12 2 and/or total

Coccidiostatics nicarbazin, robenidine, salinomycin, lasalocid, narasin- lactams penicillin V, penicillin G, amoxicillin, ampicillin

rifampicin, spiramycin, tilmicosin, tylosin A, tylosin B,

Histamine histamineMalachite Green malachite green and leucomalachite green

virginiamycin

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 2 of 15

Page 3: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered with the test material.

   

Progetto Trieste - Veterinary Drug Residues 2018 Programme

Those proficiency tests could distinguish between participations with confirmatory methods (HPLC-GC) or screening methods (ELISA, RIA, biosensors, microbial inhibition assays, lateral flow, etc...).For participating with confirmatory methods the code is A and quantification is requested. Evaluation of performance

For participating with screening methods the code is B and quantification is optional. Qualitative results will be

When the shipment includes 2 test materials, they are at a different concentration of analyte. The laboratory will receive an evaluation for each test material.

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 3 of 15

will be in z-score terms.

assesed by dedicated criteria (see Evaluation Criteria at www.testveritas.com).

Analytes Matrix Status Code Quantity Euro

E1810 A 30g x 2 Test Materials B

330,00 285,00

Chloramphenicol egg

ROUND of MARCH

spiked15g x 2 Test Materials

Shipping date: March 19th 2018. Result submission deadline: April 20st 2018. Final Report available in May 2018. Order deadline: January 31st 2018

MI1811 A 20ml x 2 Test Materials B

3300,00 285,00 Chloramphenicol

10ml x 2 Test Materials

E1813 A 30g x 2 Test Materials B

330,00 285,00

Quinolones and Fluoroquinolones 15g x 2 Test Materials

MI1814 A 20ml x 2 Test Materials B

430,00 325,00

Tetracyclines andQuinolones/ 10ml x 2 Test Materials partial participations in MI1814

Only for analysis of Quinolones/Fluoroquinolones: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1814/Q

Only for analysis of Tetracyclines: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1814/T

spiked

eggs

M1815 A 20g x 2 Test Materials B

330,00 285,00 Nitrofuran metabolites 10g x 2 Test Materials

swine muscle

bovine milk

incurredor spiked

incurred

spiked

M1812 A 20g x 2 Test Materials B

330,00 285,00 Chloramphenicol 10g x 2 Test Materials

rabbit muscle incurred

bovine milk

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesChloramfenicol chloramfenicol eggs, milk, muscle: < 3 ppb or blank

Tetracyclines oxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers milk: < 300 ppb or blank Quinolones and fluoroquinolones

enrofloxacin, ciprofloxacin, flumequine, marbofloxacin, danofloxacin, sarafloxacin, nalidixic acid, oxolinic acid, norfloxacin

milk: < 200 ppb or blank

Nitrofuran metabolites AOZ, AMOZ, AHD, SEM muscle: < 6 ppb or blank

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.Milk test materials would contain preservative solutions.It is not requested to research all the molecules of each group.

Fluoroquinolones

L1785 A 20g x 1 Test Material B

330,00 285,00 Avermectins 10g x 1 Test Material

bovine liver spiked

Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin

eggs: < 200 ppb

liver: < 200 ppb

LIO

LIO

LIO

LIO

LIO

LIO

Page 4: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

   

 

Progetto Trieste - Veterinary Drug Residues 2018 Programme

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

   

   

 

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 4 of 15

Shipping date: May 21st 2018. Result submission deadline : June 22nd 2018. Final Report available in July 2018. Order deadline: March 23rd 2018

Analytes Matrix Status Code Quantity Euro

U1820 A 18ml x 2 Test Materials B

380,00 285,00 Synthetic steroids bovine urine

ROUND of MAY

12ml x 2 Test Materials

U1821 A 18ml x 2 Test Materials B

380,00 285,00

RAL 6ml x 2 Test Materials

U1822 A 18ml x 2 Test Materials B

380,00 285,00 Stilbenes 6ml x 2 Test Materials

U1823 A 18ml x 2 Test Materials B

380,00 285,00

-agonists(ractopamine included) 6ml x 2 Test Materials

partial participations in U1823

Only for analysis of -agonists: A 18ml x 2 Test Materials B 6ml x 2 Test Materials

