report no d3155-13 - apps2.staffordshire.gov.uk
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Report No D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL, STOKE-ON-TRENT FACTUAL REPORT ON GROUND INVESTIGATION Carried out for: Education Funding Agency Engineer: Mott MacDonald Ltd January 2014
www.esg.co.uk Environmental Scientifics Group Limited
Reg office: ESG House, Bretby Business Park, Ashby Road, Burton upon Trent, DE15 0YZ Incorporated in England: 02880501
Issue No Date Details 1.0 December 2013 Draft Report 2.0 January 2014 Second draft ; complete geotechnical testing 3.0 January 2014 Final Report
The title to this report is vested in the Employer named but title to copyright is retained. The Contracts (Rights of Third Parties) Act 1999 does not apply to the contract with the Employer and the provisions of the said Act are hereby excluded.
CLOUGH HALL TECHNOLOGY SCHOOL, STOKE-ON-TRENT FACTUAL REPORT ON GROUND INVESTIGATION
Unit 4, Gainsborough Trading Estate, Leamington Road, Southam, Warwickshire, CV47 1RA, UK
Tel: +44 (0) 1926 819300 Fax: +44 (0) 1926 815030 email: [email protected]
Report No: D3155-13
Date: January 2014
Employer: Education Funding Agency 33 Greycoat Street London SW1P 2QF
Engineer: Mott MacDonald Ltd 35 Newhall Street Birmingham B3 3PU
January 2014 Report No D3155-13 Issue 3.0 Page 1 of 7
C O N T E N T S
Page 1 INTRODUCTION 2 2 THE SITE AND GEOLOGY 2 2.1 The Site 2.2 Published Geology 3 FIELDWORK 3 3.1 General 3.2 Exploratory Holes 3.3 Instrumentation and Monitoring 4 LABORATORY TESTING 4 4.1 Geotechnical Testing 4.2 Geoenvironmental Testing REFERENCES 7 ENCLOSURES A EXPLORATORY HOLE RECORDS B INSTRUMENTATION AND MONITORING C GEOTECHNICAL LABORATORY TEST RESULTS D GEOENVIRONMENTAL LABORATORY TEST RESULTS E PHOTOGRAPHS F DRAWINGS
January 2014 Report No D3155-13 Issue 3.0 Page 2 of 7
1 INTRODUCTION
In September 2013 Environmental Scientifics Group (ESG) was commissioned by Mott MacDonald
Ltd, on behalf of the Education Funding Agency, to carry out a ground investigation at Clough Hall
Technology School, First Avenue, Kidsgrove, Stoke-on-Trent. The investigation was required to
obtain preliminary geotechnical and geoenvironmental information to assist in the planning and
design of new buildings at the school as part of the Priority Schools Building Programme.
The scope of the investigation, which was specified by Mott MacDonald Ltd, comprised cable
percussion and rotary cored boreholes, windowless sampler boreholes, hand excavated trial pits
and laboratory testing. The investigation was carried out in accordance with the contract
specification, Eurocode 7 and relevant related standards identified below (see also References).
The fieldwork was carried out between the 10th and 24th October 2013.
This report presents the factual records of the fieldwork and laboratory testing undertaken. The
data is also presented separately in digital format following AGS (2005).
2 THE SITE AND GEOLOGY
2.1 The Site
Clough Hall Technology School lies on the south western side of Kidsgrove, see Site Location
Plan in Enclosure F, about 9km north of Stoke-on-Trent and 4km south east of Alsager. The site is
at National Grid reference SJ 836 542.
The school grounds are irregular in shape, with existing residential development to the north, west
and south. First Avenue lies beyond to the south with Fifth Avenue on the western side. The
northern portal of the Harecastle Tunnel on the Trent and Mersey Canal lies on the eastern side.
Existing buildings and hardstanding covers much of the school ground with small grassed areas on
the western side.
2.2 Published Geology
Published geological information covering the area, British Geological Survey (BGS) Sheet 123
'Stoke-on-Trent' and the BGS website, show superficial Glaciofluvial Deposits across the site,
covering the underlying Carboniferous age bedrock. This comprises the Pennine Middle Coal
January 2014 Report No D3155-13 Issue 3.0 Page 3 of 7
Measures Formation, a succession of mudstone, siltstone, sandstone and occasional coal,
beneath the eastern and western parts of the site with the Ten-feet Rock, a significant sandstone
bed within the Coal Measures strata. The Bellringer coal seam is believed to subcrop beneath the
eastern side of the site.
3 FIELDWORK
3.1 General
The fieldwork was carried out in general accordance with BS 5930+A2 (2010), BS EN 1997-2
(2007) and BS EN ISO 22475-1 (2006).
The exploratory hole locations were selected by Mott MacDonald Ltd and set out from local
features. The co-ordinates and reduced levels were surveyed by ESG to National Grid and
Ordnance Datum. The exploratory hole locations are shown on the Site Plan in Enclosure F.
3.2 Exploratory Holes
The exploratory holes are listed in the following table.
SUMMARY OF EXPLORATORY HOLES
TYPE QUANTITY MAXIMUM DEPTH (m) REMARKS
Cable Percussion Boreholes 2 6.20 BH3 and BH5
Cable Percussion Borehole extended by Rotary Core Drilling 3 29.60 BH1, BH2 and BH4
Windowless Sampler Boreholes 6 5.00 WS1, WS2, WS3, WS4, WS5 and WS6
Trial Pits 2 1.20 TP1 and TP2
The exploratory hole records are presented in Enclosure A and should be read in conjunction with
the Key which is included in that enclosure. The records provide descriptions of the materials
encountered in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003), for soils and
rocks respectively, as amplified by BS 5930+A2 (2010). The records also give details of the
samples taken together with observations made during boring, drilling, windowless sampling and
trial pitting. Standard penetration tests (SPT) were carried out in accordance with BS EN ISO
22476-3:2005+A1 (2011) in the boreholes and windowless sampler holes and the results are
January 2014 Report No D3155-13 Issue 3.0 Page 4 of 7
included on the exploratory hole records. The SPT hammer energy ratio calibration certificates are
also included in Enclosure A.
Photographs of the recovered cores are presented in Enclosure E.
On completion of the fieldwork geotechnical samples were transported to the Southam office of
ESG for temporary retention, with those required for testing being transferred to the in-house
Daventry laboratory. Geoenvironmental samples were taken and stored in accordance with Mott
MacDonald Ltd requirements and BS EN ISO/IEC 17025 (2005) prior to and during transport to the
ESG Scientifics' Burton-on-Trent laboratory.
3.3 Instrumentation and Monitoring
The instruments installed in the exploratory holes are shown on the logs and detailed in
Enclosure B. Records of groundwater and gas monitoring carried out by ESG after the fieldwork
period are presented in Enclosure B.
Following purging of the instruments, groundwater samples for laboratory testing were taken after
the fieldwork.
4 LABORATORY TESTING
4.1 Geotechnical Testing
The testing was scheduled by Mott MacDonald Ltd and was carried out in accordance with
BS 1377 (1990) unless otherwise stated. The testing is summarised below and the results are
presented in Enclosure C.
SUMMARY OF GEOTECHNICAL LABORATORY TESTING
TYPE REMARKS
Moisture Content Determination
Atterberg Limit Determination
Particle Size Distribution Analysis
Total Sulphate Content, Water Soluble Sulphate Content, Total Sulphur Content and pH Value of Soils
Testing by ESG Scientifics; test methods are BS 1377 or others recognised in BRE Special Digest 1 (2005); they are indicated on the results report sheets in Enclosure C
Organic Matter Content
January 2014 Report No D3155-13 Issue 3.0 Page 5 of 7
TYPE REMARKS
Dry Density/Moisture Content Relationship (Light 2.5g compaction)
Moisture Condition Value/Moisture Content Relationship
California Bearing Ratio
One Dimensional Oedometer Consolidation Testing
Unconsolidated Undrained Triaxial Compression Tests
Unconfined Compressive strength
Point Load Index
4.2 Geoenvironmental Testing
The testing was scheduled by Mott MacDonald Ltd and was carried out by ESG Scientifics. Details
of the suites scheduled are summarised below and the results are presented in Enclosure D.
SUMMARY OF GEOENVIRONMENTAL LABORATORY TESTING
TYPE REMARKS
Soil Contamination Suites
PSBP Schools Soil Suite
Asbestos screen and ID, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium,
Copper, Iron, Lead, Mercury, Molybdenum, Nickel, Selenium, Vanadium, Zinc, Water Soluble
Sulphate, Total Sulphur (BRE), pH, TPH CWG to include GRO/BTEX, Speciated PAH, VOC, Phenol
Index, Fraction Organic Carbon
20No
Polychlorinated biphenyl (PCB) 12 congeners 2No
Leachate and Water Contamination Suites
PSBP Schools Leachate Suite
Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium (trivalent), Chromium
(hexavalent), Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Selenium,
Sodium, Vanadium, Zinc, Ammoniacal Nitrogen, Chloride, Sulphide, Sulphate, pH, Cyanide (free),
Cyanide (total), Nitrate, Thiocyanate , BTEX, 16 PAH, Phenols by HPLC
20No
PSBP Schools Water Suite
Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Copper, Iron, Lead,
Magnesium, Manganese, Mercury, Nickel, Selenium, Vanadium, Zinc, Chloride, Fluoride, Sulphide,
Sulphate, pH, Cyanide (free), Cyanide (total), Thiocyanate , BTEX, 16 PAH, Phenols by HPLC, TPH
CWG
3 No
January 2014 Report No D3155-13 Issue 3.0 Page 7 of 7
REFERENCES
AGS : 2005 : Electronic transfer of geotechnical and geoenvironmental data (Edition 3.1 including addendum May 2005). Association of Geotechnical and Geoenvironmental Specialists.
BGS Sheet 123: 1994 : Stoke-on-Trent. 1:50000 geological map (solid and drift). British Geological Survey
Baldwin M, Gosling R C and Brownlie N : 2007 : Soil and rock descriptions - a practical guide to the implementation of BS EN ISO 14688 and 14689. Ground Engineering, July.
BRE Special Digest 1 : 2005 : Concrete in aggressive ground. Building Research Establishment.
BS 1377 : 1990 : Methods of test for soils for civil engineering purposes. British Standards Institution.
BS 5930+A2 : 2010 : Code of practice for site investigations (Amendment 2). British Standards Institution.
BS EN 1997-2 : 2007 : Eurocode 7 - Geotechnical design - Part 2 Ground investigation and testing. British Standards Institution.
BS EN ISO 14688-1 : 2002 : Geotechnical investigation and testing - Identification and classification of soil - Part 1 Identification and description. British Standards Institution.
BS EN ISO 14689-1 : 2003 : Geotechnical investigation and testing - Identification and classification of rock - Part 1 Identification and description. British Standards Institution.
BS EN ISO 22475-1 : 2006 : Geotechnical investigation and testing – Sampling methods and groundwater measurements - Part 1 Technical principles for execution. British Standards Institution.
BS EN ISO 22476-3:2005+A1 : 2011 : Geotechnical investigation and testing - Field testing - Part 3 Standard penetration test. British Standards Institution.
BS EN ISO/IEC 17025 : 2005 : General requirements for the competence of testing and calibration laboratories. British Standards Institution.
GIFA10 : 2010 : Ground Investigation Services Framework Agreement. Mott Macdonald Ltd.
January 2014 Report No D3155-13 Issue 3.0 Enclosure A
ENCLOSURE A
EXPLORATORY HOLE RECORDS
Key to Exploratory Hole Records Key
Hammer Energy Ratio Reports Calibration certificates for SM19, SM39 and 100 87MR
Borehole Logs BH1, BH2, BH3, BH4 and BH5
Windowless Sampler Logs WS1, WS2, WS3, WS4, WS5 and WS6
Trial Pit Logs TP1 and TP2
Notes: See report text for full references of standards
Project
Project No. Carried out for
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13 Education Funding Agency
Key Sheet 1 of 2
Key to Exploratory Hole Records
SAMPLES Undisturbed U UT TW P L CBR BLK CS AMAL
Driven tube sample Driven thin wall tube sample nominally 100 mm diameter and full recovery unless otherwise stated Pushed thin wall tube sample Pushed piston sample Liner sample (from Windowless or similar sampler), full recovery unless otherwise stated CBR mould sample Block sample Core sample (from rotary core) taken for laboratory testing Amalgamated sample
Disturbed D B
Small sample Bulk sample
Other W G ES EW
Water sample Gas sample Environmental chemistry samples (in more than one container where appropriate) Soil sample Water sample
Comments Sample reference numbers are assigned to every sample taken. A sample reference of 'NR' indicates that attempt was made to take a tube sample, however, there was no recovery. Monitoring samples taken after completion of hole construction are not shown on the exploratory hole logs.
TESTS SPT S or SPT C IV HV PP KFH, KRH, KPI
Standard Penetration Test, open shoe (S) or solid cone (C) The Standard Penetration Test is defined in BS EN ISO 22476-3 (2005). The incremental blow counts are given in the Field Records column; each increment is 75 mm unless stated otherwise and any penetration under self weight in mm (SW) is noted. Where the full 300 mm test drive is achieved the total number of blows for the test drive is presented as N = ** in the Test column. Where the test drive blows reach 50 the total blow count beyond the seating drive is given (without the N = prefix). in situ Vane shear strength, peak (p) and remoulded (r) Hand vane shear strength, peak (p) and remoulded (r) Pocket penetrometer test, converted to shear strength Permeability tests (KFH = falling head, KRH = rising head; KPI = packer inflow); results provided in Field Records column (one value per stage for packer tests)
DRILLING RECORDS The mechanical indices (TCR/SCR/RQD & If) are defined in BS 5930+A2 (2010)
TCR SCR RQD If
Total Core Recovery, % Solid Core Recovery, % Rock Quality Designation, % Fracture spacing, mm. Minimum, typical and maximum spacings are presented. The term non-intact (NI) is used where the core is fragmented.
Flush returns, estimated percentage with colour where relevant, are given in the Records column CRF AZCL NR
Core recovered (length in m) in the following run Assessed zone of core loss Not recovered
GROUNDWATER
Groundwater strike Groundwater level after standing period
Notes: See report text for full references of standards
Project
Project No. Carried out for
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13 Education Funding Agency
Key Sheet 2 of 2
Key to Exploratory Hole Records
INSTALLATION Standpipe/ piezometer SP SPIE PPIE EPIE Inclinometer or Slip Indicator ICE ICM SLIP Settlement Points or Pressure Cells ESET ETM EPCE PPCE
Details of standpipe/piezometer installations are given on the Record. Legend column shows installed instrument depths including slotted pipe section or tip depth, response zone filter material type and layers of backfill. The type of instrument installed is indicated by a code in the Legend column at the depth of the response zone: Standpipe Standpipe piezometer Pneumatic piezometer Electronic piezometer The installation of vertical profiling instruments is indicated on the Record. The base of tubing is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column at the base of the tubing: Biaxial inclinometer Inclinometer tubing for use with probe Slip indicator The installation of single point instruments is indicated on the Record. The location of the measuring device is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column: Electronic settlement cell/gauge Magnetic extensometer settlement point Electronic embedment pressure cell Electronic push in pressure cell
INSTALLATION LEGENDS
A legend describing the installation is shown in the rightmost column. Legends additional to BS5930 are used to describe the backfill materials as indicated below.
Arisings
Concrete
Grout
Bentonite
Sand
Gravel
Macadam
NOTES 1 2 3 4 5 6 7 8
Soils and rocks are described in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003) respectively as amplified by BS 5930+A2 (2010). For fine soils, consistency determined during description is reported for those strata where undisturbed samples are available. Where the logger considers that the sample may not be representative of the condition in situ, for whatever reason, the reported consistency is given in brackets. The reliability of the sample is indicated by Probably or Possibly as appropriate. Hence (Probably firm) indicates the logger is reasonably confident of the assessment, but (Possibly firm) means less certainty. Where the samples available are too disturbed to allow a reasonable assessment of the in situ condition, no consistency is given. Evidence of the occurrence of very coarse particles (cobbles and boulders) is presented on the logs, however, because of their size in relation to the exploratory hole these records may not be fully representative of their size and frequency in the ground mass. The declination of bedding and joints is given with respect to the normal to the core axis. Thus in a vertical borehole this will be the dip. The assessment of SCR, RQD and Fracture Spacing excludes artificial fractures Strata legends are in accordance with BS 5930+A2 (2010). Water level observations of discernible entries during the advancing of the exploratory hole are given at the foot of the log and in the Legend column. The term "none observed" is used where no discrete entries are identified although this does not necessarily indicate that the hole has not been advanced below groundwater level. Under certain conditions groundwater cannot be observed, for instance, drilling with water flush or overwater, or boring at a rate much faster than water can make its way into the borehole (ref BS5930+A2:2010, Clause 47.2.7). In addition, where appropriate, water levels in the hole at the time of recovering individual samples or carrying out in situ tests and at shift changes are given in the Records column. The borehole logs present the results of Standard Penetration Tests recorded in the field without correction or interpretation. However, in certain ground conditions (eg high hydraulic head or where very coarse particles are present) some judgement may be necessary in considering whether the results are representative of in situ mass conditions.
Updated March 2012
Date of test: 19/02/2013 Hammer ID: SM19Hammer mass (m ) 63.5 kg
Instrumented rod: Fall height (h ) 0.76 mType BW SPTCross-sectional area (A a) 11.30 cm2 Manufacturer: ArchwayYoung's modulus (E a) 207000 MPa Automatic Trip HammerLength 0.60 m
Rig: Beretta T51Test rod type: NWY Rig ID: T51-R59
Type: RotaryForeman: M Atkinson
Remarks:
Test type:
Model:
Data obtained from test carried out in BH1, located in ESG Doncaster yard. Test carried out at depth of 5.10mbgl, with a total blow count of 20. Energy determined from every blow.
80
120
160
200
240
Forc
e (k
N)
Force - typical blow
1.5
2.5
3.5
4.5
loci
ty (m
/s)
Particle Velocity - typical blow
Hammer Energy Report
Theoretical energy (E theor) = m x g x h = 0.473 kN-m (473 J)
Measured energy (E meas) average of 20 blows = 0.311 kN-m
E meas
E theor
Test carried out by: Malcolm Carr Test carried out in accordance with BS EN ISO 22476-3:2005
Signed for issue: Equipment used: SPT Analyzer Serial No 4032T
66 %=Energy ratio =
0
20
40
60
80
100
100 150 200 250
Ener
gy r
atio
(%)
Force (kN)
0
20
40
60
80
100
0 5 10 15 20 25
Ener
gy r
atio
(%)
Blow
average
-40
0
40
80
120
0 5 10 15
Forc
e (k
N
time (ms)
-0.5
0.5
1.5
2.5
0 5 10 15
Velo
city
(m
time (ms)
Signed for issue: Equipment used: SPT Analyzer Serial No. 4032T
Date of test: 19/02/2013 Hammer ID: SM38Hammer mass (m ) 63.5 kg
Instrumented rod: Fall height (h ) 0.76 mType BW SPTCross-sectional area (A a) 11.30 cm2 Manufacturer: ArchwayYoung's modulus (E a) 207000 MPa Automatic Trip HammerLength 0.60 m
Rig: Beretta T51Test rod type: NWY Rig ID: T51-R59
Type: RotaryForeman: M Atkinson
Remarks:
Test type:
Model:
Data obtained from test carried out in BH1, located in ESG Doncaster yard. Test carried out at depth of 5.25mbgl, with a total blow count of 20. Energy determined from every blow.
40
80
120
160
Forc
e (k
N)
Force - typical blow
1.5
2.5
3.5
eloc
ity (m
/s)
Particle Velocity - typical blow
Hammer Energy Report
Theoretical energy (E theor) = m x g x h = 0.473 kN-m (473 J)
Measured energy (E meas) average of 20 blows = 0.350 kN-m
E meas
E theor
Test carried out by: Malcolm Carr Test carried out in accordance with BS EN ISO 22476-3:2005
Signed for issue: Equipment used: SPT Analyzer Serial No 4032T
74 %=Energy ratio =
0
20
40
60
80
100
100 150 200 250
Ener
gy r
atio
(%)
Force (kN)
0
20
40
60
80
100
0 5 10 15 20 25
Ener
gy r
atio
(%)
Blow
average
-40
0
40
80
0 5 10 15
Forc
e (k
N
time (ms)
-0.5
0.5
1.5
0 5 10 15
Velo
city
(m
time (ms)
Signed for issue: Equipment used: SPT Analyzer Serial No. 4032T
7.14-7.436.60-8.00
8.00-8.11
8.00-9.60
9000
10030
1005141
100180
B 1D 2B 4
ES 3B 5
ES 6D 7B 11D 8D 10ES 9
SPT SD 12B 13
ES 14D 15
SPT SD 16B 17
SPT SD 18B 19B 20
NI2030
NI3050
NI90
300
NI70
220
Flush: 4.50-11.10Water, 90 %
N=5 (1,-/1,1,1,2)
N=15 (3,4/4,3,4,4)
N=43 (4,4/4,7,13,19)
If /NR/
CS 21
1.50
2.50
3.00
09/10/20134.30
15/10/20134.30
4.40
15/10/20134.40
16/09/20134.40
dry
dry
dry
08003.42
4.90
08003.74
0.10
0.30
0.70
1.60
2.00
3.50
3.70
4.30
4.50
4.95
6.00
(0.40)
(0.90)
(0.40)
(1.50)
(0.60)
(0.45)
(1.05)
+131.29
+131.09
+130.69
+129.79
+129.39
+127.89
+127.69
+127.09
+126.89
+126.44
+125.39
MADE GROUND: macadam.
MADE GROUND: black very sandy GRAVEL.Sand is medium to coarse. Gravel is angularfine to coarse brick, clinker, slag andmacadam.
MADE GROUND: brown slightly sandy GRAVELwith occasional coarse gravel size softgrey clay pockets. Gravel is angular fineto coarse brick, clinker and coal.
MADE GROUND: soft grey brown slightlygravelly sandy CLAY. Gravel is angular torounded fine of coal and brick.
Possible MADE GROUND: soft brown sandygravelly CLAY. Gravel is subrounded to
Time Tools used
rounded fine to coarse quartzite.
Medium dense light brown gravelly clayeyfine to medium SAND. Gravel is roundedfine to medium sandstone.(GLACIOFLUVIAL DEPOSITS)
Firm brown mottled grey slightly gravellysandy CLAY. Gravel is subangular fine tocoarse sandstone.(Possible GLACIOFLUVIAL DEPOSITS)
From
Very stiff friable grey mottled brown CLAYtending to extremely weak MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
Very weak grey mottled brownSILTSTONE.(PENNINE MIDDLE COALMEASURES FORMATION)
Very weak and weak grey SILTSTONE.
to (m)
(PENNINE MIDDLE COAL MEASURESFORMATION)Weathering: brown discolouration,penetrating up to 5mm, adjacent tofractures. Fractures are randomlyorientated, extremely closely and veryclosely spaced, undulating rough,generally silt smeared (<1mm), occasionalclayey fine gravel infill (1-5mm)
Generally weak grey sandy SILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Weathering: heavily stained dark orange
Checked
brown, penetrating up to 3mm. Fracturesare randomly orientated, very closelyspaced, undulating rough, generally clean,occasionally silt smeared (<1mm).
Weak to medium strong thinlyinterlaminated light grey fine grainedslightly micaceous SANDSTONE andSILTSTONE. Rare coal and ironstone bands.(PENNINE MIDDLE COAL MEASURESFIORMATION)Weathering: includes orange brown stainingand quartz mineralization.Fractures are 1) subvertical and inclined
Equipment, Methods and Remarks
65-80deg, extremely closely and veryclosely spaced, generally clean,occasionally clayey gravel infill (<40mm)2) randomly orientated, very closely towidely spaced, undulating rough, generally
1:50
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AH/PSMQ/MBJRL
09/10/2013
17/10/2013
TCRSCRRQD
Type & No
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m
Records/Samples
Records
426.4823/01/2014 15:57:11(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Stratum continues to 29.60 m
National Grid
Chainage
BH1Sheet 1 of 3
+131.39 mODE 383570.56N 354283.87
1.50 3.50 SPT hammer ID SM398.00 29.60 SPT hammer ID SM19
4.50m0.00m 150mm29.60m4.50m 120mm
4.30m4.40m
4.10 -4.30 60 mins
SPT S 50 (25 for 70mm/50 for 40mm)
*
*
4.30-4.38 m AZCL
6.00-6.80 mbedding
overturned,stained orange
brown,occasional
quartrzmineralization
7.00 m 80degfracture, clayey
gravel infill(15mm)
7.30 m 75degfracture
7.45-8.20 mbedding fractures
overturned,gravelly clay infill
(<25mm)7.85-8.20 m
randomlyorientated, veryclosely spaced,
stained orangishbrown
8.60-9.50 mpersistent
subverticalbedding fracture,clayey gravel infill
(10-30mm)
9.50-10.25 mfractures
occasional quartzmineralization
(<1mm)
0.00-0.100.00-0.100.10-0.30
0.200.30-0.70
0.500.50
0.70-1.200.701.001.00
1.50-1.951.50-1.951.50-2.00
2.002.00
2.50-2.952.50-2.952.50-3.00
3.50-3.953.50-3.953.50-3.703.70-4.00
4.30-5.10
5.10-6.60
fracture16.30-18.95 m
persistentsubverticalfractures,
gravelly clay infill<40mm
19.10 m 25degfracture
19.50 m 55degstepped fracture
19.60-19.80 msubverical
smooth fracture,
10.25-10.429.60-11.10
11.10-11.1911.10-11.39
11.10-12.60
12.60-15.60
14.91-15.27
15.60-15.66
15.94-16.24
15.60-18.60
18.60-18.67
19.30-19.50
1007047
978255
1008271
1006852
30100300
20100300
15130380
10140430
40200400
Flush: 11.10-22.15Water, 0 %
CS 22
CS 23
CS 24
CS 25
CS 26
4.40
4.40
4.40
(23.60)
SP
clean, sometimes silt smeared (<1mm).Bedding fractures occasionally overturned.
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AH/PSMQ/MBJRL
09/10/2013
17/10/2013
TCRSCRRQD
TCRSCRRQD
If
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m
Records/Samples
Records/Samples
426.4823/01/2014 15:57:14(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Stratum continues to 29.60 m
(Continued from Sheet 1)(Continued from Sheet 1)
National Grid
Chainage
BH1Sheet 2 of 3
+131.39 mODE 383570.56N 354283.87
4.50m0.00m 150mm29.60m4.50m 120mm
4.30m4.40m
SPT S 50 (25 for 50mm/50 for 40mm)
SPT S 50 (25 for 30mm/50 for 30mm)
SPT S 50 (25 for 30mm/50 for 40mm)
10.25-12.60 mvery closely to
medium spacedinclined,
occasionallystriated, fractures
12.00 msubvertical
fracture, quartzmineralization
12.30-12.80 minclined 65-75
deg beddingfractures, little
pyriticmineralization
(<1mm)12.90 m 35deg
fracture13.20 m 30deg
fracture13.30 m 15deg
fracture13.60 m 45degplanar fracture13.80-14.20 m2No extremelyclosely spaced
subverticalfractures, silt
smeared (<1mm)14.20-14.26 msubhorizontalstrong brown
IRONSTONE14.35-14.55 m
subverticalfracture
14.60-14.95 msubvertical
fracture15.30 m 35deg
fracture15.40 m 60deg
fracture15.90 m 10deg
29.07 msubhorizontal
fracture29.25 m 35deg
fracture
18.60-21.60
21.60-21.65
21.60-22.15
22.96-23.29
22.15-24.60
24.60-24.65
25.42-25.57
24.60-27.30
27.30-27.36
27.30-27.70
27.70-29.60
29.08-29.24
29.60-29.66
1008574
10000
1007064
1009277
100100100
978767
NI260800
NI200400
20400800
20250300
NI180310
Flush: 22.15-29.60Water, 90 %
CS 27
CS 28
CS 29
4.40
16/09/20134.40
17/10/20134.40
4.40
4.40
4.40
3.65
0800
29.60 +101.79
Weak to medium strong thinlyinterlaminated light grey fine grainedslightly micaceous SANDSTONE andSILTSTONE. Rare coal and ironstone bands.(PENNINE MIDDLE COAL MEASURESFIORMATION)Weathering: includes orange brown stainingand quartz mineralization.Fractures are 1) subvertical and inclined65-80deg, extremely closely and veryclosely spaced, generally clean,occasionally clayey gravel infill (<40mm)2) randomly orientated, very closely towidely spaced, undulating rough, generallyclean, sometimes silt smeared (<1mm).Bedding fractures occasionally overturned.
