redacted - louisiana energy services, llc, national enrichment … · 2020. 1. 7. · cc: tyrone d....

FEB 2 6 2010LES-10-00042-NRC

Document Control DeskDirectorOffice of Nuclear Material Safety and SafeguardsU.S. Nuclear Regulatory Commission

Washington, DC 20555-0001

Louisiana Energy Services, LLCNRC Docket No. 70-3103

Subject: National Enrichment Facility (NEF) Semiannual Effluent Release Report

Pursuant to 10 CFR 70.59 Effluent monitoring reporting requirements, Louisiana EnergyServices (LES) respectfully submits the Semiannual Effluent Release Report for the NationalEnrichment Facility (NEF) monitoring period of July 1, 2009 to December 31, 2009. This reportspecifically addresses release of licensed, principal radionuclides in liquid or gaseous form touncontrolled areas.If there are any questions with regard to this submission, please contact LES EnvironmentalCompliance Officer Patrick Thurman at 575.394.6024.

Sincerely,

Gregory, OD Smith,Chief Operating Officer and Chief Nuclear Officer

Enclosure:Semiannual Effluent Release Report

LES,PO Box 1789, Eunice, New Mexico 88231,USA T +1 575 394 4646 F: +1 575 394 4545 W: www.urenco.com/LES

cc:

Tyrone D. Naquin, Project ManagerTwo White FlintMail Stop EBB2-C40M11545 Rockville PikeRockville, MD 20852-2738

Deborah A. SeymourChief, Construction Projects Branch 1Sam Nunn Atlanta Federal Center, 23 T8561 Forsyth Street, SWAtlanta, GA 30303-8931

National Enrichment Facility

Facility Operating License. SNM-2010

Semi.Annual Radioactive Effluent Release Report

July 1, 2009 through December 31, 2009

NATIONALENRICHMENTFACILITY

February 18, 2010

Page 1 of 77

National Enrichment Facility Semi-Annual Radioactive Effluent Release Report

Contents

Introduction .................................................................................................................................................. 4

Release Point Inform ation ............................................................................................................................ 4

Gaseous Release Locations ............................................................................................................... 4

Gaseous Release Data ............................................................................................................................. 5

Table 1: Gaseous Effluent, Gross Alpha ........................................................................................... 5

Table 2: Gaseous Effluent, Gross Beta .............................................................................................. 6

Table 3: Gaseous Effluent, Radionuclides (Quarterly Filter Composite Results) ............................. 8

Sam pling Data Gaps .............................................................................................................................. 8

Sam pling program deviations and program adjustm ents .................................................................... 8

Significant Trends .................................................................................................................................. 9

Liquid Release Locations ........................................................................................................................... 9

Liquid Release Data ..................................................................................................... ; ......................... 9

Table 4: Domestic Wastewater Effluent, Radionuclides ......... ..................... 9

Sam pling program deviations and program adjustm ents ............................................................ 10

Significant Trends ................................................................................................................................ 10

Dose to M em bers of the Public .................................................................................................................. 10

Supplem ental Inform ation .......................................................................................................................... 11

Description of Sam pling Equipm ent ............. ...................................................................................... 11

Description of sam pling procedure ..................................................................................................... 11

Analytical procedure ............................................................................................................................... 11

Calculation m ethods ............................................................................................................................... 11

Error estim ates ........................................................................................................................................ 12

M inim um Detectable Activity (M DA) Calculation ............................................................................. 13

2

Page 2 of 77


Quality of Results .............. ................................................ 13

Calibratio n Proced ures ............................................................................................................................ 14

U n u su al R e le ase s ................................................................................... .......................................... ...... 14

APPENDIX A - Plot Plan . .............................................. ........... 15

APPENDIX B - Lab Data Sheets........................................ 17A PPEN D IX B - Lab D ata sheets ...... ................ ......:. ............. .................................. ........................... .. 1

APPENDIX C - Sampling Procedures ...................................................... 18

APPENDIX D - Calibration Procedures ....................................... ............. 19

3Page 3 of 77

National Enrichment Facility Semi-Annual Radioactive Effluent Release Report '

Introduction

A Semi-Annual Report is required under 10 CFR 70.59 and 10 CFR 40.65 to report the quantity of

principal radionuclides released to unrestricted areas from licensed nuclear facilities. In February 2009

Louisiana Energy Services (LES) began testing centrifuges using small quantities of Uranium Hexafluoride

at the National Enrichment Facility (NEF), located approximately four miles east of Eunice, NM.

During the period that began on July 1, 2009 and ended December 31, 2009, Uranium Hexafluoride was

located within the Centrifuge Assembly Building. Potential releases of radioactive effluents would have

originated from gaseous (exhaust system) or liquid (domestic wastewater / sewage) effluents from this

structure. A review of the data for gaseous and liquid effluents shows that there were no releases to the

public that would have exceeded the requirements set forth in 1OCFR20.1301.

Release Point Information

Gaseous Release LocationsCentrifuge Test and Post Mortem Facilities (CTPMF) Exhaust Filtration System

The Exhaust Filtration System (EFS) provides exhaust of potentially hazardous contaminants from the

CTPMF. The system also ensures the CTPMF is maintained at a negative pressure with respect to

adjacent areas. The EFS is located in the Centrifuge Assembly Building (CAB) and monitored from the

Control Room (Appendix A, Plot Plan).

The total airflow to be handled by the EFS is adequate to maintain negative pressure in the CTPMF. The

EFS consists of a duct network that serves the CTMPF and operates at negative pressure. The ductwork

is connected to a filter station that can handle 1i00% of the effluent. Work applications that require the

EFS to be operational can be manually shut down if the system shuts down.

For the EFS, the minimum required filter configuration is one pre-filter, one potassium carbonate

impregnated activated carbon filter, and one High-Efficiency Particulate Air (HEPA) filter. Additional

filters may be used to provide adequate airflow. The pre-filter removes dust and debris, the potassium

carbonate impregnated activated carbon filter removes Hydrogen Fluoride (HF), and the HEPA filter

removes remaining uranic particles from the air'stream. After filtration, the clean gases pass through a

fan which maintains the negative pressure upstream of the filter station. The clean gases are then

discharged through the monitored (alpha and HF) stack on the CAB.

The ABPM201S (alpha particulate monitor) is located adjacent to the filter train in the CTPMF EFS

exhaust stack and receives a stream of air from the downstream side of the filters. The filter assembly is

equipped with an isokinetic nozzle and properly located within the exhaust stack to ensure laminar flow.

This ensures that particulate matter being collected on the filter is representative of particulate matter

being released to the environment. The sample volume is pulled through a 47mmMillipore fiberglass

4

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filter to collect particulate matter. The filters are changed out on a weekly basis and sent to an off-site

analytical laboratory for alpha, beta, and isotopic uranium analysis.

Gaseous Release Data

Reporting period: July 1, 2009 - December 31, 2009

Stack Location: Centrifuge Assembly Building, Centrifuge Test and Post Mortem Facilities Exhaust

Filtration System

Stack Total Flow: 1.89 m3/sec

Table 2 of Appendix B to 10 CFR Part 20, Effluent Concentrations, Air, Class D, 234U, 235u, 238U, (lCi/ml):234U = 3E-12,235 = 3E-12,238U 3E-12

Table 1: Gaseous Effluent, Gross Alpha

Total Gross Gross Alpha Gross CTPM Exhaust.

Field Sample ID

1300-562-IMAl090713

1300-562-IMAl090720

1300-562-1MAl090727

1300-562-iMAl090803

1300-562-1MA1090810

1300-562-IMAl090817

1300-562-1MA1090824

1300-562-IMAI090902

1300-562-IMAl090909

1300-562-IMAl090916

1300-562-IMAl090923

1300-562-1MAl090930

Sample Time AlphaPeriod (min) Results

(uci/ml)

7/6/2009- 10139 <1.18E-157/13/2009

7/13/2009- 10053 <1.23E-157/20/2009

7/20/2009- 10062 <6.65E-167/27/2009

7/27/2009- 10111 <6.18E-168/3/2009

8/3/2009- 10082 <1.26E-158/10/2009

8/10/2009- 10085 <8.49E-168/17/2009

8/17/2009- 10050 <1.02E-158/24/2009

8/24/2009- 13001 <9.73E-169/2/2009

9/2/2009- 10033 <1.25E-159/9/2009

9/9/2009- 10116 <9.33E-169/16/2009

9/16/2009- 10085 <7.63E-169/23/2009

9/23/2009- 10349 <8.21E-16

ErrorEstimate

(uCi/ml)

3.78E-1 6

3.83E-16

2.63E-16

MDA

(uCi/ml)

1.18E-15

1.23E-15

6.65E-16

Flow

(M3 / sec)

1.89

1.89

1.89

ResultBelow LLD

ResultBelow LLD

ResultBelow LLD

Alpha Filtration System QuantityReleased

Ci

1.97E-16 6.18E-16 1.89 ResultBelow LLD



2.70E-16

3.22E-16

4.35E-16

2.48E-16

2.31E-16

1-.02E-15

9.73E-16

1.25E-15

9.33E-1 6

7.63E-16

1.89

1.89

1.89

1.89

1.89

ResultBelow LLD

,ResultBelow LLD

ResultBelow LLD

ResultBelow LLD

ResultBelow LLD

ResultBelow LLD

2.24E-16 8.21E-16 1.899/30/2009

5Page 5 of 77


Total Gross Gross AlphaSample Time Alpha ErrorPeriod (min) Results Estimate

Gross CTPM ExhaustAlpha Filtration System QuantityMDA Flow ReleasedField Sample ID

(uCi/ml) (uCi/ml) (uCi/ml) (m3 / sec) Ci

1300-562-1MA1 9/30/2009- 10184 <1.04E-15 3.02E-16 1.04E-15 1.89 Result091007 10/7/2009 Below LLD



1300-562-IMAl 10/21/2009- Result130-2 A 10/2/2009- 10095 <8.43E-16 2.56E-16 8.43E-16 1.89 Belt091028 10/28/2009 Below LL0

1300-562-1MAI 10/28/2009- 10061 <6.97E-16 2.84E-16 6.97E-16 1.89 Result091104 11/4/2009 Below LLD


1300-562-1MA1 11/12/2009- 9656 <7.OOE-16 2.10E-16 7.OOE-16 1.89 Result091119 11/19/2009 Below LLD

1300-562-1MAl 11/19/2009- 8705 <1.28E-15 4.23E-16 1.28E-15 1.89 Result091125 11/25/2009 Below LLD


1300-562-iMA1 12/2/2009- Result10320 <8.77E-16 3.48E-16 8.77E-16 1.89091209 12/9/2009 Below LLD

1300-562-IMAl 12/9/2009- 9849 <1.07E-15 3.09E-16 1.07E-15 1.89 Result091216 12/16/2009 Below LLD

1300-562-iMAl 12/16/2009- 9978 <9.18E-16 3.82E-16 9.18E-16 1.89 Result091223 12/23/2009 Below LLD

1300-562-iMAl 12/23/2009- Rsl10086 <9.30E-16 . 3.30E-16 9.30E-16 1.89 Result091230 12/30/2009 Below LLD

Table 2: Gaseous Effluent, Gross BetO061

Total Gross Gross Beta Gross CTPM ExhaustSample Time Beta Error Beta Filtration System Quantity

Field Sample ID Period (min) Results Estimate MDA Flow Released

(uCi/ml) (uCi/ml) (uCi/ml) (m3 / sec) Ci1300-562-1MAl 7/6/2009- 10139 <1.71E-15 6.84E-16 1.71E-15 1.89 Result

090713 7/13/2009 Below LLD

1300-562-1IMA1 7/13/2009- 10053 <1.94E-15 7.11E-16 1.94E-15 1.89 Result090720 7/20/2009 Below LLD


1300-562-IMAI 7/27/2009- 10111 <2.02E-15 7.74E-16 2.02E-15 1.89 Result090803 8/3/2009 Below LLD

6

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TotalSample TimePeriod (min)Field Sample ID

GrossBeta

Results

(uCi/ml)

Gross BetaError

Estimate

(uCi/ml)

Gross CTPM ExhaustBeta Filtration System QuantityMDA FlowReleased

(uCi/ml) (m3 / sec) Ci

1300-562-1MA1 8/3/2009- 10082 <2.32E-15 8.74E-16 2.32E-15 1.89 Result

090810 8/10/2009 Below LLD

1300-562-1MA1 8/10/2009- 10085 <1.78E-15 6.49E-16 1.78E-15 1.89 Result

090817 8/17/2009 Below LLD

1300-562-1MA1 8/17/2009- 10050 <1.87E-15 6.91E-16 1.87E-15 1.89 Result

090824 8/24/2009 Below LLD

1300-562-IMAI 8/24/2009- 13001 <2.39E-15 8.49E-16 2.39E-15 1.89 Result090902 9/2/2009 Below LLD

1300-562-iMA1 9/2/2009- 10033 <2.22E-15 8.02E-16 2.22E-15 1.89 Result

090909 9/9/2009 Below LLD

1300-562-1MA1 9/9/2009- 10116 <1.77E-15 6.82E-16 1.77E-15 1.89 Result

090916 9/16/2009 Below LLD

1300-562-1MA1 9/16/2009- 10085 <1.95E-15 6.90E-16 1.95E-15 1.89 Result

090923 9/23/2009 Below LLD

1300-562-1MA1 9/23/2009- 10349 <1.77E-15 6.44E-16 1.77E-15 1.89 Result

090930 9/30/2009 Below LLD

1300-562-1MA1 9/30/2009- 10184 <1.54E-15 5.72E-16 1.54E-15 1.89 Result

091007 10/7/2009 Below LLD

1300-562-1MA1 10/7/2009- 9688 <1.91E-15 6.75E-16 1.91E-15 1.89 Result

091014 10/14/2009 Below LLD

1300-562-1MA1 10/14/2009- 10087 <1.89E-15' 6.88E-16 1.89E-15 1.89 Result091021 10/21/2009 Below LLD