330,00 245,00 U1823/G

Only for analysis of ractopamine: A 18ml x 2 Test Materials B 6ml x 2 Test Materials

330,00 245,00 U1823/R

incurred orspiked

bovine urine

swine urine incurred or spiked

bovine or swine urine

U1824 A 18ml x 2 Test Materials B

380,00 285,00 Corticosteroids 6ml x 2 Test Materials

bovine urine

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesSynthetic steroids nortestosteron

one, methyltestosterone, stanozolol

urine: < 10 ppb or blank RAL zeranol, taleranol Stilbenes diethylstilbestrol (cis-DES and trans-DES), hexestrol, dienestrol

Corticosteroids dexamethasone, betamethasone, flumethasone, prednisolone, prednisone

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.Urine and milk test materials would contain preservative solutions.It is not requested to research all the molecules of each group.

-agonists clenbuterol, salbutamol, terbutalineRactopamine ractopamine

The updated programme is available at www.testveritas.com

incurred

incurred orspiked

incurred orspiked

Analysis of synthetic sterois and RAL intended to the homogeneity study have been subcontracted.Test Veritas is responsible of subcrontracted activities.

LIO

LIO

LIO

LIO

LIO

LIO

Page 5: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

   

 

Progetto Trieste - Veterinary Drug Residues 2018 Programme

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

   

   

 

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 5 of 15

Shipping date: May 21st 2018. Result submission deadline: June 22nd 2018 and June 8th for -lactams. Final Report available in July 2018. Order deadline: March 23rd 2018

Analytes Matrix Status Code Quantity Euro

ROUND of MAY (see previous page too)

MI1825 A 20ml x 2 Test Materials B

430,00 325,00

Avermectinslactams 10ml x 2 Test Materials

partial participations in MI1825

Only for analysis of avermectins: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1825/I

Only for analysis of -lactams: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1825/L

bovine milk

MI1826 A 20ml x 2 Test Materials B

330,00 285,00 Sulphonamides 10ml x 2 Test Materials

bovine milk

E1783 A 30g x 1 Test Material B

Macrolide 15g x 1 Test Material

spiked eggs

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material. Subscription to proficiency testing free of charge is allowed only to participants of other Progetto Trieste tests.

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .

TECHNICAL ASPECTS

Indicative concentrations

Category List of molecules

Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank

Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine,sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazol milk: < 400 ppb or blank

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.Urine and milk test materials would contain preservative solutions.It is not requested to research all the molecules of each group.

The updated programme is available at www.testveritas.com

spiked

spiked

free of charge

-lactams penicillin V, penicillin G, amoxicillin, ampicillin milk: < 30 ppb or blank

Macrolides erythromycin, josamycin, lincomycin, oleandamycin,rifampicin, spiramycin,tilmicosin, tylosin A, tylosin B, virginiamycin

eggs: < 300 ppb

LIO

LIO

LIO

LIO

Page 6: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

 

Progetto Trieste - Veterinary Drug Residues and Histamine - 2018 Programme

The updated programme is available at www.testveritas.com  

     

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 6 of 15

Shipping date: September 10th 2018. Result submission deadline: October 12th 2018. Final Report available in November 2018. Order deadline: July 21st 2018

ROUND of SEPTEMBER

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesHistamine histamine tuna: < 400 ppm or blank

Chloramfenicol chloramfenicol fish and shrimps: < 3 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine,

sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazol muscle: < 300 ppb or blank

Tetracyclines oxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers fish: < 300 ppb or blank