EXPLORATORY HOLE ENDS AT 29.60 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AH/PSMQ/MBJRL
09/10/2013
17/10/2013
TCRSCRRQD
TCRSCRRQD
If
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m
Records/Samples
Records/Samples
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
(Continued from Sheet 2)(Continued from Sheet 2)
National Grid
Chainage
BH1Sheet 3 of 3
+131.39 mODE 383570.56N 354283.87
4.50m0.00m 150mm29.60m4.50m 120mm
4.30m4.40m
SPT S 50 (25 for 20mm/50 for 30mm)
SPT S 50 (25 for 20mm/50 for 30mm)
SPT S 50 (25 for 40mm/50 for 20mm)
SPT S 50 (25 for 20mm/50 for 40mm)
quartzmineralization
20.00-22.10 mpersistent
subverticalfractures, clayey
gravel infill, quartzmineralization
22.40-22.50 mtwo inclined 60-70
deg thin coallaminae
22.55-22.95 msubverticalfractures,
generally clean,quartz
mineralization,occasional plant
remains23.25 m 50deg
planar silt coatedfracture
23.80 m 30 degfracture
23.90-24.05 minclined
60-70degfractures
24.25-24.55 msubvertical
fracture
26.10 m30degclay infilled(<5mm) fracture
26.85-27.25 m85deg fracture,
silt smeared
28.00 m 45degfracture
28.15 m 45degfracture
28.50 msubhorizontal
clay infilled(<10mm) fracture
3.50-3.60
3.50-4.15
4.15-5.905.16-5.34
6.10-6.26
5.90-8.20
8.20-8.29
8.20-9.50
1008888
916050
1006321
81238
B 1D 2
ES 3D 4B 5D 6
ES 7B 8
ES 9
D 10U 11
ES 13D 12
SPT SD 14B 15
SPT SD 16
NI100220
540
220
40100300
NI70
200
NR
Flush: 3.50-4.15Water, 80 %
Flush: 4.15-5.90Water, 70 %
Flush: 5.90-9.50Water, 60 %
33 blows
N=15 (4,4/3,4,4,4)
50 (25/50 for 30mm)
If /NR/
If NI/40/60
If /NR/
CS 17
CS 18
1.50
2.50
15/10/20133.00
18/10/20133.50
4.00
1.40
2.40
3.10
0800
0.10
0.30
0.50
1.351.40
3.503.60
5.75
6.05
6.85
7.40
(0.85)
(2.10)
(2.15)
(0.30)
(0.80)
(0.55)
(5.00)
+133.52
+133.32
+133.12
+132.27+132.22
+130.12+130.02
+127.87
+127.57
+126.77
+126.22
1
1
MADE GROUND: macadam.
MADE GROUND: black and dark brown SANDand GRAVEL. Sand is medium to coarse. Gravelis angular medium to coarse brick, clinkerand slag.
MADE GROUND: reddish brown sandy GRAVELof angular fine to coarse limestone.
Time Tools used
MADE GROUND: soft to firm grey mottledbrown slightly sandy slightly gravellyCLAY with low cobble content. Gravel isrounded fine mudstone and angular finesandstone and coal. Cobbles are quartz.
Possible MADE GROUND: brown fine SAND.
fIRM grey gravelly CLAY. Gravel is angularfine to coarse sandstone.(PENNINE MIDDLE COAL MEASURES
From
FORMATION)
Extremely weak grey SANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
Strong to very strong light grey finegrained quartzitic SANDSTONE, locally withextremely closely spaced thin grey andblack wispy laminations.(PENNINE MIDDLE COAL MEASURESFORMATION)
to (m)
Fractures are 1) inclined 20-30deg, veryclosely and closely spaced, planar rough,generally clean, occasional silty finesand infill (1-3mm), generaly stainedorangish brown 2) inclined 60-80deg,planar rough, stained orangish brown.
Weak to medium strong thinly laminatedgrey silty MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are inclined 25-30deg, veryclosely spaced, planar clean.
Checked
Medium strong laminated light grey finegrained quartzitic SANDSTONE withextremely and very closely spaced thindark grey mudstone and black coal wispylaminae.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are inclined 25-30deg, extremelyclosely to closely spaced, undulatingrough, clean.
Medium strong thinly interlaminated light
Equipment, Methods and Remarks
grey fine grained quartzitic SANDSTONE andgrey SILTSTONE.(PENNINE MIDDLE COSAL MEASURESFORMATION)Fractures are inclined 25-30 deg, closelyand medium spaced, planar smooth, clean,stained dark grey, occasionally incipient.
Weak, locally indistinctly laminated, greyMUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
Backfill/
1:50
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole LogAH/PSMQ/MBJRL
15/10/2013
23/10/2013
TCRSCRRQD
Type & No
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m
Records/Samples
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Stratum continues to 12.40 m
National Grid
Chainage
BH2Sheet 1 of 3
+133.62 mODE 383637.48N 354171.53
1.401 Rose to 1.30 m after 20 minutes. Slow -2.50 3.50 SPT hammer ID SM398.20 24.60 SPT hammer ID SM199.50 11.60 Flush: Water, 50%
3.60m0.00m 150mm25.50m3.60m 120mm
3.00m4.00m
3.30 -3.50 60 mins
SPT S 50 (25 for 40mm/50 for 50mm)
*
*
*
3.50-3.55 m NI,recovered as
angular gravel
4.60-4.70 m70deg fracture
5.40-5.65 m75deg fracture
5.75-5.90 m AZCL
6.40-6.60 m 2Nointersecting
inclined45-60degfractures
6.60-6.85 mextremely closely
spaced coallaminae
7.75-7.82 m NI,clayey gravel
8.03-8.10 m NI,clayey gravel
8.35-8.90 m veryclosely fractured,
generally NI
9.25-9.50 m AZCL
9.70-9.90 m veryclosely fractured,
NI
0.00-0.100.200.200.30
0.30-0.500.500.50
0.50-1.201.00
1.401.50-1.95
2.002.05
2.50-2.952.50-2.952.50-3.00
3.50-3.61
17.75-17.85 mstrong
IRONSTONE
18.40-18.50 mstrong
IRONSTONE18.50-19.60 m
occasionalsubvertical
quartz veining<3mm
18.75-18.90 m60deg fracture19.05-19.40 m
subverticalfracture
19.75-19.85 mstrong
9.50-10.50
10.50-10.60
10.50-11.60
11.60-13.00
13.00-13.9013.50-13.58
13.90-14.70
14.70-16.10
16.10-17.00
17.00-17.07
17.40-17.5617.00-18.10
18.10-19.6018.88-19.06
19.60-19.66
100170
100120
100130
1006717
1003613
894929
100280
1003223
935542
NI4080
NI10
200
NI150580
Flush: 11.60-17.00Water
Flush: 17.00-18.10Water, 50 %
CS 19
CS 20
18/10/20134.00
21/10/20134.00
4.00
21/10/20134.00
22/10/20134.00
4.00
08001.35
08001.15
12.40
16.35
(3.95)
+121.22
+117.27
Fractures are 1) inclined 20-30deg, veryclosely and closely spaced, planar andundulating, smooth, generally clean,occasional sandy clay infill (1-2mm) 2)randomly orientated, very closely andclosely spaced, undulating smooth, clean,sometimes incipient.
Weak to medium strong dark greyish brownMUDSTONE with occasional marine bands.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are 1) inclined 20-30 deg,closely spaced, undulating smooth,generally clean, occasional silty clayinfill (1-2mm).
Weak, locally thinly laminated, greyMUDSTONE with medium and widely spacedthin strong brown IRONSTONEinterbeds/nodules and occasional mediumstrong light grey and grey fine grainedSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
Time Tools used
Fractures are 1) inclined 20-30deg,closely and medium spaced, undulatingsmooth, generally clean, occasionalgravelly clay infill (<20mm) 2) randomlyorientated, planar and undulating,smooth,generally clean, occasional gravelly clayinfill (<20mm).
1:50
From to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole LogAH/PSMQ/MBJRL
15/10/2013
23/10/2013
TCRSCRRQD
TCRSCRRQD
If
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m
Records/Samples
Records/Samples
426.4823/01/2014 15:58:15(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Stratum continues to 25.50 m
(Continued from Sheet 1)(Continued from Sheet 1)
National Grid
Chainage
BH2Sheet 2 of 3
+133.62 mODE 383637.48N 354171.53
3.60m0.00m 150mm25.50m3.60m 120mm
3.00m4.00m
SPT S 50 (25 for 70mm/50 for 30mm)
SPT S 50 (25 for 40mm/50 for 40mm)
SPT S 50 (25 for 30mm/50 for 40mm)
SPT S 50 (25 for 30mm/50 for 30mm)
10.80-11.35 mvery closely
fractured,recovered NI
11.50-12.40 mdark grey, very
closely fractured
13.00-13.20 mextremely closelyand very closely
spaced marinebands (<5mm)
13.45 m marineband (5mm)
13.85 m marineband (5mm)
14.50-14.60 m NI
15.50-15.95 mextremely closelyand very closely
spaced marinebands (<10mm)15.95-16.10 m
AZCL16.20-16.35 m
AZCL
17.05-17.15 mstrong
IRONSTONE17.40-17.55 mmedium strongSANDSTONE
21.26-21.54
21.10-22.40
22.40-22.46
22.40-23.80
24.11-24.2523.80-24.60
24.60-24.66
24.60-26.00
26.00-27.50
1005337
1005252
862216
883928
642111
3330
NI3080
NR
NI70
160
NR
NI480
Flush: 18.10-27.50Water
If /NR/
CS 21
CS 22
4.00
22/10/20134.00
23/10/20134.00
2.46
08004.00
25.50
27.50
(9.15)
(2.00)
+108.12
+106.12
SP
Weak, locally thinly laminated, greyMUDSTONE with medium and widely spacedthin strong brown IRONSTONEinterbeds/nodules and occasional mediumstrong light grey and grey fine grainedSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are 1) inclined 20-30deg,closely and medium spaced, undulatingsmooth, generally clean, occasionalgravelly clay infill (<20mm) 2) randomlyorientated, planar and undulating,smooth,generally clean, occasional gravelly clayinfill (<20mm).
Partial recoveryRecovered core comprises weak thinlylaminated dark grey to black carbonaceousMUDSTONE with frequent plant remains andoccasional thin coal laminae.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated, veryclosely spaced, undulating rough.
EXPLORATORY HOLE ENDS AT 27.50 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole LogAH/PSMQ/MBJRL
15/10/2013
23/10/2013
TCRSCRRQD
TCRSCRRQD
If
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m
Records/Samples
Records/Samples
426.4823/01/2014 15:58:18(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
(Continued from Sheet 2)(Continued from Sheet 2)
National Grid
Chainage
BH2Sheet 3 of 3
+133.62 mODE 383637.48N 354171.53
3.60m0.00m 150mm25.50m3.60m 120mm
3.00m4.00m
SPT S 50 (25 for 20mm/50 for 40mm)
SPT S 50 (25 for 30mm/50 for 30mm)
IRONSTONE, 2No60deg fractures
20.45-20.65 m70deg fracture20.65-20.87 m
strongIRONSTONE, 2no
subverticalfractures
20.87-21.05 m NI21.20-21.30 m
strongIRONSTONE,65deg fracture21.50-21.60 m70deg fracture21.77-21.83 m
strongIRONSTONE
22.00-22.40 mvery closelyfractured, NI
22.95-23.00 mstrong
IRONSTONE
23.45-23.60 m NI23.60-23.90 m
AZCL
23.90-23.95 mstrong
IRONSTONE
24.55-24.70 mstrong
IRONSTONE24.75-25.30 m2No 75-80deg
fractures
25.40-25.45 mstrong
IRONSTONE25.50-27.00 m
AZCL
19.60-21.10
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AHMQJRL
10/10/2013
10/10/2013
Type & No
Type & No
Dando 3000Service inspection pit hand excavated to 1.20mCable percussion to 3.10m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
National Grid
Chainage
BH3Sheet 1 of 1
+137.60 mODE 383617.37N 354115.86
2.50 3.00 SPT hammer ID SM39
3.10m0.00m 150mm 3.00m
2.80 -3.00 60 mins
*
0.00-0.100.200.20
0.20-0.400.40
0.40-1.200.50
1.00
1.50-1.95
2.002.05
2.50-2.912.50-2.902.50-2.80
3.00-3.103.00-3.10
B 1D 2
ES 3B 4D 5B 7
ES 6
ES 8
U 9
ES 11D 10
SPT SD 12B 13
SPT SD 14
25 blows 315 mm rec
50 (1,1/2,2,30,16 for 30mm)
50 (25 for 40mm/50 for 60mm)
1.50
2.50
3.00
dry
0.00
dry
dry
0.10
0.40
1.40
2.80
3.10
(0.30)
(1.00)
(1.40)
(0.30)
+137.50
+137.20
+136.20
+134.80
+134.50SP
MADE GROUND: macadam.
MADE GROUND: brown silty very sandyGRAVEL. Sand is fine to coarse. Gravel isangular fine to coarse brick, macadam,coal, sandstone and concrete.
MADE GROUND: soft to firm reddish brownslightly gravelly CLAY and orangish brownfine to medium SAND with occasional greyslightly sandy silt pockets. Gravel isangular fine coal, mudstone and sandstone.
Reddish brown gravelly clayey fine tomedium SAND. Gravel is subangular tosubrounded fine to coarse sandstone.(Possible GLACIOFLUVIAL DEPOSITS)
Extremely weak light grey SILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 3.10 m
1:50
2.50-3.00
3.50-3.883.50-3.903.50-4.00
4.50-4.734.50
4.50-5.60
5.60-7.10
7.10-7.55
7.55-7.63
7.55-8.30
8.30-8.40
8.40-8.80
9.10-9.28
8.80-9.90
79110
1004127
2200
100170
1005028
1005858
B 1B 4D 2
ES 3B 5D 6
ES 7B 8
ES 9
U 10
D 11
SPT SD 12B 13
SPT SD 14B 15
SPT SD 16NR
NI1080
NI3575
NI4090
NI150400
NR
NI60
130
NI70
180Flush: 4.50-13.90
water, 100 %
80 blows
50 (6,8/10,13,17,10 for 40mm)
50 (7,11/11,15,24)
50 (7,18/50)If /NR/
TCR 100, SCR 0, RQD 0
CS 17
1.50
2.50
10/10/20132.50
11/10/20132.50
3.00
11/10/20133.00
23/10/20133.50
3.50
23/10/20133.50
24/10/20134.50
dry
dry
dry
0800dry
dry
dry
08000.15
2.10
08001.36
0.100.25
0.50
2.50
4.50
5.40
5.75
6.50
7.10
8.30
9.55
(2.00)
(2.00)
(0.90)
(0.35)
(0.75)
(0.60)
(1.20)
(1.25)
+139.38+139.23
+138.98
+136.98
+134.98
+134.08
+133.73
+132.98
+132.38
+131.18
+129.93
Time Tools usedFrom
MADE GROUND: macadam.
MADE GROUND: red and brown SAND andGRAVEL. Sand is medium to coarse. Gravelis angular fine to coarse brick, concreteand clinker.
Possible MADE GROUND: firm grey gravellySILT. Gravel is angular fine siltstone andcoal.
to (m)
Stiff grey slightly sandy slightlygravelly CLAY. Gravel is subangular fineto medium mudstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
Very stiff grey slightly sany slightlygravelly CLAY, occasionally tending toextremely weak SILTSTONE, with occasionalcoal bands. Gravel is subangular fine tomedium mudstone and siltstone.(PENNINE MIDDLE COAL MEASURES
Checked
FORMATION)
Extremely weak friable grey MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely spaced, undulatingsmooth.
Weak black COAL.(PENNINE MIDDLE COAL MEASURESFORMATION)
Equipment, Methods and Remarks
Fractures are inclined 20-25deg andsubvertical, very closely spaced.
Very weak to weak grey and light greyMUDSTONE. Occasional fossil plant remains.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely to closely spaced,undulating smooth, occasionally clayinfilled (<15mm).
Backfill/
Very weak to weak grey fine grainedslightly micaceous SANDSTONE andSILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely to medium spaced,undulating rough. Often very closelyspaced, incipient. Occasional quartziticmineralization on fractures.
Medium strong to strong light grey finegrained slightly micaceous SANDSTONE.(PENNINE MIDDLE COAL MEASURES
Coordinates
FORMATION)Fractures are randomly orientated, veryclosely and closely spaced, undulatingrough, clean stained orange brown.
1:50
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AH/PSMQ/MBJRL
10/10/2013
25/10/2013
TCRSCRRQD
Type & No
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 13.90m
Records/Samples
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
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Stratum continues to 13.60 m
National Grid
Chainage
BH4Sheet 1 of 2
+139.48 mODE 383650.32N 354068.71
2.50 4.50 SPT hammer ID SM397.55 11.85 SPT hammer ID SM19
4.50m0.00m 150mm13.90m4.50m 120mm
3.00m4.50m
4.30 -4.50 60 mins
SPT S 50 (25 for 30mm/50 for 50mm)
*
*
4.50-4.73 m AZCL
4.73-4.95 mrecovered as softgrey gravelly clay
5.30-5.40 m veryweak, extremelyclosely spaced
incipient polishedsurfaces
7.10-7.45 m AZCL
7.45-7.55 m NI,recovered ascoarse gravel
8.20-8.30 m NI,recovered as
slightly sandycoarse gravel
8.30-8.85 m withextremely closely
and closelyspaced blackcoal laminae
(<3mm)8.60-8.80 m
subverticalfracture
9.10-9.35 msubvertical
fracture9.10-9.50 m
0.00-0.100.10-0.25
0.200.20
0.25-0.500.500.50
0.50-1.201.00
1.50-1.95
2.05
2.50-2.922.50-2.90
0
NI80
220
NR
NI75
130
If /NR/
If /NR/TCR 33, SCR 0, RQD 0
If /NI/
CS 18
CS 19
4.50
24/10/20134.50 2.13
13.60
13.90
(4.05)
(0.30)+125.88
+125.58
SP
____________8.30m - 9.55m : Medium strong thinlylaminated light grey fine grainedslightly micaceous SANDSTONE and greySILTSTONE with occasional thin (<3mm)coal laminations and very thin ironstonebands. (PENNINE MIDLE COAL MEASURESFORMATION) Fractures are inclined15-20deg, very closely and closely spaced,undulating smooth, generally clean,occasionally silt smeared (<1mm).____________9.55m - 13.60m : Weak to medium stronggrey MUDSTONE with occasional very thinstrong brown IRONSTONE interbeds. (PENNINEMIDDLE COAL MEASURES FORMATION)Fractures are 1) inclined 15-20deg, very closelyand closely spaced, planar and undulatingsmooth, often clean, occasional sandygravel (<20mm) infill, occasionally claysmeared 2) randomly orientated andsubvertical, undulating smooth, clean.
Recovered core comprises medium stronglight grey fine grained quartziticSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 13.90 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AH/PSMQ/MBJRL
10/10/2013
25/10/2013
TCRSCRRQD
TCRSCRRQD
If
If
Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 13.90m
Records/Samples
Records/Samples
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CLOUGH HALL TECHNOLOGY SCHOOL
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(Continued from Sheet 1)(Continued from Sheet 1)
National Grid
Chainage
BH4Sheet 2 of 2
+139.48 mODE 383650.32N 354068.71
4.50m0.00m 150mm13.90m4.50m 120mm
3.00m4.50m
SPT S 50 (25 for 30mm/50 for 30mm)
:: 9.10m - tendingto laminated
SILTSTONE10.22-10.25 m
strongIRONSTONE
10.30-10.36 m NI10.50-10.56 m NI
11.18-11.21 mstrong
IRONSTONE11.42-11.45 m
strongIRONSTONE
11.45-11.75 m70deg fracture11.75-11.78 m
strongIRONSTONE
11.85-12.10 mAZCL
12.40-12.60 mrecovered NI
12.60-12.75 mAZCL
12.90-13.05 mrecovered NI
13.45-13.60 m NI,recovered as
very clayeygravel
13.60-13.90 mAZCL
9.90-10.70
10.94-11.15
10.70-11.85
11.85-11.91
11.85-12.60
12.60-13.60
13.32-13.44
13.60-13.90
943014
967449
67160
854621
330
(GLACIOFLUVIAL DEPOSITS)
Stiff grey slightly sandy slightlygravelly silty CLAY tending to extremelyweak SILTSTONE. Gravel is angular fine tomedium siltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
Very weak grey SILTSTONE. Recovered assilty sandy gravel.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 6.20 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
AHMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Dando 3000Service inspection pit hand excavated to 1.20mCable percussion to 6.20m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
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National Grid
Chainage
BH5Sheet 1 of 1
+139.75 mODE 383718.63N 354099.58
2.50 6.15 SPT hammer ID SM39
6.20m0.00m 150mm 4.50m
5.90 -6.15 60 mins
*
3.50-4.00 m Firm
0.200.200.25
0.25-1.200.50
1.00
1.50-1.95
2.002.05
2.50-2.952.50-2.952.50-3.00
3.00
3.50-3.953.50-4.95
4.05
4.50-4.954.50-5.00
5.50-5.805.50-5.805.50-6.00
6.15-6.226.15-6.20
ES 1D 2D 3B 5
ES 4
ES 6
U 7
ES 9D 8
SPT SD 10B 11
ES 12
U 13D 16
D 14
SPT SB 17
SPT SD 18B 19
SPT SD 20
33 blows
N=22 (3,3/5,5,6,6)
47 blows
N=12 (3,3/3,3,3,3)
50 (10,13/21,29)
50 (25 for 30mm/50 for 40mm)
1.50
2.50
3.00
4.50
4.50
4.50
dry
dry
dry
dry
dry
dry
0.25
2.00
4.00
4.40
4.65
5.50
6.20
(1.75)
(2.00)
(0.40)
(0.85)
(0.70)
+139.50
+137.75
+135.75
+135.35
+135.10
+134.25
+133.55 SP
Firm brown slightly snady gravelly CLAY.Gravel is angular to subrounded fine tocoarse sandstone, brick and quartz.(TOPSOIL)
MADE GROUND: stiff orangish brown mottledgrey slightly sandy slightly gravellyCLAY. Gravel is angular fine brick andcoal.
MADE GROUND: stiff, becoming firm, greyblack slightly gravelly CLAY. Gravel issubrounded fine to coarse mudstone,sandstone and coal.
Possible MADE GROUND: firm sandy gravellyCLAY with low cobble content. Gravel isangular fine to coarse coal and sandstone.Cobbles are sandstone.
Firm orangish brown slightly sandyslightly gravelly CLAY. Gravel issubangular fine to medium sandstone andsiltstone.
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MBMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 3.00mRefusal at 3.00m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
National Grid
Chainage
WS1Sheet 1 of 1
+132.09 mODE 383549.68N 354257.99
1.20 3.00 SPT hammer ID 110.49CB
*
0.00-0.070.10-0.15
0.200.20-0.50
0.700.80-1.00
1.101.20-1.651.20-1.651.20-2.50
2.00-2.45
2.502.602.752.90
3.00-3.383.00
B 1B 2
ES 3B 4
5B 6
ES 7SPT S
D 8B 9
SPT S
D 10D 11D 12D 13
SPT SD 14
N=9 (1,2/2,2,2,3)
N=9 (2,3/3,2,2,2)
50 (7,-/13,14,14,9 for 5mm)
dry
dry
dry
0.070.15
0.75
2.50
2.702.803.00
(0.60)
(1.75)
+132.02+131.94
+131.34
+129.59
+129.39+129.29
+129.09
MADE GROUND: macadam.
MADE GROUND: grey sandy GRAVEL with lowcobble content. Gravel is angular fine tocoarse concrete, brick and porcelain.Cobbles are concrete.
MADE GROUND: orangish brown slightlyclayey gravelly fine to medium SAND withhigh cobble content. Gravel is angular torounded fine to coarse igneous, concreteand quartz. Cobbles are igneous.
Loose brown silty very gravelly fine tocoarse SAND with low cobble content andoccasional bands of thin brown and blacksand and very occasional reddish brownbrown sand. Gravel is subangular tosubrounded fine to coarse sandstone.(GLACIOFLUVIAL DEPOSITS)
Reddish brown medium to coarse sandyGRAVEL of subrounded to rounded fine tomedium quartz and angular fine to coarsesandstone.(GLACIOFLUVIAL DEPOSITS)
Extremely weak black MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)
Very stiff grey gravelly CLAY. Gravel isangular fine to coarse siltstone andreddish brown mudstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 3.00 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole LogMBMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Service inspoection pit hand excavated to 1.20mWindowless sampler to 4.00mRefusal to 4.00m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
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National Grid
Chainage
WS2Sheet 1 of 1
+131.82 mODE 383600.14N 354237.98
0.901 - -2.002 - -
1.20 4.00 SPT hammer ID 110.49CB
*
4.00 m Possiblebedrock
0.00-0.050.200.20
0.500.50
1.001.10
1.20-1.651.201.20
1.902.00-2.45
2.00
2.50
3.00-3.453.10
3.50
4.00-4.444.00
B 1ES 2B 3
D 4ES 5
ES 6D 7
SPT SES 8D 9
D 10SPT SD 11
ES 12
SPT CD 13
D 14
SPT SD 15
N=2 (1,0/0,0,1,1)
N=7 (1,1/1,2,2,2)
N=10 (2,3/3,3,2,2)
50 (6,9/11,13,15,11 for 60mm)
0.05
0.25
0.75
1.80
2.00
3.40
4.00
(0.50)
(1.05)
(1.40)
(0.60)
+131.77
+131.57
+131.07
+130.02
+129.82
+128.42
+127.82
1
2
MADE GROUND: macadam.
MADE GROUND: black sandy GRAVEL ofangular fine to coarse brick, sandstone, clinkerand wood.
MADE GROUND: soft sandy gravelly CLAY withlow cobble content. Gravel is angularfine to coarse brick, sandstone and coal.Cobbles are brick and sandstone.
MADE GROUND: very soft dark grey slightlygravelly SILT with low cobble content.Gravel is angular fine coal. Cobbles aresandstone.
