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Report No D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL, STOKE-ON- TRENT FACTUAL REPORT ON GROUND INVESTIGATION Carried out for: Education Funding Agency Engineer: Mott MacDonald Ltd January 2014

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Page 1: Report No D3155-13 - apps2.staffordshire.gov.uk

Report No D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL, STOKE-ON-TRENT FACTUAL REPORT ON GROUND INVESTIGATION Carried out for: Education Funding Agency Engineer: Mott MacDonald Ltd January 2014

Page 2: Report No D3155-13 - apps2.staffordshire.gov.uk

www.esg.co.uk Environmental Scientifics Group Limited

Reg office: ESG House, Bretby Business Park, Ashby Road, Burton upon Trent, DE15 0YZ Incorporated in England: 02880501

Issue No Date Details 1.0 December 2013 Draft Report 2.0 January 2014 Second draft ; complete geotechnical testing 3.0 January 2014 Final Report

The title to this report is vested in the Employer named but title to copyright is retained. The Contracts (Rights of Third Parties) Act 1999 does not apply to the contract with the Employer and the provisions of the said Act are hereby excluded.

CLOUGH HALL TECHNOLOGY SCHOOL, STOKE-ON-TRENT FACTUAL REPORT ON GROUND INVESTIGATION

Unit 4, Gainsborough Trading Estate, Leamington Road, Southam, Warwickshire, CV47 1RA, UK

Tel: +44 (0) 1926 819300 Fax: +44 (0) 1926 815030 email: [email protected]

Report No: D3155-13

Date: January 2014

Employer: Education Funding Agency 33 Greycoat Street London SW1P 2QF

Engineer: Mott MacDonald Ltd 35 Newhall Street Birmingham B3 3PU

Page 3: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Page 1 of 7

C O N T E N T S

Page 1 INTRODUCTION 2 2 THE SITE AND GEOLOGY 2 2.1 The Site 2.2 Published Geology 3 FIELDWORK 3 3.1 General 3.2 Exploratory Holes 3.3 Instrumentation and Monitoring 4 LABORATORY TESTING 4 4.1 Geotechnical Testing 4.2 Geoenvironmental Testing REFERENCES 7 ENCLOSURES A EXPLORATORY HOLE RECORDS B INSTRUMENTATION AND MONITORING C GEOTECHNICAL LABORATORY TEST RESULTS D GEOENVIRONMENTAL LABORATORY TEST RESULTS E PHOTOGRAPHS F DRAWINGS

Page 4: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Page 2 of 7

1 INTRODUCTION

In September 2013 Environmental Scientifics Group (ESG) was commissioned by Mott MacDonald

Ltd, on behalf of the Education Funding Agency, to carry out a ground investigation at Clough Hall

Technology School, First Avenue, Kidsgrove, Stoke-on-Trent. The investigation was required to

obtain preliminary geotechnical and geoenvironmental information to assist in the planning and

design of new buildings at the school as part of the Priority Schools Building Programme.

The scope of the investigation, which was specified by Mott MacDonald Ltd, comprised cable

percussion and rotary cored boreholes, windowless sampler boreholes, hand excavated trial pits

and laboratory testing. The investigation was carried out in accordance with the contract

specification, Eurocode 7 and relevant related standards identified below (see also References).

The fieldwork was carried out between the 10th and 24th October 2013.

This report presents the factual records of the fieldwork and laboratory testing undertaken. The

data is also presented separately in digital format following AGS (2005).

2 THE SITE AND GEOLOGY

2.1 The Site

Clough Hall Technology School lies on the south western side of Kidsgrove, see Site Location

Plan in Enclosure F, about 9km north of Stoke-on-Trent and 4km south east of Alsager. The site is

at National Grid reference SJ 836 542.

The school grounds are irregular in shape, with existing residential development to the north, west

and south. First Avenue lies beyond to the south with Fifth Avenue on the western side. The

northern portal of the Harecastle Tunnel on the Trent and Mersey Canal lies on the eastern side.

Existing buildings and hardstanding covers much of the school ground with small grassed areas on

the western side.

2.2 Published Geology

Published geological information covering the area, British Geological Survey (BGS) Sheet 123

'Stoke-on-Trent' and the BGS website, show superficial Glaciofluvial Deposits across the site,

covering the underlying Carboniferous age bedrock. This comprises the Pennine Middle Coal

Page 5: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Page 3 of 7

Measures Formation, a succession of mudstone, siltstone, sandstone and occasional coal,

beneath the eastern and western parts of the site with the Ten-feet Rock, a significant sandstone

bed within the Coal Measures strata. The Bellringer coal seam is believed to subcrop beneath the

eastern side of the site.

3 FIELDWORK

3.1 General

The fieldwork was carried out in general accordance with BS 5930+A2 (2010), BS EN 1997-2

(2007) and BS EN ISO 22475-1 (2006).

The exploratory hole locations were selected by Mott MacDonald Ltd and set out from local

features. The co-ordinates and reduced levels were surveyed by ESG to National Grid and

Ordnance Datum. The exploratory hole locations are shown on the Site Plan in Enclosure F.

3.2 Exploratory Holes

The exploratory holes are listed in the following table.

SUMMARY OF EXPLORATORY HOLES

TYPE QUANTITY MAXIMUM DEPTH (m) REMARKS

Cable Percussion Boreholes 2 6.20 BH3 and BH5

Cable Percussion Borehole extended by Rotary Core Drilling 3 29.60 BH1, BH2 and BH4

Windowless Sampler Boreholes 6 5.00 WS1, WS2, WS3, WS4, WS5 and WS6

Trial Pits 2 1.20 TP1 and TP2

The exploratory hole records are presented in Enclosure A and should be read in conjunction with

the Key which is included in that enclosure. The records provide descriptions of the materials

encountered in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003), for soils and

rocks respectively, as amplified by BS 5930+A2 (2010). The records also give details of the

samples taken together with observations made during boring, drilling, windowless sampling and

trial pitting. Standard penetration tests (SPT) were carried out in accordance with BS EN ISO

22476-3:2005+A1 (2011) in the boreholes and windowless sampler holes and the results are

Page 6: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Page 4 of 7

included on the exploratory hole records. The SPT hammer energy ratio calibration certificates are

also included in Enclosure A.

Photographs of the recovered cores are presented in Enclosure E.

On completion of the fieldwork geotechnical samples were transported to the Southam office of

ESG for temporary retention, with those required for testing being transferred to the in-house

Daventry laboratory. Geoenvironmental samples were taken and stored in accordance with Mott

MacDonald Ltd requirements and BS EN ISO/IEC 17025 (2005) prior to and during transport to the

ESG Scientifics' Burton-on-Trent laboratory.

3.3 Instrumentation and Monitoring

The instruments installed in the exploratory holes are shown on the logs and detailed in

Enclosure B. Records of groundwater and gas monitoring carried out by ESG after the fieldwork

period are presented in Enclosure B.

Following purging of the instruments, groundwater samples for laboratory testing were taken after

the fieldwork.

4 LABORATORY TESTING

4.1 Geotechnical Testing

The testing was scheduled by Mott MacDonald Ltd and was carried out in accordance with

BS 1377 (1990) unless otherwise stated. The testing is summarised below and the results are

presented in Enclosure C.

SUMMARY OF GEOTECHNICAL LABORATORY TESTING

TYPE REMARKS

Moisture Content Determination

Atterberg Limit Determination

Particle Size Distribution Analysis

Total Sulphate Content, Water Soluble Sulphate Content, Total Sulphur Content and pH Value of Soils

Testing by ESG Scientifics; test methods are BS 1377 or others recognised in BRE Special Digest 1 (2005); they are indicated on the results report sheets in Enclosure C

Organic Matter Content

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January 2014 Report No D3155-13 Issue 3.0 Page 5 of 7

TYPE REMARKS

Dry Density/Moisture Content Relationship (Light 2.5g compaction)

Moisture Condition Value/Moisture Content Relationship

California Bearing Ratio

One Dimensional Oedometer Consolidation Testing

Unconsolidated Undrained Triaxial Compression Tests

Unconfined Compressive strength

Point Load Index

4.2 Geoenvironmental Testing

The testing was scheduled by Mott MacDonald Ltd and was carried out by ESG Scientifics. Details

of the suites scheduled are summarised below and the results are presented in Enclosure D.

SUMMARY OF GEOENVIRONMENTAL LABORATORY TESTING

TYPE REMARKS

Soil Contamination Suites

PSBP Schools Soil Suite

Asbestos screen and ID, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium,

Copper, Iron, Lead, Mercury, Molybdenum, Nickel, Selenium, Vanadium, Zinc, Water Soluble

Sulphate, Total Sulphur (BRE), pH, TPH CWG to include GRO/BTEX, Speciated PAH, VOC, Phenol

Index, Fraction Organic Carbon

20No

Polychlorinated biphenyl (PCB) 12 congeners 2No

Leachate and Water Contamination Suites

PSBP Schools Leachate Suite

Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium (trivalent), Chromium

(hexavalent), Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Selenium,

Sodium, Vanadium, Zinc, Ammoniacal Nitrogen, Chloride, Sulphide, Sulphate, pH, Cyanide (free),

Cyanide (total), Nitrate, Thiocyanate , BTEX, 16 PAH, Phenols by HPLC

20No

PSBP Schools Water Suite

Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Copper, Iron, Lead,

Magnesium, Manganese, Mercury, Nickel, Selenium, Vanadium, Zinc, Chloride, Fluoride, Sulphide,

Sulphate, pH, Cyanide (free), Cyanide (total), Thiocyanate , BTEX, 16 PAH, Phenols by HPLC, TPH

CWG

3 No

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January 2014 Report No D3155-13 Issue 3.0 Page 7 of 7

REFERENCES

AGS : 2005 : Electronic transfer of geotechnical and geoenvironmental data (Edition 3.1 including addendum May 2005). Association of Geotechnical and Geoenvironmental Specialists.

BGS Sheet 123: 1994 : Stoke-on-Trent. 1:50000 geological map (solid and drift). British Geological Survey

Baldwin M, Gosling R C and Brownlie N : 2007 : Soil and rock descriptions - a practical guide to the implementation of BS EN ISO 14688 and 14689. Ground Engineering, July.

BRE Special Digest 1 : 2005 : Concrete in aggressive ground. Building Research Establishment.

BS 1377 : 1990 : Methods of test for soils for civil engineering purposes. British Standards Institution.