Quinolones and fluoroquinolones

enrofloxacin, ciprofloxacin, flumequine, marbofloxacin, danofloxacin, sarafloxacin, nalidixic acid, oxolinic acid, norfloxacin

muscle: < 800 ppb or blank

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

Analytes Matrix Status Code Quantity Euro

T1830 A 50g x 2 Test Materials B

295,00 215,00

Histamine(2 levels)

tuna 50g x 2 Test Materials

FI+SH1831 A 20g x 2 Test Materials

B 430,00 325,00 Tetracyclines 10g x 2 Test Materials

fish and shrimps spiked

incurred

M1832 A 30g x 2 Test Materials B

330,00 285,00

Quinolones and fluoroquinoles 15g x 2 Test Materials

turkey muscle

M1833 A 20g x 2 Test Materials B

330,00 285,00 Tetracyclines 10g x 2 Test Materials

hen or bovine muscle

incurred

M1834 A 20g x 2 Test Materials B

330,00 285,00 Sulphonamides 10g x 2 Test Materials

turkey or swine muscle

or spiked

FI+SH1835 A 20g x 2 Test Materials

B 330,00 285,00 Chloramphenicol

10g x 2 Test Materials

fish and shrimps incurred or spiked

Malachite and leuco-malachite green

malachite green, leucomalachite green and the sum of both

muscle: < 500 ppb or blank

fish: < 8 ppb

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

FI1836 A 20g x 1 Test Material B

330,00 285,00

Quinolones and fluoroquinoles

10g x 1 Test Material

fish spiked

FI1837 A 20g x 1 Test Material B

330,00 285,00

Malachite and leucomalachite green

10g x 1 Test Material

fish spiked

incurred or spiked

incurred or spiked

fish: < 800 ppb

LIO

LIO

LIO

LIO

LIO

LIO

LIO

Page 7: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

 

Progetto Trieste - Veterinary Drug Residues 2018 Programme

   

   

 

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 7 of 15

Shipping date: November 12th 2018. Result submission deadlinee: December 14th 2018 and November 28th for honey. Final Report available in January 2019. Order dead line: October 5th 2018

Analytes Matrix Status Code Quantity Euro

ROUND of NOVEMBER

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .

TECHNICAL ASPECTS

Indicative concentrations

Category

List of molecules

Chloramphenicol chloramphenicol honey: < 3 ppb or blank

Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine, sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazol

honey: < 50 ppb or blank

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

L1840 A 20g x 2 Test Materials B

360,00 285,00

-agonists bovine or swine liver 20g x 2 Test Materials

L1841 A 20g x 2 Test Materials B

330,00 285,00 Corticosteroids 10g x 2 Test Materials

H1842 A 35g x 2 Test Materials B

430,00 325,00

Sulphonamides and chloramphenicol

10g x 2 Test Materials partial participations in H1842

Only for analysis of sulphonamides: A 35g x 2 Test Materials B 10g x 2 Test Materials

330,00 245,00 H1842/S

Only for analysis of chloramphenicol: A 35g x 2 Test Materials B 10g x 2 Test Materials

330,00 245,00 H1842/C

incurred or spiked

light honey spiked

H1845 A 30g x 2 Test Materials B

330,00 245,00

Quinolones and Fluoroquinolones

10g x 2 Test Materials

incurred or spiked

spiked

bovine or swineliver

light honey

H1846 A 30g x 2 Test Materials B

330,00 245,00 Tylosin 10g x 2 Test Materials spikedlight honey

(ractopamine included) partial participations in L1840

Only for analysis of -agonists: A 20g x 2 Test Materials B 20g x 2 Test Materials

330,00 260,00 L1840/G

Only for analysis of ractopamine: A 20g x 2 Test Materials B 20g x 2 Test Materials

330,00 260,00 L1840/R

Corticosteroids dexamethasone, betamethasone, flumethasone, prednisolone, prednisone

-agonists clenbuterol, salbutamol, terbutalineRactopamine ractopamine liver: < 8 ppb or blank

The updated programme is available at www.testveritas.comProgetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

L1844 A 20g x 1 Test Material B

330,00 285,00 Sulphonamides 10g x 1 Test Material

incurred or spiked

bovine or swineliver

Quinolones andfluoroquinolones

enrofloxacin, ciprofloxacin, flumequine, marbofloxacin, danofloxacin,sarafloxacin, nalidixic acid, oxolinic acid, norfloxacin

honey: < 100 ppb

Tylosin tylosin A, tylosin B honey: < 100 ppb

Coccidiostatics nicarbazin, robenidine, salinomycin, lasalocid, narasin honey: < 100 ppb

liver: < 300 ppb

M1843 A 20g x 1 Test Material B

330,00 285,00 Coccidiostatics 10g x 1 Test Material

incurred or spiked

chicken or henmuscle

LIO

LIO

LIO

LIO

Page 8: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered with the test material.