1300-562-1MA1 10/21/2009- 10095 <1.82E-15 6.59E-16 1.82E-15 1.89 Result

091028 10/28/2009 Below LLD

1300-562-1MA1 10/28/2009- 10061 <1.87E-15 6.99E-16 1.87E-15 1.89 Result

091104 11/4/2009 Below LLD

1300-562-1MA1 11/4/2009- 11910 <1.78E-15 6.55E-16 1.78E-15 1.89 Result

091112 11/12/2009 Below LLD

1300-562-1MAl 11/12/2009- 9656 <1.78E-15 6.53E-16 1.78E-15 1.89 Result

091119 11/19/2009 Below LLD

1300-562-1MA1 il/19/2009- 8705 <2.22E-15 8.31E-16 2.22E-15 1.89 Result091125 11/25/2009 Below LLD

1300-562-1MA1 11/25/2009- 10078 <2.05E-15 7.53E-16 2,05E-15 1.89esult091202 12/2/2009 Below LLD

1300-562-iMAl 12/2/2009- 10320 <1.98E-15 9.35E-16 1,98E-15 1.89 Result091209 12/9/2009 Below LLD

1300-562-iMAl 12/9/2009- 9849 <2.47E-15 1.15E-15 2,47E-15 1.89 Result

091216 12/16/2009 Below LLD1300-562-1MA1 12/16/2009- Result

091223 12/23/2009 9978 <2.30E-15 1.07E-15 2.30E-15 1.89 Belo091223 12/23/2009 Below LLD

1300-562-MAl 12/23/2009- 10086 <2.1OE-15 9.79E-16 2.10E-15 1.89Result

091230 12/30/2009 Below LLD

7

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See Appendix B for Laboratory Data Sheets

Table 3: Gaseous Effluent. Radionuclides (Ouarterlv Filter Comnosite ResultslTable 3: Gaseous Effluent Radionuclides f OuarterIv FilterComnosite Resultsl

CTPM

ExhaustFiltrationSystem

FlowRadionuclide /

Sample IDSample TotalPeriod Time

ErrorResults Estimate MDA

% of

Quantity Table 2 of

Released Appx B to10 CFR

Ci Part 20Values

(min) (uCi/ml) (uCi/ml) (uCi/ml) (M3 / sec)

U-234 / 1300-562- 7/6/2009- Result Result Below

UMA4 3RD QTR 9/30/2009 124166 <7.97E-17 7.97E-17 5.22E-17 1.89 Below Error ErrorEstimate Estimate

U-234 / 1300-562- 9/30/2009- Result Result Below

-MA3 4TH QTR 12/30/2009 130697 <6.39E-17 6.39E-17 1.01E-16 1.89 Below Error ErrorEstimate EstimateResult Result Below

U-IMA5 3RD QTR 9/30/2009 124166 <8.49E-17 8.49E-17 6.43E-17 1.89 Below Error ErrorEstimate Estimate

U-235 / 1300-562- 9/30/2009- Result Result Below130697 <5.11E-17 3.98E-18 5.11E-17 1.891MA1 4TH QTR 12/30/2009 Below MDA MDA

U-238 / 1300-562- 7/6/2009- Result Result Below124166 <8.95E-17 5.61E-17 8.95E-17 1.891IMA1 3RD QTR 9/30/2009 Below MDA MDA

U-238 / 1300-562- 9/30/2009- Result Result Below130697 <8.35E-17 3.21E-17 8.35E-17 1.891MA1 4TH QTR 12/30/2009 Below MDA MDA


Sampling Data Gaps

There were no sampling data gaps for the reporting period beginning on July 1, 2009 and ending on

December 31, 2009. The EFS was not active during power outages and down times, therefore no

effluent was released during those instances. For a list of down times and power outages, see Sampling

program deviations and program adjustments.

Sampling program deviations and program adjustments

8/24 to 9/2/09 Power outage from 8/29 to 9/1, EFS was deactivated during this time. There was no release of

effluents by this pathway during the power outage. Alpha turned off 8/29 at 03:58 and was

not reactivated until 9/1 at 13:22 following CAB filter change out.

11/4 to Monitor was shut down from 11/7 at 11:45 to 11/8 at 14:40 for CAB power outage. EFS was

11/12/09 deactivated during the interval. No release resulted.

8Page 8 of 77


11/19 to Filter changed at 6 days rather than 7 due to 4 day holiday weekend and lack of escort during

11/25/09 that time. Volume was sufficient to meet MDLs.

12/16 to Monitor and EFS were turned off on 12/17 from 03:08 to 13:20 for power outage in the CAB.

12/23/09 Changed on seventh day as the volume was acceptable.

Significant Trends

This Semiannual Radioactive Effluent Release Report is the second submitted by Louisiana Energy

Services for the National Enrichment Facility. This report and the previous report display alpha, beta,

and isotopic uranium concentrations in CTMF effluent exhaust that are not distinguishable from

background environmental monitoring at the NEF site. Future Semiannual Radioactive Effluent Release

Report will include a detailed analysis of any observed trends in radioactive uranic effluent activity.

Liquid Release Locations

Domestic waste (sewerage) generated at the CAB is discharged off site, along with other domestic waste

generated at the National Enrichment Facility, to the Eunice Waste Water Treatment Plant. Domestic

waste water is sampled quarterly at lift station 1, which is a central collection area for all domestic waste

generated at the National Enrichment Facility (Appendix A, Plot Plan)

Liquid Release Data

Reporting period: July 1, 2009 - December 31, 2009

Release Location: Lift Station 1Total Flow: 13,000 gpd

Table 3 of Appendix B to 10 CFR Part 20, Releases to Sewers, Monthly Average Concentration

(PCi/ml):234U = 3E-6231U = 3E-6

238U = 3E-6

Table 4: Domestic Wastewater Effluent, Radionuclides

Radionuclide /Sample ID

SamplePeriod

TotalTime

ErrorResults Estimate MDA Lift Station 1

uCi/ml) (Total Flow gal/day)

Quantity % of TableReleased 2 of Appx

B to 10Ci CFR Part

20 Values(day) (uCi/mIl) (uCi/ml) (i

9Page 9 of 77


U-234 / DomesticWaste 3Q 09

7/01/2009-9/30/2009

92 9.31E-10 5.84E-10 4.33E-10 13,000 4.21E-03 0.031%

U-234 / Domestic 10/01/2009 - 92 1.71E-09 3.69E-10 6.17E-11 13,000 7.74E-03 0.057%Waste 4Q 09 12/31/2009

U-235 / Domestic 7/01/2009- 92 8.17E-11 2.OE-10 4.56-10 13,000 3.70E-04 0.003%Waste 3Q 09 9/30/2009

U-235 / Domestic 10/01/2009 - 92 7.98E-11 7..06E-11 7.61E-11 13,000 3.61E-04 0.003%Waste 4Q4 09 12/31/2009

U-238 / Domestic 7/01/2009 - 92 <4.79E- 3.26E-10 4.79E-10 13,000 Below LLD Below

Waste 3Q 09 9/30/2009 10 LLD

U-238 / Domestic 10/01/2009 - 92 8.19E-10 2.25E-10 3.08E-11 13,000 3.71E-03 0.027%Waste 4Q09 12/31/2009


Sampling program deviations and program adjustments

Sample collection and analysis was performed on a quarterly basis for the second half of 2009, in

compliance with the NEF Environmental Report. Domestic wastewater samples were collected in

compliance with GL Environmental, Inc. SOP F007: Domestic Wastewater Sampling

Significant Trends

This Semiannual Radioactive Effluent Release Report is the second submitted by LES for the NEF.

Domestic wastewater effluent analytical results and the quantity of activity released are consistent with

the previous report.

It should be noted that observed isotopic uranium activity in domestic wastewater effluent are within a

single order of magnitude of observed natural isotopic uranium activity in drinking water within the

vicinity of the NEF. LES is currently collecting and analyzing samples from drinking water used to supply

the NEF. These results will be used to develop a scientifically sound correlation between isotopic

uranium activity in drinking water and wastewater effluent.

Dose to Members of the Public

Results from continuous monitoring of particulates in gaseous effluents from the CTPM EFS indicate

gross alpha and gross beta radioactivity were less than the lower limit of detection for all filters

analyzed. Isotopic uranium activity in gaseous effluent was less than laboratory error estimates or LLD

values listed in Table 2 of Appendix B to 10 CFR Part 20, Effluent Concentrations, Air, Class D, for 234U,23SU, 238U. This demonstrates compliance with 10 CFR 20.1301 dose limits to individual members of the

public from gaseous effluents.

10Page 10 of 77


Domestic waste effluent activity ranged from 0.003% to 0.057% of the value listed in Table 3 of

Appendix B to 10 CFR Part 20, Releases to Sewers, Monthly Average Concentration. This demonstrates

compliance with 10 CFR 20.1301 dose limits to individual members of the public from releases to

sewers.

Supplemental Information

Description of Sampling Equipment

Stack particulate sampling is achieved via a standard holder with 47mmMillipore (FSLW) fiberglass filters

(part # 52123 or equivalent). Samples are taken using gloves and tweezers and kept in sterile 50mm Pall

Petri Dishes. This particulate sampling system is fed with air from within the CTPMF by an isokinetic vent

system and volumetrically measured using an air volume totalizer.

The samples are collected from the main sewer line at an access location where the effluent has

sufficient velocity to keep effluent solids in suspension. Grab samples of domestic wastewater were

collected by submerging a clean container in the wastewater stream until full, and transferring contents

into clean laboratory sample containers.

Description of sampling procedure

See Appendix C

Analytical procedure

Gross alpha and Gross Beta - LANL MLR-100 Modified

Isotopic Uranium - EML U-02 Modified

Calculation methods

A. Activity

Activity Calculation

Cs -CbActivity (pCi/unit)=

Eff*Y* V* D*A*Ts *2.22

Where:

Cs= total counts in peak region

P 11•Page 11of 77


Cb = total background in peak region

Eff = counting Efficiency

Y = yield

V sample volume/weight

D = radioactive ingrowth or decay factors, as necessary

A = abundance

T,= sample count time (in minutes)

2.22 = dpm to picoCurie conversion factor

B. Effluent Released

Effluent Released = Total Volume Effluent * Analyte activity

C. % of Table 2 or 3 of Appendix B to 10 CFR Part 20 Values

% MPC = (Analyte activity / MPC) x 100

Error estimates

1.96 cpms cpmb

CU= = Ts TbEff*V*D*A*2.22

Where:

CU = Counting uncertainty (sometimes referred to as "error")

1.96 = Conversion to two-sigma (95.5%) uncertainty

cpms = counts per minute sample

cpmb = counts per minute background

12Page 12 of 77


T, = count time, minutes, sample

Tb. = count time, minutes, background

Eff = Counting Efficiency

V = sample volume/weight

D = radioactive ingrowth or decay factors, as necessary

A = abundance

2.22 = dpm to picoCurie conversion factor

Minimum Detectable Activity (MDA) Calculation

3 +3.29 RbTsr1+L-

MDA=KTs

Where:

3.29 = statistical factor for Type I and Type II error probabilities

selected to be 0.05 each

3 = a constant applied when the blank count approaches zero

Rb = background count rate in cpm

K = Efficiency, in-growth/decay, aliquot, abundance, dpm to pCi

conversion factor

T, = sample count time

Tb = background count time

Quality of Results

Probe sampling conditions are maintained so as to simulate conditions within the duct. The air volume

totalizer is calibrated yearly per specification. The axis of the sampling probe head is parallel to the air

flow lines in the ductwork, to ensure laminar flow.

13

Page 13 of 77


The air sample filters consist of 47mmMillipore paper, rated for high recoverability. Pall 50mm Petri

Dishes used for filter sample storage and shipment are sterile and free of trace particulates or other

potential sources of contamination. Sample collection utilizes gloves and tweezers to avoid radiological

contamination of sampling media during the sampling event. Additionally, media storage records are

compiled for collected samples including sample location, total flow, date, time, sampler, and any

irregularities associated with the sampling event. Collected samples are shipped under standard chain of

custody procedures.

The laboratory used for analytics (Eberline Services) holds NELAP, DOECAP, USACE, and DOD

certifications. LES holds a quality purchase agreement with the lab, and has audited Eberline Services

per the NEF Quality Assurance Program Description (QAPD). GL Environmental is currently an approved

supplier for LES, and the GL Environmental Quality Assurance Program has been determined satisfactory

per NEF QAPD.

Calibration Procedures

See Appendix D

Unusual Releases

No unusual releases are reported from the National Enrichment Facility for the period beginning July 1,

2009 through December 31, 2009.