BS 5930+A2 : 2010 : Code of practice for site investigations (Amendment 2). British Standards Institution.

BS EN 1997-2 : 2007 : Eurocode 7 - Geotechnical design - Part 2 Ground investigation and testing. British Standards Institution.

BS EN ISO 14688-1 : 2002 : Geotechnical investigation and testing - Identification and classification of soil - Part 1 Identification and description. British Standards Institution.

BS EN ISO 14689-1 : 2003 : Geotechnical investigation and testing - Identification and classification of rock - Part 1 Identification and description. British Standards Institution.

BS EN ISO 22475-1 : 2006 : Geotechnical investigation and testing – Sampling methods and groundwater measurements - Part 1 Technical principles for execution. British Standards Institution.

BS EN ISO 22476-3:2005+A1 : 2011 : Geotechnical investigation and testing - Field testing - Part 3 Standard penetration test. British Standards Institution.

BS EN ISO/IEC 17025 : 2005 : General requirements for the competence of testing and calibration laboratories. British Standards Institution.

GIFA10 : 2010 : Ground Investigation Services Framework Agreement. Mott Macdonald Ltd.

Page 10: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Enclosure A

ENCLOSURE A

EXPLORATORY HOLE RECORDS

Key to Exploratory Hole Records Key

Hammer Energy Ratio Reports Calibration certificates for SM19, SM39 and 100 87MR

Borehole Logs BH1, BH2, BH3, BH4 and BH5

Windowless Sampler Logs WS1, WS2, WS3, WS4, WS5 and WS6

Trial Pit Logs TP1 and TP2

Page 11: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: See report text for full references of standards

Project

Project No. Carried out for

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13 Education Funding Agency

Key Sheet 1 of 2

Key to Exploratory Hole Records

SAMPLES Undisturbed U UT TW P L CBR BLK CS AMAL

Driven tube sample Driven thin wall tube sample nominally 100 mm diameter and full recovery unless otherwise stated Pushed thin wall tube sample Pushed piston sample Liner sample (from Windowless or similar sampler), full recovery unless otherwise stated CBR mould sample Block sample Core sample (from rotary core) taken for laboratory testing Amalgamated sample

Disturbed D B

Small sample Bulk sample

Other W G ES EW

Water sample Gas sample Environmental chemistry samples (in more than one container where appropriate) Soil sample Water sample

Comments Sample reference numbers are assigned to every sample taken. A sample reference of 'NR' indicates that attempt was made to take a tube sample, however, there was no recovery. Monitoring samples taken after completion of hole construction are not shown on the exploratory hole logs.

TESTS SPT S or SPT C IV HV PP KFH, KRH, KPI

Standard Penetration Test, open shoe (S) or solid cone (C) The Standard Penetration Test is defined in BS EN ISO 22476-3 (2005). The incremental blow counts are given in the Field Records column; each increment is 75 mm unless stated otherwise and any penetration under self weight in mm (SW) is noted. Where the full 300 mm test drive is achieved the total number of blows for the test drive is presented as N = ** in the Test column. Where the test drive blows reach 50 the total blow count beyond the seating drive is given (without the N = prefix). in situ Vane shear strength, peak (p) and remoulded (r) Hand vane shear strength, peak (p) and remoulded (r) Pocket penetrometer test, converted to shear strength Permeability tests (KFH = falling head, KRH = rising head; KPI = packer inflow); results provided in Field Records column (one value per stage for packer tests)

DRILLING RECORDS The mechanical indices (TCR/SCR/RQD & If) are defined in BS 5930+A2 (2010)

TCR SCR RQD If

Total Core Recovery, % Solid Core Recovery, % Rock Quality Designation, % Fracture spacing, mm. Minimum, typical and maximum spacings are presented. The term non-intact (NI) is used where the core is fragmented.

Flush returns, estimated percentage with colour where relevant, are given in the Records column CRF AZCL NR

Core recovered (length in m) in the following run Assessed zone of core loss Not recovered

GROUNDWATER

Groundwater strike Groundwater level after standing period

Page 12: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: See report text for full references of standards

Project

Project No. Carried out for

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13 Education Funding Agency

Key Sheet 2 of 2

Key to Exploratory Hole Records

INSTALLATION Standpipe/ piezometer SP SPIE PPIE EPIE Inclinometer or Slip Indicator ICE ICM SLIP Settlement Points or Pressure Cells ESET ETM EPCE PPCE

Details of standpipe/piezometer installations are given on the Record. Legend column shows installed instrument depths including slotted pipe section or tip depth, response zone filter material type and layers of backfill. The type of instrument installed is indicated by a code in the Legend column at the depth of the response zone: Standpipe Standpipe piezometer Pneumatic piezometer Electronic piezometer The installation of vertical profiling instruments is indicated on the Record. The base of tubing is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column at the base of the tubing: Biaxial inclinometer Inclinometer tubing for use with probe Slip indicator The installation of single point instruments is indicated on the Record. The location of the measuring device is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column: Electronic settlement cell/gauge Magnetic extensometer settlement point Electronic embedment pressure cell Electronic push in pressure cell

INSTALLATION LEGENDS

A legend describing the installation is shown in the rightmost column. Legends additional to BS5930 are used to describe the backfill materials as indicated below.

Arisings

Concrete

Grout

Bentonite

Sand

Gravel

Macadam

NOTES 1 2 3 4 5 6 7 8

Soils and rocks are described in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003) respectively as amplified by BS 5930+A2 (2010). For fine soils, consistency determined during description is reported for those strata where undisturbed samples are available. Where the logger considers that the sample may not be representative of the condition in situ, for whatever reason, the reported consistency is given in brackets. The reliability of the sample is indicated by Probably or Possibly as appropriate. Hence (Probably firm) indicates the logger is reasonably confident of the assessment, but (Possibly firm) means less certainty. Where the samples available are too disturbed to allow a reasonable assessment of the in situ condition, no consistency is given. Evidence of the occurrence of very coarse particles (cobbles and boulders) is presented on the logs, however, because of their size in relation to the exploratory hole these records may not be fully representative of their size and frequency in the ground mass. The declination of bedding and joints is given with respect to the normal to the core axis. Thus in a vertical borehole this will be the dip. The assessment of SCR, RQD and Fracture Spacing excludes artificial fractures Strata legends are in accordance with BS 5930+A2 (2010). Water level observations of discernible entries during the advancing of the exploratory hole are given at the foot of the log and in the Legend column. The term "none observed" is used where no discrete entries are identified although this does not necessarily indicate that the hole has not been advanced below groundwater level. Under certain conditions groundwater cannot be observed, for instance, drilling with water flush or overwater, or boring at a rate much faster than water can make its way into the borehole (ref BS5930+A2:2010, Clause 47.2.7). In addition, where appropriate, water levels in the hole at the time of recovering individual samples or carrying out in situ tests and at shift changes are given in the Records column. The borehole logs present the results of Standard Penetration Tests recorded in the field without correction or interpretation. However, in certain ground conditions (eg high hydraulic head or where very coarse particles are present) some judgement may be necessary in considering whether the results are representative of in situ mass conditions.

Updated March 2012

Page 13: Report No D3155-13 - apps2.staffordshire.gov.uk

Date of test: 19/02/2013 Hammer ID: SM19Hammer mass (m ) 63.5 kg

Instrumented rod: Fall height (h ) 0.76 mType BW SPTCross-sectional area (A a) 11.30 cm2 Manufacturer: ArchwayYoung's modulus (E a) 207000 MPa Automatic Trip HammerLength 0.60 m

Rig: Beretta T51Test rod type: NWY Rig ID: T51-R59

Type: RotaryForeman: M Atkinson

Remarks:

Test type:

Model:

Data obtained from test carried out in BH1, located in ESG Doncaster yard. Test carried out at depth of 5.10mbgl, with a total blow count of 20. Energy determined from every blow.

80

120

160

200

240

Forc

e (k

N)

Force - typical blow

1.5

2.5

3.5

4.5

loci

ty (m

/s)

Particle Velocity - typical blow

Hammer Energy Report

Theoretical energy (E theor) = m x g x h = 0.473 kN-m (473 J)

Measured energy (E meas) average of 20 blows = 0.311 kN-m

E meas

E theor

Test carried out by: Malcolm Carr Test carried out in accordance with BS EN ISO 22476-3:2005

Signed for issue: Equipment used: SPT Analyzer Serial No 4032T

66 %=Energy ratio =

0

20

40

60

80

100

100 150 200 250

Ener

gy r

atio

(%)

Force (kN)

0

20

40

60

80

100

0 5 10 15 20 25

Ener

gy r

atio

(%)

Blow

average

-40

0

40

80

120

0 5 10 15

Forc

e (k

N

time (ms)

-0.5

0.5

1.5

2.5

0 5 10 15

Velo

city

(m

time (ms)

Signed for issue: Equipment used: SPT Analyzer Serial No. 4032T

Page 14: Report No D3155-13 - apps2.staffordshire.gov.uk

Date of test: 19/02/2013 Hammer ID: SM38Hammer mass (m ) 63.5 kg

Instrumented rod: Fall height (h ) 0.76 mType BW SPTCross-sectional area (A a) 11.30 cm2 Manufacturer: ArchwayYoung's modulus (E a) 207000 MPa Automatic Trip HammerLength 0.60 m

Rig: Beretta T51Test rod type: NWY Rig ID: T51-R59

Type: RotaryForeman: M Atkinson

Remarks:

Test type:

Model:

Data obtained from test carried out in BH1, located in ESG Doncaster yard. Test carried out at depth of 5.25mbgl, with a total blow count of 20. Energy determined from every blow.

