quant report quant time: 03/29/99 18:51 · quant report sample: ... 826aec10.qci page quant time:...
TRANSCRIPT
Operator ID: MC
Output File: AE01077.1A2
Data File: AE01077.MS
Name: AE01077
QUANT REPORT
Sample: Location: 516 N. Lawrence St. SB06-F
ID File: 826AEC10.QCI
Page
Quant Time: 03/29/99 18:51
Injected at: 03/13/99 03:29
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.29 g
Last Calibration: 03/10/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichloradifluoromethane.
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlor·of l uoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene ~ 2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/10/99 17:22
R.T. Scan# Q ion
13.60 1165
20.68 1772
23.41 2006
4.34
0.00
0.00
0.00
0.00
7.02
8.22
9.21
9.77
10.56
11.60
0.00
372
419
441
524
548
601
704
788
836
904
994
993
12.05 1032
0.00 1041
12.53 1073
12.80 1096
12.84 1099
13.17 1128
0.00 1128
14.23 1219
0.00 1252
0.00 1269
0.00 1287
0.00 1340
16.36 1402
0.00 1427
0.00 1450
96
95
152
85
47
61
93
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Ar.ea
112964
57588
42213
6517
Cqnc Units
5. 00 UG/L
5.00 UG/L
5.00 UG/L
0.43 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
9074
2147
203635
3527
1368
1129
0.79 UG/L
0.44 UG/L
4.43 UG/L
0.38 UG/L
0.13 UG/L
0 .11 UG/L
0 Not Found UG/L
2379 0.23 UG/L
2676
6021
4206
12178
5956
Not Found UG/L
0.17 UG/L
0.60 UG/L
0.44 UG/L
0. 43 UG/L
Not Found UG/L
0. 74 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
63171 1.18 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
998
939
909
193
638
411
610
986
902
987
875
794
768
771
797
684
826
773
940
991
902
977
499
54
714
803
986
765
780
Rf
1.000
0.510
0.374
0.668
0.000
0.000
0.000
0.000
0.508
0.217
2.035
0.408
0. 455
0.474
0.000
0.468
0.000
0. 715
0.442
0.422
1. 257
0.000
0.358
0.000
0.000
0.000
0.000
2. 372
0.000
0.000
Operator ID: MC
Output File: AE01077.1A2
Data File: AE01077.MS
Name: AE01077
QUANT REPORT
Sample: Location: 516 N. Lawrence St. SB06-F
ID File: 826AEC10.QCI
Page 2
Quant Time: 03/29/99 18:51
Injected at: 03/13/99 03:29
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.29 g
Last Calibration: 03/10/99 Last Qcal Time: 03/10/99 17:22
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38 I
630-20-6
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1480
17.32 1483
0.00 1515
0.00 1536
18.75 1606
0.00
18.88
1,3-Dimethylbenz~ne (m-Xylene 19.05
1613
1617
1632
1,4-Dimethylbenzene (p-Xylene 19.05 1632
1,2-Dimethylbenzene (a-Xylene 19.76 1692
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1697
0.00 1726
20.36 1744
0.00 1782
0.00 1793
21.01 1800
21.08 1806
21.30 1825
21.33 1827
21.47 1839
21.94 1880
22.02 1886
22.32 1912
22.53 1930
22.62 1938
22.75 1949
23.26 1993
23.45 2009
0.00 2133
26.65 2283
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
10448 0.90 UG/L
0 Not Found UG/L
Not Found UG/L
10559 0.28 UG/L
0 Not Found UG/L
45951 0.66 UG/L
72723
72723
23696
0.49 UG/L
0.49 UG/L
0.33 UG/L
0 Not Found UG/L
Not Found UG/L
33415 0.45 UG/L
0 Not Found UG/L
Not Found UG/L
11027 0.23 UG/L
58539
53467
86237
28970
47911
72264
50824
41753
33950
39464
0.60 UG/L
0.67 UG/L
1.00 UG/L
0.42 UG/L
0.55 UG/L
0.81 UG/L
0.53 UG/L
0.52 UG/L
0.72 UG/L
0.69 UG/L
46850 0.56 UG/L
35828 0.84 UG/L
Not Found UG/L
13850 0.49 UG/L
Fit
694
978
527
373
937
451
983
993
993
94 7
869
0
958
502
138
925
970
965
962
957
912
956
985
959
973
987
991
882
295
950
Rf
0.000
0.514
0.000
0.000
1. 691
0.000
3.063
6.569
6.569
3.176
0.000
0.000
3.289
0.000
0.000
2.094
4.300
3.546
3.814
3.058
3.881
3.935
4.248
3.559
2.091
2.538
3.678
1.879
0.000
1.239
Operator ID: MC
Output File: AE01077.1A2
Data File: A£01077.MS
Name: AE01077
QUANT REPORT
Sample: Location: 516 N. Lawrence St. SB06-F
ID File: 826AEC10.QCI
Page
Quant Time: 03/29/99 18:51
Injected at: 03/13/99 03:29
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.29 g
Last Calibration: 03/10/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/10/99 17:22
R.T. Scan# Q ion
26.95 2309
27.25 2335
27.83 2385
225
128
180
Area
12680
15899
12868
Cone
0.55
0.36
0.51
untf~· -~r·
Fit Rf
--------,;· UG/L: 979 1.016
UG/L 969 1.981
UG/L 934 1.121
.· ...
Operator ID: MC
Output File: AE01207.1A2
Data File: AE01207.MS
Name: AE01207
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-A
ID File: 826AEC28.QCI
Page
Quant Time: 04/08/99 08:48
Injected at: 03/30/99 13:01
Dilution Factor: 1.00
rnstrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SGl
3) 1,2-Dichlorobepzene-d4 (SG)
4) 75-71-8 DicPlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
vinyl Chloride
Brornomethane
Chlt>roethane
Tri c:hloro f l uorome thane
1.1-Dichloroethene
MetJlylene Chloride
Tra~s-1,2-Dichloroethene
1,1-Dichloroethane
Cis•1,2-Dichloroethene
2,2-Dichloropropane
Bronlochloromethane
Chlc>roform
1,1,1-Trichloroethane
1,1-Dichloropropene
Car~on Tetrachloride
Ben,:ene
1,2-Dichloroethane
Tri(.hloroethene
1,2,-Dichloropropane
Dibr"Omomethane
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
30)
75-27-4 Bro~odichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02~6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.06
21.17
23.95
4.57
0.00
0.00
6.42
0.00
7.37
0.00
9.62
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
14.68
0.00
0.00
0.00
0.00
16. 8 3
0.00
0.00
1205
1813
2052
392
438
466
550
572
632
737
824
874
942
1033
1033
1069
1079
1112
1136
1140
1167
1171
1258
1291
1309
1324
1395
1442
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2279955
898842
497833
3910
10.00
8.53
7.32
0.05
UG/L
UG(L
UG/L
UG/L
0 Not Found UG/L
0 Not Found UG/L
1724 0.09 UG/L
0 Not Found UG/L
7581 0.06 UG/L
Not Found UG/L
1612566 7.33 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
15292 0.06 UG/L
0 Not Found UG/L
667 0.01 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
21730 0.07 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
829
233
367
655
0
986
465
989
449
485
295
519
413
110
652
481
918
996
861
858
272
350
720
736
984
585
586
Rf
1.000
0.4.1\3
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.966
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01207.1A2
Data File: AE01207.MS
Name: AE01207
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-A
ID File: 826AEC28.QCI
Page 2
Quant Time: 04/08/99 08:48
Injected at: 03/30/99 13:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38)
3 9)
40)
41)
42)
43)
44)
45)
4 6)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.77 1523
0.00 1556
0.00 1579
0.00 1648
0.00 1656
19.36 1659
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 0.00
1674
1674
1734
1734
1770
1785
1827
1836
1842
1848
1866
1869
1874
1921
1929
1954
1972
1987
1993
2030
2055
2182
2336
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylberizene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
0.00
0.00
0.00
0.00
0.00
21.57
0.00
21.81
0.00
0.00
22.51
0.00
23.02
0.00
23.27
23.70
0.00
0.00
27.27
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
2266 0.04 UG/L
31888
70515
70515
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.09 UG/L
0. 12 UG/L
0.12 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
115754 0.30 UG/L
Not Found UG/L
51618 0.17 UG/L
0 Not Found UG/L
0 Not Found UG/L
194419 0.67 UG/L
Not Found UG/L
35806 0.13 UG/L
Not Found UG/L
134293 0.84 UG/L
58777 0.24 UG/L
0 Not Found UG/L
Not Found UG/L
30949 0.49 UG/L
Fit
459
973
119
135
473
396
926
993
995
573
4 33
111
667
720
39
487
895
954
927
859
459
911
0
974
974
983
871
654
312
957
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1. 510
2. 64 9
2. 64 9
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.673
0.000
1.354
0.000
0.000
1.277
0.000
1.224
0.000
0.703
1.075
0.000
0.000
0. 276
Operator ID: MC
Output File: AE01207.1A2
Data File: AE01207.MS
Name: AE01207
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-A
ID File: 826AEC28.QCI
Page
Quant Time: 04/08/99 08:48
Injected at: 03/30/99 13:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2364
27.95 2395
28.51 2443
225
128
180
Area
32126
80564
19797
Cone Units
0.53 UG/L
0.59 UG/L
0.30 UG/L
Fit
981
990
976
Rf
0.269
0.596
0. 291
Operator ID: MC
Output File: AE01208.1A2
Data File: AE01208.MS
Name: AE01208
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 17:57
Injected at: 03/29/99 22:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.16 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2 -Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.03
21.14
23.92
4.54
0.00
5.41
6.41
0.00
7.37
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
14.68
0.00
0.00
0.00
0.00
16.81
0.00
0.00
1202
1811
2050
388
438
463
549
564
631
737
822
874
943
1033
1033
1069
1079
1112
1136
1139
1166
1165
1257
1291
1309
1327
1390
1440
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2149111
969256
622087
4628
10.00
9.76
9.70
0.06
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
312 0.01 UG/L
6847 0.39 UG/L
0 Not Found UG/L
7569 0.07 UG/L
Not Found UG/L
866095 4.16 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
16808 0.07 UG/L
Not Found UG/L
899 0.01 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
23668 0.08 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
950
832
38
652
626
736
974
232
960
556
600
537
558
519
118
646
576
769
989
894
714
385
60
461
635
981
610
697
Rf
1.000
0.463
0.299
0.361
0.000
0.226
0.081
0.000
0.526
0.000
0.970
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01208.1A2
Data File: AE01208.MS
Name: AE01208
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-B
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 17:57
Injected at: 03/29/99 22:27
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.16 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
4 7)
48)
49)
50)
51)
52)
53)
54)
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
55) 541-73-1
56) 106-46-7
57JV 104-51-a
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1523
0.00 1556
0.00 1579
0.00 1648
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.21
1656
1658
1671
1671
1733
1731
1770
1785
1825
1836
1846
1841
1869
1868
1884
1920
1926
1950
1969
1991
1991
2035
2052
2183
2337
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.84
o.oo 0.00
21.54
21.49
0.00
21.80
21.99
22.41
22.48
22.76
22.98
23.24
23.24
23.75
23.96
o.oo 27.27
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
2293 0.04 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
110488 0.34 UG/L
145596
145596
65848
29826
0.26 UG/L
0.26 UG/L
0.23 UG/L
0.20 UG/L
0 Not Found UG/L
80654 0.26 UG/L
Not Found UG/L
0 Not Found UG/L
18694 0.10 UG/L
33675 0.09 UG/L
0 Not Found UG/L
241817 0.83 UG/L
23293 0.10 UG/L
103852 0.35 UG/L
126271
110812
93703
140793
140793
71862
82369
0.46 UG/L
0.34 UG/L
0. 3 6 UG/L
1.06 UG/L
0.93 UG/L
0.31 UG/L
0.66 UG/L
0 Not Found UG/L
22836 0.39 UG/L
Fit
402
917
634
361
573
508
978
991
992
766
958
320
919
457
677
839
928
959
959
985
926
941
934
959
970
978
980
703
415
948
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.702
0.000
1. 470
0.000
0.000
0.855
1.673
0.000
1.354
1.120
1.386
1. 277
1. 530
1.224
0.620
0.703
1.075
0.579
0.000
0.276
Operator ID: MC
Output File: AE01208.1A2
Data File: AE01208.MS
Name: AE01208
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 17:57
Injected at: 03/29/99 22:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.16 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.60 2364
27.93 2393
28.54 2445
225
128
180
Area
22468
56028
24983
Cone Units
0. 39 UG/L
0.44 UG/L
0.40 UG/L
Fit
971
985
950
Rf
0.269
0.596
0. 291
~------------------------------------------------------------------ - - --
Operator ID: MC
Output File: AE01209.1A2
Data File: AE01209.MS
Name: AE01209
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:02
Injected at: 03/29/99 23:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 4.98 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Mechylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,~-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Ca~bon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
R.T. Scan# Q ion Area Cone Units
14.04 1201
21.14 1810
23.92 2048
4.53
0.00
0.00
6.42
0.00
7.34
0.00
9.61
0.00
387
438
466
549
565
629
737
821
874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1134
0.00 1134
13.62 1165
13.59 1163
14.64 1253
0.00 1296
0.00 1309
0.00 1327
0.00 1389
16.81 1439
0.00 1464
0.00 1495
96 2121308
95 1010176
152 623273
10.00 UG/L
10.30 UG/L
9.85 UG/L
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4212 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
18593 1.09 UG/L
0 Not Found UG/L
6714 0.06 UG/L
Not Found UG/L
749988 3.64 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
11445 0.05 UG/L
1172 0.01 UG/L
769 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
19869 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
948
854
53
211
691
797
985
488
993
4 94
374
512
501
451
45
266
787
912
987
870
825
472
428
601
652
980
653
761
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.430
0.291
0.000
0.000
0.000
0.000
l. 369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01209.1A2
Data File: AE01209.MS
Name: AE01209
Quant Time: 03/30/99 18:02
Injected at: 03/29/99 23:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 221 Randolph St. SB07-C
ID File: 826AEC28.QCI
Comment: Sampling: 02/18/1999 by J. Conway, use 4.98 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
3 3)
34)
35)
3 6)
3 7)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.78
0.00
0.00
0.00
0.00
19.38
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.21
Styrene 20.23
Bromoform 0.00
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
0.00
21.48
21.53
21.83
21.77
21.98
22.40
22.48
22.77
23.00
23.16
23.24
23.76
24.02
25.49
27.27
1520
1522
1S55
1578
1648
1655
1659
1670
1670
1731
1732
1769
1784
1824
1835
1840
1844
1869
1864
1882
1918
1925
1950
1969
1983
1990
2034
2057
2182
2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
1656
94408
108865
108865
61197
15843
Cone Units
Not Found UG/L
0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.29 UG/L
0.19 UG/L
0.19 UG/L
0.22 UG/L
0.11 UG/L
Not Found UG/L
71303 0.23 UG/L
0 Not Found UG/L
0 Not Found UG/L
17117 0.09 UG/L
84 734
125275
210965
25180
88785
114195
91689
89596
12766
12 04 8 3
64442
12159
1749
23531
0.24 UG/L
0.48 UG/L
0.73 UG/L
0.11 UG/L
0.30 UG/L
0.42 UG/L
0.28 UG/L
0.35 UG/L
0.10 UG/L
0.81 UG/L
0.28 UG/L
0.10 UG/L
0.10 UG/L
0.40 UG/L
Fit
356
921
698
518
623
390
981
992
990
753
896
417
930
306
513
902
94 5
953
959
984
945
938
954
936
977
973
982
720
569
935
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1. 510
2.649
2.649
1. 305
0.701
0.000
1.470
0.000
0.000
0.855
1.673
1. 234
1.354
1.120
1. 386
1.277
1.530
1.224
0.620
0.703
1.075
0.579
0.083
0.276
Operator ID: MC
Output File: AE01209.1A2
Data File: AE01209.MS
Name: AE01209
QUAN'I' REPORT Page
Quant Time: 03/30/99 18:02
Injected at: 03/29/99 23:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 221 Randolph St. SB07-C
ID File: 826AEC28.QCI
Comment: Sampling: 02/18/1999 by J. Conway, use 4.98 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.60 2364 225 22985 0.40
62) 91-20-3 Naphthalene 27.94 2393 128 52211 0.41
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2445 180 264 02 0.43
* Compound is ISTD
Units Fit Rf
--------
UG/L 972 0.269
UG/L 984 0.596
UG/L 962 0.291
... '1
Operator ID: MC
Output File: AE01210.1A2
Data File: AE01210.MS
Name: AE01210
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:03
Injected at: 03/29/99 23:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2)
3)
4)
4-Bromofluorobenzene (SG)
1,2-Dichlorobenzene-d4 (SG)
75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Tiichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.04 1202 96 2140704 10.00 UG/L
10.13 UG/L
9.58 UG/L
0.06 UG/L
21.14
23.93
4.54
0.00
0.00
6. 4 9
0.00
7.35
0.00
9.59
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.23
0.00
13.59
0.00
14.67
0.00
0.00
0.00
0.00
16.78
0.00
0.00
1811
2050
388
438
469
556
566
629
737
821
874
943
1033
1027
1069
1079
1112
1133
1133
1164
1164
1256
1291
1309
1334
1390
1438
1464
1498
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91.
75
83
1002681
612052
4452
Not Found UG/L
Not Found UG/L
1599 0.09 UG/L
Not Found UG/L
7812 0.07 UG/L
0 Not Found UG/L
785636 3.78 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
332 0.00 UG/L
0 Not Found UG/L
15424 0.07 UG/L
0 Not Found UG/L
1115 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
22473 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
945
847
529
712
910
981
521
994
308
642
634
777
516
0
354
750
830
996
895
746
"363
193
811
516
989
660
710
Rf
1. 0 0 0
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.402
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1. 369
0.000
0.000
QUANT REPORT Page 2
Operator ID: Me
Output File: AE01210.1A2
Data File: AE01210.MS
Name: AE01210
Quant Time: 03/30/99 18:03
Injected at: 03/29/99 23:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 221 Randolph St. SB07-D
ID File: 826AEC28.QCI
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33 I
34)
35)
36 I
37)
38)
39)
40 I
41)
42)
43)
44)
4 5 I
4 6)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-.8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-i
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.75
o.oo o.oo o.oo o.oo
19.32
1,3-Dimethylbenzene (m-Xylene 19.51
1,4-Dimethylbenzene (p-Xylene 19.51
1,2-Dimethylbenzene (a-Xylene 20.22
Styrene 20.20
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec,Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.80
o.oo o.oo o.oo
21.51
21.89
21.75
21.93
22.41
22.47
22.76
22.98
23.10
23.22
23.75
o.oo 25.43
27.28
1521
1521
1556
1579
1648
1656
1655
1671
1671
1732
1730
1770
1782
1825
1836
1841
184 3
1875
1864
1879
1919
1925
1950
1969
1979
1990
2035
2055
2179
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
2576 0.04 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
86722 0.27 UG/L
127162
127162
50201
18536
0.22 UG/L
0.22 UG/L
0.18 UG/L
0.12 UG/L
Not Found UG/L
91656 0.29 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
117541
15627
215600
43524
100773
118989
99920
89648
54122
136026
70130
3220
25090
0.33 UG/L
0.06 UG/L
0.74 UG/L
0.18 UG/L
0.34 UG/L
0.44 UG/L
0. 31 UG/L
0.34 UG/L
0.41 UG/L
0.90 UG/L
0.31 UG/L
Not Found UG/L
0.18 UG/L
0.42 UG/L
Fit
251
962
613
615
689
440
972
990
991
741
929
105
950
290
589
828
958
973
957
980
930
936
960
955
987
971
983
683
501
954
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.702
0.000
1. 4 70
0.000
0.000
0.000
1.673
1.234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.000
0.083
0.276
Operator ID: MC
Output File: AE01210.1A2
Data File: AE01210.MS
Name: AE01210
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:03
Injected at: 03/29/99 23:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2364
27.94 2394
28.51 2443
225
128
180
Area
24223
51733
25244
Cone Units
0.42 UG/L
0.41 UG/L
0.41 UG/L
Fit
971
985
966
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01211.1A2
Data File: AE01211.MS
Name: AE01211
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:03
Injected at: 03/30/99 00:26
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. conway, use 4.48 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1.2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13)
14)
15)
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Ben~ene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
26) 75-27-4 Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.04
21.15
23.93
4.54
0.00
0.00
6.40
0.00
7.36
8.60
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
13.61
14.67
0.00
0.00
1202
1811
2049
388
438
466
548
572
630
735
821
878
938
1033
1033
1069
1078
1112
1136
1137
1166
1164
1255
1291
1309
0.00 1327
0.00 1389
16.81 1439
0.00 1464
0.00 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area· Cone Units
1978641
955417
562532
5426
10.00 UG/L
10.45 UG/L
9.53 UG/L
0.08 UG/L
Not Found UG/L
Not Found UG/L
8712 0.54 UG/L
0 Not Found UG/L
8514 0.08 UG/L
507 0.01 UG/L
823731 4.29 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
18690 0.09 UG/L
1979
1183
0.02
0.02
UG/L
UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
23282 0.09 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
1000
953
827
65
478
811
807
983
918
976
756
762
603
483
452
83
647
663
852
996
896
856
200
411
519
449
981
551
556
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.225
0.970
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.430
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01211.1A2
Data File: AE012ll.MS
Name: AE01211
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-E
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:03
Injected at: 03/30/99 00:26
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 4.48 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.77 1521
18.18 1556
0.00
19.22
0.00
19.35
1,3-Dimethylbenzene 1m-Xylene 19.52
1575
1645
1655
1656
1671
1,4-Dimethylbenzene (p-Xylene 19.52 1671
1,2-Dimethylbenzene (a-Xylene 20.23 1732
Styrene 20.24 1733
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1769
20.82 1782
0.00 1824
0.00 1835
21.50 1841
21.53 1844
21.83 1869
21.79 1866
21.93 1878
22.43 1920
22.50 1926
22.80 1952
22.98 1968
23.10 1978
23.24 1990
23.77 2035
0.00 2054
0.00 2182
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
8262
1316
Cone Units
Not Found UG/L
0.15 UG/L
0.02 UG/L
Not Found UG/L
3822 0.02 UG/L
0 Not Found UG/L
85703 0.29 UG/L
99552
99552
50186
23684
0.19 UG/L
0.19 UG/L
0.19 UG/L
0.17 UG/L
Not Found UG/L
87923 0.30 UG/L
Not Found UG/L
Not Found UG/L
24168 0.14 UG/L
68285
24184
209581
54 098
99875
11722 3
104960
89531
33614
118934
69223
0.21 UG/L
0.10 UG/L
o.78 ug/L
0.24 UG/L
0.36 UG/L
0.46 UG/L
0.35 UG/L
0.37 UG/L
0.27 UG/L
0.86 UG/L
0.33 UG/L
0 Not Found UG/L
0 Not Found UG/L
25908 0.47 UG/L
Fit
351
981
863
811
869
353
977
993
993
762
912
298
943
317
84
914
947
954
953
988
938
955
978
964
987
972
984
691
341
934
Rf
0.000
0.284
0.282
0.000
0.858
0.000
1. 510
2.649
2.649
1.305
0.702
0.000
1.470
0.000
0.000
0.855
1.673
1. 234
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0. 276
Operator ID: MC
Output File: AE01211.1A2
Data File: AE0121l.MS
Name: AE01211
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:03
Injected at: 03/30/99 00:26
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 4.48 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.58 2362
27.94 2393
28.53 2444
225
128
180
Area
25164
53508
26296
Cone Units
0.47 UG/L
0.45 UG/L
0.46 UG/L
Fit
976
985
975
Rf
0.269
0.596
0.291
'·
Operator ID: MC
Output File: AE01212.1A2
Data File: AE01212.MS
Name: AE01212
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:04
Injected at: 03/30/99 01:05
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
16)
17)
18)
19)
2 0)
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
3 0)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.05
21.15
23.94
4.54
0.00
0.00
6.41
0.00
7.37
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
14.69
0.00
0.00
0.00
0.00
16.81
0.00
0.00
1203
1812
2051
389
438
466
549
573
631
737
823
879
941
1033
1033
1069
1079
1112
1136
1144
1167
1165
1'258
1284
1309
1327
1390
1440
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2061759
927905
587941
5050
10.00 UG/L
9. 74 UG/L
9.56 UG/L
0.07 UG/L
Not Found UG/L
Not Found UG/L
12780 0.77 UG/L
Not Found UG/L
7170 0.07 UG/L
Not Found UG/L
715561 3.58 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
14554 0.06 UG/L
Not Found UG/L
824 0.01 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
22310 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
950
899
113
350
715
717
987
556
979
744
898
661
569
631
46
551
498
906
993
883
722
452
342
502
611
976
640
576
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01212.1A2
Data File: AE01212.MS
Name: AE01212
Quant Time: 03/30/99 18:04
Injected at: 03/30/99 01:05
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 221 Randolph-st. SB07-F
ID File: 826AEC28.QCI
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
4 3)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1523
0.00
0.00
19.23
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.24
Bromoform 0.00
Isopropylbenzene 20.75
1,1,2,2-Tetrachloroethane 0.00
1,2,3-Trichloropropane
Bromobenzene
·n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-0ichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
21.47
21.56
21.82
21.76
21.92
22.40
22.50
22.80
22.99
23.14
23.26
23.77
24.01
0.00
27.30
1555
1579
1647
1656
1657
1673
1673
1733
1734
1770
1777
1825
1836
1839
1847
1869
1864
1878
1919
1927
1953
1969
1982
1993
2036
2057
2187
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
• Compound is ISTD
Area Cone Units
0 Not Found UG/L
2795 0.05 UG/L
0 Not Found UG/L
Not Found UG/L
3560 0.02 UG/L
Not Found UG/L
69774 0.22 UG/L
1032 3 7
103237
46422
21731
0. 19 UG/L
0.19 UG/L
0.17 UG/L
0.15 UG/L
Not Found UG/L
28084 0.09 UG/L
0 Not Found UG/L
Not Found UG/L
8449
94033
79830
11194 6
58515
87424
110601
86632
81691
60687
128744
80714
0. 05 UG/L
0.27 UG/L
0. 31 UG/L
0.40 UG/L
0.25 UG/L
0. 31 UG/L
0.42 UG/L
0.27 UG/L
0.32 UG/L
0.48 UG/L
0.89 UG/L
0.36 UG/L
29961 0.25 UG/L
Not Found UG/L
21942 0.39 UG/L
Fit
273
946
718
592
732
523
978
986
990
738
926
309
956
262
642
815
930
945
959
982
916
950
984
957
983
984
976
711
733
94 7
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2.649
2.649
1.305
0.702
0.000
1.470
0.000
0.000
0.855
1.673
1.234
1. 3 54
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01212.1A2
Data File: AE01212.MS
Name: AE01212
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:04
Injected at: 03/30/99 01:05
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.60 2365 225 21359 0.39
62) 91-20-3 Naphthalene 27.94 2394 128 55600 0.45
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2446 180 22928 0.38
• Compound is ISTD
Units Fit Rf
--------UG/L 973 0. 269
UG/L 986 0.596
UG/L 971 0. 291
Operator ID, MC
Output File, AE01213.1A2
Data File' AE01213.MS
Name, AE01213
QUANT REPORT
Sample, Location, 221 Randolph St. SB07-G
ID File: 826AEC28.QCI
Page
Quant Time, 03/30/99 18,05
Injected at, 03/30/99 01,44
Dilution Factor' 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/18/1999 by J. Conway, use 4.74 g
Last Calibration, 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/29/99 09,28
R.T. Scan# Q ion
14.03
21.14
23.93
4.57
0.00
1201
1810
2049
391
438
0.00 466
6.40 548
0.00 572
7.36 630
0.00 737
9.60 821
0.00 877
0.00 936
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1133
13.60 1164
0.00 1161
14.68 1256
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.80 1438
0.00 1464
0.00 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2363542
931478
611290
4353
10.00 UG/L
8.53 UG/L
8.67 UG/L
0.05 UG/L
Not Found UG/L
Not Found UG/L
1794 0.09 UG/L
Not Found UG/L
8955 0.07 UG/L
Not Found UG/L
823699 3.59 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
·a Not Found UG/L
Not Found UG/L
16041 0.06 UG/L
0 Not Found UG/L
747 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
30845 0.10 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
952
826
219
421
688
65
979
97
983
725
721
199
380
345
4
252
431
773
997
892
704
369
582
388
221
987
616
473
Rf
1.000
0. 4 63
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1. 369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01213.1A2
Data File: AE01213.MS
Name: AE01213
Quant Time: 03/30/99 18:05
Injected at: 03/30/99 01:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 221 Randolph St. SB07-G
ID File: 826AEC28.QCI
Comment: Sampling: 02/18/1999 by J. Conway, use 4.74 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.76
0.00
0.00
0.00
0.00
19.30
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.18
Styrene 20.26
1520
1520
1558
1578
1648
1655
1653
1670
1670
1728
1734
1769
1777
1824
1835
1837
1842
1870
1863
1878
1917
1923
1951
1969
1988
1988
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzen·e
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.76
0.00
0.00
21.46
21.51
21.84
21.76
21.94
22.39
22.45
22.79
23.00
23.22
23.22
23.73 2032
24.02 2057
0.00 2182
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
14 6
75
180
Area Cone Units
0 Not Found UG/L
2121 0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
50033 0.14 UG/L
110361 0.18 UG/L
110361
18595
10576
0.18 UG/L
0.06 UG/L
0.06 UG/L
0 Not Found UG/L
27463 0.08 UG/L
Not Found UG/L
0 Not Found UG/L
11998 0.06 UG/L
69668 0.18 UG/L
40598
193464
334 04
91243
95710
90514
80380
73024
73024
75190
10120
0.14 UG/L
0. 60 UG/L
0.13 UG/L
0.28 UG/L
0.32 UG/L
0.25 UG/L
0.28 UG/L
0.50 UG/L
0.44 UG/L
0.30 UG/L
0.07 UG/L
0 Not Found UG/L
20266 0.31 UG/L
Fit
281
900
700
560
640
566
978
991
993
708
902
145
929
322
488
797
963
960
950
985
929
942
969
950
983
980
966
752
461
939
RE
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1.470
0.000
0.000
0.855
1. 673
1.234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.704
1.075
0.579
0.000
0.276
Operator ID: MC
Output File: AE01213.1A2
Data File: AE01213.MS
Name: AE01213
QUANT REPORT
Sample: Location: 221 Randolph St. SB07-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:05
Injected at: 03/30/99 01:44
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/18/1999 by J. Conway, use 4.74 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2363
27.93 2391
28.53 2443
225
128
180
Area
22037
49879
21813
Cone Units
0.35 UG/L
0.35 UG/L
0.32 UG/L
Fit
972
977
972
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01216.1A2
Data File: AE01216.MS
Name: AE01216
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 02:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 2.14 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene ISG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5)
6)
7)
8)
9)
10)
11)
12)
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachlgride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.04
21.16
23.94
4.54
0.00
0.00
6.40
6. 71
7.36
0.00
9.61
0.00
1202
1812
2050
389
438
470
548
574
630
737
822
874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1111
0.00 1136
0.00 1134
13.62 1165
0.00 1164
14.68 1256
0.00 1291
0.00 1309
0.00 1327
0.00
16.81
0.00
0.00
1389
1439
1463
1493
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
19616 52
765486
475285
4148
10708
327
6828
826486
Cone
10.00
8.44
8.12
0.06
Units
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
Not Found UG/L
0.68 UG/L
0.03 UG/L
0.07 UG/L
Not Found UG/L
4.35 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
19197 0.09 UG/L
0 Not Found UG/L
548 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
61011 0.23 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
954
843
0
531
738
780
984
368
991
558
320
331
293
672
294
812
560
906
993
903
821
224
493
638
480
981
508
656
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.970
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01216.1A2
Data File: AE01216.MS
Name: AE01216
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-A
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 02:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 2.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100,41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56)
57)
58)
59)
60)
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.78
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.51
1,4-Dimethylbenzene (p-Xylene 19.51
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.23
1522
1555
1578
1648
1655
1656
1671
1671
1732
1732
1769
1784
1824
1835
1829
1844
1873
1867
1878
1921
1926
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
.20. 83
0.00
0.00
21.36
21.54
0.00
21.80
21.94
22.44
22.50
22.81 1953
23.01 1970
23.25 1991
23.25
23.74
23.98
o.oo 27.31
1991
2033
2054
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
3639 0.07 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
94775 0.32 UG/L
220645 0.42 UG/L
220645
83527
18100
0.42 UG/L
0.33 UG/L
0.13 UG/L
0 Not Found UG/L
79046 0.27 UG/L
4089
96539
Not Found UG/L
Not Found UG/L
0.02 UG/L
0.29 UG/L
0 Not Found UG/L
171061 0.64 UG/L
46654
62535
304311
86651
72597
221208
221208
63176
42448
21366
0.21 UG/L
0.23 UG/L
1.22 UG/L
0.29 UG/L
0.30 UG/L
1.82 UG/L
1. 61 UG/L
0. 30 UG/L
0.38 UG/L
Not Found UG/L
0.39 UG/L
Fit
227
958
585
626
575
301
991
996
998
964
855
87
945
399
505
820
970
963
992
977
920
993
969
947
987
986
982
811
936
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2. 649
1.305
0.702
0.000
1.470
0.000
0.000
0.855
1.673
0.000
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.579
0.000
0.276
Operator ID: MC
Output File: AE01216.1A2
Data File: AE01216.MS
Name: AE01216
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 02:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. conway, use 2.14 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62 2366
27.95 2394
28.53 2444
225
128
180
Area
9803
186175
21622
Cone Units
0.19 UG/L
1.59 UG/L
0.38 UG/L
Fit
961
993
919
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01217.1A2
Data File: AE01217.MS
Name: AE01217
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 03:03
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. conway, use 4.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3)
4)
5)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14. 06
21.16
23.97
4.55
0.00
0.00
6.42
6.69
7.37
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
0.00
0.00
0.00
0.00
1204
1813
2053
389
438
466
549
573
631
737
823
874
94 5
1033
1033
1069
1079
1110
1136
1139
1167
1170
1259
12 91
1309
1327
0.00 1390
16.82 1441
0.00 1464
0.00 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1931237
833237
519741
4082
10.00 UG/L
9. 3 3 UG/L
9.02 UG/L
0.06 UG/L
0 Not Found UG/L
Not Found UG/L
0. 93 UG/L 14531
769 0.07 UG/L
6199 0.06 UG/L
0 Not Found UG/L
683774 3.65 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
13025 0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
18120 0.07 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
953
833
401
709
887
976
12
993
71
898
426
530
418
308
756
608
761
993
880
506
323
467
421
577
969
553
628
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.000
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01217.1A2
Data File: AE01217.MS
Name: AE01217
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 03:03
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence St. SB08-B
ID File: 826AEC28.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 4.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion
31)
32)
33)
34)
35)
36)
3 7)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.25
Styrene 20.25
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4 -·chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.76
0.00
0.00
21.54
21.53
0.00
21.77
21.96
22.41
22.49
22.78
23.01
23.16
23.16
23.77
0.00
0.00
27.30
• Compound is ISTD
1521
1523
1556
1579
1648
1656
1658
1673
1673
1735
1735
1770
1778
1825
1836
1845
1844
1874
1865
1881
1920
1927
1952
1971
1984
1984
2037
2055
2188
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
2667 0.05 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
76897 0.26 UG/L
99801 0.20 UG/L
99801
35657
17421
0.20
0.14
0.13
UG/L
UG/L
UG/L
0 Not Found UG/L
29471 0.10 UG/L
Not Found UG/L
Not Found UG/L
19926 0.12 UG/L
36128 0. 11 UG/L
0 Not Found UG/L
90857 0.35 UG/L
55615 0.26 UG/L
85400
105507
82255
80822
17643
17295
0.32 UG/L
0.43 UG/L
0. 28 UG/L
0.34 UG/L
0.15 UG/L
0.13 UG/L
74777 0.36 UG/L
Not Found UG/L
Not Found UG/L
20634 0.39 UG/L
Fit
127
963
638
627
603
664
980
993
996
745
958
443
94 0
240
565
813
962
944
963
980
941
94 9
94 0
954
988
978
969
699
539
94 3
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2. 64 9
1.305
0.702
0.000
1.470
0.000
0.000
0.855
1.673
0.000
1.354
1.120
1 . 3 86
1.277
1.530
1.224
0.620
0. 704
1. 074
0.000
0.000
0.276
I'
Operator ID: MC
Output File: AE01217.1A2
Data File: AE01217.MS
Name: AE01217
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:06
Injected at: 03/30/99 03:03
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.14 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.61 2365
27.95 2395
28.56 2447
225
128
180
Area
18903
69843
22713
Cone Units
0.37 UG/L
0.61 UG/L
0.41 UG/L
Fit
975
986
926
Rf
0.269
0. 596.
0.291
a '
Operator ID: MC
Output File: AE01218.1A2
Data File: AE01218.MS
Name: AE01218
QUANT REPORT
Samplg: Location: N. Lawrence St. SB08-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:07
Injected at: 03/30/99 03:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.81 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9 Bromomethane
8) 75-00-3 Chloroethane
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.15
23.94
4.56
0.00
0.00
6.41
0.00
7.37
0.00
9.61
0.00
0.00
1203
1812
2051
390
438
466
54 9
573
631
737
823
874
945
0.00 1033
0.00 1023
0.00 1069
a.aa 1079
0.00 1112
0.00 1136
0.00 1145
13.62 1167
0.00
14.70
0.00
0.00
0.00
0.00
16.81
0.00
0.00
1167
1259
1291
1309
1327
1390
1440
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2039060
921678
548326
3981
10.00 UG/L
9.78 UG/L
9.01 UG/L
0.05 UG/L
10871
5829
749649
Not Found UG/L
Not Found UG/L
0.66 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
3.79 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
15421 0.07 UG/L
Not Found UG/L
617 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
18503 0.07 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
997
999
94 9
855
0
333
638
640
984
0
979
577
898
307
615
706
22
636
545
881
994
870
728
282
673
639
604
977
606
609
Rf
1.000
0. 463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1. 369
0.000
0.000
Operator ID: MC
Output File: AE01218.1A2
Data File: AE01218.MS
Name: AE01218
QUANT REPORT
Sample: Location: N. Lawrence St. SBOB-C
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:07
Injected at: 03/30/99 03:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.81 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35)
36)
37)
38)
39)
40)
41)
42)
43)
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-~
47) 103-65-~
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-1
57) 104-51-S
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is !STD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
o.oo· 1521
17.78 1523
18.19 1558
0.00 1585
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene '20.23
1648
1656
1657
1672
1672
1733
1735
1770
1782
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.25
0.00
20.80
0.00 1825
21.34 1828
21.51 1843
21.51 1843
0.00 1872
21.81 1868
21.92 1878
22.40 1919
22.50 1928
22.80 1953
23.01 1971
23.14 1982
23.26 1993
23.75 2035
0.00 2055
0.00 2183
27.30 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
2944 0.05 UG/L
694 0. 01 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
37483 0.12 UG/L
97223
97223
0.18 UG/L
0.18 UG/L
29995 0.11 UG/L
15732 0.11 UG/L
Not Found UG/L
43159 0.14 UG/L
Not Found UG/L
7334 0.10 UG/L
19834
45005
0.11 UG/L
0.13 UG/L
0 Not Found UG/L
172503 0.63 UG/L
47665
44894
97874
84271
69629
27800
112354
53617
0.21 UG/L
0.16 UG/L
0. 3 8 UG/L
0.27 UG/L
0.28 UG/L
0.22 UG/L
0.78 UG/L
0.24 UG/L
0 Not Found UG/L
0 Not Found UG/L
18538 0.33 UG/L
Fit
347
912
BOO
876
608
455
980
990
989
761
898
349
953
544
753
780
953
971
960
983
947
932
943
943
979
968
944
666
290
918
Rf
0.000
0. 284
0.282
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1. 470
0.000
0.357
0.855
1.673
0.000
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01218.1A2
Data File: AE01218.MS
Name: AE01218
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:07
Injected at: 03/30/99 03:42
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.81 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62 2366
27.94 2394
28.55 2446
225
128
180
Area
19853
52684
22409
Cone Units
0.36 UG/L
0.43 UG/L
0.38 UG/L
Fit
966
982
966
Rf
0.269
0. 596
0. 291
Operator ID: MC
Output File: AE01219.1A2
Data File: AE01219.MS
Name: AE01219
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-D
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page
03/30/99 18:08
03/30/99 04:22
1.00
20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.91 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14. 03
21.14
23.92
4.55
1200
1810
2048
390
0.00 438
0.00 466
6.51 557
0.00 572
7.36 630
0.00 737
9.60 821
0.00 874
o.oo 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1129
0.00 1132
13.59 1163
0.00 1163
0.00 1258
0.00 1289
0.00 1309
0.00 1327
0.00 1389
16.80 1438
0.00 1464
0.00 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2406878
818285
532869
3885
10.00 UG/L
7. 3 5 UG/L
7.42 UG/L
0. 04 UG/L
Not Found UG/L
0 Not Found UG/L
1650 0.08 UG/L
Not Found UG/L
7695 0.06 UG/L
Not Found UG/L
760531 3.25 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
12514 0.05 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
19890 0.06 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
954
808
185
273
670
987
294
989
582
87
294
288
668
0
544
740
846
995
879
537
411
541
432
607
988
699
582
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.000
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01219.1A2
Data File: AE01219.MS
Name: AE01219
QUANT REPORT
Sample: Location: N. Lawrence St. SBOB-D
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:08
Injected at: 03/30/99 04:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.91 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52)
53)
54)
55)
56)
57)
58)
59)
60)
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.76 1520
0.00 1553
0.00
0.00
0.00
19.38
1,3-Dimethylbenzene 1m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (o-Xylene 20.22
Styrene 20.22
1578
1648
1655
1659
1670
1670
1730
1730
1769
1782
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.82
0.00 1824
0.00 1835
21.41 1833
21.52 1842
21.91 1876
21.79 1865
21.92 1877
22.39 1917
22.45
22.77
22.98
23.11
23.24
23.76
0.00
0.00
27.27
1923
1950
1968
1979
1990
2034
2061
2182
2335
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
2621 0.04 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
70949
104468
104468
4 7182
15789
55699
0.20 UG/L
0.16 UG/L
0.16 UG/L
0.15 UG/L
0.09 UG/L
Not Found UG/L
0. 16 UG/L
Not Found UG/L
0 Not Found UG/L
16739 0.08 UG/L
61770
51462
177449
47663
48933
96437
80910
70767
27431
104857
26182
19387
0.15 UG/L
0.17 UG/L
0.54 UG/L
0.18 UG/L
0.15 UG/L
0. 31 UG/L
0.22 UG/L
0.24 UG/L
0.18 UG/L
0. 62 UG/L
0.10 UG/L
Not Found UG/L
Not Found UG/L
0.29 UG/L.
Fit
327
964
850
596
626
280
975
993
993
819
903
142
950
4 63
72
887
947
934
967
983
965
969
953
954
986
969
956
716
64
928
Rf
o.ooo 0.284
0.000
o.ooo o.ooo 0.000
1.510
2. 64 9
2. 649
1.305
0.701
o.ooo 1. 470
0.000
o.ooo 0.855
1. 673
1. 234
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.075
o.ooo 0.000
0.276
Operator ID: MC
Output File: AE01219.1A2
Data File: AE01219.MS
Name: AE01219
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:08
Injected at: 03/30/99 04:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 4.91 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2363
27.93 2392
28.53 2444
225
128
180
Area
17993
45533
20174
Cone
0.28
0.32
0.29
Units Fit Rf
--------'
UG/L 963 0.269
UG/L 988 0.596
UG/L 968 0.291
Operator ID: MC
Output File: AE01220.1A2
Data File: AE01220.MS
Name: AE01220
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-E
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 17:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
/
Comment: Sampling: 02/19/1999 by J. Conway, use 5.27 g
Last Calibration: 03/25/99
Compound
11 *107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SGI
31 1,2-Dichlorobenzene-d4 (SGI
41 75-71-8
51 74-87-3
61 75-01-4
71 74-83-9
81 75-00-3
91 75-69-4
101 75-35-4
111 75-09-2
121 156-60-5
131 75-34-3
141 156-59-4
151 590-20-7
161 74-97-5
171 67-66-3
181 71-55-6
191 563-58-6
201 56-23-5
211 71-43-2
221 107-06-2
231 79-01-6
241 78-87-5
251 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane 261
271
281
29 I
30 I
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.95 2051
4.55 390
0.00 438
0.00 468
0.00 549
0.00 571
7.38 632
0.00 737
9.62 823
0.00 874
11.03 943
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1132
13.64 1167
13.62 1165
14.69 1257
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1440
0.00 1464
0.00 1493
96 2308776 10.00 UG/L
95 1117878 11.02 UG/L
152 696294 11.01 UG/L
85 6272 0.11 UG/L
47 Not Found UG/L
61
96
49
101
96
49
61
63 61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
6556 0.06 UG/L
Not Found UG/L
498274 1.74 UG/L
0 Not Found UG/L
413 0.00 UG/L
22554
1826
2604
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.11 UG/L
0.02 UG/L
0.04 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
123530 0.45 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
997
999
964
868
578
539
915
968
536
957
187
758
392
699
534
233
688
431
918
981
901
876
74
349
417
352
975
574
860
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.000
0.000
0. 455
0.000
1.240
0.000
0.393
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.355
0.255
0.000
0.000
0.000
0.000
1 . 195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01220.1A2
Data File: AE01220.MS
Name: AE01220
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 17:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence St. SB08-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 5.27 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
4 0)
41)
42)
43)
44)
45)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
46) 108-86-l
47) 103-65-l
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54)
55)
56)
57)
58)
59)
60)
99-87-6
541-73-l
106-46-7
104-51-8
95-50-l
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00 1555
0.00
19.25
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1578
1648
1655
1657
1672
1,4-Dimethylbenzene (p-Xylene 19.53 1672
1,2-Dimethylbenzene (a-Xylene 20.24 1733
1735
1769
1789
1824
1835
Styrene 20.26
Bromoform 0.00
Isopropylbenzene 0.00
1,1,2,2-Tetrachloroethane 0.00
1,2,3-Trichloropropane 0.00
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1841
21.56 1846
21.79 1866
21.83 1869
22.00 1884
22.37 1915
22.50 1927
22.81 1953
23.00
23.11
23.26
23.77
0.00
0.00
27.17
1970
1978
1992
2036
2054
2182
2327
78
166
129
107
112
131
91
91
9l
91
104
171
lOS
83
75
77
91
9l
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Unit.s
Not Found UG/L
6512 0.11 UG/L
Not Found UG/L
Not Found UG/L
11837 0.07 UG/L
Not Found UG/L
51437 0.17 UG/L
85097 0.16 UG/L
85097
34 611
22599
0.16 UG/L
0.14 UG/L
0.17 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
137833 0.42 UG/L
33136 0.13 UG/L
44236
9477
20325
61841
26269
37810
51321
86459
57715
0.17 UG/L
0.04 UG/L
0.07 UG/L
0.23 UG/L
0.09 UG/L
0.16 UG/L
0.39 UG/L
0.67 UG/L
0.25 UG/L
0 Not Found UG/L
0 Not Found UG/L
41767 0.60 UG/L
Fit
247
921
129
162
707
581
746
953
963
814
751
91
843
423
364
764
833
935
799
951
872
854
948
949
900
763
917
149
609
953
R[
0.000
0.266
0.000
0.000
0.717
0.000
1.319
2.360
2.360
1.076
0.576
0.000
0.000
0.000
0.000
0.000
l. 439
l. 099
1.137
0.960
1 . 2 0 9
1.169
1 . 3 04
1.051
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID: MC
Output File: AE01220.1A2
Data File: AE01220.MS
Name: AE01220
QUANT REPORT
Sample: Location: N. Lawrence St. SB08-E
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 17:27
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.27 g
Last Calibration: 03/25/99
61} 87-68-3
62} 91-20-3
63} 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.58 2362
27.94 2393
28.53 2443
225
128
180
Area
54141
66726
39584
Cone Units
0.76 UG/L
0.49 UG/L
0.57 UG/L
Fit
984
970
981
Rf
0.309
0.586
0.304
Operator ID: MC
Output File: AE01221.1A2
Data File: AE01221.MS
Name: AE01221
QUANT REPORT
Sample: Location: N. Lawrence St. S808-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 18:22
Dilution Factor: 1.00
Instru~ent ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.05 g ·
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2·Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2 ' 23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01·5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.08 1205
21.18 1814
23.96 2053
4.55
0.00
0.00
6.42
0.00
7. 37
0.00
9.62
0.00
390
438
466
550
579
631
737
824
874
0.00 943
0.00 1033
b.oo 1033
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1137
13.64 1168
0.00 1169
14.70 1259
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.83 1442
0.00 1464
0.00 1494
96 2297623
95 1190889
152 745334
10.00 UG/L
11.81 UG/L
11.84 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4257
13656
0.07 UG/L
Not Found UG/L
Not Found UG/L
0.81 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
2.41 UG/L
Not Found UG/L
0 Not Found UG/L
5151
680851
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
14840
831
0.07 UG/L
Not Found UG/L
0.01 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
111654 0.41 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
999
999
955
830
201
271
707
851
979
222
983
650
478
575
578
539
568
374
896
980
835
785
351
521
469
349
980
560
846
Rf
1.000
0.439
0. 274
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 231
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01221 .1A2
Data File: AE01221.MS
Name: AE01221
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 18:22
Dilution Factot·: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence St. SB08-F
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 5.05 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50)
51)
52)
53)
106-43-4
98-06-6
95-63-6
135-98-8
54) 99-87-6
55)
56)
57)
58)
59)
60)
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Ch1orobenzene
1,1,1,2-Tetrachloroethane
0.00 1521
17.79 1524
0.00 1556
0.00 1579
19.26
0.00
Ethylbenzene 19.35
1,3-Dimethylbenzene 1m-Xylene 19.55
1,4-Dimethylbenzene (p-Xylene 19.55
1,2-Dimethylbenzene (a-Xylene 20.26
1650
1658
1657
1674
1674
1735
1731
1770
1786
1825
Styrene 20.21
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichloroben~ene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.85
0.00
0.00 1836
21.53 1844
21.56 1847
21.85 1872
21.74 1863
21.97
22.46
22.52
0.00
1882
1924
1929
1954
23.03 1973
23 .15
23.28
23.80
24.00
0.00
27.32
1983
1994
2039
2056
2181
2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
5333 0.09 UG/L
0 Not Found UG/L
Not Found UG/L
9585 0.06 UG/L
0 Not Found UG/L
78964
117799
117799
57600
9908
0.26 UG/L
0.22 UG/L
0.22 UG/L
0.23 UG/L
0.07 UG/L
Not Found UG/L
57020 0.20 UG/L
0 Not Found UG/L
Not Found UG/L
48587
94203
37584
64590
32617
84 902
72487
0.31 UG/L
0.29 UG/L
0.15 UG/L
0.25 UG/L
0.15 UG/L
0.31 UG/L
0.27 UG/L
0 Not Found UG/L
724 94 0.30 UG/L
85719 0.65 UG/L
96790 0.75 UG/L
80435 0.35 UG/L
49985 0.41 UG/L
Not Found UG/L
25339 0.36 UG/L
Fit
335
898
2
195
847
719
977
984
988
751
929
372
909
4 56
664
865
958
925
915
949
920
975
696
928
969
982
936
788
549
932
Rf
0.000
0.266
0.000
0.000
0.717
.000
.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.685
1.438
1.099
1.137
0. 960
1.209
1.169
0.000
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator lD: MC
Output File: AE01221.1A2
Data File: AE01221.MS
Name: AE01221
QUANT REPORT
Sample: Location: N. Lawrence St. SBOS-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:06
Injected at: 03/26/99 18:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.05 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.64 2368
27.98 2397
28.58 2448
225
128
180
27291
52144
254 73
Cone Units
0.38 UG/L
0.39 UG/L
0.37 UG/L
Fit
952
975
957
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01224.1A2
Data File: AE01224.MS
Name: AE01224
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 07:57
Injected at: 03/31/99 03:11
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 0.248 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9
B) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.07 1204
21.18 1813
23.97 2053
4.59 392
0.00 438
0.00 466
0.00 549
0.00 572
7.38 632
0.00 736
9.64 824
10.21 873
0.00 942
0.00 1030
0.00 1028
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00
13.65
0.00
0.00
15.09
0.00
0.00
0.00
16.85
0.00
0.00
1142
1168
1169
1258
1291
1309
1327
1384
1442
1464
14 94
96 3854254 10.00 UG/L
95. 1357145 7.62 UG/L
152 837737 7.28 UG/L
85 24807 0.18 UG/L
4 7 Not Found UG/L
62 Not Found UG/L
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
0 Not Found UG/L
28395 0.14 UG/L
Not Found UG/L
923412 2.47 UG/L
19435 0.11 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
40062 0.09 UG/L
0 Not Found UG/L
0 Not Found .UG/L
32655 0.45 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
337179 0.64 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
988
941
885
151
424
564
48
948
872
962
922
643
731
765
368
423
501
686
796
736
718
861
741
0
0
799
846
566
248
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.000
0.000
0.526
0.000
0.972
0.452
0.000
0.000
0.000
0.000
0.000
0.000
o.ooo o.ooo 1.098
0.000
0.000
0.189
o.ooo 0.000
o.ooo 1.369
0.000
0.000
Operator ID: Me
Output File: AE01224.1A2
Data File: AE01224.MS
Name: AE01224
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-A
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 07:57
Injected at: 03/31/99 03:11
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 0.248 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
630-20-5
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-l
47) 103-65-l
48) 95-49-8
49) 108-67-B
50) 106-43-4
51) 98-06-6
52) 95-€3-6
53) 135-98-B
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-B
58) 95-S0-1
59) 96-12-8
60) 120-82-l
• Compound is lSTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
0.00 1524
0.00 1555
0.00 1578
0.00 1648
0.00
19.35
1,3-Dimethylbenzene 1m-Xylene 19.53
1655
1656
1672
1,4-Dimethylbenzene lp-Xylene 19.53 1672
1,2-Dimethylbenzene lo-Xylene 20.16 1726
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5°Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-lsopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
0.00 1734
0.00 1769
20.86 1786
0.00 1824
0.00 1835
0.00 1841
0.00 1846
0.00 1867
21.70 1858
21.96 1880
0.00 1921
22.51 1927
22.82 1954
23.02 197i
23.14 1981
23.17 1984
23.80 2038
23.97 2053
1,2-Dibromo-3-Chloropropane 0.00 2182
1,2,4-Trichlorobenzene .27.31 2339
78
166
129
107
112
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found. UG/L
Not Found UG/L
131 Not Found UG/L
91 4667239 8.01 .UG/L
91 10062961 9.88 UG/L
91 10062961
91 1004880
9.88 UG/L
2.00 UG/L
104
171
105
0 Not Found UG/L
Not Found UG/L
83
75
77
91
837900 1.48 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
91 0 Not Found UG/L
105 25191956 49.11 UG/L
91 128496 0.30 UG/L
119 0 Not Found UG/L
105 19479570
105 595936
119 3033195
146 339732
146 137288
91 14 91030
146 435008
39.57 UG/L
1.01 UG/L
6.45 UG/L
1.42 UG/L
0.51 UG/L
3.61 UG/L
1. 95 UG/L
Not Found UG/L 75
180 257747 2.43 UG/L
Fit
330
644
134
217
292
77
982
989
991
931
629
18
885
521
268
672
576
978
848
522
996
931
943
913
852
811
814
0
720
Rf
0.000
0.000
0.000
0.000
0.000
0.000
1. 511
2.644
2.644
1.305
0.000
0.000
1. 4 71
0.000
0.000
0.000
0.000
0.000
1.331
1.120
0.000
1.278
1. 530
1.221
0.620
0.704
1. 072
0.579
0.000
0.276
Operator ID, MC
Output File, AE01224.1A2
Data File' AE01224.MS
Name' AE01224
QUANT REPORT
Sample' Location' 100 Madison Ave, SB09-A
ID File' 826AEC28.QCI
Quant Time'
Injected at,
Dilution Factor'
Instrument ID,
Comment' Sampling, 02/19/1999 by J. Conway, use 0.248 g
Page
03/31/99 07,57
03/31/99 03 'll
1.00
20701-1284
Last calibration' 03/29/99 Last Qcal Time, 03/29/99 09,28
Compound
----------------------------------------61) 87-68-3
62) 91-20-3
63) 82-61-6
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
• Compound is ISTD
R.T. Scan# Q ion Area
27.64 2367
27.97 2396
28.58 2448
225 147274
128 8263118
180 241339
cone Units
1.43 UG/L
37.15 UG/L
2.16 UG/L
Fit
949
989
933
Rf
0.268
0.578
0.290
Operator ID: MC
Output File: AE01225.1A2
Data File: AE01225.MS
Name: AE01225
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-B
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:07
Injected at: 03/26/99 19:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
!