14Page 14 of 77


APPENDIX A - Plot Plan

15

Page 15 of 77


APPENDIX B - Lab Data Sheets

17

Page 17 of 77

Printed: 2/2512010 3:45 PM Page 1 of I

";Reporh To: Work Order Details

Eberline Analytical Debra Edwards SDG- 09-12127LES Purchase Order: LES-GSA-3080

Final Report of Analysis 275 Hwy 176 Analysis Category: ENVIRONMENTALEunice, NM 88231 Sample Matrix: AF

Lab Sample Client Sample Receipt Analysis Batch ReportID Tp DDt ae Dt D Analyte Method Result CU CSU MDA Rpr

ID Type ID Date-Date Date ID Units

09-12127-01 LCS KNOWN 12/29109 00:00 12/29/2009 1/6/2010 09-12127 GROSS ALPHA LANL MLR-100 Modified 3.14E-04 1.35E-05 uCi/ml

09-12127-01 LCS SPIKE 12/29/09 00:00 12/29/2009 1/6/2010 -09-12127 GROSS ALPHA LANL MLR-100 Modified 3.12E-04 7.86E-06 8.00E-06 5.70E-07 uCi/mI

09-12127-02 MBL BLANK 12/29/09 00:00 12/29/2009 1/6/2010 09-12127 GROSS ALPHA LANL MLR-100 Modified -2.40E-16 2.58E-16 2.58E-16 8.62E-16 uCi/mI

09-12127-03 DUP 1300-562-1MA1 090713 07/13/09 10:02 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -1.43E-16 3.57E-16 3.57E-16 1.07E-15 uCi/ml

09-12127-04 DO 1300-562-1MA1 090713 07/13/09 10:02 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -3.33E-16 3.78E-16 3.78E-16 1.18E-15 uCi/mI

09-12127-05 TRG 1300-562-1MA1 090720 07/20/09 09:35 12/17/2009 1/712010 09-12127 Gross Alpha LANL MLR-100 Modified -4.74E-16 3.83E-16 3.83E-16 1.23E-15 uCi/mI

09-12127-06 TRG 1300-562-1MA1 090727 07/27109 09:17 12/17/2009 117/2010 09-12127' Gross Alpha LANL MLR-100 Modified 2.10E-16 2.63E-16 2.63E-16 6.65E-16 uCi/mi

09-12127-07 TRG 1300-562-1MAl 090803 08/03109 09:48 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -2.60E-17 1.97E-16 1.97E-16 6.18E-16 uCi/ml

09-12127-08 TRG 130G-562-1MAl 090810 08/10/09 09:50 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -8.99E-17 4.28E-16 4.28E-16 1.26E-15 uCi/ml

09-12127-09 TRG 130G-562-1MA1 090817 08/17/09 09:55 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -2.60E-16 2.50E-16 2.50E-16 8.49E-16 uCi/ml

09-12127-10 TRG 1300-562-1MAl 090824. 08/24/09 09:25 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -5.84E-16 2.70E-16 2.70E-16 1.02E-15 uCi/ml

09-12127-11 TRG 1300-562-1MAl 090902 09/02/09 10:06 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -6.00E-17 3.22E-16 3.22E-16 9.73E-16 uCi/ml

09-12127-12 TRG 1300-562-1MAI 090909 09/09/09 09:19 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -7.58E-17 4.35E-16 4.35E-16 1.25E-15 uCi/mI

09-12127-13 TRG 1300-562-1MAI 090916 09/16/09 09:55 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -4.78E-16 2.48E-16 2.48E-16 9.33E-16 uCi/ml


'09-12127-15 - TRG 1300-562-1MA1 090930 09/30/09 14:29 12/17/2009 1/7/2010 09-12127 Gross'Alpha" LANL MLR-100 Modified -3.43E-16 2.24E-16 2.24E-16 8.21E-16 uCi/mr

09-12127-16 TRG 1300-562-1MA1 091007 10/07/09 16:13 12/17/2009 1/7/2010 09-12127 Gross Alpha LANL MLR-100 Modified -5.81E-16 3.02E-16 3.02E-16 1.04E-15 uCi/ml

09-12127-01 LCS KNOWN 12/29/09 00:00 12/17/2009 1/6/2010 09-12127 Gross Beta LANL MLR-100 Modified 2.39E-04 7.16E-06 uCi/mI

09-12127-01 LCS SPIKE 12/29/09 00:00 12/17/2009 1/6/2010 09-12127 Gross Beta LANL MLR-100 Modified 2.89E-04 6.24E-06 6.28E-06 8.83E-07 uCi/ml

09-12127-02 MBL BLANK 12/29/09 00:00 12/17/2009 1/61/2010 09-12127 Gross Beta LANL MLR-100 Modified -1.95E-16 6.10E-16 6.10E-16 1.68E-15 uCi/mi

09-12127-03 DUP 1300-562-1MA1 090713 07/13/09 10:02 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -2.08E-16 6.06E-16 6.06E-16 1.67E-15 uCi/mI09-12127-04 DO 1300-562-1MA1 090713 07113/09 10:02 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified 1.39E-15 - 6.84E-16 6.84E-16 1.716-15 uCi/ml

09-12127-05 TRG 1300-562-1MA1 090720 07/20/09 09:35 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -8.44E-17 7.11E-16 7.11E-16 1.94E-15 uCi/mI

09-12127-06 TRG 1300-562-1MA1 090727 07/27/09 09:17 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified 3.80E-16 6.59E-16 6.590-16 1.75E-15 uCi/ml09-12127-07 TRG 1300-562-1MA1 090803 08/03/09 09:48 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified 7.60E-16 7.74E-16 7.74E-16 2.02E-15 uCi/ml

09-12127-08 TRG 1300-562-1MA1 090810 08/10/09 09:50 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified 5.09E-16 8.74E-16 8.74E-16 2.32E-15 uCi/mI

09-12127-09 TRG 1300-562-1MA1 090817 08/17/09 09:55 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -1.78E-16 6.49E-16 6.49E-16 1.78E-15 uCi/ml

09-12127-10 TRG 1300-562-1MA1 090824 08/24/09 09:25 12/17/2009 117/2010 09-12127 Gross Beta LANL MLR-100 Modified 1.02E-16 6.91E-16 6.91E-16 1.87E-15 uCi/mI

09-12127-11 TRG 1300-562-1MA1 090902 09/02/09 10:06 12/17/2009 117/2010 09-12127 Gross Beta LANL MLR-100 Modified -7.76E-16 8.49E-16 8.49E-16 2.39E-15 uCi/mI

09-12127-12 TRG 1300-562-1MA1 090909 09/09/09 09:19 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -4.52E-16 8.02E-16 8.02E-16 2.22E-15 uCi/ml

09-12127-13 TRG 1300-562-1MA1 090916 09/16/09 09:55 12/17/2009 1/7/2010 09-12127 , Gross Beta LANL MLR-100 Modified 7.64E-16 6.82E-16 6.82E-16 1.77E-15 uCi/ml09-12127-14 TRG 1300-562-1MA1 090923 09/23/09 10:00 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -7.89E-16 6.90E-16 6.90E-16 1.95E-15 uCi/mI

09-12127-15 TRG 1300-562-1MAl 090930 09/30/09 14:29 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified -1.60E-16 6.44E-16 6.44E-16 1.77E-15 uCi/m2

09-12127-16 TRG 1300-562-1MA1 091007 10/07/09 16:13 12/17/2009 1/7/2010 09-12127 Gross Beta LANL MLR-100 Modified 9.66E-17 5.72E-16 5.72E-16 1.54E-15 uCi/ml

CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original

Page 18 of 77

Printed: 212512010 3:45 PM Page I of I

Report To:,' Wbik Order Details:ý

Eberline Analytical Debra Edwards SDG: 09-12128LES Purchase Order: LES-GSA-3080

Final Report of Analysis 275 Hwy 176 Analysis Category: ENVIRONMENTALEunice, NM 88231 Sample Matrix: AF

Lab Sample Client Sample Receipt Analysis Batch ReportID Type ID Date Date Date ID A M U Units

09-12128-01 LCS KNOWN -. 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Alpha LANL MLR-100 Modified 3.15E-04 1.36E-05 uCi/mI

09-12128-01 LCS SPIKE 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Alpha LANL MLR-100 Modified 3.01E-04 7.64E-06 7.77E-06 6.28E-07 uCi/mi

09-12128-02 MBL BLANK 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Alpha LANL MLR-100 Modified 1.76E-16 3.66E-16 3.66E-16 9.83E-16 uCi/ml

09-12128-03 DUP 1300-562-1MA1 091014 10/14/09 09:41 12/29/2009 1/6/2010 09-12128 Gross Alpha LANL MLR-100 Modified -7.53E-16 3.63E-16 3.63E-16 1.29E-15 uCi/ml

09-12128-04 DO 1300-562-1MA1 091014 10/14/09 09:41 12/29/2009 1/7/2010 09-12128 Gross Alpha LANL MLR-100 Modified 2.50E-17 2.02E-16 2.02E-16 5.95E-16 uCi/ml


09-12128-06 TRG 1300-562-1MAl 091028 10/26/09 10:03 12/29/2009 1/7/2010 09-12128 Gross Alpha LANL MLR-100 Modified -2.11E-16 2.56E-16 2.56E-16 8.43E-16 uCi/ml

09-12128-07 TRG 1300-562-1MAl 091104 11/04/0909:44 12/29/2009 1/7/2010 09-12128 Gross Alpha LANL MLR-100 Modified 2.69E-16 2.84E-16 2.84E-16 6.97E-16 uCi/ml

09-12128-08 TRG 1300-562-1MA1 091112 11/12/09 16:14 12/29/2009 1/7/2010 09-12128 Gross Alpha LANL MLR-100 Modified 2.35E-17 2.64E-16 2.64E-16 7.61E-16 uCi/ml

09-12128-09 TRG 1300-562-1MA1 091119 11/19/09 09:10 12/29/2009 1/7/2010 09-12128 Gross Alpha LANL MLR-100 Modified -1.23E-16 2.1OE-16 2.10E-16 7.OOE-16 uCi/ml



09-12128-01 LCS KNOWN 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Beta LANL MLR-100 Modified 2.40E-04 7.20E-06 uCi/mI

09-12128-01 LCS SPIKE 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Beta LANL MLR-100 Modified 2.68E-04 6.02E-06 6.05E-06 8.85E-07 uCi/ml

09-12128-02 MBL BLANK 12/29/09 00:00 12/29/2009 1/6/2010 09-12128 Gross Beta LANL MLR-100 Modified -2.55E-16 7.48E-16 7.48E-16 2.06E-15 uCi/ml

09-12128-03 DUP 1300-562-IMAl 091014 10/14/09 09:41 12/29/2009 1/6/2010 09-12128 Gross Beta LANL MLR-100 Modified -6.84E-16 7.81E-16 7.81E-16 2.19E-15 uCi/mI

09-12128-04 DO 1300-562-1MA1 091014 10/14/09 09:41 12/29/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified -6.24E-16 6.75E-16 6.75E-16 1.91E-15 uCi/ml

09-12128-05 TRG 1300-562-1MA1 091021 10/21/09 09:48 12/29/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified -1.57E-16 6.88E-16 6.88E-16 " 1.89E-15 uCi/mi

09-12128-06 TRG 1300-562-1MAl 091028 10128/09 10:03 12/29/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified -2.63E-16 6.59E-16 6.59E-16 1.82E-15 uCi/ml

09-12128-07 TRG 1300-562-1MA1 091104 11/04/09 09:44 12/29/2009 1/7/2010 09-12128 Gross Beta - LANL MLR-100 Modified 2.38E-16 6.99E-16 6.99E-16 1.87E-15 uCi/ml

09-12128-08 TRG 1300-562-IMAl 091112 11/12/09 16:14 12/29/2009 - 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified 2.76E-17 6.55E-16 6.55E-16 1.78E-15 uCi/mI

09-12128-09 TRG 1300-562-1MAI 091119 11119/09 09:10 12129/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified -2.93E-17 6.53E-16 6.53E-16 1.78E-15 uCi/ml

09-12128-10 TRG 1300-562-1MAl 091125 11125/09 10:15 12/29/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified 3.40E-16 8.31E-16 8.31E-16 2.22E-15 uCi/ml

09-12128-11 TRG 1300-562-1MA1 091202 12/02/09 10:13 12/29/2009 1/7/2010 09-12128 Gross Beta LANL MLR-100 Modified -7.53E-17 7.53E-16 7.53E-16 2.05E_-15 uCi/ml

CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL-Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original

Page 19 of 77

Eberline AnalyticalOak Ridge Laboratory Generic Data Report Printed: 2/25/2010 3:43 PM

Page 1 of 6

-4 080InternallD InternalWorkOrder Fraction AnalysisCode Isotope Run ClientName SampleType ClientiD

10-02080-01 10-02080 01 UUISO U-234 1 Louisiana Energy Services, LLC LCS LCS

10-02080-02 10-02080 02 UUISO U-234 1 Louisiana Energy Services, LLC MBL BLANK

10-02080-03 10-02080 03 UUISO U-234 1 Louisiana Energy Services, LLC DUP 1300-562-1MA1 3RD QTR

10-02080-04 10-02080 04 UUISO U-234 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 3RD QTR



10-02080-03 10-02080 03 UUISO U-235 1 Louisiana Energy Services, LLC DUP 1300-562-1MA1 3RD QTR

10-02080-04 10-02080 04 UUISO U-235 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 3RD QTR

10-02080-01 10-02080 01 UUISO U-238 1 Louisiana Energy Services, LLC LCS LCS10-02080-02 10-02680 02 UUISO U-238 1 Louisiana Energy Services, LLC MBL BLANK

10-02080-03 10-02080, 03 UUISO U-238 1 Louisiana Energy Services, LLC DUP 1300-562-1MA1 3RD QTR10-02080-04 10-02080 04 UUISO U-238 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 3RD QTR

Page 20 of 77

Eberline AnalyticalOak Ridge Laboratory Generic Data Report

.4 1 &1r % a^

Printed: 2/25/2010 3:43 PMPage 2 of 6

ReportUnits Result Uncertainty MDA LSCKnown LCSPercentR LCSFIag RPDFIag MDAFLag BlankFlag SampleDate

uCi/ml 7.16E-06 1.21E-06 8.60E-08 8.16E-06 8.77E+01 OK INV 2/15/2010

uCi/mI 4.56E-17 7.66E-17 1.55E-16 OK INV 2/15/2010

uCi/ml 7.87E-17 7.97E-17 5.22E-17 OK OK 9/30/2009

uCi/ml 8.37E-17 6.97E-17 7.70E-17 OK 9/30/2009

uCi/mI 5.34E-07 2.03E-07 8.77E-08 INV 2/15/2010

uCi/ml 4.17E-17 6.52E-17 1.04E-16 OK INV 2/15/2010

uCi/ml 7.28E-17 8.49E-17 6.43E-17 INV OK 9/30/2009

uCi/ml 4.50E-17 5.58E-17 7.27E-17 OK 9/30/2009

uCi/mi 7.07E-06 1.20E-06 8.56E-08 7.96E-06 8.88E+01 OK INV 2/15/2010

uCi/ml 2.74E-17 5.33E-17 1.10E-16 OK INV 2/15/2010

uCi/mI 3.59E-17 5.61E-17 8.95E-17 INV OK 9/30/2009

uCi/ml 2.13E-17 3.70E-17 6.89E-17 OK 9/30/2009

Page 21 of 77


in n' non


AliquotNetEquiv RadioPercentRec GravPercentRec MeanPercentRec SF Sept0Date SeptIDate CountDate Halflifedays Detector Carrier