40

80

120

160

Forc

e (k

N)

Force - typical blow

1.5

2.5

3.5

eloc

ity (m

/s)

Particle Velocity - typical blow

Hammer Energy Report

Theoretical energy (E theor) = m x g x h = 0.473 kN-m (473 J)

Measured energy (E meas) average of 20 blows = 0.350 kN-m

E meas

E theor

Test carried out by: Malcolm Carr Test carried out in accordance with BS EN ISO 22476-3:2005

Signed for issue: Equipment used: SPT Analyzer Serial No 4032T

74 %=Energy ratio =

0

20

40

60

80

100

100 150 200 250

Ener

gy r

atio

(%)

Force (kN)

0

20

40

60

80

100

0 5 10 15 20 25

Ener

gy r

atio

(%)

Blow

average

-40

0

40

80

0 5 10 15

Forc

e (k

N

time (ms)

-0.5

0.5

1.5

0 5 10 15

Velo

city

(m

time (ms)

Signed for issue: Equipment used: SPT Analyzer Serial No. 4032T

Page 15: Report No D3155-13 - apps2.staffordshire.gov.uk
Page 16: Report No D3155-13 - apps2.staffordshire.gov.uk

7.14-7.436.60-8.00

8.00-8.11

8.00-9.60

9000

10030

1005141

100180

B 1D 2B 4

ES 3B 5

ES 6D 7B 11D 8D 10ES 9

SPT SD 12B 13

ES 14D 15

SPT SD 16B 17

SPT SD 18B 19B 20

NI2030

NI3050

NI90

300

NI70

220

Flush: 4.50-11.10Water, 90 %

N=5 (1,-/1,1,1,2)

N=15 (3,4/4,3,4,4)

N=43 (4,4/4,7,13,19)

If /NR/

CS 21

1.50

2.50

3.00

09/10/20134.30

15/10/20134.30

4.40

15/10/20134.40

16/09/20134.40

dry

dry

dry

08003.42

4.90

08003.74

0.10

0.30

0.70

1.60

2.00

3.50

3.70

4.30

4.50

4.95

6.00

(0.40)

(0.90)

(0.40)

(1.50)

(0.60)

(0.45)

(1.05)

+131.29

+131.09

+130.69

+129.79

+129.39

+127.89

+127.69

+127.09

+126.89

+126.44

+125.39

MADE GROUND: macadam.

MADE GROUND: black very sandy GRAVEL.Sand is medium to coarse. Gravel is angularfine to coarse brick, clinker, slag andmacadam.

MADE GROUND: brown slightly sandy GRAVELwith occasional coarse gravel size softgrey clay pockets. Gravel is angular fineto coarse brick, clinker and coal.

MADE GROUND: soft grey brown slightlygravelly sandy CLAY. Gravel is angular torounded fine of coal and brick.

Possible MADE GROUND: soft brown sandygravelly CLAY. Gravel is subrounded to

Time Tools used

rounded fine to coarse quartzite.

Medium dense light brown gravelly clayeyfine to medium SAND. Gravel is roundedfine to medium sandstone.(GLACIOFLUVIAL DEPOSITS)

Firm brown mottled grey slightly gravellysandy CLAY. Gravel is subangular fine tocoarse sandstone.(Possible GLACIOFLUVIAL DEPOSITS)

From

Very stiff friable grey mottled brown CLAYtending to extremely weak MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

Very weak grey mottled brownSILTSTONE.(PENNINE MIDDLE COALMEASURES FORMATION)

Very weak and weak grey SILTSTONE.

to (m)

(PENNINE MIDDLE COAL MEASURESFORMATION)Weathering: brown discolouration,penetrating up to 5mm, adjacent tofractures. Fractures are randomlyorientated, extremely closely and veryclosely spaced, undulating rough,generally silt smeared (<1mm), occasionalclayey fine gravel infill (1-5mm)

Generally weak grey sandy SILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Weathering: heavily stained dark orange

Checked

brown, penetrating up to 3mm. Fracturesare randomly orientated, very closelyspaced, undulating rough, generally clean,occasionally silt smeared (<1mm).

Weak to medium strong thinlyinterlaminated light grey fine grainedslightly micaceous SANDSTONE andSILTSTONE. Rare coal and ironstone bands.(PENNINE MIDDLE COAL MEASURESFIORMATION)Weathering: includes orange brown stainingand quartz mineralization.Fractures are 1) subvertical and inclined

Equipment, Methods and Remarks

65-80deg, extremely closely and veryclosely spaced, generally clean,occasionally clayey gravel infill (<40mm)2) randomly orientated, very closely towidely spaced, undulating rough, generally

1:50

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AH/PSMQ/MBJRL

09/10/2013

17/10/2013

TCRSCRRQD

Type & No

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m

Records/Samples

Records

426.4823/01/2014 15:57:11(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Stratum continues to 29.60 m

National Grid

Chainage

BH1Sheet 1 of 3

+131.39 mODE 383570.56N 354283.87

1.50 3.50 SPT hammer ID SM398.00 29.60 SPT hammer ID SM19

4.50m0.00m 150mm29.60m4.50m 120mm

4.30m4.40m

4.10 -4.30 60 mins

SPT S 50 (25 for 70mm/50 for 40mm)

*

*

4.30-4.38 m AZCL

6.00-6.80 mbedding

overturned,stained orange

brown,occasional

quartrzmineralization

7.00 m 80degfracture, clayey

gravel infill(15mm)

7.30 m 75degfracture

7.45-8.20 mbedding fractures

overturned,gravelly clay infill

(<25mm)7.85-8.20 m

randomlyorientated, veryclosely spaced,

stained orangishbrown

8.60-9.50 mpersistent

subverticalbedding fracture,clayey gravel infill

(10-30mm)

9.50-10.25 mfractures

occasional quartzmineralization

(<1mm)

0.00-0.100.00-0.100.10-0.30

0.200.30-0.70

0.500.50

0.70-1.200.701.001.00

1.50-1.951.50-1.951.50-2.00

2.002.00

2.50-2.952.50-2.952.50-3.00

3.50-3.953.50-3.953.50-3.703.70-4.00

4.30-5.10

5.10-6.60

Page 17: Report No D3155-13 - apps2.staffordshire.gov.uk

fracture16.30-18.95 m

persistentsubverticalfractures,

gravelly clay infill<40mm

19.10 m 25degfracture

19.50 m 55degstepped fracture

19.60-19.80 msubverical

smooth fracture,

10.25-10.429.60-11.10

11.10-11.1911.10-11.39

11.10-12.60

12.60-15.60

14.91-15.27

15.60-15.66

15.94-16.24

15.60-18.60

18.60-18.67

19.30-19.50

1007047

978255

1008271

1006852

30100300

20100300

15130380

10140430

40200400

Flush: 11.10-22.15Water, 0 %

CS 22

CS 23

CS 24

CS 25

CS 26

4.40

4.40

4.40

(23.60)

SP

clean, sometimes silt smeared (<1mm).Bedding fractures occasionally overturned.

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AH/PSMQ/MBJRL

09/10/2013

17/10/2013

TCRSCRRQD

TCRSCRRQD

If

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m

Records/Samples

Records/Samples

426.4823/01/2014 15:57:14(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Stratum continues to 29.60 m

(Continued from Sheet 1)(Continued from Sheet 1)

National Grid

Chainage

BH1Sheet 2 of 3

+131.39 mODE 383570.56N 354283.87

4.50m0.00m 150mm29.60m4.50m 120mm

4.30m4.40m

SPT S 50 (25 for 50mm/50 for 40mm)

SPT S 50 (25 for 30mm/50 for 30mm)

SPT S 50 (25 for 30mm/50 for 40mm)

10.25-12.60 mvery closely to

medium spacedinclined,

occasionallystriated, fractures

12.00 msubvertical

fracture, quartzmineralization

12.30-12.80 minclined 65-75

deg beddingfractures, little

pyriticmineralization

(<1mm)12.90 m 35deg

fracture13.20 m 30deg

fracture13.30 m 15deg

fracture13.60 m 45degplanar fracture13.80-14.20 m2No extremelyclosely spaced

subverticalfractures, silt

smeared (<1mm)14.20-14.26 msubhorizontalstrong brown

IRONSTONE14.35-14.55 m

subverticalfracture

14.60-14.95 msubvertical

fracture15.30 m 35deg

fracture15.40 m 60deg

fracture15.90 m 10deg

Page 18: Report No D3155-13 - apps2.staffordshire.gov.uk

29.07 msubhorizontal

fracture29.25 m 35deg

fracture

18.60-21.60

21.60-21.65

21.60-22.15

22.96-23.29

22.15-24.60

24.60-24.65

25.42-25.57

24.60-27.30

27.30-27.36

27.30-27.70

27.70-29.60

29.08-29.24

29.60-29.66

1008574

10000

1007064

1009277

100100100

978767

NI260800

NI200400

20400800

20250300

NI180310

Flush: 22.15-29.60Water, 90 %

CS 27

CS 28

CS 29

4.40

16/09/20134.40

17/10/20134.40

4.40

4.40

4.40

3.65

0800

29.60 +101.79

Weak to medium strong thinlyinterlaminated light grey fine grainedslightly micaceous SANDSTONE andSILTSTONE. Rare coal and ironstone bands.(PENNINE MIDDLE COAL MEASURESFIORMATION)Weathering: includes orange brown stainingand quartz mineralization.Fractures are 1) subvertical and inclined65-80deg, extremely closely and veryclosely spaced, generally clean,occasionally clayey gravel infill (<40mm)2) randomly orientated, very closely towidely spaced, undulating rough, generallyclean, sometimes silt smeared (<1mm).Bedding fractures occasionally overturned.

EXPLORATORY HOLE ENDS AT 29.60 m

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AH/PSMQ/MBJRL

09/10/2013

17/10/2013

TCRSCRRQD

TCRSCRRQD

If

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 29.60m

Records/Samples

Records/Samples

426.4823/01/2014 15:57:17(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

(Continued from Sheet 2)(Continued from Sheet 2)

National Grid

Chainage

BH1Sheet 3 of 3

+131.39 mODE 383570.56N 354283.87

4.50m0.00m 150mm29.60m4.50m 120mm

4.30m4.40m

SPT S 50 (25 for 20mm/50 for 30mm)

SPT S 50 (25 for 20mm/50 for 30mm)

SPT S 50 (25 for 40mm/50 for 20mm)

SPT S 50 (25 for 20mm/50 for 40mm)

quartzmineralization

20.00-22.10 mpersistent

subverticalfractures, clayey

gravel infill, quartzmineralization

22.40-22.50 mtwo inclined 60-70

deg thin coallaminae

22.55-22.95 msubverticalfractures,

generally clean,quartz

mineralization,occasional plant

remains23.25 m 50deg

planar silt coatedfracture

23.80 m 30 degfracture

23.90-24.05 minclined

60-70degfractures

24.25-24.55 msubvertical

fracture

26.10 m30degclay infilled(<5mm) fracture

26.85-27.25 m85deg fracture,

silt smeared

28.00 m 45degfracture

28.15 m 45degfracture

28.50 msubhorizontal

clay infilled(<10mm) fracture

Page 19: Report No D3155-13 - apps2.staffordshire.gov.uk

3.50-3.60

3.50-4.15

4.15-5.905.16-5.34

6.10-6.26

5.90-8.20

8.20-8.29

8.20-9.50

1008888

916050

1006321

81238

B 1D 2

ES 3D 4B 5D 6

ES 7B 8

ES 9

D 10U 11

ES 13D 12

SPT SD 14B 15

SPT SD 16

NI100220

540

220

40100300

NI70

200

NR

Flush: 3.50-4.15Water, 80 %

Flush: 4.15-5.90Water, 70 %

Flush: 5.90-9.50Water, 60 %

33 blows

N=15 (4,4/3,4,4,4)

50 (25/50 for 30mm)

If /NR/

If NI/40/60

If /NR/

CS 17

CS 18

1.50

2.50

15/10/20133.00

18/10/20133.50

4.00

1.40

2.40

3.10

0800

0.10

0.30

0.50

1.351.40

3.503.60

5.75

6.05

6.85

7.40

(0.85)

(2.10)

(2.15)

(0.30)

(0.80)

(0.55)

(5.00)

+133.52

+133.32

+133.12

+132.27+132.22

+130.12+130.02

+127.87

+127.57

+126.77

+126.22

1

1

MADE GROUND: macadam.