Comment: Sampling: 02/19/19>9 by J. Conway, use 6.39 g J Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
B) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochlor·omethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.04 1202
21.15 1811
23.94 2050
4.55
0.00
0.00
6. 41
0.00
7.37
0.00
9.61
389
438
466
54 9
572
631
737
822
0.00 874
0.00 942
0.00 1033
0.00 1031
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1138
13.62 1166
0.00 1165
0.00 1258
0.00 1291
0.00 1305
0.00 1335
0.00 1386
16.82 1440
0.00 1464
0.00 1494
96 2214255
95 1129113
152 683700
10.00 UG/L
11.61 UG/L
11.27 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4604 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
4204
5497
0.26 UG/L
Not Found UG/L
0.05 UG/L
0 Not Found UG/L
458195 1.67 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
17320 0.09 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
83491 0.32 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
954
857
0
410
669
765
979
388
994
16
64
421
663
286
382
609
297
565
976
907
617
359
713
853
714
984
545
620
Rf
1.000
0.440
0.275
0.258
0. 000.
0.000
0.074
0.000
0.455
0.000
1.241
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01225.1A2
Data File: AE01225.MS
Name: AE01225
Quant Time: 03/27/99 19:07
Injected at: 03/26/99 19:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 100 Madison Ave, SB09-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 6.39 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
3 3)
34)
35)
36)
3 7)
38)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
40)
41)
42)
4 3)
44)
45)
46)
4 7)
4 8)
4 9)
50)
51)
52)
53)
54)
55)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
18.22
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1520
1522
1560
1578
1645
1655
1656
1671
1,4-Dimethylbenzene (p-Xylene 19.52 1671
1,2-Dimethylbenzene (a-Xylene 20.23 1732
1733
1769
1783
1824
1828
184 3
1844
1869
1866
1880
1919
1926
1952
1971
1980
Styrene 20.24
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2, 3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Buty1benzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene.
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
0.00
21.53
21.54
21.83
21.79
21.95
22.41
22.50
22.80
23.02
23.12
23.24 1990
23.77 2035
0.00 2054
0.00 2183
0.00 2346
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
* Compound is ISTD
Area Cone Units
0 Not Found UG/L
4783 0.08 UG/L
268 0.01 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
117811
122656
122656
46861
21496
0. 40
0.23
UG/L
UG/L
0. 2 3 UG/L
0.20 UG/L
0.17 UG/L
0 Not Found UG/L
89015 0.32 UG/L
0 Not Found UG/L
Not Found UG/L
22643
64 53 7
28724
77469
34224
78222
73016
80303
65057
67000
0.15 UG/L
0.20 UG/L
0.12 UG/L
0.31
0.16
0.29
0.28
0.28
0.28
0.53
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
71984 0.58 UG/L
47717 0.21 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Fit
417
909
884
0
753
611
985
989
990
734
819
374
914
412
719
851
936
939
950
975
928
960
881
921
985
976
974
670
502
954
Rf
0.000
0.266
0.214
0.000
0.000
0.000
1.320
2.360
2.360
1. 076
0.576
0.000
1.246
0.000
0.000
0.685
1.438
1 . 0 9 9
1 .137
0.960
1.209
1 . 16 9
1.304
1 . 0 51
0.575
0.560
1.005
0.000
0.000
0.000
Operator ID: MC
Output File: AE01225.1A2
Data File: AE01225.MS
Name: AE01225
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-B
ID File:· 826AEC25.QCI
Page
Quant Time: 03/27/99 19:07
Injected at: 03/26/99 19:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 6.39 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.62 2366 225 23158 0.34
62) 91-20-3 Naphthalene 27.95 2394 128 46935 0.36
63) 82-61-6 1,2,3-Trichlorobenzene 28.54 2444 180 21086 0.31
• Compound is ISTD
Units Fit Rf
--------
UG/L 976 0.310
UG/L 982 0.586
UG/L 938 0.304
Operator ID: MC
Output File: AE01226.1A2
Data File: AE01226.MS
Name: AE01226
QUANT REPORT
Sample: Location:. 100 Madison Ave, SB09-C
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:08
Injected at: 03/26/99 19:41
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.33 g J Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.17 1812
23.94 2050
4.54
0.00
0.00
6.39
0.00
7.37
0.00
9.61
389
438
466
547
572
631
737
822
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
12.58 1076
0.00 1112
0.00 1136
0.00 1145
13.62 1166
0.00 1165
14.69 1257
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1440
0.00 1463
0.00 1498
96 2321345 10.00 UG/L
11.41 UG/L
11.33 UG/L
95 1162838
152 720567
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4 711 0.08 UG/L
Not Found UG/L
0 Not Found UG/L
1919
5545
0. 11 UG/L
Not Found UG/L
0.05 UG/L
0 Nee Found UG/L
357989 1.24 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Nee Found UG/L
0 Not Found UG/L
2316 0. 02 UG/L
Not Found UG/L
0 Nee Found UG/L
14189
820
45881
Not Found UG/L
0.07 UG/L
Not Found UG/L
0.01 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.17 UG/L
Nee Found UG/L
Not Found UG/L
Fit
998
999
954
864
384
358
724
92
976
259
94 0
140
588
539
577
448
700
366
674
918
976
883
809
315
161
554
486
982
554
751
Rf
1.000
0. 44 0
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.000
1.247
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page
Opera tor ID: MC
Output File: AE01226.1A2
Data File: AE01226.MS
Name: AE01226
Quant Time: 03/27/99 19:08
Injected at: 03/26/99 19:41
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 100 Madison Ave, SB09-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 5.33 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
4 7)
4 8)
4 9)
50)
51)
52)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
53) 135-98-8
54)
55)
56)
57)
58)
59)
6 0)
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.77 1521
0.00 1555
0.00
19.23
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 0.00
Styrene 20.23
1578
1646
1655
1657
1671
1671
1733
1732
1769
1778
1824
1835
1841
1847
1873
1866
1879
1919
1927
Bromofol-m
Isopropylb.enzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.77
0.00
0.00
0.00
21.58
0.00
21.79
21.94
22.41
22.50
22.80 1952
23.00
23.14
23.31
23.77
0.00
0.00
27.30
1970
1981
1996
2035
2054
2182
2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
p9
105
105
119
146
14 6
91
146
75
180
Area
4 574
Cone Units
Not Found UG/L
0.07 UG/L
Not Found UG/L
Not Found UG/L
4556 0.03 UG/L
Not Found UG/L
57142 0.19 UG/L
107198 0.20 UG/L
107198 "0.20 UG/L
Not Found UG/L
21419 0.16 UG/L
Not Found UG/L
30700 0.11 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
91872 0.28 UG/L
Not Found UG/L
99836 0.38 UG/L
35285
70884
86899
82449
65941
62237
18758
54228
20179
0.16 UG/L
0.25 UG/L
0.32 UG/L
0.27 UG/L
0.27 UG/L
0. 4 7 UG/L
0.14 UG/L
0.23 UG/L
Not Found UG/L
Not Found UG/L
0.29 UG/L
Fit
325
896
644
154
792
565
983
989
985
587
911
689
933
415
525
875
941
903
950
986
929
956
916
941
989
962
963
675
428
94 8
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
1. 319
2.360
2.360
0.000
0.576
.000
.245
0.000
0.000
0.000
1. 438
0.000
l. 137
0.960
l. 209
1 . 16 9
1. 304
1.051
0.575
0.559
1.005
0.000
0.000
0 . 3 03
Operator ID, MC
Output File, AE01226.1A2
Data File, AE01226.MS
Name, AE01226
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-C
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:08
Injected at: 03/26/99 19:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.33 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.64 2367 225 21889 0.30
62) 91-20-3 Naphthalene 27.97 2395 128 414 03 0.30
6 3) 82-61-6 1,2,3-Trichlorobenzene 28.56 2446 180 2cB93 0.32
• Compound is ISTD
Units Fit Rf
--------
UG/L 973 0.310
UG/L 984 0.586
UG/L 922 0. 304
Operator ID: MC
Output File: AE01227.1A2
Data File: AE01227.MS
Name: AE01227
QUANT REPORT
.Sample: Location: 100 Madison Ave, SB09-D
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:08
Injected at: 03/26/99 20:20
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.61 g J Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2)
3)
4)
5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
3 0)
4-BromoEluorobenzene (SG)
1, 2-Dichlorobenzene-d4 (SG)
75-71-8 DichlorodiEluoromethane
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
TrichloroEluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Cone Units
14.04 1203 96 2214446 10.00 UG/L
11.34 UG/L
10.93 UG/L
21.15
23.92
4.55
0.00
0.00
6.46
0.00
7.34
0.00
9.60
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
13.58
14.65
0.00
0.00
1812
2050
389
438
466
553
577
629
737
822
874
943
1033
1033
1069
1079
1112
1136
1130
1166
1163
1255
1291
1309
0.00 1327
0.00 1390
16.81 1440
0.00 1464
0.00 1494
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
1102521
663119
4 998 0. 09 UG/L
Not Found UG/L
Not Found UG/L
7117 0.44 UG/L
Not Found UG/L
5561 0.06 UG/L
0 Not Found UG/L
339246 1.23 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
11772 0.06 UG/L
1265 0.02 UG/L
968 0.02 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
75276 0.28 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
955
893
185
245
685
908
980
195
951
53
673
122
348
524
4 03
684
645
869
957
881
746
224
494
446
533
981
603
698
RE
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 247
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.355
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output Fileo AE01227.1A2
Data File: AE01227.MS
Name: AE01227
QUANT REPORT
Sampleo Locationo 100 Madison Ave, SB09-D
ID Fileo 826AEC25.QCI
Page 2
Quant Time, 03/21/99 19,()\l
Injected ato 03/26/99 20o20
Dilution Factor: 1. 00
Instrument IDo 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.61 g
Last Calibration: 03/25/99 Last Qcal Timeo 03/25/99 08o34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-2o-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-B
44) 79-34-5
45) 96-18-A
46) 108-86-1
47) 103-65-1
48) 95-49-~
49) 108-67-8
50) 106-43--4
51) 98-06-~
52) 95-63-6
53) 13.5-98-·8
54) 99-87-6
55) 541-73-·1
56) 106-46-·7
57) 104-51-·B
58) 95-50-J.
59) 96-12-e
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromoch1oromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1523
0.00 1556
0.00 1579
).9.24 1648
0.00 1656
).9.33 1656
1,3-Dimethylbenzene (m-Y.ylene 19.S'J 1671
1,4-Dimethylbenzene (p-Xylene ).9.50 1671
1,2-Dimethylbenzene (o-Xylene ,0.20 1730
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylben~ene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropylto1uene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1734
0.00 1770
20.84 1785
0.00 1825
0.00 1836
21.51 1843
21.56 1847
0.00 1872
21.79 1867
21.94 1880
22.44 1922
22.48 1926
22.79 1952
23.01 1971
23.14 1982
23.26 1992
23.77 2036
0.00 2055
0.00 2183
27.27 2336
78
166
129
107
112
131
91
'll
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
3813
Cone Units
Not Found UG/L
0.06 UG/L
0 Not Found UG/L
Not Found UG/L
3902
71236
133340
21894
18297
0.02 UG/L
Not Found UG/L
0.24 UG/L
Q.26 UG/L
0.26 UG/L
0.09 UG/L
0 .14 UG/L
32291
Not Found UG/L
0.12 UG/L
Not Found UG/L
0 Not Found UG/L
51328
62592
122886
33317
72620
66889
68749
59784
16510
74301
0.34 UG/L
0.20 UG/L
Not Found UG/L
0.49 UG/L
0.16 UG/L
0.27 UG/L
0.26 UG/L
0.24 UG/L
0.26 UG/L
0.13 UG/L
0. 6 0 UG/L
57258 0.26 UG/L
19300
Not Found UG/L
Not Found UG/L
0.29 UG/L
Fit
522
874
285
305
814
656
985
984
989
746
868
450
932
276
681
869
935
948
969
967
948
957
747
922
969
978
929
669
375
953
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2. }I;Q
2.360
1.075
0.576
0.000
1.246
0.000
0.000
0.685
1 . 4 3 8
0.000
1.137
0.960
1. 209
1 . 16 9
1.304
1.051
0.575
0.560
1.005
o.ooo
0.000
0.303
Operator ID: MC
Output File: AE01227.1A2
Data File: AE01227.MS
Name: AE01227
QUANT REPORT
Sample: Locati6n: 100 Madison Ave, SB09-D
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:08
Injected at: 03/26/99 20:20
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.61 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.59 2364
27.95 2395
28.52 2443
225
128
180
Area
21328
39540
8604
Cone Units
0.31 UG/L
0.30 UG/L
0.13 UG/L
Fit
970
984
913
Rf
0.310
0.586
0. 3 04
Operator ID: MC
Output File: AE01228.1A2
Data File: AE01228.MS
Name: AE01228
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-E
ID File: 826AEC25.QCI
Page 1
Quant Time: 03/27/99 19:09
Injected at: 03/26/99 21:00
Dilution Factor: 1.00
Instrument ID: 29701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 6.98 g I Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Cone Units
14.04 1203
21.15 1812
23.93 2050
4.55
0.00
0.00
6.40
0.00
7.36
0.00
9.60
390
438
466
548
580
630
737
822
0.00 874
0.00 943
0.00 1033
0.00 1033
0.00 1069
12.58 1077
0.00 1112
0.00 1142
0.00 1144
13.62 1166
13.62 1166
0.00 1259
0.00 1291
0.00 1309
15.56 1333
0.00 1390
16.80 1439
0.00 1464
0.00 1492
96 2210416
95 1029068
152 610162
10.00 UG/L
10.59 UG/L
10.07 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4216 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
0.56 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
1.33 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
9126
5376
365893
Not Found UG/L
0 Not Found UG/L
3004 0.03 UG/L
0 Not Found UG/L
17699
1369
76
67780
Not Found UG/L
Not Found UG/L
0.09 UG/L
0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.00 UG/L
Not Found UG/L
0.26 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
813
77
281
675
754
967
34
945
452
551
562
449
579
747
529
725
928
972
927
696
198
440
753
179
980
552
776
Rf
1.000
0. 44 0
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.000
1. 246
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.355
0.000
0.000
0.000
0.327
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01228.1A2
Data File: AE01228.MS
Name: AE0122B
Quant Time: 03/27/99 19:09
Injected at: 03/26/99 21:00
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 100 Madison Ave, SB09-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 6.98 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
3 5)
3 6)
3 7)
38)
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
40)
41)
42)
43)
44)
45)
46)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56)
57)
58)
59)
60)
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.76 1521
0.00 1556
0.00 1579
19.21
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.50
1646
1656
1657
1671
1,4-Dimethylbenzene (p-Xylene 19.50 1671
1,2-Dimethylbenzene (a-Xylene 20.21 1731
1734
1770
1779
1825
1836
184 0
Styrene 20.24
Bromoform 0.00
Isopropylbenzene 0.00
1,1,2,2-Tetrachloroethane 0.00
1,2,3-Trichloropropane 0.00
Bromobenzene 0.00
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
21.55 1846
0.00 1874
21.79 1867
21.91 1877
22.41 1920
22.48 1926
22.79 1952
23.00 1970
23.26 1992
23.26
2 3 . 76
23.94
0.00
27.29
1992
2036
2051
2183
2338
78
166
129
107
112
131
91
91
91
91
104.
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
4475 0.08 UG/L
Not Found UG/L
Not Found UG/L
5148 0.03 UG/L
0 Not Found UG/L
78002 0.27 UG/L
76956
76956
31498
29510
0.15 UG/L
0. 15 UG/L
0.13 UG/L
0.23 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
65214 0.21 UG/L
0 Not Found UG/L
99125 0.39 UG/L
45634
75450
6434 9
69678
57846
97534
0.22 UG/L
0.28 UG/L
0.25 UG/L
0.24 UG/L
0.25 UG/L
0.77 UG/L
97534 0.79 UG/L
47937 0.22 UG/L
69607 0.60 UG/L
Not Found UG/L
18563 0.28 UG/L
Fit
572
967
352
117
725
532
980
985
982
819
893
381
893
351
583
951
929
931
953
951
902
965
779
94 8
979
974
943
735
364
907
RE
0.000
0.266
0.000
0.000
0.7l.7
0.000
1.320
2.360
2.360
l . 076
0.576
0.000
0.000
0.000
0.000
0.000
1. 4 38
0.000
1.137
0. 960
1.209
1.169
1. 304
1. 051
0.575
0.560
1.005
0.526
D.DOD
0.303
Operator ID: MC
Output File: AE01228.1A2
Data File: AEOl228.MS
Name: AE01228
QUANT REPORT Page
Quant Time: 03/27/99 19:09
Injected at: 03/26/99 21:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 100 Madison Ave, SB09-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/19/1999 by J. Conway, use 6.98 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone Units
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Hexachlorobutadiene
Naphthalene
1, 2, 3 -Trichlor.obenzene
27.59 2364
27.94 2394
28.53 2445
225
128
180
21093
4 0678
19059
0.31 UG/L
0.31 UG/L
0.28 UG/L
Fit
976
965
936
Rf
0.310
0.586
0.304
~--------------------------------------------------------------------------------------------------------------------
Operator ID, MC
Output File, AEOl229.lA2
Data File' AE01229.MS
Name' AE01229
QUANT REPORT
Sample, Location, 100 Madison Ave, SB09-F
ID File, 826AEC25.QCJ
Page
Quant Time, 03/27/99 19,09
Injected at, 03/26/99 21,39
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/19/1999 by J. Conway, use 5.86 g / Last Calibration' 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1, 1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 09,34
R.T. Scan# Q ion Area Cone Units
14.03 1202
21.14 1811
23.94 2051
4.53
0.00
0.00
6. 42
0.00
7.36
0.00
9.60
388
438
466
549
578
630
737
822
0.00 874
0.00 940
0.00 1033
0.00 1031
0.00 1069
12.58 1077
12.96 1110
0.00 1136
13.27 1137
13.62 1166
13.58 1163
14.67 1256
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.81 1440
0.00 1464
0.00 1493
96 2119580
95 1112880
10.00 UG/L
11.96 UG/L
11.77 UG/L 152 683424
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
5076
8923
0.09 UG/L
Not Found UG/L
Not Found UG/L
0.57 UG/L
0 Not Found UG/L
6313 0.07 UG/L
0 Not Found UG/L
335713 1.27 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
4191
1817
1883
18006
1846
1766
0. 0 5 UG/L
0. 02 UG/L
Not Found UG/L
0.03 UG/L
0.09 UG/L
0.02 UG/L
0.03 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
68621
Not Found UG/L
0.27 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
~60
848
220
716
725
981
441
992
438
835
649
627
4 01
760
825
657
916
988
912
909
231
200
643
646
984
602
785
Rf
1.000
0.439
0.274
0.258
0.000
0.000
0.074
0.000
0.455
0.000
.246
.000
0.000
0.000
0 . 00 0
0.000
0.434
0.537
0.000
0.316
0.897
0.355
0.255
0 . 00 0
0 . 0 0 0
0.000
0.000
1.195
0.000
0.000
Operator IP' MC
Output File' AE01229.1A2
Data File, AE01229.MS
Name, AE01229
QUANT REPORT
Sample, Location, 100 Madison Ave, SB09-F
ID File, B26AEC25.QCI
Page 2
Quant Time' 03/27/99 19,09
Injected at' 03/26/99 21,39
Dilution Factor, 1.00
Instrument ID' 20701-1284
Comment' sampling, 02/19/1999 by J. Conway, use 5.86 g
Last Calibration' 03/25/99 Last Qcal Time, 03/25/99 08,34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
3 9)
40)
41)
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
. 57)
58)
59)
60)
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1, 3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
0.00 1556
0.00 1579
19.21 1646
0.00 1656
19.33
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.22
1656
1671
1671
1732
1734 Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24
0.00 1770
20.83 1785
0.00 1825
0.00 1836
21.49 1841
21.54 1845
21.82 1869
21.79 1867
21.94 1879
22.42 1921
22.49 1926
22.79 1952
22.98 1969
23.11 1980
23.24 1991
23.76 2035
0.00 2055
0.00 2183
27.30 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
9l
146
75
180
Area
7208
Cone Units
Not Found UG/L
0.13 UG/L
0 Not Found UG/L
Not Found UG/L
4575 0.03 UG/L
0 Not Found UG/L
106817
14 54 3 8
145438
57614
21686
0.38 UG/L
0.29 UG/L
0. 2 9 UG/L
0.25 UG/L
0.18 UG/L
0 Not· Found UG/L
73860 0.28 UG/L
Not Found UG/L
0 Not Found UG/L
28854 0.20 UG/L
75200
44508
121711
53663
78623
111959
87956
77438
29721
90280
0.25 UG/L
0.19 UG/L
0.51 UG/L
0.26 UG/L
0.31 UG/L
0.45 UG/L
0.32 UG/L
0.35 UG/L
0.24 UG/L
0.76 UG/L
95978 0.45 UG/L
Not Found UG/L
Not Found UG/L
23988 0.38 UG/L
Fit
515
977
354
323
904
479
983
989
992
826
896
347
932
305
473
899
970
971
94 7
977
936
983
924
984
974
969
959
626
331
938
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.685
1.438
1.100
1.137
0.960
1. 209
1.169
1.305
1.051
0.575
0.560
1.004
0.000
0.000
0.303
Operator ID: MC
Output File: AE01229.1A2
Data File: AE01229.MS
Name: AE01229
QUANT REPORT
Sample: Location: 100 Madison Ave, SB09-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:09
Injected at: 03/26/99 21:39
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/19/1999 by J. Conway, use 5.86 g
Last Calibration: 03/25/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexashlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.61
27.94
28.55
2365
2394
2446
225
128
180
Area
23520
78572
13507
Cone
0.36
0.63
0.21
Unit.s
UG/L
UG/L
UG/L
Fit
958
986
895
Rf
0.310
0.585
0. 304
Operator ID: MC
Output File: AE01232.1A2
Data File: AE01232.MS
Name: AE01232
QUANT REPORT
Sample: Location: 200 N. Lawrence, SBlO-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:08
Injected at: 03/30/99 05:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 4.47 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene ISG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
13)
14)
15)
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.05
21.16
23.94
4.54
0.00
5. 45
6. 41
6.70
7.36
8.60
9.61
10.18
10.98
12.05
0.00
12.4 8
0.00
12.96
13.24
13.29
13.62
13.60
14 . 6 8
15.05
0.00
15.49
16.20
16.82
17.09
17.44
1202
1812
2050
389
438
466
54 9
574
630
735
822
871
94 0
1030
1033
1068
1078
1109
1133
1137
1165
1164
1256
1288
1307
1325
1387
1439
1463
14 93
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
2135891
850166
54 018 5
9952
Cone
10.00
8.61
8.48
0.13
Units
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
2500 0.05 UG/L
8765
701
15011
2865
742573
8994
2451
5335
2639
4639
8602
3569
24128
3016
8159
2009
2019
2681
47423
2759
1157
0. 51 UG/L
0.05 UG/L
0.13 UG/L
0.06 UG/L
3.58 UG/L
0.09 UG/L
0.02 UG/L
0. 05 UG/L
Not Found UG/L
0. 03 UG/L
Not Found UG/L
0.03 UG/L
0.10 UG/L
0.04 UG/L
0.10 UG/L
0.03 UG/L
0.13 UG/L
0. 0 5 UG/L
Not Found UG/L
0.02 UG/L
0.03 UG/L
0.16 UG/L
0.03 UG/L
0.04 UG/L
Fit
997
999
955
898
262
838
608
766
985
961
988
934
829
944
861
818
370
937
827
925
996
950
954
517
910
809
851
980
858
790
Rf
1.000
0.463
0.299
0.361
0.000
0.226
0.081
0.060
0.526
0.225
0.971
0.452
0.485
0.511
0.000
0. 4 86
0.000
0.662
0. 402
0.380
1.098
0.430
0.291
0.189
0.000
0. 4 03
0. 4 53
1.369
0.396
0.145
Operator ID: MC
Output File: AE01232.1A2
Data File: AE01232.MS
Name: AE01232
QUANT REPORT
Sample: Location: 200 N. Lawrence, SBlO-A
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:08·
Injected at: 03/30/99 05:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 4.47 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32)
33)
34)
35)
36)
37)
38)
3 9)
4 0)
41)
42)
43)
44)
45)
46)
47)
4 8)
4 9)
50)
51)
52)
53)
54)
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.77
18.18
18.42
19.23
19.33
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
1521
1556
1577
1646
1655
1656
1671
1671
1732
1732
1769
1784
1824
1835
1842
1845
1866
1867
1879
1919
1925
1953
1970
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.23
0.00
20.84
0.00
0.00
21.51
21.55
21.79
21.80
21.94
22.41
22.48
22.80
23.00
23.11 1978
23.26 1992
23.75 2034
23.98 2054
0.00 2182
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
14556
2081
932
26170
3014
1104 77
183510
183510
73976
30117
102707
0.24 UG/L
0.03 UG/L
0.02 UG/L
0.14 UG/L
0.05 UG/L
0.34 UG/L
0.32 UG/L
0.32 UG/L
0.27 UG/L
0.20 UG/L
Not Found UG/L
0.33 UG/L
Not Found UG/L
0 Not Found UG/L
42652 0.23 UG/L
14 5 719
129877
231770
115279
110610
158697
121124
126424
4 9657
150814
106090
0.41 UG/L
0.49 UG/L
0.80 UG/L
0.48 UG/L
0.37 UG/L
0.58 UG/L
0. 37 UG/L
0.48 UG/L
0.38 UG/L
1.00 UG/L
0.46 UG/L
89753 0.73 UG/L
Not Found UG/L
41986 0.71 UG/L
Fit
4 08
982
857
856
964
799
989
995
995
789
920
652
987
312
689
978
976
938
958
991
946
986
988
970
986
983
991
729
280
980
Rf
0.000
0.284
0.282
0.259
0.858
0. 311
1.510
2. 64 9
2.649
1. 305
0.702
0.000
1. 4 70
0.000
0.000
0.855
1.673
1.234
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.074
0.579
0.000
0. 276
Operator ID: MC
Output File: AE01232.1A2
Data File: AE01232.MS
Name: AE01232
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:08
Injected at: 03/30/99 05:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 4.47 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28.
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.62 2365 225 29755 0.52
62) 91-20-3 Naphthalene 27.96 2394 128 97851 0.77
63) 82-61-6 1,2,3-Trichlorobenzene 28.53 2444 180 41024 0.66
• Compound is ISTD
Units Fit Rf
--------
UG/L 982 0.269
UG/L 990 0. 596
UG/L 976 0. 291
•i
Operator ID: MC
Output File: AE01233.1A2
Data File: AE01233.MS
Name: AE01233
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:09
Injected at: 03/30/99 05:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. conway, use 4.57 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9 Bromomethane
B) 75-00-3 Chloroethane
9) 75-69-4 Trichlorofluoromethane
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
74-95-3
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Di~hloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane 25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2"Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.03
21.14
23.93
4.54
5.10
0.00
6. 40
0.00
7.34
0.00
9.60
0.00
0.00
0.00
0.00
0.00
0.00
1202
1811
2050
388
436
466
548
573
629
737
822
874
943
1033
1033
1069
1079
0.00 1112
0.00 1128
0.00 1136
13.62 1166
13.59 1164
14.65 1255
0.00 1291
0.00
0.00
0.00
16.81
0.00
0.00
1309
1325
1390
1440
1464
1488
96
95·
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1883329
764483
503015
4479
4368
11997
5353
727762
Cone Units
10.00 UG/L
8.78 UG/L
8.95 UG/L
0. 07 UG/L
0.18 UG/L
Not Found UG/L
0.79 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
3.98 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
20600 0.10 UG/L
1100 0.01 UG/L
792 0.01 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
28393 0.11 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
957
884
634
62
695
640
977
286
992
678
409
614
445
675
235
343
777
834
996
906
736
222
179
747
285
987
634
739
Rf
1.000
0.463
0.299
0.361
0.130
0.000
0.081
0.000
0.526
0.000
0.970
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.430
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01233.1A2
Data File: AE01233.MS
Name: AE01213
Quant Time: 03/30/99 18:09
Injected at: 03/30/99 05:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Lawrence, SB10-B
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 4.57 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
4 6)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-~B-9
127-18-4
124-18-1
106-93-4
108-90-7
630-20-6
100-11-4
108-18-3
106-42-3
95-47-6
100-12-5
75-25-2
98-82-8
79-31-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-61-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.77
0.00
0.00
0.00
0.00
19.33
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (o-Xylene 20.22
Styrene 20.24
Bromoform 0.00
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.85
0.00
0.00
0.00
21.52
21.89
21.74
21.94
22.40
22.48
22.80
23.00
2 3. 24
23.24
23.77
23.95
0.00
27.30
1521
1522
1556
1579
1648
1656
1656
1671
1671
1732
1734
1770
1786
1825
1836
1843
1843
1875
1863
1880
1919
1926
1953
1970
1991
1991
2036
2052
2183
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
3302 0. 06 .UG/L
0 Not Founq UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
48559 0.17 UG/L
95088 0.19 UG/L
95088
39001
15541
0.19 UG/L
0.16 UG/L
0.12 UG/L
0 Not Found UG/L
56885 0.21 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
40612 0.13 UG/L
16272
186570
43603
80367
120300
79828
77780
132076
132076
61076
72214
0.07 UG/L
0.73 UG/L
0.21 UG/L
0.31 UG/L
0.50 UG/L
0.28 UG/L
0.34 UG/L
1 .13 UG/L
1. 0 0 UG/L
0.30 UG/L
0.66 UG/L
0 Not Found UG/L
22771 0.44 UG/L
Fit
461
925
654
356
468
263
980
993
996
769
943
190
941
4 32
353
818
970
937
974
981
930
967
875
974
982
978
970
739
376
938
RE
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2. 64 9
2.649
1.305
0.701
0.000
1. 470
0.000
0.000
0.000
1 . 6 73
1.234
1. 354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.579
0.000
0.276
Operator ID: MC
Output File: AE01233.1A2
Data File: AE01233.MS
Name: AE01233
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:09
Injected at: 03/30/99 05:41
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. conway, use 4.57 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.59 2364 225 20166 0.40
62) 91-20-3 Naphthalene 27.94 2394 128 140866 1.26
63) 82-61-6 1,2,3-Trichlorobenzene 28.56 2447 180 10183 0.19
• Compound is ISTD
Units Fit Rf
. -------
UG/L 978 0.269
UG/L 993 0.596
UG/L 901 0. 291
Operator ID: MC
Output File: AE01234.1A2
Data File: AE01234.MS
Name: AE01234
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-C
ID File: 826AEC28.QCI
Page 1
Quant Time: 03/30/99 18:10
Injected at: 03/30/99 06:21
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.18 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluoroben~ene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.05 1202
21.15 1811
23.94 2050
96 1929070 10.00 UG/L
8.83 UG/L
9.28 UG/L
4. 55
0.00
5.47
0.00
0.00
7.37
0.00
9.61
0.00
0.00
390
438
468
549
578
631
737
822
880
942
12.05 1031
0.00 1027
0.00 1069
0.00 1078
0.00 1112
13.27 1135
0.00 1137
13.62 1166
0.00 1163
14.69 1257
15.05 1288
0.00 1309
0.00 1327
0.00 1389
16.83 1440
0.00 1463
0.00 1493
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
787398
534268
5179 0.07 UG/L
749
7078
768165
14 79
Not Found UG/L
0.02 UG/L
Not Found UG/L
Not Found UG/L
0.07 UG/L
Not Found UG/L
4.11 UG/L
Not Found UG/L.
Not Found UG/L
0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
932 0.01 UG/L
22451
132 9
1379
37941
Not Found UG/L
0 .11 UG/L
Not Found UG/L
0.02 UG/L
0.04 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.14 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
953
794
238
642
550
897
982
683
977
770
556
840
644
336
128
711
729
854
998
878
918
423
249
505
542
984
686
676
Rf
1.000
0.463
0.299
0.361
0.000
0.226
0.000
0.000
0.526
0.000
0.970
0.000
0.000
0.511
0.000
0.000
0.000
0.000
0. 4 02
0.000
1.098
0.000
0.291
0.189
0.000
0.000
0.000
l. 369
0.000
0.000
\
QUANT REPORT Page
Operator ID: MC
Output File: AE01234.1A2
Data File: AE01234.MS
Name: AE01234
Quant Time: 03/30/99 18:10
Injected at: 03/30/99 06:21
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Lawrence, SB10-C
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.18 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
46) 108-86-1
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.22
0.00
19.35
1,3-Dimethylbenzene 1m-Xylene 19.53
1,4-Dimethylbenzene lp-Xylene 19.53
1,2-Dimethylbenzene (o-Xylene 20.25
Styrene 20.25
Bromoform 0.00
20.85
0.00
0.00
1520
1522
1555
1578
1645
1655
1656
1672
1672
1734
1734
1769
1785
1824
1835
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1841
21.55
21.89
21.81
21.97
22.44
22.50
22.80
23.01
23.12
23.25
23.77
0.00
0.00
27.32
1845
1874
1867
1881
1921
1926
1952
1970
1980
1991
2035
2054
2190
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
3885 0.07 UG/L
Not Found UG/L
Not Found UG/L
5000 0.03 UG/L
Not Found UG/L
66468 0.23 UG/L
113919 0.22 UG/L
113919 0.22 UG/L
47930
18021
0.19 UG/L
0.13 UG/L
0 Not Found UG/L
56442 0.20 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
94 BOO
12236
128578
24925
85068
128837
91830
94 882
40651
151192
77729
0.29 UG/L
0.05 UG/L
0.49 UG/L
0.12 UG/L
0.32 UG/L
0.52 UG/L
0.31 UG/L
0.40 UG/L
0.34 UG/L
1.12 UG/L
0.38 UG/L
Not Found UG/L
O.Not Found UG/L
22668 0.43 UG/L
Fit
274
919
707
552
882
541
978
993
993
793
916
217
974
440
538
777
958
94 5
96 9
985
916
980
935
957
982
973
985
681
581
909
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2.649
2.649
1.305
0.702
0.000
1. 4 70
0.000
0.000
0.000
1.673
1.234
1. 354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.074
0.000
0.000
0.276
Operator ID: MC
Output File: AE01234.1A2
Data File: AE01234.MS
Name: AE01234
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:10
Injected at: 03/30/99 06:21
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.18 g
Last Calibration: 03/29/99
61)
62)
6 3)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62
27.94
28.53
2365
2393
2443
225
128
180
Area
21734
219584
23725
Cone Units
0.42 UG/L
1.91 UG/L
0.42 UG/L
Fit
970
990
986
Rf
0.269
0.595
0. 291
QUANT REPORT Page 1
Operator ID: Me
Output File: AE01235.1A2
Data File: AE01235.MS
Name: AE01235
Sample: Location: 200 N. Lawrence, SB10-D
ID File: 826AEC28.QCI
Quant Time: 03/30/99 18:11
Injected at: 03/30/99 07:00
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1} •107-06-2 Fluorobenzene
2} 4-Bromofluorobenzene (SG}
3} 1,2-Dichlorobenzene-d4 (SG)
4} 75-71-8
5} 74-87-3
6} 75-01-4
7} 74-83-9
8} 75-00-3
9} 75-69-4
10} 75-35-4
11} 75-09-2
12} 156-60-5
13} 75-34-3
14} .156-59-4
15} 590-20-7
16) 74-97-S
17} 67-66-3
18} 71-55-6
19} 563-58-6
20} 56-23-S
21} 71-43-2
22} 107-06-2
23} 79-01-6
24} 78-87-S
25} 74-95-3
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
26} 75-~7-4 Bromodichloromethane
27} 10061-01-5 Cis-1,3-Dichloropropene
28} 108-88-3 Toluene
29} 10061-02-6 Trans-1,3-Dichloropropene
30} 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.05 1202
21.15 1811
23.94 2050
4.54 389
0.00 438
o.oo 466
6.40 548
0.00 575
7.36 630
o.oo 737
9.60 821
0.00 876
0.00 933
o.oo 1033
0.00 1033
o.oo 1069
o.oo 1078
o.oo 1112
0.00 1136
o.oo 1137
13.62 1165
o.oo 1163
o.oo 1258
0.00 -1291
o.oo 1309
o.oo 1327
o.oo 1389
16.81 1439
0.00 1463
o.oo 1493
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1909367
636108
372689
4643
10.00
7.21
6.54
0.07
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
Not Found UG/L
2904 0.19 UG/L
Not Found UG/L
6543 0.07 UG/L
0 Not Found UG/L
708721 3.83 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
12793 0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not ·Found UG/L
Not Found UG/L
0 Not Found UG/L
21182 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
875
45
312
738
834
981
292
990
727
787
543
553
461
96
291
685
858
994
878
540
383
334
214
534
986
607
596
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.000
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01235.1A2
Data File: AE01235.MS
Name: AE01235
QUANT REPORT
Sample: Location: 200 N. Lawrence, SBlO-D
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:11
Injected at: 03/30/99 07:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.77 1521
0.00 1558
0.00 1578
0.00 1648
0.00 1655
19.33 1655
1,3-Dimethylbenzene (m-Xylene 19.50 1670
1,4-Dimethylbenzene (p-Xylene 19.50 1670
1,2-Dimethylbenzene (a-Xylene 20.21 1730
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.23 1732
0.00 1769
20.79 1780
0.00 1824
21.33 1826
21.47 1838
21.43 1835
21.85 1871
21.81 1867
21.90 1875
22.40 1918
22.49 1926
22.79 1951
23.00 1969
23.11 1979
23.24 1990
23.76 2035
23.99 2054
0.00 2182
27.30 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
1790
Cone Units
Not Found UG/L
0.03 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found" UG/L
35861
85917
85917
4 74 54
16202
0.13 UG/L
0.17 UG/L
0.17 UG/L
0.19 UG/L
0. 12 UG/L
0 Not Found UG/L
32223 0. 11 UG/L
0 Not Found UG/L
4756
7875
4877
73563
96709
39813
78694
104 315
724 03
69775
16078
146016
56984
24684
15257
0.07 UG/L
0.05 UG/L
0.02 UG/L
0.31 UG/L
0.38 UG/L
0.19 UG/L
0.30 UG/L
0.43 UG/L
0.25 UG/L
0.30 UG/L
0.14 UG/L
1.09 UG/L
0.28 UG/L
0.22 UG/L
Not Found UG/L
0.29 UG/L
Fit
212
886
782
390
606
551
974
992
994
774
886
103
932
301
730
858
956
944
959
983
931
94 6
895
937
978
974
941
719
644
941
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2. 649
1.305
0.701
0.000
1. 470
0.000
0.357
0.855
1.673
1.234
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.075
0.579
0.000
0.276
Operator ID: Me
Output File: AE01235.1A2
Data File: AE01235.MS
Name: AE01235
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:11
Injected at: 03/30/99 07:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.23 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-:l
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.61 2364
27.93 2392
28.54 2445
225
128
180
Area
18775
50625
18329
Cone Units
0.37 UG/L
0.45 UG/L
0.33 UG/L
Fit
972
982
921
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01236.1A2
Data File: AE01236.MS
Name: AE01236
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:11
Injected at: 03/30/99 07:40
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.30 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10)
11)
12)
13)
14)
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18)
19)
20)
21)
22)
23)
24)
25)
26)
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodi.chloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-18-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.03
21.13
23.91
4.54
0.00
0.00
6.48
6.68
7.36
8.58
9.60
10.17
0.00
12.05
1201
1810
2 04 8
388
438
465
555
572
630
733
821
870
943
1030
0.00 1036
0.00 1069
0.00 1079
0.00
13.23
0.00
13.62
13.59
14.66
0.00
0.00
0.00
1112
1132
1138
1165
1163
1255
1291
1309
1327
0.00 1390
16.80 1438
0.00 1464
0.00 1492
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1972 712
836111
528483
6886
2680
439
8384
666
718676
2331
1544
Cone Units
10.00 UG/L
9.17 UG/L
8.98 UG/L
0.10 UG/L
Not Found UG/L
Not Found UG/L
0. 17 UG/L
0.04 UG/L
0.08 UG/L
0.02 UG/L
3.76 UG/L
0.03 UG/L
Not Found UG/L
0.02 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
2317 0.03 UG/L
Not Found UG/L
12905 0.06 UG/L
1187 0.01 UG/L
1623 0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
22255 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
871
65
572
738
764
983
797
940
854
571
867
669
683
32
563
795
892
993
917
911
392
350
687
385
974
555
824
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.225
0.971
0.452
0.000
0.511
0.000
0.000
0.000
0.000
0.402
0.000
1.098
0.430
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01236.1A2
Data File: AE01236.MS
Name: AE01236
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-E
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:11
Injected at: 03/30/99 07:40
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.30 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
3 6)
37)
38)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20;6
100-41-4
108-38-3
39) 106-42-3
40)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.77
0.00
0.00
19.21
0.00
19.34
1,3-Dimethylbenzene {m-Xylene 19.50
1521
1522
1556
1579
1645
1656
1656
1670
1,4-Dimethylbenzene {p-Xylene 19.50 1670
1,2-Dimethylbenzene lo-Xylene 20.22 1732
1731
1770
1783
1825
1836
1839
184 5
1872
1866
1880
1920
1923
Styrene
Bromoform
Isopropylbenzene
1, 1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
~ert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.21
0.00
20.82
0.00
0.00
21.4 7
21.54
0.00
21.79
21.95
22.42
22.45
22.78 1951
22.98 1968
23.10 1979
23.23 1990
23.73 2033
0.00 2055
0.00 2183
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
• Compound is ISTD
Area Cone Units
0 Not Found UG/L
4610 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
5135 0.03 UG/L
75297
88747
88747
31121
16316
Not Found UG/L
0.25 UG/L
0.17 UG/L
0.17 UG/L
0.12 UG/L
0.12 UG/L
0 Not· Found UG/L
55379 0.19 UG/L
0 Not Found UG/L
0 Not Found UG/L
7609 0.05 UG/L
83678 0.25 UG/L
0 Not Found UG/L
179322 0.67 UG/L
53319 0.24 UG/L
89577
103420
95508
88454
59891
106602
70504
0.33 UG/L
0.41 UG/L
0.32 UG/L
0.37 UG/L
0.49 UG/L
0.77 UG/L
0.33 UG/L
0 Not Found UG/L
0 Not Found UG/L
23193 0.43 UG/L
Fit
447
954
622
320
866
359
985
990
990
713
924
132
954
359
546
917
959
939
949
985
937
958
952
977
983
974
984
688
27
963
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1. 510
2.649
2. 649
1.305
0.701
0.000
1. 470
0.000
0.000
0.855
1.673
0.000
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.074
0.000
0.000
0. 276
Operator ID' MC
Output File: AE01236.1A2
Data File' AE01236.MS
Name, AE01236
QUANT REPORT
Sample, Location, 200 N. Lawrence, SBlO-E
ID File' 826AEC28.QCI
Page
Quant Time, 03/30/99 18,11
Injected at, 03/30/99 07:40
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/22/1999 by J. Conway, use 5.30 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time, 03/29/99 09,28
R.T. Scan# Q ion
27.60 2364
27.94 2393
28.52 2443
225
128
180
Area
24102
51558
25083
Cone Units
0.46 UG/L
0.44 UG/L
0.44 UG/L
Fit
981
978
967
Rf
0.269
0.596
0.291
,.
Operator ID: MC
Output File: AE01237.1A2
Data File: AE01237.MS
Name: AE01237
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:12
Injected at: 03/30/99 08:21
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane ·
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14. OS
21.16
23.95
4.55
0.00
0.00
6.36
1204
1813
2052
390
438
467
545
0.00 578
7.36 631
0.00 737
9.61 823
0.00 874
0.00 941
0.00 1034
0.00 1034
0.00 1070
0.00 1079
0.00 1113
0.00 1137
0.00 1138
13.62 1167
0.00 1165
14.68 1258
0.00 1292
0.00 1310
0.00 1328
0.00 1390
16.83 1442
0.00 1465
0.00 1495
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1952273 10.00 UG/L
842698 9.34 UG/L
542998 9.32 UG/L
4734 0.07 UG/L
Not Found UG/L
Not Found UG/L
571 0.04 UG/L
0 Not Found UG/L
5905 0.06 UG/L
0 Not Found UG/L
694906 3.67 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
14819 0.07 UG/L
Not Found UG/L
834 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
33207 0.13 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
893
511
485
708
797
982
618
995
621
727
613
499
530
627
680
852
996
909
847
323
116
544
4 94
975
654
678
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01237.1A2
Data File: AE01237.MS
Name: AE01237
Quant Time: 03/30/99 18:12
Injected at: 03/30/99 08:21
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Lawrence, SB10-F
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.23
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 0.00
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.77
0.00
0.00
21.51
21.55
0.00
21.81
21.96
22.4 0
22.49
22.80
23.00
23.14
23.26
23.75
24.02
0.00
27.27
1521
1524
1551
1580
1648
1657
1658
1673
1673
1734
1740
1771
1780
1825
1837
1843
1847
1872
1869
1882
1920
1927
1954
1971
1983
1993
2035
2058
2184
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
2826 0.05 UG/L
Not Found UG/L
0 Not Found UG/L
2699 0.02 UG/L
Not Found UG/L
57015 0.19 UG/L
120724
120724
50057
0.23 UG/L
0.23 UG/L
0.20 UG/L
Not Found UG/L
0 Not Found UG/L
38275 0.13 UG/L
0 Not Found UG/L
0 Not Found UG/L
17157 0.10 UG/L
83037 0.25 UG/L
0 Not Found UG/L
121211 0.46 UG/L
27943
90245
150088
81164
68624
55940
100802
77045
19170
20998
0.13 UG/L
0.33 UG/L
0.60 UG/L
0.27 UG/L
0.29 UG/L
0.46 UG/L
0.73 UG/L
0.37 UG/L
0.17 UG/L
Not Found UG/L
0.39 UG/L
Fit
422
961
723
340
749
463
987
994
993
916
885
325
94 5
556
673
828
951
955
981
984
931
990
933
950
983
974
982
745
363
939
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2. 64 9
2.649
1.305
0.000
0.000
1. 4 70
0.000
0.000
0.855
1. 673
0.000
1.354
1.120
1. 386
1.277
1.530
1.224
0.620
0.703
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01237.1A2
Data File: AE01237.MS
Name: AE01237
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-F
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page
03/30/99 18:12
03/30/99 08:21
1. 00
20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/29/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
H~xachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62
27.95
28.53
2367
2395
2445
225
128
180
Area
21126
64430
22306
Cone Units
0.40 UG/L
0.55 UG/L
0.39 UG/L
Fit
974
986
972
Rf
0.269
0.596
0.291
Operator ID: l'!C
Output File: AE01238.1A2
Data File: AE01238.MS
Name: AE01238
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:12
Injected at: 03/30/99 09:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.34 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-9 Dichlorodifluoromethane
5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
3 0)
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.05
21.16
23.93
4.55
0.00
0.00
6.47
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
0.00
0.00
0.00
0.00
0.00
16.82
0.00
0.00
1204
1813
2051
390
438
461
555
573
631
737
823
874
943
1031
1035
1070
1079
1113
1140
1136
1167
1167
1259
1292
1310
1328
1390
1441
1465
1495
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1488825
613119
402677
3354
10.00 UG/L
8. 91 UG/L
9.07 UG/L
0.06 UG/L
Not Found UG/L
Not Found UG/L
528 0.04 UG/L
0 Not Found UG/L
3808 0.05 UG/L
Not Found UG/L
533950 3.70 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
10688 0.07 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not 'Found UG/L
15653 0.08 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
857
147
609
775
569
960
656
994
618
376
723
697
556
214
705
867
990
897
655
271
295
4 91
413
982
683
659
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.000
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01238.1A2
Data File: AE01238.MS
Name: AE01238
Quant Time: 03/30/99 18:12
Injected at: 03/30/99 09:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Lawrence, SB10-G
ID File: 826AEC2B.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.34 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
4 8)
49)
50)
51)
52)
53)
54)
55)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1523
0.00 1556
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
1580
164 9
1657
1658
1673
1673
1734
1728
1771
1787
1825
1813
1838
1838
1873
1868
1880
1920
1927
1954
1971
1981
Styrene 20.16
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.85
0.00
21.16
0.00
21.45
0.00
21.80
21.94
22.41
22.49
22.80
23.00
23.12
23.26 1993
23.73 2034
0.00 2056
0.00 2184
27.28 2338
78
166
12 9
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
2123 0.05 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
50965 0.23 UG/L
64745
64745
28541
2582
0.16 UG/L
0.16 UG/L
0.15 UG/L
0.02 UG/L
0 Not Found UG/L
28925 0.13 UG/L
0 Not Found UG/L
353216 6.62 UG/L
0 Not Found UG/L
1125 0.00 UG/L
Not Found UG/L
90331 0.45 UG/L
28362
76855
89544
33723
67029
4 9374
82 934
47748
0.17 UG/L
0.37 UG/L
0.47 UG/L
0.15 UG/L
0. 3 7 UG/L
0.54 UG/L
0.79 UG/L
0.30 UG/L
Not Found UG/L
0 Not Found UG/L
19299 0.47 UG/L
Fit
283
959
691
507
594
353
977
987
990
755
882
324
926
340
817
856
955
953
957
986
915
936
921
931
968
978
964
676
479
943
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1. 510
2.649
2.649
1.305
0.701
0.000
1.470
0.000
0.359
0.000
1. 673
0.000
1 . 3 54
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1. 075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01238.1A2
Data File: AE01238.MS
Name: AE01238
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:12
Injected at: 03/30/99 09:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.34 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.58 2364 225 21841 0.55
62) 91-20-3 Naphthalene 27.95 2395 128 47839 0.54
63) 82-61-6 1,2,3-Trichlorobenzene 28.53 2445 180 21413 0.50
* Compound is ISTD
Units Fit Rf
--------
UG/L 974 0.269
UG/L 984 0.596
UG/L 968 0.291
Operator ID: MC
Output File: AE01239.1A2
Data File: AE01239.MS
Name: AE01239
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:46
Injected at: 03/24/99 23:26
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: sampling: 02/22/1999 by J. Conway, use 9.09 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene 28)
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is tSTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.08 1204
21.18 1814
23.97 2052
4.55 390
5.11 438
0.00 466
6.45 552
0.00 576
7.39 633
0.00 737
9.62 823
0.00 874
0.00 940
0.00 1033
0.00 1033
0.00 1069
12.60 1078
0.00 1112
0.00 1136
0.00 1142
13.65 1168
0.00 1168
14.71 1259
0.00 1291
0.00 1308
0.00 1327
0.00 1389
16.84 1441
0.00 1458
0.00 1484
96 3031636
95 1439457
152 830595
10.00 UG/L
10.81 UG/L
10.CO UG/L
85 5043 0.06 UG/L
0.29 UG/L 47 10254
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
0 Not Found UG/L
25445 1. 14 UG/L
0 Not Found UG/L
9138 0.07 UG/L
0 Not Found UG/L
258879 0.68 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
6295 0.05 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
30411 0.11 UG/L
Not Found UG/L
4233 0.05 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
201318 0.56 UG/L
Not Found UG/L
0 Not Found UG/L
Fit.