Firm reddish brown slightly sandy slightlygravelly CLAY. Gravel is angular finesandstone.(GLACIOFLUVIAL DEPOSITS)
Loose to medium dense grey and reddishbrown SAND and GRAVEL with occasionalreddish brown clay pockets. Sand is fineto medium. Gravel is angular fine tomedium sandstone.(GLACIOFLUVIAL DEPOSITS)
Firm grey slightly gravelly CLAY. Gravelis subangular fine mudstone and sandstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 4.00 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MBMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
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National Grid
Chainage
WS3Sheet 1 of 1
+132.76 mODE 383512.32N 354244.82
0.00 5.00 SPT hammer ID 110.49CB
*
4.00-5.00 m Norecovery
0.200.20-0.80
0.80
1.20-1.651.20
1.80
2.00-2.452.00
2.00-2.70
3.00-3.453.003.00
3.50-4.00
4.00-4.454.00
5.00-5.455.00
ES 1B 2
ES 3
SPT SD 4
ES 5
SPT SD 6B 7
SPT SES 8D 9
B 10
SPT SD 11
SPT SD 12
N=8 (1,2/2,2,2,2)
N=22 (3,4/5,5,6,6)
N=13 (2,3/3,3,3,4)
N=4 (1,1/1,1,1,1)
N=15 (2,3/3,4,4,4)
0.40
1.45
2.20
2.70
4.00
5.00
(0.40)
(1.05)
(0.75)
(0.50)
(1.30)
(1.00)
+132.36
+131.31
+130.56
+130.06
+128.76
+127.76
MADE GROUND: stiff brown slightly sandyslightly gravelly CLAY. Gravel is angularfine to coarse brick, concrete, coal andsandstone. Frequent rootlets. (Topsoil)
MADE GROUND: firm brown slightly sandyslightly gravelly CLAY. Gravel is angularfine to coarse brick, concrete, coal andsandstone.
MADE GROUND: dark grey slightly sandysilty GRAVEL with occasional stiff darkgrey silty clay pockets. Gravel is angularfine to coarse mudstone and siltstone.
MADE GROUND: medium dense light grey siltyvery sandy GRAVEL. Gravel is angular tosubrounded fine to coarse sandstone,igneous and quartz.
Medium dense reddish brown, becomingbrown, slightly gravelly silty fine tomedium SAND. Gravel is subrounded finesandstone.(Possible GLACIOFLUVIAL DEPOSITS)
No recoveryDescription of disturbed samples: softbrown CLAY.(Possible GLACIOFLUVIAL DEPOSITS)
EXPLORATORY HOLE ENDS AT 5.00 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MBMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
National Grid
Chainage
WS4Sheet 1 of 1
+137.24 mODE 383534.16N 354183.40
1.20 5.00 SPT hammer ID 110.49CB
*
3.70-3.80 mStained black
0.200.30
0.40-0.600.50
0.70-1.000.80
1.20-1.651.201.40
1.60-2.00
2.00-2.452.00
2.60
2.80
3.00-3.453.00
3.70-3.80
4.00-4.454.00
4.50-5.00
5.00-5.455.00
ES 1D 2B 4
ES 3B 5
ES 6
SPT SD 7D 8
ES 9
SPT SD 10
D 11
ES 12
SPT SD 13
ES 14
SPT SD 15
D 16
SPT SD 17
N=1 (1,0/0,0,1,0)
N=2 (1,0/1,0,1,0)
N=11 (4,6/4,3,2,2)
N=4 (1,0/1,1,1,1)
N=8 (2,2/2,2,2,2)
0.60
1.00
1.55
2.50
3.40
3.70
5.00
(0.60)
(0.40)
(0.55)
(0.95)
(0.90)
(0.30)
(1.30)
+136.64
+136.24
+135.69
+134.74
+133.84
+133.54
+132.24
MADE GROUND: dark brown clayey gravellyfine to coarse SAND with low cobblecontent. Gravel is angular fine to coarsebrick, sandstone, steel, concrete, glassand polystyrene. Cobbles are concrete.Frequent rootlets.
MADE GROUND: orangish brown silty gravellyfine to medium SAND with frequent gravelsize reddish brown clay pockets. Gravel isangular fine clinker.
MADE GROUND: soft to firm orangish brownmottled black slightly sandy slightlygravelly CLAY. Gravel is subangular fineto medium mudstone.
MADE GROUND: soft brown slightly sandygravelly CLAY. Gravel is angular fine tocoarse mudstone, sandstone and siltstone.
MADE GROUND: firm reddish brown slightlygravelly sandy CLAY. Gravel is angularfine to medium sandstone and quartz.
MADE GROUND: black slightly sandy GRAVELof angular fine to medium clinker, quartzand glass.
Very loose to loose reddish brown,occasionally stained black, slightlygravelly fine SAND. Gravel is subroundedfine to mediium sandstone and quartz.(GLACIOFLUVIAL DEPOSITS)
EXPLORATORY HOLE ENDS AT 5.00 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MBMQJRL
15/10/2013
15/10/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 1.80mRefusal at 1.80m
Records
Records
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CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
National Grid
Chainage
WS5Sheet 1 of 1
+139.51 mODE 383684.17N 354076.17
1.20 1.80 SPT hammer ID 110.49CB
*
0.00-0.070.100.20
0.600.60-1.00
1.20-1.651.20
1.20-1.80
1.80-2.071.80
B 1ES 2ES 3
ES 4B 5
SPT SD 6B 7
SPT SD 8
N=46 (7,9/11,12,14,9)
50 (12,13 for 45mm/22,24,4 for 0mm)
0.070.150.25
1.00
1.80
(0.75)
(0.80)
+139.44+139.36+139.26
+138.51
+137.71
MADE GROUND:macadam.
MADE GROUND: black SAND and GRAVEL.Sand is coarse. Gravel is angular fine tocoarse brick, sandstone and clinker.
MADE GROUND: dark brown sandy gravellyCLAY. Gravel is angular fine to coarsesandstone and brick.
Firm light grey slightly sandy gravellyCLAY. Gravel is angular fine to coarsesiltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
Grey slightly gravelly sandy SILT tendingto extremely weak grey SILTSTONE. Gravelis subangular fine to medium siltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)
EXPLORATORY HOLE ENDS AT 1.80 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MBMQJRL
14/10/2013
14/10/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m
Records
Records
426.4823/01/2014 15:59:53(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
National Grid
Chainage
WS6Sheet 1 of 1
+132.40 mODE 383683.55N 354176.57
1.20 5.00 SPT hammer ID 110.49CB
*
0.00-0.070.20
0.20-0.30
0.500.60
1.001.10
1.20-1.651.20
1.20-2.00
2.00-2.452.00
2.00-3.00
3.00-3.453.00
3.00-3.803.00
3.80
4.00-4.45
4.40
5.00-5.455.00
B 1ES 2B 3
D 4ES 5
ES 6D 7
SPT SD 8B 9
SPT SD 10B 11
SPT SD 12B 13D 14
B 15
SPT S
D 16
SPT SD 17
N=9 (2,2/2,2,2,3)
N=17 (2,3/4,5,4,4)
N=20 (2,3/4,5,5,6)
N=24 (5,5/6,6,6,6)
N=24 (5,6/6,6,6,6)
0.07
0.35
0.90
1.20
3.80
4.40
5.00
(0.28)
(0.55)
(0.30)
(2.60)
(0.60)
(0.60)
+132.33
+132.05
+131.50
+131.20
+128.60
+128.00
+127.40
MADE GROUND: macadam.
MADE GROUND: black brown slightly siltyvery sandy GRAVEL. Sand is fine to coarse.Gravel is angular to subangular fine tocoarse sandstone, igneous, macadam andsteel.
Soft orangish brown sandy CLAY with lowsandstone cobble content. Rare rootlets.(GLACIOFLUVIAL DEPOSITS)
Soft orangish brown slightly gravellysandy CLAY with low cobble content. Gravelis angular to subrounded fine to mediumsandstone. Cobbles are sandstone.(GLACIOFLUVIAL DEPOSITS)
Loose to medium dense orangish brown,occasionally stained black, slightlygravelly slightly silty fine to mediumSAND with occasional thin reddish brownsand bands. Gravel is rounded finepossible quartz.(GLACIOFLUVIAL DEPOSITS)
Medium dense orangish brown very sandyGRAVEL. Sand is fine to coarse. Gravel issubrounded to rounded fine to mediumquartz, mudstone and subangular coarsesandstone.(GLACIOFLUVIAL DEPOSITS)
Orangish brown slightly gravelly fine tomedium SAND. Gravel is angular tosubangular medium to coarse sandstone.(GLACIOFLUVIAL DEPOSITS)
EXPLORATORY HOLE ENDS AT 5.00 m
1:50
Type & No.
Instruments
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
DateRecords
Samples and Tests
Ground Level
Project
Project No.Carried out for
Date
LengthWidth
No. Post Strike Behaviour(m)
StrataDepth
RecordsDescription Depth, Legend(Thickness)
Groundwater Entries
Dimensions and Orientation
Level
Struck
Notes: For explanation of symbols andabbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
From to (m)Stability
Shoring
Weather
Scale
Start
End
Depth Related Remarks *
Logged
Depth
Trial Pit Log
None observed (see Key Sheet)
MQ
JRL15/10/2013
15/10/2013
Hand excavated to 1.20m
426.4823/01/2014 15:49:40(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
0.50 m0.50 m - National Grid
Chainage
Trial Pit
Stable
None
TP1Sheet 1 of 1
+137.67 mODE 383571.46N 354159.53
0.00-0.07
0.25
0.50
0.70
1.001.00-1.20
B 1
ES 2
D 3
ES 4
ES 5B 6
0.05
0.20
0.75
1.20
(0.55)
(0.45)
+137.62
+137.47
+136.92
+136.47
1 MADE GROUND: macadam.
2 MADE GROUND: grey sandy GRAVEL of angular fine tocoarse limestone.
3 MADE GROUND: dark grey slightly sandy gravelly CLAYwith medium cobble content. Gravel is angular tosubrounded fine to coarse sandstone, concrete andquartz. Cobbles are igneous.
4 Brown gravelly clayey fine to medium SAND with lowcobble content. Gravel is angular fine to coarsesandstone. Cobbles are subangular sandstone.(Possible GLACIOFLUVIAL DEPOSITS)
EXPLORATORY HOLE ENDS AT 1.20 m
1:25
Type & No.
A
B
C
D
Type & No.
Instruments
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
DateRecords
Samples and Tests
Ground Level
Project
Project No.Carried out for
Date
LengthWidth
No. Post Strike Behaviour(m)
StrataDepth
RecordsDescription Depth, Legend(Thickness)
Groundwater Entries
Dimensions and Orientation
Level
Struck
Notes: For explanation of symbols andabbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
From to (m)Stability
Shoring
Weather
Scale
Start
End
Depth Related Remarks *
Logged
Depth
Trial Pit Log
None observed (see Key Sheet)
MQ
JRL15/10/2013
15/10/2013
Hand excavated to 1.20m
426.4823/01/2014 15:50:37(c) ESG www.esg.co.uk
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
0.50 m0.50 m - National Grid
Chainage
Trial Pit
Stable
None
TP2Sheet 1 of 1
+137.44 mODE 383603.81N 354143.39
0.00-0.04
0.20
0.30
0.55
0.85-1.00
1.20
B 1
ES 2
ES 3
ES 4
B 5
ES 6
0.04
0.15
0.25
0.450.50
0.95
1.20
(0.45)
+137.40
+137.29
+137.19
+136.99+136.94
+136.49
+136.24
1 MADE GROUND: macadam.
2 MADE GROUND: black very sandy GRAVEL. Sand is mediumto coarse. Gravel is angular fine to medium slag,clinker and concrete.
3 MADE GROUND: light grey gravelly medium to coarseSAND. Gravel is angular fine to medium sandstone.
4 MADE GROUND: firm grey slightly sandy slightlygravelly CLAY. Gravel is angular fine to coarseconcrete.
5 MADE GROUND: extremely weak concrete
6 MADE GROUND: dark grey silty gravelly fine to coarseSAND with low cobble content. Gravel is angular fine tocoarse mudstone, sandstone and quartz. Cobbles aresubangular quartz.
7 MADE GROUND: orangish brown fine SAND with abundantcoarse gravel size reddish brown clay pockets.
EXPLORATORY HOLE ENDS AT 1.20 m
1:25
Type & No.
A
B
C
D
January 2014 Report No D3155-13 Issue 3.0 Enclosure B
ENCLOSURE B
INSTRUMENTATION AND MONITORING
Installation Details B1
Groundwater Monitoring B2 and B3
Gas Monitoring
Hol
e N
o
Inst
rum
ent I
D
Inst
alla
tion
Typ
e
Dat
e of
Inst
alla
tion
Ref
eren
ce d
epth
(m
BG
L)
Pie
zom
eter
D
iam
eter
(m
m)
Top
of r
espo
nse
zone
(m
BG
L)
Bas
e of
res
pons
e zo
ne (
mB
GL)
Tub
ing
Com
plet
ion
Det
ails
Hea
dwor
ks Remarks
BH1 SP 17 Oct 2013 0.00 50 4.30 14.40 Gas tap Stop cock cover
BH2 SP 23 Oct 2013 0.00 50 3.50 26.00 Gas tap Stop cock cover
BH3 SP 10 Oct 2013 0.00 50 1.40 2.80 Gas tap Stop cock cover
BH4 SP 25 Oct 2013 0.00 50 0.75 13.90 Gas tap Stop cock cover
BH5 SP 25 Oct 2013 0.00 50 4.50 6.20 Gas tap Stop cock cover
Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Electronic Piezometer Prepared: 03/12/2013 11:37
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13 Education Funding Agency
Project
Project No.Carried out for
B1
Groundwater Installation Details
Sheet 1 of 1
DateTime
(hhmmss)Comments
BH1 SP 14.3 0.00 7 Nov 2013 2.51
BH1 SP 14.3 0.00 12 Nov 2013 2.23
BH1 SP 14.3 0.00 14 Nov 2013 2.26
BH1 SP 14.3 0.00 26 Nov 2013 2.27
BH1 SP 14.3 0.00 29 Nov 2013 2.52
BH1 SP 14.3 0.00 3 Dec 2013 2.53
BH1 SP 14.3 0.00 23 Dec 2013 2.25
BH1 SP 14.3 0.00 30 Dec 2013 2.26
BH1 SP 14.3 0.00 3 Jan 2014 2.29
BH1 SP 14.3 0.00 10 Jan 2014 2.63
BH1 SP 14.3 0.00 13 Jan 2014 2.59
BH1 SP 14.3 0.00 17 Jan 2014 2.30
BH2 SP 26 0.00 7 Nov 2013 5.32
BH2 SP 26 0.00 12 Nov 2013 5.26
BH2 SP 26 0.00 14 Nov 2013 5.14
BH2 SP 26 0.00 26 Nov 2013 4.92
BH2 SP 26 0.00 29 Nov 2013 4.92
BH2 SP 26 0.00 3 Dec 2013 5.01
BH2 SP 26 0.00 23 Dec 2013 4.77
BH2 SP 26 0.00 30 Dec 2013 4.51
BH2 SP 26 0.00 3 Jan 2014 4.27
BH2 SP 26 0.00 10 Jan 2014 4.02
BH2 SP 26 0.00 13 Jan 2014 3.89
BH2 SP 26 0.00 17 Jan 2014 3.69
BH3 SP 2.8 0.00 7 Nov 2013 2.81
BH3 SP 2.8 0.00 12 Nov 2013 Dry
BH3 SP 2.8 0.00 14 Nov 2013 Dry
BH3 SP 2.8 0.00 26 Nov 2013 2.80
BH3 SP 2.8 0.00 29 Nov 2013 2.89
BH3 SP 2.8 0.00 3 Dec 2013 2.80
BH3 SP 2.8 0.00 23 Dec 2013 Dry
BH3 SP 2.8 0.00 30 Dec 2013 Dry
BH3 SP 2.8 0.00 3 Jan 2014 Dry
BH3 SP 2.8 0.00 10 Jan 2014 Dry
BH3 SP 2.8 0.00 13 Jan 2014 Dry
BH3 SP 2.8 0.00 17 Jan 2014 Dry
BH4 SP 13.9 0.00 7 Nov 2013 5.61
BH4 SP 13.9 0.00 12 Nov 2013 6.21
BH4 SP 13.9 0.00 14 Nov 2013 4.63
BH4 SP 13.9 0.00 26 Nov 2013 6.73
BH4 SP 13.9 0.00 29 Nov 2013 5.87
Hole ID
Inst
rum
ent I
D
Inst
rum
ent
Typ
e
Bas
e of
In
stru
men
t(m
BG
L)
Ref
eren
ce
Dep
th(m
BG
L)
Reading
Water Level (mBGL)
* calculated
Head(m above Tip)
* calculated
Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13 Education Funding Agency
Project
Project No.Carried out for
B2
Groundwater Monitoring
DateTime
(hhmmss)Comments
BH4 SP 13.9 0.00 3 Dec 2013 5.86
BH4 SP 13.9 0.00 23 Dec 2013 6.01
BH4 SP 13.9 0.00 30 Dec 2013 6.06
BH4 SP 13.9 0.00 3 Jan 2014 5.77
BH4 SP 13.9 0.00 10 Jan 2014 6.06
BH4 SP 13.9 0.00 13 Jan 2014 5.94
BH4 SP 13.9 0.00 17 Jan 2014 5.31
BH5 SP 6 0.00 7 Nov 2013 5.70
BH5 SP 6 0.00 12 Nov 2013 3.69
BH5 SP 6 0.00 14 Nov 2013 5.48
BH5 SP 6 0.00 26 Nov 2013 5.25
BH5 SP 6 0.00 29 Nov 2013 5.11
BH5 SP 6 0.00 3 Dec 2013 5.29
BH5 SP 6 0.00 23 Dec 2013 5.36
BH5 SP 6 0.00 10 Jan 2014 4.39
BH5 SP 6 0.00 13 Jan 2014 4.38
BH5 SP 6 0.00 17 Jan 2014 4.18
Hole ID
Inst
rum
ent I
D
Inst
rum
ent
Typ
e
Bas
e of
In
stru
men
t(m
BG
L)
Ref
eren
ce
Dep
th(m
BG
L)
Reading
Water Level (mBGL)
* calculated
Head(m above Tip)
* calculated
Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well
CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13 Education Funding Agency
Project
Project No.Carried out for
B3
Groundwater Monitoring
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH32.81 0.0
0.0 0.00.0BH3 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
1.1
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
20.0
0.8
-0.30 0.0
1.2
20.0 1.2 0.0
0.0
0.0
1.9
1.1
Gas tap open
21.1 0.0 0.00.0
DryLight
SlightNone
Gas tap open
20.1
21.4 0.0 0.0
20.2 1.2 0.0
2.1
2.1
21.2 0.5 1.9941.0
21.2 0.0 2.0
21.2 0.4 1.9
899.0
918.0
21.2 0.0 0.0
21.2 0.0 1.9
781.0
823.0
0.0 0.0
0.0
0.0
0.0 0.0
992 10
BH3 0.00 00:01:30
0.00 00:00:30
BH3 0.00 00:01:00 -0.100.0
0.0
0.0
-0.300.0
-0.30 0.00.0
BH3 0.00 00:02:00 -0.300.0
BH2 0.00
0.00
5.32
2.51 0.00.00.00 00:00:00
BH1 0.00
BH1 0.00 00:00:30
00:01:30
BH1
993
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH4 0.00 5.61
0.00 00:01:30
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
BH1
BH5
BH5 0.00 00:02:00 0.0
00:00:00
BH1 0.00 00:02:00
BH5
BH5 0.00 00:01:00
BH5 0.00 00:00:30
0.00 0.205.70
0.0
0.0
0.000.0
0.0
0.0
0.0 18.4
0.1
0.1
21.0
0.0
21.0
20.4
Reading Depth
(mBGL)
0.20.3
0.1
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 5429 + Dip
992
10
11
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00
CO(ppm)
1.00
07/11/2013
SW
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
12/11/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
3.7
3.3
2.6
2.4
0.7
1.5
0.6
1.6
2.2
17.3
16.4
Reading Depth
(mBGL)
5.05.2
4.3
0.1
0.1
0.2 14.6
3.3
2.6
2.0
18.9
0.2
0.1
0.10.0
0.00
0.00
0.1
0.0
0.000.0
0.00 0.00
BH5 0.00 00:02:00
BH5 0.00 00:01:30
00:01:00
00:00:30
BH5
BH4
BH5
BH5 0.00 00:03:00
0.0
0.0
0.0
0.000.0
0.00 00:02:30
BH5 0.00
BH5 0.00998 00:00:00 3.69 0.0
2.23
0.00
BH1 0.00
0.1
6.21
00:03:00
BH2 0.00
BH2 0.00
00:02:30
BH2 0.00 00:02:00 0.000.0
0.00 0.20.0
0.000.0
0.3
0.2
0.000.0
00:01:30
0.00 00:00:30
BH2 0.00 00:01:00
998
BH2 0.00 0.8 0.0
2.3
1.5
1.4 0.0
0.020.3 0.4 0.0
18.3 2.4 0.0
19.4 1.8 0.0
0.0
0.0
20.0 1.4 0.0
20.6 0.9 0.0
0.0
0.0
78.5
78.4
21.3
Flooded; unable to
79.0
gas monitor
Flooded; unable to
monitor
79.2
WetLight
SlightNone
82.981.5
79.3
19.5 0.6 0.0
20.0 0.5 0.0
1.4
1.1
0.0
0.0
0.0
78.3
78.2
0.0
78.3
78.3
81.0
80.1
79.6
21.1 0.5 0.0
0.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.2
0.0
0.00 1.4
0.4
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH25.26 0.0
1.7 0.02.7BH2 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
12/11/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5429 + Dip
0.8
0.0
21.6
21.6
Reading Depth
(mBGL)
1.30.3
0.5
0.0
0.0
0.0 21.4
0.6
0.2
0.7
21.6
0.000:03:00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
998
BH3 0.00 0.0 0.0
0.0
0.0
0.0 0.0
0.021.6 0.0 0.0 78.3
Light
SlightNone
78.578.3
78.3
21.6 0.0 0.0
21.6 0.0 0.0
0.0
0.0
78.3
78.3
78.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH3Dry 0.0
0.0 0.00.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
14/11/2013
GM
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
995
995
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
1.7
17.2
14.1
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 16.6
0.0
0.0
0.0
18.4
0.0
0.0
0.0
0.0
0.00
0.00
0.0
0.00
00:01:00 0.00
BH5 0.00 00:02:30
00:02:00
BH5 0.00 00:00:00
00:00:30
00:01:30
BH5 0.00
BH5
BH4
BH3
0.0
BH3 0.00 00:00:30 0.0
BH3 0.00
BH3
0.0
-0.40Dry 0.00.0
-0.10
0.00 0.0
0.00 00:00:00
0.0
BH5 0.00
BH5 0.00 00:01:00 0.0
0.0
0.0
5.48 0.00.0 0.10
0.00 00:05:00
0.00 00:04:00
BH4 0.00 00:04:30
BH4
0.0
0.0
0.0
00:03:00
00:03:30BH4 0.00
BH4 0.00
BH4 0.00
00:02:30
BH4 0.00 00:02:00
0.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH4 0.00 00:01:00
995
BH4 0.00 1.2 0.0
0.0
0.0
1.6 0.0
20.3 0.5 0.0
0.0
0.0
19.7 0.7 0.0
20.4 0.4 0.0
20.5 0.4 0.0
0.0
0.0
20.6 0.4 0.00.0
20.9 0.4 0.0
21.0 0.3 0.0
0.0
0.0
21.1 0.2 0.0
21.2 0.1 0.0
0.0
0.0
21.3 0.0 0.0
21.3 0.0 0.0
0.0
0.0
-0.100.0
21.3
WetCalmNorth eastSlightSlight
18.7 1.1 0.0
19.2 0.9 0.0
0.0
0.0
0.0
0.00.0
0.0 21.4
0.0
0.0
0.00 00:01:30 -0.300.0BH3
0.0
BH3 0.00 00:02:30 0.00
00:02:00
0.0 0.00.0
21.4 0.0
-0.20
0.0 21.4
0.0
0.0 0.0 0.0
0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.5
0.0
0.00 0.0
0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH44.63 0.0
2.7 0.00.0BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH25.14 0.0
0.7 0.01.1BH2 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.0
35.2
0.00 0.0
0.0
0.0 0.026.8
28.8
20.9 0.0 0.0
21.0 0.0
0.0 21.0
0.0
0.0
0.0
0.0
0.0 0.031.2BH1
0.0
BH1 0.00 00:06:00 0.0 2.0
00:05:30
0.00 00:05:00 -4.0
0.0
0.0
21.0
35.4
0.0
48.5
42.1
20.0 0.4 0.0
20.2 0.3 0.0
0.0
0.0
WetModerateNorth eastSlightSlight
21.0
BH1 0.00 00:06:30 0.0 21.1 0.0 0.026.40.0
20.7 0.0 0.0
20.8 0.0 0.0
66.7
55.2
20.5 0.0 0.0
20.6 0.0 0.0
104.0
81.0
20.5 0.0 0.0
20.1 0.0 0.0
126.0
142.0
20.9 0.0 0.00.0
20.7 0.1 0.0
20.8 0.0 0.0
0.0
0.0
20.6 0.2 0.0
0.0
0.0
20.4 0.2 0.0
0.4 0.0
0.0
0.0
0.4 0.0
995
BH2 0.00 00:01:30
0.00 00:00:30
BH2 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.0
BH2 0.00 00:02:00
00:02:30
BH2 0.00
BH2 0.00
BH2 0.00 00:03:00
00:03:30
0.0
0.0
0.0
0.00 00:04:00
BH2 0.00 00:04:30
BH2 0.00 00:05:00
0.0 0.00
00:01:00 0.0
0.0
0.0
2.26 0.0
BH1 0.00
BH1 0.00
0.00 -4.0
0.00 00:03:30
BH1
0.0
0.0
0.0
-4.0
-4.0
BH2
BH1
BH1 0.00 00:04:00 -3.0
BH1 0.00
00:02:00
BH1 0.00 00:00:00
00:00:30
00:01:30
BH1 0.00
BH1
BH1 0.00 00:03:00
BH1 0.00 00:02:30
0.00
00:04:30
0.0
-3.0
-4.0
0.00
0.00-4.0
0.0
0.0
0.0
0.0
0.0
0.0 19.5
0.0
0.0
0.0
19.9
0.6
19.7
18.4
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
996
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00
CO(ppm)
1.00
14/11/2013
GM
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH12.27 0.0BH1 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.3
32.4
0.00
0.0
77.9
21.1 0.1 0.0
21.3 0.00.5
78.6
78.3
0.0
0.0
78.2
78.1
78.127.9
0.0
42.4
39.2
78.9
22.0 0.0 0.0
21.0 0.0 0.0
0.0
49.8
DryCalm
CloudyNone
78.9
78.8
78.6
78.6
78.6
79.9
21.3
22.0 0.0 0.0
20.8 0.2 0.0
0.0
49.8
21.2 0.0 0.027.9
21.3 0.0 0.0
21.2 0.0 0.0
32.4
27.9
21.1 0.0 0.0
42.4
39.2
21.0 0.0 0.0
1011
BH1 0.00 00:01:30
0.00 00:00:30
BH1 0.00 00:01:00 0.000.0
0.000.0
0.000.0
BH1 0.00 00:02:00
00:02:30
BH1 0.00
BH1 0.00
BH1 0.00 00:03:00
00:03:30
0.0
0.0
0.0
0.00 00:04:00
BH1 0.00 00:04:30
BH1
0.00
0.00 00:05:00
0.0
0.0
4.92 0.0
0.0
BH2 0.00
BH2 0.00 00:01:00 0.0
0.00
0.00 00:03:30
BH2
0.5
0.5
0.5
BH1
BH2
BH2 0.00 00:04:00
00:02:00
BH2 0.00 00:00:00
00:00:30
00:01:30
BH2 0.00
BH2
BH2 0.00 00:03:00
BH2 0.00 00:02:30
0.00
00:04:30
0.4
0.0
0.0
0.00
0.00
0.00
0.0
0.0 0.0
0.0
Reading Depth
(mBGL)
0.0
0.0
0.0
0.0
9.0
9.0
10.0
11.7
1011
0.0
0.0
8.3
Equipment Used LMSxi 1904 + Dip
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
26/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
26/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
1009
0.0
0.3