Progetto Trieste - Veterinary Drug Residues 2018 Programme

Subscriptions to COMING SOON proficiency test is allowed only for participants of other Progetto Trieste tests.Subscriptions to COMING SOON contributes to elaborate a survey of the interest in this specific proficiency test.Shipping date and price will be communicated as soon as the number of subscriptions will be significant. Therefore, this subscription will not be invoiced. It should be take in consideration that test could be run at the beginning of 2019.

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 8 of 15

Analytes Matrix Status Code Quantity

E1882

Nitroimidazoles eggs

COMING SOON 2018-2019

spiked

Deadline subcription: January 31st 2018

M1883 A 30g x 1 Test Material B

Macrolides 15g x 1 Test Material

spikedbovine muscle

TECHNICAL ASPECTS

Category

List of moleculesMacrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin,

spiramycin, tilmicosin, tylosin A, tylosin B, virginiamycin

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .

Nitroimidazoles dimetridazole, 2-hydroxydimetridazole, ipronidazole, 2-hydroxyipronidazole, metronidazole, 2-hydroxymetronidazole, ronidazole, total nitroimidazoles

free of charge

Euro

330,00 285,00

AB

30g x 1 Test Material 15g x 1 Test Material

LIO

LIO

Page 9: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

 

Progetto Trieste - Pesticide Residues, Heavy Metals, Nitrite and Nitrate - 2018 Programme

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 9 of 15

Shipping date: October 15th 2018. Result submission deadline: November 16th 2018, but November 2nd for nitrate. Final Report available in January 2019. Order deadline: September 14th 2018

ROUND of OCTOBER

Analytes Matrix Status Code Quantity Euro

L1873 75g x 1 Test Material 220,00 Lead/Cadmium/

swine liver

E1786 30g x 1 Test Material eggsCyromazin

VF1870+1+2 4 Test Materials

350,00 Pesticides/Cadmium/Nitrate

partial participations

Only for the analysis of pesticides:

60g x 2 Test Materials (blank included)

220,00 VF1870

Only for the analysis of cadmium: 70g x 1 Test Material VF1871

spinach

220,00

The quantification with chromatographic method is requested. Evaluation will be in z-score terms.

spiked

spiked

spiked

Only for the analysis of nitrate: 70g x 1 Test Material VF1872 220, 00

Only for the analysis of pesticides and cadmium: 3 Test Materials VF1870+1 300, 00

Only for the analysis of pesticides and nitrate: 3 Test Materials VF1870+2 300, 00

Only for the analysis of cadmium and nitrate: 2 Test Materials VF1871+2 300, 00

* Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

In each participation they are included the evaluations of 2 technicians.

Mercury

free of charge

Analysis of pesticides, lead, cadmium and nitrate intended to the homogeneity study have been subcontracted.Test Veritas is responsible of subcrontracted activities.Subscription to proficiency testing free of charge is allowed only to participants of other Progetto Trieste tests.

LIO

LIO

LIO

Page 10: programma 2013pag 1 - Test Veritas · Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine,

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

 

Progetto Trieste - Pesticide Residues, HeavyMetals, Nitrite and Nitrate - 2018 Programme

MO 01COM rev.1 del 06/10/2017, emiss.2 dd 20/11/17 10 of 15

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesPesticides Acephate, Acetamiprid, Acetochlor, Aldicarb, Atrazine,