997
999
951
818
628
415
682
802
983
439
932
429
759
557
537
683
82 9
633
414
740
955
931
853
132
720
413
548
976
707
839
Rf
1.000
0. 440
C.275
0.258
0.118
0.000
0.074
0.000
0. 455
0.000
1.254
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.196
0.000
0.000
''
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01239.1A2
Data File: AE01239.MS
Name: AE01239
Quant Time: 03i25/99 09:46
Injected at: 03/24/99 23:26
Pi lution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 200 N. Lawrence, SB10-H
ID File: 826AEC25.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 9.09 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
4 0)
41)
42)
4 3)
44)
4 5)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
S41-73-l
:lOG-46-7
:l04-51-8
95-50-1
96-12-8
].20-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Pichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Pibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.80 1524
0.00 1555
0.00 1578
0.00 1648
0.00 1655
19.35 1656
1,3-Pimethylbenzene (m-Xylene 19.54 1673
1,4-Pimethylbenzene (p-Xylene 19.54 1673
1,2-Pimethylbenzene (o-Xylene 0.00
Styrene 0.00
Bromoform 0.00
Isopropylbenzene 20.82
1,1,2,2-Tetrachloroethane 0.00
1,2,3-Trichloropropane 0.00
Bromobenzene 0.00
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Pichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Pichlorobenzene
1,2-Pibromo-3-Chloropropane
1,2,4-Trichlorobenzene
21.56
21.88
21.82
21.97
22.45
22.52
22.82
23.01
23.15
23.29
23.80
24. 01
25.51
27.30
1733
1729
1769
1782
1824
1835
1832
1846
1873
1868
1881
1922
1928
1954
1971
1982
1994
2038
2056
2185
2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
12518 0.16 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
251451
348908
348908
0.63 UG/L
0.49 UG/L
0.49 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
13 614 8 0.36 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
3 024 71
103697
366291
160528
279889
273542
285489
201016
116106
328372
237442
292052
16855
26197
0.69
0.31
1. 06
0.55
0.76
0.77
0.72
0.63
0.67
1. 94
0.78
1. 83
0.77
0.29
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
193
923
674
378
931
578
977
984
984
4 91
940
647
954
618
237
953
965
956
892
988
956
972
835
932
977
980
983
833
721
980
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
0.000
0.000
0.000
l. 246
0.000
0.000
0.000
1.439
1.100
1.139
0.961
1.210
1 . 16 8
1.305
1.051
0.575
0.560
1.003
0.526
0.073
0.303
Operator lD: MC
Output File: AE01239.1A2
Data File: AE01239.MS
Name: AE01239
QUANT REPORT
Sample: Location: 200 N. Lawrence, SB10-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:46
Injected at: 03/24/99 23:26
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 9.09 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.65 2368
27.99 2397
28.59 2448
225
128
180
Area
82295
154927
75590
Cone Units
0.88 UG/L
0. 88 UG/L
0.82 UG/L
Fit
970
984
969
Rf
0.308
0.585
0. 3 04
Operator ID, MC
Output File, AE01242.1A2
Data File' AE01242.MS
Name' AE01242
QUANT REPORT
Sample, Location, 209 Madison Ave SEll-A
ID File, 826AEC25.QCI
Page
Quant Time' 03/30/99 18,16
Injected at, 03/30/99 14,44
Dilution Factor, 1.00
Instrument ID' 20701-1284
Comment' Sampling, 02/22/1999 by J. Conway, use 4.98 g
Last Calibration, 03/25/99
Compound
l) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time' 03/25/99 08,34
R.T. Scan# Q ion Area Cone Units
14.07 1206
21.18 1815
23.96 2053
4.57 392
0.00 438
0.00 467
6.43 551
0.00 573
7.37 632
0.00 737
9.63 825
0.00 874
0.00 938
0.00 1034
0.00 1034
0.00 1070
0.00 1079
0.00 1113
0.00 1137
0.00 1146
13.63 1168
0.00 1168
0.00 1259
0.00 1292
0.00 1310
0.00 1328
0.00 1390
16.84 1443
0.00 1465
0.00 1495
96
95
152
85
47
2331917
894391
505197
4286
10.00 UG/L
8. 71 UG/L
7.90 UG/L
0.07 UG/L
0 Not Found UG/L
61 0 Not Found UG/L
96 1787 0.10 UG/L
4 9 Not Found UG/L
101 7880 0.07 UG/L
96 Not Found UG/L
49 2082108 7.66 UG/L
61 0 Not Found UG/L
63 0 Not Found UG/L
61 Not Found UG/L
97 Not Found UG/L
49 Not Found UG/L
83 Not Found UG/L
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
Not Found UG/L
Not Found UG/L
18652 0.09 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
27401 0.10 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
94 9
815
267
381
698
90
986
363
993
595
889
350
457
661
258
64 0
515
888
993
895
678
288
355
534
565
986
609
630
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.166
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01242.1A2
Data File: AE01242.MS
Name: AE01242
QUANT REPORT
Sample: Location: 209 Madison Ave SB11-A
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/30/99 18:16
Injected at: 03/30/99 14:44
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 4.98 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
3 3)
34)
35)
3 6)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-l
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.80 1525
0.00
0.00
0.00
0.00
19.36
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (o-Xylene 20.25
Styrene 20.22
1556
1580
1649
1657
1659
1674
1674
1735
1733
1771
1783
1825
1837
1841
1837
1873
1861
1874
1922
1929
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,~~Trichlorobenzene
0.00
20.81
0.00
0.00
0.00
21.44
21.86
21.72
21.87
22.43
22.51
22.81 1955
23.02 1973
23.22 1990
23.28 1995
23.77 2037
0.00 2056
0.00 2184
27.30 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
3298 0.05 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
34524 0.11 UG/L
69637 0.13 UG/L
69637
22566
3138
0. 13 UG/L
0.09 UG/L
0.02 UG/L
0 Not Found UG/L
11748 0.04 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
2911 0.01 UG/L
42251 0.16 UG/L
106079
3 9451
79394
114736
72651
73600
27567
88292
54714
0.40
0.18
0.28
0.42
UG/L
UG/L
UG/L
UG/L
0.24 UG/L
0.30 UG/L
0.21 UG/L
0.68 UG/L
0.23 UG/L
Not Found UG/L
0 Not Found UG/L
15285 0.22 UG/L
Fit
159
937
600
515
386
604
979
991
993
820
841
177
917
413
542
786
906
954
960
974
904
967
921
959
970
974
964
634
4 94
955
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1. 319
2.360
2.360
1.075
0. 576
0.000
1.245
0.000
0.000
0.000
1.438
1.099
1.137
0. 960
1.209
1 . 16 9
1. 304
1 . 051
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID: MC
Output File: AE01242.1A2
Data File: AE01242.MS
Name: AE01242
QUANT REPORT
Sample: Location: 209 Madison Ave SB11-A
ID File: 826AEC25.QCI
Page
Quant Time: 03/30/99 18:16
Injected at: 03/30/99 14:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 4.98 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2367
27.96 2396
28.55 2447
225
128
180
Area
17322
78363
18796
Cone Units
0.24 UG/L
0.57 UG/L
0.27 UG/L
Fit
965
989
943
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01243.1A2
Data File;. AE01243 .MS
Name: AE01243
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-B
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:46
Injected at: 03/25/99 00:45
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.21 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Brcmofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlcrodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chlorcethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.09
21.21
24.00
4.57
0.00
0.00
6.45
0.00
7. 4 0
0.00
9.65
1206
1816
2055
391
438
466
552
572
634
737
825
0.00 874
0.00 942
0.00 1033
0.00 1037
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1142
13.67 1170
0.00 1167
0.00 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.87 1444
0.00 1464
0.00 1496
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2929739
1404465
926307
6005
10.00 UG/L
10.91 UG/L
11.54 UG/L
0.08 UG/L
30945
8410
548305
Not Found UG/L
Not Found UG/L
1.43 UG/L
Not Found UG/L
0.06 UG/L
Not Found UG/L
1.51 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
21199 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
119581 0.34 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
961
850
341
759
549
975
433
993
306
538
533
758
382
506
682
620
850
962
904
690
263
275
380
560
980
590
844
Rf
1.000
0. 44 0
0.274
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.243
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01243.1A2
Data File: AE01243.MS
Name: AE01243
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-B
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/25/99 09:46
Injected at: 03/25/99 00:45
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.21 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
3 9)
4 0)
41 I
42)
43)
44)
45)
46)
47)
4 8)
4 9)
50)
51 I
52)
53)
54)
55)
56)
57)
58)
59 I
60 I
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.83 1526
0.00 1555
0.00
0.00
0.00
19.41
1,3-Dimethylbenzene (m-Xylene 19.55
1,4-Dimethylbenzene (p-Xylene 19.55
1,2-Dimethylbenzene (a-Xylene 0.00
1578
1651
1655
1661
1673
1673
1733
1727
1769
1786
1824
1835
184 3
1850
1863
1871
1881
1923
1930
1956
1974
1983
1985
2039
2057
2185
2344
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.17
0.00
20.86
0.00
0.00
21.53
21.60
0.00
21.85
0.00
22.45
22.54
22.85
23.06
23.16
23.18
23.81
24.02
25.51
27.37
78
166
129·
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
14 6
75
180
Area Cone Units
0 Not Found UG/L
10825 0.14 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
280727 0.73 UG/L
293273
293273
0.42 UG/L
0.42 UG/L
Not Found UG/L
14935 0.09 UG/L
0 Not Found UG/L
162575 0.45 UG/L
0 Not Found UG/L
0 Not Found UG/L
31290 0.16 UG/L
201483
160924
218577
211839
216013
185036
142292
141559
174996
214432
704 3
49604
0. 4 8 UG/L
Not Found UG/L
0. 4 8 UG/L
Not Found UG/L
0.62 UG/L
0.62
0.57
0.60
. 0. 85
0.86
0.60
1. 39
0.33
0.56
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
196
959
623
280
858
590
981
984
983
523
958
478
967
226
187
929
948
912
944
976
969
968
930
938
972
974
981
751
599
947
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1. 320
2.360
2.360
0.000
0.576
0.000
1. 24 7
0.000
0.000
0.685
1.439
0.000
1.13 7
0.000
1.210
1.169
1. 305
1.051
0.575
0.560
1.004
0.526
0.072
0.303
Opera tor ID: MC
Output File: AE01243.1A2
Data File: AE01243.MS
Name: AE01243
QUANT REPORT Page
Quant Time: 03/25/99 09:46
Injected at: 03/25/99 00:45
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 209 Madison Ave, SB11-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.21 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone Units
----------------------------------------
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
27.68 2370
28.03 2400
28.61 2450
225
128
180
55222
107394
54851
0. 61 UG/L
0.63 UG/L
0.62 UG/L
Fit
988
986
975
Rf
0.309
0.585
0.304
Operator ID: MC
Output File: AE01244.1A2
Data File: AE01244.MS
Name: AE01244
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-C
ID File: 826AEC25.QCI
Page 1
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 01:25
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.43 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
J) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
61 75-01-4
71 74-8)-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-l
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
BenZene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
18)
19)
20)
211
22)
23)
24)
25)
26)
27)
28)
29)
301
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.07
21.19
23.96
4.56
0.00
0.00
6.42
0.00
7.38
0.00
9.62
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.64
0.00
14.70
0.00
0.00
0.00
0.00
16.83
0.00
0.00
1204
1814
2052
390
438
466
550
572
632
737
823
874
942
1033
1033
1069
1078
1112
1136
1134
1167
1167
1258
1291
1309
1327
1389
1441
1463
1495
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
9!
75
83
Area Cone Units
2730519 10.00 UG/L
1152229 9.59 UG/L
735840 9.83 UG/L
5622 0.08 UG/L
Not Found UG/L
Not Found UG/L
33096 1.65 UG/L
Not Found UG/L
6419 0.05 UG/L
Not Found UG/L
412792 1.21 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
19015 0.08 UG/L
Not Found UG/L
1601 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
114242 0.35 UG/L
Not found UG/L
Not found UG/L
Fit
999
999
957
830
89
246
709
482
976
377
947
231
600
522
4 9B
271
651
659
305
952
992
903
853
213
276
458
661
983
625
759
Rf
1. 000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 24 7
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01244.1A2
Data File: AE01244.MS
Name: AE01244
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-C
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 01:25
Dilution Factor: 1. oo
Instrument ID: 20701-1284
comment: Sampling: 02/22/1999 by J. Conway, use 5.43 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
4 5)
46)
47)
4 8)
4 9)
50)
51)
52)
53)
54)
55)
S6)
57)
58)
S9)
108-90-7
630-20-6
100-41-4
108-38-3
106-42·3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-B
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scann Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00 1555
0.00 1578
0.00
0.00
19. 4 0
1,3-Dimethylbenzene 1m-Xylene 19.56
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (o-Xylene 0.00
1646
1657
1661
1675
1672
1733
1736
1769
1785
1824
1835
1840
1845
1862
1869
1882
1917
1927
1955
1971
1987
1987
2036
2057
2187
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloroprapane
1,2,4-Trichlorobenzene
20.27
0.00
20.85
0.00
0.00
21.49
21.54
21.74
21.83
21.98
22.39
22.50
22.83
23.01
23.21
23.21
23.78
24.02
o.oo
27.34 2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
7047 0.10 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
78939 0.22 UG/L
172794 0.27 UG/L
238257 0.37 UG/L
0 Not Found UG/L
69321 0.44 UG/L
0 Not Found UG/L
137707 0.40 UG/L
0 Not Found UG/L
Not Found UG/L
90174
119705
119576
110470
89790
55317
151881
97147
151931
70827
70252
121355
5744 7
41904
0.48 UG/L
0.30 UG/L
0.40 UG/L
0.36 UG/L
0. 34 UG/L
0.17 UG/L
0.48 UG/L
0.27 UG/L
0.53 UG/L
0.45 UG/L
0.46 UG/L
0.44 UG/L
0.40 UG/L
Nat Found UG/L
0. 51 UG/L
Fit
239
928
518
842
719
984
978
980
572
974
608
927
418
658
921
946
931
909
980
927
937
768
936
988
986
962
827
663
934
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1. 319
2.360
2.360
0.000
0.577
0.000
1. 24 6
0.000
0.000
0.685
1.438
1 . 100
1.137
0. 961
1. 209
1 . 16 9
1.304
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator lD: MC
Output File: AE01244.1A2
Data File: AE01244.MS
Name: AE01244
QUANT REPORT
Sample: Locat~on: 209 Madison Ave, SB11-C
ID Pile: 826ABC25.QCI
Page
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 01:25
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.43 g
Last calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
compound R.T. Scan# Q ion Area Cone
-------- -------------------------------------------61) 87-68-3 Hexachlorobutadiene 27.65 2368 225 52731 0.63
62) 91-20-3 Naphthalene 27.99 2397 128 105830 0.66
6 3) 82-61-6 1,2,3-Trichlorobenzene 28.57 2447 180 50740 0.61
• Compound is ISTD
units Fit Rf
--------
UG/L 968 0.309
UG/L 990 0.585
UG/L 959 0.304
Operator ID: MC
Output File: AE01245.1A2
Data File: AE01245.MS
Name: AE01245
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-D
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 02:05
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.74 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane·
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
l4. 07
21.18
23.95
4.55
0.00
0.00
6.42
0.00
7.38
0.00
9.62
0.00
0.00
0.00
0.00
0.00
12.60
0.00
0.00
0.00
13.62
0.00
14.70
15.00
0.00
0.00
0.00
16.82
0.00
0.00
1205
1814
2052
390
438
466
550
573
632
737
824
874
943
1033
1033
1071
1078
1112
1136
1144
1167
1167
1259
1285
1307
1327
1390
1441
1464
14 93
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2838193
114 7212
7 34 219
7282
10.00 UG/L
9.18 UG/L
9.44 UG/L
0.10 UG/L
Not Found UG/L
0 Not Found UG/L
22541 1.08 UG/L
Not Found UG/L
7026 0.05 UG/L
0 Not Found UG/L
384552 1.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
3366 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
18948 0.07 UG/L
0 Not Found UG/L
1867 0.03 UG/L
739 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
125320 0.37 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
953
884
166
633
659
596
971
373
983
296
507
432
490
797
721
468
543
835
967
900
874
410
721
565
532
983
645
738
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.249
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0. 14 9
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID' MC
Output File, AE01245.1A2
Data File, AE01245.MS
Name, AE01245
QUANT REPORT
Sample' Location, 209 Madison Ave, SB11-D
ID File' 826AEC25.QCI
Page 2
Quant Time, 03/25/99 09,47
Injected at, 03/25/99 02,05
Dilution Factor, 1. 00
Instrument ID, 20701-1284
Comment, Sampling, 02/22/1999 by J. Conway, use 5.74 g
Last Calibration' 03/25/99 Last Qcal Time, 03/25/99 09,34
31)
32)
33)
34)
35)
3 6)
37)
38)
39)
40)
41)
42)
43)
44)
4 5)
46)
47)
4 8)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.80
0.00
0.00
19.2 5
0.00
19.43
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 0.00
1521
1525
1550
1579
1649
1656
1664
1674
1674
1734
1736
1771
1787
1825
1836
184 3
184 7
1864
1869
1881
1923
1927
1954
1972
1981
1993
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.26
0.00
20.86
0.00
0.00
21.51
21.56
0.00
21.82
21.96
22.45
22.50
22.80
23.02
23.13
23.26
23.79 2038
.23.97 2054
25.49 2184
27.30 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
-- -tr---Not Found UG/L
9208 0.12 UG/L
Not Found UG/L
Not Found UG/L
41467 0.20 UG/L
Not Found UG/L
43370 0.12 UG/L
146462 0.22 UG/L
146462 0.22 UG/L
0 Not Found UG/L
62702 0.38 UG/L
Not Found UG/L
101816 0.29 UG/L
73229
182264
235807
114 704
151260
156716
178275
127350
73776
163170
179102
110549
14654
37798
Not Found UG/L
Not Found UG/L
0.38 UG/L
0.45 UG/L
Not Found UG/L
0.73 UG/L
0.42 UG/L
0.44 UG/L
0.47 UG/L
0.48 UG/L
0.43 UG/L
0.45 UG/L
1.03 UG/L
0.63 UG/L
0.74 UG/L
0.72 UG/L
0. 44 UG/L
Fit
324
899
849
351
841
491
980
986
988
590
954
781
940
460
567
921
976
963
926
962
958
953
932
931
977
979
968
776
532
976
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.319
2.360
2.360
0.000
0.576
0.000
1.246
0.000
0.000
0.685
1. 439
0.000
1.138
0.961
1.209
1.169
1.305
1.051
0.575
0.560
1.004
0.526
0.073
0.303
Operator ID: MC
Output File: AE01245.1A2
Data File: AE01245.MS
Name: AE01245
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-D
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 02:05
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.74 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Ti~e: 03/25/99 08:34
R.T. Scan# Q ion· Area
27.63 2367
27.99 2398
28.58 2448
225
128
180
52803
93168
48035
Cone Units
0.60 UG/L
0.56 UG/L
0.56 UG/L
Fit
971
981
972
Rf
0.309
0.586
0.304
Operator ID: MC
Output File: AE01246.1A2
Data File: AE01246.MS
Name: AE01246
QUANT REPORT
Sample: Location: 209 Madison Ave, SEll-E
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 02:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/25/99
Compound
11 *107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SGI
31 1,2-Dichlorobenzene-d4 (SGI
41 75-71-8 Dichlorodifluoromethane
51 74-87-3
61 75-0l-4
71 74-83-9
81 75-00-3
91 75-69-4
101 75-35-4
lll 75-09-2
121 156-60-5
131 75-34-3
141 156-59-4
151 590-20-7
161 74-97-5
171 67-66-3
181 71-55-6
191 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Brornomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
201
211
221
23 I
241
251
26)
27)
281
29 I
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.08 1204 96
21.18 1813 95
23.97 2053 152
4.58 392 85
0.00 438 47
o.oo 466 61
6.44 551- 96
0.00 572 49
7.39 633 101
o.oo 737 96
9.64 824 49
0.00 874 61
0.00 942 63
0.00 1033
o.oo 1033
0.00 1069
12.59 1077
o.oo lll2
0.00 1136
0.00
13.65
o.oo 14.70
0.00
0.00
0.00
0.00
16.83
0.00
0.00
1138
1168
ll65
1258
1297
1309
1327
1389
1441
1463
14 93
61
97
49
83
97
75
ll7
78
62
130
63
93
83
75
91
75.
83
Area Cone Units
2731382
1035223
717963
5144
10.00 UG/L
8.60 UG/L
9.59 UG/L
0.07 UG/L
0 Not Found UG/L
Not Found UG/L
15277 0.76 UG/L
0 Not Found UG/L
6819 0.05 UG/L
Not Found UG/L
414550 1.22 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
2979 0.03 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
16025 0.07 UG/L
0 Not Found UG/L
2080 0.03 UG/L
No"t Found UG/L
Not Found UG/L
0 Not Found UG/L·
0 Not Found UG/L
94890 0.29 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
997
999
959
874
302
490
689
195
979
632
979
353
540
412
373
578
778
34 7
436
801
976
915
708
403
355
441
266
977
671
663
Rf
1.000
0. 441
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.000
1.247
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01246.1A2
Data File: AE01246.MS
Name: AE01246
Quant Time: 03/25/99 09:47
Injected at: 03/25/99 02:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 209 Madison Ave, SBll-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
3 6)
3 7)
38)
3 9)
40)
41)
42)
43)
44)
4 5)
46)
47)
48)
4 9)
so)
51)
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
0.00
17.80
0.00
0.00
19.26
1,1,1,2-Tetrachloroethane 0.00
Ethylbenzene 0.00
1,3-Dimethylbenzene (m-Xylene 19.56
1,4-Dimethylbenzene (p-Xylene 19.56
1,2-Dimethylbenzene (a-Xylene 0.00
Styrene
Bromoform.
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.27
0.00
20.87
0.00
21.19
0.00
21.57
0.00
21.79
21.97
22.46
22.51
22.82
23.03
23.14
23.28
23.77
24.06
0.00
27.34
1520
1524
1555
1578
1649
1655
1666
1674
1674
1733
1735
1769
1787
1824
1814
1846
1847
1874
1866
1881
1923
1928
1954
1972
1981
1993
2036
2060
2184
2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
14708 0.20 UG/L
0 Not Found UG/L
Not Found UG/L
17089 0.09 UG/L
0 Not Found UG/L
Not Found UG/L
207341 0.32 UG/L
207341 0.32 UG/L
0 Not Found UG/L
44856 0.29 UG/L
0 Not Found UG/L
122065 0.36 UG/L
Not Found UG/L
584594 7.23 UG/L
0 Not Found UG/L
118197 0.30 UG/L
0 Not Found UG/L
143732 0.46 UG/L
74281 0.28 UG/L
145337
151259
159652
122025
62376
110742
113679
52099
35454
0.44 UG/L
0.47 UG/L
0.45 UG/L
0.43 UG/L
0.40 UG/L
0.73 UG/L
0.41 UG/L
0.36 UG/L
Not Found UG/L
0.43 UG/L
Fit
82
976
688
379
852
810
980
973
979
617
939
476
939
537
723
934
963
924
905
977
947
941
824
920
958
969
974
793
605
930
Rf
0.000
0.266
0.000
0.000
0.717
0.000
0.000
2.360
2.360
0.000
0.576
0.000
1.246
0.000
0.297
0.000
1.438
0.000
1.137
0.961
1.209
1.169
1.305
1. 051
.575
0.560
1. 004
0.526
0.000
0.303
---------------------------------------------------------------------------------------
Operator ID: MC
Output File: AE01246.1A2
Data File: AE01246.MS
Name: AE01246
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-E
ID File: 826AEC25.QCI
Page
Quant 'rime: 03/25/99 09:47
Injected at: 03/25/99 02:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.32 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
-----~---------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.67 2369 225 42746 0.51
62) 91-20-3 Naphthalene 28.00 2398 128 82781 0.52
63 I 82-61-6 1,2,3-Trichlorobenzene 28.59 2448 180 42104 0.51
• Compound is ISTD
Units Fit Rf
--------
UG/L 966 0.309
UG/L 975 0.586
UG/L 962 0. 304
Operator ID: MC
Output File: AEOl247.lA2
Data File: AE01247.MS
Name: AE01247
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 03:24
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.62 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
71-55-6
563-58-6
56-"23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
18)
19)
2 0)
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
3 0)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.08
21.20
23.98
4.59
0.00
0.00
6.44
0.00
7.38
0.00
9.64
1205
1815
2054
392
438
473
551
572
632
737
824
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00
0.00
0.00
13.65
0.00
14.69
0.00
0.00
0.00
0.00
16.85
0.00
0.00
1112
1136
1131
1168
1167
1257
1291
1309
1327
1389
1442
1464
14 88
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2765625
1194875
766507
5620
10.00 UG/L
9.82 UG/L
10.11 UG/L
0.08 UG/L
18129
5324
561624
Not Found UG/L
Not Found UG/L
0.89 UG/L
Not Found UG/L
0.04 UG/L
Not Found UG/L
1.64 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
25880 0.10 UG/L
0 Not Found UG/L
1278 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
115312 0.35 UG/L
0 Not Found .UG/L
Not Found UG/L
Fit
998
999
955
821
178
567
618
444
969
347
988
323
479
486
588
397
453
164
550
750
976
831
757
132
529
243
352
978
543
809
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0.456
0.000
1.241
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01247.1A2
Data File: .AE01247 .MS
Name: AE01247
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-F
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 03:24
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.62 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) l-06-93-4
35) l-08-90-7
36) 630-20-6
37) l-00-41-4
38) l-08-38-3
39) 106-42-3
40) %-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.83 1526
0.00 1555
·o.oo 1578
19.26 1649
0.00 1655
19.32 1654
1,3-Dimethylbenzene (m-Xylene 19.56 1675
1,4-Dimethylbenzene (p-Xylene 19.56 1675
1,2-Dimethylbenzene (a-Xylene 0.00 1733
Styrene 20.27 1736
Bromoform
Isopropylbenzene
44) 79-3~-5 1,1,2,2-Tetrachloroethane
0.00 1769
20.79 1780
0.00 1824
0.00 1835
21.49 1840
21.56 1846
45) 96-18-4 ·1,2,3-Trichloropropane
46) 108-86-1 Bromobenzene
47) 103-65-1 n-Propylbenzene
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1~2,4-Trichlorobenzene
0.00 1873
21.77 1864
22.03 1886
22.41 1919
22.62 1937
0.00 1953
23.04 1973
23.16 1983
23.29 1994
23.80 2038
21.08 2062
0.00 2183
27.32 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
6371 0.09 UG/L
Not Found UG/L
Not Found UG/L
22066 0.11 UG/L
0 Not Found UG/L
13 3 8 82
176755
176755
0.37 UG/L
0. 27 UG/L
0.27 UG/L
0 Not Found UG/L
9593 0.06 UG/L
Not Found UG/L
53883 0.16 UG/L
0 Not Found UG/L
Not Found UG/L
47739
104664
0.25 UG/L
0.26 UG/L
Not Found UG/L
88248 0.28 UG/L
19876 0.07 UG/L
59487 0.18 UG/L
222032 0.69 UG/L
Not Found UG/L
126166 0.43 UG/L
64327
107555
132539
40753
35752
0.40 UG/L
0.70 UG/L
0.48 UG/L
0.28 UG/L
Not Found UG/L
0.43 UG/L
Fit
327
899
555
616
876
574
982
982
978
594
944
563
909
295
606
881
956
918
893
966
937
937
541
935
967
981
968
729
575
914
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1 . 3 2 0
2.360
2.360
0.000
0.576
0.000
l. 246
0.000
0.000
0.685
l. 438
0.000
1.137
0. 960
l. 209
1.169
0.000
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01247.1A2
Data File: AE01247.MS
Name: AE01247
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 03:24
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.62 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.65 2368 225 44841 0.53
62) 91-20-3 Naphthalene 28.00 2398 128 75442 0.4 7
6 3) 82-61-6 1,2,3-Trichlorobenzene 28.62 2451 180 37959 0. 45
• Compound is ISTD
Units Fit Rf
--------
UG/L 976 0.309
UG/L 984 0.586
UG/L 939 0.304
Operator ID: MC
Output File: AE01248.1A2
Data File: AE01248.MS
Name: AE01248
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 04:04
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 6.41 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.08
21.20
23.97
4.55
0.00
0.00
6. 43
0.00
7.38
0.00
9.65
0.00
0.00
0.00
0.00
0.00
0.00
13.02
0.00
0.00
13.66
0.00
14.71
0.00
0.00
0.00
1206
1816
2054
390
438
466
551
573
632
737
826
874
943
1033
1036
1069
1079
1114
1136
1135
1170
1172
1260
1291
1309
1327
0.00 1390
16.85 1443
0.00 1464
0.00 1492
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Unir.s
2562245 10.00 UG/L
1087260 9.64 UG/L
668979 9.53 UG/L
4812 0.07 UG/L
Not Found UG/L
Not Found UG/L
15691 0.83 UG/L
Not Found UG/L
6065 0.05 UG/L
Not Found UG/L
569167 1.79 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
1171 0.01 UG/L
Not Found UG/L
0 Not Found UG/L
52431 0.23 UG/L
0 Not Found UG/L
1173 0.02 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
122749 0.40 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
948
848
417
25
713
545
967
389
986
102
539
463
604
368
410
749
525
911
998
872
838
253
513
557
396
985
544
723
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0. 4 55
0.000
l. 239
0.000
0.000
0.000
0.000
0.000
0.000
0.537
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01248.lA~
Data File: AE01248.MS
Name: AE01248
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 04:04
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/2~/1999 by J. Conway, use 6.41 g
Last Calibration: 03/~5/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
39)
100-41-4
108-38-3
106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-D~chloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Eth'/lbenzene
0.00 1521
17.81 1526
18.25 1563
0.00 1579
19.16 1642
0.00 1656
19.37
1,3-Dimethylbenzene (m-Xylene 19.56
1,4-Dimethylbenzene (p-Xylene 19.56
1659
1676
1676
1,2-Dimethylbenzene (a-Xylene 0.00 1734
Styrene 20.32 1740
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Brornobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1779
20.83 1784
0.00 1825
0.00 1836
21.54 1845
21.57 1848
0.00 1869
21.82 1869
22.01 1886
22.39 1918
22.54 1931
0.00 1954
23.03 1973
23.18 1986
23.30 1996
23.80 2039
24.04 2060
0.00 2183
27.36 2344
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
10086
2051
0 .15 UG/L
0.04 UG/L
0 Not Found UG/L
7599 0.04 UG/L
0 Not Found UG/L
214924
239427
239427
0.64 UG/L
0.40 UG/L
0.40 UG/L
0 Not Found UG/L
51443 0.35 UG/L
Not Found UG/L
20237 0.06 UG/L
Not Found UG/L
Not Found UG/L
67609 0.39 UG/L
110750 0.30 UG/L
0 Not Found UG/L
112848
35921
38160
14 0 34 9
0.39 UG/L
0.15 UG/L
0.12 UG/L
0.47 UG/L
Not Found UG/L
106171 0.39 UG/L
25721
156637
115570
67006
0.17 UG/L
1.09 UG/L
0.45 UG/L
0.50 UG/L
0 Not Found UG/L
35006 0.45 UG/L
Fit
226
936
725
312
825
617
975
990
992
646
937
730
913
442
672
871
954
916
930
969
942
944
608
928
966
986
964
761
444
909
Rf
0.000
0.266
0.214
0.000
0.717
0.000
1.320
2.360
2.360
0.000
0.576
0.000
1. 245
0.000
0.000
0.685
1.438
0.000
1.137
0.960
l. 209
1.16 9
0.000
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01248.1A2
Data File: AE01248.MS
Name: AE01248
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 04:04
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 6.41 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.66 2370 225 40692 0.51
62) 91-20-3 Naphthalene 28.00 2399 128 77282 0.52
6 3) 82-61-6 1,2,3-Trichlorobenzene 28.62 2452 180 39272 0.51
• Compound is ISTD
Units Fit Rf
--------
UG/L 962 0.309
UG/L 980 0.586
UG/L 964 0. 304
Operator ID: MC
Output File: AE01249.1A2
Data File: AE01249.MS
Name: AE01249
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 04:43
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.78 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 ISG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.08 1205
21.18 1814
23.97 2053
4.60 394
0.00 438
0.00 466
0.00 549
0.00 572
7.39 633
0.00 737
9.65 825
0.00 874
0.00 934
0.00 1033
0.00 1033
0.00 1069
12.61 1079
0.00 1112
0.00 1136
0.00 1143
13.66 1169
0.00 1167
14.70 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.85 1442
0.00 1464
0. 00 1487
96 3075828
95 1296308
152 776814
10.00 UG/L
9.58 UG/L
9_21 UG/L
0.07 UG/L 85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
5351
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
7827 0.06 UG/L
0 Not Found UG/L
749549 1.97 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
3326 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
21549 0.08 UG/L
0 Not Found UG/L
1547 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
136920 0.37 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
958
783
129
571
167
984
377
966
387
763
490
563
226
767
635
295
748
986
860
749
289
196
468
622
980
595
812
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.000
0.000
0. 4 55
0.000
1. 237
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01249.1A2
Data File: AE01249.MS
Name: AE01249
QUANT RE,PORT
Sample: Location: 209 Madison Ave, SB11-H
ID File: 826AEC25.QCI
Page 2
Quant Tim~: 03/25/99 09:48
Injected at: 03/25/99 04:43
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.78 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
39)
40)
41)
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.82 1525
0.00 1555
0.00 1578
0.00 1650
0.00 1655
19.38
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 20.26
1659
1673
1673
1735
1731 Styrene
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n~Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.22
0.00 1769
20.86 1786
0.00 1824
0.00 1835
21.52 1842
21.58 1847
0.00 1866
21.84 1870
22.02 1885
22.46 1923
22.54 1930
22.85 1956
23.05 1973
23.17 1984
23.29 1994
23.81 2039
24.03 2058
0.00 2187
27.35 2342
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
14 6
91
146
75
180
Area Cone Units
Not Found UG/L
10222 0.13 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
230188
206540
206540
78268
34909
0.57 UG/L
0.28 UG/L
0.28 UG/L
0.24 UG/L
0.20 UG/L
Not Found UG/L
63219 0.17 UG/L
Not Found UG/L
Not Found UG/L
21917 0.10 UG/L
76481
l 0244 3
464 74
133922
91265
102704
106732
102679
0. 17 UG/ L
Not Found UG/L
0.29 UG/L
0.16 UG/L
0.36 UG/L
0.25 UG/L
0.26 UG/L
0. 33 UG/L
0.58 UG/L
131468 0.76 UG/L
110980 0.36 UG/L
54491 0.34 UG/L
Not Found UG/L
31921 0.34 UG/L
Fit
295
951
454
86
859
626
985
982
988
702
962
619
918
448
611
863
952
949
916
961
937
917
729
902
986
972
969
776
663
920
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1. 246
0.000
0.000
0.685
1.438
0.000
1.137
0.960
1. 209
1 . 16 9
1. 304
1 . 051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01249.1A2
Data File: AE01249.MS
Name: AE01249
QUANT REPORT
Sample: Location: 209 Madison Ave, SB11-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/25/99 09:48
Injected at: 03/25/99 04:43
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.78 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.68 2371
28.01 2398
28.59 2449
225
128
180
Area
19003
67326
39958
Cone Units
0.20 UG/L
0.37 UG/L
0.43 UG/L
Fit
962
983
974
Rf
0.310
0.586
0.304
Operator IDo MC
Output Fileo AE01252.1A2
Data Fileo AE01252.MS
Nameo AE01252
QUANT REPORT
Sampleo Locationo 300 Madison Ave, SB12-A
ID Fileo 826AEC25.QCI
Page
Quant Timeo 03/27/99 19o10
Injected ato 03/26/99 22o18
Dilution Factoro 1. 00
Instrument IDo 20701-1284
Commento Samplingo 02/23/1999 by J. Conway, use 6.71 g / Last Calibration, 03/25/99
Compound
1 I *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3 I
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroeth~ne
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1, 1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Timeo 03/25/99 08o34
R.T. Scan# Q ion Area Cone Units
14.05 1203
21.15 1812
23.94 2051
4.54
0.00
0.00
6.39
6.64
7.36
0.00
9.60
388
438
469
547
569
630
737
822
0.00 874
0.00 943
0.00 1033
0.00 1033
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1140
13.62 1166
0.00 1162
14.68 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.81 1440
17.15 1469
0.00 1494
96 2181196
95 1071583
10.00 UG/L
11.18 UG/L
11.21 UG/L 152 670221
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
5252
2973
326
4435
157660
0.09 UG/L
Not Found UG/L
Not Found UG/L
0.18 UG/L
0.03 UG/L
0. 04 UG/L
Not Found UG/L
0.58 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
12215 0.06 UG/L
0 Not Found UG/L
486 0. 01 UG/L
Not Found UG/L
0 Not Found UG/L
61081
136481
Not Found UG/L
Not Found UG/L
0.23 UG/L
1.93 UG/L
0 Not Found UG/L
Fit
998
1000
950
887
90
656
691
729
980
137
966
170
550
297
368
326
425
647
498
BOO
980
807
742
277
385
680
572
978
707
819
Rf
1.000
0. 44 0
0.275
0.258
0.000
0.000
0.074
0.047
0.455
.000
1.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.324
0.000
Operator ID, MC
Output File, AE01252.1A2
Data File, AE01252.MS
Name, AE01252
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-A
ID File, 826AEC25.QCI
Page
Quant Time, 03/27/99 19:10
Injected at, 03/26/99 22:18
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 6.71 g
Last Calibration, 03/25/99 Last Qcal Time, 03/25/99 08:34
Compound R. T. Scan# Q _ion
31) 142-28-9 1,3-Dichloropropane 0.00 1521
17.78 1523 32) 127-18-4 Tetrachloroethene
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
45)
4 6)
4 7)
48)
4 9)
50)
51)
52)
53)
54)
55)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
0.00
0.00
0.00
19.35
1, 3-Dimethylbenzene 1m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.23
1556
1579
1647
1656
1657
1671
1671
1733
1735
1770
1785
1825
1836
1844
184 5
1870
1867
1885
192 0
1927
1954
1971
1981
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.26
0.00
20.83
0.00
0.00
0.00
21.53
21.83
21.80
22.00
22.41
22.4 9
0.00
23.00
23.12
23.25 1992
23.76 2036
23.97 2054
0.00 2183
27.29 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
6247 0.11 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
88531 0.31 UG/L
98712
98712
47417
8367
0.19 UG/L
0.19 UG/L
0.20 UG/L
0.07 UG/L
Not Found UG/L
36673 0.14 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
82803
45447
91025
2366
72985
97305
59445
35225
27580
54 792
65581
0.26 UG/L
0.19 UG/L
0.37 UG/L
0.01 UG/L
0.28 UG/L
0.38 UG/L
Not Found UG/L
0.26 UG/L
0.28 UG/L
0.23 UG/L
0.25 UG/L
0.57 UG/L
0 Not Found UG/L
17046 0.26 UG/L
Fit
322
950
332
26
777
620
978
986
991
765
905
306
959
410
666
822
950
928
943
965
945
970
634
930
969
984
884
732
177
922
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1. 246
0.000
0.000
0.000
1.438
1 . 0 9 9
1.137
0. 960
1. 209
1 .169
0.000
1.051
0.575
0.559
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01252.1A2
Data File: AE01252.MS
Name: AE01252
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-A
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:10
Injected at: 03/26/99 22:18
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 6.71 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.62 2366 225 20284 0.30
62) 91-20-3 Naphthalene 27.95 2395 128 39966 0.31
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2446 180 19627 0.30
* Compound is ISTD
Units Fit Rf
--------
UG/L 953 0.310
UG/L 981 0.586
UG/L 951 0.304
Operator ID: MC
Output File: AE01253.1A2
Data File: AE01253.MS
Name: AE01253
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-B
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:10
Injected at: 03/26/99 22:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.69 g j Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.02 1199
21.13 1809
23.91 2047
4.51
0.00
0.00
6.39
0.00
7.33
. 0. 00
9.57
386
438
463
547
571
628
737
819
0.00 874
0.00 942
0.00 1033
0.00 1040
0.00 1069
0.00 1078
0.00 1107
0.00 1136
0.00 1133
13.59 1163
0.00 1162
0.00 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.79 1437
0.00 1463
0.00 1493
96 2235891
95 1016265
152 653987
10.00 UG/L
1 0. 34 UG/L
10.67 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4705 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
5193
4939
145535
1534 5
0.31 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
0.52 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.08 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
46 948
Not Found UG/L
Not Found UG/L
0.18 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
950
863
90
530
676
884
977
240
981
410
635
485
699
621
358
809
609
912
986
887
585
364
307
316
459
981
593
678
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.000
1.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID, MC
Output File, AE01253.1A2
Data File\ AE01253.MS
Name, AE01253
QUANT REPORT
Sample, Location, 300 Madison Ave, SB12-B
ID File, 826AEC25.QCI
Page 2
Quant Time, 03/27/99 19,10
Injected at' 03/26/99 22,57
Dilution Factor' 1.00
Instrument ID' 20701-1284
Comment, Sampling, 02/23/1999 by J. Conway, use 5.69 g
Last Calibration, 03/25/99 Last Qcal Time, 03/25/99 08,34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-4\-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.76 1520
0.00 1555
0.00 1578
19.18 1642
0.00 1656
19.34 1655
1, 3-Dimethylbenzene (m-Xylene 19.48 1668
1,4-Dimethylbenzene (p-Xylene 19.48 1668
1,2-Dimethylbenzene (a-Xylene 20.18 1728.
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,~,4-Trichlorobenzene
20.25 1734
0.00 1769
0.00 1785
0.00 1824.
0.00 1835
0.00 1842
21.51 1842
21.88 1873
21.79 1865
21.86 1872
22.39 1917
22.47 1924
22.77 1950
22.96 1966
23.20 1986
23.22 1988
23.76 2034
0.00 2054
0.00 2182
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Pound UG/L
3774 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
4757
50980
84095
84 095
42153
4 966
0.03 UG/L
Not Found UG/L
0.17 UG/L
0.16 UG/L
0.16 UG/L
0.18 UG/L
0.04 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
45294
43373
134224
40184
6764 9
79994
71014
55582
28394
45707
46786
Not Found UG/L
Not Found UG/L
0.14 UG/L
0.18 UG/L
0.53 UG/L
0.19 UG/L
0.25 UG/L
0.31 UG/L
0.24 UG/L
0.24 UG/L
0.22 UG/L
0.37 UG/L
0.21 UG/L
Not Found UG/L
0 Not Found UG/L
16335 0.24 UG/L
Fit
671
. 84 9
406
108
831
712
984
987
988
738
894
255
906
413
680
802
924
956
921
986
916
944
859
929
972
973
940
64 9
343
932
Rf
0.000
0.266
0.000
0.000
.717
0.000
1.319
2.360
2.360
1.076
0.576
0.000
0.000
0.000
0.000
0.000
1. 4 3 8
1.099
1.137
0. 960
1.209
1.169
1.304
1 . 0 51
0.575
0.559
1.005
0.000
0.000
0.303
Operator ID, MC
Output File, AE01253.1A2
Data File, AE01253.MS
Name, AE01253
QUANT REPORT
Sample, Location' 300 Madison Ave, S812-8
ID File, 826AEC25.QCI
Page
Quant Time, 03/27/99 19,10
Injected at, 03/26/99 22,57
Dilution Factor' 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/23/1999 by J. Conway, use 5.69 g
Last Calibration' 03/25/99 Last Qcal Time, 03/25/99 09,34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.57 2361 225 19255 0.28
62) 91-20-3 Naphthalene 27.93 2392 128 35723 0.27
63) 82-61-6 1,2,3-Trichlorobenzene 28.53 2443 180 17459 0.26
• Compound is ISTD
units Fit Rf
--------
UG/L 967 0.310
UG/L 988 0.586
UG/L 8 54 0. 3 04
Operator ID: MC
Output Pile: AE01254.1A2
Data Pile: AE01254.MS
Name: AE01254
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-C
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:11
Injected at: 03/26/99 23:36
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.86 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dich1orobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromo~hloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.94 2050
4.55
0.00
0.00
6.41
6.67
7. 36,
0.00
9.61
389
438
466
549
571
630
737
822
0.00 874
0.00 944
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1138
13.62 1166
0.00 1164
0.00 1258
0.00 1291
0.00 1309
15.51 1328
0.00 1389
16.82 1440
0.00 1463
0.00 1493
96 2196326
95 1084556
152 653105
10.00 UG/L
11.24 UG/L
10.85 UG/L
· 0. 09 UG/L 85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4864
Not Found UG/L
0 Not .Found UG/L
7992
453
54 88
0.49 UG/L
0.04 UG/L
0.05 UG/L
0 Not Found UG/L
199436 0. 72 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
·Not Found UG/L
'13 941 0.07 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
70 0.00 UG/L
0 Not Found UG/L
514 94 0.20 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
94 7
828
0
165
728
BOB
985
478
989
196
898
19·
430
573
553
570
315
623
981
868
657
216
284
719
418
984
580
602
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0. 04 7
0.455
0.000
1. 254
0.000
0.000
0.000
0.000
0.000
0.000
.o. 0 0 0
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.327
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01254.1A2
Data File: AE01254.MS
Name: AE01254
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-C
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/27/99 19:11
Injected at: 03/26/99 23:36
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.86 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. ScanU Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
111,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00 1555
0.00 1578
19.25 1648
0.00 1655
19.53 1672
1,3-Dimethylbenzene (m-Xylene 19.53 1672
1,4-Dimethylbenzene (p-Xylene 19.53 1672
1,2-Dimethylbenzene (~-Xylene 20.23 1732
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
te~t-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-i3utylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1733
0.00 1769
20.83 1784
0.00 1824
0.00 1835
0.00 1841
21.57 1847
21.91 1876
21.82 1868
21.89 1874
22.42 1920
22.49 1926
22.81 1953
23.01 1970
23.10 1978
23.25 1991
23.77 2035
0.00 2054
0.00 2182
27.30 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
3761
4043
110054
110054
110054
46269
12127
Cone Units
Not Found UG/L
0.06 UG/L
Not Found UG/L
Not Found UG/L
0.03 UG/L
Not Found UG/L
0.38 UG/L
0.21 UG/L
0.21 UG/L
0. 20 UG/L
0.10 UG/L
0 Not Found UG/L
3394 9 0.13 UG/L
Not Found UG/L
0 Not Found UG/L
·o Not Found UG/L
48524
51442
135564
48329
63803
59756
4 7711
45530
29276
57056
51234
0.15 UG/L
0.21 UG/L
0.54 UG/L
0.23 UG/L
0.24 UG/L
0.23 UG/L
0.17 UG/L
0.20 UG/L
0.23 UG/L
0.46 UG/L
0.23 UG/L
0 Not Found UG/L
Not Found UG/L
14952 0.22 UG/L
Fit
454
896
442
735
680
975
991
988
742
860
314
922
356
573.
843
889
943
933
973
951
939
740
929
964
964
920
684
365
905
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
1.320
2.360
2.360
1 . 076
0.576
0.000
l. 246
0.000
0.000
0.000
1.438
1.100
1.138
0.960
1.209
l. 169
1.304
1.051
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID, MC
Output File, AE01254.1A2
Data File, AE01254.MS
Name' AE01254
QUANT REPORT
Sample' Location, 300 Madison Ave, SB12-C
ID File, 826AEC25.QCI
Page
Quant Time, 03/27/99 19,11
Injected at, 03/26/99 23,36
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/23/1999 by J. Conway, use 5.86 g
Last Calibration, 03/25/99
61) 87-68-3
62) 91-20-3
1;3) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time, 03/25/99 09,34
R.T. Scan# Q ion
27.61 2364
27.94 2392
28.56 2446
225
128
180
Area
17456
35918
17733
Cone Units
0.26 UG/L
0.28 UG/L
0.27 UG/L
Fit
957
975
930
Rf
0.310
0.586
0. 3 04
Operator ID: MC
Output File: AE01255.1A2
Data File: AE01255.MS
Name: AE01255
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-D
Page
Quant Time: 03/27/99 19:12
Injected at: 03/27/99 00:16
Dilution Factor: 1. oo
Instrument ID: 20701-1284
ID File: 826AEC25.QCI /
Comment: Sampling: 02/23/1999 by J. Conway, use 7.31 g ~ Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-BromoEluorobenzene ISGI
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 DichlorodiEluoromethane
51 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
121 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
171 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
211 71-43-2
221 107-06-2
23) 79-01-6
241 78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
ChloroEorm
1,1, l-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
251
26)
271
28 I
29 I
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.05 1202
21.16 1812
23.94 2050
4.54 388
0.00 438
0.00 466
6.40 548
0.00 579
7.36 630
0.00 737
9.61 822
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 -1129
13.62 1165
0.00 1165
14.65 1254
0.00 1283
0.00
0.00
0.00
16.82
0.00
0.00
1309
1327
1389
1440
1463
14 93
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Unit.s
2264580
1076572
693872
4363
10.00 UG/L
10.82 UG/L
11.18 UG/L
0.07 UG/L
Not Found UG/L
0 Not Found UG/L
8880 0.53 UG/L
Not Found UG/L
5034 0.05 UG/L
0 Not Found UG/L
271434 0.96 UG/L
o·Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
16938 0.08 UG/L
0 Not Found UG/L
557 0.01 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
65413 0.24 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
953
798
55
404
686
836
983
130
935
392
371
515
174
496
588
647
453
825
986
888
724
401
4 76
528
605
986
617
621
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
l . 2 51
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID, MC
Output File, AE01255.1A2
Data File, AE01255.MS
Name, AE01255
QUANT REPORT
Sample' Location' 300 Madison Ave, SB12-D
ID File, 826AEC2S.QCI
Quant Time:
Injected at,
Dilution Factor:
Instrument ID:
Comment, Sampling' 02/23/1999 by J. Conway, use 7.31 g
Page 2
03/27/99 19,12
03/27/99 00,16
l. 00
20701-1284.
Last Calibration' 03/25/99 Last Qcal Time, 03/25/99 09,34
31)
32)
3 3)
34)
35)
36)
3 7)
38)
3 9)
4 0 I
41)
42)
43)
44)
4.5)
46)
47)
48)
4 9)
50)
51)
142-28-9
127-18-4
124-4.8-1
106-93-4.
108-90-7
630-20-6
100-4.1-4
108-38-3
106-4.2-3
95-47-6
100-42-5
75-25-2
98-82-B
79-34-5
96-18-4
108-86-1
103-65-1
95-49-B
108-67-8
106-43-4.
98-06-6
52) 95-63-6
53)
54)
55)
56)
57)
58)
59)
6 0)
135-98-8
99-87-6
54.1-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.2 0
0.00
19.3 5
1,3-Dimethylbenzene 1m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (o-Xylene 20.22
Styrene 20.23
Bromoform 0.00
20.83
0.00
0.00
21.43
21.54
0.00
21.79
21.90
22.40
1520
1522
1555
1578
1643
1655
1657
1670
1670
1731
1732
1769
1783
1824
1835
1835
184.5
1870
1866
1875
1918
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4.-Trimethylbenzene
sec-Butylbenzene
4.-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
22.50 1926
22.82
23.02
23.12
23.24
23.77
0.00
0.00
27.29
1954.
1971
1980
1990
2035
2054
2182
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
14 6
91
146
75
180
Area Cone Units
Not Found UG/L
4607 0.08 UG/L
Not Found UG/L
0 Not Found UG/L
2814 0.02 UG/L
Not Found UG/L
71380 0.24 UG/L
1024.69
1024.69
36508
19579
0.19 UG/L
0. 19 UG/L
0.15 UG/L
0.15 UG/L
Not Found UG/L
45207 0.16 UG/L
21673
53829
Not Found UG/L
Not Found UG/L
0.14 UG/L
0.17 UG/L
0 Not Found UG/L
92630 0.36 UG/L
43200
30250
49345
41567
56752
24019
764 03
48266
0.20 UG/L
0. 11 UG/L
0.19 UG/L
0.14
0.24
0.18
0.60
0.21
UG/L
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
0 Not Found UG/L
14781 0.22 UG/L
Fit
403
908
264
250
707
624
981
989
989
772
903
531
920
4.49
632
94 6
925
946
931
966
951
930
824
94 0
976
978
921
638
291
915
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1. 246
0.000
0.000
0.685
1. 4 38
0.000
1.137
0.960
1. 209
1. 16 9
1. 3 04
1 . OS 1
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID: ~!C
Output File: AE01255.1A2
Data File: AE01255.MS
Name: AE01255
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-D
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:12
Injected at: 03/27/99 00:16
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 7.31 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.59 2363
27.95 2394
28.55 2445
225
128
180
Area
16866
32011
15548
Cone Units
0. 24 UG/L
0.24 UG/L
0. 23 1JG/L
Fit
961
958
902
Rf
0.310
0.586
0. 3 04
Operator ID: MC
Output File: AE01256.1A2
Data File: AE01256.MS
Name: AE01256
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-E
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:22
Injected at: 03/27/99 05:29
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.53 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
221 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T: Scan# Q ion Area Cone Units
14.03 1202
21.14 1811
96 2103899 10.00 UG/L
9.33 UG/L
8.18 UG/L
0.08 UG/L
23.92 2049
4.53
0.00
0.00
6.50
0.00
7.35
0.00
9.59
0.00
0.00
388
438
4 64
557
573
629
737
821
874
943
0.00 1033
0.00 1033"
0.00 1069
0.00 1079
12.97 1111
0.00 1136
0.00 1140
13.62 1166
0.00 1164
14.65 1255
0.00 1291
0.00 13.09
0.00 1327
0.00 1390
16.80 1439
0.00 1464
0.00 1489
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
863603
471730
4584
1552
5130
1932 94
Not Found UG/L
Not Found UG/L
0.10 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
0.73 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
1202
19214
1102
Not Found UG/L
0.01 UG/L
Not Found UG/L
Not Found UG/L
0.10 UG/L
Not Found UG/L
0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
51611 0.21 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
950
874
36
544
736
573.