MADE GROUND: black and dark brown SANDand GRAVEL. Sand is medium to coarse. Gravelis angular medium to coarse brick, clinkerand slag.

MADE GROUND: reddish brown sandy GRAVELof angular fine to coarse limestone.

Time Tools used

MADE GROUND: soft to firm grey mottledbrown slightly sandy slightly gravellyCLAY with low cobble content. Gravel isrounded fine mudstone and angular finesandstone and coal. Cobbles are quartz.

Possible MADE GROUND: brown fine SAND.

fIRM grey gravelly CLAY. Gravel is angularfine to coarse sandstone.(PENNINE MIDDLE COAL MEASURES

From

FORMATION)

Extremely weak grey SANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

Strong to very strong light grey finegrained quartzitic SANDSTONE, locally withextremely closely spaced thin grey andblack wispy laminations.(PENNINE MIDDLE COAL MEASURESFORMATION)

to (m)

Fractures are 1) inclined 20-30deg, veryclosely and closely spaced, planar rough,generally clean, occasional silty finesand infill (1-3mm), generaly stainedorangish brown 2) inclined 60-80deg,planar rough, stained orangish brown.

Weak to medium strong thinly laminatedgrey silty MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are inclined 25-30deg, veryclosely spaced, planar clean.

Checked

Medium strong laminated light grey finegrained quartzitic SANDSTONE withextremely and very closely spaced thindark grey mudstone and black coal wispylaminae.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are inclined 25-30deg, extremelyclosely to closely spaced, undulatingrough, clean.

Medium strong thinly interlaminated light

Equipment, Methods and Remarks

grey fine grained quartzitic SANDSTONE andgrey SILTSTONE.(PENNINE MIDDLE COSAL MEASURESFORMATION)Fractures are inclined 25-30 deg, closelyand medium spaced, planar smooth, clean,stained dark grey, occasionally incipient.

Weak, locally indistinctly laminated, greyMUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

Backfill/

1:50

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole LogAH/PSMQ/MBJRL

15/10/2013

23/10/2013

TCRSCRRQD

Type & No

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m

Records/Samples

Records

426.4823/01/2014 15:58:11(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Stratum continues to 12.40 m

National Grid

Chainage

BH2Sheet 1 of 3

+133.62 mODE 383637.48N 354171.53

1.401 Rose to 1.30 m after 20 minutes. Slow -2.50 3.50 SPT hammer ID SM398.20 24.60 SPT hammer ID SM199.50 11.60 Flush: Water, 50%

3.60m0.00m 150mm25.50m3.60m 120mm

3.00m4.00m

3.30 -3.50 60 mins

SPT S 50 (25 for 40mm/50 for 50mm)

*

*

*

3.50-3.55 m NI,recovered as

angular gravel

4.60-4.70 m70deg fracture

5.40-5.65 m75deg fracture

5.75-5.90 m AZCL

6.40-6.60 m 2Nointersecting

inclined45-60degfractures

6.60-6.85 mextremely closely

spaced coallaminae

7.75-7.82 m NI,clayey gravel

8.03-8.10 m NI,clayey gravel

8.35-8.90 m veryclosely fractured,

generally NI

9.25-9.50 m AZCL

9.70-9.90 m veryclosely fractured,

NI

0.00-0.100.200.200.30

0.30-0.500.500.50

0.50-1.201.00

1.401.50-1.95

2.002.05

2.50-2.952.50-2.952.50-3.00

3.50-3.61

Page 20: Report No D3155-13 - apps2.staffordshire.gov.uk

17.75-17.85 mstrong

IRONSTONE

18.40-18.50 mstrong

IRONSTONE18.50-19.60 m

occasionalsubvertical

quartz veining<3mm

18.75-18.90 m60deg fracture19.05-19.40 m

subverticalfracture

19.75-19.85 mstrong

9.50-10.50

10.50-10.60

10.50-11.60

11.60-13.00

13.00-13.9013.50-13.58

13.90-14.70

14.70-16.10

16.10-17.00

17.00-17.07

17.40-17.5617.00-18.10

18.10-19.6018.88-19.06

19.60-19.66

100170

100120

100130

1006717

1003613

894929

100280

1003223

935542

NI4080

NI10

200

NI150580

Flush: 11.60-17.00Water

Flush: 17.00-18.10Water, 50 %

CS 19

CS 20

18/10/20134.00

21/10/20134.00

4.00

21/10/20134.00

22/10/20134.00

4.00

08001.35

08001.15

12.40

16.35

(3.95)

+121.22

+117.27

Fractures are 1) inclined 20-30deg, veryclosely and closely spaced, planar andundulating, smooth, generally clean,occasional sandy clay infill (1-2mm) 2)randomly orientated, very closely andclosely spaced, undulating smooth, clean,sometimes incipient.

Weak to medium strong dark greyish brownMUDSTONE with occasional marine bands.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are 1) inclined 20-30 deg,closely spaced, undulating smooth,generally clean, occasional silty clayinfill (1-2mm).

Weak, locally thinly laminated, greyMUDSTONE with medium and widely spacedthin strong brown IRONSTONEinterbeds/nodules and occasional mediumstrong light grey and grey fine grainedSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

Time Tools used

Fractures are 1) inclined 20-30deg,closely and medium spaced, undulatingsmooth, generally clean, occasionalgravelly clay infill (<20mm) 2) randomlyorientated, planar and undulating,smooth,generally clean, occasional gravelly clayinfill (<20mm).

1:50

From to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole LogAH/PSMQ/MBJRL

15/10/2013

23/10/2013

TCRSCRRQD

TCRSCRRQD

If

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m

Records/Samples

Records/Samples

426.4823/01/2014 15:58:15(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Stratum continues to 25.50 m

(Continued from Sheet 1)(Continued from Sheet 1)

National Grid

Chainage

BH2Sheet 2 of 3

+133.62 mODE 383637.48N 354171.53

3.60m0.00m 150mm25.50m3.60m 120mm

3.00m4.00m

SPT S 50 (25 for 70mm/50 for 30mm)

SPT S 50 (25 for 40mm/50 for 40mm)

SPT S 50 (25 for 30mm/50 for 40mm)

SPT S 50 (25 for 30mm/50 for 30mm)

10.80-11.35 mvery closely

fractured,recovered NI

11.50-12.40 mdark grey, very

closely fractured

13.00-13.20 mextremely closelyand very closely

spaced marinebands (<5mm)

13.45 m marineband (5mm)

13.85 m marineband (5mm)

14.50-14.60 m NI

15.50-15.95 mextremely closelyand very closely

spaced marinebands (<10mm)15.95-16.10 m

AZCL16.20-16.35 m

AZCL

17.05-17.15 mstrong

IRONSTONE17.40-17.55 mmedium strongSANDSTONE

Page 21: Report No D3155-13 - apps2.staffordshire.gov.uk

21.26-21.54

21.10-22.40

22.40-22.46

22.40-23.80

24.11-24.2523.80-24.60

24.60-24.66

24.60-26.00

26.00-27.50

1005337

1005252

862216

883928

642111

3330

NI3080

NR

NI70

160

NR

NI480

Flush: 18.10-27.50Water

If /NR/

CS 21

CS 22

4.00

22/10/20134.00

23/10/20134.00

2.46

08004.00

25.50

27.50

(9.15)

(2.00)

+108.12

+106.12

SP

Weak, locally thinly laminated, greyMUDSTONE with medium and widely spacedthin strong brown IRONSTONEinterbeds/nodules and occasional mediumstrong light grey and grey fine grainedSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are 1) inclined 20-30deg,closely and medium spaced, undulatingsmooth, generally clean, occasionalgravelly clay infill (<20mm) 2) randomlyorientated, planar and undulating,smooth,generally clean, occasional gravelly clayinfill (<20mm).

Partial recoveryRecovered core comprises weak thinlylaminated dark grey to black carbonaceousMUDSTONE with frequent plant remains andoccasional thin coal laminae.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated, veryclosely spaced, undulating rough.