0.2
0.0
0.0
0.0
0.0
0.0
0.0
0.2
0.0
0.0
Reading Depth
(mBGL)
0.1
0.0 0.2
3.4
0.0
0.0
0.0
0.00
0.0
0.00
00:05:30
BH4 0.00 00:04:00
BH4 0.00 00:03:30
00:03:00
BH4 0.00 00:01:00
00:01:30
00:02:30
BH4 0.00
BH4
BH3
BH4
BH4 0.00 00:05:00
BH4
0.0
0.0
0.0
0.00
0.00 00:04:30
0.0
BH4 0.00
BH4 0.00 00:02:00
6.73
0.0 0.00
0.00
0.00 00:00:00 0.000.0
0.0
0.00 00:04:00
BH4 0.00 00:00:30
BH4
0.0
0.0
0.0
00:03:00
00:03:30BH3 0.00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00
0.000.0
0.000.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
1010
BH3 0.00
21.3 0.0 0.0
0.0
0.0
21.2 0.0 0.0
21.3 0.0 0.00.0
22.0 0.0 0.0
1.1 4.3 0.0
0.0
0.0
1.8 4.3 0.0
3.7 3.8 0.0
0.0
1.0
94.3
93.0
7.8
77.9
78.7
78.6
78.6
DryCalm
CloudyNone
78.8
22.0 0.0 0.0
21.2 0.0 0.0
0.0
0.0
1.3
0.0
1.2
1.1
92.4
91.5
0.0
0.0
90.2
88.8
86.3
0.00 00:06:00BH4 2.7 0.01.3 86.3
10.9 2.7
0.0 10.9
0.0
77.9
4.6 3.7 0.0
3.2
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
6.1
1.3
0.00
3.4
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH32.80 0.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 3Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH55.25 0.0BH5 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00
77.922.0 0.0 0.0
15.4 3.1 0.0
0.0
0.0
DryCalm
CloudyNone
80.2
79.6
79.7
79.619.4 0.9 0.0
19.4 0.9 0.0
0.0
0.0
18.8 1.3 0.0
19.1 1.1 0.0
0.0
0.0
18.1 1.9 0.0
0.0
0.0
17.3 2.2 0.0
1009
BH5 0.00 00:01:30
0.00 00:00:30
BH5 0.00 00:01:00 0.000.0
0.000.0
0.000.0
BH5 0.00 00:02:00
00:02:30
BH5 0.00
BH5 0.00
BH5 0.00 00:03:00
00:03:30
0.0
<<<<
<<<<
0.00 00:04:00
BH5 0.00 00:04:30
BH5 0.00 00:05:00
0.0
0.0
0.0
BH5
<<<<
0.0 0.0
>>>>
Reading Depth
(mBGL)
0.0
>>>>
>>>>
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
26/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
29/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxI 1904 + Dip
994
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Reading Depth
(mBGL)
0.0
0.0 0.0
0.0
0.0
0.0
0.00
0.00
0.0
0.00
00:05:00
BH2 0.00 00:03:30
BH2 0.00 00:03:00
00:02:30
BH2 0.00 00:00:30
00:01:00
00:02:00
BH2 0.00
BH2
BH1
BH2
BH2 0.00 00:04:30
BH2
0.0
0.0
0.0
0.00
0.00 00:04:00
0.0
BH2 0.00
BH2 0.00 00:01:30 0.0
0.0
4.92
0.0 0.00
0.000.0
0.00 00:04:00
BH2 0.00
BH1 0.00 00:04:30
00:00:00
0.0
0.0
0.0
00:03:00
00:03:30BH1 0.00
BH1 0.00
BH1 0.00
00:02:30
BH1 0.00 00:02:00
-1.10-2.0
-1.10-2.0
-1.00-2.0
00:01:30
0.00 00:00:30
BH1 0.00 00:01:00
996
BH1 0.00
21.6 0.0 0.0
26.2
11.3
21.5 0.0 0.0
21.6 0.0 0.0
21.6 0.0 0.0
9.7
9.7
21.9 0.0 0.00.0
19.8 0.7 0.0
20.4 0.5 0.0
0.0
0.0
78.0
79.4
21.3
78.5
78.3
78.3
78.3
DryCalm
CloudyNone
79.0
21.9 0.0 0.0
20.9 0.0 0.0
0.0
49.6
0.0
0.0
0.0
0.0
79.0
78.8
0.0
0.0
78.7
78.6
78.621.3 0.00.0
78.0
20.9 0.2 0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.1
0.0
-1.10
0.1
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH12.52 -2.0BH1 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
29/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
994
0.0
3.0
2.8
1.5
1.0
1.1
1.0
0.0
0.0
0.0
Reading Depth
(mBGL)
0.0
0.0 0.0
0.0
0.0
0.3
0.4
0.00
0.2
0.00
BH4 0.00 00:04:00
BH4 0.00 00:03:30
00:03:00
BH4 0.00 00:01:00
00:01:30
00:02:30
BH4 0.00
BH4
BH3
BH4
BH4 0.00 00:05:00
0.1
0.1
0.10.00 00:04:30
0.0
BH4 0.00
BH4 0.00 00:02:00
5.87
0.0 0.00
0.00
0.00 00:00:00 0.000.0
0.0
0.00 00:04:00
BH4 0.00 00:00:30
BH4
0.0
0.0
0.0
00:03:00
00:03:30BH3 0.00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00
0.000.0
0.000.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
994
BH3 0.00
20.6 0.2 0.0
0.0
0.0
20.5 0.2 0.0
20.6 0.2 0.00.0
21.9 0.0 0.0
0.6 6.9 0.0
0.0
0.0
2.0 5.3 0.0
5.5 5.0 0.0
0.0
0.0
92.1
90.3
7.6
78.0
79.2
79.1
79.1
DryCalm
CloudyNone
79.2
21.9 0.0 0.0
20.5 0.2 0.0
0.0
0.0
0.0
0.0
0.0
88.9
87.7
0.0
87.7
87.7
78.0
8.8 4.1 0.0
4.6
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
7.6
0.0
0.00
4.6
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH32.89 0.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 3Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
29/11/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
0.0
0.0
0.0
0.0
0.0
Reading Depth
(mBGL)
0.0
0.0 0.0
0.0
BH5
0.0
0.00.00 00:05:00
0.00 00:04:00
BH5 0.00 00:04:30
BH5
0.0
0.0
0.0
00:03:00
00:03:30BH5 0.00
BH5 0.00
BH5 0.00
00:02:30
BH5 0.00 00:02:00
0.000.0
0.000.0
0.000.0
00:01:30
0.00 00:00:30
BH5 0.00 00:01:00
994
BH5 0.00
14.2 4.6 0.0
0.0
0.0
13.4 5.1 0.0
15.2 4.0 0.0
16.3 3.3 0.0
0.0
0.0
16.3 3.3 0.00.0
81.6
81.1
80.7
80.4
80.4
DryCalm
CloudyNone
82.2
21.9 0.0 0.0
11.9 5.7 0.0
0.0
0.0
78.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH55.11 0.0BH5 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
03/12/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
21.4
21.4
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 21.9
0.0
0.0
0.0
21.6
0.0
0.0
0.00.0
0.00
0.00
0.0
0.0
0.000.0
0.00 0.00
BH3 0.00 00:02:00
BH3 0.00 00:01:30
00:01:00
BH2 0.00 00:02:30
00:00:30
BH3
BH2
BH3
0.0
0.00.00 00:02:30
BH3 0.00
BH3 0.00998 00:00:00 2.80 0.0
0.0
0.0
0.0
0.0
0.000.0
0.00 00:01:30 0.000.0
0.00 00:00:30
BH2 0.00
BH2 0.00 00:01:00
00:02:00
BH2
0.0
5.01 0.00.0
0.0
0.00
0.00
00:00:00BH2 0.00
BH1 0.00
998
00:02:30
BH1 0.00 00:02:00
-1.50 0.0-3.0
-1.50-3.0
0.0
0.0
-1.70-3.0
00:01:30
0.00 00:00:30
BH1 0.00 00:01:00
999
BH1 0.00 0.0 0.0
16.0
11.1
0.0 0.0
21.9 0.0 0.00.0
19.5 0.9 0.0
20.1 0.6 0.0
0.0
0.0
20.6 0.4 0.0
21.1 0.2 0.0
0.0
0.0
21.1 0.2 0.00.0
0.0
21.9 0.0 0.0
20.9 0.1 0.0
0.0
0.0
21.1 0.0 0.0
21.2 0.0 0.0
0.0
0.0
78.9
78.8
78.0
78.0
79.5
78.6
78.6
79.2
78.8
DryCalm
CloudyNone
78.078.5
78.5
21.4 0.0 0.0
21.4 0.0 0.0
15.1
13.6
0.0
0.0
0.0
78.7
78.6
78.6
78.5
78.3
78.5
21.3 0.0 0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.3
-10.00 0.0
0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH12.53 -30.0
0.0 0.018.3BH1 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH45.86 0.0
7.1 0.00.0BH4 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.6
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
20.2
0.0
0.00 0.0
0.6
91.3
90.3
88.8
20.1 0.7 0.0
79.1
79.1
0.0
79.1
79.1
0.0
0.0
0.0
87.2
5.7 5.1 0.0
8.1 4.5 0.0
0.0
0.0
DryCalm
CloudyNone
78.091.3
86.4
86.2
85.7
78.0
83.3
82.9
83.3
79.5
79.2
20.2
80.1
19.3 1.4 0.0
19.8 1.0 0.0
0.0
0.0
16.6 3.2 0.0
18.3 2.0 0.0
0.0
0.0
21.9 0.0 0.00.0
14.0 2.6 0.0
14.0 2.6 0.0
0.0
0.0
10.5 3.7 0.0
14.7 2.2 0.0
0.0
0.0
9.7 3.9 0.0
0.0
0.0
9.3 4.1 0.0
6.3 0.0
0.0
0.0
6.7 0.0
998
BH4 0.00 00:01:30
0.00 00:00:30
BH4 0.00 00:01:00 0.000.0
0.4
0.2
0.000.0
0.00 0.30.0
BH4 0.00 00:02:00
00:02:30
BH4 0.00
BH4 0.00
BH4 0.00 00:03:00
00:03:30
0.0
0.0
0.0
0.00 00:04:00
BH4 0.00
BH4 0.00 00:05:00
00:06:00
BH4 0.00 00:05:30
0.0
0.0
0.0
0.0
BH5 0.00
BH5 0.00 00:00:30 0.0
0.00 00:03:00
0.0
0.0
0.0
BH4
BH5
BH5 0.00 00:03:30
00:01:30
00:00:00
00:01:00
BH5 0.00998
BH5
BH5 0.00 00:02:30
BH5 0.00 00:02:00
0.00 0.00
0.0
0.0
0.0
0.0
0.0
0.00.0
5.29
0.00
0.00
0.00
0.1
0.2
0.0 21.9
1.8
1.8
1.0
2.9
0.0
1.8
0.8
Reading Depth
(mBGL)
0.03.0
1.8
0.6
0.2
0.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
03/12/2013
CH
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
23/12/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
1.6
0.0
0.0
7.0
6.0
5.2
Reading Depth
(mBGL)
0.01.9
2.1
0.2
0.3
0.4 4.3
1.8
1.5
1.4
6.8
0.0
0.0
0.0Dry
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH3 0.00 00:01:00
BH3 0.00 00:00:30
00:00:00
BH5 0.00 00:02:00
00:02:30BH5 0.00
BH3
BH5
BH3
BH3 0.00 00:02:00 0.0
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH5 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH5 0.00
BH5 0.00 00:00:30
00:01:30
BH5
0.3
5.36 0.00.0
00:03:00
0.00
BH4 0.00
BH4 0.00
00:02:30
BH4 0.00 00:02:00 0.000.0
0.00 0.30.0
0.000.0
0.3
0.2
0.000.0
00:01:30
0.00 00:00:30
BH4 0.00 00:01:00
BH4 0.00 6.3 0.0
0.0
0.0
6.6 0.0
0.09.2 5.6 0.0
18.9 2.9 0.0
19.2 2.6 0.0
0.0
0.0
19.6 2.3 0.0
20.0 1.7 0.0
0.0
0.0
20.5 1.2 0.0
20.9 0.7 0.0
0.0
0.0
21.2 0.1 0.00.0
18.1 0.8 0.0
18.4 0.5 0.0
0.0
0.0
81.0
19.3
78.6
84.7
78.1
78.3
78.2
78.2
78.1
78.0
WetModerateWesterlyCloudyModerate
88.687.6
85.6
7.5 6.1 0.0
8.3 5.8 0.0
0.0
0.0
0.0
0.0
0.0
0.0
81.0
80.8
0.0
0.0
80.6
80.4
80.1
0.00 00:03:00BH3 0.1 0.00.0 79.9
19.6 0.2
0.0 19.9
0.0
87.8
86.5
86.0
18.7 0.4 0.0
0.2
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
19.0
0.0
0.00 0.0
0.3
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH46.01 0.0
6.8 0.00.0BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
23/12/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
0.0
0.0
0.0
0.0
0.0
0.8
0.0
0.0
1.8
19.2
18.5
Reading Depth
(mBGL)
2.52.6
2.1
0.0
0.0
0.1 18.1
1.6
1.3
1.0
19.8
0.0
0.0
BH1 0.00 00:02:00
00:02:30BH1 0.00
BH1
BH1 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH1 0.00
BH1 0.00 00:00:30
00:01:30
BH1
0.0
2.25 0.00.0
00:03:00
0.00
BH2 0.00
BH2 0.00
00:02:30
BH2 0.00 00:02:00 0.000.0
0.00 0.10.0
0.000.0
0.2
0.1
0.000.0
00:01:30
0.00 00:00:30
BH2 0.00 00:01:00
BH2 0.00 1.0 0.0
0.0
0.0
1.4 0.0
0.021.4 0.0 0.0
19.9 0.6 0.0
30.3 0.5 0.0
0.0
0.0
20.5 0.4 0.0
20.6 0.3 0.0
0.0
0.0
20.7 0.2 0.0
20.7 0.2 0.0
0.0
0.0
20.8 0.1 0.00.0 79.0
78.5
79.4
79.0
79.0
79.0
79.1
79.0
WetModerateWesterlyCloudyModerate
79.979.5
78.7
20.4 0.6 0.0
21.0 0.2 0.0
0.0
0.0
79.2
79.0
78.9
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH24.77 0.0
1.6 0.00.0BH2 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
30/12/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.9
0.0
0.0
8.4
5.9
5.8
Reading Depth
(mBGL)
1.61.5
1.9
0.2
0.2
0.5 6.1
1.3
0.8
0.7
6.3
0.0
0.0
0.04.51
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH2 0.00 00:01:00
BH2 0.00 00:00:30
00:00:00
BH3 0.00 00:02:00
00:02:30BH3 0.00
BH2
BH3
BH2
BH2 0.00 00:02:00 0.0
BH2
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH3 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH3 0.00
BH3 0.00 00:00:30
00:01:30
BH3
0.2
Dry 0.00.0
00:03:00
0.00
BH4 0.00
BH4 0.00
00:02:30
BH4 0.00 00:02:00 0.000.0
0.00 0.30.0
0.000.0
0.4
0.3
0.000.0
00:01:30
0.00 00:00:30
BH4 0.00 00:01:00
BH4 0.00 7.3 0.0
0.0
0.0
7.6 0.0
0.07.2 6.3 0.0
19.0 0.3 0.0
19.9 0.2 0.0
0.0
0.0
20.5 0.1 0.0
20.9 0.1 0.0
0.0
0.0
21.2 0.0 0.0
21.5 0.0 0.0
0.0
0.0
21.6 0.0 0.00.0
21.4 0.0 0.0
21.2 0.2 0.0
0.0
0.0
78.5
21.1
78.3
86.2
80.6
78.4
78.9
78.7
79.8
79.3
WetModerateSoutherlyCloudyModerate
85.085.7
85.2
6.6 7.0 0.0
6.9 6.7 0.0
0.0
0.0
0.0
0.0
0.0
0.0
78.6
78.4
0.0
0.0
78.5
78.5
78.6
0.00 00:03:00BH2 0.2 0.00.0 78.6
21.1 0.2
0.0 21.1
0.0
86.1
86.0
86.1
21.2 0.3 0.0
0.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.1
0.0
0.00 0.0
0.3
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH46.06 0.0
8.0 0.00.0BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
30/12/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
0.0
0.3
20.3
20.2
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 20.1
0.0
0.0
0.0
20.3
BH5 0.00
0.000:03:00
BH1 0.00
BH1 0.00
00:02:30
BH1 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH1 0.00 00:01:00
BH1 0.00 0.2 0.0
0.0
0.0
0.2 0.0
0.020.4 0.1 0.0
No access
79.4
WetModerateSoutherlyCloudyModerate
79.579.4
79.4
20.3 0.2 0.0
20.4 0.1 0.0
0.0
0.0
79.4
79.4
79.4
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH12.26 0.0
0.3 0.00.0BH1 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
03/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
988
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
1.2
18.1
17.8
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 16.5
0.0
0.0
0.0
18.0
0.0
0.0
0.02.29
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH1 0.00 00:01:00
BH1 0.00 00:00:30
00:00:00
BH2 0.00 00:02:00
00:02:30BH2 0.00
BH1
BH2
BH1
BH1 0.00 00:02:00 0.0
BH1
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH2 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH2
988
0.0
4.27 0.00.0
00:03:00
0.00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
988
BH3 0.00 0.8 0.0
0.0
0.0
0.8 0.0
0.018.5 0.7 0.0
20.8 0.0 0.0
21.3 0.0 0.0
0.0
0.0
21.1 0.1 0.0
21.1 0.0 0.0
0.0
0.0
21.1 0.0 0.0
21.2 0.0 0.0
0.0
0.0
21.2 0.0 0.00.0
19.5 0.4 0.0
19.7 0.4 0.0
0.0
0.0
80.0
20.0
78.7
80.7
79.1
78.7
78.8
78.8
78.7
78.8
DampLightSouth westerlySlightSlight
82.781.1
80.9
18.1 0.8 0.0
18.2 0.7 0.0
0.0
0.0
0.0
0.0
0.0
0.0
79.8
79.7
0.0
0.0
79.6
79.6
79.5
0.00 00:03:00BH1 0.2 0.00.0 79.5
20.1 0.3
0.0 20.2
0.0
81.0
81.1
81.0
19.9 0.3 0.0
0.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
20.0
0.0
0.00 0.0
0.3
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH3Dry 0.0
0.9 0.00.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
03/01/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 5427 + Dip
Reading Depth
(mBGL)
00:00:00BH5 0.00
DryLightSouth westerlySlightSlight
to monitor
No access
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
Under water; unable5.77BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
10/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
981
2.7
2.7
2.9
0.0
0.0
0.0
2.8
2.8
0.0
0.0
0.0
0.0
0.0
2.0
2.8
0.8
21.6
21.6
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 21.1
0.0
0.0
0.0
21.6
0.4
0.4
0.04.39
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH5 0.00 00:01:00
BH5 0.00 00:00:30
00:00:00
BH2 0.00 00:02:00
00:02:30BH2 0.00
BH5
BH2
BH5
BH5 0.00 00:02:00 0.0
BH5
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH2 0.00 00:03:00
0.4
0.3
0.4
0.4
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH2
981
0.0
4.02 0.30.0
00:03:00
0.00
BH1 0.00
BH1 0.00
00:02:30
BH1 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH1 0.00 00:01:00
981
BH1 0.00 0.1 0.0
0.0
0.0
0.3 0.0
0.021.6 0.0 0.0
2.0 6.1 0.0
2.2 6.1 0.0
0.0
0.0
1.9 6.2 0.0
1.7 6.2 0.0
0.0
0.0
1.5 6.2 0.0
1.3 6.1 0.0
0.0
0.0
1.2 6.2 0.00.0
10.1 7.8 0.0
9.8 6.6 0.0
0.0
0.0
10.1
DampModerateSouth eastCloudyNone
21.6 0.1 0.0
21.6 0.0 0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.00 00:03:00BH5 3.7 0.00.0
10.1 4.1
0.0 10.1
0.0
9.9 5.6 0.0
4.4
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
10.0
0.0
0.00 0.0
4.8
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH12.63 0.0
0.6 0.00.0BH1 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
10/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
2.1
2.2
2.2
2.2
2.2
0.0
2.1
2.1
0.0
21.6
21.4
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 21.2
0.0
0.0
0.0
21.6
0.4
0.3
BH4 0.00 00:02:00
00:02:30BH4 0.00
BH4
BH4 0.00 00:03:00
0.3
0.3
0.4
0.4
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH4 0.00
BH4 0.00 00:00:30
00:01:30
BH4
981
0.0
6.06 0.30.0
00:03:00
0.00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
981
BH3 0.00 0.0 0.0
0.0
0.0
0.0 0.0
0.021.6 0.0 0.0
2.0 6.0 0.0
2.1 5.8 0.0
0.0
0.0
2.0 5.9 0.0
1.9 5.9 0.0
0.0
0.0
1.8 5.9 0.0
1.7 5.8 0.0
0.0
0.0
1.6 5.8 0.00.0
DampModerateSoutherlyCloudyNone
21.6 0.0 0.0
21.6 0.0 0.0
0.0
0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH3Dry 0.0
0.0 0.00.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
13/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
973
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
7.4
8.6
7.5
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 6.5
0.0
0.0
0.0
8.7
0.0
0.0
0.02.59
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH1 0.00 00:01:00
BH1 0.00 00:00:30
00:00:00
BH3 0.00 00:02:00
00:02:30BH3 0.00
BH1
BH3
BH1
BH1 0.00 00:02:00 0.0
BH1
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH3 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH3 0.00
BH3 0.00 00:00:30
00:01:30
BH3
973
0.0
Dry 0.00.0
00:03:00
0.00
BH5 0.00
BH5 0.00
00:02:30
BH5 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH5 0.00 00:01:00
973
BH5 0.00 4.6 0.0
0.0
0.0
5.3 0.0
0.09.7 3.9 0.0
21.1 0.0 0.0
21.8 0.0 0.0
0.0
0.0
21.8 0.0 0.0
21.8 0.0 0.0
0.0
0.0
21.8 0.0 0.0
21.8 0.0 0.0
0.0
0.0
21.8 0.0 0.00.0
20.6 0.5 0.0
21.5 0.4 0.0
0.5
0.4
78.8
21.5
78.1
86.3
78.8
78.1
78.1
78.1
78.1
78.1
DampCalm
CloudyNone
86.086.4
86.5
9.1 4.1 0.0
9.4 3.9 0.0
0.0
0.0
0.2
0.0
0.2
0.3
78.1
77.5
0.0
0.0
78.1
78.1
78.2
0.00 00:03:00BH1 0.2 0.00.2 78.2
21.5 0.2
0.0 21.5
0.0
86.7
86.7
86.7
22.3 0.2 0.0
0.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.5
0.3
0.00 0.0
0.3
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH54.38 0.0
6.2 0.00.0BH5 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
13/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
2.8
2.7
2.8
2.4
3.0
0.0
2.4
2.8
0.1
21.6
21.6
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 20.9
0.0
0.0
0.0
21.6
0.4
0.4
BH4 0.00 00:02:00
00:02:30BH4 0.00
BH4
BH4 0.00 00:03:00
0.4
0.4
0.3
0.4
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH4 0.00
BH4 0.00 00:00:30
00:01:30
BH4
973
0.0
5.94 0.40.0
00:03:00
0.00
BH2 0.00
BH2 0.00
00:02:30
BH2 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH2 0.00 00:01:00
973
BH2 0.00 0.0 0.0
0.0
0.0
0.0 0.0
0.021.6 0.0 0.0
1.6 5.7 0.0
2.2 5.6 0.0
0.0
0.0
1.8 5.8 0.0
1.5 5.8 0.0
0.0
0.0
1.4 5.7 0.0
1.3 5.8 0.0
0.0
0.0
1.2 5.9 0.00.0 92.4
78.3
92.2
92.3
92.1
92.4
91.8
91.8
DampCalm
CloudyNone
78.978.3
78.3
21.6 0.0 0.0
21.6 0.0 0.0
0.0
0.0
78.3
78.3
78.3
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH23.89 0.0
0.0 0.00.0BH2 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
17/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
958
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.7
20.8
20.8
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 20.3
0.0
0.0
0.0
20.8
0.0
0.0
0.0Dry
0.0
0.0
0.000.0
0.00
00:02:30
0.00
BH3 0.00 00:01:00
BH3 0.00 00:00:30
00:00:00
BH2 0.00 00:02:00
00:02:30BH2 0.00
BH3
BH2
BH3
BH3 0.00 00:02:00 0.0
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
0.00
0.00 00:01:30
BH2 0.00 00:03:00
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH
959
0.0
3.69 0.00.0
00:03:00
0.10
BH1 0.00
BH1 0.00
00:02:30
BH1 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH1 0.00 00:01:00
959
BH1 0.00 0.7 0.0
0.0
0.0
0.7 0.0
0.020.9 0.7 0.0
21.1 0.1 0.0
21.8 0.0 0.0
0.0
0.0
21.8 0.0 0.0
21.7 0.0 0.0
0.0
0.0
21.7 0.0 0.0
21.8 0.0 0.0
0.0
0.0
21.8 0.0 0.00.0
21.2 0.0 0.0
21.8 0.0 0.0
0.0
0.0
78.7
21.7
78.1
78.3
78.7
78.1
78.2
78.2
78.1
78.1
DampCalm
CloudyNone
78.978.4
78.3
20.8 0.7 0.0
20.9 0.7 0.0
0.0
0.0
0.0
0.0
0.0
0.0
78.1
78.1
0.0
0.0
78.2
78.2
78.2
0.00 00:03:00BH3 0.0 0.00.0 78.2
21.7 0.0
0.0 21.7
0.0
78.4
78.4
78.4
21.8 0.0 0.0
0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.7
0.0
0.00 0.0
0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH12.30 0.0
0.7 0.00.0BH1 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
17/01/2014
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3155-13
CH4(% LEL)
0.10 0.100.10
CLOUGH HALL TECHNOLOGY SCHOOL
1.00 0.10
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
958
0.0
0.0
0.0
8.7
0.0
0.0
2.5
0.0
6.0
0.3
0.5
Reading Depth
(mBGL)
2.02.0
2.0
0.3
0.3
0.3 1.2
2.0
2.0
2.1
0.3
0.0
0.0
0.0
0.00
BH5 0.00 00:01:30
00:02:00
00:03:00
BH5 0.00 0.0
BH5 0.00
BH5 0.00 00:02:30
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
4.18
0.00
0.00 00:00:30 0.000.0
0.0BH5 0.00
BH5 0.00 00:00:00
00:01:00
BH5
0.400:03:00
BH4 0.00
BH4 0.00
00:02:30
BH4 0.00 00:02:00 0.000.0
0.00 0.30.0
0.000.0
0.3
0.3
0.000.0
00:01:30
0.00 00:00:30
BH4 0.00 00:01:00
958
BH4 0.00 6.0 0.0
0.0
0.0
6.1 0.0
0.00.2 5.9 0.0
6.5 6.0 0.00.0
6.6 6.2 0.0
5.7 6.1 0.0
0.0
0.0
5.0 6.0 0.0
4.6 6.0 0.0
0.0
0.0
4.2 5.9 0.0
4.0 5.9 0.0
0.0
0.0 87.2
87.2
93.4
87.2
86.7
87.0
85.7
86.1
DampCalm
CloudyNone
92.492.8
93.5
0.2 6.0 0.0
0.2 5.9 0.0
0.0
0.0
93.2
93.2
93.5
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH45.31 0.0
6.2 0.00.0BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
January 2014 Report No D3155-13 Issue 3.0 Enclosure C
ENCLOSURE C
GEOTECHNICAL LABORATORY TEST RESULTS
Determination of Moisture Content and Atterberg Limits INDX 1
Particle Size Distribution Analyses PSD 1 to 21
Soil Sample Analysis ESG Scientifics Report No EFS/136829
Chemical Tests – Summary of Results CHEM 1 Determination of Moisture Content/Dry Density Relationship (Light 2.5kg Compaction) COMPL 1
Determination of Moisture Content/Moisture Condition Value MCVREL 1 to 4
Determination of California Bearing Ratio CBR 1
One Dimensional Consolidation Test OED 1 to 4 Unconsolidated Undrained Triaxial Compression Tests – Summary of Results UUSUM 1
Unconfined Compressive Strength RUCS 1
Point Load Index PLT 1
Project No Project Name
p p d w < 425 WL WP IP p sµm
sieve
from to % % % % Mg/m3
10 1.00 DGreyish brown slightly gravelly sandy silty CLAY.