974
544
967
160
523
289
625
619
785
472
871
989
886
794
196
146
499
484
981
596
854
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.254
0.000
0.000
0.000
0.000
0.000
0.000
0.537
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01256.1A2
Data File: AE01256.MS
Name: AE01256
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-E
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/27/99 19:22
Injected at: 03/27/99 05:29
Dilution Factor: l. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.53 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan~ Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoet~ane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
0.00 1556
0.00 1579
19.24 1648
0.00 1656
19.33 1656
1,3-Dimethylbenzene 1m-Xylene 19.49 1669
1,4-Dimethylbenzene {p-Xylene 19.49 1669
1,2-Dimethylbenzene (a-Xylene 20.23 1733
Styrene 20.24 1734
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1770
20.83 1784
0.00 1825
0.00 1836
21.48 1840
21.54 1845
0.00 1868
21.79 1867
21.94 1879
22.40 1919
22.47 1925
22.81 1954
22.98 1969
23.10 1979
23.24 1991
23.76 2035
23.97 2054
0.00 2175
27.27 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Unit.s
0 Not Found UG/L
4845 0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
8162 0.05 UG/L
0 Not Found UG/L
135114 0.49 UG/L
146365
146365
39117
33462
0.29 UG/L
0.29 UG/L
0.17 UG/L
0.28 IJG/L
0 Not Found UG/L
42893 0.16 UG/L
0 Not Found UG/L
Not Found UG/L
77888 0.54 UG/L
80547 0.27 UG/L
101866
50164
111558
81114
112973
90135
50445
107118
90064
36539
Not Found UG/L
0.43 UG/L
0.25 UG/L
0.44 UG/L
0.33 UG/L
0.41 UG/L
0.41 UG/L
0.42 UG/L
0.91 UG/L
0.43 UG/L
0.33 UG/L
Not Found UG/L
24580 0.39 UG/L
Fit
551
839
366
211
780
679
981
988
986
842
903
582
946
416
471
941
959
946
924
966
908
959
800
971
968
984
94 9
809
703
943
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.685
1.438
0.000
1.137
0.960
l. 209
1.169
l. 305
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01256.1A2
Data File: AE01256.MS
Name: AE01256
QUANT REPORT Page
Quant Time: 03/27/99 19:22
Injected at: 03/27/99 05:29
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 300 Madison Ave, SB12-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.53 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.59 2364
27.93 2393
28.53 2445
225
128
180
Area
294 63
59318
28853
Cone Units
0.45 UG/L
0.48 UG/L
0.45 UG/L
Fit
976
981
938
Rf
0.309
0.586
0.304
Operator ID, MC
Output File, AE01257.1A2
Data File, AE01257.MS
Name, AE01257
QUANT REPORT
Sample, Location' 300 Madison Ave, SB12-F
ID File, B26AEC25.QCI
Page 1
Quant Time, 03/27/99 19,23
Injected at, 03/27/99 06,09
Dilution Factor, 1. oo
Instrument ID, 29j01-1294
,.If
Comment, Sampling, 02/23/1999 by J. Conway, use 6.12 g_/
Last Calibration, 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-·5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 08,34
R.T. Scan# Q ion Area Cone Units
14.05 1203
21.16 1813
23.94 2051
96 2154402 10.00 UG/L
10.43 UG/L
10.89 UG/L
4.55
0.00
5.42
6.41
0.00
389
438
464
549
573
7.37 631
8.60 736
9.61 823
10.18 872
10.98 940
12.06 1033
12.08 1034
12.48 1069
12.57 1077
12.97 1111
13.26 1135
13.30 1139
13.62 1166
13.62 1166
14.69 1258
0.00 1291'
0.00 1309
15.48 1326
16.21 1388
16.82 1441
17.17 1470
0.00 1494
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
987393
643141
18711
1099
12251
22067
3512
149952
10512
4002
4107
535
2983
4509
5721
14731
7670
2654 0
3893
11294
0. 34 UG/L
Not Found UG/L
0. 16 UG/L
0.77 UG/L
Not Found UG/L
0.23 IJG/L
0.08 UG/L
0.55 UG/L
0.13 UG/L
0.05 UG/L
0.04 UG/L
0.03 UG/L
0.03 UG/L
0.05 UG/L
0.05 UG/L
0.23 UG/L
0. 11 UG/L
0.14 UG/L
0.05 UG/L
0.21 UG/L
0 Not Found UG/L
0 Not Found UG/L
2750
4900
61284
113298
0.04 UG/L
0.07 UG/L
0.24 UG/L
1.63 UG/L
Not Found UG/L
Fit
998
999
958
920
891
641
674
989
962
984
964
866
974
760
829
903
949
877
943
992
977
965
319
548
777
925
982
775
885
Rf
1 . 00 0
0. 44 0
0.275
0.258
0.000
0.032
0.074
0.000
0.455
0.208
1. 256
0.386
0.393
0.432
0.083
0. 406
0.434
0.537
0.302
0.316
0.897
0.355
0.255
0.000
0.000
0.327
0.340
1.195
.324
.000
QUANT REPORT Page 2
Opera tor ID: MC
Output File: AE01257.1A2
Data File: AE01257.MS
Name: AE01257
Quant Time: 03/27/99 19:23
Injected at: 03/27/99 06:09
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 300 Madison Ave, SB12-F
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.12 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35 I
36)
37)
38 I
39)
40)
41 I
42)
43)
44)
45)
4 6 I
47)
4 8)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58 I
59)
60)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00 1521
17.80 1525
0.00 1556
18.42
19.23
19.30
Ethylbenzene 19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.24
Bromoform 20.65
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
0.00
21.50
21.55
21.96
21.81
21 . 96
22.42
22.50
22.81
23.01
23.11
23.25
23.77
23.98
0.00
27.30
1578
1647
1654
1657
1673
1673
1733
1734
1769
1785
1825
1836
1842
1846
1881
1868
1881
1921
1927
1954
1971
1980
1992
2036
2055
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
12465 0.22 UG/L
2692
30889
4015
147971
243049
243049
91483
29900
2514
124932
Not Found UG/L
0.06
0.20
0.06
0.52
0.48
0.48
0.39
0.24
0.04
0.47
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
0 Not Found UG/L
74804 0.51 UG/L
150715
126664
224321
126664
129038
177397
189588
186385
123185
1114 6 5
227100
114101
65140
0.49 UG/L
0.53 UG/L
0.92 UG/L
0. 61 UG/L
0.50 UG/L
0.70 UG/L
0.67 UG/L
0.82 UG/L
1.00 UG/L
0.93 UG/L
1.05 UG/L
1.01 UG/L
Not Found UG/L
1.00 UG/L
Fit
498
979
699
732
94 6
751
990
996
994
891
905
890
988
339
513
965
986
919
962
985
932
984
986
971
988
988
993
763
741
987
Rf
0.000
0.266
0.000
0.213
0.717
0.318
1.320
2.360
2.360
1.076
0.576
0.266
1.247
0.000
0.000
0.685
1. 439
1.100
1.138
0. 961
1. 210
1.169
1.305
1.051
0.575
0.560
1.003
0.526
0.000
0.302
Operator ID, .MC
Output File, AE01257.1A2
Data File, AE01257.MS
Name, AE01257
QUANT REPORT
Sample, Location, 300 Madison Ave, SB12-F
ID File, 826AEC25.QCI
Page
Quant Time' 03/27/99 19,23
Injected at, 03/27/99 06,09
Dilution Factor. 1.00
Instrument ID, 20701-1284
Comment, Sampling, 02/23/1999 by J_ Conway, use 6.12 g
Last Calibration, 03/25/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time, 03/25/99 08,34
R.T. Scan# Q ion
27.61
27.95
28.55
2365
2395
2446
225
128
180
Area
61409
65968
58596
Cone
0.93
0.52
0.90
Units
UG/L
UG/L
UG/L
Fit
982
980
972
Rf
0.308
0.586
0.304
Operator ID' MC
Output File, AE01258.1A2
Data File' AE0125B.MS
Name, AE0125B
QUANT REPORT
Sample, Location, 300 Madison Ave, SB12-G
ID File, B26AEC25.QCI
Page
Quant Time, 03/27/99 19,24
Injected at, 03/27/99 06,48
Dilution Factor, 1.00
Instrument ID, 20701-12B4
Comment, Sampling, 02/23/1999 by J. Conway, use 6.04 g J Last Calibration, 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-B
5) 74-87-3
6) 75-01-4
7) 74-B3-9
B) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 7B-B7-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27)
2B)
10061-01-5 Cis-1,3-Dichloropropene
10B-B8-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time, 03/25/99 OB,34
R.T. Scan# Q ion Area Cone Units
14.03 1202
21.14 1Bll
23.92 2050
96 19B2806 10.00 UG/L
B.14 UG/L
B.40 UG/L
4.55
0.00
0.00
3B9
43B
461
6.39 547
6.70 573
7.34 629
B.62 73B
9.60 B22
10.1B B72
10.9B 940
12.05 1031
0.00 1029
0.00 1067
12.56 1076
12.97 1110
13.23 1133
13. 2B 1137
13.62 1166
13.59 1164
14.6B 1257
0.00 1291
0.00 1309
15.45 1324
16.20 13B7
16.BO 1439
0.00 1464
0.00 1496
95
152
B5
47
61
96
49
101
96
49
61
63
61
97
49
B3
97
75
117
7B
62
130
63
93
B3
75
91
75
B3
710976
456731
11B3B 0.23 UG/L
9264
644
11827
254 3
153639
52B6
1366
1992
Not Found UG/L
Not Found UG/L
0.63 UG/L
0.07 UG/L
0.13 UG/L
0.06 UG/L
0.62 UG/L
0.07 UG/L
0.02 UG/L
0. 02 UG/L
0 Not Found UG/L
Not Found UG/L
3213
2567
6B81
3592
15B64
1759
4440
0.04 UG/L
0.02 UG/L
0.12 UG/L
0.06 UG/L
0.09 UG/L
0.03 UG/L
0.09 UG/L
Not Found UG/L
0 Not Found UG/L
14 97
1151
56089
0.02 UG/L
0.02 UG/L
0.24 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
99B
999
954
B95
154
671
673
B51
986
B97
969
B04
BOB
B69
702
753
B5B
825
B13
957
9B9
944
937
230
361
757
913
9B2
61B
753
Rf
1.000
0.441
0. 275
0.25B
0.000
0.000
0.074
0. 04 7
0.455
0.20B
1. 255
0.3B6
0.393
0. 4 32
0.000
0.000
0.434
0.537
0.302
0.316
O.B97
0.355
0.255
0.000
0.000
0.327
0. 34 0
1 . 195
0.000
0.000
Operator ID: MC
Output File: AE01258.1A2
Data File: AE01258.MS
Name: AE01258
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:24
Injected at: 03/27/99 06:48
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 6.04 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90.-7
36) 630-20-6
37) 100-41-4
381 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
0.00 1556
0.00 1579
19.21 1646
0.00 1655
19.33 1656
1,3-Dimethylbenzene 1m-Xylene 19.50 1671
1,4-Dimethylbenzene (p-Xylene 19.50 1671
1,2-Dimethylbenzene (a-Xylene 20.22 1732
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1, 3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.17 1728
0. 00 •1770
20.83 1784
0.00 1825
0.00 1836
21.49 1841
21.54 1845
21.94 1880
21.78 1866
21.94 1880
22.41 1920
22.50 1927
22.79 1952
23.00 1970
23.11 1979
23.25 1991
23.76 2035
24.02 2058
25.47 2182
27.27 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
13579 0.26 UG/L
Not Found UG/L
0 Not Found UG/L
11739 0.08 UG/L
Not Found UG/L
118385 0.45 UG/L
156880
156880
56740
3224
0.34 UG/L
0. 34 UG/L
0.27 UG/L
0.03 UG/L
Not Found UG/L
83624 0.34 UG/L
Not Found UG/L
0 Not Found UG/L
52977 0.39 UG/L
120468
73110
161607
73110
88989
774 86
116995
96805
75819
81452
103854
23062
3113
31699
0.42 UG/L
0.34 UG/L
0. 72 UG/L
0.38 UG/L
0.37 UG/L
0.33 UG/L
0.45 UG/L
0.46 UG/L
0.67 UG/L
0.73 UG/L
0.52 UG/L
0. 22 UG/L
0.22 UG/L
0.53 UG/L
Fit
453
977
664
433
911
825
985
992
994
822
869
686
986
386
486
929
986
968
94 0
991
950
972
967
969
986
979
986
715
589
953
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1. 320
2.360
2.360
1.076
0.576
0.000
1. 246
0.000
0.000
0.685
1. 439
1.100
1.138
0.961
1.209
1.169
1.305
1.051
0.575
0.560
1. 004
0.526
0.072
0.303
Operator ID: MC
Output File: AE01258.1A2
Data File: AE01258.MS
Name: AE01258
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:24
Injected at: 03/27/99 06:48
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 6.04 g
Last Calibration: 03/25/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.61
27.92
28.53
2365
2392
2444
225
128
180
Area
32013
42956
29858
Cone
0.52
0.37
0.50
Units
UG/L
UG/L
UG/L
Fit
982
974
974
Rf
0.309
0.586
0.304
Operator ID: MC
Output File: AE01259.1A2
Data File: AE01259.MS
Name: AE01259
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:27
Injected at: 03/27/99 07:27
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.36 g J Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1200
21.12 1808
23.91 2047
96 2109718 10.00 UG/L
9.16 UG/L
8. 84 UG/L
0.25 UG/L 4.53
0.00
0.00
387
438
4 62
6.43 551
6.68 572
7.33 628
8.58 733
9.59 820
10.15 868
10.95 937
12.03 1029
0.00 1030
12.46 1066
12.56 1074
12.94 1107
13.22 1130
13.27 1135
13.60 1163
13.57 1162
14.65 1254
0.00 1291
15.24 1304
15.45 1323
16.17 1384
16.79 1437
17.12 1465
17.41 1490
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
850528
511426
13412
0 Not Found UG/L
Not Found UG/L
5430
942
15391
3392
229135
13539
2634
6594
4122
6487
6051
16016
6372
30812
4359
11919
0.35 UG/L
0.10 UG/L
0.16 UG/L
0.08 UG/L
0.87 UG/L
0.17 UG/L
0.03 UG/L
0.07 UG/L
Not Found UG/L
0.05 UG/L
0.07 UG/L
0.05 UG/L
0.25 UG/L
0.10 UG/L
0.16 UG/L
0.06 UG/L
0.22 UG/L
0 Not Found UG/L
1781
3814
6773
112354
192340
1601
0.06 UG/L
0.06 UG/L
0.09 UG/L
0.45 UG/L
2.81 UG/L
0.06 UG/L
Fit
998
999
945
908
880
699
772
994
950
967
920
830
977
843
892
893
939
818
941
994
968
969
387
802
747
928
986
858
829
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.047
0.455
0.208
1. 252
0.386
0.393
0.432
0.000
0. 4 06
0.434
0.537
0.302
0.316
0.897
0.355
0.255
0.000
0.147
0.327
0.340
1.195
0.325
0.122
Operator ID: MC
Output File: AE01259.1A2
Data File: AE01259.MS
Name: AE01259
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-H
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/27/99 19:27
Injected at: 03/27/99 07:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.36 g'
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00
17.74
0.00
0.00
19.20
19.31
Ethylbenzene 19.32
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (o-Xylene 20.21
1520
1519
1555
1578
1644
1653
1654
1669
1669
1730
1730 Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.21
20.64 1767
20.80 1781
0.00 1824
0.00 1835
21.47 1838
21.50 1841
21.76 1863
21.78 1865
21.92 1877
22.39 1917
22.47 1924
22.77 1950
22.99 1968
23.07 1976
23.21 1988
23.72 2031
23.95 2051
0.00 2178
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
27278 0.49 UG/L
0. Not Found UG/L
0 Not Found UG/L
40478 0.27 UG/L
4455
141914
281137
281137
11164 7
43132
1282
136097
0.07 UG/L
0.51 UG/L
0.56 UG/L
0. 56 UG/L
0.49 UG/L
0.36 UG/L
0.02 UG/L
0.52 UG/L
0 Not Found UG/L
Not Found UG/L
71974 0.50 UG/L
15 94 04
183115
2 34 841
164448
137793
237339
1 9 3 94 0
187742
106980
159717
199408
101023
0.53 UG/L
0.79 UG/L
0.98 UG/L
0.81 UG/L
0.54 UG/L
0.96 UG/L
0.70 UG/L
0.85 UG/L
0.88 UG/L
1.35 UG/L
0.94 UG/L
0.91 UG/L
Not Found UG/L
71751 1.13 UG/L
Fit
476
983
552
627
9.54
890
989
994
995
939
872
771
991
599
488
992
994
968
967
991
956
989
989
989
984
980
995
767
764
983
Rf
0.000
0.266
0.000
0.000
0. 717
0.318
1.320
2.360
2.360
1.077
0.576
0.266
1.247
0.000
0.000
0.685
1.439
1.101
1.138
0.961
1. 210
1.168
1. 3 OS
1.051
0.575
0.560
1.003
0.526
0.000
0.302
Operator ID: MC
Output File: AE01259.1A2
Data File: AE01259.MS
Name: AE01259
QUANT REPORT
Sample: Location: 300 Madison Ave, SB12-H
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:27
Injected at: 03/27/99 07:27
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.36 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.59 2363
27.91 2390
28.50 2441
225
128
180
Area
61628
62639
60286
Cone Units
0.95 UG/L
0.51 UG/L
0.94 UG/L
Fit
986
989
978
Rf
0.308
0.586
0. 3 04
Operator ID: MC
Output File: AE01262D.1A2
Data File: AE01262D.MS
QUANT REPORT
Quant Time:
Injected at:
Dilution Factor:
Page
03/29/99 19:53
03/25/99 06:02
1. 00
Name: AE01262D Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-A(Dupll
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 2.74 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
R.T. Scan# Q ion
14.08
21.18
23.96
4.57
0.00
0.00
6.45
0.00
7.38
0.00
9.62
0.00
0.00
0.00
0.00
0.00
1205
1814
2052
391
438
467
552
573
632
737
824
874
943
1033
1033
1069
0.00 1079
0.00 1112
o.oo 1136
0.00 1144
13.64 1168
o.oo 1169
14.70 1259
0.00 1291
o.oo 1309
0.00 1327
0.00 1390
16.83 1442
0.00 1464
0.00 1494
96
95
152
as
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2613629
1089744
668978
54 52
10.00 UG/L
9.47 UG/L
9.34 UG/L
0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
14238 0.74 UG/L
Not Found UG/L
8317 0.07 UG/L
0 Not Found UG/L
251332 0.77 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
15720 0.07 UG/L
0 Not Found UG/L
852 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
30036 0.10 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
999
999
951
842
315
631
636
604
979
588
966
395
314
428
444
241
463
531
446
763
972
877
754
398
373
358
4 01
977
688
687
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.253
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
o·. ooo 0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01262D.lA2
Data File: AE01262D.~S
Name: AE01262D
Quant Time: 03/29/99 19:53
Injected at: 03/25/99 06:02
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N McDonough St., SBlJ -A /Dupl.\
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 2.74 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
630-20-6
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
SO) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.82 1526
0.00 1556
0.00 1579
19.26 1649
0.00
19.33
1,3-Dimethylbenzene (m-Xylene 19.53
1656
1656
1673
1,4-Dimethylbenzene (p-Xylene 19.53 1673
1,2-Dimethylbenzene (o-Xylene 0.00 1734
Styrene 20.21 1731
Bromoform 0.00 1770
Isopr·opylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromc.benzene
n-Prc.pylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Sutylbenzene
4-Isc.propyltoluene
1,3-Uichlorobenzene
1,4-Dichlorobenzene
n-But.ylbenzene
1,2-~ichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.85 1786
0.00 1825
0.00 1836
21.53 1844
21.56 1847
0.00 1867
21.80 1868
22.06 1890
22.42 1921
22.51 1929
22.82 1955
23.04 1974
23.10 1979
23.27 1994
23.78 2037
24.00 2056
0.00 2188
27.33 2342
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
2024 0.03 UG/L
0 Not Found UG/L
Not Found UG/L
11643 0.06 UG/L
0 Not Found UG/L
170245
108948
108948
0.49 UG/L
0. 18 UG/L
0.18 UG/L
Not Found UG/L
7671 0.05 UG/L
0 Not Found UG/L
39704 0.12 UG/L
0 Not Found UG/L
0 Not Found UG/L
42123 0.24 UG/L
82727 0.22 UG/L
Not Found UG/L
133541 0.45 UG/L
3286
102543
89089
108940
81263
25859
163348
78414
63533
0.01 UG/L
0. 32 UG/L
0.29 UG/L
0.32 UG/L
0.30 UG/L
0.17 UG/L
1.12 UG/L
0.30 UG/L
0.46 UG/L
0 Not Found UG/L
28331 0.36 UG/L
Fit
26
943
684
658
840
668
985
984
986
529
934
518
976
298
54 7
934
932
918
895
958
928
938
887
933
974
981
961
813
648
947
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
1. 320
2.360
2.360
0.000
0.576
0.000
1. 246
0.000
0.000
0.685
1.438
0.000
1.137
0.960
1. 209
1.169
1.305
1.051
0.575
0.560
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01262D.1A2
Data File: AE01262D.MS
Name: AE01262D
QUANT REPORT Page
Quant Time: 03/29/99 19:53
Injected at: 03/25/99 06:02
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-A(Dupl)
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 2.74 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.64 2368
27.99 2398
28.59 2449
225
128
180
Area
32290
80317
34598
Cone units
0.40 UG/L
0.53 UG/L
0.44 UG/L
Fit
969
982
956
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01263.1A2
Data Pile: AE01263.MS
Name: AE01263
QUANT REPORT Page
Quant Time: 03/29/99 19:55
Injected at: 03/25/99 17:28
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sampl~: Location: 224 N. McDonough St., SB13-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.79 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12)
13)
14)
15)
16)
17)
18)
19)
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
l,l,l~Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomet.hane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene 28)
2 9) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.07 1204
21.18 1813
23.97 2052
4.60
0.00
0.00
6.42
0.00
7.38
8.62
9.64
0.00
11.01
12.06
0.00
12.50
0.00
13.01
0.00
394
438
466
550
572
632
737
824
874
942
1032
1034
1069
1078
1113
1136
0.00 1140
13.64 1167
13.64 1167
14.70 1258
·o.oo 1291
0.00 1309
0.00 1327
16.25 1391
16.83 1441
0.00 1464
0.00 1487
96 3139851
95 1273994
10.00 UG/L
9.22 UG/L
7.99 UG/L
0.02 UG/L
152
85
47
61
96
49
101.
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
687692
1722
0 Not Found UG/L
Not Found UG/L
7908 0.34 UG/L
Not Found UG/L
8916 0.06 UG/L
1264
960013
0.02 UG/L
2.49 UG/L
0 Not Found UG/L
4250 0.03 UG/L
4897 0.04 UG/L
0 Not Found UG/L
2772 0.02 UG/L
0 Not Found UG/L
2965 0.02 UG/L
0 Not Found UG/L
Not Found UG/L
32618 0.12 UG/L
6055 0.05 UG/L
7357 0.09 ~G/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
3960
165774
0.04 UG/L
0.44 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
951
837
316
75
698
352
970
831
957
282
780
790
662
915
695
839
649
925
988
972
933
255
604
635
741
985
650
936
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.208
1.230
0.000
0.393
0.432
0.000
0.406
0.000
0.537
0.000
0.000
0.897
0. 3 55
0.255
0.000
0.000
0.000
0.340
1.195
0.000
0.000
Operator ID' MC
Output File, AE01263.1A2
Data File' AE01263.MS
Name' AE01263
QUANT REPORT Page 2
Quant Time, 03/29/99 19,55
Injected at, 03/25/99 17,28
Dilution Factor, 1.00
Instrument ID, 20701-1284
Sample, Location, 224 N. McDonough St., SB13-B
ID File, 826AEC25.QCI
Comment, Sampling' 02/23/1999 by J. Conway, use 6.79 g
Last Calibration, 03/25/99 Last Qcal Time, 03/25/99 08,34
31) 142-28-9
32) 127-18-4
33) 124-48-1
341 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.81 1524
0.00 1555
0.00 1578
19.25 1648
19.36 1658
19.35 1657
1,3-Dimethylbenzene (m-Xylene 19.54 1673
1,4-Dimethylbenzene (p-Xylene 19.54 1673
1,2-Dimethylbenzene (a-Xylene 20.26 1735
Styrene
Bromoform
Isopropylbenzene
1, 1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.33 1741
20.68 1771
20.86 1786
0.00 1824
0.00 1835
21.53 1844
21.56 1846
21.81 1867
21.83 1869
21.99 1882
22.45 1922
22.52 1928
22.82 1954
23.03 1972
23.14 1981
23.18 1985
23.79 2037
24.03 2058
0.00 2182
27.33 2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
20217
95151
5942
370430
498415
498415
192692
33340
Cone Units
Not Found UG/L
0.24 UG/L
Not Found UG/L
Not Found UG/L
0.42 UG/L
0.06 UG/L
0.89 UG/L
0.67 UG/L
0. 67 UG/L
0.57 UG/L
0.18 UG/L
18440 0.22 UG/L
235906 0.60 UG/L
16 984 9
303031
295808
258150
129003
223847
228099
325880
235919
207386
48366
247938
105145
78620
Not Found UG/L
Not Found UG/L
0.79 UG/L
0. 67 UG/L
0.86 UG/L
0.72 UG/L
0.43 UG/L
0.59 UG/L
0.62 UG/L
0.80 UG/L
0.72 UG/L
1. 15 UG/L
0.28 UG/L
0.79 UG/L
0.64 UG/L
Not Found UG/L
0.83 UG/L
Fit
770
967
605
481
920
858
987
994
996
743
963
819
984
642
610
958
981
966
935
982
955
981
950
965
982
978
982
902
4 01
978
Rf
0.000
0.266
0.000
0.000
0.718
0. 318
1. 321
2.360
2.360
1.077
0.576
0.266
1. 24 7
0.000
0.000
0.686
1.439
1.101
1.138
0. 961
1. 210
1.169
1.305
1.051
0.575
0.559
1.003
0.526
0.000
0.302
Operator ID: MC
Output File: AE01263.1A2
Data File: AE01263.MS
Name: AE01263
QUANT REPORT Page
Quant Time: 03/29/99 19:55
Injected at: 03/25/99 17:28
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.79 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.64 2367
27.98 2396
28.59 2449
225
128
180
Area
82674
220986
74 752
Cone Units
0.86 UG/L
1.21 UG/L
0.79 UG/L
Fit
982
989
970
Rf
0. 3 08
0.584
0.304
Operator ID: MC
Output File: AE01264.1A2
Data File: AE01264.MS
Name: AE01264
QUANT REPORT Page
Quant Time: 03/29/99 19:57
Injected at: 03/25/99 18:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.54 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SGI
3) 1, 2- Dichlorobenzene- d4 ( SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
.20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-8.7-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene 28)
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.09 1207
21.20 1816
24.00 2056
4.58
0.00
0.00
6.46
0.00
7.39
8.64
9.66
392
438
469
553
573
633
739
826
0.00 874
0.00 943
0.00 1033
0.00 1033
12.51 1071
12.61 1080
13.02 1115
13.27 1137
0.00 1140
13.66 1170
13.64 1168
14.73 1261
0.00 1291
0.00 1309
0.00 1327
16.24 1391
16.86 1444
0.00 1464
0.00 1499
96 2640624
95 1200549
152 782667
10.00 UG/L
10.34 UG/L
10.82 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
6988 0.10 UG/L
Not Found UG/L
0 Not Found UG/L
14346 0.74 UG/L
0 Not Found UG/L
9077 0.08 UG/L
1389
959536
0.03 UG/L
2.97 UGiL
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
1934 0.02 UG/L
4781
3324
4921
0.04 UG/L
0.02 UG/L
0.06 UG/L
0 Not Found UG/L
29393 0.13 UG/L
3459 0.04 UG/L
4403 0.07 UG/L
Not Found UG/L
0 Not Found UG/L
1919
Not Found UG/L
0.02 UG/L
114133 0.36 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
94 9
866
585
829
729
426
980
761
951
397
682
630
558
764
728
74 7
701
911
979
949
922
358
218
653
759
982
530
874
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0. 208
1.224
0.000
0.000
0.000
0.000
0. 406
0.434
0.537
0.302
0.000
0.897
0.355
0.255
0.000
0.000
0.000
0. 34 0
1.195
0.000
0.000
QUANT REPORT Page 2
Opera tor ID: MC
Output File: AE01264.1A2
Quant Time: 03/29/99 19:57
Injected at: 03/25/99 18:07
Dilution Factor: 1.00 Data File: AE01264.MS
Name: AE01264 Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-C
ID File: 826AEC25.QCX
Comment: Sampling: 0~/23/1999 by J. Conway, use 6.54 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33 I
34)
35 I
36)
37)
38)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
4 0)
41)
42)
43 I
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
53 I
54)
55)
56 I
57)
58)
59)
60 I
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
~ Compound is ISTD
Compound R.T. Scan# Q ion
1, 3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00
17.81
0.00
0.00
19.26
0.00
Ethylbenzene 19.41
1,3-Dimethylbenzene (m-Xylene 19.56
1521
1526
1556
1579
1650
1659
1662
1676
1,4-Dimethylbenzene (p-Xylene 19.56 1676
1,2-Dimethylbenzene (a-Xylene
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Brcmobenzene
n-Propylbenzene
2-Chlo,rotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.30
0.00
20.88
0.00
0.00
0.00
21.58
0.00
21.85
21.98
22.47
22.52
22.85
23.05
23.15
23.29
23.80
24.04
0.00
27.36
1734
1739
1770
1788
1825
1836
1841
1849
1865
1872
1883
1925
1929
1957
1975
1983
1995
2039
2060
2183
2344
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Cone Units
Not Found UG/L
15759 0.22 UG/L
Not Found UG/L
Not Found UG/L
25507 0.13 UG/L
Not Found UG/L
234249 0.67 UG/L
228963 0.37 UG/L
228963 0.37 UG/L
0 Not Found UG/L
38659 0.25 UG/L
0 Not Found UG/L
138167 0.42 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
176838 0.47 UG/L
0 Not Found UG/L
223098 0.74 UG/L
87345 0.34 UG/L
147273
167177
173312
139131
113350
135657
169983
96702
0.46 UG/L
0.54 UG/L
0.50 UG/L
0.50 UG/L
0.75 UG/L
0.92 UG/L
0. 64 UG/L
0.70 UG/L
0 Not Found UG/L
49343 0.62 UG/L
Fit
4 73
966
256
320
871
700
983
983
984
465
94 7
642
938
463
497
966
971
930
923
972
966
961
94 8
957
985
980
979
811
358
962
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
1.320
2.360
2.360
0.000
0.576
0.000
1. 246
0.000
0.000
0.000
1.439
0.000
1.138
0.961
1. 210
1.169
1.305
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01264.1A2
Data File: AE01264.MS
Name: AE01264
QUANT REPORT Page
Quant Time: 03/29/99 19:57
Injected at: 03/25/99 18:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.54 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.68 2371
28.00 2399
28.59 2450
225
128
180
Area
56914
88774
46589
Cone Units
0.70 UG/L
0.57 UG/L
0.58 UG/L
Fit
976
987
975
Rf
0.309
0.586
0.304
Operator ID: MC
Output File: AE01265.1A2
Data File: AE01265.MS
Name: AE01265
QUANT REPORT Page
Quant Time: 03/29/99 19:58
Injected at: 03/25/99 18:47
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-D
ID File: 826AEC2S.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.14 g
Last Calibration: 03/25/99
Compound
1) '107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-S Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.08
21.20
23.97
4.56
0.00
0.00
6.42
0.00
7.38
0.00
9.64
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.64
0.00
14.72
0.00
0.00
0.00
1206
1816
2054
390
438
466
550
573
632
737
825
874
94 3
1033
1034
1069
1079
1112
1136
114 3
1168
1166
1261
1291
1309
1327
0.00 1390
16.83 1442
0.00 1461
0.00 1497
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1824167
873956
566326
3602
10.00 UG/L
10.90 UG/L
11.33 UG/L
0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
12741 0.95 UG/L
0 Not Found UG/L
4082 0.05 UG/L
0 Not Found UG/L
646316 2.89 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
14771 0.09 UG/L
0 Not Found UG/L
547 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
52920 0.24 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
956
810
154
388
642
212
977
434
991
172
663
464
607
526
54 9
648
325
780
954
879
843
108
336
584
579
984
719
707
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.000
1. 225
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01265.1A2
Data File: AE01265.MS
Name: AE01265
QUANT REPORT Page 2
Quant Time: 03/29/99 19:58
Injected at: 03/25/99 18:47
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-D
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.14 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53)
54)
55)
56)
57)
58)
59)
60)
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.82
0.00
0.00
19.26
0.00
1521
1526
1556
1579
1649
1649
0.00 1660
1,3-Dimethylbenzene (m-Xylene 19.56 1675
1,4-Dimethylbenzene (p-Xylene 19.56 1675
1,2-Dimethylbenzene (a-Xylene 0.00 1734
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.26
0.00
20.83
0.00
0.00
1735
1771
1784
1825
1836
21.50 1842
21.58 . 1849
21.86 1873
21.79 1866
21.98 1883
22.41 1920
22.55 1931
22.82
22.96
23.15
23.14
23.79
24.05
0.00
27.32
1955
1967
1983
1982
2038
2060
2183
2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
7066 0.15 UG/L
Not Found UG/L
Not Found UG/L
12845 0.10 UG/L
Not Found UG/L
Not Found UG/L
174212 0.40 UG/L
174212 0.40 UG/L
0 Not Found UG/L
27035 0.26 UG/L
0 Not Found UG/L
58372 0.26 UG/L
0 Not Found UG/L
0 Not Found UG/L
20277 0.16 UG/L
109615 0.42 UG/L
31913
35764
53556
111375
77148
134217
24633
108981
108394
98500
56051
0.16 UG/L
0.17 UG/L
0. 31 UG/L
0.50 UG/L
0.36 UG/L
0.56 UG/L
0.13 UG/L
1.04 UG/L
1.06 UG/L
0.54 UG/L
0.58 UG/L
0 Not Found UG/L
33922 0.62 UG/L
Fit
514
904
628
253
827
765
981
988
983
619
945
706
934
439
698
879
965
955
913
982
962
931
836
939
981
978
978
797'
489
964
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
0.000
2.360
2.360
0.000
0.576
0.000
1. 246
0.000
0.000
0.685
1.439
1.099
1.137
0. 961
1.210
1.169
1 . 3 05
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01265.1A2
Data File: AE01265.MS
Name: AE01265
QUANT REPORT Page
Quant Time: 03/29/99 19:58
Injected at: 03/25/99 18:47
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-D
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.14 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
611 87-68-3
621 91-20-3
631 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.65 2369
28.00 2399
28.58 2448
225
128
180
Area
35955
65817
16961
Cone Units
0. 64 UG/L
0.62 UG/L
0.31 UG/L
Fit
974
984
965
Rf
0.309
0.585
0. 3 04
QUANT REPORT Page
Operator ID: MC Quant Time:
Injected at: Output File: AE01266.1A2
Data File: AE01266.MS
Name: AE01266
Dilution Factor:
03/29/99 19:59
03/25/99 19:26
1. 00
20701-1284 Instrument ID:
Sample: Location: 224 N. McDonough St., SB13-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.88 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27)
28)
2 9)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.08
21.19
23.97
4.55
0.00
0.00
6.42
0.00
7.38
1204
1814
2053
389
438
466
550
572
632
96
95
152
85
47
61
96
49
101
8.61 736 96
9.62 823 49
0.00 874 61
0.00 942 63
0.00 1033 61
0.00 1033 97
12.50 1069 49
12.61 1079 83
0.00 1112 97
0.00 1136 75
0.00 1141 117
13.65 1168" 78
0.00 1165 62
14.71 1259 130
0.00 1291 63
0.00 1309 93
0.00 1327
0.00 1389
16.84 1441
0.00 1464
0.00 1491
83
75
91
75
83
Area Cone Units
2481523
1348262
830939
4564
10.00 UG/L
12.38 UG/L
12.22 UG/L
0.07 UG/L
Not Found UG/L
0 Not Found UG/L
17687 0.97 UG/L
0 Not Found UG/L
6525 0.06 UG/L
147
848195
0.00 UG/L
2.79 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
1504 0.01 UG/L
2967 0.03 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
16964 0.08 UG/L
0 Not Found UG/L
724 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
68263 0.23 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
1000
950
837
309
762
315
979
702
991
281
898
607
533
782
768
670
435
886
986
884
868
366
165
491
516
979
600
747
Rf
1.000
0.439
0.274
0.258
0.000
0.000
0.074
0.000
0.455
0.208
1.226
0.000
0.000
0.000
0.000
0.406
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01266.1A2
Data File: AE01266.MS
Name: AE01266
Quant Time: 03/29/99 19:59
Injected at: 03/25/99 19:26
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.88 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
630-20-6
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dich1oropropane
Tetrach1oroethene
Dibromochloromethane
1,2-Dibromoethane
Ch1orobenzene
1,1,1,2-Tetrachloroethane
Ethy1benzene
0.00 1520
17.80 1524
0.00 1555
0.00 1578
19.15 1639
0.00
19.36
1,3-Dimethylbenzene (m-Xylene 19.54
1655
1658
1673
1,4-Dimethy1benzene (p-Xy1ene 19.54 1673
1,2-Dimethylbenzene (a-Xylene 0.00 1733
Styrene 20.33 1741
Bromoform 0.00 1769
Isopropy1benzene 0.00 1785
1,1,2,2-Tetrachloroethane 0.00 1824
1,2,3-Trichloropropane 0.00 1835
Bromobenzene 0.00 1843
n-Propylbenzene 21.57 1847
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1864
21.84 1870
22.00 1884
22.40 1918
22.50 1927
22.84 1956
23.02 1971
23.17 1984
23.16 1983
23.77 2036
24.03 2058
0.00 2182
27.33 2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105.
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
9734 0.15 UG/L
0 Not Found UG/L
0 Not Found UG/L
10445 0.06 UG/L
0 Not Found UG/L
179557 0.55 UG/L
164052 0.28 UG/L
164052 0.28 UG/L
0 Not Found UG/L
6298 0.04 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
79399 0.22 UG/L
Not Found UG/L
97365 0.35 UG/L
4 904 0
45449
68655
111425
76594
26093
25510
87622
37874
0.21 UG/L
0.15 UG/L
0.24 UG/L
0.34 UG/L
0.29 UG/L
0 .18 UG/L
0.18 UG/L
0.35 UG/L
0.29 UG/L
0 Not Found.UG/L
31805 0.42 UG/L
Fit
400
959
637
364
838
589
980
982
984
659
925
681
933
392
581
805
944
945
918
936
922
94 3
794
937
972
966
955
801
2 96
936
RE
0.000
0.266
0.000
0.000
0. 717
0.000
1. 320
2.360
2.360
0.000
0.576
0.000
0.000
0.000
0.000
0.000
1.438
0.000
1.137
0. 960
1.209
1.169
1.305
1.051
0.575
0.559
1 . 0 04
0.526
0.000
0.303
Operator ID: MC
Output File: AE01266.1A2
Data File: AE01266.MS
Name: AE01266
QUANT REPORT Page
Quant Time: 03/29/99 19:59
Injected at: 03/25/99 19:26
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 224 N. Mcbonough St., SB13-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.88 g
Last calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
611 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.64 2367
27.98 2396
28.58 2447
225
128
180
Area
29763
60927
36276
Cone Units
0. 3 9 UG/L
0.42 UG/L
0.48 UG/L
Fit
980
979
963
Rf
0. 310
0.586
0.304
Operator ID: MC
Output File: AE01267.1A2
Data File: AE01267.MS
Name: AE01267
QUANT REPORT Page
Quant Time: 03/29/99 20:00
Injected at: 03/25/99 20:07
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-F
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 5.56 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2)
3)
4)
5)
4-Bromofluorobenzene (SG)
1,2-Dichlorobenzene-d4 (SG)
75-71-8
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5•
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1204 96 2500895 10.00 UG/L
21.17
23.96
4.54
0.00
1813
2052
388
438
0.00 466
6.51 557
0.00 575
7.36 630
0.00 737
9.62 824
0.00 874
0.00 948
0.00 1033
0.00 1031
0.00 1069
12.59 1078
0.00 1112
0.00 1136
0.00 1139
13.63 1167
0.00 1166
14.70 1259
o.oo 1291
0.00 1309
0.00 1327
0.00 1390
16.82 1441
0.00 1464
0.00 1494
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
1284541
820717
5245
11.70
11.98
0.08
UG/L
UG/L
UG/L
Not Found UG/L
0 Not Found UG/L
3863 0.21 UG/L
Not Found UG/L
6764 0.06 UG/L
932176
Not Found UG/L
3.05 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2965 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
15863 0.07 UG/L
Not Found UG/L
1289 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
62549 0.21 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
952
831
28
191
695
810
974
271
985
199
819
395
663
539
757
701
610
763
987
891
793
311
648
656
587
978
638
799
Rf
1.000
0.440
0.274
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1.223
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Op<i!rator ID, MC
Output File, AE01267.1A2
Data File, AE01267.MS
Name: AE01267
QUANT REPORT
Quant Time:
Injected at'
Dilution Factor,
Instrument ID:
Sample, Location' 224 N. McDonough St., SB13-F
ID File: 826AEC25.QCJ
Comment: Sampling, 02/23/1999 by J. Conway, use 5.56 g
Page 2
03/29/99 20:00
03/25/99 20,07
1. 00
20701-1284
Last Calibration: 03/25/99 Last Qcal Time' 03/25/99 08:34
Compound R.T. Scan# Q ion
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35)
36)
37)
38)
39)
40)
11)
12)
13)
14)
45)
46)
47)
48)
49)
SO)
s 1)
S2)
53)
S4l
S5)
S6)
S7)
sal
S9 J
60)
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1523
o.oo 1556
0.00 1579
0.00
0.00
19.36
1,3-Dimethylbenzene 1m-Xylene 19.55
1,4-Dimethylbenzene lp-Xylene 19.55
1,2-Dimethylbenzene (a-Xylene 0.00
1651
1656
1659
1674
1674
1734
1731
1770
1785
1825
1836
1840
1847
1868
1870
1881
1917
1928
1953
1970
1980
1993
2037
2058
2177
2340
Styrene
Bromoform
Isopropylb<i>nzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
.Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.22
o.oo 20.83
o.oo 0.00
21.49
21.56
o.oo 21.83
21.95
22.38
22.50
22.80
23.00
23.11
23.26
23.78
24.02
0.00
27.32
• Compound is ISTD
78
166
129
107
112
131
91
91
91
91
104
171
105
83.
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
5568 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found .UG/L
0 Not Found UG/L
177243 0.54 UG/L
113998 0.19 UG/L
113998 0.19 UG/L
0 Not Found UG/L
12660 0.09 UG/L
0 Not Found UG/L
73354 0.24 UG/L
0 Not Found UG/L
0 Not Found UG/L
19386 0.11 UG/L
88884 0.25 UG/L
0 Not Found UG/L
112434 0.40 UG/L
50889 0.21 UG/L
45187
78374
78748
50742
56833
128191
90906
5224 3
0.15 UG/L
0.27 UG/L
0. 24 UG/L
0. 19 UG/L
0.40 UG/L
0.92 UG/L
0.36 UG/L
0.40 UG/L
Not Found UG/L
24510 0.32 UG/L
Fit
245
885
676
352
863
413
976
979
981
643
940
574
956
4 91
399
829
950
919
920
959
919
950
791
936
964
971
953
800
592
911
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1. 320
2.360
2.360
0.000
0.576
0.000
1.246
0.000
0.000
0.685
1.438
0.000
1 .137
0. 960
1. 209
1.169
1 . 3 04
1.051
·a. 575
0.560
1.004
0.526
0.000
0.303
Operator ID' MC
Output File, AE01267.1A2
Data File, AE01267.MS
Name, AE01267
QUANT REPORT Page
·Quant Time' 03/29/99 20,00
Injected at, 03/25/99 20,07
Dilution Factor, 1.00
Instrument ID, 20701-1284
Sample' Location' 224 N. McDonough St., SB13-F
ID File, 826AEC25.QCI
Comment, Sampling, 02/23/1999 by J. Conway, use 5.56 g
Last Calibration, 03/25/99 Last Qcal Time, 03/25/99 08,34
61)
62)
6 3)
87-68-3
91-20-3
82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.62
27.99
28.56
2367
2398
2447
225
128
180
Area
32765
5414 9
29962
Cone Units
0.42 UG/L
0.37 UG/L
0.39 UG/L
Fit
977
978
941
Rf
0.310
0.586
0.304
Operator IDo MC
Output Fileo AE01268.1A2
Data Fileo AE01268.MS
Nameo AE0126B
QUANT REPORT Page
Quant Timeo 03/29/99 20o02
Injected ato 03/25/99 20o46
Dilution Factor, 1.00
Instrument !Do 20701-1284
Sampleo Location, 224 N. McDonough St., SB13-G
ID Fileo 826AEC25.QCI
Commento Sampling, 02/23/1999 by J. Conway, use 6.35 g
Last Calibration, 03/25/99
Compound
1) *107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-8:3-9
B) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27)
28)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 08o34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.18 1813
23.96 2051
4.57 391
5.00 428
0.00 471
6.42 550
0.00 575
7.38 632
0.00 737
9.62 823
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1129
13.63 1166
0.00 1165
14.68 1256
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.83 1441
0.00 1464
0.00 1500
96 2521204
95 1270076
152 733797
10.00 UG/L
11.47 UG/L
10.62 UG/L
85 5339 0.08 UG/L
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
1746 0.06 UG/L
0 Not Found UG/L
16190 0.87 UG/L
0 Not Found UG/L
7375 0.06 UG/L
Not Found UG/L
849035 2.75 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
16981 0.08 UG/L
0 Not Found UG/L
1610 0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
66343 0.22 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
997
999
954
814
745
576
604
908
989
217
936
163
392
372
3 71
448
582
552
463
849
988
881
853
212
389
297
473
977
606
843
Rf
1.000
0.440
0.275
0.258
0.119
0.000
0.074
0.000
0.455
0.000
1.227
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01268.1A2
Data File: AE01268.MS
Name: AE01268
Quant Time: 03/29/99 20:02
Injected at: 03/25/99 20:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-G
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.35 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
3 6)
37)
38)
39)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
40) 95-47-6
41) 100-42-5
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00 1555
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1578
1648
1655
1656
1672
1672
1,2-Dimethylbenzene (a-Xylene 20.23 1732
Styrene 20.26 1735
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.86
0.00
0.00
0.00
21.55
0.00
21.79
21.97
22.44
22.50
22.80
23.02
23.11
23.29
23.79
24.08
0.00
27.33
1769
1786
1824
1835
184 0
1845
1865
1866
1881
1921
1927
1952
1971
1979
1994
2037
2062
2179
2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
9l
146
75
180
Area Cone Units
0 Not Found UG/L
5374 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
168383 0.51 UG/L
176166 0.30 UG/L
176166
76072
14627
0.30 UG/L
0.28 UG/L
0.10 UG/L
0 Not Found UG/L
37909 0.12 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
93814 0.26 UG/L
0 Not Found UG/L
98351 0.34 UG/L
40229
105365
76892
103366
86989
0.17
0.35
0.26
0.31
0.33
UG/L
UG/L
UG/L
UG/L
UG/L
84377 0.58 UG/L
52514 0.37 UG/L
94345 0.37 UG/L
27983 0.21 UG/L
Not Found UG/L
26764 0.35 UG/L
Fit
203
899
576
28
779
485
978
989
989
783
866
672
937
375
471
867
937
952
928
966
940
959
733
943
971
981
962
745
540
925
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.000
1.438
0.000
1 .137
0.960
1.209
1.169
1.304
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01268.1A2
Data File: AE01268.MS
Name: AE01268
QUANT REPORT Page
Quant Time: 03/29/99 20:02
Injected at: 03/25/99 20:46
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 224 N. McDonough St., SB13-G
ID File: 826AEC25.QCI
Comment: Sampling: 02/23/1999 by J. Conway, use 6.35 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61)
62)
63)
87-68-3
91-20-3
82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.65
27.97
28.57
2368
2395
2447
225
128
180
Area
15490
60412
29031
Cone
0.20
0.41
0.38
Units
UG/L
UG/L
UG/L
Fit
967
980
94 9
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01269.1A2
Data File: AE01269.MS
Name: AE01269
QUANT REPORT
Sample: Location: 224 N. McDonough St. SB13-H
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:17
Injected at: 03/30/99 14:03
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.10 g
Last Calibration: 03/29/99
Compound
1) «107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
RoTo Scan# Q ion
14.05
21.16
23o95
4o55
OoOO
OoOO
6 0 40
OoOO
7o37
OoOO
9o62
OoOO
OoOO
OoOO
OoOO
12o50
OoOO
0.00
OoOO
OoOO
13o63
13 0 61
14 0 69
OoOO
OoOO
OoOO
1204
1813
2052
390
438
469
54 9
575
632
737
824
874
943
1033
1033
1071
1079
1112
1136
1129
1168
1166
1259
1291
1309
1327
OoOO 1390
16.83 1442
0.00 1464
OoOO 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83.
Area Cone Units
1894512
780753
4 8194 9
4225
10000
8092
8o53
Oo06
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
0 Not Found UG/L
4531 Oo30 UG/L
0 Not Found UG/L
6554 0.07 UG/L
0 Not Found UG/L
2218992 12.21 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2757 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
13830 0.07 UG/L
1078 0001 UG/L
542 0001 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not. Found UG/L
Not Found UG/L
18041 0007 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
954
858
0
559
676
797
981
618
963
213
319
487
573
771
335
737
642
881
999
896
805
177
91
396
676
981
581
589
Rf
1.000
0. 463
00299
00361
0.000
00000
00081
OoOOO
0.526
0.000
0.960
0.000
00000
0.000
0.000
0.486
00000
00000
0.000
00000
10098
Oo430
Oo291
0.000
0.000
OoOOO
OoOOO
1. 369
OoOOO
0.000
Operator ID: MC
Output File: AE01269.1A2
Data File: AE01269.MS
Name: AE01269
QUANT REPORT
Sample: Location: 224 N. McDonough St. SB13-H
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:17
Injected at: 03/30/99 14:03
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.10 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
3 7)
38)
3 9)
4 0)
41)
42)
4 3)
44)
4 5)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.77
0.00
0.00
0.00
0.00
19.32
·1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 0.00
Styrene
Bromoform
20.25
0.00
0.00
0.00
0.00
0.00
21.59
21.89
21.77
0.00
22.42
22.48
0.00
23.01
23.13
23.26
23.73
0.00
1521
1523
1556
1579
1648
1656
1656
1673
1673
1734
1735
1770
1786
1825
1836
1842
1850
1875
1865
1881
1921
1926
1954
1971
1981
1993
2033
2055
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 2181
27.30 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
5764 0.11 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
76596 0.27 UG/L
54254 0.11 UG/L
54254 0.11 UG/L
0 Not Found UG/L
10403 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
90385
45777
39441
50218
96960
0.29 UG/L
0.20 UG/L
0.15 UG/L
Not Found UG/L
0.19 UG/L
0.40 UG/L
Not Found UG/L
81388 0.35 UG/L
28553
292333
54651
0.24 UG/L
2.20 IJG/L
0.27 UG/L
Not Found UG/L
Not Found UG/L
18199 0.35 UG/L
Fit
278
975
681
218
368
387
973
988
988
652
900
196
894
153
625
715
891
924
944
975
883
956
660
927
974
978
947
625
592
936
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2.649
0.000
0.701
0.000
0.000
0.000
0.000
0.000
1.673
1.234
1.354
0.000
1.386
1. 277
0.000
1.224
0.620
0.702
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01269.1A2
Data File: AE01269.MS
Name: AE01269
QUANT REPORT
Sample: Location: 224 N. McDonough St. SB13-H
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:17
Injected at: 03/30/99 14:03
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/23/1999 by J. Conway, use 5.10 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
-------------~-------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.61 2366 225 19117 0.38
62) 91-20-3 Naphthalene 27.95 2395 128 62877 0.56
63) 82-61-6 1,2,3-Trichlorobenzene 28.54 2446 180 19906 0.36
* Compound is ISTD
Units Fit Rf
--------
UG/L 977 0.269
UG/L 990 0.596
UG/L 912 0.291
Operator ID' MC
Output File, AE01295.1A2
Data File, AE01295.MS
Name, AE01295
QUANT REPORT
Sample, Location' 200 N. Hull SB14-A
ID File' 826AEC28.QCI
Page
Quant Time, 03/30/99 18,18
Injected at, 03/30/99 15,25
Dilution Factor' 1.00
Instrument ID' 20701-1284
Comment, Sampling' 02/24/1999 by J. Conway, use 5.00 g
Last Calibration, 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6)
7)
8)
9)
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time' 03/29/99 09,28
R.T. Scan# Q ion
14.06 1205
21.18 1815
23.95 2053
4.56 391
0.00 438
0.00
6.43
0.00
7.37
0.00
9.62
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.63
0.00
14.69
0.00
0.00
0.00
467
551
573
632
737
824
874
940
1034
1034
1070
1079
1113
1137
1139
1168
1165
1259
1292
1310
1328
0.00 1390
16.83 1442
0.00 1465
0.00 1495
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1841645
857788
563377
4019
10.00 UG/L
10.08 UG/L
10.26 UG/L
0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
3766 0.25 UG/L
Not Found UG/L
5899 0.06 UG/L
0 Not Found UG/L
1796219 10.14 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
13193 0.07 UG/L
0 Not Found UG/L
414 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
17050 0.07 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
999
999
953
891
34 3
623
486
984
309
938
307
724
156
484
370
403
611
455
783
995
890
765
340
109
636
271
983
503
697
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 962
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01295.1A2
Data File: AE01295.MS
Name: AE01295
QUANT REPORT
Sample: Location: 200 N. Hull SB14-A
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:18.
Injected at: 03/30/99 15:25
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.00 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1521
0.00 1525
0.00 1556
0.00 1580
0.00 1649
0.00 1657
19.35
1,3-Dimethylbenzene (m-Xylene 19.48
1,4-Dimethylbenzene (p-Xylene 19.48
1,2-Dimethylbenzene (a-Xylene 20.26
1658
1669
1669
1736
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.26 1736
0.00 1771
20.86 1788
0.00 1825
0.00 1837
21.53 1845
21.53 1845
21.89 1876
21.73 1862
22.04 1889
22.41 1920
22.51 1929
22.80 1954
23.04 1974
23.12 1981
23.27 1994
23.77 2037
0.00 2056
0.00 2184
27.32 2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
14 6
75
180
Area Cone Units
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
19113
21249
21249
23661
3015
52593
6279
29212
47443
4 0455
195
28927
76528
75595
53416
30410
88763
40827
13832
0.07 UG/L
0.04 UG/L
0.04 UG/L
0. 10 UG/L
0.02 UG/L
Not Found UG/L
0.19 UG/L
Not Found UG/L
Not Found UG/L
0.04 UG/L
0.09 UG/L
0.21 UG/L
0.16 UG/L
0.00 UG/L
0.11 UG/L
0. 3 3 UG/L
0.27 UG/L
0.24 UG/L
0.27 UG/L
0.69 UG/L
0.21 UG/L
Not Found UG/L
Not Found UG/L
0.27 UG/L
Fit
684
326
451
426
494
985
992
991
836
893
113
944
217
689
819
903
924
946
94 0
928
968
928
947
975
979
950
600
400
919
Rf
0.000
0.000
0.000
0.000
0.000
0.000
l. 510
2.649
2.649
1.305
0.701
0.000
1.470
0.000
0.000
0.855
l. 673
1.234
1. 354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID, MC
Output File, AE01295.1A2
Data File, AE01295.MS
Name, AE01295
QUANT REPORT
Sample, Location, 200 N. Hull SB14-A
ID File: 826AEC28.QCI
Page
Quant Time, 03/30/99 18,18
Injected· at, 03/30/99 15:25
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.00 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- ---- ----61) 87-68-3 Hexachlorobutadiene 27.63 2368 225 15038 0.30
62) 91-20-3 Naphthalene 27.97 2397 128 66532 0.61
63) 82-61-6 1,2,3-Trichlorobenzene 28.56 2448 180 15163 0.28
• Compound is ISTD
Units Fit Rf
--------UG/L 977 0.269
UG/L 987 0.596
UG/L 913 0.291
Operator ID: MC
Output File: AE01296.1A2
Data File: AE01296.MS
Name: AE01296
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:11
Injected at: 03/30/99 18:39
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 1.52 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
ll) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 56)-58-6
20) 56-23-5
21) 71-43-2
101-06-2
79-01-6
78-87-5
74-95-3
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
1<1.06
21.15
23.95
4.55
0.00
5.44
6.42
0.00
7.37
8.60
9.61
10.17
0.00
12.04
0.00
12.50
0.00
12.97
13.24
0.00
13.63
1204
1812
2052
390
438
466
549
567
631
736
823
871
947
1032
1036
1070
1079
1111
1134
1139
1167
13.59 1164
14.69 1258
0.00 1291
0.00 1310
15.50 1328
16.21 1388
16.82 1441
11.15 1469
0.00 1495
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1828087
836275
501426
8766
Cone Units
10.00 UG/L
9.90 UG/L
9.19 UG/L
0.13 UG/L
Not Found UG/L
1285 0.03 UG/L
5562 0.38 UG/L
0 Not Found UG/L
10899 0.11 UG/L
1380 0.03 UG/L
538584
3104
3.03 UG/L
0.04 UG/L
0 Not Found UG/L
2892 0.03 UG/L
Not Found UG/L
1192 0.01 UG/L
0 Not Found UG/L
2089 0.02 UG/L
4178 0.06 UG/L
Not Found UG/L
18209 0.09 UG/L
2478 0.03 UG/L
3315 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
1229 0.02 UG/L
1253
26223
6298
0.02 UG/L
0.10 UG/L
0.09 UG/L
Not Found UG/L
Fit
998
999
951
890
69
614
715
909
988
899
991
853
770
881
651
739
533
829
755
883
991
965
932
327
851
749
813
975
779
884
Rf
1.000
0.463
0.299
0.361
0.000
0. 226
0.081
0.000
0.526
0.225
0.972
0. 4 52
0.000
0.511
0.000
0.486
0.000
0.662
0. 402
0.000
1. 098
0.430
0.291
0.000
0.000
0. 4 03
0.453
1.369
0.396
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01296.1A2
Data File: AE01296.MS
Name: AE01296
Quant Time: 03/31/99 08:11
Injected at: 03/30/99 18:39
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Hull, SB14-B
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 1.52 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46/
47)
48)
49)
50)
51)
52)
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00 1521
17.79 1524
18.18 1557
18.44 1580
19.23 1647
19.33
Ethylbenzene 19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.24
Styrene 20.23
1656
1657
1673
1673
1734
1733
1770
1785
1825
1836
1843
1846
1867
1869
1881
1921
1927
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1.3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.84
0.00
0.00
21.51
21.55
21.79
21.81
21.95
22.42
22.50
22.81 1954
23.01 1972
23.12 1981
23.12 1981
23.78 2037
0.00 2055
0.00 2183
27.31 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
10684 0.21 UG/L
2570
578
8758
1581
55698
9074 3
90743
34651
16532
69807
0.05 UG/L
0.01 UG/L
0.06 UG/L
0.03 UG/L
0.20 UG/L
0. 19 UG/L
0.19 UG/L
0.15 UG/L
0.13 UG/L
Not Found UG/L
0. 26 UG/L
0 Not Found UG/L
0 Not Found UG/L
28477 0.18 UG/L
100023 0.33 UG/L
81514
158326
5064 7
83181
12 04 6 3
0.36 UG/L
0.64 UG/L
0.25 UG/L
0.33 UG/L
0.52 UG/L
99942 0.36 UG/L
108924 0.49 UG/L
62879 0.56 UG/L
62687 0.49 UG/L
118813 0.61 UG/L
Not Found UG/L
Not Found UG/L
36786 0.73 UG/L
Fit
428
978
776
777
955
810
987
994
992
792
952
613
980
311
554
938
987
961
964
991
941
982
979
973
985
981
992
661
326
974
Rf
0.000
0. 284
0.282
.259
0.858
0. 311
1.510
2.649
2. 64 9
1.305
0.702
0.000
1. 4 70
0.000
0.000
0.855
1.673
1.234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.704
1.074
0.000
0.000
0.276
Operator ID, MC
Output File, AE01296.1A2
Data File' AE01296.MS
Name' AE01296
QUANT REPORT
Sample' Location, 200 N. Hull, SB14-B
ID File' 826AEC28.QCI
Page
Quant Time, 03/31/99 08,11
Injected at' 03/30/99 18,39
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment' Sampling, 02/24/1999 by J. Conway, use 1.52 g
Last Calibration, 03/29/99
61)
62)
6 3)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time, 03/29/99 09,28
R.T. Scan# Q ion
27.62
27.96
28.59
2366
2396
2449
225
128
180
Area
36906
51625
30964
Cone
0.75
0.47
0.58
Units
UG/L
UG/L
UG/L
Fit
982
984
971
Rf
0.269
0.596
0.291
Operator ID, MC
Output File, AE01297.1A2
Data File, AE01297.MS
Name, AE01297
QUANT REPORT
Sample, Location' 200 N. Hull, SB14-C
ID File' 826AEC28.QCI
Page
Quant Time, 03/29/99 16,50
Injected at, 03/28/99 06,00
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment' Sampling, 02/24/1999 by J. ·Conway, use 7. 77 g
Last Calibration' 03/29/99
Compound
1) +107-06-2 Fluorobenzene
2)
3)
4)
5)
4-Bromofluorobenzene (SG)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochlorornethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
' Compound is ISTD
Last Qcal Time, 03/29/9~ 09,28
R.T. Scan# Q ion
14.06
21.16
23.95
4. 54
0.00
0.00
6.42
6.72
7.36
0.00
9.61
0.00
0.00
0.00
0.00
1203
1812
2051
389
438
466
54 9
576
630
736
822
874
941
1033
1032
0.00 1069
12.56 1075
0.00 1112
0.00 1136
0.00
13.63
13.60
14.68
0.00
0.00
0.00
0.00
16.82
0.00
0.00
1139
1166
1164
1256
1291
1309
1325
1389
1440
1456
1494
96
95
152
85
'47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2169846
888996
587352
4631
10.00
8.86
9.07
0.06
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
Not Found UG/L
27986 1.60 UG/L
307 0.02 UG/L
7176 0.06 UG/L
Not Found UG/L
170896 0.81 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
3656 0.03 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
16683 0.07 UG/L
1882 0.02 UG/L
1368 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
69392 0.23 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
997
999
94 9
840
125
223
675
819
989
707
993
691
898
541
684
671
885
627
637
947
989
923
730
314
89
837
485
977
761
877
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.975
0.000
0.000
0.000
0.000
0.000
0.524
0.000
0.000
0.000
1.098
0.430
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01297.1A2
Data File: AE01297.MS
Name: AE01297
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-C
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/29/99 16:50
Injected at: 03/28/99 06:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 7.77 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
3 9)
4 0)
41)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.77 1521
0.00
0.00
19.24
0.00
19.39
1,3-Dimethylbenzene (m-Xylene 19.56
1,4-Dimethylbenzene (p-Xylene 19.56
1,2-Dimethylbenzene (o-Xylene 0.00
1548
1578
1647
1653
1660
1674
1674
1733
1735 Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.27
20.65 1768
20.85 1785
0.00 1824
0.00 1835
21.47 1838
0. 00 1847
0.00 1873
21.79 1866
21.94
22.44
22.50
22.78
23.01
23.14
23.26
23.77
24.06
25.50
27.32
1878
1921
1927
1951
1971
1981
1992
2036
2060
2184
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
3834 0.06 UG/L
Not Found UG/L
Not Found UG/L
10452 0.06 UG/L
Not Found UG/L
26655 0.08 UG/L
145152 0.25 UG/L
145152 0.25 UG/L
0 Not Found UG/L
75808 0.50 UG/L
4771 0.07 UG/L
70968 0.22 UG/L ·
Not Found UG/L
Not Found UG/L
70937 0.38 UG/L
Not Found UG/L
Not Found UG/L
234340 0.80 UG/L
87905
163386
145187
179101
139600
107279
318534
110961
24435
11456
39002
0.36 UG/L
0. 54 UG/L
0.52 UG/L
0.54 UG/L
0.53 UG/L
0.80 UG/L
2.09 UG/L
0.48 UG/L
0.19 UG/L
0.64 UG/L
0.65 UG/L
Fit
87
925
94 0
602
772
750
984
981
986
568
948
788
94 9
467
397
916
966
973
900
984
943
924
980
939
980
978
982
801
748
973
Rf
0.000
0.284
0.000
0.000
0.858
0.000
. 1. 510
2.649
2. 64 9
0.000
0.702
0.320
1. 4 70
0.000
0.000
0.855
0.000
0.000
1.354
1.120
1.386
1.277
1. 530
1.224
0.620
0.702
1.074
0.579
0.083
0. 276
Operator ID: MC
Output File: AE01297.1A2
Data File: AE01297.MS
Name: AE01297
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:50
Injected at: 03/28/99 06:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 7.77 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound
----------------------------------------'
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.62 2366
27.95. 2394
28.53 2444
225
128
180
Area
43974
88268
41538
Cone Units
0.76 UG/L
0. 6 8 UG/L
0.66 UG/L
Fi(.