1 105.78 2/24/2010 0 A_Spec 28875800000 91.98 2/24/2010 0 A-Spec 29875800000 81.58 2/23/2010 0 A_Spec 4i875800000 118.11 2/23/2010 0 A-Spec 42

1 105.78 2/24/2010 0 ASpec 28

875800000 91.98 2/24/2010 0 A-Spec 29875800000 81.58 2/23/2010 0 A-Spec 41875800000 118.11 2/23/2010 0 A-Spec 42

1 105.78 2/24/2010 0 A-Spec 28875800000 91.98 2/24/2010 0 A-Spec 29875800000 81.58 2/23/2010 0 A _Spec 41875800000 118.11 2/23/2010 0 A Spec 42

Page 22 of 77

Eberline AnalyticalOak Ridge Laboratory Generic Data Report Printed: 2/2512010 3:43 PM

Page 4 of 6

20811CountTime Counts BkgCPM Eff UserName ModDate RPD Value Matrix-DateReceived GrossWetWt PercentLiq PercentSolid Date t_0

170.03 18.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010170.03 17.8 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010

170 18.9 AGRIGSBY 2/25/2010 6.144941814 AF 2/15/2010 2/23/2010

170 19.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010170.03 18.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010

170.03 17.8 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010170 18.9 AGRIGSBY 2/25/2010 47.17461395 AF 2/15/2010 2/23/2010170 19.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010

170.03 18.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010

170.03 17.8 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010170 18.9 AGRIGSBY 2/25/2010 50.85694299 AF 2/15/2010 2/23/2010170 19.9 AGRIGSBY 2/25/2010 AF 2/15/2010 2/23/2010

Page 23 of 77


Page 5 of 6

Ietfe 0-020j'ooUserName t 0 DilutionRatio SolutionNo PrepDate AliquotDate Identified CoordinateY XYUnits CoordinateZ ýZUnits GravFilterNet InstCode

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS I U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010O 2/16/2010 3

Page 24 of 77


Method TPUFactor CSU LCSKnownError

EML U-02 Modified 0.004212 1.21038E-06 2.93844E-07

EML U-02 Modified 0.004212 7.65802E-17

EML U-02 Modified 0.004212 7.96807E-17

EML U-02 Modified 0.004212 6.97009E-17

EML U-02 Modified 0.004212 2.03412E-07

EML U-02 Modified 0.004212 6.52302E-17

EML U-02 Modified 0.004212 8.48706E-17

EML U-02 Modified 0.004212 5.57503E-17

EML U-02 Modified 0.004212 1.19537E-06 2.86423E-07

EML U-02 Modified 0.004212 5.33101E-17

EML U-02 Modified 0.004212 5.61002E-17

EML U-02 Modified 0.004212 3.69701E-17


Page 25 of 77


Page 1 of 6

V - 081InternallD InternalWorkOrder Fraction AnalysisCode Isotope Run ClientName SampleType ClientiD10-02081-01 10-02081 01 UUISO U-234 1 Louisiana Energy Services, LLC LCS LCS


10-02081-03 10-02081 03 UUISO U-234 1 Louisiana Energy Services, LLC DUP 1300-562-1MA1 4TH QTR

10-02081-04 10-02081 04 UUISO U-234 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 4TH QTR



10-02081-03 10-02081 03 UUISO U-235 1 Louisiana Energy Services, LLC DUP 1300-562-1MAI 4TH QTR

10-02081-04 10-02081 04 UUISO U-235 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 4TH QTR

10-02081-01 10-02081 01 UUISO U-238 1 Louisiana Energy Services, LLC LCS LCS10-02081-02 10-02081 02 UUISO U-238 1 Louisiana Energy Services, LLC MBL BLANK •

10-02081-03 10-02081 03 UUISO U-238 1 Louisiana Energy Services, LLC DUP 1300-562-1MA1 4TH QTR10-02081-04 10-02081 04 UUISO U-238 1 Louisiana Energy Services, LLC DO 1300-562-1MA1 4TH QTR

Page 26 of 77


4Al r #%Ao04


ReportUnits Result Uncertainty. MDA LSCKnown LCSPercentR LCSFIag RPDFIag MDAFLag BlankFlag SampleDate

uCi/ml 7.45E-06 1.23E-06 5.75E-08 8.16E-06 9.14E+01 OK INV

uCi/ml 4.96E-17 5.79E-17 8.48E-17 OK INVuCi/ml 5.83E-17 5.89E-17 3.86E-17 OK OK

uCi/ml 5.19E-17 6.39E-17 1.01E-16 OK

uCi/ml 4.82E-07 1.86E-07 4.12E-08 INV

uCi/ml 1.05E-16 8.71E-17 4.64E-17 OK INV

uCi/ml 0.00E+00 3.72E-18 4.76E-17 OK OK

uCi/ml 0.OOE+00 3.98E-18 5.11E-17 OK

uCi/ml 7.81 E-06 1.28E-06 7.49E-08 7.95E-06 9.82E+01 OK INV

uCi/ml 1.63E-17 4.15E-17 9.81E-17 OK INV

uCi/ml 2.90E-17 4.13E-17 3.85E-17 INV OK

uCi/ml 1.03E-17 3.21E-17 8.35E-17 _OK

Page 27 of 77


A N 0% lu -


AliquotNetEquiv RadioPercentRec GravPercentRec MeanPercentRec SAF" ept0Date SeptlDate CountDate Halflifedays Detector Carrier

1 104.1 2/23/2010 0 ASpec 34

850800000 111.19 2/23/2010 0 ASpec 35

850800000 107.54 2/23/2010 0 A-Spec- 37

850800000 112.41 2/23/2010 0 A-Spec 38

1 104.1 2/23/2010 0 A-Spec 34

850800000 111.19 2/23/2010 0 A Spec 35

850800000 107.54 2/23/2010 0 A_Spec 37

850800000 112.41 2/23/2010 0 A-Spec 38

1 104.1 2/23/2010 0 A-Spec 34

850800000 111.19 2/23/2010 0 A_Spec 35

850800000 107.54 2/23/2010 0 A-Spec 37

850800000 112.41 2/23/2010 0 A Spec 38

Page 28 of 77


Page 4 of 6

10-C_.,CountTime Counts BkgCPM Eff UserName ModDate RPD Value Matrix DateReceived GrossWetWt PercentLiq PercentSolid Date t_0

170 20.3 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.9 AGRIGSBY 2/24/2010 11.54055525 AF 2/15/2010 2/23/2010

170 17.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 20.3 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.9 AGRIGSBY 2/24/2010 0 AF 2/15/2010 2/23/2010

170 17.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 20.3 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

170 19.9 AGRIGSBY 2/24/2010 95.36895674 AF 2/15/2010 2/23/2010

170 17.8 AGRIGSBY 2/24/2010 AF 2/15/2010 2/23/2010

Page 29 of 77


Page 5 of 6

UserName t 0 DilutionRatio SolutionNo PrepDate AliquotDate Iden7tied CoordinateY XYUnits CoordinateZ ZUnits GravFilterNet InstCodeJDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3

JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 3JDEMELAS 1 U-10a 2/16/2010 2/16/2010 I 3

JDEMELAS 1U-10a 2/16/2010 2/16/2010,. 3

Page 30 of 77


1 -208l4-Method TPUFactor CSU" LCSKnownError

EML U-02 Modified 0.004212 1.2324E-06 2.93616E-07

EML U-02 Modified 0.004212 5.78504E-17

EML U-02 Modified 0.004212 5.88905E-17

EML U-02 Modified 0.004212 6.39204E-17

EML U-02 Modified 0.004212 1.86311E-07

EML U-02 Modified 0.004212 8.71211E-17

EML U-02 Modified 0.004212 3.71902E-18

EML U-02 Modified 0.004212 3.97765E-18

EML U-02 Modified 0.004212 1.28342E-06 2.862E-07

EML U-02 Modified 0.004212 4.14801E-17,

EML U-02 Modified 0.004212 4.12502E-17

EML U-02 Modified 0.004212 3.207E-17_

Printed: 2/2512010 3:43 PMPage 6 of 6

Page 31 of 77


APPENDIX C - Sampling Procedures

.18Page 32 of 77

Procedure Title: Error! Reference source not found.

Attachment 5 Error! Reference source not

PIS Change Out found.Rev. Error! Reference

(Pages 1 to 2) source not found.Error! Reference source not

found.Page 1 of 4

1. PIS Change Out

1.1 Notify the Operations Center (Control Room) of potential for a low flow fault due to PISchange out.

1.2 Record the functional location of the monitor and date on CH-3-4000-01-F-2, PIS ChangeOut.

1.3 Close V2 (PIS Isolation) and record time on CH-3-4000-01-F-2.

1.4 Scroll to the Volume screen on the LPDU and record the total volume through the PIS onCH-3-4000-01-F-2 (as "volume since last PIS change out).

1.5 Reset the totalizer from the LPDU by performing the following:

1.5.1 Press both scroll keys simultaneously

1.5.2 Enter the pass code

1.5.3 Scroll to "OK" then press the "SELECT" key

1.5.4 Scroll to the command screen

1.5.5 Use the "SELECT" key to move the cursor over "CD"

1.5.6 Press "SELECT" key until "reset dose" is displayed

1.5.7 Using the scroll keys, scroll to "EXE" and press the "SELECT" key

1.6 As required, slightly unscrew the two sample line bracket screws above the PIS.

1.7 Don gloves.

1.8 Disconnect the PIS from the sample line by performing the following:

1.8.1 Disconnect the outlet quick disconnect.

1.8.2 Disconnect the inlet quick disconnect

1.9 Place the PIS in a bag for transport.

1.10 Connect pre-staged PIS to the sample line by performing the following:

1.10.1 Connect the inlet quick disconnect

1.10.2 Connect the outlet quick disconnect

1.11 Perform a smear survey on the connection points of the PIS and the immediate workarea to verify there was no spread of contamination.

1.11.1 IF contamination is present, THEN decontaminate per approved procedure andnotify Radiation Protection Manager of the results.

1.12 Doff gloves.

Page 33 of 77


Attachment 5 Error! Reference source not

PIS Change Out found.Rev. Error! Reference

(Pages 1 to 2) source not found.Error! Reference source not

found.Page 2 of 4

1.13

1.14

1.15

1.16

1.17

As required, tighten the two sample line bracket screws above the PIS.

Open V2 (PIS Isolation) and record time on CH-3-4000-01-F-2.

Verify that the sample low flow fault on the LPDU clears.

Notify the Operations that PIS change out is complete.

Ensure custody of the removed PIS and the completed CH-3-4000-01-F-2 is turned overto a qualified Chemistry/Environmental Compliance Technician.

Page 34 of 77


CH-3-4000-01-F-2 Error! Reference source not

PIS Change Out found.Rev.Error! Reference

(Pages Error! Reference source not found.Error! Bookmark source not found.not defined, to 4) Error! Reference source not

found.Page 3 of 4

1. Replacing the PIS Filter Paper

f-1

/2 - -

Recess for

47mm fifter

1.1

1.2

1.3

1.4

NOTE:

Refer to the pictures above while performing this attachment.

Don gloves.

Unscrew the top housing (1) of the standard holder containing the filter paper.

Visually inspect o-rings for cracks, wear, and that they are properly seated.

IF placing a filter paper in an empty PIS, THEN go to Step 1.6

Page 35 of 77


CH-3-4000-01-F-2 Error! Reference source notfound.PIS Change Out Rev.Error! Reference

(Pages Error! Reference source not found.Error! Bookmark source not found.not defined, to 4) Error! Reference source not

found.Page 4 of 4

1.5 IF replacing a used filter, THEN:

1.5.1 Using tweezers, gently remove the filter paper from the standard holder and placethe filter paper into the Petri dish or storage envelope pre-labeled with thefollowing information:

a. Alpha/Beta monitor functional location

b. Total flow through the PIS since last change out

c. Date

d. Time

e. Name and initials of person replacing filter paper

1.6 IF necessary, THEN lightly apply a small amount of vacuum grease to the inner lip of thetop housing (1).

1.7 Using tweezers, place a new filter paper onto the lip of the top housing (2) ensuring thefilter paper is arranged such that the Teflon side (smooth side) is facing the inlet side ofthe PIS.

1.8 Screw the middle housing onto the top housing so that the filter paper seats in therecessed area (3).

1.9 Verify the filter paper is properly seated by looking through the bottom of the middlehousing (4).

1.10

1.11

Verify the PIS is free of contamination and doff gloves.

Stow PIS in an approved storage location for subsequent PIS change outs.

Page 36 of 77

Project: National Enrichment FacilitymF007

Revision: 1GLEnvirOnmeintal, inc. Date: December 9, 2008

Standard Operating Procedure

Subject: Domestic wastewater sampling

1.0 Purpose

This procedure establishes a method to collect a sample of domestic wastewater.

2.0 Scope

This procedure is applicable to domestic waste stream generated by the NEF.

3.0 References

American Public Health Association. 1995. Standard Methods for the Examination of Water and

Wastewater, 19'h edition. Baltimore, Maryland.

4.0 Definitions

* Grab sample - a sample collected at a particular time and place. This sample is

representative of a longer time or larger volume if the source is relatively constant over an

extended time or over substantial distances in all directions.