22 90 s 28 a 16 12
20 3.70 4.00 BBrown slightly sandy slightly gravelly CLAY.
27 58 s 32 a 18 14
11 1.50 1.95 UStiff grey friable slightly sandy CLAY with siltstone.
15 100 n 44 a 23 21
12 2.05 DGrey slightly sandy silty CLAY.
11 100 n 39 a 21 18
16 3.50 3.60 DDark grey sandy sliightly silty GRAVEL.
8.5
9 1.95 UBrown slightly gravelly SAND.
16 69 s 24 b NP
10 2.05 0.00 DBrown slightly sandy slightly gravelly CLAY.
19 97 s 32 a 17 15
14 3.00 3.10 DLight grey and cream slightly sandy GRAVEL.
1.6
10 1.50 1.95 UVery stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.
9.5 100 n 38 a 19 19
12 2.50 2.90 DGreyish brown slighty sandy slightly gravelly silty CLAY Gravel is siltstone.
6.1 79 s 36 a 21 15
14 3.50 3.90 DDark grey slightly gravelly silty CLAY.
8.5 69 s 40 a 22 18
3 0.25 DBrownish grey slightly gravelly silty CLAY.
18 87 s 39 a 20 19
8 2.05 DBrown slightly sandy slightly gravelly CLAY.
14 75 s 35 a 18 17
16 3.50 4.95 DGreyish brown slightly gravelly sandy silty CLAY.
1.9 73 s 37 a 20 17
20 6.15 6.20 DLight greyish brown slightly sandy SILT.
6.7
3 0.50 DGrey slightly sandy slightly gravelly CLAY.
19 90 s 40 a 20 20
10 2.50 DBrown slightly gravelly SAND.
7.3 29 s 22 b NP
14 3.00 DGreyish brown slightly gravelly sandy silty CLAY.
7.3 51 s 38 a 21 17
4 0.50 DDark brown and grey sandy gravelly CLAY.
14 39 s 29 a 17 12
7 1.10 DDark greyish brown slightly sandy slightly gravelly CLAY.
28 75 s 35 a 22 13
10 1.90 DBrown slightly gravelly very sandy CLAY.
14 78 s 25 a 15 10
14 3.50 DGrey and brown slightly sandy slightly gravelly silty CLAY.
16 81 s 36 a 18 18
15 4.00 DGreyish brown slightly gravelly sandy silty CLAY.
12 80 s 44 a 25 19
4 1.20 DDark grey slightly gravelly sandy CLAY.
16 52 s 42 b 25 17
11 4.00 DDark brown slightly sandy slightly gravelly CLAY.
26 96 s 35 a 18 17
8 1.40 DOrangish brown slightly sandy slightly gravelly CLAY.
21 91 s 34 a 13 21
11 2.60 DReddish brown slightly sandy slightly gravelly CLAY.
17 79 s 30 a 14 16
6 1.20 DLight greyish brown slightly sandy slightly gravelly silty CLAY.
6.8 66 s 41 a 21 20
8 1.80 DLight grey slightly gravelly SILT. Gravel is siltstone.
6.7
7 1.10 DLight brown slightly gravelly very clayey SAND.
11 68 s 26 a 14 12
General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.
Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density
p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar
w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer
QA Ref
WS6
WS4
WS4
WS5
WS5
WS2
WS2
WS3
WS3
WS1
WS2
WS2
WS2
BH5
BH5
TP1
WS1
BH4
BH4
BH5
BH5
BH3
BH3
BH3
BH4
BH1
BH2
BH2
BH2
CLOUGH HALL TECHNOLOGY SCHOOL
INDEX PROPERTIES - SUMMARY OF RESULTS
Soil Description
D3155-13
SLR 1Rev 91Mar 12
BH1
Hole No.
Printed:04/12/2013 14:08
Mg/m3
INDX 1
Remarks
Plasticity Index
Sample
Depth (m)No. type
Table
2117
08542117
0.0048Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0354
%Passing
100756350
9593
0.0015
870.6001.18 91
9728
9796
97201410
14.3
2.65
0.063 390.150
790.425
6453
0.300
Particle density, Mg/m3
5.0
92
95
3.352.00
6.3
89
Clay
Sample Proportions
*<60mm values to aid description only
Sand
20
Silt
17 Cobbles / boulders
2521
Gravel
Remarks
854
Soil description%Passing
Brown slightly gravelly sandy CLAY.
3310010097
0.02540.01800.009537.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0494
3936
3029
PSD 1
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
11 B
ESGD3155-13201311040000000008
QA Ref
SLR 2,9Rev 88Aug 11
0.70
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:12
118
03645118
0.0048Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0354
%Passing
100756350
7268
0.0015
520.6001.18 61
9728
8679
92201410
22.4
2.65
0.063 190.150
450.425
3527
0.300
Particle density, Mg/m3
5.0
64
74
3.352.00
6.3
56
Clay
Sample Proportions
*<60mm values to aid description only
Sand
9
Silt
7 Cobbles / boulders
1110
Gravel
Remarks
3645
Soil description%Passing
Brown sandy gravelly CLAY.
1610010099
0.02540.01810.009537.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
182
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment
0.06300.0494
1918
1513
PSD 2
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
13 B
ESGD3155-13201311040000000013
QA Ref
SLR 2,9Rev 88Aug 11
1.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:12
116
0677116
0.0050Whole *<60mm
00.0036
0.212
Particle Size mm
Particle Size mm
0.0378
%Passing
100756350
9695
0.0016
840.6001.18 92
10028
10098
100201410
2.4
2.65
0.063 170.150
640.425
3926
0.300
Particle density, Mg/m3
5.0
94
96
3.352.00
6.3
90
Clay
Sample Proportions
*<60mm values to aid description only
Sand
6
Silt
5 Cobbles / boulders
107
Gravel
Remarks
677
Soil description%Passing
Brown gravelly clayey SAND.
14100100100
0.02690.01910.009937.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
28
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0532
1715
1211
PSD 3
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
17 B
ESGD3155-13201311040000000017
QA Ref
SLR 2,9Rev 88Aug 11
2.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:12
198
02647198
0.0048Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0340
%Passing
100756350
8279
0.0015
620.6001.18 70
9628
9087
93201410
18.3
2.65
0.063 270.150
520.425
4134
0.300
Particle density, Mg/m3
5.0
74
84
3.352.00
6.3
65
Clay
Sample Proportions
*<60mm values to aid description only
Sand
10
Silt
7 Cobbles / boulders
1411
Gravel
Remarks
2647
Soil description%Passing
Brown slightly gravelly sandy CLAY.
241009997
0.02460.01770.009437.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
123
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment
0.06300.0474
2726
2119
PSD 4
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
19 B
ESGD3155-13201311040000000019
QA Ref
SLR 2,9Rev 88Aug 11
3.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =9
05140
9
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
6760
330.6001.18 42
9528
8779
91201410
5.80.063 90.150
260.425
1813
0.300
5.0
49
70
3.352.00
6.3
36
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
5140
Soil description%Passing
Brown very sandy GRAVEL with occasional clay pockets.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
44
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 5
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH3
4 B
ESGD3155-13201311040000000040
QA Ref
SLR 2,9Rev 88Aug 11
0.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
1215
08651215
0.0050Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0379
%Passing
100756350
9593
0.0015
880.6001.18 92
10028
9696
98201410
11.1
2.65
0.063 280.150
800.425
6041
0.300
Particle density, Mg/m3
5.0
92
95
3.352.00
6.3
90
Clay
Sample Proportions
*<60mm values to aid description only
Sand
19
Silt
14 Cobbles / boulders
2320
Gravel
Remarks
865
Soil description%Passing
Brown slightly gravelly very sandy CLAY.
25100100100
0.02690.01900.009837.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0535
2826
2424
PSD 6
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH3
13 B
ESGD3155-13201311040000000049
QA Ref
SLR 2,9Rev 88Aug 11
2.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
7017
0677017
0.0049Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0364
%Passing
100756350
9796
0.0016
920.6001.18 93
10028
9898
100201410
16.7
2.65
0.063 900.150
910.425
9190
0.300
Particle density, Mg/m3
5.0
94
97
3.352.00
6.3
92
Clay
Sample Proportions
*<60mm values to aid description only
Sand
27
Silt
13 Cobbles / boulders
6345
Gravel
Remarks
67
Soil description%Passing
Greyish brown slightly sandy slightly gravelly silty CLAY with mudstone.
79100100100
0.02580.01830.009637.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0513
9081
7876
PSD 7
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
8 B
ESGD3155-13201311040000000058
QA Ref
SLR 2,9Rev 88Aug 11
0.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
6727
0336727
0.0047Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0331
%Passing
100756350
9897
0.0015
970.6001.18 97
9928
9999
99201410
10.9
2.65
0.063 950.150
960.425
9696
0.300
Particle density, Mg/m3
5.0
97
98
3.352.00
6.3
97
Clay
Sample Proportions
*<60mm values to aid description only
Sand
38
Silt
22 Cobbles / boulders
7250
Gravel
Remarks
33
Soil description%Passing
Greyish brown slightly sandy slightly gravelly silty CLAY with mudstone.
89100100100
0.02350.01680.008937.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0464
9592
8683
PSD 8
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
13 B
ESGD3155-13201311040000000063
QA Ref
SLR 2,9Rev 88Aug 11
2.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
2222
025272424
0.0043Whole *<60mm
80.0031
0.212
Particle Size mm
Particle Size mm
0.0305
%Passing
92756350
7371
0.0014
640.6001.18 67
8928
8278
86201410
12.2
2.65
0.063 440.150
600.425
5450
0.300
Particle density, Mg/m3
5.0
69
74
3.352.00
6.3
66
Clay
Sample Proportions
*<60mm values to aid description only
Sand
25
Silt
19 Cobbles / boulders
3429
Gravel
Remarks
2325
Soil description%Passing
Brown slightly sandy slightly gravelly CLAY with one cobble.
40929290
0.02190.01560.008337.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0424
4442
3938
PSD 9
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
17 B
ESGD3155-13201311040000000082
QA Ref
SLR 2,9Rev 88Aug 11
4.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
5327
010105327
0.0047Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0336
%Passing
100756350
9593
0.0015
870.6001.18 88
10028
9999
100201410
2.8
2.65
0.063 810.150
860.425
8584
0.300
Particle density, Mg/m3
5.0
90
97
3.352.00
6.3
87
Clay
Sample Proportions
*<60mm values to aid description only
Sand
35
Silt
23 Cobbles / boulders
5640
Gravel
Remarks
1010
Soil description%Passing
Brown slightly sandy slightly gravelly CLAY.
75100100100
0.02410.01720.009137.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0471
8178
7166
PSD 10
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
19 B
ESGD3155-13201311040000000084
QA Ref
SLR 2,9Rev 88Aug 11
5.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =14
0976
15
Whole *<60mm5
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
8787
790.6001.18 85
9328
9089
92201410
9.30.063 140.150
590.425
3721
0.300
5.0
86
87
3.352.00
6.3
83
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
972
Soil description%Passing
Brown gravelly clayey SAND with one cobble.
95959537.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 11
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
TP1
6 B
ESGD3155-1320131104499609
QA Ref
SLR 2,9Rev 88Aug 11
1.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
1813
016531813
0.0049Whole *<60mm
10.0035
0.212
Particle Size mm
Particle Size mm
0.0367
%Passing
100756350
8685
0.0015
780.6001.18 82
9428
9290
92201410
7.8
2.65
0.063 330.150
680.425
5242
0.300
Particle density, Mg/m3
5.0
83
87
3.352.00
6.3
81
Clay
Sample Proportions
*<60mm values to aid description only
Sand
15
Silt
13 Cobbles / boulders
2016
Gravel
Remarks
1652
Soil description%Passing
Brown gravelly SAND wth frequent clay pockets.
261009694
0.02630.01870.009737.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0516
3328
2321
PSD 12
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
TP2
5 B
ESGD3155-1320131104382114
QA Ref
SLR 2,9Rev 88Aug 11
0.85
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
115
02559115
0.0050Whole *<60mm
00.0036
0.212
Particle Size mm
Particle Size mm
0.0378
%Passing
100756350
7776
0.0016
630.6001.18 73
8828
8381
86201410
14.0
2.65
0.063 160.150
490.425
3525
0.300
Particle density, Mg/m3
5.0
75
79
3.352.00
6.3
69
Clay
Sample Proportions
*<60mm values to aid description only
Sand
5
Silt
5 Cobbles / boulders
87
Gravel
Remarks
2559
Soil description%Passing
Brown very gravelly silty SAND.
131009992
0.02690.01910.010037.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
22
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment
0.06300.0529
1615
1110
PSD 13
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
6 B
ESGD3155-13201311040000000091
QA Ref
SLR 2,9Rev 88Aug 11
0.80
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =6
02569
6
Whole *<60mm1
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
7876
600.6001.18 71
9028
8583
86201410
5.70.063 60.150
400.425
179
0.300
5.0
74
80
3.352.00
6.3
67
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
2568
Soil description%Passing
Brown very gravelly SAND with rare clay pockets.
100949437.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
3
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 14
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
9 B
ESGD3155-13201311040000000094
QA Ref
SLR 2,9Rev 88Aug 11
1.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =14
05432
14
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
5550
330.6001.18 43
8828
7266
80201410
2.80.063 140.150
260.425
2017
0.300
5.0
46
58
3.352.00
6.3
37
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
5432
Soil description%Passing
Greyish brown slightly sandy gravelly CLAY.
1001008837.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: pre dried, Preparation / Pretreatment
PSD 15
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS3
7 B
ESGD3155-13201311040000000121
QA Ref
SLR 2,9Rev 88Aug 11
2.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =6
0292
6
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
9999
920.6001.18 98
10028
10099
100201410
1.20.063 70.150
720.425
3513
0.300
5.0
98
99
3.352.00
6.3
96
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
292
Soil description%Passing
Brown slightly gravelly SAND with rare clay pockets.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
3
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 16
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS3
10 B
ESGD3155-13201311040000000124
QA Ref
SLR 2,9Rev 88Aug 11
3.50
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
97
0206497
0.0050Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0376
%Passing
100756350
8382
0.0016
750.6001.18 79
9828
9188
95201410
11.6
2.65
0.063 170.150
660.425
4933
0.300
Particle density, Mg/m3
5.0
80
84
3.352.00
6.3
77
Clay
Sample Proportions
*<60mm values to aid description only
Sand
8
Silt
7 Cobbles / boulders
109
Gravel
Remarks
2064
Soil description%Passing
Brown gravelly clayey SAND.
13100100100
0.02670.01900.009937.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
24
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0526
1715
1211
PSD 17
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS4
5 B
ESGD3155-13201311040000000131
QA Ref
SLR 2,9Rev 88Aug 11
0.70
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
2714
039202714
0.0043Whole *<60mm
00.0032
0.212
Particle Size mm
Particle Size mm
0.0283
%Passing
100756350
7166
0.0015
520.6001.18 57
9528
8882
93201410
9.5
2.65
0.063 410.150
500.425
4745
0.300
Particle density, Mg/m3
5.0
61
74
3.352.00
6.3
53
Clay
Sample Proportions
*<60mm values to aid description only
Sand
19
Silt
12 Cobbles / boulders
2822
Gravel
Remarks
3920
Soil description%Passing
Grey slightly sandy gravelly CLAY.
37100100100
0.02040.01490.008137.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0389
4139
3533
PSD 18
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS5
5 B
ESGD3155-13201311040000000148
QA Ref
SLR 2,9Rev 88Aug 11
0.60
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
5021
02455021
0.0046Whole *<60mm
00.0034
0.212
Particle Size mm
Particle Size mm
0.0327
%Passing
100756350
8078
0.0015
730.6001.18 75
10028
9490
97201410
7.7
2.65
0.063 710.150
730.425
7372
0.300
Particle density, Mg/m3
5.0
76
82
3.352.00
6.3
74
Clay
Sample Proportions
*<60mm values to aid description only
Sand
30
Silt
16 Cobbles / boulders
5540
Gravel
Remarks
245
Soil description%Passing
Grey slightly sandy slightly gravelly CLAY.
66100100100
0.02310.01650.008837.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0461
7167
6663
PSD 19
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS5
7 B
ESGD3155-13201311040000000150
QA Ref
SLR 2,9Rev 88Aug 11
1.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =4
0096
4
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
100100
980.6001.18 100
10028
100100
100201410
5.60.063 40.150
880.425
6331
0.300
5.0
100
100
3.352.00
6.3
99
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
096
Soil description%Passing
Brown slightly silty SAND.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
3
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 20
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS6
11 B
ESGD3155-13201311040000000162
QA Ref
SLR 2,9Rev 88Aug 11
2.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
silt+clay =5
0194
5
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
10099
970.6001.18 99
10028
100100
100201410
3.20.063 50.150
890.425
6634
0.300
5.0
99
100
3.352.00
6.3
98
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
194
Soil description%Passing
Orangish brown slightly gravelly SAND.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
3
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 21
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS6
15 B
ESGD3155-13201311040000000166
QA Ref
SLR 2,9Rev 88Aug 11
3.80
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:04/12/2013 14:13
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Clough Hall Technology School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 29-Nov-2013Declan Burns Operations Director
Laboratory and Analytical Business
29-Nov-2013
The 13 samples described in this report were registered for analysis by ESG on 21-Nov-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/136829 (Ver. 1)
Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 5Where individual results are flagged see report notes for status.
EFS/136829 Ver. 1
Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50
Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No
LAB
ID N
umber C
L/
Client Sample Description
SO
4-- (acid sol)
SO
4-- (H2O
sol) mg/l
Total S
ulphur.
pH (B
S1377)
1329122 BH1 D 2 0.00 242 28 0.121 8.7
1329123 BH1 D 12 1.50 181 13 0.022 7.9
1329124 BH2 B 8 0.50 706 62 0.084 7.9
1329125 BH3 D 2 0.20 6200 436 0.423 9.0
1329126 BH4 D 6 0.50 1170 122 0.096 6.6
1329127 BH5 D 2 0.20 719 70 0.084 7.8
1329128 BH5 D 10 2.50 913 83 0.044 5.7
1329129 WS1 D 13 2.90 237 63 0.015 7.0
1329130 WS2 ES 4 0.50 1110 38 0.102 8.0
1329131 WS3 B 2 0.20 787 28 0.058 7.6
1329132 WS4 D 8 1.20 296 34 0.015 7.5
1329133 WS6 D 4 0.50 740 225 0.023 5.5
1329134 WS6 D 17 5.00 369 92 0.125 7.1
Contact
Date Printed
Report Number EFS/136829
Table Number 1
Fax +44 (0) 1283 554422
Soil Sample Analysis
Mr J Litten
29-Nov-2013
Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 5Where individual results are flagged see report notes for status.
EFS/136829 Ver. 1
SOIL Analysis S136829
CustomerSiteReport No S136829
MethodID
CustS
erv
Dep.O
pt
ICP
AC
IDS
ICP
BR
E
ICP
WS
S
KoneN
O3
TS
BR
E1
WS
LM43
WS
LM50
ID Number Description Sampled
Report B
DO
Cl if pH
<5.5
DO
Mg if S
O4(W
)>3000
DO
NO
3 if pH<5.5
SO
4-- (acid sol)
Magnesium
(BR
E)
SO
4-- (H2O
sol) mg/l
Nitrate (2:1): m
g/l
Total S
ulphur.
Chloride (W
) BS
1377
pH (B
S1377)
���� ����
CL/1329122 BH1 0.00-0.10 DCL/1329123 BH1 1.50 DCL/1329124 BH2 0.50 DCL/1329125 BH3 0.20 DCL/1329126 BH4 0.50 DCL/1329127 BH5 0.20 DCL/1329128 BH5 2.50 DCL/1329129 WS1 2.90 DCL/1329130 WS2 0.50 DCL/1329131 WS3 0.20 DCL/1329132 WS4 1.20 DCL/1329133 WS6 0.50 DCL/1329134 WS6 5.00 D
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S38194
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
Clough Hall Technology School Date Logged 21-Nov-2013
Report Due 29-Nov-2013
Page 3 of 5Where individual results are flagged see report notes for status.
EFS/136829 Ver. 1
Matrix MethodID Analysis Basis
Method Description
Soil ICPACIDS Air Dried Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil WSLM50 Air Dried Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Report Number: EFS/136829
Method Descriptions
Page 4 of 5Where individual results are flagged see report notes for status.
EFS/136829 Ver. 1
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 5 of 5Where individual results are flagged see report notes for status.
EFS/136829 Ver. 1
Project No Project Name
LOI pH CO2 <2
2:1watersol.
groundwater
acidsol.
TSMgNO3
NH4
mg/Lmg/L
watersol.
acidsol.
mm
from to % g/L g/L % % % % % %
7 0.50 DDark brownish grey sandy gravelly CLAY. 2.4 c 52
10 1.40 DDark grey and black slightly sandy slightly gravelly silty CLAY.
16.7 c 100
5 0.40 DOrangish brown and grey slightly gravelly very sandy CLAY.
0.8 c 96
6 0.50 DGreyish brown slightly sandy slightly gravelly CLAY.
1.9 c 82
2 0.20 DBrown slightly sandy slightly gravelly CLAY. 3.8 c 66
13 2.90 DGreyish brown slightly sandy slightly gravelly CLAY.
6.2 c 100
4 0.50 DDark brown and grey sandy gravelly CLAY. 1.5 c 76
2 0.20 0.80 BBrown slightly sandy slightly gravelly CLAY with occasional rootlets.
2.4 c 96
2 0.30 DBrownish grey slightly sandy slightly gravelly CLAY with plant remains
1.5 c 72
13 3.00 DDark grey gravelly clayey SAND. 1.5 c 74
4 0.50 DGreyish brown slightly sandy slightly gravelly CLAY.
3.2 c 100
17 5.00 DLight brown slightly gravelly SAND. 0.5 c 100
BS 1377 : definitive method unless stated : * Sulphate tests preparation / test methods : BRE Special Digest SD1, dependent options :
Org1. BS 1377:Part 3:1990:clause 5.3 4. TRL447 - 1 water soluble sulphate TS Total Sulphur to BR279 / EN ISO15178
LOI Mass loss on ignition at 440oC 2. BS 1377:Part 3:1990:clause 5.4 5. TRL447 - 2 acid soluble sulphate Mg Soluble Magnesium to BR279, colorimetric
CO2 Carbonate content ( rapid titration ) 3. BS 1377:Part 3:1990:clause 5.5 6. BR279 - groundwater sulphate NO3 Soluble Nitrate to BR279, colorimetric
Cl Chloride content < 2mm material passing 2mm sieve NH4 qualitative
QA Ref
WS6
WS6
WS4
WS4
WS2
WS3
Sample
Depth (m)No. type
Hole No. Soil Description
Sulphate as SO4 SD1 options
Pre
para
tion/
test
*
Org
%
Chloride, Cl
Printed:04/12/2013 14:09
BH1
Remarks
Organic matter content ( s-sulphides, c-chlorides identified )
BH2
BH3
CHEMICAL TESTS - SUMMARY OF RESULTS
CHEM 1SLR 3Rev 95Aug 11
D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL
BH4
BH5
WS1
Table
Soil description Derived Parameters +
Test method BS 1377:part 4:1990: clause 3.3, 2.5 kg rammer in a 1 litre mould Maximum dry density, Mg/m3
Preparation Original material was natural, single sample tested
Material > 37.5mm %
Material < 37.5mm > 20mm % Optimum moisture content, %
Particle density, Mg/m3 assumed
Remarks
1.77
16
Brown slightly sandy slightly gravelly CLAY.
2.65
0
3
COMPL 1
DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
0.25
5 B
ESGD3155-13201311040000000070
QA Ref
SLD 4, 3.3/4Rev 66Aug 11
1.4
1.5
1.6
1.7
1.8
1.9
2.0
2.1
2.2
0 4 8 12 16 20 24 28 32
MOISTURE CONTENT %
DR
Y D
EN
SIT
Y M
g/m
3
----- zero, 5% and 10% air voids
Spec Ref
Figure
� Printed:04/12/2013 14:10
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Characteristics of calibration line (determined using linear regression)
25.7
-0.52
1.93
Intercept
Slope
Method of interpretation of MCV
-0.95
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
MCVREL 1
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
0.10
4 B
ESGD3155-13201311040000000052
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
5
10
15
20
25
30
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:04/12/2013 14:11
Test No * ineffective / invalid point 1 2 3 4
%
sheet 2 of 2
1.75
18.7
2.182.08
12.1 10.5 17.2
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
5.8
Soil description
19.8 19.7 16.4
14.2
18.7
1.87
2.03 2.04
1.69 1.70
Mg/m³
Mg/m³
% Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test
Reddish brown sandy gravelly CLAY.
Remarks
%
MCVREL 1
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
0.10
4 B
ESGD3155-13201311040000000052
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:04/12/2013 14:11
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Characteristics of calibration line (determined using linear regression)
15.7
-0.36
2.82
Intercept
Slope
Method of interpretation of MCV
-1.00
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
MCVREL 2
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
0.20
4 B
ESGD3155-13201311040000000089
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
4
8
12
16
20
24
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:04/12/2013 14:11
Test No * ineffective / invalid point 1 * 2 3 4 5
%
sheet 2 of 2
1.84
16.6
12.2
9.9
2.01
2.222.15
2.7 4.6 6.7
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
33.7
Soil description
2.25
14.7 14.2 13.3
#N/A
16.6
1.96
2.18 2.18
1.90 1.91
Mg/m³
Mg/m³
% Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test
Brown sandy gravelly CLAY with two cobbles.