Azoxystrobin, Benalaxyl, Bendiocarb, Boscalid, Bromuconazole, Carbaryl, Carbendazim, Carbofuran, Chlorpyrifos methyl, Cyazofamid, Cimoxanyl, Cyproconazole, Cyprodinil, Cyromazine, Clomazone, Cumaphos, Demeton-s-methyl, Demeton-S-methyl-sulfon, Desmethyl-pirimicarb, Diclobutrazol, Dicrotophos, Diethofencarb, Difenoconazole, Diflubenzuron, Dimethenamid, Dimethoate, Dimehtomorph, Disulfoton, Diuron, Epoxiconazole, Hexaconazole, Ethiofencarb, Etofenprox, Famoxadone, Fenamidone, Fenazaquin, Fenbuconazole, Fenhexamid, Fenoxaprop-p-ethyl, Fenoxycarb, Fenpropathrin, Fenpropidin, Fluazifop-p-butyl, Fluazinam, Fludioxonil, Fluquinconazole, Flutriafol, Fosetyl-aluminium, Fuberidazole, Flufenacet, Fosfamidon, Furathiocarb, Haloxyfop-2 ethoxyethyl, Haloxyfop-p-methyl, Hexythiazox, Imazalil, Imidacloprid,Indoxacarb, Iprodion, Iprovalicarb, Isofenphos, Isofenphos-methyl, Isoxaben, Kresoxim-methyl, Linuron, Lufenuron, Malaoxon, Mecarbam, Mepanipyrim, Metalaxyl, Methamidophos, Metamitron, Metazachlor, Methiocarb, Methiocarb sulfoxide, Methomyl, Myclobutanil, Nuarimol, Omethoate, Oxadixyl, Oxamyl, Oxycarboxin, Oxydemeton-methyl, Paclobutrazol, Pencycuron, Penconazole, Piperonyl-butoxide,Pyraclostrobin, Pyridaben, Pyrifenox, Pyrimethanil, Pirimicarb, Pirimiphos-ethyl, Pirimiphos-methyl, Pyriproxyfen, Prochloraz, Procymidone, Promecarb, Prometon, Prometryn, Propamocarb, Propaquizafop, Propazine, Propiconazole, Propyzamide, Propoxur, Prosulfocarb, Quinoxyfen, Quizalofop-ethyl, Spinetoram, Spinosad (A and D), Spiroxamine, Sulfotep, Tebuconazole, Tebufenpyrad, Terbumeton, Terbuthylazine, Terbutryn, Tetraconazole, Thiabendazole, Thiodicarb, Thiophanate methyl, Triadimenol, Trichlorphon, Triadimefon, Trifloxystrobin, Vamidotion.

spinach: < 800 ppb

Nitrate nitrate spinach: < 6000 ppmLead, cadmium,mercury

lead, cadmium, mercury lead in liver: < 2 ppmcadmium in liver and spinach: < 2 ppmmercury in liver: < 2 ppm

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

Cyromazin cyromazin eggs: < 1 ppm

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Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

   

Progetto Trieste - Mycotoxins2018 Programme

Those proficiency tests could distinguish between participations with confirmatory methods (HPLC-GC) or screening methods (ELISA, RIA, biosensors, microbial inhibition assays, lateral flow, etc...).For participating with confirmatory methods the code is A and quantification is requested. Evaluation of performance

For participating with screening methods the code is B and quantification is optional. Qualitative results will be

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will be in z-score terms.

assesed by dedicated criteria (see Evaluation Criteria at www.testveritas.com).

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesAflatoxins B/G aflatoxins B1, B2, G1, G2 and/or total aflatoxins maize, peanuts, paprika: < 40 ppb or blank Fumonisins fumonisin B1, B2 and/or sum (B1+B2) maize: < 6000 ppb or blank

Ochratoxin A ochratoxin A paprika, coffee, cocoa: < 30 ppb or blank

Patulin patulin apple juice: < 150 ppb

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

Shipping date: June 18th 2018. Result submission deadline: July 20th 2018. Final Report available in September 2018.

Order deadline: April 27th 2018

GC+C1854

A B incurred green coffee

and cocoa

N1852 A 55g x 2 Test Materials B incurred 55g x 2 Test Materials

Aflatoxins B/G

Ochratoxin A

hazelnuts and peanuts

260,00 190,00

260,00 190,00

ss

s

Ochratoxin A andAflatoxins B/G

ROUND of JUNE

Analytes Matrix Status Code Quantity Euro

SP1853 A 260,00 paprika incurred s

VF1855 A 55ml x 1 Test Material spikedapple juice

(clear)

Patulin 260,00

sMaterial has been irradied. The irradiation process has been subcontracted.