EXPLORATORY HOLE ENDS AT 27.50 m

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole LogAH/PSMQ/MBJRL

15/10/2013

23/10/2013

TCRSCRRQD

TCRSCRRQD

If

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 3.60m, rotary core to 27.50m

Records/Samples

Records/Samples

426.4823/01/2014 15:58:18(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

(Continued from Sheet 2)(Continued from Sheet 2)

National Grid

Chainage

BH2Sheet 3 of 3

+133.62 mODE 383637.48N 354171.53

3.60m0.00m 150mm25.50m3.60m 120mm

3.00m4.00m

SPT S 50 (25 for 20mm/50 for 40mm)

SPT S 50 (25 for 30mm/50 for 30mm)

IRONSTONE, 2No60deg fractures

20.45-20.65 m70deg fracture20.65-20.87 m

strongIRONSTONE, 2no

subverticalfractures

20.87-21.05 m NI21.20-21.30 m

strongIRONSTONE,65deg fracture21.50-21.60 m70deg fracture21.77-21.83 m

strongIRONSTONE

22.00-22.40 mvery closelyfractured, NI

22.95-23.00 mstrong

IRONSTONE

23.45-23.60 m NI23.60-23.90 m

AZCL

23.90-23.95 mstrong

IRONSTONE

24.55-24.70 mstrong

IRONSTONE24.75-25.30 m2No 75-80deg

fractures

25.40-25.45 mstrong

IRONSTONE25.50-27.00 m

AZCL

19.60-21.10

Page 22: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AHMQJRL

10/10/2013

10/10/2013

Type & No

Type & No

Dando 3000Service inspection pit hand excavated to 1.20mCable percussion to 3.10m

Records

Records

426.4823/01/2014 15:58:37(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

BH3Sheet 1 of 1

+137.60 mODE 383617.37N 354115.86

2.50 3.00 SPT hammer ID SM39

3.10m0.00m 150mm 3.00m

2.80 -3.00 60 mins

*

0.00-0.100.200.20

0.20-0.400.40

0.40-1.200.50

1.00

1.50-1.95

2.002.05

2.50-2.912.50-2.902.50-2.80

3.00-3.103.00-3.10

B 1D 2

ES 3B 4D 5B 7

ES 6

ES 8

U 9

ES 11D 10

SPT SD 12B 13

SPT SD 14

25 blows 315 mm rec

50 (1,1/2,2,30,16 for 30mm)

50 (25 for 40mm/50 for 60mm)

1.50

2.50

3.00

dry

0.00

dry

dry

0.10

0.40

1.40

2.80

3.10

(0.30)

(1.00)

(1.40)

(0.30)

+137.50

+137.20

+136.20

+134.80

+134.50SP

MADE GROUND: macadam.

MADE GROUND: brown silty very sandyGRAVEL. Sand is fine to coarse. Gravel isangular fine to coarse brick, macadam,coal, sandstone and concrete.

MADE GROUND: soft to firm reddish brownslightly gravelly CLAY and orangish brownfine to medium SAND with occasional greyslightly sandy silt pockets. Gravel isangular fine coal, mudstone and sandstone.

Reddish brown gravelly clayey fine tomedium SAND. Gravel is subangular tosubrounded fine to coarse sandstone.(Possible GLACIOFLUVIAL DEPOSITS)

Extremely weak light grey SILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 3.10 m

1:50

Page 23: Report No D3155-13 - apps2.staffordshire.gov.uk

2.50-3.00

3.50-3.883.50-3.903.50-4.00

4.50-4.734.50

4.50-5.60

5.60-7.10

7.10-7.55

7.55-7.63

7.55-8.30

8.30-8.40

8.40-8.80

9.10-9.28

8.80-9.90

79110

1004127

2200

100170

1005028

1005858

B 1B 4D 2

ES 3B 5D 6

ES 7B 8

ES 9

U 10

D 11

SPT SD 12B 13

SPT SD 14B 15

SPT SD 16NR

NI1080

NI3575

NI4090

NI150400

NR

NI60

130

NI70

180Flush: 4.50-13.90

water, 100 %

80 blows

50 (6,8/10,13,17,10 for 40mm)

50 (7,11/11,15,24)

50 (7,18/50)If /NR/

TCR 100, SCR 0, RQD 0

CS 17

1.50

2.50

10/10/20132.50

11/10/20132.50

3.00

11/10/20133.00

23/10/20133.50

3.50

23/10/20133.50

24/10/20134.50

dry

dry

dry

0800dry

dry

dry

08000.15

2.10

08001.36

0.100.25

0.50

2.50

4.50

5.40

5.75

6.50

7.10

8.30

9.55

(2.00)

(2.00)

(0.90)

(0.35)

(0.75)

(0.60)

(1.20)

(1.25)

+139.38+139.23

+138.98

+136.98

+134.98

+134.08

+133.73

+132.98

+132.38

+131.18

+129.93

Time Tools usedFrom

MADE GROUND: macadam.

MADE GROUND: red and brown SAND andGRAVEL. Sand is medium to coarse. Gravelis angular fine to coarse brick, concreteand clinker.

Possible MADE GROUND: firm grey gravellySILT. Gravel is angular fine siltstone andcoal.

to (m)

Stiff grey slightly sandy slightlygravelly CLAY. Gravel is subangular fineto medium mudstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

Very stiff grey slightly sany slightlygravelly CLAY, occasionally tending toextremely weak SILTSTONE, with occasionalcoal bands. Gravel is subangular fine tomedium mudstone and siltstone.(PENNINE MIDDLE COAL MEASURES

Checked

FORMATION)

Extremely weak friable grey MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely spaced, undulatingsmooth.

Weak black COAL.(PENNINE MIDDLE COAL MEASURESFORMATION)

Equipment, Methods and Remarks

Fractures are inclined 20-25deg andsubvertical, very closely spaced.

Very weak to weak grey and light greyMUDSTONE. Occasional fossil plant remains.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely to closely spaced,undulating smooth, occasionally clayinfilled (<15mm).

Backfill/

Very weak to weak grey fine grainedslightly micaceous SANDSTONE andSILTSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)Fractures are randomly orientated,extremely closely to medium spaced,undulating rough. Often very closelyspaced, incipient. Occasional quartziticmineralization on fractures.

Medium strong to strong light grey finegrained slightly micaceous SANDSTONE.(PENNINE MIDDLE COAL MEASURES

Coordinates

FORMATION)Fractures are randomly orientated, veryclosely and closely spaced, undulatingrough, clean stained orange brown.

1:50

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AH/PSMQ/MBJRL

10/10/2013

25/10/2013

TCRSCRRQD

Type & No

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 13.90m

Records/Samples

Records

426.4823/01/2014 15:58:46(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Stratum continues to 13.60 m

National Grid

Chainage

BH4Sheet 1 of 2

+139.48 mODE 383650.32N 354068.71

2.50 4.50 SPT hammer ID SM397.55 11.85 SPT hammer ID SM19

4.50m0.00m 150mm13.90m4.50m 120mm

3.00m4.50m

4.30 -4.50 60 mins

SPT S 50 (25 for 30mm/50 for 50mm)

*

*

4.50-4.73 m AZCL

4.73-4.95 mrecovered as softgrey gravelly clay

5.30-5.40 m veryweak, extremelyclosely spaced

incipient polishedsurfaces

7.10-7.45 m AZCL

7.45-7.55 m NI,recovered ascoarse gravel

8.20-8.30 m NI,recovered as

slightly sandycoarse gravel

8.30-8.85 m withextremely closely

and closelyspaced blackcoal laminae

(<3mm)8.60-8.80 m

subverticalfracture

9.10-9.35 msubvertical

fracture9.10-9.50 m

0.00-0.100.10-0.25

0.200.20

0.25-0.500.500.50

0.50-1.201.00

1.50-1.95

2.05

2.50-2.922.50-2.90

Page 24: Report No D3155-13 - apps2.staffordshire.gov.uk

0

NI80

220

NR

NI75

130

If /NR/

If /NR/TCR 33, SCR 0, RQD 0

If /NI/

CS 18

CS 19

4.50

24/10/20134.50 2.13

13.60

13.90

(4.05)

(0.30)+125.88

+125.58

SP

____________8.30m - 9.55m : Medium strong thinlylaminated light grey fine grainedslightly micaceous SANDSTONE and greySILTSTONE with occasional thin (<3mm)coal laminations and very thin ironstonebands. (PENNINE MIDLE COAL MEASURESFORMATION) Fractures are inclined15-20deg, very closely and closely spaced,undulating smooth, generally clean,occasionally silt smeared (<1mm).____________9.55m - 13.60m : Weak to medium stronggrey MUDSTONE with occasional very thinstrong brown IRONSTONE interbeds. (PENNINEMIDDLE COAL MEASURES FORMATION)Fractures are 1) inclined 15-20deg, very closelyand closely spaced, planar and undulatingsmooth, often clean, occasional sandygravel (<20mm) infill, occasionally claysmeared 2) randomly orientated andsubvertical, undulating smooth, clean.

Recovered core comprises medium stronglight grey fine grained quartziticSANDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 13.90 m

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AH/PSMQ/MBJRL

10/10/2013

25/10/2013

TCRSCRRQD

TCRSCRRQD

If

If

Dando 3000/Beretta T51Service inspection pit hand excavated to 1.20mCable percussion to 4.50m, rotary core to 13.90m

Records/Samples

Records/Samples

426.4823/01/2014 15:58:51(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

(Continued from Sheet 1)(Continued from Sheet 1)

National Grid

Chainage

BH4Sheet 2 of 2

+139.48 mODE 383650.32N 354068.71

4.50m0.00m 150mm13.90m4.50m 120mm

3.00m4.50m

SPT S 50 (25 for 30mm/50 for 30mm)

:: 9.10m - tendingto laminated

SILTSTONE10.22-10.25 m

strongIRONSTONE

10.30-10.36 m NI10.50-10.56 m NI

11.18-11.21 mstrong

IRONSTONE11.42-11.45 m

strongIRONSTONE

11.45-11.75 m70deg fracture11.75-11.78 m

strongIRONSTONE

11.85-12.10 mAZCL

12.40-12.60 mrecovered NI

12.60-12.75 mAZCL

12.90-13.05 mrecovered NI

13.45-13.60 m NI,recovered as

very clayeygravel

13.60-13.90 mAZCL

9.90-10.70

10.94-11.15

10.70-11.85

11.85-11.91

11.85-12.60

12.60-13.60

13.32-13.44

13.60-13.90

943014

967449

67160

854621

330

Page 25: Report No D3155-13 - apps2.staffordshire.gov.uk

(GLACIOFLUVIAL DEPOSITS)

Stiff grey slightly sandy slightlygravelly silty CLAY tending to extremelyweak SILTSTONE. Gravel is angular fine tomedium siltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

Very weak grey SILTSTONE. Recovered assilty sandy gravel.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 6.20 m

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

AHMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Dando 3000Service inspection pit hand excavated to 1.20mCable percussion to 6.20m

Records

Records

426.4823/01/2014 15:58:57(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

BH5Sheet 1 of 1

+139.75 mODE 383718.63N 354099.58

2.50 6.15 SPT hammer ID SM39

6.20m0.00m 150mm 4.50m

5.90 -6.15 60 mins

*

3.50-4.00 m Firm

0.200.200.25

0.25-1.200.50

1.00

1.50-1.95

2.002.05

2.50-2.952.50-2.952.50-3.00

3.00

3.50-3.953.50-4.95

4.05

4.50-4.954.50-5.00

5.50-5.805.50-5.805.50-6.00

6.15-6.226.15-6.20

ES 1D 2D 3B 5

ES 4

ES 6

U 7

ES 9D 8

SPT SD 10B 11

ES 12

U 13D 16

D 14

SPT SB 17

SPT SD 18B 19

SPT SD 20

33 blows

N=22 (3,3/5,5,6,6)

47 blows

N=12 (3,3/3,3,3,3)

50 (10,13/21,29)

50 (25 for 30mm/50 for 40mm)

1.50

2.50

3.00

4.50

4.50

4.50

dry

dry

dry

dry

dry

dry

0.25

2.00

4.00

4.40

4.65

5.50

6.20

(1.75)

(2.00)

(0.40)

(0.85)

(0.70)

+139.50

+137.75

+135.75

+135.35

+135.10

+134.25

+133.55 SP

Firm brown slightly snady gravelly CLAY.Gravel is angular to subrounded fine tocoarse sandstone, brick and quartz.(TOPSOIL)

MADE GROUND: stiff orangish brown mottledgrey slightly sandy slightly gravellyCLAY. Gravel is angular fine brick andcoal.