Remarks
%
MCVREL 2
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
0.20
4 B
ESGD3155-13201311040000000089
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:04/12/2013 14:11
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Characteristics of calibration line (determined using linear regression)
22.2
-0.67
1.50
Intercept
Slope
Method of interpretation of MCV
-0.99
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
MCVREL 3
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS4
0.40
4 B
ESGD3155-13201311040000000129
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
4
8
12
16
20
24
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:04/12/2013 14:11
Test No * ineffective / invalid point 1 2 3 4 5
%
sheet 2 of 2
1.80
16.4
13.9
12.6
1.89
2.032.09
6.9 10.5 5.0
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
24.2
Soil description
2.15
17.8 15.4 19.1
7.9
16.4
1.70
2.06 2.12
1.75 1.84
Mg/m³
Mg/m³
% Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test
Brown slightly sandy slightly gravelly CLAY with two cobbles.
Remarks
%
MCVREL 3
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS4
0.40
4 B
ESGD3155-13201311040000000129
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:04/12/2013 14:11
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Characteristics of calibration line (determined using linear regression)
12.0
-0.31
3.25
Intercept
Slope
Method of interpretation of MCV
-1.00
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
MCVREL 4
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS6
0.20
3 B
ESGD3155-13201311040000000154
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
4
8
12
16
20
24
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:04/12/2013 14:11
Test No * ineffective / invalid point 1 2 3 4
%
sheet 2 of 2
2.16
9.1
2.232.36
6.2 13.7 0.8
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
25.2
Soil description
10.2 7.9 11.8
9.1
9.1
1.99
2.27 2.37
2.06 2.20
Mg/m³
Mg/m³
% Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test
Dark brown slightly sandy clayey GRAVEL.
Remarks
%
MCVREL 4
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS6
0.20
3 B
ESGD3155-13201311040000000154
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:04/12/2013 14:11
%
Notes :
Soil description
%
Mg/m³
17
2.02
17
18
Test Conditions
Sample Retained on 20 mm sieve
Sample Conditions
%
%
BASETOP
1.73Mg/m³
CBR Values %
Moisture Content - BASE
Bulk Density
Dry Density
mm
Method of Compaction
days 6Soaking PeriodPre
para
tion
3
Recompacted - Rammer compaction with specified effort ( 2.5kg )
Soaked test
2.61.8
5.0 2.2 3.30
0
2.2
Amount of Swell 0.19
Brown slightly sandy slightly gravelly CLAY.
Initial Moisture Content
Moisture Content - TOP
YES
Penetration mm
Accepted CBR % 3.3
kgSurcharge applied
2.5
kPa
CBR 1
0.00
0.10
0.20
0.30
0.40
0.50
0.60
0.70
0.80
0.90
1.00
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5
Penetration - mm
For
ce o
n P
lung
er -
kN
TOPBASE
California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
0.25
5 B
ESGD3155-13201311040000000070
QA Ref
SLR 4.7Rev 89Aug 11
Spec Ref
Figure
� Printed:04/12/2013 14:10
Soil description
Preparation
Index properties 44 23( if available )
Specimen detailsParticle density Mg/m3
Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3
Dry density Mg/m3
Saturation %Average temperature for test oC
Swelling pressure kPa
Notes :
Specimen taken 20 mm from base of sample
0.1371824
m2/MN
0.3888330.3737
kPa
Applied
PressureMv
Cv
( t50, log )Cv
( t90, root )Voids ratio
m2/year m2/year
3060
2.00
17.89
13
2.65 assumed
74.99
960
240480
120
18.850.395
122.141.9083
0.152 46 49
18
31221716- -
0.28280.095
0.325
2.2660
0.059
19
0.3247
0.35110.181
0.036
0.3204
Stiff grey friable slightly sandy CLAY with siltstone.
Undisturbed
>30
Liquid limit % Plastic limit %
0.3952
105
Initial Final
0.200
0.220
0.240
0.260
0.280
0.300
0.320
0.340
0.360
0.380
0.400Applied pressure kPa
Voi
ds r
atio
ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details:
Hole No
Depth (m BGL)
Samp No Type
ID
BH2
1.50
11 U
ESGD3155-13201311040000000031
QA Ref
SLR 5.3Rev 140Mar 12
00.00
10.00
20.00
30.00
40.00
50.00
1 10 100 1000 10000Applied pressure kPa
Cv
m2 /y
ear
( lo
g t )
Log pressure / voids ratio
Log pressure / Cv
Spec Ref
OED 1
Figure
� Printed:04/12/2013 14:10
Soil description
Preparation
Index properties 24 NP( if available )
Specimen detailsParticle density Mg/m3
Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3
Dry density Mg/m3
Saturation %Average temperature for test oC
Swelling pressure kPa
Notes :
Specimen taken 40 mm from base of sample
0.032--
m2/MN
0.5846-0.5825
kPa
Applied
PressureMv
Cv
( t50, log )Cv
( t90, root )Voids ratio
m2/year m2/year
020
1.68
18.85
17
2.65 assumed
75.02
320
80160
40
19.030.590
171.941.6775
0.168 - -
-
----- -
0.57450.020
0.575
1.9620
0.014
19
0.5752
0.58050.066
0.001
0.5780
Brown slightly gravelly SAND.
Undisturbed
not measured
Liquid limit % Plastic limit %
0.5899
77
Initial Final
Insufficient movement after intial settlement to interpret t50 and t90, hence no Cv's.
0.570
0.572
0.574
0.576
0.578
0.580
0.582
0.584
0.586
0.588
0.590Applied pressure kPa
Voi
ds r
atio
ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details:
Hole No
Depth (m BGL)
Samp No Type
ID
BH3
1.95
9 U
ESGD3155-13201311040000000045
QA Ref
SLR 5.3Rev 140Mar 12
00.00
00.02
00.04
00.06
00.08
00.10
1 10 100 1000 10000Applied pressure kPa
Cv
m2 /y
ear
( lo
g t )
Log pressure / voids ratio
Log pressure / Cv
Spec Ref
OED 2
Figure
� Printed:04/12/2013 14:11
Soil description
Preparation
Index properties 38 19( if available )
Specimen detailsParticle density Mg/m3
Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3
Dry density Mg/m3
Saturation %Average temperature for test oC
Swelling pressure kPa
Notes :
Specimen taken 0 mm from base of sample
0.0711928
m2/MN
0.3249170.3088
kPa
Applied
PressureMv
Cv
( t50, log )Cv
( t90, root )Voids ratio
m2/year m2/year
60120
2.10
18.07
10
2.65 assumed
75.01
1920
480960
240
19.030.332
112.211.9987
0.083 47 50
19
16231817- -
0.22530.048
0.264
2.32120
0.026
19
0.2643
0.28650.101
0.018
0.2570
Very stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.
Undisturbed
>60
Liquid limit % Plastic limit %
0.3315
105
Initial Final
0.140
0.160
0.180
0.200
0.220
0.240
0.260
0.280
0.300
0.320
0.340Applied pressure kPa
Voi
ds r
atio
ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details:
Hole No
Depth (m BGL)
Samp No Type
ID
BH4
1.50
10 U
ESGD3155-13201311040000000060
QA Ref
SLR 5.3Rev 140Mar 12
00.00
10.00
20.00
30.00
40.00
50.00
1 10 100 1000 10000Applied pressure kPa
Cv
m2 /y
ear
( lo
g t )
Log pressure / voids ratio
Log pressure / Cv
Spec Ref
OED 3
Figure
� Printed:04/12/2013 14:11
Soil description
Preparation
Index properties( if available )
Specimen detailsParticle density Mg/m3
Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3
Dry density Mg/m3
Saturation %Average temperature for test oC
Swelling pressure kPa
Notes :
Specimen taken 0 mm from base of sample
0.2701325
m2/MN
0.40389.70.4001
kPa
Applied
PressureMv
Cv
( t50, log )Cv
( t90, root )Voids ratio
m2/year m2/year
010
1.92
18.61
15
2.65 assumed
75.00
160
4080
20
19.040.411
142.151.8893
0.536 7.9 8.2
20
9.5231218- -
0.36970.180
0.380
2.2010
0.116
19
0.3800
0.39260.264
0.050
0.3826
Firm greyish brown slightly sandy slightly gravelly CLAY.
Undisturbed
not measured
Liquid limit % Plastic limit %
0.4114
101
Initial Final
0.365
0.370
0.375
0.380
0.385
0.390
0.395
0.400
0.405
0.410
0.415Applied pressure kPa
Voi
ds r
atio
ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3
Project No
Project Name
D3155-13
CLOUGH HALL TECHNOLOGY SCHOOL
Sample Details:
Hole No
Depth (m BGL)
Samp No Type
ID
BH5
3.50
13 U
ESGD3155-13201311040000000079
QA Ref
SLR 5.3Rev 140Mar 12
00.00
05.00
10.00
15.00
20.00
25.00
1 10 100 1000 10000Applied pressure kPa
Cv
m2 /y
ear
( lo
g t )
Log pressure / voids ratio
Log pressure / Cv
Spec Ref
OED 4
Figure
� Printed:04/12/2013 14:11
w Test Dia. ó3
bulk drytype Axial
strain ó1 - ó3 c u
from to % mm kPa % kPa kPa
11 1.50 1.95 UStiff grey friable slightly sandy CLAY with siltstone. 2.13 1.86 15 UUM
102.4 102.4 102.4
20 40 80
3.0 4.5 8.9
69 89
125
35 45 63
B
9 1.95 UBrown slightly gravelly SAND.
2.14 1.85 16 UU 101.9 20 13.5 263 132 C
10 1.50 1.95 UVery stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.
2.33 2.13 9.5 UUM102.6 102.6 102.6
30 60 90
3.5 4.9 6.9
230 240 256
115 120 128
B
7 1.50 1.95 UStiff yellowish brown slightly sandy slightly gravelly CLAY with mudstone.
1.93 1.60 21 UUM103.7 103.7 103.7
15 30 60
3.5 4.9 8.4
196 211 248
98 106 124
B
13 3.50 3.95 UFirm greyish brown slightly sandy slightly gravelly CLAY. 2.14 1.84 17 UU 103.1 35 19.8 84 42 C
General notes: Tests carried out in accordance with BS1377: Part 7: 1990, clause 8 for single stage, clause 9 for multistage tests. Specimens nominally 2:1 height
diameter ratio and tested at a rate of strain of 2%/minute, unless annotated otherwise. See individual test reports for further details.
Legend UU - single stage test ( may be in sets of specimens ) ó3 cell pressure Mode of failure P plastic
UUM - multistage test on a single specimen ó1 - ó3 deviator stress B brittle
suffix R - remoulded or recompacted c u undrained shear strength C compound
QA Ref
UNCONSOLIDATED UNDRAINED TRIAXIAL COMPRESSION TESTS WITHOUT MEASUREMENT OF PORE PRESSURE - SUMMARY OF RESULTS
Project No
D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL
Project Name
UUSUM 1Printed:04/12/2013 14:09
RemarksMODE
At failure / end of stage
BH2
SLR 2Rev 71Mar 12
BH3
BH4
BH5
BH5
DensitySample
Depth (m)No. type
Hole No. Soil Description
Mg/m3
Table
Dia. Height H/DLoad Rate
Time to failure
Mode of failure
UCS
from to mm mm Mg/m3 % kN/min secs MPa
24 14.91 15.27 CS SILTSTONE 86.8 221.0 2.5 2.60 2.5 7.5 254 S 5.35
27 22.96 23.29 CS SILTSTONE 86.1 162.9 1.9 2.61 1.6 10 407 SMS 11.7Outside ISRM Specification
17 5.16 5.34 CSSANDSTONE/SILTSTONE
86.8 140.7 1.6 2.57 1.8 80 449 MS 101Outside ISRM Specification
21 21.26 21.54 CS SILTSTONE 86.3 172.8 2.0 2.60 2.0 10 345 AC 9.83Outside ISRM Specification
17 9.10 9.28 CS SILTSTONE 86.1 115.3 1.3 2.61 1.7 20 304 S 17.4
Notes : Test Specification : International Society for Rock Mechanics, The complete ISRM suggested methods for Rock Characterization Testing and Monitoring, 2007
1 ISRM p87 test 1, water content at 105 ± 3 oC, specimen as received at the laboratory
2 ISRM p86 clause (vii), Caliper method used for determination of bulk volume and derivation of bulk density Mode of failure :
3 ISRM p153 part 1, determination of Uniaxial Compressive Strength ( UCS ) of Rock Materials S - Single shear MS - multiple shear
above notes apply unless annotated otherwise in the remarksAC - Axial cleavage F - Fragmented
Ref
BH1
BH2
BH2
BH4
UNIAXIAL COMPRESSIVE STRENGTH OF ROCK - SUMMARY OF RESULTS
D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL
BH1
RemarksRock Type
Project NameProject No
Specimen
Dimensions2 Bulk
Density2
Sample
Depth (m)No. type
Hole No.
RLR 2Rev 16Aug 11
Water
Content1
Uniaxial Compression3
RUCS 1
Table
Printed:04/12/2013 14:14
LOADP
Typ
e(D
, A, I
, B)
Dire
ctio
n(L
, P o
r U
)
Lnemm
Wmm
Dpsmm
Dps'mm
kN Is Is(50)
BH110.25 - 10.42
22 CS MUDSTONE A U Y 86.6 36.0 34.0 1.50 61.23 0.40 0.44
BH115.94 - 16.24
25 CS MUDSTONE A U Y 86.2 41.0 38.0 2.20 64.58 0.53 0.59
BH119.30 - 19.50
26 CS MUDSTONE A U Y 86.4 43.0 41.0 1.50 67.16 0.33 0.38
BH125.42 - 25.57
28 CS MUDSTONE A U Y 86.6 44.0 41.0 3.50 67.24 0.77 0.88
BH129.08 - 29.24
29 CS MUDSTONE A U Y 86.3 43.0 42.0 3.60 67.93 0.78 0.90
BH26.10 - 6.26
18 CS MUDSTONE A L N 86.7 46.0 44.0 4.00 69.69 0.82 0.96 Laminated
BH218.88 - 19.06
20 CS MUDSTONE A U Y 85.8 42.0 43.0 4.50 68.54 0.96 1.10
BH224.11 - 24.25
22 CS MUDSTONE A U Y 85.7 42.0 41.0 1.20 66.89 0.27 0.31
BH49.10 - 9.28
17 CS SILTSTONE I P Y 43.0 86.4 55.0 53.0 3.40 76.36 0.58 0.71
BH413.32 - 13.44
19 CS MUDSTONE A L N 86.2 41.0 38.0 1.40 64.58 0.34 0.38 Laminated
All specimens tested at as received water content unless shown otherwise
Test TypeD - Diametral, A - Axial, I - Irregular Lump, B - BlockDirection ( U = unknown or random )L - parallel to planes of weaknessP - perpendicular to planes of weaknessDimensions Dps - Distance between platens ( platen separation )Dps' - at failure ( see ISRM note 6 )Lne - Length from platens to nearest free endW - Width of shortest dimension perpendicular to load, P
Point Load IndexMPa
F = (De/50)0.45
De
equi
vale
nt d
iam
eter
,m
m
Fai
lure
Val
id (
Y/N
)
Dimensions
Sam
ple
Typ
e
Sam
ple
Ref
Test Typesee ISRM
Fig 5 and 8
Rock typeRemarks
Spe
cim
en R
ef
Bor
ehol
e
Dep
th, m
Spe
cim
en D
epth
Point Load Index TestISRM:1985
Project No Project Name
D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL
QA Ref
RLR 104Rev 65May 12
PLT 1
Figure
� Printed:04/12/2013 14:12
Dps
P
Lne
Diametral
P
WDps
Axial
P
W
Lne Dps
Block/irregular lump
January 2014 Report No D3155-13 Issue 3.0 Enclosure D
ENCLOSURE D
GEOENVIRONMENTAL LABORATORY TEST RESULTS
ESG Scientifics Report EFS/136756M
ESG Scientifics Report EFS/136757M
ESG Scientifics Report EFS/136819M
ESG Scientifics Report EXR/167084
ESG Scientifics Report EXR/167086
ESG Scientifics Report EXR/167224
ESG Scientifics Report EXR/169647
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Clough Hall Technology School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 02-Dec-2013Declan Burns Operations Director
Laboratory and Analytical Business
Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)
(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.
ESG accepts no responsibility for any sampling not carried out by our personnel.
02-Dec-2013
The 4 samples described in this report were registered for analysis by ESG on 19-Nov-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/136756M (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 7)Table of PCB Congener (12) Results (Page 8)Table of GRO Results (Page 9)Table of TPH (Si) banding (std) (Page 10)GC-FID Chromatograms (Pages 11 to 18)Table of VOC (HSA) Results (Pages 19 to 22)Table of Asbestos Screening Results (Page 23)Analytical and Deviating Sample Overview (Pages 24 to 25)Table of Additional Report Notes (Page 26)Table of Method Descriptions (Page 27)Table of Report Notes (Page 28)Table of Sample Descriptions (Appendix A Page 1 of 1)
Tests marked '^' have been subcontracted to another laboratory.
All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 1 of 28
Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL
Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 16 1 0.1 36Accreditation Code: UM U UM UM UM UM UM UM UM UM UM UM UM UM UM
LAB
ID N
umber C
L/
Client Sample Description
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
1328802 WS4 ES 6 0.80 Req <0.5 0.4 5 <0.20 11.6 12.9 12.0 <0.5 0.8 12.0 0.8 30.7 101 0.78 16400
1328803 WS4 ES 14 3.70 Req 1.6 5.7 33.0 0.57 45.5 389.5 961.9 <0.51 5.2 45.6 1 190.9 202 1.11 140000
1328804 WS5 ES 2 0.10 Req <0.5 1 8.5 1.75 13.2 39.9 51.8 <0.50 2.4 19.4 1.5 80.6 478 1.2 22700
1328805 WS5 ES 4 0.60 Req <0.5 0.4 8.0 0.33 13.6 24.1 24.5 <0.5 0.6 29.4 0.8 70.9 266 1.07 45900
Contact
Date Printed
Report Number EFS/136756M
Table Number 1
Fax +44 (0) 1283 554422
Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
02-Dec-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 2 of 28
Units : mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg mg/kg µg/kg % % M/M mg/kgMethod Codes : ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 ICPMSS KONECR PCBUSECDAR TSBRE1 WSLM59 PAHMSUS
Method Reporting Limits : 10 0.5 0.5 0.2 10 0.5 0.6 0.1 0.005 0.02Accreditation Code: UM UM UM U U U N N N N N
LAB
ID N
umber C
L/
Client Sample Description
SO
4-- (H2O
sol) mg/l
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
VO
C H
SA
-GC
MS
Chrom
ium (III)
Vanadium
(MS
)
Chrom
ium vi:
PC
B-12 C
ongeners Analysis
Total S
ulphur.
Total O
rganic Carbon
PA
H (16) by G
CM
S
1328802 WS4 ES 6 0.80 197 8.0 <0.6 <0.6 NAIIS 11.1 Req Req <11.6 15.8 <0.1 Req 0.110 3.48 Req
1328803 WS4 ES 14 3.70 1060 5.3 <0.6 <0.6 NAIIS 19.2 Req Req <45.5 96.6 <0.1 Req 0.562 >25 Req
1328804 WS5 ES 2 0.10 456 8.5 <0.5 <0.5 NAIIS 8.3 Req Req <13.2 25.6 <0.1 0.915 5.69 Req
1328805 WS5 ES 4 0.60 480 6.9 <0.6 <0.6 NAIIS 9.6 Req Req <13.6 18.6 <0.1 0.436 3.04 Req
Contact
Date Printed
Report Number EFS/136756M
Table Number 1
Fax +44 (0) 1283 554422
Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
02-Dec-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 3 of 28
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS4 ES 6 0.80 Job Number: S13_6756MLIMS ID Number: CL1328802 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13
Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.22 0.15 92 UMPyrene 129-00-0 7.52 0.13 99 UMBenzo[a]anthracene 56-55-3 9.24 0.09 79 UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.80 0.10 85 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.55 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 115 2-Fluorobiphenyl 109Acenaphthene-d10 112 Terphenyl-d14 76Phenanthrene-d10 114Chrysene-d12 109Perylene-d12 114
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 4 of 28
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS4 ES 14 3.70 Job Number: S13_6756MLIMS ID Number: CL1328803 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13
Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.83 0.30 97 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 7.22 0.35 97 UMPyrene 129-00-0 7.52 0.31 80 UMBenzo[a]anthracene 56-55-3 9.23 0.27 99 UMChrysene 218-01-9 9.29 0.26 96 UMBenzo[b]fluoranthene 205-99-2 10.79 0.32 79 UMBenzo[k]fluoranthene 207-08-9 10.83 0.14 82 UMBenzo[a]pyrene 50-32-8 11.22 0.21 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.63 0.17 75 UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 12.96 0.14 94 UMTotal (USEPA16) PAHs - - < 3.06 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 111 2-Fluorobiphenyl 110Acenaphthene-d10 110 Terphenyl-d14 76Phenanthrene-d10 109Chrysene-d12 110Perylene-d12 118
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 5 of 28
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS5 ES 2 0.10 Job Number: S13_6756MLIMS ID Number: CL1328804 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13
Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2213PAH.GC5\ Matrix: SoilDilution: 5.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.38 1.37 98 UMAcenaphthylene 208-96-8 4.43 1.60 99 UAcenaphthene 83-32-9 4.55 3.69 99 UMFluorene 86-73-7 4.95 3.00 85 UMPhenanthrene 85-01-8 5.83 41.10 99 UMAnthracene 120-12-7 5.88 20.40 93 UFluoranthene 206-44-0 7.22 178.00 98 UMPyrene 129-00-0 7.51 158.00 99 UMBenzo[a]anthracene 56-55-3 9.23 86.50 96 UMChrysene 218-01-9 9.28 66.70 99 UMBenzo[b]fluoranthene 205-99-2 10.78 88.50 99 UMBenzo[k]fluoranthene 207-08-9 10.82 35.10 95 UMBenzo[a]pyrene 50-32-8 11.22 76.60 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.62 46.30 89 UMDibenzo[a,h]anthracene 53-70-3 12.65 8.02 95 UMBenzo[g,h,i]perylene 191-24-2 12.94 43.00 99 UMTotal (USEPA16) PAHs - - 857.84 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 111 2-Fluorobiphenyl 98Acenaphthene-d10 110 Terphenyl-d14 72Phenanthrene-d10 120Chrysene-d12 142Perylene-d12 146
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 6 of 28
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS5 ES 4 0.60 Job Number: S13_6756MLIMS ID Number: CL1328805 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13
Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.43 0.20 94 UAcenaphthene 83-32-9 4.55 0.38 98 UMFluorene 86-73-7 4.94 0.35 95 UMPhenanthrene 85-01-8 5.83 6.58 98 UMAnthracene 120-12-7 5.88 3.88 96 UFluoranthene 206-44-0 7.22 27.90 98 UMPyrene 129-00-0 7.51 24.20 100 UMBenzo[a]anthracene 56-55-3 9.23 14.20 96 UMChrysene 218-01-9 9.28 10.06 98 UMBenzo[b]fluoranthene 205-99-2 10.78 11.80 98 UMBenzo[k]fluoranthene 207-08-9 10.82 4.21 94 UMBenzo[a]pyrene 50-32-8 11.22 10.82 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.61 6.36 89 UMDibenzo[a,h]anthracene 53-70-3 12.65 1.04 96 UMBenzo[g,h,i]perylene 191-24-2 12.95 4.77 98 UMTotal (USEPA16) PAHs - - < 126.84 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 109 2-Fluorobiphenyl 105Acenaphthene-d10 110 Terphenyl-d14 74Phenanthrene-d10 114Chrysene-d12 120Perylene-d12 136
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 7 of 28
Customer and Site Details: ESG Southam: Clough Hall Technology School Matrix:Job Number: S13_6756M Date Booked in:QC Batch Number: 130280 Date Extracted:Directory: 1122PCB.GC8 Date Analysed:Method: UltrasonicAccreditation code: N
Concentration, (µg/kg)
Sample ID Customer ID PCB 81 PCB 77 PCB 123 PCB 118 PCB 114 PCB 105 PCB 126 PCB 167 PCB 156 PCB 157 PCB 169 PCB 189* CL1328802 WS4 ES 6 0.80 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6* CL1328803 WS4 ES 14 3.70 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2
25-Nov-13
Polychlorinated Biphenyls (congeners)
Soil19-Nov-1321-Nov-13
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 8 of 28
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: Soil
Job Number: s13_6756 Date Booked in: 19-Nov-13
Directory: D:\TES\DATA\Y2013\1127HSA_GC12\112713 2013-11-27 13-49-22\035F3501.D Date extracted: 26-Nov-13
Method: Headspace GCFID Date Analysed: 28-Nov-13, 00:59:12Accreditation Code: UM
y * Sample data with an asterisk are not UKAS accredit ed.
Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
CL1328802 WS4 ES 6 0.80 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328803 WS4 ES 14 3.70 <0.012 0.038 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328804 WS5 ES 2 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328805 WS5 ES 4 0.60 <0.011 0.244 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 0.3
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 9 of 28
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: SoilJob Number: S13_6756 Separation: Silica gel Date Booked in: 19-Nov-13QC Batch Number: 130923 Eluents: Hexane, DCM Date Extracted: 21-Nov-13Directory: D:\TES\DATA\Y2013\02\1122TPH_GC3\066B1201.D Date Analysed: 22-Nov-13Method: Ultra Sonic
This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics
CL1328802 WS4 ES 6 0.80 <4 <4 <4 <4 <4 <4 <4 <4 <9.85 <9.85 <22 <22
CL1328803 WS4 ES 14 3.70 <5 <5 <5 <5 <5 <5 <5 5.9 40.6 31.2 47.8 42.7
CL1328804 WS5 ES 2 0.10 <4 <4 <4 <4 18.3 34.7 44.8 482 133 2240 253 2900
CL1328805 WS5 ES 4 0.60 <4 <4 <4 <4 8.84 12.8 9.52 88.6 <9.69 312 32.9 427
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 10 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328802ALI Job Number: S13_6756MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 6 0.80Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\013F0901.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1122TPH_GC3\013F0901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 11 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328802ARO Job Number: S13_6756MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 6 0.80Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\063B0901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (1122TPH_GC3\063B0901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 12 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328803ALI Job Number: S13_6756MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 14 3.70Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\014F1001.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1122TPH_GC3\014F1001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 13 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328803ARO Job Number: S13_6756MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 14 3.70Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\064B1001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
700
FID2 B, (1122TPH_GC3\064B1001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 14 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328804ALI Job Number: S13_6756MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 2 0.10Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\015F1101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (1122TPH_GC3\015F1101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 15 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328804ARO Job Number: S13_6756MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 2 0.10Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\065B1101.D
min0 1 2 3 4 5
pA
0
500
1000
1500
2000
2500
3000
FID2 B, (1122TPH_GC3\065B1101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 16 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328805ALI Job Number: S13_6756MMultiplier: 15.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\016F1201.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1122TPH_GC3\016F1201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 17 of 28
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328805ARO Job Number: S13_6756MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\066B1201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1122TPH_GC3\066B1201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 18 of 28
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS4 ES 6 0.80 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328802 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 13
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 4 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 11 88 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 10 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 92 Toluene-d8 98
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 89Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 801,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 64m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 52Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 19 of 28
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS4 ES 14 3.70 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328803 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 14
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 62 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 11 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 87 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 80 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 62Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 461,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 10Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 20 of 28
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 2 0.10 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328804 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 15
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 9 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 13 M UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 11 90 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 23 61 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 85 Dibromofluoromethane 1091,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 84 Toluene-d8 88
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 63Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.98 491,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 36m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 13Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 21 of 28
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 4 0.60 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328805 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 16
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.79 3 M UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 2.17 6 M UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 6 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 3 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 33 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 650 97 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 92 86 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 73 Dibromofluoromethane 1071,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 66 Toluene-d8 84
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 36Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 201,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 13m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.26 4Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 22 of 28
Page 1 of 1
Report No:
Report Date: 28/11/2013Project Number:
Sample Number
Sample Date
Sample Location Test DateTotal Sample Dry Weight
(g)
Weight of <2mm
Fraction (g)
Asbestos(g) in >8mm+>2mm
Asbestos(g) in <2mm
% Asbestos by weight of Total Dried Sample
CL/1328802 WS4 0.80 28/11/2013 Screen OnlyCL/1328803 WS4 3.70 28/11/2013 Screen OnlyCL/1328804 WS5 0.10 28/11/2013 Screen OnlyCL/1328805 WS5 0.60 28/11/2013 Screen Only
Name: Louise JamesAuthorised Signatory:
Position: Lab Project Manager
Sampling has been carried out by a third party
For the attention of:
Address:
ESG Environmental Chemistry
ANO-0488-07139Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent
Client:
Detection limit of Method SCI-ASB-020 is 0.001%
ESG Asbestos Limited Certificate of Analysis for Asbestos in Soils
ESG Southam
Asbestos Fibre Types Identified
ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS
S136756Clough Hall Technology SchoolSite Address:
NAIISNAIIS
NAIISNAIIS
The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.