5.0 Procedure

5.1 Equipment

" Analytical lab-provided container, properly labeled, attached to a rope, chain or pole

" Cooler with ice

" Personal protective equipment - i.e. nitrile gloves, protective eyewear, and tyvek suit

" If sampling is conducted in an enclosed space a half mask cartridge respirator must be used

" Handheld multi-parameter instrument

5.2 Sample collection

" The sample will be collected from the main sewer line at an access location where the

effluent has sufficient velocity to keep effluent solids in suspension.

" Sampler will don personal protective equipment.

Page 37 of 77

" Grab samples will be collected by submerging the lab sample container in the wastewater

stream until full. Retrieve the container, cap, and store on ice in cooler.

o Lab Analysis Samples - sample containers intended for shipment to an off-site

analytical laboratory will be sealed, labeled, and logged according to appropriate

chain-of-custody procedures.

o Field Samples - sample containers intended for field measurements will be taken

from the last volume removed from the sewer line.

" Measure field samples with the handheld multi-parameter instrument (temperature, pH,

and conductance) according to operating instructions and record results.

" Refer to NEF.Standard Operating Procedures for Decontamination of Sampling Equipment

6.0 Personal Protective Equipment

0 Refer to NEF SOP #1, Section 5.4 for use of Personal Protective Equipment.

Page 38 of 77


APPENDIX D - Calibration Procedures

19

Page 39 of 77

) Pro2ServeProfessional Project Services, Inc.

Start-up and Functional Test for the APBM 201-SAlpha Particulate Monitor

Page 40 of 77

of 27

Start-Up and Functional Test for the ABPM 201-S AlphaParticulate Monitor

Revision Summary

Change Reason for ChangeNew Procedure

Page 41 of 77

of 27


TABLE OF CONTENTS

1. PU R PO SE ............................................................................................................................. 4

2. S C O P E ..................................................................................................................... .............. 4

3. TERMS, DEFINITIONS, ABBREVIATIONS, AND ACRONYMS ....................................... 4

4. PRECAUTIONS AND LIMITATIONS ............................................................................... 5

5. EQUIPMENT, MATERIAL, AND PARTS ..................................... 5

6. ACCEPTANCE CRITERIA ................................................................................................ 6

7. PREREQ UISITES .................................................................................................................. 6

.8. DATA REQ UIRED ....................... n ....................................................................... 6.................6

9. M A IN B O DY ........................................................................................................................... 6

10. RESTORATIONIRECOVERY ........................................................................................... 12

11. DOCUMENTATION AND RECORDS .............................................................................. 13

12. LICENSE COMMITMENTS AND REQUIREMENTS ............................ 13

13. REFER ENC ES ..................................................................................................................... 13

12.SECTION 9.3.13 UPS VERIFICATION ....................................... 18

ATTACHMENTS

Attachment # 1, INSTALLER'S CHECKLIST ........................................................................ 14

ACCEPTANCE/SIGNATURE PAGE-TEST RESULTS SATISFACTORY ........................... 21

Page 42 of 77

of 27


1. PURPOSE

1.1 The purpose of this procedure is to confirm functionality for the start-up and acceptanceof the ABPM 201-S Alpha Particulate Monitor installed in the Special Filter Unit in theCAB. It will include verification of the following aspects of operation:

1.1.1 The proper startup and operation of the Alpha Particulate Monitor.

1.1.2 Verification of correct measurement of activity levels and functioning ofinstrument fault conditions and alarms.

2. SCOPE

2.1 This procedure governs the start-up and testing of the ABPM 201-S Alpha ParticulateMonitor and its supporting components

3. TERMS, DEFINITIONS, ABBREVIATIONS, AND ACRONYMS

LES The party placing the contract and the Buyer.

Supplier The party accepting the contract and the Seller

NEF National Enrichment Facility

CAB Centrifuge Assembly Building

FAT Factory Acceptance Test--

FAT Procedure Factory AcceptanceTest Procedure for ABPM201 SAlpha Beta Particulate Monitor

UF6 Uranium Hexafluoride

SAT Site Acceptance Test

HAT Hot Acceptance Test

PIS Particulate Iodine Sampler-For collecting samplesfor laboratory analysis-will not have an iodinecartridge

PDCU Power Distribution and Control Unit-Unit thatprovides power to the pump and the LPDU

LPDU Local Processing and Display Unit that providesdetector coupling, processing, filter advancemanagement, alphanumeric screen display, audibleand-light-signals,-keypad ,-testing ,-and-interfacemanaemen~ft. ____ _

Page 43 of 77

of 27


LDU

PFCV

MASS Software

SAMS Software

Local Display Unit--Unit that receives the analog signalfrom the stack flow element and relays theinformation to the Local Processing and Display Unitfor control of the proportional flow control valve andcalculations for release. Unit also displays readingsand alarms associated with the ABPM 201S.

Proportional Flow Control Valve - Valve thatregulates sample flow rate passing through themonitor to maintain proportionality with the stack flowrate.

Software for routine maintenance operations, set-upand periodic tests, SAMS software for spectrahandling and interpretation.Software for spectra handling and interpretation.

4.

4.1

4.2

5.

PRECAUTIONS AND LIMITATIONS

Read through this entire procedure to ensure understanding prior to conducting this test.

Ensure that appropriate electrical safety practices are utilized during this test inaccordance with MA-3-1000-06, Electrical Safety.

EQUIPMENT, MATERIAL, AND PARTS

5.1 Basic Tools and Software

5.1.1 Laptop or workstation PC

5.1.2 MASS2 software

5.1.3 SAS/PIPS Application Software

5.1.4 RS232 serial link cable with DB9 connectors

5.1.5 Vacuum/pressure hand pump

5.2 Calibrated Instruments

5.2.1 Digital multi-meter

5.2.2 Electronic thermometer or temperature sensor for the DMM (0.1 0 C resolution)

5.2.3 Pressure/vacuum gauge (0.2 psig resolution, 20 psig max full scale)

5.2.4 Mass flow meter

5-.2:5 "Do-Js•-e ratemet-r (0. i-R/hesolution) . . . . .

5.3 Radioactive Sources

5.3.1 24 1Am,1500 alpha/s nominal activity

Page 44 of 77

of 27


5.3.2 Source holder, MGP reference number 69553

6. ACCEPTANCE CRITERIA

6.1 Conformance of the inspection and measured values listed in the Checklist,Attachment 1, with requirements shown.

6.2 Proper operation of the alarms and faults.

6.3 Proper operation of the monitor.

7. PREREQUISITES

7.1 Notify Commissioning Manager of intent to perform test.

8. DATA REQUIRED

8.1 Data contained in the checklist, Attachment 1.

8.2 Calibration data.

9. MAIN BODY

NOTE: Record all observations and data on Attachment 1. Attachment 1 contains a SourceCalibration Data- Sheet and the process of calibration of the monitor.

NOTE: Steps may be performed in a sequence different from that shown in the test plan below,unless otherwise specified in the test plan.

9.1 Physical Inspection

9.1.1 Verify Alpha Monitor Identification and Condition

0 Serial numbers of components match serial numbers on data sheet whichcame from FAT.

* No visible damage.

* Adequate clearances have been provided for servicing.

* Name plate affixed to Instrument showing model number, serial number, dateof manufacture, UL listing.

* Calibration data sheet available for flow meter.

* Monitor skid is level and properly anchored to the building.

* All packing material and debris have been removed from the equipment,inside and exterior of all components are clean and dust-free.

9.-1..2 hCheck-that.-pipe-co n nectior•-fio'r•_fh'•.s-a ling'_oioe.iitieih'epecial[Fiter-U nitstack are compliant with the following:

* Sample inlet line 1 inch OD seamless stainless steel.

Page 45 of 77

of 27


* Sample outlet line 2 inch OD seamless stainless steel.

" No internal diameter change along line after union to nozzle.

* Minimal horizontal runs, no upward flowing sections between sampling nozzleand instrument inlet.

" Horizontal distance between nozzle and instrument < 15 feet.

* Radius of bends at least 3 times pipe outside diameter.

" Pipe connections made with Swagelok fittings.

" Verify sample inlet/sample return manual isolation valves are operable.

" Ensure components of system (line between nozzle and monitor, andmonitor) have been leak checked. To leak check the monitori open allinternal valves, close inlet and exit valves, and connect a pressure gauge andmanual hand pump to the inlet manifold. Draw a vacuum of approximately6 inches mercury in the system and hold for 10 minutes. The vacuum shallnot decrease by more than 10%.

9.2 Verify Electrical Connections

a Power supply and instrument voltages are compatible.

* LDU is in communication with LPDU (RS485 link between the LDU and theLPDU).

* The LDU has the following connections:

1. 120 V AC, 60 Hz instrument quality power line.

2. Analog input from the stack flow transmitter.

0 Using a DMM or milli-ohmmeter, check the resistance between the buildingground and the skid ground bus (welded threaded stud at lower left side ofthe skid). Resistance shall be less than 0.1 ohm.

9.3 Start-Up

9.3.1 Filter paper and cartridge

a. Check that a filter paper roll has been placed in the filter cassette.

b. Check that a filter paper is installed in the PIS.

9.3.2 Monitor Power On

a. In the Power Distribution and Control Unit (PDCU), check that fuses areinstalled in the fuse holders, and close the fuse holders.

b. Check that the filter cassette elevator is closed(up).7ZL.-Ve-rif~y_-th-e-[-PDUIp ower- Sup-plýi,,uit..breaker. on-the-distribution-unitis

Page 46 of 77

of 27


d. Power on the LPDU by turning the front panel key switch to "ON". Thebuzzer should sound for approximately one second, the orange lightilluminate for one second, and the red light briefly flash.

9.3.3 LPDU or LDU Software Check

a. Connect a PC to the LPDU (RS232 port on front of unit), scan withMASS2 on the PC, and verify that the LPDU is found.

b. Verify that the LPDU base software (Ref.735 index 1) is revision E orlater, Verify that the LPDU/SAS/PIPS application (Ref.774 index 2) isrevision P or later. Record the index and revision levels of the base andapplication software, and the parameter set.

c. Update LPDU time and date, if necessary.

d. Verify the LPDU serial number.

e. Backup any changes required, clear histories and events, and reset theunit.

f. Test the communication by reading the event summary of the unit usingMASS2.

9.3.4 LDU Software Check

a. Verify that the LDU is receiving information for LPDU.

9.3.5 Flow Rate Verification for Monitor

a. Place a calibrated flowmeter on the inlet or outlet manifold.

b. Bypass the isokinetic PFCV (Proportional Flow Control Valve).

c. Place the pump manual switch to "MAN" (operate the pump in manualmode).

Page 47 of 77

of 27


d. Provide sample flow to the monitor and adjust the manual regulating valveto obtain the flow rates listed below and verify the value indicated for theflow channel against the reading from the calibrated flowmeter.

Measurement Reference flow rate

Test # in I/min (CFM)

1 30(1.1)

2 -45 (1.6)

3 460(2.1)

ChcKeJ af o 14e r C,

e. The measurements shall match the gauge reading within +/-10 %.

9.3.6 Isokinetic Flow Control Test

The purpose of this test is to verify that the sample flow rate is maintained at avalue which is proportional to the process flow rate, above a certain sample flowthreshold. The stack flow scaling and the target sample flow rate may be modifiedand calibrated during this test.

a. With the PC connected to the LPDU and/or LDU, scan with MASS2.

b. Ensure the monitor components (LPDU and LDU) are configured toaccept stack flow data.

c. Adjust the Special Filter Unit Fan Speed by use of either the local FanSpeed Controller or the Building Automation System, as needed toachieve the Target Stack Flow Values (+/- 200 SCFM) used in this test.See Isokinetic Flow Control Test Table at end of Attachment 1, Installer'sChecklist

d. Record the stack flow as indicated on 1300-671-2MQ2, CTF Exhaust AirFlow Measuring Station.

e. Record the stack flow rate indicated on the LPDU display or by MASS2.

f. Record the sample flow rate to the Alpha monitor, as indicated by the totalflow rate channel (SkidFlow).

g. Verify sample flow rate is within acceptable tolerance for the stack flowrate (+/- 25 percent of the expected value).

h. If the scaling data must be updated, only the stack flow rate (StkFlow) andtarget sample flow rate (Target) channels need to be modified. See

17 - d--_1 -ii-he-g --§M hil-dr-B- -0 -- ,Aýi--i-x 2I-.-lsokietcFlow-Control_ Updamaenrmatio th-eStkFl6W-aidTarg-et-s-iam-Ie-flbWrate channels, If required.

Page 48 of 77

of 27


i. If changes to the calibration are required, repeat steps d-h untilacceptable sample flow rates are obtained. Record final results.

9.3.7 Detector Fault Test

a. With the monitor in normal operating condition, turn off power to the LPDUand the sampling pump and disconnect the detector cable at the LPDUside.

b. Restore power to the LPDU and check that the events list is similar to thefollowing list:

Date Time Event06107/00 15:05:21 Stop unit06107/00 15:05:37 Start unit06/07100 15:05:44 Unit In normal operation mode ON06107100 15:05:48 Detector probe not present ON06/07100 15:05:54 Electrical test counting: 006/07100 15:05:54 Electrical test fault ON06107/00 15:05:57 Internal fault ON06/07100 15:05:57 Temperature fault ON

c. Turn off power to the LPDU and reconnect the detector cable.

d. Restore power to the pump and the LPDU and check that the events list issimilar to the following list:

Date Time Event06/07100 15:05:21 Stop unit06107100 15:05:37 Start unit06/07/00 15:05:44 Unit in normal operation mode ON06107)00 15:05:44 Filter advance ON06/07100 15:05:54 Filter advance OFF

9.3.8 Relay and Alarm Test

4Note: The system must be operating without any faults. The pump control switch shouldbe in "Auto".

a. Verify the monitor is operating normally with no faults.

b. Using MASS2, open the relay status screen of the LPDU and verify thatthe relay statuses match the following table:

Relay Status

Operate On

Test Off

High 1OffHigh-High Off

I ____________________ ____________________ .1

AJ1A4~ C~ 'L~A ~A~A(4&t~b(

of 27


c. Create each scenario described in the table below by setting the trip pointbelow the actual measurement value.

d. Verify the relay and buzzer status indicated in the table.