MA1850+1 A 55g x 3 Test Materials

B 295,00 215,00

Aflatoxins B/G

55g x 3 Test Materials partial participations in MA1850+1

Only for the analysis of fumonisins: A 55g x 1 Test Material B 55g x 1 Test Material

260,00 190,00 MA1851

Only for the analysis of aflatoxins (two levels): A 55g x 2 Test Materials B 55g x 2 Test Materials

MA1850

maize flour incurred

260,00190,00

(two levels)and Fumonisins

s

When the shipment includes 2 test materials , they are at a different concentration of analyte. The laboratory

B 55g x 1 Test Material 190,00 55g x 1 Test Material

s55g x 2 Test Materials 55g x 2 Test Materials

Analysis of patuline, aflatoxins B&G and fumonisins intended to the homogeneity study have been subcontracted.

will receive an evaluation for each test material.

Test Veritas is responsible of subcrontracted activities.

s

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Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

   

   

 

   

   

Progetto Trieste - Mycotoxins2018 Programme

Those proficiency tests could distinguish between the participation with confirmatory methods (HPLC-GC) or screening methods (ELISA, RIA, biosensors, microbial inhibition assays, lateral flow, etc...).For participation with confirmatory methods the code is A and quantification is requested. Evaluation of performance

For participation with screening methods the code is B and quantification is optional. Qualitative results will be

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will be in z-score terms.

assesed by dedicated criteria (see Evaluation Criteria at www.testveritas.com).

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesAflatoxin M1 aflatoxin M1 milk: < 100 ppt or blank

cheese: < 700 ppt DON deoxynivalenol wheat: < 6000 ppb

Zearalenone zearalenone maize: < 500 ppb

Ochratoxin A ochratoxin A maize: < 500 ppb

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.Milk test materials would contain preservative solutions.It is not requested to research all the molecules of each group.

Shipping date: October 15th 2018. Result submission deadline: November 16th 2018. Final Report available in January 2019. Order deadline: September 14th 2018

ROUND of OCTOBER

Analytes Matrix Status Code Quantity Euro

sMaterial has been irradied. The irradiation process has been subcontracted.

WH1862 A 55g x 1 Test Material B

260,00 190,00

DON 55g x 1 Test Material

wheat

F1865 A 55g x 1 Test Material B

240,00 190,00 55g x 1 Test Material

feedAflatoxins B/G

s

s

MI1860 A 110ml x 2 Test Materials B

260,00 165,00 Aflatoxin M1 bovine milk 20ml x 2 Test Materials incurred

CE1861 A 50g x 1 Test Material B

260,00 190,00 Aflatoxin M1 fresh cheese

(ricotta) 50g x 1 Test Material spiked

MA1863+4 A 55g x 2 Test Materials B

295,00 215,00

Zearalenone and

55g x 2 Test Materials

partial participations in MA1863+4

Only for the analysis of Zearalenone: A 55g x 1 Test Material B 55g x 1 Test Material

260,00 190,00 MA1863

Only for the analysis of ochratoxin A: A 55g x 1 Test Materia B 55g x 1 Test Material

MA1864

maize flour

260,00190,00

Ochratoxin As

Aflatoxins B/G aflatoxins B1, B2, G1, G2 and/or total feed: < 80 ppb

incurred

incurred

incurred

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

Analysis of patuline, aflatoxins B&G and fumonisins intended to the homogeneity study have been subcontracted.

When the shipment includes 2 test materials , they are at a different concentration of analyte. The laboratory will receive an evaluation for each test material.

Test Veritas is responsible of subcontracted activities.

LIO

LIO

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Progetto Trieste c/o Test Veritas Srl Head Quarter: Via Svizzera 16 – 35127 Padova (PD) - ItalyTel. +39 049 8256292 Fax 049 21064938 [email protected] www.testveritas.com

For order placement...