973
986
983
Rf
0.269
0.596
0. 291
Operator ID: MC
Output File: AE01298.1A2
Data File: AE01298.MS
Name: A.E01298
QUANT RE?ORT
Sample: Location: 200 N. Hull, SB14-D
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page
03/29/99 16:49
03/28/99 06:39
l. 00
20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.07 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2 -Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13)
14)
15)
75-34-3
156-59-4
590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
3 0)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.03 1201
21.14 1810
23.92 2048
4.54
0.00
0.00
6.42
0.00
7.36
8.60
9.60
10.16
10.96
12.05
0.00
389
438
469
549
570
630
735
821
869
937
1030
1030
0.00 1068
12.56 1074
12.94 1107
13.23 1132
13.26 1135
13.60
13.59
14.67
0.00
0.00
0.00
0.00
16.80
0.00
0.00
1164
1163
1255
1291
1309
1327
1387
1438
1463
14 88
96 2621848
95 984163
152 627083
10.00 UG/L
8.12 UG/L
8. 02 UG/L
0.09 UG/L 85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
8870
Not Found UG/L
0 Not Found UG/L
5736 0.27 UG/L
14867
194 3
126203
Not Found UG/L
0.11 UG/L
0.03 UG/L
0.49 UG/L
6301 0.05 UG/L
2081 0.02 UG/L
3264 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
3422 0.02 UG/L
3619 0.02 UG/L
6573 0.06 UG/L
2970 0.03 UG/L
194 37
2556
4664
0.07 UG/L
0.02 UG/L
0.06 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
53909 0.15 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
950
893
418
538
684
895
980
906
937
971
864
883
927
701
780
767
820
917
994
939
94 3
126
647
626
840
970
580
892
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0. 081
0.000
0.526
0.225
0.975
0.452
0.485
0. 511
0.000
0.000
0.524
0.662
0.402
0.380
1.098
0.430
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01298.1A2
Data File: AE01298.MS
Name: AE01298
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-D
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/29/99 16:49
Injected at: 03/28/99 06:39
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.07 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.76 1520
0.00 1555
0.00 1578
19.21 1645
0.00 1655
19.32 1654
1,3-Dimethylbenzene (m-Xylene 19.50 1670
1,4-Dimethylbenzene (p-Xylene 19.50 1670
1,2-Dimethylbenzene (o-Xylene 20.21 1730
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1733
0.00 1769
20.83 1783
0.00 1824
0.00 1835
21.50 1841
21.53 1844
0.00 1867
21.78 1865
21.94 1879
22.48 1925
22.47 1924
22.78 1950
22.99 1968
23.23 1989
23.23 1989
0.00 2036
24.00 2055
0.00 2182
27.30 2338
~ .... --. ........ - ·-
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
0 Not Found UG/L
252665 3.39 UG/L
0 Not Found UG/L
Not Found UG/L
32556
417833
810877
810877
196092
66710
0.14 UG/L
Not Found UG/L
1.06 UG/L
1.17 UG/L
1.17 UG/L
0.57 UG/L
0.36 UG/L
0 Not Found UG/L
228274 0.59 UG/L
Not Found UG/L
0 Not Found UG/L
61430
285905
0.27 UG/L
0.65 UG/L
0 Not Found UG/L
105 1779977 5.02 UG/L
0.10 UG/L
1.05 UG/L
91 30473
119 382110
105 2151907
105 241299
119 384041
146 433057
146 433057
6.43 UG/L
0.60 UG/L
1.20 UG/L
2.67 UG/L
2.35 UG/L
91
146
75
180
0 Not Found UG/L
42012 0.28 UG/L
0 Not Found UG/L
2234 9 0.31 UG/L
Fit
663
985
257
652
840
306
993
998
997
927
873
19
956
668
162
806
988
476
973
802
782
995
965
839
961
960
688
769
815
Rf
0.000
0. 284
0.000
0.000
0.858
0.000
1.510
2. 64 9
2.649
1.305
0.702
0.000
1.470
0.000
0.000
0.855
1. 6 73
0.000
1.352
1 . 12 0
1.386
1.277
1.530
1.223
0.620
0.702
0.000
0.579
0.000
0.276
Operator ID: MC
Output File: AE01298.1A2
Data File: AE01298.MS
Name: AED1298
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:49
Injected at: 03/28/99 06:39
Dilution Factor: 1.00.
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.07 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------~------------------ ------ -------- --------61) 87-68-3 Hexachlorobutadiene 27.59 2363 225 51462 0.73
62) 91-20-3 Naphthalene 27.93 2392 128 226884 1. 45
63) 82-61-6 1,2,3-Trichlorobenzene 28.53 2444 180 46012 0.60
• Compound is ISTD
Units Fit Rf
--------
UG/L 979 0.269
UG/L 989 0 0 596
UG/L 948 0.291
Operator ID: MC
Output File: AE01299.1A2
Data File: AE01299.MS
Name: AE01299
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:51
Injected at.: 03/28/99 07:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.37 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene ISGl
3)
4)
5)
1,2-Dichlorobenzene-d4 (SG)
75-71-8
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, "Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. ScanU Q ion Area Cone Units
14.04 1201
21.14 1810
23.93 2049
4.54 388
0.00 438
0.00
6.40
0.00
7.36
0.00
9.60
0.00
466
548
572
630
737
821
874
0.00 939
0.00 1033
0.00 1031
0.00 1069
12.56 1075
0.00 1112
0.00 1136
0.00 1138
13.62 1165
0.00 1164
14.67 1255
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.81 1438
0.00 1464
0.00 1489
96 2256558
95 759007
10.00 UG/L
7.28 UG/L
7.20 UG/L
0.06 UG/L
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
4 84 580
4782
0 Not Found UG/L
Not Found UG/L
18754 1.03 UG/L
Not Found UG/L
7711 0.06 UG/L
Not Found UG/L
301413 1.37 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not. Found UG/L
3742 0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
15211 0.06 UG/L
0 Not Found UG/L
1670 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not. Found UG/L
0 Not Found UG/L
47327 0.15 UG/L
0 Not. Found UG/L
0 Not Found UG/L
Fit
998
999
956
810
209
343
699
625
981
201
962
161
786
375
615
517
838
687
644
688
993
915
784
34 9
54 5
511
408
981
624
743
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.974
0.000
0.000
0.000
0.000
0.000
0.524
0.000
0.000
0.000
1 . 09 8
0.000
0.291
0.000
0.000
0.000
0.000
1. 369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01299.1A2
Data File: AE01299.MS
Name: AE01299
Quant Time: 03/29/99 16:51
Injected at: 03/28/99 07:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sampl~: Location: 200 N. Hull, 5814-E
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 5.37 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
630-20-6
100-41-4
108-38-3
39) 106-42-3
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.77 1521
18.17 1555
0.00 1578
19.23 1646
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.51
1655
1657
1670
1,4-Dimethylbenzene (p-Xylene 19.51 1670
1,2-Dimethylbenzene (o-Xylene 0.00
Styrene 20.24
Bromoform 20.67
Isopropylbenzene 20.82
1,1,2,2-Tetrachloroethane 0.00
1,2,3-Trichloropropane 0.00
Bromobenzene 21.42
n-Propylbenzene 21.53
2-Chlorotoluene 0.00
1,3,5-Trimethylbenzene 21.79
21.94
22.40
22.48
22.79
22.99
23.09
23.24
1733
1733
1769
1782
1824
1835
1834
1844
1865
1866
1878
1918
1925
1951
1968
1977
1990
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
23.74 2033
23.97 2053
0.00 2182
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
6173 0.10 UG/L
5491 0.09 UG/L
Not Found UG/L
24333 0.13 UG/L
0 Not Found UG/L
154889 0.45 UG/L
153901
153901
0.26 UG/L
0.26 UG/L
Not Found UG/L
22361 0.14 UG/L
2836 0.04 UG/L
100493 0.30 UG/L
Not Found UG/L
Not Found UG/L
34156 0.18 UG/L
105461 0.28 UG/L
Not Found UG/L
243627 0.80 UG/L
78042
138781
155717
146471
13 2 94 6
58268
184 772
0.31 UG/L
0.44 UG/L
0. 54 UG/L
0.42 UG/L
0.48 UG/L
0.42 UG/L
1.17 UG/L
122777 0.51 UG/L
60477 0.46 UG/L
Not Found UG/L
32750 0.53 UG/L
Fit
512
806
769
694
863
717
986
986
987
661
904
790
937
236
179
926
945
94 5
926
989
915
952
912
946
982
982
976
84 0
667
946
Rf
0.000
0.284
0.282
0.000
0.858
0.000
1.510
2.649
2.649
0.000
0.702
0.320
1. 4 70
0.000
0.000
0.855
1.673
0.000
1.354
1 . 12 0
1.386
1.277
1. 530
1.224
0.620
0.703
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01299.1A2
Data File: AE01299.MS
Name: AE01299
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:51
Injected at: 03/28/99 07:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.37 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.61 2364 225 39218 0.65
62) 91-20-3 Naphthalene 27.93 2392 128 76767 0.57
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2445 180 34783 0.53
• Compound is ISTD
Units Fit Rf
--------
UG/L 976 0.269
UG/L 986 0.596
UG/L 971 0.291
Operator ID: MC
Output File: AE01300.1A2
Data File: AE01300.MS
Name: AE01300
QUANT REPORT
Sample: Location: 200 N. Hull, S814-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:58
Injected at: 03/28/99 07:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.18 g
Last Calibration: 03/29/99
Compound
1) '107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-97-5
25) 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomer.hane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27)
29)
2 9)
3 0)
10061-01-5 Cis-1,3-Dichloropropene
109-98-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.03 1202
21.14 1911
23.94 2051
96 2294319 10.00 UG/L
7.86 UG/L
7.96 UG/L
0.06 UG/L 4. 54 399
0.00 438
0.00 466
6.42 549
0.00 567
7.36 630
0.00 737
9.60 822
0.00 974
0.00 943
0.00 1033
0.00 1033
0.00 1069
12.56 1076
0.00 1112
0.00 1136
0.00 1137
13.62 1166
13.62 1166
14.67 1256
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.92 1440
0.00 1464
0. 00 1492
95
152
95
47
62
96
49
101
96
49
61
63
61
97
49
93
97
75
117
78
62
130
63
93
93
75
91
75
93
834123
544822
4905
Not Found UG/L
0 Not Found UG/L
6459 0.35 UG/L
0 Not Found UG/L
7102 0.06 UG/L
0 Not Found UG/L
139372 0.62 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2731 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
13748 0.05 UG/L
1203
1747
0.01 UG/L
0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
76946 0.25 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
954
862
153
223
716
727
993
165
987
245
459
447
459
539
722
699
482
739
982
932
890
297
411
659
417
983
605
947
Rf
1.000
0.463
0. 2 99
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.975
0.000
0.000
0.000
0.000
0.000
0.524
0.000
0.000
0.000
1.099
0.430
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01300.1A2
Data File: AE01300.MS
Name: AE01300
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-F
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/29/99 16:58
Injected at: 03/28/99 07:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.18 g
Last Calibration: 03/29/99 Last Qca1 Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
4 5)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
0.00
0.00
0.00
0.00
0.00
19.33
1,3-Dimethylbenzene 1m-Xylene 19.61
1,4-Dimethylbenzene (p-Xylene 19.51
1,2-Dimethylbenzene (a-Xylene 0.00
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.27
0.00
20.73
0.00
0.00
21.46
21.54
0.00
21.74
21.94
22.34
22.50
22.78
23.00
23.14
23.24
23.74
24.00
0.00
27.28
1521
1522
1556
1579
1651
1656
1656
1680
1672
1734
1736
1770
1776
1825
1836
1838
1846
1874
1863
1880
1914
1927
1952
1971
1982
1991
2034
2056
2183
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
125407 0.36 UG/L
35881
154803
0.06 UG/L
0.25 UG/L
Not Found UG/L
15453 0.10 UG/L
0 Not Found UG/L
41804 0.12 UG/L
0 Not Found UG/L
0 Not Found UG/L
76221 0.39 UG/L
111659 0.29 UG/L
0 Not Found UG/L
93862 0.30 UG/L
49076
35519
124008
140341
96285
88536
284560
116678
35674
29952
0.19 UG/L
0.11 UG/L
0.42 UG/L
0.40 UG/L
0.34 UG/L
0.62 UG/L
1.77 UG/L
0.47 UG/L
0. 27 UG/L
Not Found UG/L
0.47 UG/L
Fit
432
889
526
2 91
787
658
975
985
985
689
885
615
950
262
188
931
944
978
933
972
935
934
894
955
974
976
963
770
312
933
Rf
0.000
0.000
0.000
0.000
0.000
0.000
1.510
2. 64 9
2. 64 9
0.000
0.701
0.000
1. 4 70
0.000
0.000
0.855
1.673
0.000
l. 354
1.120
l. 3 86
l. 277
l. 530
1.224
0.620
0.702
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01300.1A2
Data File: AE01300.MS
Name: AE01300
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 16:58
Injected at: 03/28/99 07:57
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.18 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2, 3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2364
27.93 2393
28.55 2446
225
128
180
Area
38609
74 013
32036
Cone Units
0.63 UG/L
0.54 UG/L
0.48 UG/L
Fit
974
995
977
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01301.1A2
Data File: AE01301.MS
Name: AE01301
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:00
Injected at: 03/28/99 08:36
Dilution Factor: 1. 00
Instrument ID: 2b701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.82 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29)
30)
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.05 1202
21.15 1811
23.93 2049
4.54
0.00
388
438
5.43 465
6.40 548
6.72 575
7.37 631
8.59 734
9.60 821
10.18 871
10.98 939
12.03 1029
0.00 1032
12.48 1068
12.56 1075
12.97 1110
13.24 1133
13.27 1136
13.62 1165
13.59 1163
14.67 1255
15.05 1288
15.26 1306
15.47 1324
16.21 1387
16.80 1438
17.15 1468
17.42 1491
96 2201449
95 912004
152 583238
10.00 UG/L
8.96 UG/L
8.88 UG/L
85
47
62
96
49
14455 0.18 UG/L
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
3258
13903
705
21082
4463
104878
17691
4417
104 97
Not Found UG/L
0.07 UG/L
0.78 UG/L
0.05 UG/L
0.18 UG/L
0.09 UG/L
0.49 UG/L
0. 18 UG/L
0.04 UG/L
0.09 UG/L
0 Not Found UG/L
5659
8136
8622
17646
6669
38653
9215
16571
3505
3298
4597
9180
97744
91644
3808
0.05 UG/L
0.07 UG/L
0.06 UG/L
0.20 UG/L
0.08 UG/L
0. 16 UG/L
0.10 UG/L
0. 2 6 UG/L
0.08 UG/L
0.08 UG/L
0.05 UG/L
0.09 UG/L
0.32 UG/L
1.05 UG/L
0.12 UG/L
Fit
997
999
956
915
271
778
727
778
989
970
942
980
862
955
84 7
853
918
958
868
967
995
989
971
444
978
864
924
984
870
920
Rf
1.000
0.463
0.299
0.361
0.000
0.226
0.081
0.060
0.526
0.225
0.975
0. 4 52
0.485
0.511
0.000
0. 4 86
0.524
0.662
0.402
0.380
1. 098
0.430
0.291
0.189
0.182
0.403
0. 453
1. 369
0. 3 96
0.145
Operator ID: MC
Output File: AE01301.1A2
Data File: AE0130l.MS
Name: AE01301
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:00
Injected at: 03/28/99 08:36
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.82 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
3 3)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
17.73
17.77
18.16
18.41
19.21
19.32
19.33
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (o-Xylene 20.23
Styrene 20.32
Bromoform
78
166
129
107
112
131
91
91
91
91
104
171
105
Area
4132
33469
2448
5215
67200
9035
220042
360032
360032
159722
6713
5092
170:i22
Cone
0.18
0.54
0.04
0.09
0.36
0.13
0.66
0.62
0.62
0.56
0.04
0.07
0.53
Units
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
44) 79-34-5
45) 96-18-4
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.64
20.83
0.00
0.00
21.49
1518
1521
1555
1576
1645
1654
1655
1670
1670
1732
1740
1767
1783
1824
1835
184 0
1844
1865
1866
1878
1918
1925
1951
1969
1978
1990
2034
2052
2179
2337
83
75
77
91
91
0 Not Found UG/L
0 Not Found UG/L
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
21.53
21.79
21.79
21.94
22.40
22.48
22.79
23.00
23.10
23.24
23.76
23.97
25.44
27.29
105
91
119
105
105
119
146
146
91
146
75
180
138363 0.74 UG/L
198027 0.54 UG/L
287855
321235
229764
192550
204602
253278
239686
174 712
349610
276443
161940
954 9
100216
1. 06
1. 08
0.93
0.63
0.73
0.75
0.89
1. 28
2.26
1.17
1.27
0.52
1. 65
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
711
983
867
839
962
876
993
994
997
930
905
838
993
564
596
984
990
950
952
992
955
987
982
978
986
970
995
837
646
985
Rf
0.104
0.284
0.282
0.259
0.858
0.311
1.510
2.649
2. 64 9
1.305
0.701
0.320
1.470
0.000
0.000
0.855
1.673
1.234
1.354
1 .119
1.386
1. 2-77
1. 530
1.223
0.620
0.702
1. 074
0.579
0.083
0.276
Operator ID: MC
Output File: AEOl30l.lA2
Data File: AE01301.MS
Name: AE0130l
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:00
Injected at: 03/28/99 08:36
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.82 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.60 2364 225 93975 1. 59
62) 91-20-3 Naphthalene 27.93 2392 128 8604 3 0.66
63) 82-61-6 1,2,3-Trichlorobenzene 28.53 2443 180 87700 1. 38
• Compound is ISTD
Units Fit Rf
--------
UG/L 988 0.268
UG/L 988 0.596
UG/L 985 0.290
Operator ID: MC
Output File: AE01302.1A2
Data File: AE01302.MS
Name: AE01302
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-H
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:01
Injected at: 03/28/99 09:15
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 7.42 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
12)
13)
14)
15)
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.04 1202
21.15 1811
23.93 2049
4.53 387
0.00 438
5.43 465
6.40 548
0.00 574
7.33 628
8.59 734
9.60 821
10.17
0.00
12.04
0.00
12.47
12.57
12.96
0.00
13.26
13.62
13.60
14.66
0.00
0.00
15.4 7
0.00
16.81
0.00
0.00
870
939
1030
1033
1067
1075
1109
1139
1135
1165
1164
1255
1291
1309
1324
1389
1438
1464
1491
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75 ..
83
Area Cone Units
2025708
774 79B
51B935
9717
10.00 UG/L
8.27 UG/L
B.59 UG/L
0.13 UG/L
0 Not Found UG/L
1172 0.03 UG/L
12B77 0.79 UG/L
0 Not Found UG/L
123B6 0.12 UG/L
1112 0.02 UG/L
22B130 1.16 UG/L
3512 0.04 UG/L
Not Found UG/L
1563 0.02 UG/L
0 Not Found UG/L
2BB5 0.03 UG/L
3355 0.03 UG/L
2026 0.02 UG/L
0 Not Found UG/L
2646 0.03 UG/L
1596B
2974
3 54 3
0.07 UG/L
0.03 UG/L
0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
1B32 0.02 UG/L
0 Not Found UG/L
6B195 0.25 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
956
904
0
694
69B
B53
9B5
791
9B9
793
74 8
B30
537
B08
BOB
B25
B14
942
9B6
965
936
157
679
724
651
9B1
564
864
Rf
1.000
0.463
0.299
0.361
0.000
0.226
0.081
0.000
0.526
0.225
0.974
0.452
0.000
0.511
0.000
0.486
0.524
0.662
0.000
0.380
1. 09B
0.430
0.291
0.000
0.000
0.403
0.000
l. 369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01302.1A2
Data File: AE01302.MS
Name: AE01302
Quant Time: 03/29/99 17:01
Injected at: 03/28/99 09:15
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 N. Hull, SB14-H
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 7.42 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
3 7)
38)
3 9)
4 0)
41)
42)
4 3)
44)
45)
4 6)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.77
0.00
18.42
19.23
0.00
19.32
1,3-Dimethylbenzene 1m-Xylene 19.50
1,4-Dimethylbenzene lp-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.21
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
0.00
21.4 9
21.53
21.79
21.79
21.94
22.41
22.49
22.78
23.00
23.10
23.23
23.74
24.02
0.00
27.29
1520
1521
1555
1577
1646
1654
1654
1670
1670
1732
1730
1769
1783
1824
1835
1840
1844
1866
1866
1879
1919
1925
1950
1969
1978
1989
2033
2057
2182
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
11508 0.20 UG/L
0 Not Found UG/L
2313
15341
0.04 UG/L
0.09 UG/L
Not Found UG/L
136688 0.45 UG/L
188435 0.35 UG/L
188435
54785
13602
0.35 UG/L
0.21 UG/L
0.10 UG/L
Not Found UG/L
101890 0.34 UG/L
0 Not Found UG/L
Not Found UG/L
4 694 7
135669
129189
209785
66442
115560
129300
145111
118790
99574
256146
130590
32187
40108
0.27 UG/L
0.40 UG/L
0.52 UG/L
0.77 UG/L
0.29 UG/L
0.41 UG/L
0.50 UG/L
0.47 UG/L
0.48 UG/L
0.79 UG/L
1. 8 0 UG/L
0.60 UG/L
0.27 UG/L
Not Found UG/L
0.72 UG/L
Fit
585
973
638
714
921
821
982
994
995
785
935
671
977
508
452
943
974
976
943
988
956
973
960
961
972
980
984
759
375
950
Rf
0.000
0.284
0.000
0.259
0.858
0.000
1.510
2. 64 9
2. 64 9
1.305
0.701
0.000
1. 470
0.000
0.000
0.855
1.673
1. 234
1.354
1.120
1.386
1.277
1 . 53 0
1.224
0. 620
0.702
1. 074
0.579
0.000
0.276
Operator ID, MC
Output File, AE01302.1A2
Data File' AE01302.MS
Name' AE01302
QUANT REPORT
Sample, Location, 200 N. Hull, SB14-H
ID File: 826AEC28.QCI
Page
Quant Time' 03/29/99 17,01
Injected at, 03/28/99 09:15
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 7.42 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.60 2364
27.93 2392
28.53 2444
225
128
180
Area
44 894
76569
38958
Cone Units
0.83 UG/L
0. 63 UG/L
0. 66 UG/L
Fit
975
989
980
Rf
0.268
0.596
0.291
Operator ID: MC
Output File: AE01303.1A2
Data File: AE01303.MS
Name: AE01303
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-I
ID File: 826AEC28.QCI
Page
Quant· Time: 03/29/99 17:01
Injected at: 03/28/99 09:54
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.25 g
Last Calibration: 03/29/99
Compound.
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Brornomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroechane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.03 1201
21.13 1810
23.92 2049
4.52
0.00
0.00
6.37
0.00
7.33
8.58
9.57
10.16
10.95
387
438
466
545
566
628
734
820
870
938
12.01 1029
0.00 1029
0.00 1069
12.56 1075
12.94 1108
13.22 1132
13.23 1133
13.59 1164
13.58 1163
14.65 1255
0.00 1291
0.00 1309
0.00 1327
16.18 1386
16.78 1437
17.12 1466
0.00 1489
96 2102517
95 839987
10.00 UG/L
8.64 UG/L
8.10 UG/L
0.12 UG/L
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
508287
9058
12131
Not Found UG/L
Not Found UG/L
0. 71 UG/L
Not Found UG/L
12976 0.12 UG/L
1808 0.04 UG/L
95719 0.47 UG/L
6003 0.06 UG/L
1554 0.02 UG/L
3502 0.03 UG/L
Not Found UG/L
0 Not Found UG/L
3009 0.03 UG/L
2909
7142
3737
21429
2805
5359
0.02 UG/L
0.08 UG/L
0.05 UG/L
0.09 UG/L
0.03 UG/L
0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
3563 0.04 UG/L
48318
44596
0.17 UG/L
0.54 UG/L
0 Not Found UG/L
Fit
998
999
94 9
899
140
390
708
84 7
989
887
985
890
777
786
762
593
772
918
828
953
996
928
967
237
413
650
901
980
719
847
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0. 225
0.975
0.452
0.485
0.511
0.000
0.000
0.524
0.662
0. 4 02
0.380
1.098
0.430
0.291
0.000
0.000
0.000
0.453
1.369
0.396
0.000
Operator ID: MC
Output File: AE01303.1A2
Data File: AE01303.MS
Name: AE01303
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-I
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/29/99 17:01
Injected at: 03/28/99 09:54
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 6.25 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) .630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40)
41)
42)
43)
44)
4 5)
46)
47)
4 8)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.73
0.00
18.39
19.20
19.30
19.32
1,3-Dimethylbenzene (rn-Xylene 19.49
1521
1519
1556
1576
1644
1653
1655
1669
1,4-Dimethylbenzene (p-Xylene 19.49 1669
1,2-Dimethylbenzene (a-Xylene 20.20
Styrene 20.22
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.80
0.00
0.00
21.47
21.50
21.77
21.77
21.94
22.39
22.47
22.76
22.98
23.21
23.21
23.74
23.97
25.44
27.29
1730
1732
1770
1782
1825
1836
1839
1842
1865
1865
1879
1918
1925
1950
1969
1989
1989
2034
2053
2179
2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119.
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
16293 0.27 UG/L
0 Not Found UG/L
1951 0.04 UG/L
21715
23 94
172707
157160
157160
84230
61754
0.12 UG/L
0.04 UG/L
0.54 UG/L
0. 28 UG/L
0.28 UG/L
0. 31 UG/L
0.42 UG/L
0 Not Found UG/L
112777 0.36 UG/L
0 Not Found UG/L
0 Not Found UG/L
77496 0.43 UG/L
151666 0.43 UG/L
169449 0.65 UG/L
214627
106038
129789
99678
194182
143074
289203
289203
151495
118327
9942
27859
0.75 UG/L
0.45 UG/L
0.45 UG/L
0. 3 7 UG/L
0.60 UG/L
0.56 UG/L
2.22 UG/L
1.96 UG/L
0.67 UG/L
0.97 UG/L
0. 57 UG/L
0.48 UG/L
Fit
556
980
667
724
933
708
992
992
993
825
917
684
957
527
358
953
982
966
947
988
956
973
94 9
983
969
976
988
740
802
976
Rf
0.000
0.284
0.000
0.259
0.858
0. 311
1. 510
2. 64 9
2. 64 9
1.305
0.702
0.000
1. 4 70
0.000
0.000
0.855
1.673
1. 234
1.354
1.120
1.386
1. 277
1.530
1.223
0.620
0.702
1.074
0.579
0.083
0.276
Operator ID: MC
Output File: AE01303.1A2
Data File: AE01303.MS
Name: AE01303
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-I
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:01
Injected at: 03/28/99 09:54
Dilution Factor: l. 00
Instrument ID: 20701-1284
Commenc: Sampling: 02/24/1999 by J. Conway, use 6.25 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.57 2362 225 46257 0.82
62) 91-20-3 Naphthalene 27.92 23 92 128 64 562 0.52
63) 82-61-6 1,2,3-Trichlorobenzene 28.50 2442 180 21843 0.36
* Compound is ISTD
Units Fit Rf
--------
UG/L 982 0.268
UG/L 982 0.596
UG/L 963 0.291
Operator ID: MC
Output File: AE01304 .1A2
Data File: AE01304.MS
Name: AE01304
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-J
ID File: 826AEC28.QCI
Page 1
Quant Time: 03/29/99 17:02
Injected at: 03/28/99 10:33
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 8.81 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
26) 75-27-4 Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-BB-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.03
21.15
23.93
4.54
0.00
0.00
6.39
6.67
7.36
0.00
9.60
0.00
0.00
0.00
0.00
0.00
12.58
0.00
0.00
0.00
13.62
0.00
14.68
o.oo 0.00
0.00
o.oo 16.80
1202
1812
2050
389
438
466
547
571
630
737
822
874
943
1033
1033
1069
1077
1112
1136
1143
1166
1164
1257
1291
1309
1327
1390
1439
0.00 1464
0.00 1491
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2093480
898441
598041
5182
10.00
9.28
9.58
0.07
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
Not Found UG/L
13318 0.79 UG/L
451 0.04 UG/L
8262 0.08 UG/L
Not Found UG/L
290377 1.43 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
3626 0.03 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
18892 0.08 UG/L
0 Not Found UG/L
1157 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
51467 0.18 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
951
877
193
217
718
858
978
445
983
481
422
615
584
481
920
365
436
866
989
917
BOO
109
410
698
454
981
619
814
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.974
0.000
0.000
0.000
0.000
0.000
0.524
0.000
0.000
0.000
1.098
0.000
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01304.1A2
Data File: AE01304.MS
Name: AE01304
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-J
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Comment: Sampling: 02/24/1999 by J. Conway, use 8.81 g
Page 2
03/29/99 17:02
03/28/99 10:33
1.00
20701-1284
Last Calibration: 03/29/99. Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
45)
142-28-9
127-18-4
124-48-l
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.77
0.00
0.00
19.21
0.00
19.33
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.27
1521
1522
1556
1579
1646
1656
1656
1672
1672
1733
1737
1770
1784
1825
1836
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.83
0.00
0.00
0.00 1841
21.53 1844
0.00 1871
21.80 1868
21.94
22.40
22.50
22.77
23.00
23.12
23.24
23.76
24.02
0.00
27.29
1879
1919
1927
1951
1970
1981
1991
2035
2058
2183
2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
14 6
75
180
Area Cone Units
Not Found UG/L
4057 0.07 UG/L
Not Found UG/L
Not Found UG/L
11923 0.07 UG/L
Not Found UG/L
113094 0.36 UG/L
121555
121555
62109
16834
0.22 UG/L
0.22 UG/L
0.23 UG/L
0.11 UG/L
0 Not Found UG/L
65328 0.21 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
100369 0.29 UG/L
Not Found UG/L
184617 0.65 UG/L
67933
103417
79146
110528
97371
64313
257987
89195
32500
32372
0.29 UG/L
0.36 UG/L
0.30 UG/L
0.35 UG/L
0.38 UG/L
0.50 UG/L
1.76 UG/L
0.40 UG/L
0.27 UG/L
Not Found UG/L
0.56 UG/L
Fit
608
918
684
458
792
433
980
986
986
759
915
451
952
254
289
818
979
967
954
989
956
930
926
94 0
980
980
940
732
4 99
933
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2. 64 9
2.649
1.305
0.701
0.000
1.470
0.000
0.000
0.000
1. 673
0.000
1. 354
1.120
1. 386
1.277
1.530
1.224
0.620
0.702
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01304.1A2
Data File: AE01304.MS
Name: AE01304
QUANT REPORT
Sample: Location: 200 N. Hull, SB14-J
ID File: 826AEC28.QCI
Page
Quant Time: 03/29/99 17:02
Injected at: 03/28/99 10:33
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 8.81 g
Last Calibration: 03/29/99
61)
62)
6 3)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.60
27.95
28.53
2365
2395
2445
225
128
180
Area
27832
60953
3004 9
Cone Units
0.50 UG/L
0. 4 9 UG/L
0.49 UG/L
Fit
962
974
975
Rf
0.269
0. 596
0.291
Operator ID: MC
Output File: AE01272.1A2
Data File: AE01272.MS
Name: AE01272
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:14
Injected at: 03/30/99 21:16
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.01 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
3 0)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.04 1203
21.15 1812
23.94 2051
4.54 389
0.00
0.00
6.39
0.00
7.35
0.00
9.60
0.00
0.00
438
470
547
567
630
737
822
874
939
0.00 1033
0.00 1030
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1138
13.62 1167
0.00 1162
14.69 1258
0.00 1291
0.00 1309
15.48 1326
0.00 1390
16.82 1440
0.00 1464
0.00 1494
96 1703095
95 825539
152 509462
10.00 UG/L
10.49 UG/L
10.03 UG/L
85 4510 0.07 UG/L
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
Not Found UG/L
5240 0.38 UG/L
0 Not Found UG/L
4931 0.06 UG/L
0 Not Found UG/L
429609 2.60 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
10733 0.06 UG/L
0 Not Found UG/L
588 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
789 0.01 UG/L
Not Found UG/L
22612 0.10 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
94 9
881
109
588
661
903
979
543
993
558
884
466
629
393
398
651
487
804
996
898
825
143
29
818
224
986
563
623
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0. 291
0.000
0.000
0.403
0.000
1.369
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01272.1A2
Data File: AE01272.MS
Name: AE01272
Quant Time: 03/31/99 08:14
Injected at: 03/30/99 21:16
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: Comala-Madison Ave, SB15-A
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 5.01 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
3 6)
37)
38)
39 I
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.77
0.00
0.00
0.00
0.00
19.33
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.22
Styrene 20.34
1521
1522
1556
1579
1648
1651
1656
1672
1672
1732
1742
1770
1781
1825
1836
1841
1845
1866
1868
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.79
0.00
0.00
0.00
21.54
0.00
21.81
21.94 1879
22.36 1916
22.48 1926
22.79 1952
23.00 1970
23.12 1981
23.24 1991
23.76 2035
0.00 2055
0.00 2183
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
8688 0.18 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
42807
59587
59587
32004
1428
0.17 UG/L
0. 13 UG/L
0.13 UG/L
0.14 UG/L
0.01 UG/L
0 Not Found UG/L
25299 0.10 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
57488 0.20 UG/L
0 Not Found UG/L
129228 0.56 UG/L
29280
21177
83824
63063
57785
36330
0.15 UG/L
0.09 UG/L
0.39 UG/L
0.24 UG/L
0.28 UG/L
0. 34 UG/L
88660 0.74 UG/L
57151 0.31 UG/L
Not Found UG/L
Not Found UG/L
7350 0.16 UG/L
Fit
114
985
651
627
673
724
983
992
996
901
864
238
944
202
583
837
918
933
975
964
920
967
966
955
964
978
956
589
311
919
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2. 64 9
1.305
0.701
0.000
1. 4 70
0.000
0.000
0.000
1.673
0.000
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01272.1A2
Data File: AE01272.MS
Name: AE01272
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-A
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:14
Injected at: 03/30/99 21:16
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.01 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.59 2364
27.94 2394
28.53 2445
225
128
180
Area
14 825
127811
15863
Cone Units
0.32 UG/L
1.26 UG/L
0.32 UG/L
Fit
973
990
970
Rf
0.269
0. 596
0. 291
Operator ID' MC
Output File, AE01273.1A2
Data File, AE01273.MS
Name, AE01273
QUANT REPORT
Sample' Location, Comala-Madison Ave, SB15-B
ID File, 826AEC28.QCI
Page
Quant Time' 03/31/99 08,19
Injected at' 03/31/99 00,34
Dilution Factor' 1.00
Instrument ID, 20701-1284
Comment, Sampling' 02/24/1999 by J. Conway, use 0.261 g
Last Calibration, 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1~2-Dichloroethane
Trichloroethene
1,2, ~Dichloropropane
Dibromomethane
Bromodichloromethane
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/29/99 09,28
R.T. Scan# Q ion
14.06
21.17
23.94
4.54
0.00
0.00
6.40
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.31
0.00
0.00
0.00
1203
1812
2050
388
438
466
548
572
630
737
822
874
942
1033
1033
1069
1078
1112
1136
1138
1167
1166
1258
0.00 1291
0.00 1309
0.00 1331
0.00 1389
0.00 1440
0.00 1463
17.53 1501
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1896589
2478250
996879
4473
10.00 UG/L
28.30 UG/L
17. 6 5 UG/L
0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
3269 0.21 UG/L
Not Found UG/L
5498 0.06 UG/L
0 Not Found UG/L
458678 2.49 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
769 0.01 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
612179 22.12 UG/L
Fit
997
799
840
885
368
367
729
673
980
596
942
584
655
488
510
590
597
424
901
480
424
665
103
64
733
0
410
168
710
Rf
1.000
0.462
0. 298
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.380
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.146
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01273.1A2
Data File: AE01273.MS
Name: AE01273
Quant Time: 03/31/99 08:19
Injected at: 03/31/99 00:34
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: Comala-Madison Ave, SB15-B
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 0.261 g
Last calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
3 3)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
0.00
17.79
0.00
18.41
0.00
1,1,1,2-Tetrachloroethane 0.00
Ethylbenzene 19.35
1,3-Dimethylbenzene (m-Xylene 19.55
1,4-Dimethylbenzene (p-Xylene 19.55
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 0.00
Bromoform 0.00
20.85
0.00
0.00
0.00
21.55
0.00
21.82
0.00
0.00
22.50
22.80
23.02
0.00
0.00
1520
1523
1555
1576
1648
1655
1657
1673
1673
1732
1734
1769
1785
1820
1835
1841
1845
1867
1868
1883
1921
1927
1953
1971
1979
1992
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 2036
0.00 2054
0.00 2182
0.00 2338
78
166
12 9
107
112
131
91
91
91
91
104
171
105
83
75
0 Not Found UG/L
594906 10.98 UG/L
0 Not Found UG/L
16663 0.34 UG/L
0 Not Found UG/L
0 Not Found UG/L
1866093 6.51 UG/L
3370934
3370934
962468
6.72
6.72
3.89
UG/L
UG/L
UG/L
0 Not Found UG/L
0 Not Found UG/L
2156115 7.71 UG/L
0 Not Found UG/L
Not Found UG/L
77 0 Not Found UG/L
91 3733695 11.80 UG/L
91 Not Found UG/L
105 39899326 164.24 UG/L
91
119
0 Not Found UG/L
Not Found UG/L
175.18 UG/L
9.70 UG/L
105 42511738
105 2819452
119 11098757
146
146
91
146
75
180
48.51 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Fit
4 94
958
707
246
931
992
990
824
280
917
732
736
495
965
839
592
992
789
968
506
469
601
445
Rf
0.000
0.286
0.000
0.259
0.000
0.000
1. 511
2.646
2.646
1.305
0.000
0.000
1. 474
0.000
0.000
0.000
1.669
0.000
1. 281
0.000
0.000
1. 280
1.534
1.207
0.000
0.000
0.000
0.000
0.000
0.000
Operator ID: MC
Output File: AE01273.1A2
Data File: AE01273.MS
Name: AE01273
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-B
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:19
Injected at: 03/31/99 00:34
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.261 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 0.00 2364 225 Not Found
62) 91-20-3 Naphthalene 27.97 2395 128 5573393 51.55
63) 82-61-6 1,2,3-Trichlorobenzene 0.00 2445 180 Not Found
• Compound is ISTD
Units Fit Rf
--------
UG/L 308 0.000
UG/L 988 0.571
UG/L 616 0.000
Operator ID: MC
Output File: AE01274.1A2
Data File: AE01274.MS
Name: AE01274
QUANT REPORT
Sample: Location: Comala-Madison Ave, 5815-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:21
Injected at: 03/31/99 01:13
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.240 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
S) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9 Bromomethane
8) 75-00-3 Chloroethane
9) 75-69-4
10) 75-35-4
H) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Tri chloroethene
1,2, -Dichloropropane
Dibromomethane
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-J Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.04 1203
21.15 1812
0.00 2051
4.54 389
0.00 438
0.00 466
0.00 558
0.00 568
7.37 631
0.00 737
9.60 822
0.00 874
10.88 931
0.00 1033
0.00 1033
0.00 1069
0.00 1079
0.00 1112
0.00
13.35
0.00
0.00
0.00
0.00
0.00
0.00
0.00
16.82
0.00
0.00
1136
1143
1168
1166
1259
1291
1309
1327
1390
1441
1464
1489
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
2456063
3600183
10.00 UG/L
31.75 UG/L
0 Not Found UG/L
6391 0.07 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
6801 0.05 UG/L
0 Not Found UG/L
580512 2.43 UG/L
0 Not Found UG/L
6058 0.05 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
75 0 Not Found UG/L
117 5213 0.06 UG/L
78 Not Found UG/L
62 0 Not Found UG/L
130 0 Not Found UG/L
63 0 Not Found UG/L
93 0 Not Found UG/L
83 Not Found UG/L
75 0 Not Found UG/L
91 68934465 200.47 UG/L
75 Not Found UG/L
83 0 Not Found UG/L
Fit
809
848
740
865
0
419
762
760
980
443
926
436
898
501
235
405
459
116
763
655
600
397
181
756
16
991
322
760
Rf
1. 000
0.462
0.000
0.361
0.000
0.000
0.000
0.000
0.526
0.000
0. 972
0.000
0. 485
0.000
0.000
0.000
0.000
0.000
0.000
0.380
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.401
0.000
0.000
Operator ID: MC
Output File: AE01274.1A2
Data File: AE01274.MS
Name: AE01274
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-C
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 08:21
Injected at: 03/31/99 01:13
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.240 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
39)
4 0)
100-41-4
108-38-3
106-42-3
95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
0.00 1524
0.00 1556
0.00 1579
0.00 1648
0.00 1656
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
1658
1672
1672
1733
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1735
0.00 1770
20.83 1785
0.00 1821
0.00 1836
0.00 1842
21.54 1846
21.66 1856
21.81 1868
0.00 1882
22.50 1927
22.50 1927
22.81 1954
23.01 1972
0.00 1980
0.00 1993
23.77 2036
0.00 2055
0.00 2183
0.00 2340
78
166
129
107
112
131
0 Not Found UG/L
Not Found UG/L
0 Not Found .UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
91 103612091
91 309599703
91 309599703
91 169325504
267.66 UG/L
526.62 UG/L
526.62 UG/L
519.83 UG/L
104
171
0 Not Found UG/L
Not Found UG/L
105 41017683 108.93 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
83
75
77
91 81449650 207.28 UG/L
91 48574348 156.30 UG/L
105 170640075 623.88 UG/L
91 0 Not Found UG/L
119 101640035 252.48 UG/L
105 323241526 1017.43 UG/L
105 26850518
119 54484523
70.04 UG/L
191.41 UG/L
146
146
0 Not Found UG/L
0 Not Found UG/L
91 40673566
146
75
180
174. 34 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Fit
54 7
557
689
146
988
989
985
992
232
0
977
747
2
971
803
963
667
730
986
990
979
479
460
880
553
Rf
0.000
0.000
0.000
0.000
0.000
0.000
1.577
2.394
2.394
1.327
0.000
0.000
1.534
0.000
0.000
0.000
1.600
1. 266
1.114
0.000
1. 64 0
1.294
1. 561
1.159
0.000
0.000
0.950
0.000
0.000
0.000
Operator ID: MC
Output File: AE01274.1A2
Data File: AE01274.MS
Name: AE01274
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-C
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:21
Injected at: 03/31/99 01:13
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.240 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Al-e a Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 0.00 2365 225 Not Found
62) 91-20-3 Naphthalene 27.97 2396 128 237477571 0.00
63) 82-61-6 1,2,3-Trichlorobenzene 0.00 2447 180 0 Not Found
• Compound is ISTD
Units Fit Rf
--------UG/L 346 0.000
UG/L 990 -0.253
UG/L 361 0.000
Opera tor ID: MC
Output File: AE01275.1A2
Data File: AE01275.MS
Name: AE01275
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:22
Injected at: 03/31/99 01:52
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.230 g
Last calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromoflucrobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
].07-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichlorcethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichlorcethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
].0061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.06 1203
0.00 1812
0.00 2051
4.56 390
0.00 438
0.00 472
6.47 554
0.00 572
7.37 631
0.00 737
9.62 823
0.00 874
0.00 940
0.00 1033
0.00 1039
0.00
0.00
0.00
0.00
0.00
13.64
13.59
0.00
0.00
0.00
0.00
0.00
16.82
1069
1078
1112
1136
1138
1167
1163
1258
1291
1309
1327
1389
1440
0.00 1464
o.oo. 1486
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
2853724 10.00 UG/L
0 Net Found UG/L
Not Found UG/L
6652 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
2009 0.09 UG/L
Not Found UG/L
6619 0.04 UG/L
0 Not Found UG/L
601573 2.17 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
4 9 Not Found UG/L
83 0 Not Found UG/L
97 Not Found UG/L
75 Not Found UG/L
117 0 Not Found UG/L
78 683818 2.18 UG/L
62 8714 0.07 UG/L
130 0 Not Found UG/L
63 Not Found UG/L
93 0 Not Found UG/L
83 0 Not Found UG/L
75 Not Found UG/L
91 225875734 543.14 UG/L
75
83
Not Found UG/L
0 Not Found UG/L
Fit
868
443
646
809
50
514
618
396
959
678
973
690
791
4 96
600
370
470
0
189
389
836
758
238
208
990
286
704
Rf
1.000
0.000
0.000
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.973
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.100
0.430
0.000
0.000
0.000
0.000
0.000
1. 458
0.000
0.000
Operator ID' MC
Output File, AE01275.1A2
Data File' AE01275.MS
Name, AE01275
QUANT REPORT
Sample, Location, Comala-Madison Ave, SB15-D
ID File, 826AEC28.QCI
Page 2
Quant Time, 03/31/99 08,22
Injected at, 03/31/99 01,52
Dilution Factor, 1.00
Instrument ID' 20701-1284
Comment' Sampling, 02/24/1999 by J. Conway, use 0.230 g
Last Calibration, 03/29/99 Last Qcal Time, 03/29/99 09,28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48)
49)
95-49-8
108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
0.00 1524
0.00 1555
0.00 1578
0.00 1648
0.00 1655
0.00 1656
1,3-Dimethylbenzene (m-Xylene 0.00 1673
1,4-Dimethylbenzene (p-Xylene 0.00 1673
1,2-Dimethylbenzene (a-Xylene 20.27 1735
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1734
0.00 1769
20.85 1785
0.00 1823
0.00 1835
0.00 1841
21.56 1846
21.74
21.74
1861
1861
0.00 1881
0.00 1921
0.00 1926
0.00 1953
23.03 1972
0.00 1979
0.00 1992
23.79 2037
0.00 2054
0.00 2182
0.00 2339
78
166
129
107
112
131
91
91
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
91 Not Found UG/L
91 368962594 961.06 UG/L
104 0 Not Found UG/L
171 Not Found UG/L
105 134857199 286.49 UG/L
83
75
Not Found UG/L
0 Not Found UG/L
77 0 Not Found UG/L
91 224646555 524.84 UG/L
91 42485194 118.39 UG/L
UG/L 105 376881547 1471.47
91
119
105
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
105 Not Found UG/L
119 141505863 459.27 UG/L
146 0 Not Found UG/L
146 Not Found UG/L
91 84366306 346.91 UG/L
146 Not Found UG/L
75
180
0 Not Found UG/L
0 Not Found UG/L
Fit
573
105
661
41
297
268
919
262
893
831
2
67
881
899
760
63
696
552
144
957
455
380
865
339
Rf
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.346
0.000
0.000
l. 650
0.000
0.000
0.000
1.500
1.258
0.898
0.000
0.000
0.000
0.000
1.080
0.000
0.000
0.853
0.000
0.000
0.000
Operator ID: MC
Output File: AE01275.1A2
Data File: AE01275.MS
Name: AE01275
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-D
ID File: 826AEC28.QC!