Test Scenario Monitor Status Relay Status Buzzer(Display or MASS) (Read from MASS2)

H-.... OP Test AL H H1 Alert alarm (modify Normal/AL alarm On Off On Off Off SlowLPDU threshold)2 High alarm (modify Normal/H alarm2___ LPDU threshold) On Off On On Off Medium

3 H-H alarm (modify Normal/H-H alarm On Off On On On FastLPDU threshold) _

4 Fault (turn off sample Slave fault Off Off Off Off Off Continuouspump) _

5 Test (Place LPDU in Normal/Bypass On On off Off Off OffBypass mode) Normal/Bypass On _On _fo Off _Off

e. If the relay, light, or buzzer configuration was modified to accommodatethe test, place the LPDU in maintenance mode and restore the correctsettings.

9.3.9 Verify High and High High alarm thresholds are set to approved levels.

High: 3.7E 12 uCi/cc

High High: 7.3E 12 uCi/cc

9.3.10 Temperature calibration verification

a. Using the MASS2 software, and a calibrated temperature sensor,measure the temperature near the PIPS detector, and record themeasured value as TMeasured in °C.

b. Read the "Temp" channel in °C on the MASS2 main screen, and recordas TLPDU

c. Calculate the offset (difference) between measured and read, TLPDU -

TMeasured.

d. If the offset is between -2 °C and +2 °C, the temperature measurement. .~-;.- -.... calibration-is-acceptable. .... . .. --- -. -- ---------- -

Page 50 of 77

of 27


9.3.11 Energy and Source Calibration

Perform the energy calibration before the source calibration, in the order given in the testplan. Perform a source calibration, as directed in Attachment 2, which includes steps toperform the Source Calibration. Record all source calibration data on Attachment 1,Installer Checklist under the Source calibration Section.

9.3.12 Restoration and final check

a. If applicable, restore any parameters modified for the test to the normaloperating values.

b. Put the LPDU into maintenance mode.

c. Back up parameters into flash memory, and onto a diskette or CD, ifrequired.

d., Reset the LPDU and run the pump for 24 hours.

e. Check that there are no unusual events in the event summaries and thatthere is no activity in the historical trends which cannot be accounted for.

f. Review the test procedure and verify that all tests have been completed.

g. Review the test log and verify that all required entries are complete.

h. Repeat any steps if required.

i. Sign the test log.

NOTE:

UPS verification may be performed at a later time with an addendum to the testprocedure.

9.3.13 Verify UPS function

a. With the instrument functioning under normal operating conditions, removenormal power to the UPS.

b. Verify that the instrument continues to function for 1 hour after normalpower is removed.

O. -- RESTORATIONIRECOVERY- -

10.1 See section 9.3.12. No additional action required to restore system to normal operation.

Page 51 of 77

of 27Start-Up and Functional Test for the ABPM 201-S Alpha

Particulate Monitor

11. DOCUMENTATION AND RECORDS

11.1 Retain this procedure, the Installer's Checklist, and a record of any calibration performed,with required initials, lAW commissioning procedure(s).

12. LICENSE COMMITMENTS AND REQUIREMENTS

12.1 SAR 4.1

12.2 SAR 4.7

12.3 SAR, Section 9.2.21

13. REFERENCES

13.1 MA-3-1000-06, Electrical Safety

13.2 User's Manual, ABPM 201-S Alpha Beta Particulate Monitor, 15-00068 Rev. 0, dated 10-10-2008, MGP Instruments

13.3 Post Production Test Procedure for ABPM201S Alpha Beta Particulate Monitor,Document 12-00098 Rev 1, dated 7-15-2008, MGP Instruments

13.4 Factory Acceptance Test Procedure for LES ABPM201 S, Document 12-00124, Rev. 0,dated 9-19-2008, MGP Instruments

13.5 Post Production Test Data Sheet, ABPM201S Alpha Beta Particulate Monitor, Document14-00098-080925, dated 10-1-2008, MGP Instruments

13.6 LES ABPM201S Factory Acceptance Test Log, dated 10-3-2008, MGP Instruments

13.7 MASS Software User's Manual

13.8 LPDU User's Manual

13.9 ANSI/HPS N13.1-1999 Sampling and .Monitoring Releases of Airborne RadioactiveSubstances From the Stacks and Ducts of Nuclear Facilities

13.10 WPA-08-002-S-SP-0001-0, Specification for the Alpha Particulate Monitor

Page 52 of 77

Procedure Title: Start-Up and Functional Test for the ABPM 201 -S Alpha Particulate Monitor

Attachment #1 Page 14 of 27

Installer's Checklist

(Pages 14 to 14)

Calibrated Equipment

Item Model No. Serial No. Cal Due Comments

Digital Multimeter &,-,4 lee CA -V-5 07•,01,, 9//1/o 7 -r CEI

Temperature Sensor -7-(uk, 1zHI 131 L. L35

Pressurelacuum Gaugeand hand vacuum pump • 1I//o' K; A<-

Mass Flow Meter A9)i476 C. At0(J91- V1,:

p l o.+ ,,j F R ".r/$1,,5/ 1 6"- Iq - / l ¢' " J

ABPM201S System and Component Numbers C•"/ ,'333c/7F

Item FAT Log Part FAT Log Installed Part Installed

No. Serial No. No. Serial No.

Assembly (skid) 02-00384 080925 0 - 003:? 0 y'; -

LPDUIPIPS 131838A 080502 I0j1y'• r *•O•O 2.

PIPS Detector 45445 GOO0 071481 t/o .A -Z, NO• I e b6/i---

Particulate Flow Meter 120114 JM1 081579 /ml//l Y I o•'I5 "7

PIS Flow Meter 120112 F 040683 0

Filter cassette 43775 P 081118 4377 091118_____Flow Control Valve 209129 24690 0p/c 14L '90

Physical Inspection

Item Inspected By Verified By

Yes No Initials Date/Time Initials Date/Time

Serial numbers match FAT Data Sheet,Ref 13.6-See above HO- ( cJ c - 3q-01

No visible damage . .. i.3 -09(g5• -

.Dt.

I---- i-Adequate-clearances , I .. |. I

Label affixed . I _ ci -iI Z . J "

Page 53 of 77

Procedure Title: Start-Up and Functional Test for the ABPM 201-S Alpha Particulate Monitor



(Pages 14 to 15)

Item Inspected By Verified By

Yes No Initials Date/Time Initials Date/Time

Calibration data sheet availablefor flowmeter~fe _e '0:Al

71/2

Monitor skid level, foundation bolts 1Re, i Vtightened 3ooq ___ ____

Packing material removed and /Ie 1/30/07interiorlexterior clean 0/,150

Inlet pipe I inch OD seamless stainless OLD,/ /

steel V-

Return pipe diameter %e Inch OD .1-- /1. iaseamless stainless steel1.0

No diameter change along inlet line 0, ' KU

after union with nozzle

Minimal horizontal runs, no upwardflowing sections between samplingnozzle and instrument inlet / A/,/ 9:,___Horizonal distance between nozzle and

monitor <15 ft

Radius of bends at least 3X OD cp.

Pipe connections made with Swagelokfittings VL11Manual isolation valves operable V C • /, 3 AAii "j?•k u±zDcrease in vacuum after 10 min. • . -, /- -

Decreese <10% .6 a. •..-_ _ '

Electrical Connections

I

b I-J 2-ob Ase~ 41 D t'- 5 C, 0 /- -C~e l Af 6 - ,- le CtAl

+ ~ ~ ~~~2 7,ve /C~~/ec1 WA+S p hc/ fA)d~~J~~voje, ,g -7c Y' la e 34e

tlle~-A ,O. - 4-re-i- /b,,4 ;o4"4ý-~r -1 1' 1-.,eL - e 1 A NO f4LA20oe1r1




(Pages 14 to 16)

Start Up/Functionality

Item Acceptable Inspected By Verified By

tn Yes No Initials Datel Initials Date/.Time Time

a. Filter paper roll In cassette u11: +j t f

b. Filter paper in PISSec. 9.3.2

a. Fuses checked /b. Elevator up 0- i) 1

c. LPDU breaker ON (OZ•

d. LPDU ON, display correct

Sec. 9.3.3

a. LPDU found 11

b. Base software number, Index, and revision

Application software number, index, andrevision:

Parameters set number, index, and revision:

c.. Time and date correct [I

d. LPDU serial number: X

e. Any changes backed up, unit reset

1 U LtiI1"O

Dq-i-

- F~* I I' -~-~--~-***-*-I' *-...----I If. Event summary correct:

___________________________ ___ IZt _____ _____ I* I _____

.Page 55 of 77




(Pages 14 to 17)

Item Acceptable Inspected By Verified By

Yes No Initials Date/ Initials Date/

Time TimeSec. 9.3.4"",• // i l

a. Verify LDU is receiving information - [ j/' • //, •/'(' _-_ ]_'___

Sec. 9.3.5 Monitor flow rate (Skidflow) -

Calibrated Monitor ReadingsFlowmeter Reading within +1- z,4v-/ s d•/3

n10% I

.- ~ArO •e

3L1 e- 4-e /9:302LL.5 e.5~ ___P_

Section 9.3.7 Detector fault thst--

a-b Correctr Ac45c // 'dZ-c-d Correct

ection 9.3.8 Relay and Alarm TestTest I //A•"-j~je,:O--~a Lk-ý- correct.lE-•_0(

Test 2 Correct

Test 3 correct Ole.Test 4 Correct

Test 5 Correct

Section 9.3.9 Alarm settings

High alarm setpoint: 9 ,7yi0 d',.i_-,i

Correct l ""--O[0 k-^ C "

High High alarm setpoint: •'L, 3 I•/ 13 u

Corrects

Section 9.3.10 Temperature CalibrationVerification I/Tm.asud Reference Temperature Sensor: Ca$, 'C--TLPDU:~4 CHReadings within 20 C

Section 9.3.11

- So-urce calibration completed and recorded "-- - 41;L- 1-30-0

0S7A4 (k . ~ .do c~A~&Lf ~~ottC


Attachment #1


(Pages 14 to 18)

Page 18 of 27

Item Acceptable

OlU LIUiIf W•,. I• Ir• IMIULP1dif

Parameters restored

LPDU in maintenance mode

Monitor post test satisfactory

All tests complete

Entries complete

Test log signed

Section 9.3.13 UPS Verification

Instrument functioned 1 hr after normal powerremoved.

* #Te ýý4--s b c~aH-rbttd k) k-" LkP5 4ýIsokinetic Flow Control Test , e-ef -.

e•o S4- f 93q1o(Section 9.3.6 p3VPerA rm, 2-I

Measured Stack Measured Alpha Tre tTarget Stack Flow CFM from Process Monitor Sample Target Alpha Monitor Tolerance

,__ _ _ _ _ low Meter •Flow Rate. ampe1, iNo Stack Flow j 7j,0. joj 301I/min(1.1 SCFM) -I

2000+/- 200 00(50% Nominal 30 I/min (1.1 SCFM)Stack Flow) (170 oI-,5 t- SCFM) '3000+1- 200 16 o/t7 ,-S ,•

(75% Nominal i?,02c1Stack Flow) . 45m(SMqy4000+1- 200 LZ

(100% Nominal (,4IbVl L-- 7E 1402•(o 60 1/min (2,1 SCFM) It e-.5Stack Flow) ____1______

Maximum Stack 41.-/ i'..Flow . ....

---------------- i--'-----------------a----------'----'~ a'- -'----i

~C4)4c4 "Q L' fev m*,es e-k, COFD f-e1AZj P34,t$

7/' 5/0 ý

Page 57 of 77


Attachment #1 Page 19 of 27Installer's Checklist

(Pages 14 to 19)

Source Calibration Data Sheet

Name of Person Performing Calibration 1AMonitor Functional Location j 1306-W-1MA1

Date/Time i/s 6 /0 C /3"00

Test ConditionsUnits Required Value Measured Value

Temperature 0C 15-35 OC-General Area Radiation mR/hr < 0.1

Energy Calibration 0,- CUV2- (•A, A44.)

Complete? es! No q j •-,Jr,-( I,O "j

Source Activity

I Source-Type I Serial No. A(Bq)Am Alpha F5-247 2980 (A)

Gain Verification/Detection Efficiency Check

Description Units Required Value As found As left

Alpha-Beta gain cps 0.7-1.3 , '

Gamma gain cps 0.7-1.3 0 AI7 • 0

0 Gamma Gain As Left = (Alpha-Beta Gain As Left) (Gamma Gain As Found)(Alpha- Beta Gain As Found)

Background Units Required Value Measured Value Comments

Alphacps cps < 0.005 0 o ,5- N /,APo2lx.cps cps <0.005 C) / 0 A 7 /A- W

Measurement with Alpha Units Required Value Measured Value Comments

SourceAlpha-cps cps K) ,

Po21x cps cps f• •'

cps/Bq 0.0326 to (3) r

Alpha Efficiency (Eff) 0.0398 , 0 1 '369 AJcps/g Ci 7(7 )

W ipna t-ricency kcpslbq) -- -tlpna_cps/,L8u tiuq,.....@ Alpha Efficiency (cps/g Ci).= G x 37000

Page 58 of 77


Attachment #1 Page 20 of 27Installer's Checklist

(Pages 14 to 20)

Remarks: tIoT " r .e / I- x e Ve v- ct,, - o -e 7l. 6 0 4 ) 4e S,

ý A 6 P A Af

LA-

OL-0 , , " J A

Page 59 of 77

I 82/086/2889 11:25 865--531-9424 FEDEX KINKO'S 8522 PAGE 02

PoEdure Title: Start-Up and Functional Test for the ABPM 201-8 Alpha Particulate Monitor

Attachment 1 Page 21 of 27

Installers Checklist

(Pages 14 to 21)

AcceptanceISIgnatur Page-Test Results Satisfactory

L

• • . Am

I - - - -

Signature

JQ4'4A-V

Dats

$Igneturt

Ca/t7 C~~ ~6

Page 60 of 77

I ,Procedure Title: Start-Up and Functional Test for the ABPM 201-S Alpha Particulate Monitor


Energy and Source Calibration

(Pages 22 to 23)

Source Calibration

Section 9.3.11

NOTE: Record all data for the source calibration on the Attachment 1, InstallersChecklist.