MADE GROUND: stiff, becoming firm, greyblack slightly gravelly CLAY. Gravel issubrounded fine to coarse mudstone,sandstone and coal.

Possible MADE GROUND: firm sandy gravellyCLAY with low cobble content. Gravel isangular fine to coarse coal and sandstone.Cobbles are sandstone.

Firm orangish brown slightly sandyslightly gravelly CLAY. Gravel issubangular fine to medium sandstone andsiltstone.

Page 26: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log

None observed (see Key Sheet)

MBMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 3.00mRefusal at 3.00m

Records

Records

426.4823/01/2014 15:59:05(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS1Sheet 1 of 1

+132.09 mODE 383549.68N 354257.99

1.20 3.00 SPT hammer ID 110.49CB

*

0.00-0.070.10-0.15

0.200.20-0.50

0.700.80-1.00

1.101.20-1.651.20-1.651.20-2.50

2.00-2.45

2.502.602.752.90

3.00-3.383.00

B 1B 2

ES 3B 4

5B 6

ES 7SPT S

D 8B 9

SPT S

D 10D 11D 12D 13

SPT SD 14

N=9 (1,2/2,2,2,3)

N=9 (2,3/3,2,2,2)

50 (7,-/13,14,14,9 for 5mm)

dry

dry

dry

0.070.15

0.75

2.50

2.702.803.00

(0.60)

(1.75)

+132.02+131.94

+131.34

+129.59

+129.39+129.29

+129.09

MADE GROUND: macadam.

MADE GROUND: grey sandy GRAVEL with lowcobble content. Gravel is angular fine tocoarse concrete, brick and porcelain.Cobbles are concrete.

MADE GROUND: orangish brown slightlyclayey gravelly fine to medium SAND withhigh cobble content. Gravel is angular torounded fine to coarse igneous, concreteand quartz. Cobbles are igneous.

Loose brown silty very gravelly fine tocoarse SAND with low cobble content andoccasional bands of thin brown and blacksand and very occasional reddish brownbrown sand. Gravel is subangular tosubrounded fine to coarse sandstone.(GLACIOFLUVIAL DEPOSITS)

Reddish brown medium to coarse sandyGRAVEL of subrounded to rounded fine tomedium quartz and angular fine to coarsesandstone.(GLACIOFLUVIAL DEPOSITS)

Extremely weak black MUDSTONE.(PENNINE MIDDLE COAL MEASURESFORMATION)

Very stiff grey gravelly CLAY. Gravel isangular fine to coarse siltstone andreddish brown mudstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 3.00 m

1:50

Page 27: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole LogMBMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Service inspoection pit hand excavated to 1.20mWindowless sampler to 4.00mRefusal to 4.00m

Records

Records

426.4823/01/2014 15:59:15(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS2Sheet 1 of 1

+131.82 mODE 383600.14N 354237.98

0.901 - -2.002 - -

1.20 4.00 SPT hammer ID 110.49CB

*

4.00 m Possiblebedrock

0.00-0.050.200.20

0.500.50

1.001.10

1.20-1.651.201.20

1.902.00-2.45

2.00

2.50

3.00-3.453.10

3.50

4.00-4.444.00

B 1ES 2B 3

D 4ES 5

ES 6D 7

SPT SES 8D 9

D 10SPT SD 11

ES 12

SPT CD 13

D 14

SPT SD 15

N=2 (1,0/0,0,1,1)

N=7 (1,1/1,2,2,2)

N=10 (2,3/3,3,2,2)

50 (6,9/11,13,15,11 for 60mm)

0.05

0.25

0.75

1.80

2.00

3.40

4.00

(0.50)

(1.05)

(1.40)

(0.60)

+131.77

+131.57

+131.07

+130.02

+129.82

+128.42

+127.82

1

2

MADE GROUND: macadam.

MADE GROUND: black sandy GRAVEL ofangular fine to coarse brick, sandstone, clinkerand wood.

MADE GROUND: soft sandy gravelly CLAY withlow cobble content. Gravel is angularfine to coarse brick, sandstone and coal.Cobbles are brick and sandstone.

MADE GROUND: very soft dark grey slightlygravelly SILT with low cobble content.Gravel is angular fine coal. Cobbles aresandstone.

Firm reddish brown slightly sandy slightlygravelly CLAY. Gravel is angular finesandstone.(GLACIOFLUVIAL DEPOSITS)

Loose to medium dense grey and reddishbrown SAND and GRAVEL with occasionalreddish brown clay pockets. Sand is fineto medium. Gravel is angular fine tomedium sandstone.(GLACIOFLUVIAL DEPOSITS)

Firm grey slightly gravelly CLAY. Gravelis subangular fine mudstone and sandstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 4.00 m

1:50

Page 28: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log

None observed (see Key Sheet)

MBMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m

Records

Records

426.4823/01/2014 15:59:30(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS3Sheet 1 of 1

+132.76 mODE 383512.32N 354244.82

0.00 5.00 SPT hammer ID 110.49CB

*

4.00-5.00 m Norecovery

0.200.20-0.80

0.80

1.20-1.651.20

1.80

2.00-2.452.00

2.00-2.70

3.00-3.453.003.00

3.50-4.00

4.00-4.454.00

5.00-5.455.00

ES 1B 2

ES 3

SPT SD 4

ES 5

SPT SD 6B 7

SPT SES 8D 9

B 10

SPT SD 11

SPT SD 12

N=8 (1,2/2,2,2,2)

N=22 (3,4/5,5,6,6)

N=13 (2,3/3,3,3,4)

N=4 (1,1/1,1,1,1)

N=15 (2,3/3,4,4,4)

0.40

1.45

2.20

2.70

4.00

5.00

(0.40)

(1.05)

(0.75)

(0.50)

(1.30)

(1.00)

+132.36

+131.31

+130.56

+130.06

+128.76

+127.76

MADE GROUND: stiff brown slightly sandyslightly gravelly CLAY. Gravel is angularfine to coarse brick, concrete, coal andsandstone. Frequent rootlets. (Topsoil)

MADE GROUND: firm brown slightly sandyslightly gravelly CLAY. Gravel is angularfine to coarse brick, concrete, coal andsandstone.

MADE GROUND: dark grey slightly sandysilty GRAVEL with occasional stiff darkgrey silty clay pockets. Gravel is angularfine to coarse mudstone and siltstone.

MADE GROUND: medium dense light grey siltyvery sandy GRAVEL. Gravel is angular tosubrounded fine to coarse sandstone,igneous and quartz.

Medium dense reddish brown, becomingbrown, slightly gravelly silty fine tomedium SAND. Gravel is subrounded finesandstone.(Possible GLACIOFLUVIAL DEPOSITS)

No recoveryDescription of disturbed samples: softbrown CLAY.(Possible GLACIOFLUVIAL DEPOSITS)

EXPLORATORY HOLE ENDS AT 5.00 m

1:50

Page 29: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log

None observed (see Key Sheet)

MBMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m

Records

Records

426.4823/01/2014 15:59:37(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS4Sheet 1 of 1

+137.24 mODE 383534.16N 354183.40

1.20 5.00 SPT hammer ID 110.49CB

*

3.70-3.80 mStained black

0.200.30

0.40-0.600.50

0.70-1.000.80

1.20-1.651.201.40

1.60-2.00

2.00-2.452.00

2.60

2.80

3.00-3.453.00

3.70-3.80

4.00-4.454.00

4.50-5.00

5.00-5.455.00

ES 1D 2B 4

ES 3B 5

ES 6

SPT SD 7D 8

ES 9

SPT SD 10

D 11

ES 12

SPT SD 13

ES 14

SPT SD 15

D 16

SPT SD 17

N=1 (1,0/0,0,1,0)

N=2 (1,0/1,0,1,0)

N=11 (4,6/4,3,2,2)

N=4 (1,0/1,1,1,1)

N=8 (2,2/2,2,2,2)

0.60

1.00

1.55

2.50

3.40

3.70

5.00

(0.60)

(0.40)

(0.55)

(0.95)

(0.90)

(0.30)

(1.30)

+136.64

+136.24

+135.69

+134.74

+133.84

+133.54

+132.24

MADE GROUND: dark brown clayey gravellyfine to coarse SAND with low cobblecontent. Gravel is angular fine to coarsebrick, sandstone, steel, concrete, glassand polystyrene. Cobbles are concrete.Frequent rootlets.

MADE GROUND: orangish brown silty gravellyfine to medium SAND with frequent gravelsize reddish brown clay pockets. Gravel isangular fine clinker.

MADE GROUND: soft to firm orangish brownmottled black slightly sandy slightlygravelly CLAY. Gravel is subangular fineto medium mudstone.

MADE GROUND: soft brown slightly sandygravelly CLAY. Gravel is angular fine tocoarse mudstone, sandstone and siltstone.

MADE GROUND: firm reddish brown slightlygravelly sandy CLAY. Gravel is angularfine to medium sandstone and quartz.

MADE GROUND: black slightly sandy GRAVELof angular fine to medium clinker, quartzand glass.