Page
Quant Time: 03/31/99 08:22
Injected at: 03/31/99 01:52
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.230 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
. Compound
He~achlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
0.00 2364
27.98 2396
0.00 2446
225 Not Found UG/L
128 409162495 0.00 UG/L
180 0 Not Found UG/L
Fit
290
989
222
Rf
0.000
-0.663
0.000
Operator ID: MC
Output File: AE01276.1A2
Data File: AE01276.MS
Name: AE01276
QUANT REPORT
Sample: Location: Comala-Madison Ave, 5815-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:25
Injected at: 03/31/99 02:32
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.221 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.03 1201
0.00 1812
0.00 2051
4.56
5.10
0.00
0.00
0.00
7.36
0.00
9.61
390
436
466
556
572
630
734
822
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1138
13.62 1165
0.00 1159
0.00 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1439
0.00 1464
0.00 1487
96 3381571 10.00 UG/L
Not Found UG/L
0 Not Found UG/L
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
10329
7115
0.08 UG/L
0.16 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
8137 0.05 UG/L
Not Found UG/L
694618 2.11 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
o Not Found uGiL
368291 0.99 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
91 85087108 180.14 UG/L
75
83
0 Not Found UG/L
Not Found UG/L
Fit
838
626
673
827
74 9
268
648
600
874
813
923
628
678
553
385
227
578
51
265
539
881
817
628
224
118
618
990
408
826
Rf
1.000
0.000
0.000
0.361
0.130
0.000
0.000
0.000
0.526
0.000
0.973
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.099
0.000
0.000
0.000
0.000
0.000
0.000
1.397
0.000
0.000
Operator ID: MC
Output File: AE01276.1A2
Data File: AE01276.MS
Name: AE01276
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-E
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 -08:25
Injected at: 03/31/99 02:32
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.221 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32)
33)
34)
35)
3 6)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
127-18-4
124-48-1
106-93-4
106-90-7
630-20-6
100-41-4
108-38-J
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
0.00
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 0.00
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.83
0.00
0.00
0.00
21.55
0.00
0.00
0.00
22.50
22.50
22.80
23.01
0.00
0.00
23.76
0.00
0.00
0.00
1524
1555
1578
1646
1655
1656
1671
1671
1732
1734
1769
1783
1821
1835
1841
1845
1867
1869
1881
1926
1926
1952
1970
1979
1992
2034
2054
2182
2339
78
166
129
107
112
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
131 0 Not Found UG/L
91 144099675 270.25 UG/L
91 381276049 465.79 UG/L
91 381276049 465.79 UG/L
91 214475148 478.86 UG/L
104 Not Found UG/L
171 Not Found UG/L
105 58923595 · 113.45 UG/L
83 Not Found UG/L
75 Not Found UG/L
77 0 Not Found UG/L
91 114328570 211.51 UG/L
91 Not Found UG/L
105 Not Found UG/L
91 Not Found UG/L
119 168470509 294.64 UG/L
105 409099452
105 37979907
119 85198886
936.24
71.92
219.04
UG/L
UG/L
UG/L
146 Not Found UG/L
146 Not Found UG/L
91 58757619 184.11 UG/L
146
75
180
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
668
45
0
64 7
239
984
957
944
962
219
0
952
806
2
2
879
318
2
63
714
961
990
960
584
516
810
680
0
Rf
0.000
0.000
0.000
0.000
0.000
0.000
1.577
2.421
2.421
1.325
0.000
0.000
1.536
0.000
0.000
0.000
1.599
0.000
0.000
0.000
1·. 6 91
1. 293
1.562
1.151
0.000
0.000
0.944
0.000
0.000
0.000
Operator ID: MC
Output File: AE01276.1A2
Data File: AE01276.MS
Name: AE01276
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-E
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page
03/31/99 08:25
03/31/99 02:32
1. 00
20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.221 g
Last Calibration: 03/29/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
0.00
27.97
0.00
2364
2395
2446
225 Not Found UG/L
128 349780348 0.00 UG/L
180 0 Not Found UG/L
Fit
236
988
3 98
Rf
0.000
-0.312
0.000
Operator ID: MC
Output File: AE01277.1A2
Data File: AE01277.MS
Name: AE01277
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-F
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:18
Injected at: 03/30/99 23:54
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.860 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3)
4)
5)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis -1, 3 -Dichloropropen·e
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.15
23.94
4.55
0.00
5.43
6.49
0.00
7.36
8.57
9.60
10.18
10.98
12.04
12.05
12.47
0.00
12.98
13.24
13.29
13.60
13.58
14.67
0.00
15.27
15.46
16 . 19
16. 81
17.08
0.00
1202
1811
2050
389
438
465
556
580
630
733
821
870
939
1030
1031
1067
1079
1110
1133
1137
1164
1162
1256
1296
1307
1323
1386
1439
1462
1493
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1880429
898910
531058
21351
2260
1744
194 00
354 3
534995
9876
2344
5691
868
Cone Units
10.00 UG/L
10.34 UG/L
9.47 UG/L
0.31 UG/L
Not Found UG/L
0.05 UG/L
0. 11 UG/L
Not Found UG/L
0.20 UG/L
0.08 UG/L
2. 93 UG/L
0.12 UG/L
0.03 UG/L
0.06 UG/L
0.05 UG/L
3905 0.04 UG/L
4481
12568
3353
19920
4 816
11704
Not Found UG/L
0.04 UG/L
0.17 UG/L
0.05 UG/L
0.10 UG/L
0.06 UG/L
0.21 UG/L
0 Not Found UG/L
1589 0.05 UG/L
2583 0.03 UG/L
4068
75839
4199
0.05 UG/L
0.29 UG/L
0.06 UG/L
0 Not Found UG/L
Fit
998
999
94 9
934
831
702
797
988
961
991
983
869
976
862
839
645
921
919
941
996
988
966
430
932
834
855
975
916
872
Rf
1.000
0.463
0. 299
0.361
0.000
0.226
0.081
0.000
0.526
0.225
0.972
0.452
0. 4 85
0. 511
0.095
0.486
0.000
0.662
0.402
0.380
1.098
0.430
0.291
0.000
0.182
0.403
0.453
1.369
0.396
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01277.1A2
Data File: AE01277.MS
Name: AE01277
Quant Time: 03/31/99 08:18
Injected at: 03/30/99 23:54
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: Comala-Madison Ave, SB15-F
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 0.860 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T~ Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
17.72 1517
17.77 1521
18.16
18.41
19.22
19.32
19.33
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.24
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
0.00
21.50
21.54
21.78
21.80
21.94
22.42
22.48
22.80
22.99
23.26
23.26
23.76
23.98
0.00
27.29
1555
1576
1646
1654
1655
1671
1671
1732
1733
1770
1783
1824
1836
1841
1844
1865
1866
1879
1920
1925
1952
1969
1991
1991
2035
2053
2182
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
2560
2 94 02
2445
2014
24642
3046
121631
316955
316955
Cone Units
0.13 UG/L
0.55 UG/L
0.05 UG/L
0. 04 UG/L
0.15 UG/L
0.05 UG/L
0.43 UG/L
0.64 UG/L
0. 64 UG/L
111239 0.45 UG/L
29957 0.23 UG/L
0 Not Found UG/L
110416 0.40 UG/L
38511
206979
13 3 34 7
227519
123731
120070
241455
185205
217556
168306
168306
279033
67044
Not Found UG/L
Not Found UG/L
0.24 UG/L
0.66 UG/L
0.57 UG/L
0.89 UG/L
0.59 UG/L
0.46 UG/L
1.01 UG/L
0.64 UG/L
0.95 UG/L
1.45 UG/L
1.27 UG/L
1. 3 8 UG/L
0.62 UG/L
0 Not Found UG/L
86312 1.67 UG/L
Fit
708
982
793
898
969
736
992
995
996
907
894
248
989
539
560
974
990
941
991
990
918
994
993
993
986
967
993
716
114
980
Rf
0.104
0.284
0.282
0.259
0.858
0. 311
1.510
2.649
2.649
1.305
0.702
0.000
1. 4 70
0.000
0.000
0.855
1. 673
1.234
1.354
1.120
1. 386
1. 277
1. 530
1.223
0.620
0.703
1.074
0.579
0.000
0.276
Operator ID: MC
Output File: AE01277.1A2
Data File: AE01277.MS
Name: AE01277
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-F
ID·File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:18
Injected at: 03/30/99 23:54
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 0.860 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone ____________ :.._ _____________ .;, _____________
-------- --------
61) 87-68-3 Hexachlorobutadiene 27.60 2364 225 78170 1. 55
62) 91-20-3 Naphthalene 27.95 2394 128 237571 2.13
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2445 180 57233 1. 05
* Compound is ISTD
Units Fit Rf
--------
UG/L 994 0.268
UG/L 991 0.595
UG/L 977 0.291
Operator ID: MC
Output File: AE01278.1A2
Data File: AE01278.MS
Name: AE01278
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:15
Injected at: 03/30/99 21:56
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 3.55 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
71 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05 1202
21.16 18i2
23.94 2050
4.54 389
0.00 438
0.00 466
6.46 553
0.00 572
7.36 630
0.00 737
9.61 822
0.00 869
0.00 938
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00
13.62
0.00
14.70
0.00
0.00
15.47
0.00
16.81
0.00
0.00
1139
1165
1164
1258
12 91
1309
1324
1389
1439
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1854030
736687
479144
5629
10.00
8.60
8.66
0.08
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
Not Found UG/L
1350 0.09 UG/L
0 Not Found UG/L
6338 0.07 UG/L
0 Not Found UG/L
504946 2.80 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
10626 0.05 UG/L
0 Not Found UG/L
807 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
1268 0.02 UG/L
Not Found UG/L
24801 0.10 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
953
837
171
272
727
699
974
676
944
820
898
707
484
561
559
555
563
840
993
906
721
340
556
726
323
979
551
696
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 972
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0. 403
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01278.1A2
Data File: AE01278.MS
Name: AE01278
Quant Time: 03/31/99 08:15
Injected at: 03/30/99 21:56
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: Comala-Madison Ave, SB15-G
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 3.55 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.22
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene lp-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.29
1520
1522
1557
1578
1645
1655
1656
1672
1672
1732
1737
1769
1784
1824
1812
1841
1844
1866
1867
1878
1920
1926
1952
1970
1977
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.84
0.00
21.16
21.50
21.54
0.00
21.80
21.94
22.42
22.50
22.81
23.01
23.10
23.26 1992
23.77 2036
0.00 2054
0.00 2182
27.31 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
9234 0.18 UG/L
0 Not Found UG/L
Not Found UG/L
1332 0.01 UG/L
0 Not Found UG/L
41977 0.15 UG/L
72846 0.15 UG/L
72846
3014 0
3941
0.15 UG/L
0.13 UG/L
0.03 UG/L
0 Not Found UG/L
42764 0.16 UG/L
Not Found UG/L
423048 6.37 UG/L
7796
53519
0.05 UG/L
0.17 UG/L
Not Found UG/L
101007 0.40 UG/L
34991
64313
94160
71188
70188
20790
0.17
0.25
0.40
UG/L
UG/L
UG/L
0.25 UG/L
0.31 UG/L
0.18 UG/L
150311 1.15 UG/L
52889 0.27 UG/L
Not Found UG/L
Not Found UG/L
15644 0.31 UG/L
Fit
251
982
701
505
710
286
979
997
996
913
864
120
899
262
733
890
942
891
958
969
898
987
943
913
975
979
872
607
437
929
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2. 64 9
2.649
1.305
0.701
0.000
1.470
0.000
0.359
0.855
1.673
0.000
1.354
1.120
1.386
1. 277
1. 530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01278.1A2
Data File: AE01278.MS
Name: AE01278
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-G
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:15
Injected at: 03/30/99 21:56
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 3.55 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62 2365
27.96 2394
28.55 2445
225
128
180
Area
16382
97520
15473
Cone Units
0.33 UG/L
0.88 UG/L
0.29 UG/L
Fit
960
990
944
Rf
0.269
0.596
0.291
'!
Operator ID: MC
Output File: AED1279.1A2
Data File: AED1279.MS
Name: AED1279
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-H
ID File: 826AEC28.QCI
Page
Quant Time: D3/31/99 D8:16
Injected at: D3/3D/99 22:35
Dilution Factor: 1.DD
Instrument ID: 2D7D1-1284
Comment: Sampling: D2/24/1999 by J. Conway, use 2.19 g
Last Calibration: D3/29/99
Compound
1) *1D7-D6-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-D1-4
7) 74-83-9
8) 75-DD-3
9) 75-69-4
1D) 75-35-4
11) 75-D9-2
12) 156-6D-5
13) 75-34-3
14) 156-59-4
.15) 59D-2D-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
2D) 56-23-5
21) 71-43-2
22) 1D7-D6-2
23) 79-D1-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
24)
25)
26)
27)
28)
29)
3D)
1DD61-D1-5 Cis-1,3-Dichloropropene
1D8-88-3 Toluene
1DD61-02-6 Trans-1,3-Dichloropropene
79-DD-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: D3/29/99 09:28
R.T. Scan# Q ion
14.D6
21.17
23.96
4.55
D.DD
5.45
6 .4D
O.DD
7. 37
8.60
9.61
1D.2D
D.OO
12.D7
D.DD
12.50
D.OO
12.99
12D3
1812
2D51
389
438
466
548
575
631
735
822
872
942
1D33
1D34
1069
1D78
1111
13.27 1135
13.29 1137
13.62 1166
13.62 1165
14.69 1257
D.DD
15.29
D.DD
D.OD
16.82
17.1D
D.DD
1291
1309
1327
1389
144D
14 64
1493
96
95
152
85
47
62
96
49
1D1
96
49
61
63
61
97
49
83
97
75
117
78
62
13D
63
93
83
75
91
75
83
Area
1867217
881929
56229D
12327
1426
5364
13358
1641
489075
5108
Cone Units
1D.OO UG/L
10.22 UG/L
1D.l0 UG/L
D. 18 UG/L
Not Found UG/L
O.D3 UG/L
0. 36 UG/L
Not Found UG/L
D.14 UG/L
D. D4 UG/L
2.7D UG/L
D.D6 UG/L
Not Found UG/L
3D47 D.03 UG/L
0 Not Found UG/L
2224 D.D2 UG/L
Not Found UG/L
2764 D.02 UG/L
6437
2D49
14354
2391
4397
D.D9 UG/L
D.D3 UG/L
D.D7 UG/L
D.03 UG/L
D.D8 UG/L
0 Not Found UG/L
963 D.D3 UG/L
Not Found UG/L
Not Found UG/L
389D7 D.15 UG/L
1625 D.D2 UG/L
D Not Found UG/L
Fit
998
999
948
915
28
76D
730
728
986
944
993
918
625
929
875
7D8
56D
925
8D5
91D
992
974
944
395
8D7
691
688
974
745
782
Rf
1. DOD
D.463
0.299
0.361
D.DDD
D.226
D.D81
O.DDO
0.526
0.225
D.972
0. 452
O.DOD
D.511
D.ODO
0.486
0.000
0.662
D.4D2
0.380
1.098
D.43D
0.291
D.DDO
0.182
0.000
0.000
1.369
D.396
O.DOO
Operator ID: MC
Output File: AE01279.1A2
Data File: AE01279.MS
Name: AE01279
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-H
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 08:16
Injected at: 03/30/99 22:35
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 2.19 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-l
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.78 1522
0.00 1556
18.42 1577
19.24 1647
19.33 1655
19.35 1657
1,3-Dimethylbenzene (m-Xylene 19.53 1672
1,4-Dimethylbenzene (p-Xylene 19.53 1672
1,2-Dimethylbenzene (a-Xylene 20.24 1733
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromoben:zene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Buty1benzene
4-Isopropyltoluene
1,3-Dichl~robenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1733
0.00 1769
20.85 1785
0.00 1824
0.00 1828
21.50 1841
21.55 1845
21.81 1867
21.82 1868
21.97 1881
22.42 1920
22.51 1927
22.81 1953
23.02 1971
23.12 1980
23.26 1992
23.78 2036
0.00 2054
0.00 2182
27.32 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
15726
Cone Units
Not Found UG/L
0.30 UG/L
0 Not Found UG/L
950
10628
1006
60763
141036
141036
49825
14 962
0.02 UG/L
0.07 UG/L
0.02 UG/L
0.22 UG/L
0.29 UG/L
0.29 UG/L
0.20 UG/L
0.11 UG/L
0 Not Found UG/L
67998 0.25 UG/L
0 Not Found UG/L
0 Not Found UG/L
27323
114 8 92
65799
129024
59266
86953
125764
111267
116429
6454 9
98050
140525
0.17 UG/L
0.37 UG/L
0.29 UG/L
0.51 UG/L
0.28 UG/L
0. 34 UG/L
0.53 UG/L
0.39 UG/L
0.51 UG/L
0.56 UG/L
0.75 UG/L
0.70 UG/L
0 Not Found UG/L
0 Not Found UG/L
42683 0.83 UG/L
Fit
340
984
918
807
961
718
988
995
996
885
927
334
987
256
768
952
985
943
988
994
923
990
986
974
982
973
994
601
298
980
Rf
0.000
0.284
0.000
0.259
0.858
0. 311
l. 510
2. 64 9
2. 64 9
1.305
0.701
0.000
1. 4 70
0.000
0.000
0.855
1.673
l. 234
l. 354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.074
0.000
0.000
0.276
Operator ID: MC
Output File: AE01279.1A2
Data File: AE01279.MS
Name: AE01279
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-H
i •;.
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:16
Injected at: 03/30/99 22:35
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 2.19 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.62 2366 225 464 01 0.93
62) 91-20-3 Naphthalene 27.97 2395 128 103104 0.93
63) 82-61-6 1,2,3-Trichlorobenzene 28.57 2447 180 31617 0.58
* Compound is ISTD
Units Fit Rf
--------
UG/L 981 0.268
UG/L 989 0. 596
UG/L 965 0.291
Operator ID: MC
Output File: AE01280.1A2
Data File: AE01280.MS
Name: AE01280
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-I
ID File: 826AEC28.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Page 1
03/31/99 08:17
03/30/99 23:15
1. 00
20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 1.29 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1~1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.16
23.96
4.54
0.00
0.00
6.40
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
0.00
0.00
1202
1812
2051
389
438
466
548
572
630
737
822
874
942
1033
1030
1069
1078
1111
1136
1143
1165
1165
1258
1291
0.00 1309
0.00 1324
0.00 1386
16.82 1439
0.00 1463
0.00 1493
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1779824
795413
514584
4082
Cone Units
10.00 UG/L
9.67 UG/L
9.69 UG/L
0.06 UG/L
Not Found UG/L
Not Found UG/L
3665 0.25 UG/L
0 Not Found UG/L
5297 0.06 UG/L
Not Found UG/L
404851 2.34 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
7620 0.04 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
17300 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
950
831
0
424
708
0
985
631
986
583
586
431
738
332
310
743
461
889
992
861
601
127
482
753
727
983
593
671
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.000
0.000
0.000
0.000
0.000
0.000
1.369
0.000
0.000
Operator ID: MC
Output File: AE01280.1A2
Data File: AE01280.MS
Name: AE01280
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-I
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 08:17
Injected at: 03/30/99 23:15
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 1.29 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.78 1522
18.18 1557
0.00 1578
0.00 1648
0.00 1655
19.35 1657
1,3-Dimethylbenzene 1m-Xylene 19.53 1672
1,4-Dimethylbenzene (p-Xylene 19.53 1672
l,i-Dimethylbenzene (a-Xylene 20.24 1733
41) 100-42-5 .Styrene 20.23 1732
0.00 1769
20.86 1786
0.00 1824
0.00 1835
21.47 1838
21.56 1846
0.00 1870
42) 75-25-2 Bromoform
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propyll:>enzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
21.78 1865
0.00 1876
22.44 1921
22.50 1926
22.80 1952
23.00 1969
23.26 1992
23.26 1992
23.77 2036
0.00 2054
0.00 2182
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
0.04 UG/L
0.01 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
1941
676
24624 0.09 UG/L
35724
35724
20970
0.08 UG/L
0.08 UG/L
0.09 UG/L
3175 0.03 UG/L
Not Found UG/L
43170 0.17 UG/L
0 Not Found UG/L
Not Found UG/L
4039 0.03 UG/L
52716 0.18 UG/L
Not Found UG/L
108651 0.45 UG/L
0 Not Found UG/L
56903 0.23 UG/L
70655
58520
48062
93349
93349
38889
0.31 UG/L
0.22 UG/L
0.22 UG/L
0.85 UG/L
0.75 UG/L
0.20 UG/L
0 Not Found UG/L
0 Not Found UG/L
11978 0. 24 UG/L
Fit
94 7
74 9
537
488
567
973
988
989
792
866
417
943
240
696
733
955
929
967
984
921
946
921
960
963
965
956
598
342
918
Rf
0.000
0.284
0.282
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1. 470
0.000
0.000
0.855
1. 673
0.000
1.354
0.000
1 . 3 86
1. 277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01280.1A2
Data File: AE01280.MS
Name: AE01280
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-I
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:17
Injected at: 03/30/99 23:15
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 1.29 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62 2365
27.98 2396
28.55 2445
225
128
180
Area
14295
38067
14 74 9
Cone Units
0.30 UG/L
0. 36 UG/L
0.29 UG/L
Fit
960
986
920
Rf
0.269
0.596
0. 2 91
Operator ID: MC
Output File: AE01281.1A2
Data File: AE01281.MS
Name: AE01281
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-J
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:12
Injected at: 03/30/99 19:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.11 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
17)
18)
19)
20 I
21)
22)
23)
24)
251
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.04
21.16
23.94
4.54
0.00
0.00
6.48
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
1202
1812
2050
389
438
466
555
563
630
737
822
874
942
1033
1033
0.00 1069
0.00
0.00
0.00
0.00
13.62
0.00
0.00
0.00
0.00
15.47
0.00
16.81
0.00
0.00
1078
1112
1136
1138
1166
1166
1258
1291
1309
1324
1389
1439
1464
1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1833081
838152
537079
4133
10.00 UG/L
9. 89 UG/L
9.82 UG/L
0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
1064 0.07 UG/L
0 Not Found UG/L
5237 0.05 UG/L
Not Found UG/L
476443 2.68 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
10280 0.05 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
1164 0.02 UG/L
0 Not Found UG/L
29016 0.12 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
952
866
106
131
665
797
984
618
936
668
561
577
543
245
467
581
452
611
992
870
680
336
716
812
669
973
668
657
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 972
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 . 0 98
0.000
0.000
0.000
0.000
0. 4 03
0.000
1. 369
0.000
0.000
Operator ID: MC
Output File: AE01281.1A2
Data File: AE01281.MS
Name: AE01281
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-J
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 08:12
Injected at: 03/30/99 19:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.11 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
3 9)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-B
44) 79-34-5
45) 96-18-4
46)
47)
48)
4 9)
SO)
51)
52)
53)
54)
108-86-1
103-65-1
95-49-8
108-67-8
106-43~4
98-06-6
95-63-6
135-98-8
99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.78 1522
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene 1m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1555
1578
1648
1655
1656
1672
1672
1,2-Dimethylbenzene (a-Xylene 20.24 1733
Styrene 20.23 1732
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1769
20.84 1784
0.00 1824
21.16 1812
21.45
21.55
21.89
21.81
21.88
22.41
22.49
22.80
23.00
1837
1845
1874
1867
1873
1919
1926
1952
1969
23.26 1991
23.26 1991
23.77 2036
0.00 2054
0.00 2189
27.31 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
3332 0. 06 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
41453 0.15 UG/L
66015
66015
26186
8939
0.14 UG/L
0.14 UG/L
0.11 UG/L
0.07 UG/L
Not Found UG/L
33126 0.12 UG/L
Not Found UG/L
483335 7.35 UG/L
13087
60662
44540
60616
42183
65910
88708
64801
60107
0.08
0.20
0.20
0.24
0.21
0.26
0.38
0.23
0.27
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
157480 1.39 UG/L
157480 1.22 UG/L
40564 0.21 UG/L
Not Found UG/L
0 Not Found UG/L
13629 0.27 UG/L
Fit
306
959
686
252
482
394
975
989
992
830
851
55
932
179
788
904
911
930
956
978
951
953
871
945
970
972
933
574
554
935
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1. 510
2.649
2.649
1.305
0.701
0.000
1.470
0.000
0.359
0.855
1.673
1.234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01281.1A2
Data File: AE01281.MS
Name: AE01281
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-J
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:12
Injected at: 03/30/99 19:18
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.11 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.62 2365 225 16530 0.34
62) 91-20-3 Naphthalene 27.95 2394 128 128498 1. 18
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2445 180 15525 0. 29
• Compound is ISTD
Units Fit Rf
--------UG/L 94 9 0.269
UG/L 989 0.596
UG/L 926 0.291
Operator ID: MC
Output File: AE01282.1A2
Data File: AE01282.MS
Name: AE01282
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-K
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:13
Injected at: 03/30/99 19:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99
Compound
1) '107- 06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2;2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,·2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.03 1201
21.14 1810
23.92 2049
96 1894336 10.00 UG/L
9.58 UG/L
9.32 UG/L
4.54
0.00
0.00
6.39
0.00
7.36
0.00
9.59
10.16
388
438
465
547
565
630
733
820
869
0.00 942
0.00 1028
0.00 1039
0.00 1069
0.00 1078
0.00 1109
0.00 1136
0.00 1138
13.62 1165
13.59 1163
14.67 1255
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.79 1437
0.00 1464
0.00 1494
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
839263
526570
5654 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
4219 0.28 UG/L
Not Found UG/L
6014 0.06 UG/L
Not Found UG/L
481212 2.61 UG/L
1831 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
15654 0.08 UG/L
1616
10599
0.02 UG/L
0.19 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
14607 0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
94 9
902
157
531
693
742
987
724
987
765
481
855
706
559
399
779
681
768
996
94 9
960
124
566
617
695
989
547
619
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0. 4 52
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.430
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01282.1A2
Data File: AE01282.MS
Name: AE01282
Quant Time: 03/31/99 08:13
Injected at: 03/30/99 19:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: Comala-Madison Ave, SB15-K
ID File: 826AEC28.QCI
Comment: Sampling: 02/24/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
4 8)
4 9)
SO)
51)
52)
53)
54)
55)
56)
57)
58)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.76 1520
18.15
0.00
19.21
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.19
Styrene 20.22
Bromoform 0.00
20.83
0.00
0.00
21. so
21.53
0.00
21.78
21.94
22.41
22.47
22.77
23.00
23.24
23.24
23.74
0.00
1554
1578
1645
1649
1656
1670
1670
1729
1731
1769
1784
1824
1835
1841
1843
1867
1864
1878
1919
1924
1950
1969
1990
1990
2033
2054
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 2182
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91"
105
91
119
105
105
119
146
14 6
91
146
75
180
Area Cone Units
0 Not Found UG/L
70216 1.31 UG/L
1208 0.02 UG/L
0 Not Found UG/L
2131 0.01 UG/L
0 Not Found UG/L
39881 0.14 UG/L
44977 0.09 UG/L
44977
23341
8362
0.09 UG/L
0.09 UG/L
0.06 UG/L
Not Found UG/L
48467 0.17 UG/L
0 Not Found UG/L
0 Not Found UG/L
16866 0.10 UG/L
65880 0.21 UG/L
0 Not Found UG/L
119728 0.47 UG/L
22312
63181
66916
67591
65498
106936
106936
4 9928
0.11 UG/L
0.24 UG/L
0.28 UG/L
0.23 UG/L
0.28 UG/L
0. 91 UG/L
0.80 UG/L
0.25 UG/L
0 Not Found UG/L
0 Not Found UG/L
15461 0.30 UG/L
Fit
983
730
441
814
880
974
989
987
712
907
231
951
151
54 7
928
948
954
949
987
928
952
962
957
981
973
974
612
460
922
Rf
0.000
0.284
0.282
0.000
0.858
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1. 470
0.000
0.000
0.855
1. 673
0.000
1.354
1.120
1.386
1. 277
1. 530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01282.1A2
Data File: AE01282.MS
Name: AE01282
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-K
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:13
Injected at: 03/30/99 19:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.59
27.93
28.53
2363
2392
2443
225
128
180
-~-------~--------------------------------------------
Area
19969
35024
17053
Cone
0.39
0.31
0.31
Units
UG/L
UG/L
UG/L
Fit
979
990
964
Rf
0.269
0.596
0. 291
Operator ID, MC
Output File, AE01283.1A2
Data File, AE01283.MS
Name, AE01283
QUANT REPORT
Sample, Location, Comala-Madison Ave, SB15-L
ID File, 826AEC28.QCI
Page
Quant Time, 03/31/99 08,13
Injected at' 03/30/99 20,37
Dilution Factor, 1. 00
Instrument ID' 20701-1284
Comment, Sampling, 02/24/1999 by J. Conway, use 3.91 g
Last Calibration' 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1~1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene 28)
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/29/99 09,28
R.T. Scan# Q ion Area Cone Units
14.07 1203
21.18 1813
23.96 2051
4.55
0.00
0.00
6.42
0.00
7.37
0.00
9.62
10.20
0.00
390
438
457
549
572
631
737
823
872
942
0.00 1033
0.00 1029
0.00 1069
0.00 1078
13.00 1112
0.00 1136
0.00 1138
13.62 1166
0.00 1166
14.69 1257
0.00 1291
0.00 1309
15.50 1326
0.00 1389
16.83 1441
17.16 1469
0.00 1493
96 1896469
95 886372
152 551435
10.00 UG/L
10.11 UG/L
9.75 UG/L
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
5415 0.08 UG/L
Not Found UG/L
0 Not Found UG/L
9017 0.59 UG/L
Not Found UG/L
6815 0. 07 UG/L
0 Not Found UG/L
443200 2.40 UG/L
1448 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
1228 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
12808 0.06 UG/L
Not Found UG/L
1316 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
803 0.01 UG/L
64030
64 72
Not Found UG/L
0.25 UG/L
0.09 UG/L
Not Found UG/L
Fit
997
999
948
868
14 7
532
693
394
978
622
945
869
681
632
709
465
506
725
576
904
998
880
797
307
438
776
649
979
755
638
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0.452
0.000
0.000
0.000
0.000
0.000
0.662
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0. 4 03
0.000
1. 36 9
0.396
0.000
Operator ID: MC
Output File: AE01283.1A2
Data File: AE01283.MS
Name: AE01283
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-L
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/31/99 08:13
Injected at: 03/30/99 20:37
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 3.91 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
39)
40)
41)
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47)
4 8)
4 9)
50)
51)
52)
53)
54)
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00 1520
17.78 1522
18.21 1559
0.00 1578
19.24 1647
0.00 1655
Ethylbenzene 19.35
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 20.24
1657
1673
1673
1733
1734 Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.26
0.00 1769
20.85 1785
0.00 1824
0.00 1835
21.48 1839
21.56
21.89
21.76
21.95
22.45
22.50
22.82
23.01
1846
1874
1863
1880
1922
1926
1954
1971
23.14 1981
23.26 1992
23.78 2036
0.00 2054
0.00 2182
27.31 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
"146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
4895 0.09 UG/L
872 0.02 UG/L
Not Found UG/L
3176 0.02 UG/L
58599
136651
136651
42831
9218
Not Found UG/L
0.20 UG/L
0.27 UG/L
0.27 UG/L
0.17 UG/L
0.07 UG/L
Not Found UG/L
53163 0.19 UG/L
0 Not Found UG/L
0 Not Found UG/L
15733 0.10 UG/L
75225
12876
89129
30911
65351
121453
72737
70809
0.24
0.06
0.35
0.15
0.25
0.50
0.25
0.31
UG/L
UG/L
UG/L
UG/L.
UG/L
UG/L
UG/L
UG/L
38444 0.33 UG/L
103501 0.78 UG/L
66972 0.33 UG/L
Not Found UG/L
Not Found UG/L
21210 0.41 UG/L
Fit
190
981
883
338
827
602
992
995
996
926
903
123
960
280
685
914
969
959
970
993
934
980
968
971
977
976
964
585
185
962
Rf
0.000
0.284
0.282
0.000
0.858
0.000
1. 510
2. 64 9
2.649
1 . 3 05
0.701
0.000
1.470
0.000
0.000
0.855
1.673
1.234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01283.1A2
Data File: AE01283.MS
Name: AE01283
QUANT REPORT
Sample: Location: Comala-Madison Ave, SB15-L
ID File: 826AEC28.QCI
Page
Quant Time: 03/31/99 08:13
Injected at: 03/30/99 20:37
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/24/1999 by J. Conway, use 3.91 g
Last Calibration: 03/29/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.62
27.97
28.55
2366
2395
2445
225
128
180
Area
21986
88914
21261
Cone
0.43
0.79
0.39
Units
UG/L
UG/L
UG/L
Fit
951
987
925
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01355.1A2
Data File: AE01355.MS
Name: AE01355
QUANT REPORT
Sample: Location: 242 Washington St., SB16-A
/).ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:25
Injected at: 03/25/99 22:06
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.80 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.07 1203
21.16 1812
23.94 2050
4.54
0.00
0.00
6. 41
0.00
7.37
8.61
9.61
10.20
11.00
389
438
467
549
573
631
736
822
872
941
12.04 1030
0.00 1033
12.50 1069
0.00 1078
12.96 1109
13.26 1134
13.30 1138
13.62 1165
13.60 1164
14.69 1257
0.00 1291
0.00 1309
15.48 1325
16.21 1387
16.82 1440
17.16 1469
0.00 1492
96 2526733
95 1153665
10.00 UG/L
10.39 UG/L
10.36 UG/L 152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
717596
14317 0.22 UG/L
Not Found UG/L
Not Found UG/L
10886 0.58 UG/L
0 Not Found UG/L
17247 0.15 UG/L
1869
819301
8169
1267
0.04 UG/L
2.64 UG/L
0.08 UG/L
0.01 UG/L
4194 0.04 UG/L
0 Not Found UG/L
2833 0.03 UG/L
0 Not Found UG/L
4017 0.03 UG/L
11004
4817
24793
3520
8748
0.14 UG/L
0.06 UG/L
0.11 UG/L
0.04 UG/L
0.14 UG/L
0 Not Found UG/L
0 Not Found UG/L
2060
394 0
79285
13 9 92 3
0.02 UG/L
0.05 UG/L
0.26 UG/L
1.71 UG/L
Not Found UG/L
Fit
997
999
952
894
172
670
623
812
981
851
972
844
759
869
662
828
699
871
758
966
989
969
977
262
470
794
773
981
730
813
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0.455
. 0. 208
l. 228
0.386
0.393
0.432
0.000
0.406
0.000
0.537
0.302
0.316
0.897
0.355
0.255
0.000
0.000
0.327
0.340
1.195
0.324
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01355.1A2
Data File: AE01355.MS
Name: AE01355
Quant Time: 04/08/99 10:25
Injected at: 03/25/99 22:06
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-A
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 4.80 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.23
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.24
Bromoform 20.65
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.84
0.00
0.00
21.49
21.55
21.88
21.79
21.95
22.42
22.50
22.80
23.01
23.11
23.25
23.77
24.00
25.48
27.32
1520
1522
1555
1578
1646
1654
1656
1672
1672
1732
1733
1768
1784
1824
1835
1840
1845
1873
1866
1880
1920
1926
1952
1970
1979
1991
2036
2055
2182
2340.
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
22550
33380
155750
252180
252180
81464
35997
2878
94 32 3
81963
150510
16991
186858
93931
111078
161406
129870
137005
104105
129733
167260
119784
9442
53699
Cone Units
Not Found UG/L
0.34 UG/L
Not Found UG/L
Not Found UG/L
0.18 UG/L
Not Found UG/L
0.47 UG/L
0.42 UG/L
0.42 UG/L
0.30 UG/L
0.25 UG/L
0.04 UG/L
0.30 UG/L
Not Found UG/L
Not Found UG/L
0.47 UG/L
0.41 UG/L
0.06 UG/L
0.65 UG/L
0.39
0.36
0.55
0.39
0.52
0.72
0.92
0.66
0.90
0.52
0.70
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
347
974
259
683
94 6
776
992
996
996
721
941
719
983
4 04
431
955
983
961
953
986
958
988
966
971
975
972
991
806
550
961
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.266
1.246
0.000
0.000
0.685
1. 439
1.099
1.138
0.961
1.209
1.169
1.305
1.051
0.575
0.560
1.004
0.526
0.072
0.303
Operator ID: MC
Output File: AE01355.1A2
Data File: AE01355.MS
Name: AE01355
QUANT REPORT
Sample: Location: 242 Washington St., SB16-A
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:25
Injected at: 03/25/99 22:06
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.80 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound. is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.58 2362
27.97 2395
28.53 2444
225
128
180
Area
1834 9
85745
22966
Cone Units
0.23 UG/L
0.58 UG/L
0.30 UG/L
Fit
980
987
975
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01356.1A2
Data File: AE01356.MS
Name: AE01356
QUANT REPORT
Sample: Location: 242 Washington St., SB16-B
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:29
Injected at: 03/25/99 22:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 3.58 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
10) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
2:2) 107-06-2
23) 79-01-6
21) 78-87-5
2S) 74-95-3
2G) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene 28)
2 9) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.07 1204
21 .18 1813
23.95 2051
4.54
0.00
0.00
6.42
0.00
7.36
0.00
9.62
389
438
466
549
572
630
737
823
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1143
13.63 1166
0.00 1166
14.70 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1440
0.00 1464
0.00 1494
96 2465243
95 1126005
152 645078
10.00 UG/L
10.39 UG/L
9.55 UG/L
85
47
61
96
49
101
96
49
61
63
61
97
49
03
97
75
117
78
62
130
63
93
83
75
91
75
83
4838 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
7279 0.40 UG/L
Not Found UG/L
6360 0.06 UG/L
0 Not Found UG/L
830337 2. 75 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
19160 0.09 UG/L
0 Not Found UG/L
1019 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
82866 0.28 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
959
834
18
270
680
12
976
551
94 9
156
553
338
431
685
629
559
299
820
987
882
819
376
230
236
107
978
589
685
Rf
1.000
0. 44 0
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 227
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01356.1A2
Data File: AE01356.MS
Name: AE01356
Quant Time: 04/08/99 10:29
Injected at: 03/25/99 22:46
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 3.58 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
3 3)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
4 7)
4 8)
49)
50)
51)
52)
53)
54)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-l
* Compound is ISTD
Compound R.T. Scan~ Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.25
0.00
19.38
1,3-Dimethylbenzene (m-Xylene 19.55
1,4-Dimethylbenzene (p-Xylene 19.55
1,2-Dimethylbenzene (a-Xylene 20.25
1520
1522
1555
1578
1648
1655
1659
1673
1673
1734
1728
1769
1786
1824
1835
1836
1646
1675
1868
1884
1916
1927
1951
1963
Styrene 20.18
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.86
0.00
0.00
21.44
21.56
0.00
21.82
22.00
22.38
22.50
22.79
22.93
23.15 1982
23.27 1993
23.77 2036
24.00 2055
0.00 2182
27.31 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
1535 0.02 UG/L
Not Found UG/L
Not Found UG/L
8193 0.05 UG/L
0 Not Found UG/L
144743 0.44 UG/L
224833 0.39 UG/L
224833
88489
10795
0.39 UG/L
0.33 UG/L
0.08 UG/L
Not Found UG/L
82488 0.27 UG/L
0 Not Found UG/L
0 Not Found UG/L
40584 0.24 UG/L
65596 0. 24 UG/L
Not Found UG/L
153413 0.55 UG/L
1116
31725
323187
44681
49438
0. 0 0 UG/L
0.11 UG/L
1.12 UG/L
0.14 UG/L
0.19 UG/L
54983 0.39 UG/L
94453 0.69 UG/L
82166 0.33 UG/L
58488 0.45 UG/L
Not Found UG/L
11886 0.16 UG/L
Fit
394
860
203
284
834
519
985
991
994
894
942
424
929
368
524
785
955
900
975
967
902
994
822
957
971
966
951
744
858
Rf
0.000
0.266
0.000
0.000
0. 717
0.000
1.320
2.360
2.360
1.076
0.576
0.000
l. 246
0.000
0.000
0.685
1.438
0.000
1.138
0.960
1. 209
1.168
1. 304
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Opera tot- ID: MC
Output File: AE01356.1A2
Data File: AE01356.MS
Name: AE01356
QUANT REPORT
Sample: Location: 242 Washington St., SB16-B
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:29
Injected at: 03/25/99 22:46
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. conway, use 3.58 g
Last Calibration: 03/25/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.67
27.97
28.58
2370
2396
2448
225
128
180
Area
27990
520764
21223
Cone Units
0.37 UG/L
3.64 UG/L
0.28 UG/L
Fit
961
991
905
Rf
0.310
0.580
0.304
Operator ID' MC
Output File, AE01357.1A2
Data File, AE01357.MS
Name, AE01357
QUANT REPORT
Sample, Location, 242 Washington St., SB16-C
ID File, 826AEC25.QCI
Page
Quant Time' 04/08/99 10,JO
Injected at' 03/25/99 23,26
Dilution Factor, 1·. 00
Instrument ID, 20701-1284
Comment' Sampling·, 02/26/1999 by J. Conway, use 5.19 g
Last Calibration, 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74·95-3
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
26) 75-27-4 Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 09,34
R.T. Scan# Q ion
14.06
21.16
23.94
4.55
0.00
0.00
6. 41
6.72
7.37
1204
1813
2051
389
438
467
549
575
631
0.00 737
9.61 823
0.00 874
0.00 951
0.00 1033
0.00 1031
12.51 1071
0.00 1079
0.00 1112
0.00 1136
0.00 1137
13.62 1167
0.00 1165
0.00 1259
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.81 1440
0.00 1464
17.42 1492
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
9l
75
83
Area Cone Units
2432134
1149852
660364
4413
10.00 UG/L
10.76 UG/L
9.91 UG/L
0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
5722 0.32 UG/L
1062 0.09 UG/L
6235 0.06 UG/L
0 Not Found UG/L
835421 2.80 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2587 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
21829 0.10 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
51142 0.18 UG/L
0 Not Found UG/L
524 0.02 UG/L
Fit
998
999
953
836
183
616
739
905
982
163
941
129
750
581
636
742
595
641
427
863
995
875
588
180
277
4 08
363
984
556
725
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0. 047
0.455
0.000
l. 226
0.000
0.000
0.000
0.000
0. 406
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
0.000
0.000
0.000
1.195
0.000
0.122
Operator ID: MC
Output File: AE01357.1A2
Data File: AE01357.MS
Name: AE01357
QUANT REPORT
Sample: Location: 242 Washington St., SB16-C
ID File: 826AEC25.QCI
Page 2
Quant Time: 04/08/99 10:30
Injected at: 03/25/99 23:26
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.19 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
0.00 1556
0.00 1579
0.00 1648
0.00 1656
19.37 1659
1,3-Dimethylbenzene (m-Xylene 19.54 1674
1,4-Dimethylbenzene (p-Xylene 19.54 1674
1,2-Dimethylbenzene (a-Xylene 20.24 1734
Styrene
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.30 1739
0.00 1770
20.84 1785
0.00 1825
0.00 1836
0.00 1839
21.59 1849
21.78 1866
21.76 1864
21.96 1881
22.40 1919
22.50 1927
22.82 1955
23.01 1971
23.21 1988
23.21 1988
23.73 2033
24.00 2056
0.00 2183
27.32 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
8151
Not Found UG/L
0. 13 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
92334
1224 94
1224 94
44447
13315
Not Found UG/L
0.29 UG/L
0.21 UG/L
0.21 UG/L
0.17 UG/L
0.10 UG/L
0 Not Found UG/L
70945 0.23 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
65614
124590
113129
36738
49507
117725
80934
72068
15792
15792
82611
55765
24828
0. 19 UG/L
0.47 UG/L
0.41 UG/L
0.16 UG/L
0.17 UG/L
0.41 UG/L
0.26 UG/L
0.28 UG/L
0. 11 UG/L
0.12 UG/L
0.34 UG/L
0.44 UG/L
Not Found UG/L
0.34 UG/L
Fit
268
972
488
529
801
558
978
983
985
760
881
680
918
250
515
902
941
914
909
954
937
966
816
935
976
971
878
766
389
924
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.000
1.438
1.100
1.137
0.960
1.209
1 . 16 9
1.304
1.051
0.575
0.559
1.004
0 .. 526
0.000
0.303
Operator ID: MC
Output File: AE01357.1A2
Data File: AE01357.MS
Name: AE01357
QUANT REPORT
Sample: Location: 242 Washington St., SB16-C
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:30
Injected at: 03/25/99 23:26
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.19 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.63 2367 225 25339 0.34
62) 91-20-3 Naphthalene 27.97 2396 128 260615 1.84
63) 82-61-6 1,2,3-Trichlorobenzene 28.58 2448 180 16293 0.22
* Compound is ISTD
~·
h
Units Fit Rf
--------
UG/L 936 0.310
UG/L 990 0.583
UG/L 917 0.304
'·
Operator ID: Me
Output File: AE01358.1A2
Data File: AE01358.MS
Name: AE01358
QUANT REPORT
Sample: Location: 242 Washington St SB16-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:24
Injected at: 03/30/99 11:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.03 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
13)
14)
15)
16)
17)
18)
19)
20)"
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.05
21.16
23.93
4.55
0.00
0.00
6.40
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
12.49
0.00
0.00
0.00
0.00
13.62
0.00
14.68
0.00
0.00
0.00
0.00
16.82
0.00
0.00
1204
1813
2051
390
438
467
54 9
580
631
737
823
875
943
1034
1032
1070
1079
1113
1137
1137
1167
1165
1258
1292
1310
1328
1390
1441
1465
1495
96
95
152
85
47
62
96
.49
1782174
851348
547415
4342
10.00
10.33
10.30
0.07
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
0 Not Found UG/L
7157 0.50 UG/L
Not Found UG/L
101 6261 0.07 UG/L
96 Not Found UG/L
49 1114420 6.47 UG/L
61 Not Found UG/L
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
1453 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
12509 0.06 UG/L
0 Not Found UG/L
780 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
18124 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
952
869
39
488
724
850
973
665
992
852
666
563
708
717
177
471
582
916
991
903
809
218
77
467
683
988
610
812
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.967
0.000
0.000
0.000
0.000
0.486
0.000
0.000
0.000
0.000
1.098
0.000
0.291
0.000
0.000
0.000
0.000
1 . 3 6 9
0.000
0.000
Operator ID: MC
Output File: AE01358.1A2
Data File: AE01358.MS
Name: AE01358
QUANT REPORT
Sample: Location: 242 Washington St SB16-D
ID File: 826AEC28.QCI
Page 2
Quant Time: 03/30/99 18:24
Injected at: 03/30/99 11:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.03 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
3 9)
40)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
41) 100-42-5
42) 75-25-2
43) 96-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 96-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1524
0.00 1556
0.00
19.23
0.00
19.34
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (o-Xylene 20.22
1580
1648
1657
1657
1673
1673
1733
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.23 1734
0.00 1771
20.84 1786
0.00 1825
0.00 1837
0.00 1840
21.55 1847
21.90 1877
21.80 1868
21.94 1880
22.41 1920
22.50 1928
22.80 1954
23.00 1971
23.12 1981
23.26 1993
23.77 2037
0.00 2056
0.00 2184
27.30 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
4411 0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
2839 0.02 UG/L
0 Not Found UG/L
65498 0.24 UG/L
100041
100041
34192
1264 7
0.21 UG/L
0.21 UG/L
0.15 UG/L
0. 10 UG/L
0 Not Found UG/L
50453 0.19 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
68811 0.23 UG/L
14229
173099
35721
73472
104201
74076
73294
15919
115503
54392
0.06 UG/L
0.72 UG/L
0.18 UG/L
0.30 UG/L
0.46 UG/L
0.27 UG/L
0.34 UG/L
0.14 UG/L
0.92 UG/L
0.28 UG/L
0 Not Found UG/L
Not Found UG/L
19408 0.39 UG/L
Fit
90
978
564
616
707
277
975
995
995
724
936
326
940
178
674
865
911
960
961
978
880
948
920
950
978
968
960
645
59
917
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2.649
2. 64 9
1.305
0.701
0.000
1. 470
0.000
0.000
0.000
1. 673
1 . 2 34
1.354
1.120
1.386
1. 277
1. 530
1.224
0.620
0.703
1.075
0.000
0.000
0.276
Opet"ator ID: MC
Output File: AE01358.1A2
Data File: AE01358.MS
Name: AE01358
QUANT REPORT
Sample: Location: 242 Washington St SB16-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:24
Injected at: 03/30/99 11:01
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.03 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.61 2366
27.95 2395
28.55 2447
225
128
180
Area
20588
55317
19124
Cone Units
0.43 UG/L
0.52 UG/L
0.37 UG/L
Fit
969
986
908
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01359.1A2
Data File: AE01359.MS
Name: AE01359
QUANT REPORT
sample: Location: 242 Washington St., SB16-E
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:31
Injected at: 03/26/99 05:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.57 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound
1) *107-06-2 Fluorobenzene
2)
3)
4)
5)
4-Bromofluorobenzene (SG)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
·cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethane
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
2 9)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.96 2051
96 2406459 10.00 UG/L
4.56 390
0.00 438
5.44 466
6.43 551
6.69 573
7.38 632
8.62 737
9.62 823
10.20 872
10.99 940
12.06 1032
0.00 1040
12.50 1069
12.60 1078
12.98 1111
13.25 1134
13 .. 28
13.64
13.61
14.69
15.07
15.27
15.49
1136
1167
1164
1257
1290
1307
1326
16.23 1389
16.82 1440
17.16 1469
17.47 1495
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
731753 6.89 UG/L
471462 7.15 UG/L
22491 0.36 UG/L
2152
13085
1158
314 38
7659
811263
194 39
5478
11614
Not Found UG/L
0.29 UG/L
0.74 UG/L
0.10 UG/L
0.29 UG/L
0.15 UG/L
2.75 UG/L
0.21 UG/L
0.06 UG/L
0.11 UG/L
0 Not Found UG/L
7261 0.07 UG/L
9968 0.10 UG/L
11319 0.09 UG/L
28318 0.39 UG/L
11377
46204
10645
22322
4289
4086
6594
10736
122370
1318 92
4707
0.15
0.21
0.13
0.36
0.12
0.12
0.08
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
0.13 UG/L
0.43 UG/L
1. 6 9 UG/L
0.16 UG/L
Fit
998
998
954
923
777
676
851
986
966
961
981
94 9
980
828
798
924
970
889
974
994
991
974
548
903
859
932
982
915
871
Rf
1.000
0.442
0.275
0.258
0.000
0.032
0.074
0. 04 7
0. 4 55
0.208
1.227
0.386
0.393
0.432
0.000
0.406
0.434
0.537
0.303
0.316
0.897
0.355
0.256
0.149
0.14 7
0.327
0. 340
1.195
0.324
0.122
QUANT REPORT Page 2
Operator ID' MC
Output File' AE01359.1A2
Data File' AE01359.MS
Name, AE01359
Quant Time: 04/08/99 10:31
Injected at: 03/26/99 05:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-E
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 4.57 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
SO)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-99-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound i~ ISTD
Compound R.T. Scan# Q ion
1,3-Dich1oropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
17.74 1519
17.79 1523
18.18 1556
18.44
19.24
19.35
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (o-Xylene 20.24
Styrene 20.27
Bromoform 20.67
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylben~ene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.85
0.00
0.00
21.53
21.56
21.79
21.81
21.97
22.44
22.50
22.82
23.01
23.11
23.26
23.77
23.98
0.00
27.32
1579
1647
1656
1657
1672
1672
1733
1735
1769
1785
1824
1835
1843
1846
1866
1867
1881
1921
1927
1954
1971
1979
1992
2036
2054
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
5677
49079
5964
6972
77862
10143
293921
399152
399152
175008
46638
12684
196043
134 5 64
254307
292202
305910
223650
220698
271179
306078
285606
200163
215770
34 64 59
166361
127795
Cone Units
0.25 UG/L
0.77 UG/L
0.12 UG/L
0.14 UG/L
0.45 UG/L
0. 13 UG/L
0.93 UG/L
0.70 UG/L
0.70 UG/L
0.68 UG/L
0.34 UG/L
0.20 UG/L
0.65 UG/L
Not Found UG/L
Not Found UG/L
0.82 UG/L
0.73 UG/L
1.10 UG/L
1.12 UG/L
0.97 UG/L
0.76 UG/L
0.97 UG/L
0.97 UG/L
1.13 UG/L
1.45 UG/L
1.60 UG/L
1.44 UG/L
1.32 UG/L
Not Found UG/L
1.76 UG/L
Fit
824
983
811
84 9
958
894
992
995
996
919
920
883
995
653
613
987
989
976
958
993
973
989
992
975
984
984
994
842
390
982
Rf
0.093
0.266
0.214
0. 213
0.718
0.318
1. 321
2.360
2.360
1.077
0.576
0.266
1.247
0.000
0.000
0.686
1.439
1.101
1.139
0.962
1. 210
1.168
1.306
1.051
0.575
0.560
1.002
0.526
0.000
0.301
Operator ID: Me
Output File: AE01359.1A2
Data File: AE01359.MS
Name: AE01359
QUANT REPORT
Sample: Location: 242 Washington St., SB16-E
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:31
Injected at: 03/26/99 05:23
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.57 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61} 87-68-3
62} 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.63 2367
27.97 2395
28.56 2446
225
128
180
Area
114446
111130
102566
Cone Units
1.55 UG/L
0.79 UG/L
1.41 UG/L
Fit
983
983
971
Rf
0.307
0.585
0.303
Operator ID: MC
Output File: AE01360.1A2
Data File: AE01360.MS
Name: AEOl360
QUANT REPORT
Sample: Location: 242 Washington St., SB16-F
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:32
Injected at: 03/26/99 06:03
Dilution Factor: 1. oo
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway. use 3.99 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
271
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.04 1203
21.16 1813
23.94 2051
4.56 390
0.00 438
0.00 466
6.41 548
0.00 573
7.37 631
0.00 737
9.61 823
0.00
0. 00 ·'
0.00
0.00
0.00
12.57
0.00
0.00
0.00
13.62
0.00
14.68
874
943
1033
1033
1069
1077
1112
1136
1147
1166
1165
1257
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.82 1440
17.01 1457
0.00 1494
96 2709809 10.00 UG/L
95 965212 8.08 UG/L
152 570457 7.68 UG/L
85 4580 0.07 UG/L
47 Not Found UG/L
61 Not Found UG/L
96 1784 0.09 UG/L
4 9 Not Found UG/L
101 7099 0.06 UG/L
96 Not Found UG/L
49 875722 2.63 UG/L
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
2546 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
16032 0.07 UG/L
Not Found UG/L
897 0.01 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
61186 0.19 UG/L
722 0.01 UG/L
Not Found UG/L
Fit
998
1000
950
838
785
118
984
608
959
434
583
43
497
484
759
667
449
918
982
882
846
304
475
353
231
981
704
640
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 228
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.323
0.000
Operator ID: MC
Output File: AE01360.1A2
Data File: AE01360.MS
Name: AE01360
QUANT REPORT
Sample: Location: 242 washington St., SB16-F
ID File: 826AEC25.QCI
Quant Time:
Injected at:
Dilution Factor:
Instrument ID:
Comment: Sampling: 02/26/1999 by J. Conway, use 3.99 g
Page 2
04/08/99 10:32
03/26/99 06:03
1. 00
20701-1284
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
3 7)
38)
39)
4 0)
41)
42)
4 3)
44)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
45) 96-18-4
46) 108-86-1
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
59) 96-12-8
60) 120-82-1
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.22
Styrene 20.23
1556
1579
1643
1656
1658
1672
1672
1732
1733
1770
1784
1825
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.83
0.00
0.00 1836
0.00 1841
21.56
21.91
21.81
21.91
22.44
22.50
22.79
23.00
23.18
23.25
23.76
23.98
184 7
1877
1868
1877
1922
1927
1952
1970
1986
1992
2035
2055
0.00 2183
27.30 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
• Compound is ISTD
Area Cone Units
Not Found UG/L
4837 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
124083 0.35 UG/L
177087
177087
68772
18554
0.28 UG/L
0.28 UG/L
0.24 UG/L
0.12 UG/L
Not Found UG/L
37603 0.11 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
103734
78114
122682
73926
97124
77955
99705
86177
64970
70596
70003
91350
0.27
0.26
0.40
0.28
0.30
0.25
0.28
0.30
0.42
0.47
0.26
0.64
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
24558 0.30 UG/L
Fit
459
891
570
264
746
602
978
988
986
711
906
593
946
141
519
877
94 3
94 5
935
970
915
937
830
939
981
973
979
779
461
922
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.245
0.000
0.000
0.000
1.438
1.100
1.137
0. 961
1.209
1.169
1.304
1.051
0.575
0.560
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01360.1A2
Data File: AE01360.MS
Name: AE01360
QUANT REPORT
Sample: Location: 242 Washington St., SB16-F
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:32
Injected at: 03/26/99 06:03
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 3.99 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2366
27.94 2394
28.55 2446
225
128
180
Area
31916
77174
26352
Cone Units
0.38 UG/L
0.49 UG/L
0.32 UG/L
Fit
961
983
976
Rf
0.310
0.586
0 . 3 04
Operator ID: MC
Output File: AE01361.1A2
Data File: AE01361.MS
Name: AE01361
QUANT REPORT
Sample: Location: 242 Washington St., SB16-G
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:33
Injected at: 03/26/99 06:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.42 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.96 2051
96 2256574 10.00 UG/L
9.50 UG/L
9.27 UG/L
0. 09 UG/L 4.54
0.00
0.00
6. 42
6.72
7. 37
0.00
9.61
389
438
466
550
576
631
737
822
0.00 874
0.00 942
0.00 1033
0.00 1031
0.00 1069
0.00 1078
0.00 1111
0.00 1136
0.00 1137
13.62 1166
13.62 1165
14.69 1257
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1439
0.00 1464
0.00 1500
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
943059
573155
5014
Not Found UG/L
0 Not Found UG/L
13540
1274
6520
836829
21037
2432
174 3
0.81 UG/L
0.12 UG/L
0.06 UG/L
Not Found UG/L
3. 03 .UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.10 UG/L
0.03 UG/L
0.03 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
61290
Not Found UG/L
0.23 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
957
84 9
0
0
660
808
986
445
977
343
623
585
658
64 0
522
794
661
910
990
896
859
252
435
308
550
982
652
755
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.047
0.455
0.000
1.223
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.355
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Ope>:ator ID: MC
Output File: AE01361.1A2
Data File: AE0136l.MS
Name: AE01361
Quant Time: 04/08/99 10:33
Injected at: 03/26/99 06:42
Dilution Factor:' 1.00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-G
ID File: 826AEC25.QCI
Com~ent: Sampling: 02/26/1999 by J. Conway, use 4.42 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
3~) 127-18-4
33)
34)
35)
36)
37)
38)
39)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43)
44)
45)
46)
47)
48)
49)
so)
51)
52)
53)
54)
55)
56)
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00
0.00
19.24
0.00
19.34
1,3-Dimethylbenzene (m-Xylene 19.51
1,4-Dimethylbenzene (p-Xylene 19.51
1555
1578
1647
1655
1656
1671
1671
1,2-Dimethylbenzene (a-Xylene 20.23 1732
Styrene 20.27 1736
Bromoform 20.64 1767
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
.4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.84
0.00
0.00
21.54
21.55
0.00
21.74
21.95
22.36
22.53
22.81
23.01
23.14
23.24
1784
1824
1835
1844
1845
1874
1861·
1880
1915
1929
1952
1970
1981
1990
23.77 2036
24.03 2058
0.00 2175
27.29 2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
* Compound is ISTD
Area Cone Units
0 Not Found UG/L
3780 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
10309 0.06 UG/L
0 Not Found UG/L
107022 0.36 UG/L
152640
152640
50501
16822
1510
73355
0.29 UG/L
0.29 UG/L
0.21 UG/L
0.13 UG/L
0.03 UG/L
0.26 UG/L
0 Not Found UG/L
Not Found UG/L
24234 0.16 UG/L
73717 0.23 UG/L
0 Not Found UG/L
59941 0.23 UG/L
49007
254 90
74267
104859
81863
90297
96939
0.23 UG/L
0.09 UG/L
0.28 UG/L
0. 36 UG/L
0.35 UG/L
0.70 UG/L
0.77 UG/L
90832 0.40 UG/L
20694 0.17 UG/L
Not Found UG/L
20050 0.29 UG/L
Fit
531
918
617
293
84 9
460
977
989
991
724
914
737
949
230
616
902
960
950
897
955
928
938
766
928
966
977
974
808
611
945
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.266
1. 246
0.000
0.000
0.685
1.438
0.000
1.137
0.960
1. 209
1. 16 9
1.305
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01361.1A2
Data File: AE01361.MS
Name: AE01361
QUANT REPORT
sample: Location: 242 Washington St., SB16-G
ID File: 826AEC25.QCI
Page 3
Quant Time: 04/08/99 10:33
Injected at: 03/26/99 06:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.42 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2365
27.95 2394
28.54 2445
225
128
180
Area
26854
4 9408
28885
Cone Units
0. 38 UG/L
0.38 UG/L
0.42 UG/L
Fit
971
983
938
Rf
0.310
0.586
0.304
QUANT REPORT Page
Operator ID: MC
Output File: AE01362.1A2
Data File: AE01362.MS
Name: AE01362
Sample: Location: 242 Washington St., SB16-H
ID File: 826AEC25.QCI
Quant Time: 04/08/99 10:34
Injected at: 03/26/99 07:22
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 5.74 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dich1orobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1, 1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichioropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1204