Progetto Trieste has a Restricted Web Area for participants at www.testveritas.com.

At www.testveritas.com it is available information about how Progetto Triesteworks, advantages,FAQ and examples of FinalReport to show elaborationdata methods.

After login in the Restricted Web Area it is possible to fill in the on-line order form.

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All prices are excluding VAT, where applicable, and shipment costs. PRICE FOR ADDITIONAL MATERIAL :

120,00 for codes containing 2 test materials90,00 Euro for codes containing 1 test material

Laboratories that order additional material will receive double quantity of material. Aditional materials will be sold only in combination with "A" or "B" Test Materials

Purchase of "additional material" does not allow to take part into the performance assessment.

PRICE REDUCTIONS (applicable only to orders placed on-line):   5% price reduction for ordering 6 or more Test Materials "A" o "B"

SHIPPING COST (Euro): for mycotoxin rounds

cereals, nuts, feed, coffee, milk: 60,00 EU

130,00 320,00 South America and Africa

220,00 other destinations

INVOICING, PAYMENT CONDITIONSThe performance assessment service will start from the registration to the proficiency program. For this reason the invoice will be issued upon the receipt of your order and has to be paid before the test materials will be shipped.Note: in case your invoice is not paid before the test materials are send, your laboratory would be

cancelled from the participant's list.

Payment can be made by bank credit transfer. Our bank details will be indicated in the order confirmation and in the invoice.

 

The updated programme is available at www.testveritas.com

General conditions

muscle : urine, milk, honey, eggs, fish, liver:

A fixed bank charge of 20,00 euro will be applied for the orders from all non-EU countries. The orders from non-EU countries would be paid against proforma-invoice; 35,00 euro for the certificate of origin can be charged.

for pesticides, heavy metals, nitrate and nitrite rounds  

Euro

apple juice, cheese:

Europe non-EU

90,00 130,00 320,00 220,00

for veterinary drug residues rounds

60,00 EU

130,00 320,00 South America and Africa

220,00 other destinations Europe non-EU

60,00

EU

130,00 320,00

South America and Africa

220,00

other destinations Europe non-EU

90,00 130,00 320,00 220,00

In case the provided volume is not enough, it is possible to order additional material.

TAX

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QUALITY SYSTEMProficiency Testing Scheme for mycotoxins and veterinary drug residues and histamine are UNI CEI EN ISO/IEC 17043:2010 accredited. (Cert. PTP N. 0008) by ACCREDIA. Scopes of accreditation are available at www.accredia.it and the details of accredited schemesat www.testveritas.com.

Accreditation excludes, in any case, ACCREDIA from any responsibility regarding the offered service.Progetto Trieste provider, Test Veritas Srl, operates in conformance with UNI EN ISO 9001:2008 (Cert. N. IT12/0502).

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

JURISDICTIONAny dispute arising from this contract is exclusively competent the Court of Trieste, excluding any competing court. Every business relationship will be settled in Italian language. If there were written communications in English, the only language accepted to the Italian alternative, the interpretation of which was contrary to written communication in Italian always prevail the sense of the latter.

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The updated programme is available at www.testveritas.com

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

Progetto Trieste submitting results

CONFIDENTIALITY OF RESULTSThe identity of partecipants is confidential: every participating laboratory receives a code.Only with specifical authorization from the participant, the Progetto Trieste Secretariat will disclose all or part of the results/evaluation to third parties. In exceptional circumstances, when a regulatory authority requires proficiency testingresults to be directly provided to the autthority by the proficiency testing provider, the affected participants shall benotified of this action in writing.The participants’ list will be published in the Final Report.

RESULTS AND REPORT

Reports will be available on the website inside the Restricted Web Area archive.Participants will be informed by email about the availability of the Final Report.

Results are returned through Progetto Trieste Restricted Web Area.

Hard-copy reports are available for an additional charge.These are sent to participants by post.

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CONTROL MATERIALS (AFTER PROFICIENCY TEST CONCLUSION)Once each round is concluded, after the release of the Final Report, test materials become available to participants for further investigations or for using them in control charts.