Very loose to loose reddish brown,occasionally stained black, slightlygravelly fine SAND. Gravel is subroundedfine to mediium sandstone and quartz.(GLACIOFLUVIAL DEPOSITS)

EXPLORATORY HOLE ENDS AT 5.00 m

1:50

Page 30: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log

None observed (see Key Sheet)

MBMQJRL

15/10/2013

15/10/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 1.80mRefusal at 1.80m

Records

Records

426.4823/01/2014 15:59:45(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS5Sheet 1 of 1

+139.51 mODE 383684.17N 354076.17

1.20 1.80 SPT hammer ID 110.49CB

*

0.00-0.070.100.20

0.600.60-1.00

1.20-1.651.20

1.20-1.80

1.80-2.071.80

B 1ES 2ES 3

ES 4B 5

SPT SD 6B 7

SPT SD 8

N=46 (7,9/11,12,14,9)

50 (12,13 for 45mm/22,24,4 for 0mm)

0.070.150.25

1.00

1.80

(0.75)

(0.80)

+139.44+139.36+139.26

+138.51

+137.71

MADE GROUND:macadam.

MADE GROUND: black SAND and GRAVEL.Sand is coarse. Gravel is angular fine tocoarse brick, sandstone and clinker.

MADE GROUND: dark brown sandy gravellyCLAY. Gravel is angular fine to coarsesandstone and brick.

Firm light grey slightly sandy gravellyCLAY. Gravel is angular fine to coarsesiltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

Grey slightly gravelly sandy SILT tendingto extremely weak grey SILTSTONE. Gravelis subangular fine to medium siltstone.(PENNINE MIDDLE COAL MEASURESFORMATION)

EXPLORATORY HOLE ENDS AT 1.80 m

1:50

Page 31: Report No D3155-13 - apps2.staffordshire.gov.uk

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log

None observed (see Key Sheet)

MBMQJRL

14/10/2013

14/10/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m

Records

Records

426.4823/01/2014 15:59:53(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

National Grid

Chainage

WS6Sheet 1 of 1

+132.40 mODE 383683.55N 354176.57

1.20 5.00 SPT hammer ID 110.49CB

*

0.00-0.070.20

0.20-0.30

0.500.60

1.001.10

1.20-1.651.20

1.20-2.00

2.00-2.452.00

2.00-3.00

3.00-3.453.00

3.00-3.803.00

3.80

4.00-4.45

4.40

5.00-5.455.00

B 1ES 2B 3

D 4ES 5

ES 6D 7

SPT SD 8B 9

SPT SD 10B 11

SPT SD 12B 13D 14

B 15

SPT S

D 16

SPT SD 17

N=9 (2,2/2,2,2,3)

N=17 (2,3/4,5,4,4)

N=20 (2,3/4,5,5,6)

N=24 (5,5/6,6,6,6)

N=24 (5,6/6,6,6,6)

0.07

0.35

0.90

1.20

3.80

4.40

5.00

(0.28)

(0.55)

(0.30)

(2.60)

(0.60)

(0.60)

+132.33

+132.05

+131.50

+131.20

+128.60

+128.00

+127.40

MADE GROUND: macadam.

MADE GROUND: black brown slightly siltyvery sandy GRAVEL. Sand is fine to coarse.Gravel is angular to subangular fine tocoarse sandstone, igneous, macadam andsteel.

Soft orangish brown sandy CLAY with lowsandstone cobble content. Rare rootlets.(GLACIOFLUVIAL DEPOSITS)

Soft orangish brown slightly gravellysandy CLAY with low cobble content. Gravelis angular to subrounded fine to mediumsandstone. Cobbles are sandstone.(GLACIOFLUVIAL DEPOSITS)

Loose to medium dense orangish brown,occasionally stained black, slightlygravelly slightly silty fine to mediumSAND with occasional thin reddish brownsand bands. Gravel is rounded finepossible quartz.(GLACIOFLUVIAL DEPOSITS)

Medium dense orangish brown very sandyGRAVEL. Sand is fine to coarse. Gravel issubrounded to rounded fine to mediumquartz, mudstone and subangular coarsesandstone.(GLACIOFLUVIAL DEPOSITS)

Orangish brown slightly gravelly fine tomedium SAND. Gravel is angular tosubangular medium to coarse sandstone.(GLACIOFLUVIAL DEPOSITS)

EXPLORATORY HOLE ENDS AT 5.00 m

1:50

Page 32: Report No D3155-13 - apps2.staffordshire.gov.uk

Type & No.

Instruments

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

DateRecords

Samples and Tests

Ground Level

Project

Project No.Carried out for

Date

LengthWidth

No. Post Strike Behaviour(m)

StrataDepth

RecordsDescription Depth, Legend(Thickness)

Groundwater Entries

Dimensions and Orientation

Level

Struck

Notes: For explanation of symbols andabbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

From to (m)Stability

Shoring

Weather

Scale

Start

End

Depth Related Remarks *

Logged

Depth

Trial Pit Log

None observed (see Key Sheet)

MQ

JRL15/10/2013

15/10/2013

Hand excavated to 1.20m

426.4823/01/2014 15:49:40(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

0.50 m0.50 m - National Grid

Chainage

Trial Pit

Stable

None

TP1Sheet 1 of 1

+137.67 mODE 383571.46N 354159.53

0.00-0.07

0.25

0.50

0.70

1.001.00-1.20

B 1

ES 2

D 3

ES 4

ES 5B 6

0.05

0.20

0.75

1.20

(0.55)

(0.45)

+137.62

+137.47

+136.92

+136.47

1 MADE GROUND: macadam.

2 MADE GROUND: grey sandy GRAVEL of angular fine tocoarse limestone.

3 MADE GROUND: dark grey slightly sandy gravelly CLAYwith medium cobble content. Gravel is angular tosubrounded fine to coarse sandstone, concrete andquartz. Cobbles are igneous.

4 Brown gravelly clayey fine to medium SAND with lowcobble content. Gravel is angular fine to coarsesandstone. Cobbles are subangular sandstone.(Possible GLACIOFLUVIAL DEPOSITS)

EXPLORATORY HOLE ENDS AT 1.20 m

1:25

Type & No.

A

B

C

D

Page 33: Report No D3155-13 - apps2.staffordshire.gov.uk

Type & No.

Instruments

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

DateRecords

Samples and Tests

Ground Level

Project

Project No.Carried out for

Date

LengthWidth

No. Post Strike Behaviour(m)

StrataDepth

RecordsDescription Depth, Legend(Thickness)

Groundwater Entries

Dimensions and Orientation

Level

Struck

Notes: For explanation of symbols andabbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

From to (m)Stability

Shoring

Weather

Scale

Start

End

Depth Related Remarks *

Logged

Depth

Trial Pit Log

None observed (see Key Sheet)

MQ

JRL15/10/2013

15/10/2013

Hand excavated to 1.20m

426.4823/01/2014 15:50:37(c) ESG www.esg.co.uk

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

0.50 m0.50 m - National Grid

Chainage

Trial Pit

Stable

None

TP2Sheet 1 of 1

+137.44 mODE 383603.81N 354143.39

0.00-0.04

0.20

0.30

0.55

0.85-1.00

1.20

B 1

ES 2

ES 3

ES 4

B 5

ES 6

0.04

0.15

0.25

0.450.50

0.95

1.20

(0.45)

+137.40

+137.29

+137.19

+136.99+136.94

+136.49

+136.24

1 MADE GROUND: macadam.

2 MADE GROUND: black very sandy GRAVEL. Sand is mediumto coarse. Gravel is angular fine to medium slag,clinker and concrete.

3 MADE GROUND: light grey gravelly medium to coarseSAND. Gravel is angular fine to medium sandstone.

4 MADE GROUND: firm grey slightly sandy slightlygravelly CLAY. Gravel is angular fine to coarseconcrete.

5 MADE GROUND: extremely weak concrete

6 MADE GROUND: dark grey silty gravelly fine to coarseSAND with low cobble content. Gravel is angular fine tocoarse mudstone, sandstone and quartz. Cobbles aresubangular quartz.

7 MADE GROUND: orangish brown fine SAND with abundantcoarse gravel size reddish brown clay pockets.

EXPLORATORY HOLE ENDS AT 1.20 m

1:25

Type & No.

A

B

C

D

Page 34: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Enclosure B

ENCLOSURE B

INSTRUMENTATION AND MONITORING

Installation Details B1

Groundwater Monitoring B2 and B3

Gas Monitoring

Page 35: Report No D3155-13 - apps2.staffordshire.gov.uk

Hol

e N

o

Inst

rum

ent I

D

Inst

alla

tion

Typ

e

Dat

e of

Inst

alla

tion

Ref

eren

ce d

epth

(m

BG

L)

Pie

zom

eter

D

iam

eter

(m

m)

Top

of r

espo

nse

zone

(m

BG

L)

Bas

e of

res

pons

e zo

ne (

mB

GL)

Tub

ing

Com

plet

ion

Det

ails

Hea

dwor

ks Remarks

BH1 SP 17 Oct 2013 0.00 50 4.30 14.40 Gas tap Stop cock cover

BH2 SP 23 Oct 2013 0.00 50 3.50 26.00 Gas tap Stop cock cover

BH3 SP 10 Oct 2013 0.00 50 1.40 2.80 Gas tap Stop cock cover

BH4 SP 25 Oct 2013 0.00 50 0.75 13.90 Gas tap Stop cock cover

BH5 SP 25 Oct 2013 0.00 50 4.50 6.20 Gas tap Stop cock cover

Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Electronic Piezometer Prepared: 03/12/2013 11:37