1.12 Test Conditions

1.12.1 Record ambient temperature near the detector, as indicated on the calibratedtemperature sensor.

1.13 Preliminary Steps

1:13.1 Verify the monitor has been running for is operational without an alarmingcondition and that it has been powered for > 30 minutes.

1.13.2 Verify general area radiation around the monitor is < 0.1 mR/hr.

1.13.3 Launch SAMS and Verify communication is established.

1.13.4 Place the LPDU into bypass mode:

a. Simultaneously press both scroll keys.

b. Enter the pass code.

c. Scroll to OK and press the "SELECT" key.

d. Press "SELECT" key until the command screen is displayed.

e. Scroll to CD.

f. Press "SELECT" key until BYP is displayed.

g. Scroll to EXE and press the "SELECT" key.

1.13.5 From the PDCU place the pump control switch to OFF.

1.14 Gain Verification

1.14.1 Pull the elevator handle to disengage it from its notch.

1.14.2 Lower the elevator.

1.14.3 Remove the filter cassette.

1.14.4 Disconnect the filter cassette power cable.

1.14.5 Place the 241Am source in the calibration source fixture such that the source seats............ . in the-small recess and the active area of-the-source is facing up out-of-the

clibratinouceitre1.14.6 Place the calibration source fixture with source on the elevator and verify that it

seats properly.

Page 62 of 77




(Pages 22 to 24)

1.14.7 Gently close the elevator.

1.14.8 Using SAMS, perform the following:

a. From the Spectrum menu, ensure real time is selected.

b. Enter 300 in true time text box.

c. Ensure Alpha Max is selected.

d. Press Start to perform the spectrum acquisition.

e. Check that a clear alpha peak is visible.

f. Place the markers around the peak and note the Alpha Max value.

g. IF the peak is at 419±20 (399 to 439), THEN perform the following:

1. From the Calibration menu, select electronic calibration.

2. Record the displayed alpha-beta gain as the "Alpha-Beta Gain AsFound" on the Source Calibration Data Sheet section that is locatedon the Installer Checklist.

3. Record the displayed gamma gain as the "Gamma Gain As Found"on the Source Calibration Data Sheet.

4. Record N/A for the "Alpha-Beta Gain As Left".

5. Record N/A for the "Gamma Gain As Left".

6., Proceed to step 1.14.9.

h. IF the peak is not at 419±20 (399 to 439), THEN adjust the alpha-beta gain:

1. From the Calibration menu, select electronic calibration.

2. Record the displayed alpha-beta gain as the "Alpha-Beta Gain AsFound" on Source Calibration Data Sheet.

3. Record the displayed gamma gain as the "Gamma Gain As Found".

4. Adjust the alpha-beta gain as appropriate.

5. Repeat Step 1.14.8h until the alpha peak location is correct.

6. Record the alpha-beta gain as "Alpha-Beta Gain As Left".

7. Calculate the "Gamma Gain As Left" as follows and record.

Gamma Gain As Left = (Alpha-Beta Gain As Left) (Gamma Gain As Found)

... (A lpha--Beta Gain As-Eound) ........ •. ... ..

8:p---Update-the gamma-gain- in-the Electronics•Calibration window.

9. Press "Write to LPU".

Page 63 of 77




(Pages 22 to 25)



1.14.11 Remove the calibration source from the calibration source fixture.

1.14.12 Place the empty fixture on the elevator and with two hands gently raise theelevator.

1.15 Detection Efficiency Check

1.15.1 Display the historical trend for the Alpha-cps and Po2lx_cps gross counting ratechannels using MASS2 as follows:

a. Right click on the "Alpha-cps" channel and select display historical trend.

b. Right click on the "Po2lx cps" channel and select display historical trend.

c. From each windows "historic" menu, ensure automatic refresh is selected.

NOTE:

Use at least five data points in the 10 minute historical trend for each channel todetermine the average.

1.15.2 Wait until the measurement is stable..

a. From the historic menu for Alpha cps AND Po2lx cps, in each windowselect "10 minute average" AND analyze the 10 minute historical trend foreach channel.

1.15.3'Record the average background count rate for Alpha cps AND Po2lx-cps.

1.15.4 Verify the background count rate is <0.005 cps for both Alpha cps ANDPo2lx-cps.

1.15.5 IF background count rate is >0.005 cps, THEN decontaminate the housing andrepeat Step 1.15, ELSE proceed to Step 1.16.

1.16 Measurement with the Alpha Source



1.16.3 Remove the empty calibration source fixture from the elevator.

_1 -16,4 Place-the-2ŽAm source in-the calibration-source-fixtu re such that-the-source seats-----:ca-inbth esmall srecess and-the -active- area-ofthe-source isfacing-upout-of-the----calibration source fixture.

Page 64 of 77




(Pages 22 to 26)

1.16.5 Place the calibration source fixture with source on the elevator and verify that itseats properly.

1.16.6 Gently close the elevator.

1.16.7 From SAMS verify the alpha peak is visible.

NOTE:

To determine the average for each channel, the first data point from each trend isdiscarded. At least five data points are used from each historical trend.

1.16.8 From MASS2 perform the following:

a. Right click on the "alpha cps"channel and select display historical trend.

b. From the "historic" menu, select "10 minute average".

c. Right click on the "Po2lx cps" channel and select "display historical trends".

d. From the historic menu, select "10 minute average"

e. Record the average count rate for the Alpha-cps channel on SourceCalibration Data Sheet.

f. Record the average count rate for the Po21x cps channel on SourceCalibration Data Sheet.

1.17 Detection Efficiency C'alculation for Source

NOTE:

Because the half life of 241Am is approximately 432 years, we will not decay correct thesource for determination of efficiency.

1.17.1 Calculate and record on Source Calibration Data Sheet the efficiency (Eff) in Bqfor the detector using the formula below:

Eff= S/A

a. Where S is the Alphacps source value determined in 1.16.8e

b. Where A is the activity of the 241Am source at 2980 Bq

1 .1 -ncpspCi-by-multiplyinrgdth--re-slt-ab6vebyD37,000. ..... .n.

1.17.3 Verify the efficiency of the detector is within ±10% of the Post Production Testvalue (0.0326 cps/Bq to 0.0398 cps/Bq) from the Factory Acceptance Test.

Page 65 of 77




(Pages 22 to 27)

1.18 Alpha Efficiency Adjustment

1.18.1 From MASS2 perform the following:

a. Right click on the appropriate LPDU box and select commands

b. Select "Go to Maintenance Mode"

c. Right click the "alphaDAC" channel and select algorithm parameters

d. Change the artificial alpha detection efficiency to the value calculated in1.17.2 AND press "Write"

e. Right click the "Cumalpha" channel AND select algorithm parameters

f. Change the artificial detection efficiency to the value calculated in 1.17.2AND press "Write"

g. Right click on the appropriate LPDU box AND select "commands"h. Select "Backup to flash"

1. 18.2 From the PDCU place the pump control switch to AUTO.

C10 1.18.3 From MASS2 perform the following:

a . Right click on the appropriate LPDU box and select commands

b. Select "reset equipment"

1.19 Final Steps

1.19.1 .Ensure normal valve line-up:

Valve Number Nomenclature Postion

V1 Detector Subassembly Isolation OPENV2 PIS Isolation OPENV3 Main Flow Rate Adjustment THROTTLED*V4 PFCV Inlet OPENV5 PFCV Outlet OPENV6 PFCV Bypass CLOSEDV7 Sample Pump Isolation OPENV8 Sample Pump Vacuum BreakV9 Grab Sample Bypass OPEN

V10 Grab Sample Inlet CLOSEDV11 Grab Sample Outlet CLOSED

Page 66 of 77

FAT# 1300-562-01Page 18 of 91

14-00098- 09O qI 9 14-00098 Rev1 Data SheetRevision INot." for electronic archival, save the completed dalasheet wIh the filename "14.00098 '##W# wheo m Is the seriat number of the monitor

Post Production Test Data Sheet

System: ABPM201S Alpha Beta Particulate MonitorPart Number including option codes: 0 7?- a'c3fSerial Number: QFO0Z 92 ,)(Note: append serial number to the document number of the data sheet)

TestDate(s): 10/1 /'ZOOR' 4 L LETestedBy: S) t"Witnessed by: t>-Ior-• W_,J ar-l S .lV t 64MGP References: So. * 'U 1;Client References: fo JA - o1 S4

Suite 1505000 Highlands Parkway-

Smyrna, GA 30082

Rev. Date Prepared By Reviewed By Origin and Description of the Changes

0 02/21/2008 Silas Stark Original Issue based on MGP SA document 1232101 07115/2008 Silas Stark Refer to ECN 641

All of the Information In this document Is the exclusive property of MGP Instruments, Inc. and is not to be disclosed, reproduced, or.used except as authorized In writing by MGP Instruments, Inc.

Page 68 of 77

FAT# 1300-562-01Page 17 of 91

SHOMGP

LSL- LES ABPM201S Factory Acceptance Test Log Page 9

Additional/supplemental test results

lp- As "covr-" . '- rIStS 04 • sr ,

b••r,

f-

All Information In this document Is the exclusive property of MGP Instruments, Inc. and Is not to be disclosed, reproduced, or used except asauthorized in writing by MGP Instruments, Inc, 1 Page 69 of 77

FAT# 1300-562-01Page 19 of 91

I14-

.Post Production Test Data Sheet:ABPM201S Alpha Beta Particulate Monitor

Page 2 of 6.V I

Tested by: ( , Date: to I I I o- INotes/Comments: "T e- ..0e,., JQLo .-iL, t'4%&JE- • •-

3.2 Calibrated Instruments'Item Model No. Serial No. Cal. Due Comments -

Digital Multimeter F'/C.e f7 9JS6as ,... 't ?_ ")Temperature Sensor (9, 3 Oe114-Q7 ,I? ' S.h'I lo IPressure/vacuum gauge , U--Z. 15:7.Pe -All tAt-TF_ *AU

Mass flow meter 0m.. fAM Zo.C97 - Z. ?LIr, 0111 its/-HI-Pot tester 47a(,-W 79P71Mega-ohmmeter 7&.-C .757_0__M_-_-_T_-C_ _5 Wi___

3.3. Radioactive Sources ...........Source Serial No. Activity (Ao) Date Comments

Alpha 16sotope . .,sOMher

§4 Test Conditions

Description Unit Req. Value Measured Value CommentsMGP Other

Temperature OF 60 - 90 77, , .' 0 -I"ZHumidity % <99 -___ _ _ _,,

Pressure - Ambient ,Am,. -- _ _.__-

Line power VAC 108-132 11-7,8 //,_ _ _ _

Frequency Hz 57-63 (,0.o1 6"o. a d

§5 Visual InspectionMeasured Value ReferenceDescription Req. Value MGP Other (Document & Revision)

Component layout, routing, Correct C a •. rr e ,% / 0 - 0- 247 N 0 0 0overall conditionFrame mounting hole o 9,7S$ -- F-4 19j7Sdimensions S1,.,I ,7S •--- .9 IS W, CZ reeu# /a _02'' -2 C,0Other Interface dimanslons (describe): Describe:

Labels, nameplates, Correct 'rlc;.* W At"' it.....

placards, etc. o c ____$-IAt% -%%-?fq#

Point-to-point wiring Correct 06 c___ a2, o' -O.z -• re.. I

Wire sizing, markers, Correct - CW,,' .e _ o,-oo3,.. t. Ifuses, etc. CorrectOther (descdbe): Describe:

gerialized equipment

Description Part No. Serial No. Condition CommentsLP(D•U/SAS/PIPS

. . ... . . -. - -- ___,--_ 1111M A _ I WSW . .......

__P IP _S 0Detd-dto-r- _ý .1 w-sat.-ounsat. 11Pi2SbD~t~6t6F

I u~Sat. oUnsat. I. 070Particulaterflow:meter : I -'sat.Unsat. -I-PIS flow meter I_____ oge61'X f Sat. oUnsat. __________

Check source F 1 4 '0^ o sat. oUnsat. f____________All of the Information In this document Is the exclusive property of MGP Instruments. Inc. and Is not to be disclosed, reproduced, or used except asauthorized In writing by MGP Instruments, Inc. Page 70 of 77-

FAT# 1300-562-01Page 20 of 91 Post Production Test Data Sheet:

ABPM201S Alpha Beta Particulate MonitorPage 3 of 5Dv. 1

Tested by: •. •,.•.tc_.Tested by: [c Date: |o/t/oP I

Notes/Comments: ,.,/ t- . .. r Su.i,•,.