21.15 1812
23.94 2051
96 2732077 10.00 UG/L
3. 15 UG/L
3.19 UG/L.
0. 44 UG/L 4.57
0.00
5.46
6.44
0.00
7. 38
8.60
9.61
10.18
10.99
391
438
467
551
573
631
737
823
872
941
12.05 1032
0.00 1039
12.48 1069
12.59 1078
12.99 1112
13.26 1135
13.29 1138
13.62 1166
13.59 1164
14.68 1257
15.06 1290
15.27 1308
15.47 1325
16.21 1388
16.82 1440
17.14 1468
17.43 1493
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
381431
239350
30787
0 Not Found UG/L
1661 0.19 UG/L
4271 0.21 UG/L
44029
10590
816995
24180
5625
11305
Not Found UG/L
0. 35 UG/L
0.19 UG/L
2.43 UG/L
0.23 UG/L
0.05 UG/L
0.10 UG/L
0 Not Found UG/L
54 97
7839
11294
31888
13056
43756
6148
22153
3285
2303
4380
8152
118500
118916
2615
0.05 UG/L
0. 07 UG/L
0. 0 8 UG/L
0.39 UG/L
0.15 UG/L
0.18 UG/L
0.06 UG/L
0.32 UG/L
0.08 UG/L
0.06 UG/L
0.05 UG/L
0.09 UG/L
0.36 UG/L
1.35 UG/L
0.08 UG/L
Fit
998
999
94 5
907
319
928
623
519
991
977
935
970
914
973
793
911
886
982
884
983
995
985
975
440
899
811
918
983
856
840
Rf
1.000
0.444
0.275
0.258
0.000
0.032
0.074
0.000
0.455
0.208
1.231
0.387
0.393
0.432
0.000
0. 406
0.434
0.537
0.303
0.316
0.897
0.355
0.256
0.149
0.147
0.327
0.340
1.195
0.324
0.122
QUANT REPORT Page
Operator ID: MC
Output File: AE01362.1A2
Data File: AE01362.MS
Name: AE01362
Quant Time: 04/08/99 10:34
Injected at: 03/26/99 07:22
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-H
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 5.74 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
3 3)
34)
35)
3 6)
37)
38)
39)
4 0)
41)
42)
4 3)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
sal
59)
60)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.77 1522
18.18
18.44
19.22
19.33
19.35
1,3-Dimethylbenzene (m-Xylene 19.51
1,4-Dimethylbenzene (p-Xylene 19.51
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 20.23
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.64
20.83
0.00
0.00
21.49
21.55
21.79
21 . 8 0
21.95
22.41
22.48
22.80
23.01
23.10
23.25
23.77
23.97
0.00
27.30
1558
1579
1647
1656
1657
1672
1672
1733
1733
1768
1784
1825
1837
1841
1846
1867
1868
1881
1920
1926
1953
1971
1979
1992
2036
2054
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Cone Units
0 Not Found UG/L
37873 0.52 UG/L
1487
3895
54286
5156
231318
315193
315193
107346
52163
2774
157308
0.03 UG/L
0.07 UG/L
0.28 UG/L
0.06 UG/L
0.64 UG/L
0.49 UG/L
0. 4 9 UG/L
0.37 UG/L
0.33 UG/L
0.04 UG/L
0.46 UG/L
0 Not Found UG/L
0 Not Found UG/L
94069 0.50 UG/L
215898 0.55 UG/L
209636
237300
1"51311
156109
189937
209879
172363
141803
149028
188388
107321
0.70 UG/L
0.76 UG/L
0.58 UG/L
0.47 UG/L
0.60 UG/L
0.59 UG/L
0.60 UG/L
0.90 UG/L
0.98 UG/L
0.69 UG/L
0.75 UG/L
0 Not Found UG/L
64380 0.78 UG/L
Fit
676
984
772
717
975
891
992
996
997
836
939
785
994
504
257
977
990
963
953
987
957
990
983
970
984
978
993
902
568
983
Rf
0.000
0.266
0.214
0. 213
0.717
0.318
1.320
2.360
2.360
1.076
0.576
0.266
1.247
0.000
0.000
0.685
1.439
1.101
1.138
0.961
1. 210
1.169
1.305
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID' MC
Output File' AE01362.1A2
Data File' AE01362.MS
Name, A£01362
QUANT REPORT
Sample, Location' 242 Washington St., SB16-H
ID File: 826AEC25.QCI
Page
Quant Time' 04/08/99 10,34
Injected at, 03/26/99 07,22
Dilution Factor' 1.00
Instrument ro, 20701-1284
Comment' Sampling: 02/26/1999 by J. Conway, use 5.74 g
Last Calibration' 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2366
27.96 2395
28.54 2446
225
128
180
Area
58008
117866
55386
Cone Units
0.69 UG/L
0. 74 UG/L
0.67 UG/L
Fit
984
990
970
Rf
0.309
0.585
0.304
Operator ID: MC
Output File: AE01363.1A2
Data File: AE01363.MS
Name: AE01363
QUANT REPORT
Sample: Location: 242 Washington St., SB16-I
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:34
Injected at: 03/26/99 08:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.29 g
Last Calibration: 03/25/99
Compound
1) 0 107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.05 1203
21.16 1812
23.96 2051
4.57
0.00
5.45
6.42
0.00
7.37
391
438
466
550
572
631
8.61 736
9.61 822
10.18 871
10.98 939
12.04 1031
0.00 1031
12.48 1068
12.58 1077
12.98 1111
13.25 1134
13.28 1137
13.62 1166
13.60 1164
14.68 1257
15.06 1289
15.28 1308
15.49 1326
16.20 1387
16.82 1440
17.17 1469
17.44 1493
96 2792870 10.00 UG/L
7.62 UG/L
6.91 UG/L
0.58 UG/L
95 937804
152 529240
85
47
61
96
49
101
96
49
61
63
·61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
41465
Not Found UG/L
i469 0.17 UG/L
4437 0.21 UG/L
Not Found UG/L
68204 0.54 UG/L
15881
928285
40023
8373
18502
0.27 UG/L
2. 71 UG/L
0.37 UG/L
0.08 UG/L
0.15 UG/L
0 Not Found UG/L
10868
13279
19493
55780
21458
61771
13388
41380
5688
4454
8735
16651
186029
228033
4959
0.10 UG/L
0.11 UG/L
0. 13 UG/L
0.66 UG/L
0.24 UG/L
0.25 UG/L
0.14 UG/L
0.58 UG/L
0.14 UG/L
0.11 UG/L
0.10 UG/L
0.18 UG/L
0.56 UG/L
2.52 UG/L
0.15 UG/L
Fit
998
999
94 9
926
301
941
744
241
988
989
958
987
901
977
939
896
938
984
867
970
994
992
977
627
980
885
939
982
904
914
Rf
1.000
0 .'441
0.275
0.258
0.000
0.032
0.074
0.000
0.455
0.208
1.227
0.387
0.393
0.432
0.000
0.406
0.434
0.537
0.303
0.316
0.897
0.355
0.256
0 .14 9
0. 14 7
0.327
0.340
1.196
0.325
0.122
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01363.1A2
Data File: AE01363.MS
Name: AE01363
Quant Time: 04iOB/99 10:34
Injected at: 03/26/99 08:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-l
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 4.29 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-B
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1, 3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.78 1522
18.18 1556
18.44
19.23
19.32
19.35
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene (p-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.24
Styrene 20.24
Bromoform 20.67
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.83
0.00
21.43
21.50
21.53
21.96
21.80
21.96
22.42
22.50
22.80
23.00
23.11
23.26
23.77
23.97
0.00
27.32
1578
1646
1654
1656
1672
1672
1733
1733
1770
1784
1824
1835
1841
1844
1880
1867
1880
1920
1926
1952
1970
1979
1992
2035
2053
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
82151 1.11 UG/L
4117 0.07 UG/L
8529
99179
12680
269836
550277
550277
0.14 UG/L
0.50 UG/L
0.14 UG/L
0.73 UG/L
0.83 UG/L
0.83 UG/L
187939 0.63 UG/L
60044 0.37 UG/L
7793 0.11 UG/L
247494 0.71 UG/L
Not Found UG/L
10030 0.13 UG/L
136240
365179
2 794 95
346907
279495
243040
268236
354984
339945
201792
227903
404944
168265
126570
0. 71
0.91
0. 91
1. 09
1. 04
0.72
0.82
0.97
1.16
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1.26 UG/L
1.46 UG/L
1.45 UG/L
1.15 UG/L
Not Found UG/L
1.50 UG/L
Fit
539
985
824
877
964
891
991
996
995
910
917
863
995
598
729
991
991
964
966
989
959
990
991
975
971
982
997
858
4 09
985
Rf
0.000
0.266
0.214
0. 213
0.718
0.318
1.321
2.360
2.360
1.077
0.576
0.266
1.247
0.000
0.286
0.686
1.439
1.101
1.139
0.962
1.210
1.168
1.306
1.051
0.575
0.560
1.002
0.526
0.000
0.302
Operator ID: MC
Output File: AE01363.1A2
Data File: AE01363.MS
Name: AE01363
QUANT REPORT
Sampl~: Location: 242 Washington St., S816-I
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:34
Injected at: 03/26/99 08:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.29 g
. Last calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2365
27.96 2394
28.57 2446
225
128
180
Area
106952
94073
98590
Cone Units
1.25 UG/L
0.58 UG/L
1.17 UG/L
Fit
988
991
979
Rf
0.307
0.586
0.303
Operator ID: MC
Output File: AE01364.1A2
Data File: AE01364.MS
Name: AE01364
QUANT REPORT
Sample: Location: 242 Washington St., SB16-J
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:35
Injected at: 03/26/99 08:40
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.68 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
22) 107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane ·
Dibromomethane
Bromodichloromethane
23)
24)
25)
26)
27)
28)
2 9)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.06
21.16
23.94
4.55
0.00
5.47
6.41
6.76
7.38
8.60
9.61
10.20
11.00
12.06
0.00
12.50
12.58
12.99
13.24
13.30
13.62
1203
1812
2050
390
438
468
549
579
631
735
822
872
941
1032
1034
1069
1076
1111
1133
1138
1166
13.62 1165
14.69
0.00
15.29
15.50
16.22
16.82
17.15
17.44
1257
1296
1308
1326
1388
1439
1468
14 93
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
2304404
919533
579733
12861
321
8838
235
16853
4279
748926
15768
3704
9398
Cone
10.00
9.06
9.18
0.22
Units
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
0.04 UG/L
0.52 UG/L
0.02 UG/L
0.16 UG/L
0.09 UG/L
2.65 UG/L
0.18 UG/L.
0.04 UG/L
0.09 UG/L
0 Not Found UG/L
5731 0.06 UG/L
7034
6844
15462
5771
36423
5315
14221
1984
3840
8012
92369
117845
2421
0.07 UG/L
0.06 UG/L
0.22 UG/L
0.08 UG/L
0.18 UG/L
0.07 UG/L
0.24 UG/L
Not Found UG/L
0.06 UG/L
0.05 UG/L
0.10 UG/L
0.34 UG/L
1.58 UG/L
0.09 UG/L
Fit
999
999
952
882
0
908
658
876
985
94 9
951
957
853
922
871
885
828
938
783
941
996
969
975
562
855
785
923
984
718
847
Rf
1.000
0.441
0.275
0.258
0.000
0.032
0.074
0.047
0. 455
0.208
1.228
0.386
0.393
0.432
0.000
0. 4 06
0. 4 34
0.537
0.302
0.316
0.897
0.355
0.255
0.000
0. 14 7
0.327
0.340
1 . 195
0.324
0.122
Operator ID: MC
Output File: AE01364.1A2
Daca File: AE01364.MS
Name: AE01364
QUANT REPORT
Sample: Location: 242 Washington St., SB16-J
ID File: 826AEC25.QCI
Page 2
Quant Time: 04/08/99 10:35
Injected at: 03/26/99 08:40
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.68 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.78 1522
0.00 1555
18.42 1577
19.24 1647
19.33 1655
19.35 1656
38) 108-38-3
39) 106-42-3
40) 95-47-6
1,3-Dimethylbenzene (m-Xylene 19.53 1672
1,4-Dimethylbenzene (p-Xylene 19.53 1672
1,2-Dimethylbenzene (o-Xylene 20.26 1734
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
108-67-8 1,3,5-Trimethylbenzene
106-43-4 4-Chlorotoluene
98-06-6 · cert-Butylbenzene
95-63-6 1,2,4-Trimethylbenzene
135-98-8 sec-Butylbenzene
99-87-6 4-Isopropyltoluene
541-73-1 1,3-Dichlorobenzene
106-46-7 1,4-Dichlorobenzene
104-51-8 n-Butylbenzene
95-50-1 1,2-Dichlorobenzene
59) 96-12-8
60) 120-82-1
• Compound is ISTD
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1733
20.65 1768
20.83 1784
0.00 1824
0.00 1835
21.50 1841
21.55 1845
21.79 1866
21.81
21.94
22.44
22.50
22.80
23.02
23.11
23.26
23.77
23.99
1867
1879
1921
1926
1953
1971
1979
1991
2035
2054
0.00 2182
27.30 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
28131 0.46 UG/L
Noc Found UG/L
4683 0.10 UG/L
52364
5593
145958
312070
312070
106464
33668
2906
0.32 UG/L
0.08 UG/L
0.48 UG/L
0.57 UG/L
0.57 UG/L
0. 4 3 UG/L
0.25 UG/L
0.05 UG/L
155861 0.54 UG/L
Not Found UG/L
Not Found UG/L
105543 0.67 UG/L
167694 0.51 UG/L
190214 0.75 UG/L
230281
169497
147152
156286
188016
174332
137836
146098
211551
125959
0.88 UG/L
0.77 UG/L
0.53 UG/L
0.58 UG/L
0.63 UG/L
0.72 UG/L
l. 04 UG/L
1.13 UG/L
0.92 UG/L
1.04 UG/L
0 Not Found UG/L
75733 1. 09 UG/L·
Fit
579
984
529
867
954
869
993
995
996
867
894
812
993
465
356
971
991
938
955
988
944
980
972
974
985
979
990
790
497
977
RE
0.000
0.266
0.000
0. 213
0. 717
0. 318
1.320
2.360
2.360
1.077
0.576
0.266
1.247
0.000
0.000
0.686
1.439
1.101
1.138
0. 961
1.210
1.169
1.305
1.051
0.575
0.560
1.003
0.526
0.000
0. 3 02
Operator ID: MC
Output File: AE01364.1A2
Data File: AE01364.MS
Name: AE01364
QUANT REPORT
Sample: Location: 242 Washington St., SB16-J
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:35
Injected at: 03/26/99 08:40
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.68 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2365
27.94 2393
28.56 2446
225
128
180
Area
64 704
7094 7
65734
Cone Units
0.91 UG/L
0.53 UG/L
0.94 UG/L
Fit
975
981
973
Rf
0.308
0.586
0. 3 04
Operator ID, MC
Output File, AE01365.1A2
Data File, AE01365.MS
Name, AE01365
QUANT REPORT
Sample, Location, 242 Washington St., SB16-K
ID File, 826AEC25.QCI
Page
Quant Time, 04/08/99 10,36
Injected at, 03/26/99 09,20
Dilution Factor, 1. 00
Instrument IO, 20701-1284
Comment, Sampling, 02/26/1999 by J. Conway, use 4.42 g
Last Calibration' 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
Chloromethane 5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1, 1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1, 1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 08,34
R.T. Scan# Q ion Area Cone Units
14.05
21.15
23.93
4.56
0.00
0.00
6. 4 0
6.59
7.37
0.00
9.62
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.60
0.00
0.00
0.00
1203
1812
2050
391
438
466
548
564
631
737
823
874
944
1033
1033
1069
1079
1112
1136
1139
1165
1165
1259
1291
0.00 1309
0.00 1327
0.00 1390
16.81 1440
0.00 1464
0.00 1494
96 2387451
95 890133
152 56544 7
10.00 UG/L
8.46 UG/L
8.64 UG/L
0.06 UG/L 85 3686
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
0 Not Found UG/L
0 Not Found UG/L
2911 0.16 UG/L
417 0.04 UG/L
6030 0.06 UG/L
0 Not Found UG/L
722677 2.46 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
16261 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
54254 0.19 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
962
807
434
493
600
757
983
405
961
235
750
571
455
644
489
436
272
662
980
906
685
332
90
603
341
981
626
569
Rf
1.000
0.441
0.275
0. 258
0.000
0.000
0.074
0. 04 7
0.455
0.000
l. 231
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.000
0.000
·0.000
0.000
0.000
1.195
0.000
0.000
Operator ID: MC
Output File: AE01365.1A2
Data File: AE01365.MS
Name: AE01365
QUANT REPORT
Sample: Location: 242 Washington St., SB16-K
ID File: 826AEC25.QCI
Page 2
Quant Time: 04/08/99 10:36
Injected at: 03/26/99 09:20
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.42 g
La&t Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
3 3)
34)
35)
36)
3 7)
38)
3 9)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
40) 95-47-6
41) 100-42-5
42)
43)
44)
45)
46)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoechane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.76
0.00
0.00
0.00
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1521
1522
1556
1579
1645
1655
1657
1671
1671
1,2-Dimethylbenzene (a-Xylene 20.22 1732
Styrene 20.30 1739
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.78
0.00
0.00
21.4 9
21.52
21.84
21.79
21.95
22.42
22.49
22.81
23.01
23.12
23.23
23.78
23.98
0.00
27.25
1770
1780
1825
1836
1841
1843
1871
1867
1881
1921
1927
1954
1971
1980
1990
2037
2054
2183
2335
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
4091 0.06 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
93105 0.30 UG/L
83983
83983
32806
4631
0.15 UG/L
0.15 UG/L
0.13 UG/L
0.03 UG/L
Not Pound UG/L
41433 0.14 UG/L
Not Found UG/L
0 Not Found UG/L
15727 0.10 UG/L
33151
36252
91413
31402
73335
53464
41035
26596
17857
81218
58537
45814
0.10 UG/L
0.14 UG/L
0. 34 UG/L
0.14 UG/L
0.25 UG/L
0.19 UG/L
0.13 UG/L
0.11 UG/L
0.13 UG/L
0.61 UG/L
0.24 UG/L
0.37 UG/L
0 Not Found UG/L
20052 0.28 UG/L
Fit
510
930
552
236
753
713
980
976
980
84 3
875
470
928
530
588
776
887
925
958
975
916
908
730
971
964
970
94 9
786
374
926
Rf
0.000
0.266
0.000
0.000
0.000
0.000
l. 320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.685
1. 438
1.099
1.137
0.960
1. 209'
1.16 9
1.304
1.051
0.575
0.560
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01365.1A2
Data File: AE01365.MS
Name: AE01365
QUANT REPORT
Sample: Location: 242 Washington St., SB16-K
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:36
Injected at: 03/26/99 09:20
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 4.42 g
Last Calibration: 03/25/99
61) 87·68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.60 2365
27.93 2393
28.55 2446
225
128
180
Area
25749
40970
22095
co"nc Units
0.35 UG/L
0.29 UG/L
0.30 UG/L
Fit
983
977
918
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01366.1A2
Data File: AE01366.MS
Name: AE01366
QUANT REPORT
Sample: Location: 242 Washington St., SB16-L
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:37
Injected at: 03/26/99 10:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 8.52 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethane
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.07
21.18
23.97
4.56
0.00
0.00
6. 4 9
0.00
7.38
8.63
9.62
0.00
0.00
0.00
0.00
12.51
0.00
0.00
0.00
1204
1813
2052
390
430
468
556
576
632
738
823
874
946
1033
1033
1070
1078
1112
1136
0.00 1139
13.65 1168
13.63 1166
14.70 1258
0.00 1291
0.00 1309
0.00 1335
16.23 1389
16.83 1441
0.00 1464
0.00 1495
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2304832
1029191
651265
8288
10.00
10.15
10.31
0.14
UG/L
UG/L
UG/L
UG/L
Not Found UG/L
0 Not Found UG/L
2383 0.14 UG/L
0 Not Found UG/L
9551 0.09 UG/L
1455 0.03 UG/L
908786 3.23 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
1829 0.02 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
21344 0.10 UG/L
2481 0.03 UG/L
4039 0.07 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
1763 0.02 UG/L
88105 0.32 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
953
890
728
554
680
702
983
867
955
691
766
593
564
809
686
659
645
909
993
941
956
311
492
726
739
985
671
809
Rf
1.000
0.440
0.275
0.258
0.000
0.000
0.074
0.000
0. 455
0.208
1.221
0.000
0.000
0.000
0.000
0. 4 06
0.000
0.000
0.000
0.000
0.897
0.355
0.255
0.000
0.000
0.000
0.340
1.195
0.000
0.000
Operator ID: MC
Output File: AE01366.1A2
Data File: AE01366.MS
Name: AE01366
QUANT REPORT
Sample: Location: 242 Washington St., SB16-L
ID File: 826AEC25.QCI
Page 2
Quant Time: 04/08/99 10:37
Injected at: 03/26/99 10:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 8.52 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38)
39)
40)
41)
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00 1520
17.80 1524
18.23 1560
0.00 1578
19.25 1648
0.00 1658
19.36 1658
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 20.25
1673
1673
1734
1734 Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.25
0.00 1769
20.87 1786
0.00 1824
0.00 1835
21.53 1843
21.55 1845
21.82 1868
21.82 1868
21.98 1882
22.43 1921
22.51 1928
22.81 1954
23.03 1972
23.15 1982
23.27 1993
23.79 2037
24.07 2061
0.00 2186
27.32 2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
7850
242
Cone Units
Not Pound UG/L
0.13 UG/L
0.00 UG/L
0 Not Pound UG/L
14556 0.09 UG/L
0 Not Pound UG/L
86677 0.29 UG/L
112133
112133
4 03 98
25181
0.21 UG/L
0.21 UG/L
0.16 UG/L
0.19 UG/L
Not Found UG/L
56990 0.20 UG/L
0 Not Found UG/L
0 Not Pound UG/L
35127 0.22 UG/L
89012
114071
171082
58718
76284
66956
95079
81555
82428
81304
72328
20884
0.27 UG/L
0.45 UG/L
0.65 UG/L
0.27 UG/L
0.27 UG/L
0.25 UG/L
0.32 UG/L
0.34 ,UG/L
0.62 UG/L
0.63 UG/L
0.31 UG/L
0.17 UG/L
Not Found UG/L
26130 0.38 UG/L
Fit
533
973
846
633
888
814
985
990
990
BOO
932
552
94 9
366
693
952
972
968
930
979
935
961
803
938
981
981
973
726
643
94 7
Rf
0.000
0.266
0.214
0.000
0.717
0.000
1.320
2.360
2.360
1. 076
0.576
0.000
1.246
0.000
0.000
0.685
1.438
1.100
1.138
0.961
1. 209
1.169
1.305
1.051
0.575
0.560
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01366.1A2
Data File: AE01366.MS
Name: AE01366
QUANT REPORT
Sample: Location: 24~ washington St., SB16-L
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:37
Injected at: 03/26/99 10:00
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 0~/26/1999 by J. Conway, use 8.52 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,~,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.63 2366
27.98 2396
28.57 2447
225
128
180
Area
32056
61315
28664
Cone Units
0.45 UG/L
0.45 UG/L
0.41 UG/L
Fit
971
987
955
Rf
0.309
0.586
0.304
Operator ID: MC
Output File: AE01367.1A2
Data File: AE01367.MS
Name: AE01367
QUANT REPORT
Sample: Location: 242 Washington St., SB16-M
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:38
Injected at: 03/26/99 10:40
Dilution Factor: 1.00
Instrument ID: 20701-1284
comment: Sampling: 02/26/1999 by J. Conway, use 6.29 g
Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-B,:omofluo,:obenzene (SGI
3)
4)
5)
6)
7)
8)
9)
1,2-Dichlorobenzene-d4 (SGI
10)
11)
121
13)
14)
75-71-8
74-87-3
75-01-4
74-83-9
75~00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
22)
23)
24)
25)
26)
27)
28)
29)
3 0)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.95
4.55
0.00
0.00
6.52
0.00
7.37
0.00
9.62
0.00
0.00
0.00
2051
389
438
472
558
572
631
737
822
874
942
1033
0.00 1033
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1135
13.63 1166
0.00
14.71
0.00
0.00
0. 00
0.00
16.82
0.00
0.00
1165
1259
1291
1309
1327
1389
1440
1464
1494
96 2234316
95 1044314
10.00 UG/L
10.63 UG/L
10.22 UG/L 152
85
47
61
96
49
101
96
49
61
63
61
97.
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
625805
4360 0.08 UG/L
Not Found UG/L
Not Found UG/L
1283 0.08 UG/L
Not Found UG/L
5760 0.06 UG/L
0 Not Found UG/L
770431 2.81 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
17993 0.09 UG/L
Not Found UG/L
296 0.01 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
67158 0.25 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
953
805
0
557
760
588
982
518
938
584
157
198
412
575
562
695
889
979
880
876
185
324
613
388
983
623
693
Rf
1.000
0. 440
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.000
l. 226
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01367.1A2
Data File: AE01367.MS
Name: AE01367
Quant Time: 04/08/99 10:38
Injected at: 03/26/99 10:40
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 242 Washington St., SB16-M
ID File: 826AEC25.QCI
Comment: Sampling: 02/26/1999 by J. Conway, use 6.29 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
46) 108-86-1
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.79
0.00
0.00
19.23
0.00
19.31
1,3-Dimethylbenzene (m-Xylene 19.53
1,4-Dimethylbenzene lp-Xylene 19.53
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene
Bromoform
20.26
0.00
20.79
0.00
21.47
1520
1523
1556
1579
1646
1656
1653
1672
1672
1733
1735
1770
1780
1824
1839
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
21.52 1843
21.57
0.00
21.75
21.97
22.43
22.51
0.00
23.02
23.10
23.26
23.77
24.08
0.00
27.29
1847
1874
1862
1881
1920
1927
1954
1971
1978
1992
2035
2062
2188
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
2671 0.05 UG/L
Not Found UG/L
0 Not Found UG/L
7750 0.05 UG/L
Not Found UG/L
66815 0.23 UG/L
140654
140654
0.27 UG/L
0.27 UG/L
35674 0.15 UG/L
26681 0.21 UG/L
Not Found UG/L
23951 0.09 UG/L
Not Found UG/L
2411 0.04 UG/L
19074
72455
2484 9
2 9642
70217
48085
63845
61568
62029
54828
15273
16953
0.13 UG/L
0.23 UG/L
Not Found UG/L
0.10 UG/L
0.14 UG/L
0.26 UG/L
0. 18 UG/L
Not Found UG/L
0.27 UG/L
0.48 UG/L
0.50 UG/L
0.24 UG/L
0.13 UG/L
Not Found UG/L
0.25 UG/L
Fit
657
896
289
99
728
658
978
980
983
831
861
416
890
323
706
822
952
944
94 9
956
906
921
587
972
979
973
924
746
626
934
Rf
0.000
0.266
0.000
0.000
0.717
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1.245
0.000
0.286
0.685
1. 438
0.000
1.137
0. 960
1. 209
1 . 16 9
0.000
1.051
0.575
0.560
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE01367.1A2
Data File: AE01367.MS
Name: AE01367
QUANT REPORT
Sample: Location: 242 Washington St., SB16-M
ID File: 826AEC25.QCI
Page
Quant Time: 04/08/99 10:38
Injected at: 03/26/99 10:40
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/26/1999 by J. Conway, use 6.29 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.60 2363
27.96 2395
28.57 2447
225
128
180
Area
23113
45250
24090
Cone Units
0. 33 UG/L
0 . 3 5 UG/L
0.36 UG/L
Fit
964
986
939
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01329.1A2
Data File: AE01329.MS
Name: AE01329
QUANT REPORT Page
Quant Time: 03/29/99 11:12
Injected at: 03/29/99 03:47
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-A
ID File: 826AEC2B.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.94 g _I
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2 -Dichlorobenzene-d4 (SG)
4) 75-71-B Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
B) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane 26)
27)
28)
2 9)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14. 06
21.16
23.95
4.56
1203
1812
2051
390
0.00 438
0.00 463
6.45 552
0.00 572
7.37 631
8.61 736
9.62 823
0.00 874
0.00 948
0.00 1033
0.00 1033
0.00 1068
0.00 1078
0.00 1112
0.00 1136
0.00 1144
13.62 1166
13.62 1165
14.69 1257
15.07 1290
0.00 1309
0.00 1327
0.00 1389
16.82 1440
0.00 1463
0.00 1491
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2273563
956014
576895
5284
10.00 UG/L
9.10 UG/L
8.50 UG/L
0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
7879 0.43 UG/L
0 Not Found UG/L
8930 0.07 UG/L
32 0.00 UG/L
54878 0.25 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
2782 0.01 UG/L
1320 0.01 UG/L
1748 0.03 UG/L
4060 0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
45995 0.15 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
948
806
519
657
321
990
706
923
474
832
64 9
764
815
131
588
690
843
986
904
826
747
655
548
664
981
643
798
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.225
0.975
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.098
0.430
0. 291
0.189
0.000
0.000
0.000
1. 36 9
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AEQ1329.1A2
Data File: AE01329.MS
Name: AE01329
Quant Time: 03/29/99 11:12
Injected at: 03/29/99 03:47
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-A
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.94 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00 1520
17.79 1523
0.00 1552
0.00 1580
19.24 1647
0.00 1655
Ethylbenzene 19.36 1658
1,3-Dimethylbenzene 1m-Xylene 19.51 1671
1,4-Dimethylbenzene (p-Xylene 19.51 1671
1,2-Dimethylbenzene (a-Xylene 0.00 1733
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24 1733
0.00 1767
20.86 1786
0.00 1824
0.00 1835
21.42 1834
21.55 1845
0.00 1873
21.76 1863
21.95 1880
22.44 1921
22.50 1926
22.80 1952
23.02 1971
23.14 1981
23.26 1991
23.77 2036
24.00 2055
25.44 2178
27.33 2341
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area
790
Cone Units
Not Found UG/L
0.01 UG/L
Not Found UG/L
Not Found UG/L
1889 0.01 UG/L
0 Not Found UG/L
5207
203356
203356
0.02 UG/L
0.34 UG/L
0.34 UG/L
Not Found UG/L
1881 0.01 UG/L
Not Found UG/L
5858 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
88697 0.46 UG/L
293187 0.77 UG/L
Not Found UG/L
95098 0.31 UG/L
163193
12755
276202
355015
251289
115585
81444
201351
132189
9658
24287
0.64 UG/L
0.04 UG/L
0.95 UG/L
1.02 UG/L
0.90 UG/L
0.82 UG/L
0.51 UG/L
0.82 UG/L
1.01 UG/L
0.51 UG/L
0.39 UG/L
Fit
499
853
877
765
805
753
981
984
982
603
891
787
953
311
324
928
952
968
944
988
955
94 9
965
961
986
979
987
851
771
982
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1. 510
2.649
2.649
0.000
0.701
0.000
1.470
0.000
0.000
0.855
1 . 6 73
0.000
1.354
1.120
1.386
1.277
1. 530
1.223
0.620
0.704
1.074
0.579
0.083
0.276
Operator ID: MC
Output File: AE01329.1A2
Data File: AE01329.MS
Name: AE01329
QUANT REPORT Page
Quant Time: 03/29/99 11:12
Injected at: 03/29/99 03:47
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-A
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.94 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.62 2366
27.97 2395
28.55 2445
225
128
180
Area
32664
136790
68649
Cone Units
0.54 UG/L
1.01 UG/L
1.04 UG/L
Fit
985
993
976
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01330.1A2
Data File: AE01330.MS
Name: AE01330
QUANT REPORT Page
Quant Time: 03/29/99 11:16
Injected at: 03/29/99 05:44
Di'lution Factor: 1.00
Instrument ID:. 20701-1284
Sample: Location: N. Lawrence;Ala.Power side, SB17-B
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.94
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1201
21.15 1811
23.92 2049
4. 54
0.00
0.00
6.41
0.00
7.34
8.60
9.59
0.00
0.00
388
438
466
549
563
629
735
820
874
942
12.05 1031
0.00 1032
0.00 1069
0.00 1078
12.95 ll08
0.00 1136
0.00 ll36
13.60 ll64
13.60 1164
14.66 1255
15.06 1289
0.00 1307
0.00 1327
0.00 1389
16.80 1438
0.00 1463
0.00 1491
96 2106089
95 1057704
10.00 UG/L
ll.63 UG/L
ll.27 UG/L 152 652166
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
ll7
78
62
130
63
93
83
75
91
75
83
7297 0.00 UG/L
0 Not Found UG/L
0 Not Found UG/L
12452
ll105
1383
76062
0.01 UG/L
Not Found UG/L
0.00 UG/L
0.12 UG/L
0.00 UG/L
0 Not Found UG/L
0 Not Found UG/L
284 7 0.00 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
1952 0.00 UG/L
Not Found UG/L
0 Not Found UG/L
24881
2672
4286
4692
0.52 UG/L
0.00 UG/L
0.44 UG/L
0.22 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
77229 0.44 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
952
873
488
393
690
845
986
907
989
575
671
864
670
506
62
795
539
881
994
953
923
809
870
637
659
979
565
832
Rf
1.000
0.432
0.275
-0.014
0.000
0.000
6. 4 78
0.000
-0.064
0.057
-0.192
0.000
0.000
-0.242
0.000
0.000
0.000
-0.050
0.000
0.000
0.226
-0.031
0.047
0.102
0.000
0.000
0.000
0.826
0.000
0.000
Operator ID: MC
Output File: AE01330.1A2
Data File: AE01330.MS
Name: AE01330
QUANT REPORT Page 2
Quant Time: 03/29/99 11:16
Injected at: 03/29/99 05:44
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, 5817-8
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.94 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6"
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17._76 1520
18.18 1556
0.00 1578
19.22 1646
19.30 1652
19.33 1655
1,3-Dimethylbenzene (m-Xylene 19.52 1671
1,4-Dimethylbenzene (p-Xylene 19.52 1671
1,2-Dimethylbenzene (a-Xylene 0.00 1733
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimechylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.23 1732
20.64 1767
20.83 1783
0.00 1824
0.00 1835
21.50 1841
21.53 1844
0.00 1868
21.79 1866
21.94 1878
22.41 1919
22.48 1925
22.78 1951
23.00 1969
23.10 1978
23.24 1990
23.76 2034
23.97 2052
25.47 2181
27.27 2336
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
11310 0.00 UG/L
2353
34387
1360
298043
370165
370165
101722
7786
214534
0.70 UG/L
Not Found UG/L
0.46 UG/L
0.29 UG/L
0.91 UG/L
0.18 UG/L
0.18 UG/L
Not Found UG/L
1.08 UG/L
0.82 UG/L
0.67 UG/L
0 Not Found UG/L
Not Found UG/L
145551
264145
432971
231107
297357
266747
341026
271343
79738
290209
303616
196692
17926
74 053
0.90 UG/L
0.40 UG/L
Not Found UG/L
1. 76 UG/L
0.92 UG/L
1.00 UG/L
1. 00 UG/L
0.89 UG/L
0.60 UG/L
0. 30 UG/L
2.20 UG/L
0.90 UG/L
1. 38 UG/L
1.06 UG/L
0.56 UG/L
Fit
641
961
731
628
889
764
983
989
992
666
904
812
966
416
441
945
974
973
942
990
925
962
986
963
977
978
993
839
594
988
Rf
0.000
-0.163
0.016
0.000
0.355
0.022
1.563
9.681
9.681
0.000
0.449
0.046
1.514
0.000
0.000
0.771
3.153
0.000
1.170
1.194
1.413
1.268
1.822
2.158
1. 281
0.628
1. 595
0.677
0.081
0.623
Operator ID' MC
Output File' AE01330.1A2
Data File, AE01330.MS
Name, AE01330
QUANT REPORT Page
Quant Time, 03/29/99 11,16
Injected at, 03/29/99 05,44
Dilution Factor, 1. 00
Instrument ID, 20701-1284
Sample, Location, N. Lawrence,Ala.Power side, S817-8
ID File, 826AEC25.QCI
Comment, Sampling, 02/25/1999 by J. Conway, use 4.94 g
Last Calibration' 03/25/99 Last Qcal Time, 03/25/99 08,34
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.60 2363
27.94 2393
28.53 2443
225
128
180
Area
79112
145387
73152
Cone Units
0.58 UG/L
1. 02 UG/L
1.01 UG/L
Fit
993
984
976
Rf
0.653
0.677
0.344
QUANT REPORT Page
Operator ID: MC
Output File: AE01331.1A2
Data File: AE01331.MS
Name: AE01331
Quant Time: 03/29/99 11:16
Injected at: 03/29/99 06:24
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, 5817-C
/ ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.61 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-,4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
26) 75-27-4 Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.04
21.15
23.94
4.54
0.00
0.00
6.42
0.00
7.36
8.60
9.61
0.00
0.00
12.05
0.00
0.00
0.00
0.00
13.25
0.00
13.62
0.00
14.68
15.04
0.00
0.00
0.00
16.82
0.00
0.00
1202
1811
2050
388
438
466
549
572
630
735
821
874
945
1031
1032
106 9
1078
1111
1134
1137
1165
1164
1256
1287
1307
1327
1386
14 3 9
14 63
1500
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
2050726
921634
618582
7388
Cone Units
10.00 UG/L
10.40 UG/L
10.97 UG/L
0.00 UG/L
Not Found UG/L
Not Found UG/L
12990 0.08 UG/L
0 Not Found UG/L
11013 0.00 UG/L
1139
55877
0.11 UG/L
0.00 UG/L
Not Found UG/L
Not Found UG/L
2037 0.00 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
5200 0.33 UG/L
Not Found UG/L
16387 6.49 UG/L
Not Found UG/L
2368 0.41 UG/L
3447 0.19 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
60601 0.39 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
953
860
581
74 9
684
977
838
980
627
886
841
729
563
0
715
758
859
999
905
909
754
782
453
738
985
674
752
Rf
1.000
0.432
0.275
-0.015
0.000
0.000
0.833
0.000
-0.065
0.050
-0.137
0.000
0.000
-0.156
0.000
0.000
0.000
0.000
0.077
0.000
0.164
0.000
0.029
0.091
0.000
0.000
0.000
0.762
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AEOl33l.lA2
Data File: AE0133l.MS
Name: AEOl331
Quant Time: 03/29/99 11:16
Injected at: 03/29/99 06:24
Dilution Factor: l. 00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.61 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
3 7)
38)
39)
4 0)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-l
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-l
103-65-l
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-l
106-46-7
104-51-8
95-50-l
96-12-8
120-82-l
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00
17.78
0.00
0.00
19.23
0.00
Ethylbenzene 19.35
1,3-Dimethylbenzene 1m-Xylene 19.52
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (o-Xylene 0.00
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bl-omobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Eutylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.24
20.62
20.77
0.00
0.00
21.44
21.54
21.86
21.80
21.94
22.41
22.50
22.80
23.01
23.11
23.25
23.77
24.02
25.48
27.29
1520
1522
1560
1578
1646
1655
1656
1671
1671
1733
1733
1766
1778
1824
1835
1836
1844
1872
1867
1879
1919
1926
1952
1970
1978
1991
2035
2057
2182
2337
78
166
129
107
112
131
91
91
9l
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
10318 0.00 UG/L
0 Not Found UG/L
0 Not Found UG/L
40213 0.50 UG/L
Not Found UG/L
236241 0.71 UG/L
290011 0.03 UG/L
290011 0.03 UG/L
0 Not Found UG/L
87311 0.99 UG/L
4791
74083
0.78 UG/L
0.18 UG/L
0 Not Found UG/L
Not Found UG/L
19495 0.08 UG/L
217983 0.26 UG/L
58691 0.58 UG/L
383056 1.60 UG/L
213053 0.86 UG/L
229322 0.77 UG/L
231799 0.88 UG/L
273292 0.67 UG/L
210332 0.34 UG/L
134819
182432
217787
53563
15911
59903
0.79
1.33
0.48
0.06
0.96
0.34
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
530
979
732
397
869
685
982
991
993
693
900
740
94 6
504
14 7
931
955
971
930
992
901
94 7
980
962
971
979
986
807
865
966
Rf
0.000
-0.147
0.000
0.000
0.392
0.000
1.617
46.585
46.585
0.000
0.429
0.030
2.055
0.000
0.000
1.151
4.061
0.498
1.167
1. 208
1. 460
1. 290
1.981
3.058
0.829
0.671
2.195
4.132
0.082
0.866
Operator ID: MC
Output File: AE01331.1A2
Data File: AE01331.MS
Name: AE01331
QUANT REPORT Page
Quant Time: 03/29/99 11:16
Injected at: 03/29/99 06:24
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, S817-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.61 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.60 2364
27.96 2394
28 .. 54 2445
225
128
180
Area
65234
112978
56378
Cone Units
0.33 UG/L
0.76 UG/L
0.75 UG/L
Fit
976
985
976
Rf
0.955
0. 727
0.367
Operator ID, MC
Output File, AE01332.1A2
Data File, AE01332.MS
Name, AE01332
QUANT REPORT Page
Quant Time, 03/29/99 11,17
Injected at, 03/29/99 Q7,Q3
Dilution Factor, 1. DO
Instrument ID, 20701-1284
Sample' Location, N. Lawrence,Ala.Power side, SB17-D
I ID File, 826AEC25.QCI
Comment, Sampling, 02/25/1999 by J. Conway, use 4.95 g
Last Calibration, 03/25/99
Compound
11 •107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SG)
31 1,2-Dichlorobenzene-d4 (SGI
41 75-71-B Dichlorodifluoromethane
51 74-87-3
61 75-01-4
71 74-83-9
B) 75-00-3
91 75-69-4
101 75-35-4
111 75-09-2
121 156-60-5
131 75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
141
15 I
16 I
17 I
181
19)
20)
21 I
221
23)
24)
25)
26)
271
28)
29)
30 I
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time, 03/25/99 08,34
R.T. Scan# Q ion Area Cone Units
14.04 1201
21.14 1810
23.92 2048
4.54 389
0.00
0.00
0.00
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
0.00
14 . 6 6
15.06
0.00
0.00
0.00
16.81
0.00
0.00
438
466
549
572
630
737
821
874
942
1031
1031
1069
1078
1109
1136
1136
1165
1163
1255
1289
1309
1327
1389
1438
1463
1495
96 2250205 10.00 UG/L
9.58 UG/L
9. 54 UG/L
0.00 UG/L
95 931512
152 592519
8 5 5 02 0
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
8186 0.00 UG/L
Not Found UG/L
81248 0.00 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
21942 0.50 UG/L
Not Found UG/L
5359 0.45 UG/L
3349 0.17 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
91761 0.48 UG/L
Not Found UG/L
Not Found UG/L
Fit
997
999
951
890
82
240
597
568
971
0
969
234
632
780
604
306
0
764
484
812
995
951
934
660
360
541
652
980
633
772
Rf
1.000
0.433
0.276
-0.009
0.000
0.000
0.000
0.000
-0. 04 2
0.000
-0.192
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0. 194
0.000
0.053
0.087
0.000
0.000
0.000
0.855
0.000
0.000
QUANT REPORT Page 2
Operator ID' MC
Output File, AE01332.1A2
Data File, AE01332.MS
Name' AE01332
Quant Time, 03/29/99 11 '17
Injected at' 03/29/99 07,03
Dilution Factor' 1.00
Instrument ID' 20701-1284
Sample, Location, N. Lawrence,Ala.Power side, SB17-D
ID File, 826AEC25.QCI
Comment, Sampling, 02/25/1999 by J. Conway, use 4.95 g
Last Calibration, 03/25/99 Last Qcal Time' 03/25/99 09,34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
3 6)
37)
38)
3 9)
4 0)
41)
42)
4 3)
44)
4 5)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.77 1521
0.00 1560
0.00 1578
19.23 1646
0.00
19.33
1,3-Dimethylbenzene (m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.16
Styrene 20.26
1655
1655
1670
1670
1726
1735
1769
1784
1824
1835
1833
184 5
1865
1867
1876
1919
1925
1951
1969
1978
1990
2033
2052
2180
2337
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
0.00
0.00
0.00
21.41
21.55
0.00
21.80
21.91
22.41
22.49
22.79
23.00
23.11
23.24
23.74
23.97
25.45
27.29
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
10481 0.00 UG/L
Not Found UG/L
Not Found UG/L
34547 0.45 UG/L
250103
288139
288139
36909
35895
Not Found UG/L
0.68 UG/L
0.00 UG/L
0.00 UG/L
0. 22 UG/L
0.60 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
41090 0.20 UG/L
230265 0.23 UG/L
Not Found UG/L
. 355022 1.36 UG/L
118075
201678
197697
215980
1744 56
158686
212182
133471
104079
5837
45519
0.34 UG/L
0.59
0.65
0.39
0.09
0.88
1.42
0.00
0.46
0.27
0.00
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
Fit
378
983
818
14 7
929
665
982
992
991
735
908
696
941
568
141
923
973
964
941
977
944
94 8
967
972
984
982
988
799
738
979
Rf
0.000
-0.130
0.000
0.000
0.343
0.000
1.629
-44.916
-44.916
0. 740
0.267
0.000
0.000
0.000
0.000
0.903
4.382
0.000
1.160
1. 541
1.519
1.351
2.453
8.996
0.803
0.663
-17.046
1.011
0.098
-42.494
Operator ID: MC
Output File: AE01332.1A2
Data File: AE01332.MS
Name: AE01332
QUANT REPORT Page
Quant Time: 03/29/99 11:17
Injected at: 03/29/99 07:03
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-D
ID File: 825AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.95 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.61 2364
27.95 2394
28.50 2441
225
128
180
Area
43212
97319
47817
Cone Units
0.00 UG/L
0.53 UG/L
0.52 UG/L
Fit
972
984
972
Rf
-0.968
0.809
0. 4 06
Operator ID: MC
Output File: AE01333.1A2
Data File: AE01333.MS
Name: AE01333
QUANT REPORT Page
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 11:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N Lawr. Ala Power side SB17-E
ID File:. 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12)
13)
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.16
23.93
4.54
0.00
0.00
6.42
6.65
7.36
0.00
9.61
10.19
0.00
0.00
0.00
0.00
0.00
12.98
0.00
0.00
13.62
0.00
14.68
0.00
0.00
0.00
1204
1813
2051
389
438
467
550
570
631
737
823
873
943
1034
1036
1070
1079
1112
1137
1141
1167
1165
1258
12 92
1310
1328
0.00 1389
16.82 1441
0.00 1465
0.00 1495
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1853476
850092
528206
5076
10.00 UG/L
9.92 UG/L
9.55 UG/L
0.08 UG/L
0 Not Found UG/L
Not Found UG/L
3257 0.22 UG/L
302 0.03 UG/L
6839 0.07 UG/L
Not Found UG/L
1169010 6.53 UG/L
1034 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
1441 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
13077 0.06 UG/L
Not Found UG/L
1314 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
21200 0.08 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
997
999
94 9
872
0
445
615
874
975
352
988
767
458
574
770
692
0
738
659
730
993
912
830
234
61
651
730
973
579
641
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.967
0.452
0.000
0.000
0.000
0.000
0.000
0.662
0.000
0.000
1.098
0. 000
0.291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01333.1A2
Data File: AE01333.MS
Name: AE01333
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 11:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N Lawr. Ala Power side SB17-E
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) .100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56)
57)
58)
59)
60)
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.78
0.00
0.00
19.22
0.00
19.35
1521
1524
1548
1580
1647
1657
1658
1,3-Dimethylbenzene (m-Xylene 19.52 1673
1,4-Dimethylbenzene (p-Xylene 19.52
1,2-Dimethylbenzene (o-Xylene 20.23
Styrene 20.25
1673
1734
1735
1771
1786
1825
1837
1841
1846
1881
1862
1881
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.84
0.00
0.00
21.48
21.54
21.95
21.73
21.95
22.43 1922
22.49 1927
22.80 1954
23.01 1972
23.13 1982
23.24
23.77
0.00
0.00
27. 30.
1992
2037
2056
2184
2340
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
5196 0.10 UG/L
Not Found UG/L
Not Found UG/L
3829 0.02 UG/L
0 Not Found UG/L
64903 0.23 UG/L
100393
100393
3421 a·
15646
0.20 UG/L
0.20 UG/L
0.14 UG/L
0.12 UG/L
0 Not Found UG/L
73877 0.27 UG/L
Not Found UG/L
Not Found UG/L
2282 0.01 UG/L
78237 0.25 UG/L
47291
76245
47291
77912
107763
78305
79945
18331
0.21 UG/L
0.30 UG/L
0.23 UG/L
0.30 UG/L
0.46 UG/L
0.28 UG/L
0.35 UG/L
0.16 UG/L
122543 0.94 UG/L
65757 0.33 UG/L
Not Found UG/L
Not Found UG/L
23407 0.46 UG/L
Fit
473
967
824
442
854
574
981
994
992
739
932
404
950
455
464
953
952
94 8
965
985
908
945
957
953
980
980
989
64 9
400
940
Rf
0.000
0.284
0.000
0.000
0.858
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1. 4 70
0.000
0.000
0.855
1.673
1. 234
1.354
1.120
1.386
1. 277
1.530
1.224
0.620
0.703
1.074
0.000
0.000
0.276
Operator ID: MC
Output File: AE01333.1A2
Data File: AE01333.MS
Name: AE01333
QUANT REPORT Page
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 11:41
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N Lawr. Ala Power side 5817-E
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.14 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.61 2366 225 23595 0. 4 7
62) 91-20-3 Naphthalene 27.95 2395 128 55987 0.51
63) 82-61-6 1,2,3-Trichlorobenzene 28.54 2446 180 24310 0.45
• Compound is ISTD
Units Fit Rf
--------UG/L 968 0.269
UG/L 985 0.596
UG/L 977 0. 291
Operator ID: MC
Output File: AE01334.1A2
Data File: AE01334.MS
Name: AE01334
QUANT REPORT Page
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 12:21
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: N Lawr. Ala Power side SB17-F
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.19 g
Last Calibration: 03/29/99
Compound
1) *1 07-06-2 Fl uorobenzene
2) 4-Bromofluorobenzene (SG)
3)
4)
5)
6)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3 Chloromethane
75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1~Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroet:hene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
14)
15)
16)
17)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion Area Cone Units
14.04
21.14
23.94
4.55
0.00
0.00
6.41
0.00
7.36
0.00
9.61
0.00
o.oo 0.00
0.00
12.53
o.oo 0.00
0.00
o.oo 13.62
13.60
0.00
0.00
0.00
0.00
0.00
16.80
o.oo o.oo
1203
1812
2052
390
438
467
549
575
631
737
823
865
934
1034
1034
1074
1079
1113
1137
1136
1167
1165
1259
1292
1310
1328
1390
144 0
1465
14 95
96 1924061
95 878572
152 527750
10.00 UG/L
9.88 UG/L
9.19 UG/L
0.06 UG/L 85 4073
47 0 Not Found UG/L
62 Not Found UG/L
96 2774 0.18 UG/L
4 9 0 Not Found UG/L
101 6339 0.06 UG/L
96 Not Found UG/L
49· 1220398 6.56 UG/L
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2131 0.02 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
13423 0.06 UG/L
450 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
17001 0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
999
954
864
47
352
731
907
974
420
995
781
854
384
530
789
489
685
955
993
904
625
303
278
645
632
984
561
512
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.967
0.000
0.000
0.000
0.000
0.486
0.000
0.000
0.000
0.000
1. 098
0.430
0.000
0.000
0.000
0.000
0.000
1 . 3 6 9
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01334o1A2
Data File: AE01334oMS
Name: AE01334
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 12:21
Dilution Factor: 1o00
Instrument ID: 20701-1284
Sample: Location: N Lawro Ala Power side SB17-F
ID File: 826AEC28oQCI
Comment: Sampling: 02/22/1999 by Jo Conway, use 5o19 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
3 9)
4 0)
41)
42)
43)
44)
4 5)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound RoTo Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
OoOO
17076
OoOO
0000
0000
OoOO
19o34
1,3-Dimethylbenzene (m-Xylene l9o50
1,4-Dimethylbenzene (p-Xylene 19050
1,2-Dimethylbenzene (a-Xylene 20o23
Styrene 20o25
Bromoform OoOO
20 0 84
OoOO
OoOO
21050
21 0 4 7
2lo87
21o80
21o93
22o42
22 0 4 9
22078
23o00
23o12
23o23
23o72
OoOO
1521
1522
1556
1580
164 9
1657
1657
1671
1671
1734
1735
1771
1786
1825
1837
1842
1840
1874
1868
1879
1921
1927
1952
1971
1981
1991
2033
2056
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
OoOO 2184
27o29 2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
3491 Oo06 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
45897 0016 UG/L
74604
74604
30978
10656
Oo15 UG/L
Oo15 UG/L
0012 UG/L
Oo08 UG/L
Not Found UG/L
48795 0017 UG/L
Not Found UG/L
0 Not Found UG/L
12172 0007 UG/L
18912
13342
76134
38062
70747
92589
67388
63666
44692
116212
44516
Oo06 UG/L
0006 UG/L
0 o 29 UG/L
0 o18 UG/L
Oo27 UG/L
Oo38 UG/L
0023 UG/L
Oo27 UG/L
0 o 38 UG/L
Oo86 UG/L
Oo22 UG/L
Not Found UG/L
Not Found UG/L
17187 Oo32 UG/L
Fit
0
962
654
4 91
439
503
982
989
990
821
898
353
930
336
609
770
950
956
964
983
939
930
874
941
969
976
958
644
370
935
Rf
00000
00284
OoOOO
OoOOO
OoOOO
OoOOO
1o510
2 0 64 9
2 0 64 9
lo305
00701
00000
1 0 4 70
00000
OoOOO
Oo855
10673
10234
lo354
1o120
lo386
1. 277
1. 530
1o224
Oo620
00703
10075
OoOOO
OoOOO
Oo276
Operator ID: MC
Output File: AE01334.1A2
Data File: ~E01334.MS
Name: AE01334
QUANT REPORT Page
Quant Time: 03/30/99 18:21
Injected at: 03/30/99 12:21
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: N Lawr. Ala Power side SB17-F
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.19 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
61) 87-68-3
62) 91-20-3
63) 82-61-6
· • Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan!l Q ion
27.60 2365
27.93 2394
28.53 2445
225
128
180
Area
16716
46660
16223
Cone Units
0.32 UG/L
0.41 UG/L
0.29 UG/L
Fit
964
985
929
Rf
0.269
0. 596
0. 291
...
Operator ID: MC
Output File: AE01335.1A2
Data File: AE01335.MS
Name: AE01335
QUANT REPORT Page
Quant Time: 03/29/99 11:18
Injected at: 03/29/99 09:01
Dilution Factor: 1. DO
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-G
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.39 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12)
13)
14)
15)
16)
1 7)
18)
19)
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28)
29)
3 0)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
* Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1202
21.13 1811
23.92 2050
4.54 389
0.00 438
0.00
6.40
6.66
7.35
8.59
9.59
10.17
10.97
12.02
0.00
12.46
12.56
12.94
13.22
466
54 9
571
630
736
822
871
94 0
103 0
1033
1068
1076
1109
1133
13.27 1137
13.61 1166
13.58 1164
14.66 1256
0.00 1292
0.00 1307
15.48 1326
16.20 1388
16.79 1439
17.12 1467
17.42 1493
96 2304819 10.00 UG/L
95 915955 9.20 UG/L
152 581198 9.13 UG/L
85 10538 0.00 UG/L
47 Not Found UG/L
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Not Found UG/L
25449 0.82 UG/L
1858
16016
3850
311486
11739
3588
7537
3948
9510
6392
9535
3273
29625
6503
9835
0.00 UG/L
0.00 UG/L
0.16 UG/L
0.00 UG/L
0.00 UG/L
0.23 UG/L
0.00 UG/L
Not Found UG/L
0.47 UG/L
0. 00 UG/L
0.00 UG/L
0. 38 UG/L
0. 38 UG/L
0.53 UG/L
0.00 UG/L
0.52 UG/L
0 Not Found UG/L
0 Not Found UG/L
1547 0.39 UG/L
4230
163575
34150
2261
0.93 UG/L
0.72 UG/L
3.29 UG/L
0.61 UG/L
Fit
997
999
94 7
905
55
803
751
839
990
953
944
928
806
937
839
763
936
863
868
94 6
991
959
974
314
897
887
865
986
799
779
Rf
1.000
0.433
0.277
-0.019
0.000
0.000
0.135
-0.022
-0.089
0.106
-1.891
-0.272
0.068
-2.377
0.000
0.037
-0.397
-0.185
0.110
0.038
0.241
-0.078
0.083
0.000
0.000
0.018
0.020
0.991
0.046
0.017
\ ...