NAACR = Not Analysed at Clients Request NAIIS = No As bestos Identified in Sample (Screens Only)
NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys
1089
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 23 of 28
SOIL Analysis S136756
CustomerSiteReport No S136756
MethodID
CA
LC_C
R3
CE
N Leachate
CustS
erv
GR
OH
SA
ICP
BO
R
ICP
MS
S
ICP
SO
IL
ICP
WS
S
KO
NE
CR
MC
ertS
PA
HM
SU
S
PC
BU
SE
CD
AR
ID Number Description Sampled
Chrom
ium (III)
CE
N Leac(P
)1
Report B
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
SO
4-- (H2O
sol) mg/l
Chrom
ium vi:
MC
ertS A
nalysis
PA
H (16) by G
CM
S
PC
B-12 C
ongeners Analysis
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
CL/1328802 WS4 0.80 DCL/1328803 WS4 3.70 DCL/1328804 WS5 0.10 DCL/1328805 WS5 0.60 D
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
Clough Hall Technology School Date Logged 19-Nov-2013
Report Due 29-Nov-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S37808
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 24 of 28
SOIL Analysis S136756
CustomerSiteReport No S136756
MethodID
PH
SO
IL
SF
AP
I
Sub002a
TM
SS
TP
HU
SS
I
TS
BR
E1
VO
CH
SA
S
WS
LM59
ID Number Description Sampled
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
Total S
ulphur.
VO
C H
SA
-GC
MS
Total O
rganic Carbon
���� ���� ���� ���� ���� ���� ����
CL/1328802 WS4 0.80 DCL/1328803 WS4 3.70 DCL/1328804 WS5 0.10 DCL/1328805 WS5 0.60 D
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
Clough Hall Technology School Date Logged 19-Nov-2013
Report Due 29-Nov-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S37808
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 25 of 28
Report Number : EFS/136756
Method Code
Sample IDThe following information should be taken into consideration when using the
data contained within this report
VOCHSAS CL/1328803
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328804
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328805
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
Additional Report Notes
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136756M Ver. 1Page 26 of 28
Matrix MethodID Analysis Basis
Method Description
Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium
Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID
Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection
Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS
Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection
Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection
Soil PCBUSECDAR As Received Determination of Polychlorinated Biphenyl (PCB) congeners/aroclors by hexane/acetone extraction followed by GCECD detection
Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on
oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil
with GCFID detection including quantitation of Aromatic and Aliphatic fractions.
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS
Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection
Report Number: EFS/136756
Method Descriptions
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 27 of 28
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 28 of 28
Client : ESG Southam
Site : Clough Hall Technology School
Report Number : S13_6756M
Note: major constituent in upper case
Lab ID Number Client ID
CL/1328802 WS4 ES 6 0.80CL/1328803 WS4 ES 14 3.70CL/1328804 WS5 ES 2 0.10CL/1328805 WS5 ES 4 0.60
Sample Descriptions
Grey Stone SILT Grey Stone SILT
Description
Brown Stone SILT Grey Stone SILT
Appendix A Page 1 of 1 END OF REPORT
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Clough Hall Technology School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 02-Dec-2013Declan Burns Operations Director
Laboratory and Analytical Business
Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)
(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.
ESG accepts no responsibility for any sampling not carried out by our personnel.
02-Dec-2013
The 15 samples described in this report were registered for analysis by ESG on 19-Nov-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/136757M (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 18)Table of PCB Congener (12) Results (Page 19)Table of GRO Results (Page 20)Table of TPH (Si) banding (std) (Page 21)GC-FID Chromatograms (Pages 22 to 51)Table of VOC (HSA) Results (Pages 52 to 66)Table of Asbestos Screening Results (Page 67)Analytical and Deviating Sample Overview (Pages 68 to 69)Table of Additional Report Notes (Page 70)Table of Method Descriptions (Page 71)Table of Report Notes (Page 72)Table of Sample Descriptions (Appendix A Page 1 of 1)
Tests marked '^' have been subcontracted to another laboratory.
All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 1 of 72
Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL
Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 16 1 0.1 36Accreditation Code: UM U UM UM UM UM UM UM UM UM UM UM UM UM UM
LAB
ID N
umber C
L/
Client Sample Description
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
1328806 BH2 ES 7 0.5 Req 0.6 0.6 6.5 0.33 12.4 18.7 25.5 <0.53 0.6 20.9 <0.5 69.3 665 1.23 42000
1328807 BH2 ES 13 2.0 Req <0.5 0.2 1.3 <0.2 13.8 15.9 9.5 <0.50 <0.5 22.0 <0.5 50.1 250 0.95 34600
1328808 BH4 ES 3 0.2 Req <0.5 1.5 14.8 0.37 35.1 63.7 79.8 <0.50 4.9 23.6 <0.5 32.4 338 1.14 134000
1328809 BH5 ES 4 0.5 Req <0.5 0.4 7.3 <0.21 17.9 20.3 23.4 <0.53 0.7 17.3 <0.5 58.3 152 1.09 64600
1328810 BH5 ES 9 2.0 Req <0.5 0.4 6.9 <0.21 17.0 23.5 33.2 <0.52 0.5 26.6 0.5 71.9 153 1.16 45900
1328811 BH5 ES 12 3.0 Req <0.5 0.4 8.1 <0.21 14.8 16.9 15.4 <0.5 <0.5 28.4 <0.5 61.4 890 0.97 48700
1328812 TP1 ES 2 0.25 Req 0.9 0.4 7.0 1.11 16.2 19.1 25.9 <0.52 0.6 28.4 0.7 90.4 205 0.93 25800
1328813 TP1 ES 4 0.7 Req <0.6 0.3 5.9 1.52 15.8 16.8 26.0 <0.6 <0.6 16.2 0.8 65.8 225 0.87 20100
1328814 TP2 ES 2 0.2 Req 0.8 1.2 5.4 0.89 39.0 31.2 21.6 <0.5 0.9 12.6 1 78.4 177 1.25 13800
1328815 TP2 ES 4 0.55 Req 2 0.4 6.7 0.29 15.8 14.8 17.7 <0.5 0.9 15.5 2.3 53.0 241 1.90 20000
1328816 WS1 ES 3 0.2 Req <0.5 0.6 12.4 <0.2 15.3 13.2 30.8 <0.5 0.8 15 <0.5 62 133 0.45 29000
1328817 WS2 ES 2 0.2 Req <0.5 0.4 6.8 1.88 17.1 23 21.7 <0.51 2.2 27.9 0.9 117.9 237 0.66 17700
1328818 WS2 ES 6 1.0 Req <0.5 0.8 24.1 0.30 21.1 30.9 37.3 <0.5 2.5 19.8 0.9 47.0 540 0.65 22100
1328819 WS3 ES 1 0.2 Req <0.5 0.8 10.3 0.57 18.0 18.7 38.9 <0.51 1.2 16.1 0.6 75.7 185 0.6 20700
1328820 WS3 ES 5 1.8 Req 0.9 1.1 36.2 0.33 16.2 42.1 45.2 0.52 1.7 48.2 2.4 81 521 1.19 17900
Contact
Date Printed
Report Number EFS/136757M
Table Number 1
Fax +44 (0) 1283 554422
Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
02-Dec-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 2 of 72
Units : mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg mg/kg µg/kg % % M/M mg/kgMethod Codes : ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 ICPMSS KONECR PCBUSECDAR TSBRE1 WSLM59 PAHMSUS
Method Reporting Limits : 10 0.5 0.5 0.2 10 0.5 0.6 0.1 0.005 0.02Accreditation Code: UM UM UM U U U N N N N N
LAB
ID N
umber C
L/
Client Sample Description
SO
4-- (H2O
sol) mg/l
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
VO
C H
SA
-GC
MS
Chrom
ium (III)
Vanadium
(MS
)
Chrom
ium vi:
PC
B-12 C
ongeners Analysis
Total S
ulphur.
Total O
rganic Carbon
PA
H (16) by G
CM
S
1328806 BH2 ES 7 0.5 344 8.1 <0.6 <0.6 NAIIS 18.0 Req Req <12.4 21.3 <0.1 0.069 2.25 Req
1328807 BH2 ES 13 2.0 613 7.2 <0.5 <0.5 NAIIS 7.6 Req Req <13.8 15.6 <0.1 0.089 1.26 Req
1328808 BH4 ES 3 0.2 356 8.6 <0.6 <0.6 CH 10.3 Req Req <35.1 78.1 <0.1 0.182 2.09 Req
1328809 BH5 ES 4 0.5 114 7.8 <0.6 <0.6 NAIIS 17.5 Req Req <17.9 26.8 <0.1 0.033 1.44 Req
1328810 BH5 ES 9 2.0 159 6.3 <0.6 <0.6 NAIIS 15.7 Req Req <17.0 22.5 <0.1 0.026 1.42 Req
1328811 BH5 ES 12 3.0 231 6.2 <0.6 <0.6 NAIIS 15.7 Req Req <14.8 20.2 <0.1 0.039 1.19 Req
1328812 TP1 ES 2 0.25 349 8.3 <0.6 <0.6 NAIIS 16.3 Req Req <16.2 21.0 <0.1 Req 0.075 2.38 Req
1328813 TP1 ES 4 0.7 193 8.4 <0.6 <0.6 NAIIS 20.4 Req Req <15.8 18.3 <0.1 0.060 1.79 Req
1328814 TP2 ES 2 0.2 567 8.4 <0.6 <0.6 NAIIS 9.8 Req Req <39.0 32.2 <0.1 Req 0.198 2.78 Req
1328815 TP2 ES 4 0.55 2390 8.6 <0.6 <0.6 NAIIS 15.9 Req Req <15.8 19.9 <0.1 0.516 3.15 Req
1328816 WS1 ES 3 0.2 188 8.4 <0.6 <0.6 NAIIS 14.5 Req Req <15.3 21 <0.1 0.040 1.86 Req
1328817 WS2 ES 2 0.2 204 8.6 <0.6 <0.6 NAIIS 13.2 Req Req <17.1 30.0 <0.1 0.328 7.03 Req
1328818 WS2 ES 6 1.0 152 7.5 <0.6 <0.6 NAIIS 22.0 Req Req <21.1 24.3 <0.1 0.163 7.31 Req
1328819 WS3 ES 1 0.2 104 7.9 <0.6 <0.6 NAIIS 9.8 Req Req <18.0 22.1 <0.1 0.072 3.68 Req
1328820 WS3 ES 5 1.8 242 7.9 <0.6 <0.6 NAIIS 9.8 Req Req <16.2 28.0 <0.1 0.303 12.50 Req
Contact
Date Printed
Report Number EFS/136757M
Table Number 1
Fax +44 (0) 1283 554422
Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
02-Dec-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 3 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH2 ES 7 0.5 Job Number: S13_6757MLIMS ID Number: CL1328806 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.56 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 100 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 74Phenanthrene-d10 98Chrysene-d12 106Perylene-d12 115
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 4 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH2 ES 13 2.0 Job Number: S13_6757MLIMS ID Number: CL1328807 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.18 97 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 102Acenaphthene-d10 101 Terphenyl-d14 74Phenanthrene-d10 99Chrysene-d12 106Perylene-d12 113
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 5 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH4 ES 3 0.2 Job Number: S13_6757MLIMS ID Number: CL1328808 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.39 0.43 98 UAcenaphthene 83-32-9 4.51 0.86 97 UMFluorene 86-73-7 4.91 0.90 92 UMPhenanthrene 85-01-8 5.78 12.00 99 UMAnthracene 120-12-7 5.83 4.18 97 UFluoranthene 206-44-0 7.16 27.00 98 UMPyrene 129-00-0 7.46 24.60 100 UMBenzo[a]anthracene 56-55-3 9.17 16.00 95 UMChrysene 218-01-9 9.22 12.00 98 UMBenzo[b]fluoranthene 205-99-2 10.72 18.20 100 UMBenzo[k]fluoranthene 207-08-9 10.76 6.56 96 UMBenzo[a]pyrene 50-32-8 11.15 16.30 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.55 11.00 89 UMDibenzo[a,h]anthracene 53-70-3 12.58 2.08 93 UMBenzo[g,h,i]perylene 191-24-2 12.87 9.52 99 UMTotal (USEPA16) PAHs - - < 161.74 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 100 Terphenyl-d14 73Phenanthrene-d10 101Chrysene-d12 114Perylene-d12 129
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 6 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 4 0.5 Job Number: S13_6757MLIMS ID Number: CL1328809 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.55 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 102Acenaphthene-d10 99 Terphenyl-d14 75Phenanthrene-d10 98Chrysene-d12 105Perylene-d12 116
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 7 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 9 2.0 Job Number: S13_6757MLIMS ID Number: CL1328810 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.52 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 98Chrysene-d12 107Perylene-d12 115
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 8 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 12 3.0 Job Number: S13_6757MLIMS ID Number: CL1328811 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.52 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 102 2-Fluorobiphenyl 102Acenaphthene-d10 101 Terphenyl-d14 75Phenanthrene-d10 99Chrysene-d12 107Perylene-d12 116
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 9 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP1 ES 2 0.25 Job Number: S13_6757MLIMS ID Number: CL1328812 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.37 97 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 7.17 0.11 95 UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.82 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 99Chrysene-d12 107Perylene-d12 115
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 10 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP1 ES 4 0.7 Job Number: S13_6757MLIMS ID Number: CL1328813 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.18 95 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.68 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 105Acenaphthene-d10 99 Terphenyl-d14 77Phenanthrene-d10 97Chrysene-d12 105Perylene-d12 113
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 11 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP2 ES 2 0.2 Job Number: S13_6757MLIMS ID Number: CL1328814 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.16 0.17 95 UMPyrene 129-00-0 7.46 0.23 97 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.72 0.16 77 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.16 0.09 83 UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.71 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 100Chrysene-d12 110Perylene-d12 127
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 12 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP2 ES 4 0.55 Job Number: S13_6757MLIMS ID Number: CL1328815 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.52 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 102Acenaphthene-d10 98 Terphenyl-d14 73Phenanthrene-d10 93Chrysene-d12 94Perylene-d12 108
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 13 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS1 ES 3 0.2 Job Number: S13_6757MLIMS ID Number: CL1328816 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 4.51 0.11 99 UMFluorene 86-73-7 4.91 0.11 84 UMPhenanthrene 85-01-8 5.78 1.02 98 UMAnthracene 120-12-7 5.84 0.32 88 UFluoranthene 206-44-0 7.17 1.01 97 UMPyrene 129-00-0 7.46 0.75 100 UMBenzo[a]anthracene 56-55-3 9.18 0.37 96 UMChrysene 218-01-9 9.23 0.28 96 UMBenzo[b]fluoranthene 205-99-2 10.73 0.27 79 UMBenzo[k]fluoranthene 207-08-9 10.76 0.13 93 UMBenzo[a]pyrene 50-32-8 11.16 0.20 93 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.14 76 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.89 0.13 70 UMTotal (USEPA16) PAHs - - < 5.13 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 91 2-Fluorobiphenyl 104Acenaphthene-d10 93 Terphenyl-d14 73Phenanthrene-d10 89Chrysene-d12 89Perylene-d12 102
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 14 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS2 ES 2 0.2 Job Number: S13_6757MLIMS ID Number: CL1328817 Date Booked in: 19-Nov-13QC Batch Number: 0 Date Extracted: 00-Jan-00
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2913PAHMS14\ Matrix: SoilDilution: 5.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.41 2.20 96 UMAcenaphthylene 208-96-8 4.46 0.86 98 UAcenaphthene 83-32-9 4.59 4.12 96 UMFluorene 86-73-7 4.98 3.68 98 UMPhenanthrene 85-01-8 5.84 56.80 99 UMAnthracene 120-12-7 5.89 16.80 99 UFluoranthene 206-44-0 7.20 136.00 95 UMPyrene 129-00-0 7.49 119.00 91 UMBenzo[a]anthracene 56-55-3 9.17 56.10 98 UMChrysene 218-01-9 9.22 49.20 100 UMBenzo[b]fluoranthene 205-99-2 10.70 56.80 97 UMBenzo[k]fluoranthene 207-08-9 10.73 23.30 96 UMBenzo[a]pyrene 50-32-8 11.13 48.70 95 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.50 32.00 91 UMDibenzo[a,h]anthracene 53-70-3 12.53 5.10 91 UMBenzo[g,h,i]perylene 191-24-2 12.81 28.70 96 UMTotal (USEPA16) PAHs - - 639.24 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 93Acenaphthene-d10 100 Terphenyl-d14 64Phenanthrene-d10 99Chrysene-d12 97Perylene-d12 100
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 15 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS2 ES 6 1.0 Job Number: S13_6757MLIMS ID Number: CL1328818 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.76 98 UMAnthracene 120-12-7 5.84 0.18 90 UFluoranthene 206-44-0 7.16 1.05 98 UMPyrene 129-00-0 7.46 0.81 100 UMBenzo[a]anthracene 56-55-3 9.17 0.59 92 UMChrysene 218-01-9 9.23 0.47 98 UMBenzo[b]fluoranthene 205-99-2 10.73 0.50 90 UMBenzo[k]fluoranthene 207-08-9 10.76 0.19 94 UMBenzo[a]pyrene 50-32-8 11.16 0.41 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.29 94 UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.21 70 UMTotal (USEPA16) PAHs - - < 5.99 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 99 Terphenyl-d14 76Phenanthrene-d10 100Chrysene-d12 112Perylene-d12 129
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 16 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS3 ES 1 0.2 Job Number: S13_6757MLIMS ID Number: CL1328819 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.64 98 UMAnthracene 120-12-7 5.84 0.16 88 UFluoranthene 206-44-0 7.16 1.43 98 UMPyrene 129-00-0 7.46 1.19 99 UMBenzo[a]anthracene 56-55-3 9.17 0.71 92 UMChrysene 218-01-9 9.23 0.58 96 UMBenzo[b]fluoranthene 205-99-2 10.73 0.80 93 UMBenzo[k]fluoranthene 207-08-9 10.76 0.29 94 UMBenzo[a]pyrene 50-32-8 11.16 0.63 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.55 0.49 100 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.38 97 UMTotal (USEPA16) PAHs - - < 7.73 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 100 2-Fluorobiphenyl 101Acenaphthene-d10 101 Terphenyl-d14 74Phenanthrene-d10 102Chrysene-d12 115Perylene-d12 132
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 17 of 72
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS3 ES 5 1.8 Job Number: S13_6757MLIMS ID Number: CL1328820 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13
Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.33 0.40 97 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.94 98 UMAnthracene 120-12-7 5.84 0.12 87 UFluoranthene 206-44-0 7.16 0.72 98 UMPyrene 129-00-0 7.46 0.62 98 UMBenzo[a]anthracene 56-55-3 9.17 0.42 94 UMChrysene 218-01-9 9.23 0.34 97 UMBenzo[b]fluoranthene 205-99-2 10.72 0.43 76 UMBenzo[k]fluoranthene 207-08-9 10.76 0.16 79 UMBenzo[a]pyrene 50-32-8 11.16 0.29 96 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.20 96 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.17 99 UMTotal (USEPA16) PAHs - - < 5.23 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 100Acenaphthene-d10 100 Terphenyl-d14 72Phenanthrene-d10 101Chrysene-d12 114Perylene-d12 127
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 18 of 72
Customer and Site Details: ESG Southam: Clough Hall Technology School Matrix:Job Number: S13_6757M Date Booked in:QC Batch Number: 130282 Date Extracted:Directory: 1122PCB.GC8 Date Analysed:Method: UltrasonicAccreditation code: N
Concentration, (µg/kg)
Sample ID Customer ID PCB 81 PCB 77 PCB 123 PCB 118 PCB 114 PCB 105 PCB 126 PCB 167 PCB 156 PCB 157 PCB 169 PCB 189* CL1328812 TP1 ES 2 0.25 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0* CL1328813 TP1 ES 4 0.7 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3
25-Nov-13
Polychlorinated Biphenyls (congeners)
Soil19-Nov-1322-Nov-13
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 19 of 72
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: Soil
Job Number: s13_6757 Date Booked in: 19-Nov-13
Directory: D:\TES\DATA\Y2013\1127HSA_GC12\112713 2013-11-27 13-49-22\026F2601.D Date extracted: 26-Nov-13
Method: Headspace GCFID Date Analysed: 27-Nov-13, 22:07:01Accreditation Code: UM
y * Sample data with an asterisk are not UKAS accredit ed.
Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
CL1328806 BH2 ES 7 0.5 <0.012 0.141 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328807 BH2 ES 13 2.0 <0.011 0.132 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328808 BH4 ES 3 0.2 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328809 BH5 ES 4 0.5 <0.012 0.022 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328810 BH5 ES 9 2.0 <0.012 0.033 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328811 BH5 ES 12 3.0 <0.012 0.058 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328812 TP1 ES 2 0.25 <0.012 0.016 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328813 TP1 ES 4 0.7 <0.013 0.021 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3
CL1328814 TP2 ES 2 0.2 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328815 TP2 ES 4 0.55 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328816 WS1 ES 3 0.2 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328817 WS2 ES 2 0.2 <0.012 0.022 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328818 WS2 ES 6 1.0 <0.013 <0.013 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3
CL1328819 WS3 ES 1 0.2 <0.011 0.080 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1328820 WS3 ES 5 1.8 <0.011 0.251 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 0.3
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 20 of 72
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: SoilJob Number: S13_6757 Separation: Silica gel Date Booked in: 19-Nov-13QC Batch Number: 130939 Eluents: Hexane, DCM Date Extracted: 27-Nov-13Directory: D:\TES\DATA\Y2013\02\1128TPH_GC3\088B4401.D Date Analysed: 28-Nov-13Method: Ultra Sonic
This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics
CL1328806 BH2 ES 7 0.5 <5 <5 <5 <5 <5 <5 <5 <5 <10.68 <10.68 <24 <24
CL1328807 BH2 ES 13 2.0 <4 <4 <4 <4 <4 5.45 <4 8.38 <9.48 17 <22 33.8
CL1328808 BH4 ES 3 0.2 <4 <4 <4 <4 <4 8.09 4.85 97.4 19.6 485 28.2 633
CL1328809 BH5 ES 4 0.5 <5 <5 <5 <5 <5 <5 <5 <5 <10.62 <10.62 <24 <24
CL1328810 BH5 ES 9 2.0 <5 <5 <5 <5 <5 <5 <5 <5 <10.39 <10.39 <24 <24
CL1328811 BH5 ES 12 3.0 <5 <5 <5 <5 <5 <5 <5 <5 <10.39 <10.39 <24 <24
CL1328812 TP1 ES 2 0.25 <5 <5 <5 <5 <5 <5 <5 <5 <10.47 <10.47 <24 <24
CL1328813 TP1 ES 4 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <11.01 <11.01 <25 <25
CL1328814 TP2 ES 2 0.2 <4 <4 <4 <4 <4 <4 17.3 11.4 324 284 404 360
CL1328815 TP2 ES 4 0.55 <5 <5 <5 <5 <5 <5 <5 <5 <10.42 23.1 <24 33.2
CL1328816 WS1 ES 3 0.2 <5 <5 <5 <5 <5 <5 <5 <5 <10.25 <10.25 <23 <23
CL1328817 WS2 ES 2 0.2 <5 <5 <5 <5 11.1 32 53.9 515 619 2590 904 3440
CL1328818 WS2 ES 6 1.0 <5 <5 <5 <5 <5 <5 <5 11.8 <11.23 47.7 <26 67.7
CL1328819 WS3 ES 1 0.2 <4 <4 <4 <4 <4 <4 <4 8.39 <9.71 35.9 <22 50.8
CL1328820 WS3 ES 5 1.8 <4 <4 <4 <4 <4 13.2 <4 22.1 <9.71 51.6 <22 90.7
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 21 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328806ALI Job Number: S13_6757MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 7 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\018F2401.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\018F2401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 22 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328806ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 7 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\074B3001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\074B3001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 23 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328807ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 13 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\019F2501.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\019F2501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 24 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328807ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 13 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\075B3101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\075B3101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 25 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328808ALI Job Number: S13_6757MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\020F2601.D
min0 1 2 3 4 5
pA
0
100
200
300
400
FID1 A, (1128TPH_GC3\020F2601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 26 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328808ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\076B3201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
700
FID2 B, (1128TPH_GC3\076B3201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 27 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328809ALI Job Number: S13_6757MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 4 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\021F2701.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\021F2701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 28 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328809ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 4 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\077B3301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\077B3301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 29 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328810ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 9 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\022F2801.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
FID1 A, (1128TPH_GC3\022F2801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 30 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328810ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 9 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\078B3401.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\078B3401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 31 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328811ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 12 3.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\023F2901.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\023F2901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 32 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328811ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 12 3.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\079B3501.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\079B3501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 33 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328812ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 2 0.25Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\024F3001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
FID1 A, (1128TPH_GC3\024F3001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 34 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328812ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 2 0.25Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\080B3601.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (1128TPH_GC3\080B3601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 35 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328813ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 4 0.7Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\025F3101.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\025F3101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 36 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328813ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 4 0.7Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\081B3701.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\081B3701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 37 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328814ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\026F3201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (1128TPH_GC3\026F3201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 38 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328814ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\082B3801.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\082B3801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 39 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328815ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 4 0.55Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\027F3301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (1128TPH_GC3\027F3301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 40 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328815ARO Job Number: S13_6757MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 4 0.55Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\083B3901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\083B3901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 41 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328816ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\028F3401.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
FID1 A, (1128TPH_GC3\028F3401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 42 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328816ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\084B4001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\084B4001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 43 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328817ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\029F3501.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (1128TPH_GC3\029F3501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 44 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328817ARO Job Number: S13_6757MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\085B4101.D
min0 1 2 3 4 5
pA
0
500
1000
1500
2000
FID2 B, (1128TPH_GC3\085B4101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 45 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328818ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 6 1.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\030F3601.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
FID1 A, (1128TPH_GC3\030F3601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 46 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328818ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 6 1.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\086B4201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\086B4201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 47 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328819ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\031F3701.D
min0 1 2 3 4 5
pA
50
100
150
200
250
300
350
400
FID1 A, (1128TPH_GC3\031F3701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 48 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328819ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\087B4301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\087B4301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 49 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.