Description Unit Req. Value Measured Value CommentsMGP Other

§6: Dielectric & Continuity6.1 Dielectric test mA <10 <0 (1 <o106.2 Isolation test Ma >100 >999. >"I_ _ _

6.3 Continuity test 0) <0.1 -o. f < &.._ _

§7: Relief valve test "Hg 20.5 - 24.5 V- ' "2.9' 95§8: Option verification

8.1 Grab sampler - Correct I N/A Cxbrf,"8.2 PIS - Correct / N/A "8.3 Check source - Correct / N/A_8.4 Sample pump - Correct / N/A -_,._._

Other _ A___,,§9: Leak Test Hg <0.6 ' o.Z.S <0o.2s_._"§10: Test configuration Correct C. .'__ '- _ _ _ _ _

Relay adjustment A (from motor) , _ _,

§11: Flow meter test*11.1 Particulate flow:

Measure 1 I/min 0 to 2 0 ioi..IiI Z IMeasure 2 VImin 17 to 23 T;o,_ I CC..,

Measure 3 I/min 27 to 33 _3_-4,% e-,_-, C",=o1 "-Measure 4 I/min 42 to 48' g,. I _._____

11.2 PIS Flow:Measure 1 I/min 0 to 2 0Measure 2 I/min 17 to 23 /_,__Measure 3 I/min 27 to 33 2k.,7Measure 4 I/mln 42 to 48 _qi "

§12: Detector fault test - Correct _,_

§13: Monitor test13.1 Automation test

13.1.1 Normal Operation - Correct co_,_,_"_13.1.2 Electrical Test - Correct Cerrc.- C. r e e,13.1.3 APmin Test - Correct LrrN.1 6 z 2',& z-N13.1 4 AfPmax Test - Correct C6 .- &,.k " /.13.1.5 Minimum flow test Correct C arr ie-,13.1.6 Flow fault test Correct Cr " -e "

13.2 Analog output test - Correct c.r.,.."- r. rrc.,-13.3 Relay & light test - Correct C,,.r"c C.,,J,•"13.4 Serial link test - Correct .,.ru I 3-,____._-_

*Note: fill in this section after the flowmeter has been calibrated, if necessary

All of the Information In this document Is the exclusive property of MGP Instruments, Inc. and Is not to be disclosed, reproduced, or used except asauthorized in writlngby MGP Instruments, Inc. Page 71 of 77

FAT# 1300-562-01Page 21 of 91

'I14-F

Post Production Test Data Sheet:ABPM201S Alpha Beta Particulate Monitor

Page 4 of 5m

I Rev. ITested by:. . , Date: I q I oP I

E

[Notes/Comments: iv •vJ. ,c , 4- 4, 0Jk,. •,•cM/4- -.k k4....Mw,.

Description Unit Req. Value Measured Value CommentsMGP Other§14: Calibration

14.1 Nuclear check,

Measured temperature °C - ".7,44 "2i/. 2.Indicated temperature °C Tra ± 2 2.3¶ "___. _.

Temperature offset °C _T- ,l I

Alpha-beta-gamma gain - 0.7-1.3 __ Po _Gamma gain - 0.7-1.3 0,97-Channel/keV slope !% - ,zedChannellkeV offset - - V€,?TZ"._

Channel/keV quadratic -

Background:AlphaCPS cps < 0.005 O0 al7 7Po218CPS cps - "_Po214CPS cpsPo212CPS cps

<0.5 With check sourceBetaCPS cps <0.2 -VIA,- Without check source

<0.5 With check sourceGammaCPS cps <0.2 /a Without check source

Alpha source counting __/.7) f____-2 Y___ IAlphaCPS cps - ,8 _____ /'.5 I -.'2.: Io7., IPo218CPS cps - -/A AX _ =_ d (16APo214CPS cps - L'in O4a-3Po212CPS cps - ________

BetaCPS cps -

GammaCPS cps -

Beta source counting Ak.AlphaCPS cpsPo218CPS cps -Po214CPS cps - A4-Po212CPS cps - "_BetaCPS cps -

GammaCPS cps -

Alpha efficiency cpsIa/s 0.0333 - 0.0407 ,0o367 o.cu.2. /o/Z r•'- 2 q .Beta Efficiency cps / ils 0.05-0.08 ,P/A - ids F-c-'3-7. b 0o3f.

14.2 Check source test _

AlphaCPS cps ,Po2I8CPS cps IPo214CPS cps. . IPo212CPS cps -

BetaCPS cps >3. _

GammaCPS c0S >0.5-r ....Z

415: FinarcnecK uorrecrI h 1.

All of the information In this document Is the exclusive property of MGP Instruments, Inc. and is not to be disclosed, reproduced, or used except asauthorized In writing by MGP Instruments, Inc. Page 72 of 77

FAT# 1300-562-01Page 22 of 91

14-00

Post Production Test Data Sheet:ABPM201S Alpha Beta Particulate Monitor

Pans 5 of 5V. ITested by: I S- 4 Date: to I/Iop I

[Notes/Comments: (0 13.LOP

Flow meter calibration data (if applicab _)

Flow Meter Measurement Indicated Flow Measured Flow Relative analog(before correction) (calibrated meter) input (%)

I Y1 = 0 X11 = I2 Y2= 7. ' X2= 1I1

Particulate 3 IA', Y3 = iS X3=(Flowmeter + 4 (Aot-,, uA- Y4 = X4 =DP switches) 5 Cl I k-t-> Y5 = - X5 = 67

6 ._.._Ye = .. X__ x6 = 79__ 7 . .. Y__7"_ =. (•o X7 = 100%

I ... .... _1_ Y1 0 _L2 Y2= " X2-= ft

PIS 3 _ _,Y3 = , X3 = -Vq

(if applicable) 4 r4)___,__-,- _-_f- Y4= zo X4 =S'.. 5 -• - 0416,w,-.) Y;5= VOe x5= -716 Y6 = Vo X6 = •1

_ 7 y7* = (P X7 = 100%*Note: the final measurement is the extrapolated flow rate at 100% relative analog Input

qp. ,(

Cz-

it, ZVI, Zi I

/;;L- j

All of the Information in this document Is the exclusive property of MGP Instruments, Inc. and Is not to be disclosed, reproduced, or used except asauthorized In writing by MGP Instruments, Inc, Page 73 of 77

FAT# 1300-562-01Page 29 of 91

jEckert& ZieglerIsotope Products

24937 Avenue TibbittsValencia, California 91355

Tel 661-309.1010Fax 661.257-8303

CERTIFICATE OF CALIBRATIONALPHA STANDARD SOURCE

Radionuclide:Half-life:Catalog No.:Source No.:

Am-241432.17 ± 0.66 yearsRFQ994-241-81NF5-247

Customer:P.O. No.:Reference Date:Contained Radioactivity:

MGP INSTRUMENTS00228651-Nov-08 12:00 PST80.54 nCi 2980 Bq

Physical Description:A. Capsule type:E. Nature of active deposit:

C. Active diameter/volume:D. Backing:E. Cover:

Disk (38 mm OD x 3.0 mm THK)Electrodeposited and diffusion bonded oxide15 mmStainless steelNone

CAUTION!DELICATE SURFACE

DO NOT WIPEACTIVE AREA

Radioimpurities:

None detected

Method of Calibration:

This source was assayed using a windowless internal gas flow proportional counter.

Uncertainty of Measurement:A. Type A (random) uncertainty:B. Type B (systematic) uncertainty:C. Uncertainty in aliquot weighing:D. Total uncertainty at the 99% confidence level:

± 0.5 %

± 3.0 %± 0.0 %+ 3.0 %

Notes:- See reverse side for leak test(s) performed on this source.- EZIP participates in a NIST measurement assurance program to establish and maintain implicit traceability

for a number of nuclides, based on the blind assay (and later NIST certification) of Standard ReferenceMaterials (as in NRC Regulatory Guide 4.15). %

- Nuclear data was taken from IAEA-TECDOC-619, 1991.- This source has a working life of 2 years.- The surface emission rate for the unmounted foil was 90310 cdmin in 27r on 22 Sep 08.- The surface emission rate for the foil mounted in an aluminum holder was 86030 cdmin in 2n on 22 Sep 08.

Oua itCqrkto0ý?_3-

Dfite SEZIP R~ef.,No.:._1.31_8-42_71

Medical Imaging Laboratory

24937 Avenue Tlbbitts Valencia, California 91355

ISO 9001 CERTIFIED

Industrial Gauging La bfteO, of 77

1800 North Keystone Street Burbank, California 91504

THE LEAK TEST(S) INDICATED BY THE CHECKED BOX(ES) WAS(WERE) APPLIED TO DETERMINE THE INTEGRITY OF ,t!0-F.SOURCE(S) DESCRIBED ON THE FRONT SIOE. THE LEAK TEST(S) INDICATED BELOW WERE EITHER TAKEN DIRECTLY_FROM ISO 9978:1992 OR DERIVED FROM THE LEAK TEST METHODS LISTED IN ISO 9978:1992 WHEN AN APPROPRIATETEST WAS NOT SPECIFICALLY LISTED.

.J Standard Wipe Test'The source was wiped over its entire surface with a moistened filter paper disk. After drying, the disk was checkedfor activity using a scintillation detector. There was <0.001 [tCi bela-gamma and <0.0001 pCi alpha of removableactivity.

=J Special Wipe TestThe source was wiped over its entire surface with moistened polystyrene. The polystyrene was then dissolved in aliquid scintillation cocktail and counted in a liquid scintillation counter. There was <0.001 pCi beta-gamma and<0.0001 pCi alpha of removable activity.

J Distilled Water Soak TestThe source was immersed in distilled water and maintained at 50QC ± 59C for a minimum of four hours or roomtemperature (20-°C t 59C) for 24 hours. After removal of the source, the liquid was a) checked for activity using aliquid scintillation counter, or b) evaporated in a planchet and the residue checked for activity using a windowlessproportional counter or end-window G.M. tube. There was <0.001 .Ci beta-gamma and <0.0001 pCi alpha ofremovable activity.

J Liquid Scintillation Soak TestThe source was immersed for a minimum of 3 hours at room temperature in a liquid scintillation cocktail, which doesnot attack the source's outer surface material. The source was stored away from light to avoid photoluminescence.The sealed source was then removed and the activity of the liquid scintillation cocktail was measured. There was<0.001 pCi beta-gamma and <0.0001 .Ci alpha of removable activity.

J Gas Source TestThe source was placed in a vacuum desiccator and maintained at a pressure of <10 mm Hg for not less than 12 hours.The activity was checked by introducing air into the desiccator and monitoring the air with an end-window G.M. tube.There was <0.001 0Cibeta-gamma of removable activity.

_j Ampoule Leak TestThe ampoule was kept in an inverted position on a filter paper disk or polystyrene wipe for a minimum of 16 hours. Thewipe was then checked for activity using a scintillation detector or liquid scintillation counter. There was <0.001 uCibeta-gamma and <0.0001 I.Ci alpha of removable activity.

IJ Bubble Leak TestThe container was pressurized to its fill pressure; then soapy water was applied over its valve and neck or, the valveand neck of the vessel were immersed in water. If no growing bubbles were observed, the container was consideredleak free.

_j Wipe Test for Industrial Ni-63 SourcesThe sources were wipe tested by an approved sampling plan, which called for either 100% of the batch to beindividually wipe tested, or, a subset thereof. The wipe test(s) used to test for removable contamination and the results

of those tests are recorded on the front of this form.

J Pressure Test for Triotech Kr-85 SourcesPrior to filling the vessel with Kr-85 gas, the vessel was evacuated to <5 mm Hg, the gas manifold system shut off andthe system allowed to stand for a minimum of 30 minutes. A vacuum difference not greater than the known vacuum lossof the manifold system itself signified the vessel did not leak.

JLeak Test Not ApplicableThe active area of the source is uncovered or is protected by a very thin coating. Although the deposit is adherent, it isnot designed or certified to pass a standard leak test. The inactive portions of the source have been checked using thestandard wipe test or special wipe test depending on the nuclide. There was <0.001 pCi beta-gamma and <0.0001 ptCialpha of removablW activity.

I ter LekTest .-

I-

Page 75 of 77/PL FormOOS Rev. C

Site Acceptance Testing was performed on the 1300-S62-1 MA1 Alpha Monitor in for theCentrifuge Assembly Building with final signatures being on 2/6/2009. During thetesting, Section 9.3.5, Flow Rate Verification for Monitor, could not be performed for thefull operating range of the vacuum pump for the skid. The following data was.obtainedon 2/2/2009 using a calibrated flow meter with limited range.

Calibrated Monitor ReadingsFlowmeter Reading within +1-

Ar-O130

F

iLL 7UY24L7i__ • *• ±L ... w• J _

The flow rate recorded is for the total skid flow which is a combination of theParticulate/Iodine Sampler and the Continuous Alpha Monitor.

The calibrated flow meter that maintenance will be using to perform this surveillance inthe future was not available at the time. Condition Report 2009-427 was generated toensure the flow verification was performed when we had the calibrated equipment andhook ups available.

On 6/15/2009 we performed the verification of the flow meter using:

Omega Mass flow meter, Model #FMA1 843, Serial # 230235-3, Cal Due 4/1/2010

We got the following data:

Calibrated Flow meter Monitor Reading Reading within(Ipm) (Ipm) +/-10%

64 58.6 Yes59 55 Yes55 50.6 Yes47 35 No

We test each leg of the skid and found that the Particulate/Iodine Sampler read:

Calibrated Flow meter Monitor Reading Reading within(Ipm) (Ipm) +/- 10%40 44.2 (PIS) Yes40 53.1 (Monitor) No

This indicates the total volume we have been using for our effluent filters wereacceptable because it is calculated from the Particulate/Iodine flow transmitter. Basedon these results, we calibrated the monitor using the manual and the vendorrecommendations. The attached document contains the results from the calibration.

Page 76 of 77

The flow rate test was performed again following the calibration with the followingresults:

Calibrated Flow meter Monitor Reading (Ipm) Reading within(Ipm) +/- 10%

63 58.7 Yes58 55.2 Yes54 50 Yes49 45.1 Yes43 40.1 Yes36 35 Yes30 30.1 Yes23 25 Yes18 20.2 Yes14 15.4 Yes

Page 77 of 77

redacted - louisiana energy services, llc, national enrichment … · 2020. 1. 7. · cc: tyrone d....

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