QUANT REPORT Page 2
Operator IDo MC
Output Fileo AE01335.1A2
Data Fileo AE01335.MS
Nameo AE01335
Quant Timeo 03/29/99 llolB
Injected ato 03/29/99 09o01
Dilution Factor, 1.00
Instrument IDo 20701-1284
Sample, Location' N. Lawrence,Ala.Power side, SB17-G
ID Fileo 826AEC25.QCI
Commento Samplingo 02/25/1999 by J. Conway, use 4.39 g
Last Calibration' 03/25/99 Last Qcal Timeo 03/25/99 08o34
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
0.00 1521
17.75 1521
18.12
0.00
19.21
0.00
Ethylbenzene 19.32
1,3-Dimethylbenzene (m-Xylene 19.50
1553
1580
1646
1657
1656
1671
1,4-Dimethylbenzene (p-Xylene 19.50 1671
1,2-Dimethylbenzene (a-Xylene 20.21 1732
Styrene 20.21 1732
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.61 1766
20.81 1783
0.00 1825
0.00 1837
21.48 1841
21.53 1845
21.93 1879
21.79
21.93
22.39
22.47
22.78
22.98
23.22
23.22
23.73
24. 04
25.47
27.27
1867
1879
1919
1926
1952
1969
1990
1990
2034
2060
2183
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
20058 0.00 UG/L
5566 0.75 UG/L
Not Found UG/L
43067 0.49 UG/L
0 Not Found UG/L
545869 1.61 UG/L
662122
662122
255860
61250
3412
209256
0.67 UG/L
0.67 UG/L
1.03 UG/L
0.76 UG/L
0.76
0.59
UG/L
UG/L
0 Not Found UG/L
Not Found UG/L
108224 0.59 UG/L
288234 0.40 UG/L
213832 1.12 UG/L
425863
213832
242026
424774
272800
279186
391375
391375
213786
30605
4220
70273
1.58 UG/L
0.75 UG/L
0.71 UG/L
1.52 UG/L
0.56 UG/L
0.52 UG/L
2. 65 UG/L
2.77 UG/L
0.34 UG/L
0.00 UG/L
0.16 UG/L
0. 3 9 UG/L
Fit
670
968
869
549
920
630
986
993
995
869
897
882
965
338
94
962
953
973
946
991
920
985
982
990
979
978
982
862
607
979
Rf
0.000
-0.443
0.033
0.000
0.382
0.000
1.475
4.272
4.272
1.079
0.352
0. 020
1. 541
0.000
0.000
0.791
3 . 164
0.832
1.166
1.241
l. 475
1.216
2.113
2.329
0.641
0. 614
2.767
-0.705
0.113
0.790
Operator ID: MC
Output File: AE01335.1A2
Data File: AE01335.MS
Name: AE01335
QUANT REPORT Page
Quant Time: 03/29/99 11:18
Injected at: 03/29/99 09:01
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-G
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.39 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexach1orobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.57 2363
27.94 2394
28.51 2443
225
128
180
Area
62868
137841
74725
Cone Units
0.14 UG/L
0.85 UG/L
0.93 UG/L
Fit
979
989
972
Rf
1.921
0.707
0.350
Operator ID: MC
Output File: AE01336.1A2
Data File: AE01336.MS
Name: AE01336
QUANT REPORT Page
Quant Time: 03/30/99 18:22
Injected at: 03/30/99 16:04
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: ~ocation: N. Lawrence,Ala.Power side, SB17-H
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 2.51 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5)
6)
7)
8)
9)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
78-87-5
74-95-3
75-27-4
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
24)
25)
26)
27)
28)
29)
30)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.15
23.94
4.55
0.00
0.00
6. 40
6.69
7.35
0.00
9.60
0.00
0.00
0.00
0.00
0.00
0.00
12.97
0.00
1203
1812
2051
389
438
474
548
573
629
737
822
874
943
1033
1032
1069
1079
1111
1136
0.00 1137
13.62 1166
13.59 1164
14.67 1256
0.00
0.00
0.00
0.00
16.82
0.00
17.40
1291
1309
1334
1390
144 0
1464
1490
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
1928169
908429
577185
6595
10.00
10.19
10.04
0.09
UG/L
UG/L
UG/L
UG/L
0 Not Found UG/L
Not Found UG/L
2762 0.18 UG/L
441 0.04 UG/L
7080 0.07 UG/L
0 Not Found UG/L
370325 1.97 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
970 0.01 UG/L
Not Found UG/L
Not Found UG/L
12286 0.06 UG/L
1090
1510
0.01 UG/L
0.03 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
48055 0.18 UG/L
Not Found UG/L
778 0.03 UG/L
Fit
998
999
951
880
0
546
715
820
985
451
969
266
570
459
650
464
233
793
641
904
966
917
889
179
666
751
562
985
536
816
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.060
0.526
0.000
0.973
0.000
0.000
0.000
0.000
0.000
0.000
0.662
0.000
0.000
1.098
0.430
0.291
0.000
0.000
0.000
0.000
1 . 3 6 9
0.000
0. 145
QUANT REPORT Page
Operator ID: MC
Output File: AEOl336.lA2
Data File: AE01336.MS
Name: AE01336
Quant Time: 03/30/99 18:22
Injected at: 03/30/99 16:04
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-H
ID File: 826AEC28.QCI
Comment: ~ampling: 02/25/1999 by J. Conway, use 2.51 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
43)
44)
45)
46)
47)
48)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-l
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-l
96-12-8
120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.77
0.00
o.oo 19.20
0.00
19.34
1,3-Dimethylbenzene 1m-Xylene 19.52
1,4-Dimethylbenzene lp-Xylene 19.52
1,2-Dimethylbenzene (a-Xylene 20.23
Styrene 0.00
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Broniobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1, )-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.85
0.00
0.00
21.47
21.54
0.00
21.79
21.94
22.42
0.00
0.00
22.99
23.24
23.24
23.74
0.00
25.40
27.27
1521
1522
1556
1579
1645
1656
1657
1672
1672
1733
1735
1770
1786
1825
1836
1839
1846
1871
1867
1880
1921
1935
1954
1969
1991
1991
2034
2055
2176
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
14 6
75
180
Area Cone Units
Not Found UG/L
5460 0.10 UG/L
0 Not Found UG/L
Not Found UG/L
2770 0.02 UG/L
24444
66987
66987
20177
Not Found UG/L
0.08 UG/L
0.13 UG/L
0.13 UG/L
0.08 UG/L
Not Found UG/L
Not Found UG/L
27693 0.10 UG/L
0 Not Found UG/L
Not Found UG/L
10045 0.06 UG/L
172001 0.53 UG/L
Not Found UG/L
90290 0.35 UG/L
9447
52870
73604
92640
92640
102083
2424
33955
0.04 UG/L
0.20 UG/L
Not Found UG/L
Not Found UG/L
0.31 UG/L
0.78 UG/L
0.68 UG/L
0.49 UG/L
Not Found UG/L
0.15 UG/L
0.64 UG/L
Fit
481
959
63
0
845
435
972
990
987
884
584
334
819
325
320
754
749
845
903
848
827
920
604
975
987
983
899
684
701
960
Rf
0.000
0. 284
0.000
0.000
0.858
0.000
1.510
2.649
2 ._64 9
1.305
0.000
0.000
l. 470
0.000
0.000
0.855
1.673
0.000
1.354
1.120
1.386
0.000
0.000
1.224
0. 620
0.703
1.074
0.000
0.083
0.276
Operator ID: MC
Output File: AE01336.1A2
Data File: AE01336.MS
Name: AE01336
QUANT REPORT Page
Quant Time: 03/30/99 18:22
Injected at: 03/30/99 16:04
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-H
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 2.51 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
R.T. Scan# Q ion
27.60 2365
27.93 2393
28.53 2444
225
128
180
Area
40556
67676
30678
Cone Units
0.78 UG/L
0.59 UG/L
0.55 UG/L
Fit
982
982
969
Rf
0.269
0. 596
0.291
Operator ID: MC
Output File: AE01337.1A2
Data File: AE01337.MS
Name: AE01337
QUANT REPORT Page
Quant Time: 03/30/99 18:44
Injected at: 03/30/99 17:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-I
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 2.90 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
21 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4 Vinyl Chloride
7) 74-83-9 Bromomethane
8) 75-00-3 Chloroethane
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.06
21.17
23.94
4.55
0.00
0.00
6.42
0.00
7.37
0.00
9.63
0.00
0.00
0.00
0.00
1204
1814
2052
390
438
467
550
573
632
737
825
874
943
1033
1039
0.00 1070
0.00 1079
12.99 1113
0.00 1136
0.00 1137
13.63 1168
0.00 1167
14.69 1259
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.82 1441
0.00 1465
0.00 1494
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2042373
910549
10.00 UG/L
9.64 UG/L
9.11 UG/L
0.06 UG/L
. 555002
4738
Not Found UG/L
0 Not Found UG/L
3500 0.21 UG/L
0 Not Found UG/L
6453 0.06 UG/L
Not Found UG/L
509479 2.57 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
744 0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
9832 0.04 UG/L
Not Found UG/L
1038 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
33701 0.12 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
1000
956
890
0
172
698
6
979
622
993
554
271
802
679
282
168
754
464
726
988
903
895
231
141
809
592
959
515
736
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0.972
0.000
0.000
0.000
0.000
0.000
0.000
0.662
0.000
0.000
1.098
0.000
0. 291
0.000
0.000
0.000
0.000
1.369
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01337.1A2
Data File: AE01337.MS
Name: AE01337
Quant Time: 03/30/99 18:44
Injected at: 03/30/99 17:57
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-l
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 2.90 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37)
38)
100-41-4
108-38-3
39) 106-42-3
4 0)
41)
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45)
4 6)
47)
4 8)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
96-18-4
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dib~omoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
17.78 1524
0.00 1556
0.00 1579
0.00 1649
0.00 1656
0.00
1,3-Dimethylbenzene 1m-Xylene 19.51
1657
1672
1,4-Dimethylbenzene (p-Xylene 19.51 1672
1,2-Dim~thylbenzene
Styrene
lo-Xylene 20.26
0.00
1736
1734
Bromofo~m
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-T~ichloropropane
Bromoben.zene
n-Propylbenzene
2-Chlorotoluene
1,3,5-T~imethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1770
20.84 1786
0.00 1825
0.00
0.00
21.48
0.00
21.82
22.01
22.36
0.00
22.80
23.02
0.00
23.26
23.78
0.00
0.00
27.24
1836
1842
1841
1873
1869
1886
1916
1927
1954
1973
1980
1993
2038
2056
2183
2334
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
1107 0.02 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
24824 0.05 UG/L
24 824 0.05 UG/L
9546 0.04 UG/L
0 Not Found UG/L
0 Not Found UG/L
36046 0.12 UG/L
25576
30356
2001
38834
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.07 UG/L
Not Found UG/L
0.11 UG/L
0.01 UG/L
0.14 UG/L
0 Not Found UG/L
12007 0.04 UG/L
4711 0.02 UG/L
Not Found UG/L
127476 0.89 UG/L
164 09 0.07 UG/L
0 Not Found UG/L
0 Not Found UG/L
23880 0.42 UG/L
Fit
430
889
0
401
502
280
660
967
974
904
723
87
859
298
428
698
809
904
84 8
936
867
364
925
936
707
911
910
579
245
94 9
Rf
0.000
0.284
0.000
0.000
0.000
0.000
0.000
2.649
2. 64 9
1.305
0.000
0.000
1.470
0.000
0.000
0.000
1.673
0.000
1.354
1.120
1.386
0.000
1.529
1.224
0.000
0.703
1.075
0.000
0.000
0.276
Operator ID: MC
Output File: AE01337.1A2
Data File: AE01337.MS
Name: AE01337
QUANT REPORT Page
Quant Time: 03/30/99 18:44
Injected at: 03/30/99 17:57
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: N. Lawrence,Ala.Power side, SB17-I
ID File: 826AEC28.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 2.90 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.60 2365 225 21512 0.39
62) 91-20-3 Naphthalene 27.95 2394 128 53604 0.44
63) 82-61-6 1,2,3-Trichlorobenzene 28.51 2443 180 35987 0.61
* Compound is ISTD
Units Fit Rf
----- ---
UG/L 971 0.269
UG/L 979 0.596
UG/L 978 0.291
Operator ID: MC
Output File: AE01307.1A2
Data File: AE01307.MS
Name: AE01307
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-A
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:27
Injected at: 03/27/99 08:06
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 3.89 g
Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromornethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Dibromomethane
Bromodichloromethane
27)
28).
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1200
21.13 1809
23.92 2048
4.52
0.00
0.00
6.38
0.00
7.33
0.00
9.59
387
438
466
546
573
628
737
820
0.00 874
0.00 938
0.00 1033
0.00 1033
0.00 1069
12.56 1074
0.00 1112
0.00 1136
0.00 1138
13.59 1163
0.00 1163
14.67 1255
0.00 1291
0.00 1309
0.00 1327
0.00
16.79
1389
1437
17.12 1466
0.00 1501
96 1959159
95 695278
10.00 UG/L
8.05 UG/L
8.30 UG/L 152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
445858
4033 0.08 UG/L
0 Not Found UG/L
Not Found UG/L
5481 0.38 UG/L
4 943
Not Found UG/L
0.06 UG/L
Not Found UG/L
226572 0.92 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
2209 0.03 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
27728 0.16 UG/L
0 Not Found UG/L
745 0.01 UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
60928 0.26 UG/L
79456 1.25 UG/L
Not Found UG/L
Fit
998
998
958
805
487
677
712
988
121
963
334
859
315
237
474
825
484
437
656
998
899
746
319
443
656
369
986
712
708
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0. 074
0.000
0. 4 55
0.000
1. 251
0.000
0.000
0.000
0.000
0.000
0.434
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.324
0.000
------------------ --------· ----------------------------------------------------------------------------------------------
Operator ID' MC
Output File' AE01307.1A2
Data File, AE01307.MS
Name, AE01307
QUANT REPORT
Sample, Location' 200 Dexter Ave., SB18-A
ID File, 826AEC25.QCI
Page 2
Quant Time, 03/27/99 19,27
Injected at, 03/27/99 08,06
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment, Sampling' 02/25/1999 by J. Conway, use 3.89 g
Last Calibration, 03/25/99 Last Qcal Time, 03/25/99 08,34
311 142-28-9
321 127-18-4
33) 124-48-1
34)
35)
36 I
37)
38)
39 I
4 0 I
411
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
431. 98-82-8
44) 79-34-5
451 96-18-4
461 108-86-1
471 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
511 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane·
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.76 1520
0.00 1555
0.00
0.00
0.00
19.30
1,3-Dimethylbenzene 1m-Xylene 19.50
1,4-Dimethylbenzene (p-Xylene 19.50
1,2-Dimethylbenzene (a-Xylene 20.21
1578
1648
1655
1653
1669
1669
1730
1736
1769
1780
1824
1835
1836
1843
1874
1863
1879
1919
1924
1949
1968
1977
1990
2033
2052
2180
2336
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bt-omobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.28
0.00
20.79
0.00
0.00
21.44
21.53
21.89
21.76
21.94
22.41
22.4 7
22.76
22.99
23.09
23.24
23.74
23.97
0.00
27.27
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Unit.s
0 Not Found UG/L
4803 0.09 UG/L
0 Not Found UG/L
0 Not Found.UG/L
0 Not Found UG/L
0 Not Found UG/L
86611 0.34 UG/L
134476
1344 76
62520
8055
0.29 UG/L
0.29 UG/L
0.30 UG/L
0.07 UG/L
0 Not Found UG/L
54968 0.23 UG/L
0 Not Found UG/L
Not Found UG/L
11540 0.09 UG/L
75645
45539
121354
22893
64865
100708
72927
57107
57922
67397
59288
384 91
0.27 UG/L
0.21 UG/L
0. 54 UG/L
0.12 UG/L
0.27 UG/L
0.44 UG/L
0.29 UG/L
0.28 UG/L
0.51 UG/L
0.62 UG/L
0.30 UG/L
0. 3 7 UG/L
Not Found UG/L
17395 0.29 UG/L
Fit
4 94
929
622
81
633
649
988
995
995
940
890
132
946
466
617
845
971
953
969
973
934
987
828
975
979
980
962
817
668
921
Rf
0.000
0.266
0.000
o .ooo·
0.000
0.000
1. 320
2.360
2.360
1.076
0.576
0.000
1. 246
0.000
0.000
0.685
1. 4 38
1.100
1.138
0.960
1. 209
1.169
1. 3 04
1 . 051
0.575
0.560
1.005
0.526
0.000
0. 303
Operator ID: MC
Output File: AE01307.1A2
Data File: AE01307.MS
Name: AE01307
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-A
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:27
Injected at: 03/27/99 08:06
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 3.89 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
He~achlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.59 2363
27.93 2392
28.51 2442
225
128
180
Area
22655
58536
16075
Cone Units
0.38 UG/L
0.51 UG/L
0.27 UG/L
Fit
947
978
907
Rf
0.310
0.586
0. 3 04
Operator ID: MC
Output File: AE01308.1A2
Data File: AE01308.MS
Name: AE01308
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-8
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:28
Injected at: 03/27/99 08:45
Dilution Factor: 1.00
Instrument ID: 2,0701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 3.69 g I Last Calibration: 03/25/99
Compound
1) •107-06-2 Fl uorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1;1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1200
21.13 1809
23.92 2048
96 2060672 10.00 UG/L
8.04 UG/L
9.03 UG/L
0. 07 UG/L 4.53
0.00
0.00
6.36
0.00
7.34
0.00
9.57
387
438
4 64
545
572
629
737
819
0.00 874
0.00 942
0.00 1033
0.00 1030
0.00 1069
0.00 1078
0.00 1112
0.00 1136
0.00 1139
13.59 1163
0.00 1164
14.70 1258
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.80 1438
0.00 1464
0.00 1490
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
730477
510268
3881
Not Found UG/L
Not Found UG/L
0.52 UG/L
Not Found UG/L
0.05 UG/L
Not Found UG/L
0.67 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
7967
4446
171856
12861
38
30136
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.07 UG/L
Not Found UG/L
0.00 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.12 UG/L
Not Found UG/L
Not Found UG/L
Fit.
997
999
952
829
0
522
744
688
982
229
988
356
586
633
653
492
652
650
622
876
985
913
778
103
373
444
535
980
567
769
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0. 074
0.000
0. 4 55
0.000
1. 254
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
Opera tor ID, MC
Output File, AE01308.1A2
Data File, AE01308.MS
Name, AE01308
QUANT REPORT
Sample, Location, 200 Dexter Ave., SB18-B
ID File, 826AEC25.QCI
Page
Quant Time, 03/27/99 19,28
Injected ar, 03/27/99 09,45
Dilution Factor, 1.00
Instrument ID, 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 3.69 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-38-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.76 1520
0.00 1555
0.00 1578
0.00 1644
0.00 1655
19.35 1657
1,3-Dimethylbenzene 1m-Xylene a9.50 1669
1,4-Dimethylbenzene (p-Xylene 19.50 1669
1,2-Dimethylbenzene (a-Xylene 20.22 1731
Styrene
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Burylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-T~ichlorobenzene
20.22 1731
0.00 1769
20.83 1783
0.00 1824
0.00 1835
21.52 1842
21.53 1844
21.86 1872
21.77 1864
21.86 1872
22.41 1919
22.47 1924
22.76 1949
22.98 1968
23.22 1988
23.24 1990
23.72 2031
24.00 2055
0.00 2178
27.25 2334
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
3344 0.06 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
70421
67646
67646
27316
25146
Not Found UG/L
0.26 UG/L
0.14 UG/L
0.14 UG/L
0.12 UG/L
0.21 UG/L
0 Not Found UG/L
22413 0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
16661
54248
11156
80888
41946
52137
67881
65348
52667
33635
18334
60127
15933
0.12 TJG/L
0.18 UG/L
0. 05 UG/L
0.35 UG/L
0.21 UG/L
0.21 UG/L
0.28 UG/L
0.24 UG/L
0.24 TJG/L
0.28 UG/L
0.16 UG/L
0.29 UG/L
0.15 UG/L
0 Not Found UG/L
15510 0.25 UG/L
Fit
637
893
332
376
702
662
981
992
991
705
906
162
907
451
351
844
948
947
945
969
916
943
BSS
909
972
964
914
815
6 01
934
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.320
2.360
2.360
1.076
0.576
0.000
1. 245
0.000
0.000
0.685
1.438
1.099
1.137
0.960
1.209
1.169
1.304
1.051 I
0.575
0.559
1.005
0.526
0.000
0.303
Operator ID: MC
Output File: AE0<308.1A2
Data File: AE01308.MS
Name: A£01308
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-B
ID File: 826AEC2S.QCI
Page
Quant Time: 03/27/99 19:28
Injected at: 03/27/99 08:45
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 3.69 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------61) 87-68-3 Hexachlorobutadiene 27.59 2363 225 9296 0. 15
62) 91-20-3 Naphthalene 27.91 2390 128 40096 0.33
63) 82-61-6 1,2,3-Trichlorobenzene 28.4 7 2438 180 14 779 0.24
• Compound is ISTD
Units Fit Rf
--------UG/L 984 0.310
UG/L 983 0.586
UG/L 948 0. 3 04
Operator ID: MC
Output File: AE01309.1A2
Data File: AE01309.MS
Name: AE01309
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-C
ID File: 826AEC2S.QCI
Page
Quant Time: 03/27/99 19:29
Injected at: 03/27/99 09:24
Dilution Factor: 1. 00
Instrument ID: 20?01-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.83 g
j Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2)
3)
4)
5)
6)
7)
8)
9)
4-Bromofluorobenzene (SG)
1,2-Dichlorobenzene-d4 (SG)
10)
11)
12)
13)
14)
15)
16)
17)
18)
19)
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
20) 56-23-5
21) 71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1, 1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
22)
23)
24)
25)
26)
27)
28)
2 9)
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1200 96 1974905 10.00 UG/L
10.61 UG/L
11.51 UG/L
21.13
23.92
4.55
0.00
0.00
6.42
0.00
7.35
1809
2048
389
438
466
550
567
630
0.00 737
9.60 820
0.00 874
0.00 943
0.00 1033
0.00 1033
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1137
13.60 1164
0.00
14.64
0.00
0.00
0.00
0.00
16.79
0.00
1162
1253
1291
1309
1334
1390
1437
1464
0.00 1494
95
152
85
47
61
96
49
101
96
4 9 .
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
920721
622772
4400 0.09 UG/L
0 Not Found UG/L
0 Not Found UG/L
5201 0.36 UG/L
0 Not Found UG/L
4463 0.05 UG/L
Not Found UG/L
210557 0.85 UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not ·Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
13444 0.08 UG/L
Not Found UG/L
691 0.01 UG/L
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
31936 0.14 UG/L
Not Found UG/L
Not Found UG/L
Fit
998
999
953
864
0
339
6 76
821
980
94 9
178
419
314
527
637
532
643
455
874
967
942
707
71
298
705
606
983
606
538
Rf
1.000
0.440
0.274
0.258
0.000
0.000
0.074
0.000
0.455
0.000
1. 252
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page
Operator ID: MC
Output File: AE01309.1A2
Data File: AE01309.MS
Name: AE01309
Quane Time: 03/27/99 19:29
Injected at: 03/27/99 09:24
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 Dexter Ave., SB18-C
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.83 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33)
34)
35)
36)
37)
38)
3 9)
40)
41)
42)
43)
44)
45)
46)
47)
4 8)
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4"
108-86-1
103-65-1
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
0.00 1521
0.00 1524
Dibromochloromethane 0.00
1,2-Dibromoethane 0.00
Chlorobenzene 0.00
1,1,1,2-Tetrachloroethane 0.00
Ethylbenzene 19.36
1,3-Dimethylbenzene (m-Xylene 19.49
1,4-Dimethylbenzene (p-Xylene 19.49
1,2-Dimethylbenzene (a-Xylene 20.12
Styrene 20.25
Bromoform 0.00
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.81
0.00
0.00
0.00
21.56
21.90
21.77
21.95
22.41
22.4 6
22.76
22.98
23.15
23.24
23.77
0.00
0.00
27.27
1556
1579
1648
1656
1657
1668
1668
1722
1734
1770
1782
1825
1836
1842
184 6
1875
1864
1880
1919
1923
1948
1968
1982
1990
2035
2055
2183
2335
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
14 6
14 6
91
146
75
180
Area Cone Units
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
29492 0.11 UG/L
68024 0.15 UG/L
68024 0.15 UG/L
9303
13880
0.04 UG/L
0.12 UG/L
0 Not Found UG/L
49189 0.20 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
53247 0.19 UG/L
32506
83 94 8
15390
55674
56966
54 922
66315
12341
63656
34 020
0.15 UG/L
0.37
0.08
0.23
0.25
0.21
0.32
0.11
0.58
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
0.17 UG/L
0 Not Found UG/L
0 Not Found UG/L
14782 0.25 UG/L
Fit
517
508
676
127
691
682
978
984
988
829
905
257
915
362
596
639
887
960
927
949
967
955
809
957
972
976
892
681
435
916
Rf
0.000
0.000
0.000
0.000
0.000
0.000
1. 319
2.360
2.360
1.075
0.576
0.000
1.246
0.000
0.000
O.GCO
1.438
1.099
1.137
0.960
1.209
1. 16 9
1.304
1.051
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID: MC
Output File: AE01309.1A2
Data File: AE01309.MS
Name: AEOl309
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-C
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:29
Injected at: 03/27/99 09:24
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.83 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.58 2362
27.91 2390
28.51 2442
225
128
180
Area
1594 9
38477
13293
Cone Units
0.26 UG/L
0.33 UG/L
0.22 UG/L
Fit
963
981
952
Rf
0.310
0.586
0.304
Operator ID: MC
Output File: AE01310.1A2
Data File: AE01310.MS
Name: AE01310
QUANT REPORT
Sample: Location: 200 Dexter Ave SB1B-D
ID File: 826AEC2B.QCI
Page
Quant Time: 03/30/99 18:19
Injected at: 03/30/99 09:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/22/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3)
4)
5)
6)
7)
B)
9)
1,2-Dichlorobenzene-d4 (SG)
75-71-B Dichlo~odifluoromethane
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
Chloromethane
10) 75-35-4
Vinyl Chloride
Bromome,thane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methyle,ne Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
11) 75-09-2
12) 156-60-5
13)
14)
15)
16)
1 7)
18)
19)
20)
21)
22)
23)
24)
25)
26)
27)
28)
29)
30)
75-34-3
156-59-4
590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5
74-95-3
1,2, -Dichloropropane
Dibromornethane
75-27-4 Bromodichlorornethane
10061-01-5 Cis-1,3-Dichloropropene
108-BB-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.05
21.16
23.93
4.56
0.00
0.00
6.50
0.00
7.36
0.00
9.61
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.62
13.62
0.00
0.00
0.00
0.00
0.00
16.82
0.00
0.00
1204
1813
2051
391
438
467
557
574
631
737
823
874
94 3
1034
1034
1070
1079
1113
1137
1139
1167
1167
1259
1292
1310
1331
1390
1441
1465
1489
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area Cone Units
2065771 10.00 UG/L
943295 9.88 UG/L
579928 9.41 UG/L
4217 0.06 UG/L
Not Found UG/L
Not Found UG/L
2065 0.12 UG/L
Not Found UG/L
6288 0.06 UG/L
Not Found UG/L
700962 3.50 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found.UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
95509 0.42 UG/L
2655 0.03 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
4754381 16.78 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
994
999
94 5
859
412
671
703
974
689
989
528
485
319
302
387
416
0
252
581
980
869
425
102
0
848
36
984
471
736
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.099
0.430
0.000
0.000
0.000
0.000
0.000
1.372
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01310.1A2
Data File: AE01310.MS
Name.: AE01310
Quant Time: 03/30/99 18:19
Injected at: 03/30/99 09:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 Dexter Ave SB18-D
ID File: 826AEC28.QCI
Comment: Sampling: 02/22/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
3l) 142-28-9
3~) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36)
37)
38)
630-20-6
100-41-4
108-38-3
39) 106-42-3
4Q)
41)
42)
43)
44)
45)
46)
47)
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-1
103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52)
53)
54)
55)
56)
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
* Compound is ISTD
Compound R.T. Scan# Q ion Area Cone Units
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1521
0.00 1525
0.00 1556
0.00 1580
0.00 1649
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.52
1657
1658
1673
1,4-Dimethylbenzene (p-Xylene 19.52 1673
1,2-Dimethylbenzene lo-Xylene 20.23
Styrene 0.00
1734
1735
1771
1786
1825
1837
1847
1846
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.84
0.00
0.00
21.55
21.54
0.00 1868
21.81 1869
0.00 1880
22.49 1927
22.49
22.80
23.01
23.14
23.23
1927
1954
1972
1983
1991
23.76 2036
23.99 2056
0.00 2184
27.30 2340
78
166
129
107
112
Not Found UG/L
0 Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
131 0 Not Found UG/L
91 2598598 8.32 UG/L
91 10688695 19.61 UG/L
91 10688695 19.61 UG/L
11.30 UG/L 91
104
171
105
83
75
77
91
3045619
0 Not Found UG/L
0 Not Found UG/L
383208 1.26 UG/L
0 Not Found UG/L
0 Not Found UG/L
47568 0.27 UG/L
823402 2.38 UG/L
91 0 Not Found UG/L
105 1389946 4.98 UG/L
91 Not Found UG/L
119 389729 1.36 UG/L
105
105
119
146
146
91
146
75
180
3440661
167289
251111
17754
57829
267437
46230
13.04 UG/L
0.53 UG/L
0.99 UG/L
0.14 UG/L
0.40 UG/L
1.21 UG/L
0.39 UG/L
0 Not Found UG/L
25567 0.45 UG/L
651
463
663
348
0
994
998
998
994
470
971
438
306
729
992
457
968
717
803
997
959
920
94 9
942
808
734
0
919
Rf
0 .. 000
0.000
0.000
0.000
0.000
0.000
1.512
2.639
2.639
1.305
0.000
0.000
1.471
0.000
0.000
0.855
1.672
0.000
1.352
0.000
1.387
1.277
1.530
1.223
0.620
0.704
1.074
0.579
0.000
0. 276
Operator ID: MC
Output File: AE01310.1A2
Data File: AE01310.MS
Name: AE01310
QUANT REPORT
Sample: Location: 200 Dexter Ave SB18-D
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:19
Injected at: 03/30/99 09:42
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: sampling: 02/22/1999 by J. Conway, use 5.06 g
Last Calibration: 03/29/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.61 2366
27.95 2395
28.54 2446
225
128
180
Area
22261
562868
25395
Cone Units
0.40 UG/L
4.59 UG/L
0. 42 UG/L
Fit
952
989
959
Rf
0.269
0.594
0.291
Operator ID: MC
Output File: AE01311.1A2
Data File: AE01311.MS
Name: AE01311
QUANT REPORT
Sample: Location: 200 Dexter Ave SB18-E
ID Pile: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:20
Injected at: 03/30/99 10:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/199~ by J. Conway, use 4.42 g
Last Calibration: 03/29/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3)
4)
5)
6)
7)
8)
1,2-Dichlorobenzene-d4 (SG)
75-71-8 Dichlorodifluoromethane
74-87-3 Chloromethane
75-01-4 Vinyl Chloride
74-83-9 Bromomethane
75-00-3
9) 75-69-4
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
74-97-5
67-66-3
71-55-6
563-58-6
56-23-5
71-43-2
107-06-2
79-01-6
78-87-5 1,2, -Dichloropropane
16)
1?)
18)
19)
20)
21)
22)
23)
24)
2'5)
26)
27)
28)
2 9)
30)
74-95-3 Dibromomethane
75-27-4 Bromodichloromethane
10061-01-5 Cis-1,3-Dichloropropene
108-88-3 Toluene
10061-02-6 Trans-1,3-Dichloropropene
79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
14.02
21.12
23.91
4 . .54
0.00
0.00
6.39
0.00
7.35
0.00
9.60
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
13.58
13.60
14.64
15.10
0.00
0.00
0.00
16.79
0.00
0.00
1201
1810
204 9
389
438
467
548
573
630
737
822
874
94 3
1034
1032
1070
1079
1109
1137
1147
1163
1165
1254
1293
1310
1328
1390
14 38
14 65
14 95
96
95
152
85
47
62
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
2384312
905214
547666
4300
Cone Units
10.00 UG/L
8.21 UG/L
7.70 UG/L
0.05 UG/L
Not Found UG/L
0 Not Found UG/L
2109 0.11 UG/L
0 Not Found UG/L
8359 0.07 UG/L
Not Found UG/L
812843 3.51 UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
16651 0.06 UG/L
1220 0.01 UG/L
1161 0.02 UG/L
1057 0.02 UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
35588 0.11 UG/L
0 Not Found UG/L
Not Found UG/L
Fit
998
999
956
805
304
458
653
694
981
322
994
475
490
469
709
610
708
631
886
996
895
866
565
329
421
392
983
561
530
Rf
1.000
0.463
0.299
0.361
0.000
0.000
0.081
0.000
0.526
0.000
0. 971
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
l. 0 98
0. 4 30
0. 2 91
0.189
0.000
0. 00.0
0.000
l. 3 6 9
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AEOl3ll.lA2
Data File: AE01311.MS
Name: AE013ll
Quant Time: 03/30/99 18:20
Injected at: 03/30/99 10:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 Dexter Ave S818-E
ID File: 826AEC28.QCI
Comm~nt: Sampling: 02/25/1999 by J. Conway, use 4.42 g
Last Calibration: 03/29/99 Last Qcal Time: 03/29/99 09:28
31)
32)
33)
34)
35)
36)
37)
38)
39)
40)
41)
42)
4 3)
44)
4 5)
4 6)
47)
48)
49)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
60)
142-28-9
127-18-4
124-48-l
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
75-25-2
98-82-8
79-34-5
96-18-4
108-86-l
103-65-l
95-49-8
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-l
106-46-7
104-51-8
95-50-l
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethyl benzene
0.00
17.74
0.00
0.00
0.00
0.00
19.32
1,3-Dimethylbenzene (m-Xylene 19.48
1,4-Dimethylbenzene (p-Xylene 19.48
1,2-Dimethylbenzene (a-Xylene 20.21
Styrene 20.25
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2cDibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00
20.81
0.00
0.00
21.49
21.53
21.81
21.78
21.92
22.40
22.46
22.74
22.94
23.21
23.21
23.71
23.96
0.00
27.27
1521
1519
1556
1580
1649
1657
1655
1669
1669
1731
1735
1771
1783
1825
1837
1842
184 5
1869
1866
1878
1919
1924
1948
1966
1989
1989
2032
2053
2184
2337
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
14 6
146
91
146
75
180
Area Cone Units
Not Found UG/L
2190 0.03 UG/L
70243
146863
146863
55707
4552
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.20 UG/L
0.23 UG/L
0.23 UG/L
0.18
0.03
UG/L
UG/L
0 Not Found UG/L
61779 0.18 UG/L
0 Not Found UG/L
Not Found UG/L
15585 0.08 UG/L
104610
31738
117048
30365
86317
144568
78913
77324
106387
106387
61036
29081
14315
0.26
0.11
0.36
0.11
0.26
0. 47
0.22
0.27
0.72
0.63
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
0.24 UG/L
0.21 UG/L
Not Found UG/L
0.22 UG/L
Fit
280
919
683
450
516
65
981
993
994
658
902
400
933
494
61
779
872
961
962
984
891
966
952.
979
982
972
874
779
191
954
Rf
0.000
0.284
0.000
0.000
0.000
0.000
1.510
2.649
2.649
1.305
0.701
0.000
1.470
0.000
0.000
0.855
1. 673
1. 234
1.354
1.120
1.386
1.277
1.530
1.224
0.620
0. 703
1.075
0.579
0.000
0.276
Operator ID: MC
Output File: AE01311.1A2
Data File: AE01311.MS
Name: AE01311
QUANT REPORT
Sample: Location: 200 Dexter Ave SB18-E
ID File: 826AEC28.QCI
Page
Quant Time: 03/30/99 18:20
Injected at: 03/30/99 10:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: sampling: 02/25/1999 by J. Conway, use 4.42 g
Last Calibration: 03/29/99
61)
62)
63)
87-68-3
91-20-3
82-61-6
* Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/29/99 09:28
R.T. Scan# Q ion
27.57
27.91
28.52
2363
2392
2444
225
128
180
Area
22124
65598
23553
Cone Units
0.35 UG/L
0.46 UG/L
0.34 UG/L
Fit
958
989
921
Rf
0.269
0.596
0.291
Operator ID: MC
Output File: AE01312.1A2
Data File: AE01312.MS
Name: AE01312
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:32
Injected at: 03/27/99 11:22
Dilution Factor: 1.00
Instrument ID: ~0701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.23 g / Last Calibration: 03/25/99
Compound
1) •107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
··~ ... • Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.03 1201
21.13 1810
23.91 2048
96 2543766 10.00 UG/L
8.58 UG/L
8.62 UG/L
0.06 UG/L 4.55
0.00
0.00
6.40
0.00
7.35
0.00
9.59
390
438
466
548
573
629
737
821
0.00 874
0.00 943
0.00 1033
0.00 1033
0.00 1069
0.00 1079
0.00 1112
0.00 1136
0.00 1130
13.60 1165
0.00 1162
14.66 1256
0.00 1291
0.00 1309
0.00 1327
0.00 1390
16.79 1438
0.00 1464
0.00 1494
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
961028
601324
3836
1162
Not Found UG/L
Not Found UG/L
0.06 UG/L
0 Not Found UG/L
0.05 UG/L
Not Found UG/L
0.88 UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
6280
278776
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
17278
864
0.08 UG/L
Not Found UG/L
0.01 UG/L
0 Not Found UG/L
0 Not Found UG/L
0 Not Found UG/L
Not Found UG/L
57228 0.19 UG/L
Not Found UG/L
0 Not Found UG/L
Fit
998
999
94 7
801
216
698
633
975
155
988
130
234
310
631
102
642
491
252
890
981
909
819
288
160
661
432
983
687
596
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0. 074
0.000
0.455
0.000
1.252
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.897
0.000
0.255
0.000
0.000
0.000
0.000
1.195
0.000
0.000
QUANT REPORT Page 2
Operator ID: MC
Output File: AE01312.1A2
Data File: AE01312.MS
Name: AE01312
Quant Time: 03/27/99 19:32
Injected at: 03/27/99 11:22
Dilution Factor: 1.00
Instrument ID: 20701-1284
Sample: Location: 200 Dexter Ave., SB18-F
ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway, use 4.23 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31)
32)
33)
34)
35)
36)
37)
38)
3 9)
4 0)
41)
142-28-9
127-18-4
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
4 9)
50)
51)
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
108-67-8
106-43-4
98-06-6
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00
17.75
0.00
0.00
0.00
0.00
19.34
1,3-Dimethylbenzene (m-Xylene 19.48
1,4-Dimethylbenzene (p-Xylene 19.48
1,2-Dimethylbenzene (a-Xylene 20.21
Styrene 20.23
1521
1520
1556
1579
1648
1656
1656
1669
1669
1731
1733
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
0.00 1770
·20.82 1783
0.00 1825
0.00 1836
0.00 1842
21.53 1844
21.83 1870
21.79
21.91
22.40
22.45
0.00
22.97
23.21
23.21
23.74
0.00
0.00
27.26
1866
1877
1919
1923
1954
1968
1989
1989
2034
2055
2178
2335
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
3790 0.06 UG/L
53222
88151
88151
42 910
11594
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.16 UG/L
0.15 UG/L
0.15 UG/L
0.16 UG/L
0.08 UG/L
Not Found UG/L
33064 0.10 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
47960 0.13 UG/L
20765 0.07 UG/L
120689
30537
64 644
46400
0. 42 UG/L
0.13 UG/L
0.21 UG/L
0. 16 UG/L
0 Not Found UG/L
64044 0.24 UG/L
65113
65113
39598
0.45 UG/L
0.46 UG/L
0.15 UG/L
0 Not Found UG/L
Not Found UG/L
14 938 0.19 UG/L
Fit
4 94
941
503
217
697
695
978
982
984
778
937
667
938
404
466
680
945
932
957
971
931
927
515
927
983
977
926
658
511
938
Rf
0.000
0.266
0.000
0.000
0.000
0.000
1.319
2.360
2.360
1.076
0.576
0.000
1.245
0.000
0.000
0.000
l. 438
1.099
1.137
0.960
1.209
1 . 16 9
0.000
1.051
0.575
0.560
1.005
0.000
0.000
0.303
Operator ID: MC
Output File: AE01312.1A2
Data File: AE01312.MS
Name: AE01312
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-F
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:32
Injected at: 03/27/99 11:22
Dilution Fact.or: 1. 00
Instrument ID: 20701-1284
Comment.: Sampling: 02/25/1999 by J. Conway, use 4.23 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.59 2364 225 16274 0.21
62) 91-20-3 Naphthalene 27.92 2392 128 29056 0.20
63 I 82-61-6 1,2,3-Trichlorobenzene 28.51 2443 180 16610 0.22
* Compound is ISTD
Units Fit. Rf
--------UG/L 956 0.310
UG/L 982 0.586
UG/L 905 0.304
Operator ID: MC
Output File: AE01313.1A2
Data File: AE01313.MS
Name: AE01313
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-G
ID File: 826AEC25.QCI
Page 1
Quant Time: 03/27/99 19:34
Injected at: 03/27/99 12:02
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.54 g J Last Calibration: 03/25/99
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1,2-Dichlorobenzene-d4 (SGl
4) 75-71-8 Dichlorodifluoromethane
5) 74-87-3 Chloromethane
6) 75-01-4
7) 74·83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22)
23)
24)
25)
26)
107-06-2
79-01-6
78-87-5
74-95-3
75-27-4
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1, 1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2, -Dichloropropane
Dibromomethane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 1~061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
14.05
21.15
23.93
4.54
0.00
0.00
6. 4 9
0.00
7.37
8.58
9.61
10.20
10.98
12.05
0.00
12.47
12.59
12.97
13.26
13.28
13.62
13.60
14.68
0.00
0.00
15.47
1202
1811
2049
388
438
465
556
573
631
733
822
872
939
1030
1032
1067
1077
1ll0
1134
1136
1165
ll64
1256
1291
1309
1324
16.21 1387
16.82 1439
17.15 1468
0.00 1491
96
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
Area
1962457
734686
4 77864
8715
1916
10731
1200
446491
4838
1584
3237
2724
4434
2416
6645
2803
19807
2657
4717
2782
Cone Units
10.00 UG/L
8.50 UG/L
8.88 UG/L
0.17 UG/L
Not Found UG/L
Not Found UG/L
0.13 UG/L
Not Found UG/L
0.12 UG/L
.0. 03 UG/L
1.84 UG/L
0.06 UG/L
0.02 UG/L
0.04 UG/L
Not Found UG/L
0.03 UG/L
0.05 UG/L
0.02 UG/L
0. 11 UG/L
0.05 UG/L
O.ll UG/L
0.04 UG/L
0.09 UG/L
Not Found UG/L
Not Found UG/L
0.04 UG/L
2917 0.04 UG/L
67628 0.29 UG/L
69614 1.10 UG/L
Not Found UG/L
Fit
999
999
949
889
60
625
721
769
984
907
987
745
744
869
825
755
851
793
773
915
988
954
939
264
518
787
746
983
724
816
Rf
1.000
0.441
0.275
0.258
0.000
0.000
0.074
0.000
0.455
0.208
1.239
0.386
0.393
0.432
0.000
0.406
0.434
0.537
0.302
0.316
0.897
0.355
0.255
0.000
0.000
0.327
0.340
1.195
0.324
0.000
Operator ID: MC
Output File: AE01313.1A2
Data File: AE01313.MS
Name: AE01313
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB16-G
ID File: 826AEC25.QCI
Page 2
Quant Time: 03/27/99 19:34
Injected at: 03/27/99 12:02
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.54 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-26-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35) 108-90-7
36) 630-20-6
37) 100-41-4
38) 108-36-3
39) 106-42-3
40) 95-47-6
41) 100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 106-86-1
47) 103-65-1
46) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52) 95-63-6
53) 135-98-8
54) 99-87-6
55) 541-73-1
56) 106-46-7
57) 104-51-8
58) 95-50-1
59) 96-12-8
60) 120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
18.18 1557
0.00 1578
19.23 1646
19.30 1653
19.35 1656
1,3-Dimethylbenzene (m-Xylene 19.52 1671
1,4-Dimethylbenzene (p-Xylene 19.52 1671
1,2-Dimethylbenzene (a-Xylene 20.23 1732
Styrene
Bromoform
Isopropyl benzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chlorotoluene
1,3,5-Trimethylbenzene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
20.25 1734
0.00 1769
20.83 1783
0.00 1824
0.00 1835
21.49 1840
21.54 1845
21.79 1866
21.80 1867
21.95 1880
22.42 1920
22.50 1926
22.80 1952
23.00 1970
23.06 1975
23.25 1991
23.77 2035
23.97 2053
0.00 2182
27.30 2338
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
0 Not Found UG/L
10638
469
0.20 UG/L
0.01 UG/L
0 Not Found UG/L
14569
14 6 3
674 50
132401
1324 01
53800
14 918
76302
0.10 UG/L
0.02 UG/L
0.26 UG/L
0.29 UG/L
0.29 UG/L
0.25 UG/L
0. 13 UG/L
Not Found UG/L
0.31 UG/L
0 Not Found UG/L
Not Found UG/L
32565
99068
86523
146393
59339
70424
81391
101652
93589
28788
"94 56 0
94857
60519
29207
0.24 UG/L
0.35 UG/L
0.40 UG/L
0.66 UG/L
0.31 UG/L
0.30 UG/L
0.35 UG/L
0.40 UG/L
0.45 UG/L
0.26 UG/L
0.86 UG/L
.0. 48 UG/L
0.59 UG/L
Not Found UG/L
0.49 UG/L
Fit
513
972
736
570
956
829
992
997
997
887
871
325
978
4 52
431
960
990
970
966
987
937
975
824
962
976
982
986
727
342
950
Rf
0.000
0.266
0.214
0.000
0.717
0.318
1.320
2.360
2.360
1.076
0.576
0.000
1.246
0.000
0.000
0.685
1. 439
1 . 10 0
1.138
0.961
1. 209
1.169
1.305
1.051
0.575
0.560
1.004
0.526
0.000
0.303
Operator ID: MC
Output File: AE01313.~A2
Data File: AE01313.MS
Name: AE01313
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-G
ID File: 826AEC25.QCI
Page
Quant Time: 03/27/99 19:34
Injected at: 03/27/99 12:02
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 4.54 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
Compound R.T. Scan# Q ion Area Cone
---------------------------------------- -------- --------
61) 87-68-3 Hexachlorobutadiene 27.62 2365 225 32172 0.53
62) 91-20-3 Naphthalene 27.96 2394 128 37819 0.33
63) 82-61-6 1,2,3-Trichlorobenzene 28.55 2445 180 27279 0.46
• Compound is ISTD
Units Fit Rf
--------UG/L 980 0.309
UG/L 971 0.586
UG/L 963 0.304
Operator ID: MC
Output File: AE01314.1A~
Data File: AE01314.MS
Name: AE01314
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-H
Page
Quant Time: 03/27/99 19:41
Injected at: 03/27/99 12:43
Dilution Factor: 1.00
Instrument ID: r20701-1284
><? ~~~Ptj ID File: 826AEC25.QCI
Comment: Sampling: 02/25/1999 by J. Conway,
Last Calibration: 03/25/99
use 7.48 g j
Compound
1) *107-06-2 Fluorobenzene
2) 4-Bromofluorobenzene (SG)
3) 1, 2-Dichlorobenzene-d4 (SG)
4) 75-71-8
5) 74-87-3
6) 75-01-4
7) 74-83-9
8) 75-00-3
9) 75-69-4
10) 75-35-4
11) 75-09-2
12) 156-60-5
13) 75-34-3
14) 156-59-4
15) 590-20-7
16) 74-97-5
17) 67-66-3
18) 71-55-6
19) 563-58-6
20) 56-23-5
21) 71-43-2
22) 107-06-2
23) 79-01-6
24) 78-87-5
25) 74-95-3
26) 75-27-4
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Trans-1,2-Dichloroethene
1,1-Dichloroethane
Cis-1,2-Dichloroethene
2,2-Dichloropropane
Bromochloromethane
Chloroform
1,1,1-Trichloroethane
1,1-Dichloropropene
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethene
1,2,-Dichloropropane
Di b romomet hane
Bromodichloromethane
27) 10061-01-5 Cis-1,3-Dichloropropene
28) 108-88-3 Toluene
29) 10061-02-6 Trans-1,3-Dichloropropene
30) 79-00-5 1,1,2-Trichloroethane
• Compound is ISTD
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion Area Cone Units
14.06 1203
21.16 1812
23.94 2050
96. 1816914 10.00 UG/L
4.95 UG/L
4.89 UG/L
0.00 UG/L 4.55
0.00
0.00
6. 42
0.00
7.36
0.00
9.61
389
438
457
550
572
630
737
822
0.00 874
0.00 942
0.00 1033
0.00 1033
0.00 1069
12.58 1076
0.00 1111
0.00 1136
0.00 1138
13.63 1166
0.00 1165
14.69 1257
0.00 1291
0.00 1309
0.00 1327
0.00 1389
16.82 1440
0.00 1463
0.00 1492
95
152
85
47
61
96
49
101
96
49
61
63
61
97
49
83
97
75
117
78
62
130
63
93
83
75
91
75
83
389754
251241
5212
0 Not Found UG/L
0 Not Found UG/L
4 74 5
584 0
0.00 UG/L
Not Found UG/L
0.00 UG/L
0 Not Found UG/L
288629 0.00 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0 Not Found UG/L
2174
Not Found UG/L
0.00 UG/L
Not Found UG/L
0 Not Found UG/L
21434
1648
41517
Not Found UG/L
0.52 UG/L
Not Found UG/L
0.40 UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
Not Found UG/L
0.33 UG/L
0 Not Found UG/L
0 Not Found UG/L
Fit
998
1000
953
853
151
574
770
699
981
644
985
607
634
592
513
631
742
788
496
755
995
898
84 9
331
280
488
569
987
637
720
Rf
1.000
0.434
0.283
-0.011
0.000
0.000
-0.050
0.000
-0.036
0.000
-3.630
0.000
0.000
0.000
0.000
0.000
-0.071
0.000
0.000
0.000
0.225
0.000
0.023
0.000
0.000
0.000
0.000
0.683
0.000
0.000
, Ope,·ator ID: MC
Output File: AE01314.1A2
Data File: AE01314.MS
Name: AE01314
QUANT REPORT
Sample: Location: 200 Dexter Ave., SB18-H
ID file: 826AEC25.QCI
Page 2
Quant Time: 03/27/99 19:41
Injected at: 03/27/99 12:43
Dilution Factor: 1. 00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 7.48 g
Last Calibration: 03/25/99 Last Qcal Time: 03/25/99 08:34
31) 142-28-9
32) 127-18-4
33) 124-48-1
34) 106-93-4
35)
3 6)
37)
38)
3 9)
4 0)
41)
108-90-7
630-20-6
100-41-4
108-38-3
106-42-3
95-47-6
100-42-5
42) 75-25-2
43) 98-82-8
44) 79-34-5
45) 96-18-4
46) 108-86-1
47) 103-65-1
48) 95-49-8
49) 108-67-8
50) 106-43-4
51) 98-06-6
52)
53)
54)
55)
56)
57)
58)
59)
6 0)
95-63-6
135-98-8
99-87-6
541-73-1
106-46-7
104-51-8
95-50-1
96-12-8
120-82-1
• Compound is ISTD
Compound R.T. Scan# Q ion
1,3-Dichloropropane
Tetrachloroethene
Dibromochloromethane
1,2-Dibromoethane
Chlorobenzene
1,1,1,2-Tetrachloroethane
Ethylbenzene
0.00 1520
17.79 1523
0.00 1555
0.00 1578
19.24
0.00
19.35
1,3-Dimethylbenzene (m-Xylene 19.54
1,4-Dimethylbenzene (p-Xylene 19.54
1,2-Dimethylbenzene (a-Xylene 20.24
Styrene 20.15
1647
1655
1657
1673
1673
1733
1725
Bromoform
Isopropylbenzene
1,1,2,2-Tetrachloroethane
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Ch1orotoluene
1,3,5-Trimethy1benzene
4-Ch1orotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
4-Isopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dich1orobenzene
1,2-Dibromo-3-Ch1oropropane
1,2,4-Trichlorobenzene
20.67 1770
20.85 1785
0.00 1824
0.00 1835
21.53 1843
21.54 1845
21.79 1866
21.77 1864
21.92 1877
22.41 1919
22.51
0.00
23.03
23.11
23.26
23.77
24.01
0.00
27.31
1927
1953
1972
1978
1992
2036
2056
2182
2339
78
166
129
107
112
131
91
91
91
91
104
171
105
83
75
77
91
91
105
91
119
105
105
119
146
146
91
146
75
180
Area Cone Units
Not Found UG/L
4222 0.00 UG/L
Not Found UG/L
0 Not Found UG/L
5120 0.29 UG/L
Not Found UG/L
75361 0.17 UG/L
89546 0.00 UG/L
89546
19309
4122
0.00 UG/L
0.17 UG/L
0.40 UG/L
929 0.73 UG/L
46345 0.10 UG/L
Not Found UG/L
Not Found UG/L
28874 0.17 UG/L
71243 0.00 UG/L
65836 0.64 UG/L
67189 0.36 UG/L
37972 0.02 UG/L
59275 0.14 UG/L
21101 0.00 UG/L
0 Not Found UG/L
66333
3 74 90
82881
60235
19489
0.00 UG/L
0.00 UG/L
0.56 UG/L
0.00 UG/L
0.00 UG/L
0 Not Found UG/L
17254 0.00 UG/L
Fit.
378
943
333
426
877
544
985
986
987
788
929
874
909
341
537
867
937
936
939
968
94 9
94 7
628
964
976
963
94 0
74 5
362
936
Rf
0.000
-0.051
0.000
0.000
0.097
0.000
2.430
-1.313
-1.313
0.617
0.058
0.008
2.672
0.000
0.000
0.936
-1.817
0.567
1.036
9. 613
2.367
-3.437
0.000
-1.132
-17.357
0.820
-1.022
-0.450
0.000
-0.229
Operator ID: MC
Output File: AE01314.1A2
Data File: AE01314.MS
Name: AE01314
QUANT REPORT
Sample: Location: 200 DexteJ:c Ave., SB18-H
ID File: 826AEC25.QCI
Page 3
Quant Time: 03/27/99 19:41
Injected at: 03/27/99 12:43
Dilution Factor: 1.00
Instrument ID: 20701-1284
Comment: Sampling: 02/25/1999 by J. Conway, use 7.48 g
Last Calibration: 03/25/99
61) 87-68-3
62) 91-20-3
63) 82-61-6
• Compound is ISTD
Compound
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Last Qcal Time: 03/25/99 08:34
R.T. Scan# Q ion
27.62 2366
27.98 2396
28.56 2446
225
128
180
Area
18488
30909
18441
Cone Units
0.00 UG/L
0.04 UG/L
0.12 UG/L
Fit
939
977
893
Rf
-0.175
4. 213
0.831