Sample ID: CL1328820ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 5 1.8Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\032F3801.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, (1128TPH_GC3\032F3801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 50 of 72
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.
Sample ID: CL1328820ARO Job Number: S13_6757MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 5 1.8Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\088B4401.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (1128TPH_GC3\088B4401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 51 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 128VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 7 0.5 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328806 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 14
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 6 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 59 92 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 33 83 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1111,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 93 Toluene-d8 94
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 84Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 721,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 60m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 31Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 52 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 13 2.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328807 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 26
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 2.12 4 M UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 3 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 1 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 15 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 393 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 26 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 63 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 57 Toluene-d8 84
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 35Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 251,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 15m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 53 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH4 ES 3 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328808 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 27
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 2 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.26 27 M UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 81 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 78 Toluene-d8 95
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 67Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 42m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 22Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 54 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 4 0.5 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328809 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 28
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 12 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 82 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 82 Toluene-d8 96
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 76Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 691,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 67m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 49Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 55 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 9 2.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328810 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 29
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 19 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 56 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 17 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 74 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 71 Toluene-d8 92
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 61Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 41m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 56 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 12 3.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328811 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 30
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 1 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 19 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 50 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 17 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 76 Dibromofluoromethane 1161,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 74 Toluene-d8 95
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 67Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 43m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 57 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP1 ES 2 0.25 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328812 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 31
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 4.06 16 M UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 35 90 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 80 Dibromofluoromethane 1051,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 75 Toluene-d8 91
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 401,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 11Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 58 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP1 ES 4 0.7 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328813 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 32
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 3 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 5 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 40 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 9 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 75 Toluene-d8 92
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 65Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.97 551,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 47m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 59 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP2 ES 2 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328814 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 1
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 3 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 20 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 22 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 18 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 71 Dibromofluoromethane 1101,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 72 Toluene-d8 87
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 421,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 30m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 14Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 60 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP2 ES 4 0.55 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328815 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 2
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 5 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 12 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 11 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 10 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 921,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 72 Toluene-d8 95
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 66Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 541,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 47m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 27Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 61 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS1 ES 3 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328816 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 3
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 6 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 82 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 81 Toluene-d8 96
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 74Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 681,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 62m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 40Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 62 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 2 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328817 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 4
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 9 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 13 M UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 29 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 16 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 69 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 68 Toluene-d8 84
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 46Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 311,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 23m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 63 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 6 1.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328818 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 5
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 3 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 3 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 1201,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 73 Toluene-d8 94
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.97 391,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 8Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 64 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 1 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328819 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 6
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.79 6 M UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 6 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 160 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 23 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 64 Dibromofluoromethane 1281,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 62 Toluene-d8 91
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 45Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 331,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 21m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 65 of 72
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 5 1.8 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328820 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 7
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.78 3 M UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 2.14 7 M UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 4 M UM
Chloroform 67-66-3 4.07 1 M UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 1 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 20 M N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 533 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 51 83 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 42 Dibromofluoromethane 1301,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 41 Toluene-d8 81
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 23Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 151,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 9m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.26 2Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 66 of 72
Page 1 of 1
Report No:
Report Date: 02/12/2013Project Number:
Sample Number
Sample Date
Sample Location Test DateTotal Sample Dry Weight
(g)
Weight of <2mm
Fraction (g)
Asbestos(g) in >8mm+>2mm
Asbestos(g) in <2mm
% Asbestos by weight of Total Dried Sample
CL/1328806 BH2 0.50 29/11/2013 Screen OnlyCL/1328807 BH2 2.00 29/11/2013 Screen OnlyCL/1328808 BH4 0.20 29/11/2013 Screen & IDCL/1328809 BH5 0.50 29/11/2013 Screen OnlyCL/1328810 BH5 2.00 29/11/2013 Screen OnlyCL/1328811 BH5 3.00 29/11/2013 Screen OnlyCL/1328812 TP1 0.25 29/11/2013 Screen OnlyCL/1328813 TP1 0.70 29/11/2013 Screen OnlyCL/1328814 TP2 0.20 29/11/2013 Screen OnlyCL/1328815 TP2 0.55 29/11/2013 Screen OnlyCL/1328816 WS1 0.20 02/12/2013 Screen OnlyCL/1328817 WS2 0.20 02/12/2013 Screen OnlyCL/1328818 WS2 1.00 02/12/2013 Screen OnlyCL/1328819 WS3 0.20 02/12/2013 Screen OnlyCL/1328820 WS3 1.80 02/12/2013 Screen Only
Name: Louise JamesAuthorised Signatory:
Position: Lab Project Manager
Sampling has been carried out by a third party
For the attention of:
Address:
ESG Environmental Chemistry
ANO-0488-07141Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent
Client:
Detection limit of Method SCI-ASB-020 is 0.001%
ESG Asbestos Limited Certificate of Analysis for Asbestos in Soils
ESG Southam
Asbestos Fibre Types Identified
ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS
S136757Clough Hall Technology School
NAIISNAIIS
Site Address:
NAIISNAIIS
Chrysotile(Free Fibres)NAIISNAIIS
NAIISNAIIS
NAIISNAIISNAIISNAIIS
NAIISNAIIS
The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.
NAACR = Not Analysed at Clients Request NAIIS = No As bestos Identified in Sample (Screens Only)
NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys
1089
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 67 of 72
SOIL Analysis S136757
CustomerSiteReport No S136757
MethodID
CA
LC_C
R3
CE
N Leachate
CustS
erv
GR
OH
SA
ICP
BO
R
ICP
MS
S
ICP
SO
IL
ICP
WS
S
KO
NE
CR
MC
ertS
PA
HM
SU
S
PC
BU
SE
CD
AR
ID Number Description Sampled
Chrom
ium (III)
CE
N Leac(P
)1
Report B
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
SO
4-- (H2O
sol) mg/l
Chrom
ium vi:
MC
ertS A
nalysis
PA
H (16) by G
CM
S
PC
B-12 C
ongeners Analysis
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
CL/1328806 BH2 0.50 DCL/1328807 BH2 2.00 DCL/1328808 BH4 0.20 DCL/1328809 BH5 0.50 DCL/1328810 BH5 2.00 DCL/1328811 BH5 3.00 DCL/1328812 TP1 0.25 DCL/1328813 TP1 0.70 DCL/1328814 TP2 0.20 DCL/1328815 TP2 0.55 DCL/1328816 WS1 0.20 DCL/1328817 WS2 0.20 DCL/1328818 WS2 1.00 DCL/1328819 WS3 0.20 DCL/1328820 WS3 1.80 D
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
Clough Hall Technology School Date Logged 19-Nov-2013
Report Due 29-Nov-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S37808.01
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 68 of 72
SOIL Analysis S136757
CustomerSiteReport No S136757
MethodID
PH
SO
IL
SF
AP
I
Sub002a
TM
SS
TP
HU
SS
I
TS
BR
E1
VO
CH
SA
S
WS
LM59
ID Number Description Sampled
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
Total S
ulphur.
VO
C H
SA
-GC
MS
Total O
rganic Carbon
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CL/1328806 BH2 0.50 DCL/1328807 BH2 2.00 DCL/1328808 BH4 0.20 DCL/1328809 BH5 0.50 DCL/1328810 BH5 2.00 DCL/1328811 BH5 3.00 DCL/1328812 TP1 0.25 DCL/1328813 TP1 0.70 DCL/1328814 TP2 0.20 DCL/1328815 TP2 0.55 DCL/1328816 WS1 0.20 DCL/1328817 WS2 0.20 DCL/1328818 WS2 1.00 DCL/1328819 WS3 0.20 DCL/1328820 WS3 1.80 D
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
Clough Hall Technology School Date Logged 19-Nov-2013
Report Due 29-Nov-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S37808.01
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 69 of 72
Report Number : EFS/136757
Method Code
Sample IDThe following information should be taken into consideration when using the
data contained within this report
VOCHSAS CL/1328807
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328812
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328814
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328818
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328819
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1328820
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
Additional Report Notes
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/136757M Ver. 1Page 70 of 72
Matrix MethodID Analysis Basis
Method Description
Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium
Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID
Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection
Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS
Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection
Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection
Soil PCBUSECDAR As Received Determination of Polychlorinated Biphenyl (PCB) congeners/aroclors by hexane/acetone extraction followed by GCECD detection
Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on
oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil
with GCFID detection including quantitation of Aromatic and Aliphatic fractions.
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS
Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection
Report Number: EFS/136757
Method Descriptions
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 71 of 72
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 72 of 72
Client : ESG Southam
Site : Clough Hall Technology School
Report Number : S13_6757M
Note: major constituent in upper case
Lab ID Number Client ID
CL/1328806 BH2 ES 7 0.5CL/1328807 BH2 ES 13 2.0CL/1328808 BH4 ES 3 0.2CL/1328809 BH5 ES 4 0.5CL/1328810 BH5 ES 9 2.0CL/1328811 BH5 ES 12 3.0CL/1328812 TP1 ES 2 0.25CL/1328813 TP1 ES 4 0.7CL/1328814 TP2 ES 2 0.2CL/1328815 TP2 ES 4 0.55CL/1328816 WS1 ES 3 0.2CL/1328817 WS2 ES 2 0.2CL/1328818 WS2 ES 6 1.0CL/1328819 WS3 ES 1 0.2CL/1328820 WS3 ES 5 1.8
Sample Descriptions
Grey Stone SILT
Grey SILT Brown Stone SILT Grey Stone SILT Grey Stone SILT
Brown Stone SILT
Brown SILT Grey Stone SILT
Grey Stone SILT Brown Stone CLAY Brown Stone CLAY Brown Stone SILT Brown Stone CLAY
Description
Brown Stone CLAY Grey SILT
Appendix A Page 1 of 1 END OF REPORT
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: D3155-13 Clough Hall Technology School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 20-Jan-2014Declan Burns Operations Director
Laboratory and Analytical Business
20-Jan-2014
The 3 samples described in this report were registered for analysis by ESG on 07-Jan-2014. This report supersedes any versions previously issued by the laboratory.
TEST REPORTWATER SAMPLE ANALYSIS
Report No. EXR/169647 (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 5)Table of PAH (MS-SIM) (10) Results (Pages 6 to 8)Table of GRO Results (Page 9)Table of TPH (Si) banding (0.01) (Page 10)Table of VOC (HSA) Results (Pages 11 to 13)Table of Subcontracted Analysis Results (Pages 14 to 24)Analytical and Deviating Sample Overview (Pages 25 to 26)Table of Additional Report Notes (Page 27)Table of Method Descriptions (Page 28)Table of Report Notes (Page 29)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Units : pH units mg/l mg/l mg/l mg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF VOCHSAW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW
Method Reporting Limits : 0.01 7 1 0.1 1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
pH units w
Chrom
ium (III)
Total H
ardness as CaC
O3
Chloride as C
l w
Fluoride as F
a
VO
C H
SA
-GC
MS
o
Total S
ulphur as SO
4 (Dissolved) a
Calcium
as Ca (D
issolved) a
Magnesium
as Mg (D
issolved) a
Barium
as Ba (D
issolved) a
Sodium
as Na (D
issolved) a
Nickel as N
i (Dissolved)
Chrom
ium as C
r (Dissolved)
Cadm
ium as C
d (Dissolved)
PA
H G
C-M
S (16) o
Copper as C
u (Dissolved)
1453767 BH1 W 03-Jan-14 8.3 <0.01 308 65 0.2 Req 38 77 28 0.75 28 0.001 0.004 <0.0001 Req <0.001
1453768 BH2 W 03-Jan-14 8.3 <0.01 329 67 0.2 Req 42 84 29 0.59 30 0.005 0.004 <0.0001 Req <0.001
1453769 BH4 W 03-Jan-14 8.0 <0.01 319 19 0.2 Req 54 93 21 0.19 18 0.01 0.003 <0.0001 Req <0.001
Contact
Date Printed
Report Number EXR/169647
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
20-Jan-2014
D3155-13 Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAS
Method Reporting Limits : 0.001 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.05UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Lead as Pb (D
issolved)
Zinc as Z
n (Dissolved)
Manganese as M
n (Dissolved)
Iron as Fe (D
issolved) a
Arsenic as A
s (Dissolved)
Boron as B
(Dissolved) a
Mercury as H
g (Dissolved)
Selenium
as Se (D
issolved)
Vanadium
as V (D
issolved)
Molybdenum
as Mo (D
issolved)
Antim
ony as Sb (D
issolved)
Am
moniacal N
itrogen as N
Nitrate as N
Chrom
ium V
I as Cr
Cyanide (T
otal) as CN
Sulphide as S
1453767 BH1 W 03-Jan-14 <0.001 0.01 0.371 <0.01 <0.001 0.1 <0.0001 <0.001 0.001 <0.001 <0.001 0.5 <0.2 <0.01 <0.02 <0.05
1453768 BH2 W 03-Jan-14 <0.001 0.006 0.43 <0.01 <0.001 0.09 <0.0001 <0.001 0.001 <0.001 <0.001 0.4 <0.2 <0.01 <0.02 <0.05
1453769 BH4 W 03-Jan-14 <0.001 0.012 0.583 <0.01 0.002 0.02 <0.0001 <0.001 0.001 0.002 <0.001 0.3 <0.2 <0.01 <0.02 1.41
Contact
Date Printed
Report Number EXR/169647
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
20-Jan-2014
D3155-13 Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 3 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Units : mg/l ug/l mg/l µg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/lMethod Codes : TPHFID-Si Sub045 ICPWATVAR Sub045 GROHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW
Method Reporting Limits : 0.01 5 0.01 0.1 5 5 5 15 10 5 1 1 1 2 1UKAS Accredited : Yes No No No No Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
TP
H by G
C(S
i) o
^Cyanide (F
ree) 5ug/l
Beryllium
as Be (D
issolved) a
^VO
C Low
Level
GR
O-H
SA
(AA
)
Ethyl B
enzene
Benzene
Toluene
Xylenes
m/p X
ylenes
o Xylene
Benzene
Toluene
Ethyl B
enzene
Xylenes
m/p X
ylenes
1453767 BH1 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 3 <1 4 3
1453768 BH2 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 <1 <1 <2 <1
1453769 BH4 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 <1 <1 <2 <1
Contact
Date Printed
Report Number EXR/169647
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
20-Jan-2014
D3155-13 Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 4 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Units : µg/l mg/l mg/l mg/l mg/lMethod Codes : VOCHSAW PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL
Method Reporting Limits : 1 0.0005 0.0005 0.0005 0.0005UKAS Accredited : Yes No No No No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
o Xylene
Phenol
Cresols
Dim
ethylphenols
Trim
ethylphenols
1453767 BH1 W 03-Jan-14 1 <0.0005 <0.0005 <0.0005 <0.0005
1453768 BH2 W 03-Jan-14 <1 <0.0005 <0.0005 <0.0005 <0.0005
1453769 BH4 W 03-Jan-14 <1 <0.0005 <0.0005 <0.0005 <0.0005
Contact
Date Printed
Report Number EXR/169647
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
20-Jan-2014
D3155-13 Clough Hall Technology School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 5 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH1 W Job Number: W16_9647LIMS ID Number: EX1453767 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14
Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 10.0 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 3.50 14.300 98Acenaphthylene 208-96-8 4.56 0.299 MAcenaphthene 83-32-9 4.68 0.873 80Fluorene 86-73-7 5.08 5.310 94Phenanthrene 85-01-8 5.97 14.900 99Anthracene 120-12-7 6.02 1.060 98Fluoranthene 206-44-0 7.36 4.460 74Pyrene 129-00-0 7.66 3.510 73Benzo[a]anthracene 56-55-3 9.37 1.820 97Chrysene 218-01-9 9.42 1.980 99Benzo[b]fluoranthene 205-99-2 10.91 1.950 80Benzo[k]fluoranthene 207-08-9 10.95 0.761 80Benzo[a]pyrene 50-32-8 11.34 1.550 86Indeno[1,2,3-cd]pyrene 193-39-5 12.74 1.160 74Dibenzo[a,h]anthracene 53-70-3 - < 0.100 -Benzo[g,h,i]perylene 191-24-2 13.08 1.280 53Total (USEPA16) PAHs - - < 55.313 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 81 2-Fluorobiphenyl 71Acenaphthene-d10 77 Terphenyl-d14 54Phenanthrene-d10 78Chrysene-d12 78Perylene-d12 83
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 6 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH2 W Job Number: W16_9647LIMS ID Number: EX1453768 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14
Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 3.50 0.340 86Acenaphthylene 208-96-8 4.55 0.010 MAcenaphthene 83-32-9 4.68 0.082 90Fluorene 86-73-7 5.08 0.109 MPhenanthrene 85-01-8 5.97 0.100 97Anthracene 120-12-7 6.01 0.012 97Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3 - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.753 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 79 2-Fluorobiphenyl 80Acenaphthene-d10 74 Terphenyl-d14 66Phenanthrene-d10 75Chrysene-d12 70Perylene-d12 70
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 7 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH4 W Job Number: W16_9647LIMS ID Number: EX1453769 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14
Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 1.4 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 3.51 3.700 90Acenaphthylene 208-96-8 4.56 0.106 MAcenaphthene 83-32-9 4.68 0.703 81Fluorene 86-73-7 5.08 1.180 89Phenanthrene 85-01-8 5.97 1.730 97Anthracene 120-12-7 6.01 0.216 96Fluoranthene 206-44-0 7.36 0.612 91Pyrene 129-00-0 7.66 0.870 97Benzo[a]anthracene 56-55-3 9.37 0.389 88Chrysene 218-01-9 9.42 0.387 90Benzo[b]fluoranthene 205-99-2 10.91 0.531 75Benzo[k]fluoranthene 207-08-9 10.95 0.235 76Benzo[a]pyrene 50-32-8 11.34 0.450 99Indeno[1,2,3-cd]pyrene 193-39-5 12.74 0.306 98Dibenzo[a,h]anthracene 53-70-3 - < 0.014 -Benzo[g,h,i]perylene 191-24-2 13.08 0.352 59Total (USEPA16) PAHs - - < 11.781 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 79 2-Fluorobiphenyl 79Acenaphthene-d10 76 Terphenyl-d14 60Phenanthrene-d10 77Chrysene-d12 77Perylene-d12 78
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 8 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : D3155-13 Clough Hall Technology School Matrix: Water
Job Number: w16_9647 Date Booked in: 07-Jan-14
Directory: D:\TES\DATA\Y2014\0112HSA_GC12\011214 2014-01-12 11-42-47\128B2801.D Date extracted: 10-Jan-14
Method: Headspace GCFID Date Analysed: 12-Jan-14, 21:45:10
y * Sample data with an asterisk are not UKAS accredit ed.
Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
* EX1453767 BH1 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
* EX1453768 BH2 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
* EX1453769 BH4 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Page 9 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : D3155-13 Clough Hall Technology School Matrix: WaterJob Number: W16_9647 Separation: Silica gel Date Booked in: 07-Jan-14QC Batch Number: 140021 Eluents: Hexane, DCM Date Extracted: 09-Jan-14Directory: D:\TES\DATA\Y2014\011314TPH_GC16\011314 2014-01-13 10-20-12\058B0801.D Date Analysed: 13-Jan-14, 12:33:57Method: Bottle
Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics
EX1453767 BH1 W 0.039 0.043 0.038 0.067 0.069 0.226 0.116 0.289 1.24 0.852 1.75 1.63
EX1453768 BH2 W <0.01 <0.01 <0.01 0.014 <0.01 0.036 <0.01 0.012 <0.01 0.013 <0.01 0.08
EX1453769 BH4 W <0.01 <0.01 0.095 0.115 1.09 0.566 1.9 0.662 0.778 0.286 3.88 1.65
Page 10 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Volatile Organic Compounds by HSA-GCMS
UKAS accredited?: NoCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH1 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453767 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 28
Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l
Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -
Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 5.47 6 M2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 - < 1 -Chloroform 67-66-3 3.31 4 86 sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 4.41 3 82trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 57 Dibromofluoromethane 120Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.78 67 Toluene-d8 70
Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.93 29 Bromofluorobenzene 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.74 6m and p-Xylene 108-38-3/106-42-3 5.02 3 Mo-Xylene 95-47-6 5.15 1 MNote: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.
Page 11 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Volatile Organic Compounds by HSA-GCMS
UKAS accredited?: YesCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH2 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453768 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 29
Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l
Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -
Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 - < 1 -2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 - < 1 -Chloroform 67-66-3 - < 1 - sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 - < 1 -trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 100 Dibromofluoromethane 109Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.77 100 Toluene-d8 99
Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.92 99 Bromofluorobenzene 1011,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.72 93m and p-Xylene 108-38-3/106-42-3 - < 1 -o-Xylene 95-47-6 - < 1 -Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.
Page 12 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Volatile Organic Compounds by HSA-GCMS
UKAS accredited?: YesCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH4 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453769 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 30
Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l
Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -
Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 - < 1 -2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 5.59 1 88Chloroform 67-66-3 - < 1 - sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 - < 1 -trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 102 Dibromofluoromethane 108Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.77 104 Toluene-d8 98
Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.92 104 Bromofluorobenzene 991,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.72 100m and p-Xylene 108-38-3/106-42-3 - < 1 -o-Xylene 95-47-6 - < 1 -Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.
Page 13 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Louise SmithEnvironmental Scientifics Group
ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ
Dear Louise
Please find attached the results for the batch of 3 samples described below.
Samples Registered on: 09-Jan-2014
Analysis Started on: 10-Jan-2014
Analysis Completed on: 14-Jan-2014
Results for Batch Number 20060742
Your Purchase Order Number: 56037 BEC
You will be invoiced shortly by our accounts department.
If we can be of further assistance then please do not hesitate to contact us.
Yours sincerely
Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and
performance data are available on request. The date of sample analysis is available on request.
The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no
knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were
representative of the need for which the information was required.
The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on
the basis of the analysis or advice or interpretation provided.
William FardonCustomer Services Team Manager
Tel: (0113) 231 [email protected]
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 1 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002686163 Sampled on: 3-Jan-14 @ (Time not supplied)
Comments: W1453767 - BH1
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l
1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,4-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 2 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 3 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Hexachloroethane SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Naphthalene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 4 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002686165 Sampled on: 3-Jan-14 @ (Time not supplied)
Comments: W1453768 - BH2
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l
1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,4-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 5 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 6 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Hexachloroethane SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Naphthalene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 7 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002686166 Sampled on: 3-Jan-14 @ (Time not supplied)
Comments: W1453769 - BH4
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l
1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,3-Trimethylbenzene SX4.06 UKAS0.1 1296ug/l DB, DC
1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2,4-Trimethylbenzene SX1.42 UKAS0.1 1296ug/l DB, DC
1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 8 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Hexachloroethane SX<3 None0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 9 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Naphthalene SX4.33 None0.5 1296ug/l DB, DC
n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC
ELEVATED_MRV : Matrix interference
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 10 of 11
Report ID - 20060742 - 1
Analytical Report
0754
Final Report
Batch description: W169647Reported on:
14-Jan-2014
Method Description Summary for all samples in batch Number 20060742SX I Cyanide - (free) - determined colorimetrically by CF analyser 183
SX O Volatiles - direct aqueous injected; determined by P and T GCMS 1296
Laboratory Site Manager
Simon Padley
All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are
necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be
quoted and will be above the MRV.
Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"
sample was used.
Key to Results Flags:
DB Samples received outside analysis holding times. It is possible that the results may be compromised.
DC Analysis started outside of specified holding time. It is possible that the results may be compromised.
The analysis start date specified is the date of the first test, dates for other analysis are available on request.
Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless
otherwise agreed with Customer Services
Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated
Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard
for testing of soils, none = Methodology not accredited
Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions
END OF TEST REPORT
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 11 of 11
WATER Analysis W169647
CustomerSiteReport No W169647
MethodID
BT
EX
HS
A
Calc_C
R3
Calc_H
D
CU
ST
SE
RV
GR
OH
SA
ICP
MS
W
ICP
WA
TV
AR
ID Number Description Sampled
BT
EX
-HS
A A
nalysis
Chrom
ium (III) (C
ALC
)
Total H
ardness as CaC
O3 (C
ALC
)
Report A
GR
O-H
SA
GC
FID
(AA
)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Sodium
as Na (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1453767 BH1 03/01/14EX/1453768 BH2 03/01/14EX/1453769 BH4 03/01/14
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W64308
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
D3155-13 Clough Hall Technology School Date Logged 07-Jan-2014
Report Due 13-Jan-2014
Page 25 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
WATER Analysis W169647
CustomerSiteReport No W169647
MethodID
ICP
WA
TV
AR
ISE
F
KO
NE
NS
PA
HM
SW
PH
EH
PLC
VL
SF
AP
I
SF
AS
Sub045
TP
HF
ID-S
i
VO
CH
SA
W
WS
LM3
ID Number Description Sampled
Beryllium
as Be (D
issolved) VA
R
Fluoride as F
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
Nitrate as N
(Kone calc)
Chrom
ium V
I. as Cr (K
one)
PA
H G
C-M
S (16)
Phenols by H
PLC
(Low Level)
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
^Cyanide (F
ree) 5ug/l
^VO
C Low
Level
TP
H by G
C(S
i)
BT
EX
Analysis H
SA
GC
-MS
Benzene (µg/l)
Toluene (µg/l)
Ethyl B
enzene (µg/l)
Xylenes (µg/l)
m/p X
ylenes (µg/l)
o Xylene (µg/l)
VO
C H
SA
-GC
MS
pH units
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EX/1453767 BH1 03/01/14EX/1453768 BH2 03/01/14EX/1453769 BH4 03/01/14
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W64308
Accredited to ISO17025
Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.
In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.
D3155-13 Clough Hall Technology School Date Logged 07-Jan-2014
Report Due 13-Jan-2014
Page 26 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Report Number : W/EXR/169647
Method Code
Sample IDThe following information should be taken into consideration when using the
data contained within this report
VOCHSAW EX1453767Due to the matrix effect on the internal standards and surrogates, the sample has been reported as non-UKAS.
Additional Report Notes
Page 27 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Matrix MethodID Analysis Basis
Method Description
Water BTEXHSA As Received Benzene, Toluene, Ethylbenzene, & Xylenes by headspace extraction GCFID quantitation
Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI
Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons
(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using
ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using
ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective
Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane
extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with
colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Water TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in
water by GCFIDWater VOCHSAW As Received Determination of Volatile Organics Compounds by Headspace
GCMSWater WSLM3 As Received Determination of the pH of water samples by pH probe
Report Number: W/EXR/169647
Method Descriptions
Page 28 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 29 of 29Where individual results are flagged see report notes for status.
EXR/169647 Ver. 1
January 2014 Report No D3155-13 Issue 3.0 Enclosure E
ENCLOSURE E
PHOTOGRAPHS
Rotary Core BH1, BH2 and BH4
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH1
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH1
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH1
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH1
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH1
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH2
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH2
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH2
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH2
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH2
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH4
Core Photographs
Notes: CLOUGH HALL TECHNOLOGY SCHOOL
D3155-13Education Funding Agency
Project
Project No.Carried out for
Figure
BH4
Core Photographs
January 2014 Report No D3155-13 Issue 3.0 Enclosure F
ENCLOSURE F
DRAWINGS
Site Location Plan 1
Site Plan 2