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13 Education Funding Agency

Project

Project No.Carried out for

B1

Groundwater Installation Details

Sheet 1 of 1

Page 36: Report No D3155-13 - apps2.staffordshire.gov.uk

DateTime

(hhmmss)Comments

BH1 SP 14.3 0.00 7 Nov 2013 2.51

BH1 SP 14.3 0.00 12 Nov 2013 2.23

BH1 SP 14.3 0.00 14 Nov 2013 2.26

BH1 SP 14.3 0.00 26 Nov 2013 2.27

BH1 SP 14.3 0.00 29 Nov 2013 2.52

BH1 SP 14.3 0.00 3 Dec 2013 2.53

BH1 SP 14.3 0.00 23 Dec 2013 2.25

BH1 SP 14.3 0.00 30 Dec 2013 2.26

BH1 SP 14.3 0.00 3 Jan 2014 2.29

BH1 SP 14.3 0.00 10 Jan 2014 2.63

BH1 SP 14.3 0.00 13 Jan 2014 2.59

BH1 SP 14.3 0.00 17 Jan 2014 2.30

BH2 SP 26 0.00 7 Nov 2013 5.32

BH2 SP 26 0.00 12 Nov 2013 5.26

BH2 SP 26 0.00 14 Nov 2013 5.14

BH2 SP 26 0.00 26 Nov 2013 4.92

BH2 SP 26 0.00 29 Nov 2013 4.92

BH2 SP 26 0.00 3 Dec 2013 5.01

BH2 SP 26 0.00 23 Dec 2013 4.77

BH2 SP 26 0.00 30 Dec 2013 4.51

BH2 SP 26 0.00 3 Jan 2014 4.27

BH2 SP 26 0.00 10 Jan 2014 4.02

BH2 SP 26 0.00 13 Jan 2014 3.89

BH2 SP 26 0.00 17 Jan 2014 3.69

BH3 SP 2.8 0.00 7 Nov 2013 2.81

BH3 SP 2.8 0.00 12 Nov 2013 Dry

BH3 SP 2.8 0.00 14 Nov 2013 Dry

BH3 SP 2.8 0.00 26 Nov 2013 2.80

BH3 SP 2.8 0.00 29 Nov 2013 2.89

BH3 SP 2.8 0.00 3 Dec 2013 2.80

BH3 SP 2.8 0.00 23 Dec 2013 Dry

BH3 SP 2.8 0.00 30 Dec 2013 Dry

BH3 SP 2.8 0.00 3 Jan 2014 Dry

BH3 SP 2.8 0.00 10 Jan 2014 Dry

BH3 SP 2.8 0.00 13 Jan 2014 Dry

BH3 SP 2.8 0.00 17 Jan 2014 Dry

BH4 SP 13.9 0.00 7 Nov 2013 5.61

BH4 SP 13.9 0.00 12 Nov 2013 6.21

BH4 SP 13.9 0.00 14 Nov 2013 4.63

BH4 SP 13.9 0.00 26 Nov 2013 6.73

BH4 SP 13.9 0.00 29 Nov 2013 5.87

Hole ID

Inst

rum

ent I

D

Inst

rum

ent

Typ

e

Bas

e of

In

stru

men

t(m

BG

L)

Ref

eren

ce

Dep

th(m

BG

L)

Reading

Water Level (mBGL)

* calculated

Head(m above Tip)

* calculated

Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13 Education Funding Agency

Project

Project No.Carried out for

B2

Groundwater Monitoring

Page 37: Report No D3155-13 - apps2.staffordshire.gov.uk

DateTime

(hhmmss)Comments

BH4 SP 13.9 0.00 3 Dec 2013 5.86

BH4 SP 13.9 0.00 23 Dec 2013 6.01

BH4 SP 13.9 0.00 30 Dec 2013 6.06

BH4 SP 13.9 0.00 3 Jan 2014 5.77

BH4 SP 13.9 0.00 10 Jan 2014 6.06

BH4 SP 13.9 0.00 13 Jan 2014 5.94

BH4 SP 13.9 0.00 17 Jan 2014 5.31

BH5 SP 6 0.00 7 Nov 2013 5.70

BH5 SP 6 0.00 12 Nov 2013 3.69

BH5 SP 6 0.00 14 Nov 2013 5.48

BH5 SP 6 0.00 26 Nov 2013 5.25

BH5 SP 6 0.00 29 Nov 2013 5.11

BH5 SP 6 0.00 3 Dec 2013 5.29

BH5 SP 6 0.00 23 Dec 2013 5.36

BH5 SP 6 0.00 10 Jan 2014 4.39

BH5 SP 6 0.00 13 Jan 2014 4.38

BH5 SP 6 0.00 17 Jan 2014 4.18

Hole ID

Inst

rum

ent I

D

Inst

rum

ent

Typ

e

Bas

e of

In

stru

men

t(m

BG

L)

Ref

eren

ce

Dep

th(m

BG

L)

Reading

Water Level (mBGL)

* calculated

Head(m above Tip)

* calculated

Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well

CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13 Education Funding Agency

Project

Project No.Carried out for

B3

Groundwater Monitoring

Page 38: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH32.81 0.0

0.0 0.00.0BH3 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

1.1

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

20.0

0.8

-0.30 0.0

1.2

20.0 1.2 0.0

0.0

0.0

1.9

1.1

Gas tap open

21.1 0.0 0.00.0

DryLight

SlightNone

Gas tap open

20.1

21.4 0.0 0.0

20.2 1.2 0.0

2.1

2.1

21.2 0.5 1.9941.0

21.2 0.0 2.0

21.2 0.4 1.9

899.0

918.0

21.2 0.0 0.0

21.2 0.0 1.9

781.0

823.0

0.0 0.0

0.0

0.0

0.0 0.0

992 10

BH3 0.00 00:01:30

0.00 00:00:30

BH3 0.00 00:01:00 -0.100.0

0.0

0.0

-0.300.0

-0.30 0.00.0

BH3 0.00 00:02:00 -0.300.0

BH2 0.00

0.00

5.32

2.51 0.00.00.00 00:00:00

BH1 0.00

BH1 0.00 00:00:30

00:01:30

BH1

993

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH4 0.00 5.61

0.00 00:01:30

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

BH1

BH5

BH5 0.00 00:02:00 0.0

00:00:00

BH1 0.00 00:02:00

BH5

BH5 0.00 00:01:00

BH5 0.00 00:00:30

0.00 0.205.70

0.0

0.0

0.000.0

0.0

0.0

0.0 18.4

0.1

0.1

21.0

0.0

21.0

20.4

Reading Depth

(mBGL)

0.20.3

0.1

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

Equipment Used LMSxi 5429 + Dip

992

10

11

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00

CO(ppm)

1.00

07/11/2013

SW

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 39: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

12/11/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

3.7

3.3

2.6

2.4

0.7

1.5

0.6

1.6

2.2

17.3

16.4

Reading Depth

(mBGL)

5.05.2

4.3

0.1

0.1

0.2 14.6

3.3

2.6

2.0

18.9

0.2

0.1

0.10.0

0.00

0.00

0.1

0.0

0.000.0

0.00 0.00

BH5 0.00 00:02:00

BH5 0.00 00:01:30

00:01:00

00:00:30

BH5

BH4

BH5

BH5 0.00 00:03:00

0.0

0.0

0.0

0.000.0

0.00 00:02:30

BH5 0.00

BH5 0.00998 00:00:00 3.69 0.0

2.23

0.00

BH1 0.00

0.1

6.21

00:03:00

BH2 0.00

BH2 0.00

00:02:30

BH2 0.00 00:02:00 0.000.0

0.00 0.20.0

0.000.0

0.3

0.2

0.000.0

00:01:30

0.00 00:00:30

BH2 0.00 00:01:00

998

BH2 0.00 0.8 0.0

2.3

1.5

1.4 0.0

0.020.3 0.4 0.0

18.3 2.4 0.0

19.4 1.8 0.0

0.0

0.0

20.0 1.4 0.0

20.6 0.9 0.0

0.0

0.0

78.5

78.4

21.3

Flooded; unable to

79.0

gas monitor

Flooded; unable to

monitor

79.2

WetLight

SlightNone

82.981.5

79.3

19.5 0.6 0.0

20.0 0.5 0.0

1.4

1.1

0.0

0.0

0.0

78.3

78.2

0.0

78.3

78.3

81.0

80.1

79.6

21.1 0.5 0.0

0.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.2

0.0

0.00 1.4

0.4

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH25.26 0.0

1.7 0.02.7BH2 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 40: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

12/11/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5429 + Dip

0.8

0.0

21.6

21.6

Reading Depth

(mBGL)

1.30.3

0.5

0.0

0.0

0.0 21.4

0.6

0.2

0.7

21.6

0.000:03:00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

998

BH3 0.00 0.0 0.0

0.0

0.0

0.0 0.0

0.021.6 0.0 0.0 78.3

Light

SlightNone

78.578.3

78.3

21.6 0.0 0.0

21.6 0.0 0.0

0.0

0.0

78.3

78.3

78.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH3Dry 0.0

0.0 0.00.0BH3 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 41: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

14/11/2013

GM

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

995

995

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

1.7

17.2

14.1

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 16.6

0.0

0.0

0.0

18.4

0.0

0.0

0.0

0.0

0.00

0.00

0.0

0.00

00:01:00 0.00

BH5 0.00 00:02:30

00:02:00

BH5 0.00 00:00:00

00:00:30

00:01:30

BH5 0.00

BH5

BH4

BH3

0.0

BH3 0.00 00:00:30 0.0

BH3 0.00

BH3

0.0

-0.40Dry 0.00.0

-0.10

0.00 0.0

0.00 00:00:00

0.0

BH5 0.00

BH5 0.00 00:01:00 0.0

0.0

0.0

5.48 0.00.0 0.10

0.00 00:05:00

0.00 00:04:00

BH4 0.00 00:04:30

BH4

0.0

0.0

0.0

00:03:00

00:03:30BH4 0.00

BH4 0.00

BH4 0.00

00:02:30

BH4 0.00 00:02:00

0.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH4 0.00 00:01:00

995

BH4 0.00 1.2 0.0

0.0

0.0

1.6 0.0

20.3 0.5 0.0

0.0

0.0

19.7 0.7 0.0

20.4 0.4 0.0

20.5 0.4 0.0

0.0

0.0

20.6 0.4 0.00.0

20.9 0.4 0.0

21.0 0.3 0.0

0.0

0.0

21.1 0.2 0.0

21.2 0.1 0.0

0.0

0.0

21.3 0.0 0.0

21.3 0.0 0.0

0.0

0.0

-0.100.0

21.3

WetCalmNorth eastSlightSlight

18.7 1.1 0.0

19.2 0.9 0.0

0.0

0.0

0.0

0.00.0

0.0 21.4

0.0

0.0

0.00 00:01:30 -0.300.0BH3

0.0

BH3 0.00 00:02:30 0.00

00:02:00

0.0 0.00.0

21.4 0.0

-0.20

0.0 21.4

0.0

0.0 0.0 0.0

0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.5

0.0

0.00 0.0

0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH44.63 0.0

2.7 0.00.0BH4 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 42: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH25.14 0.0

0.7 0.01.1BH2 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.0

35.2

0.00 0.0

0.0

0.0 0.026.8

28.8

20.9 0.0 0.0

21.0 0.0

0.0 21.0

0.0

0.0

0.0

0.0

0.0 0.031.2BH1

0.0

BH1 0.00 00:06:00 0.0 2.0

00:05:30

0.00 00:05:00 -4.0

0.0

0.0

21.0

35.4

0.0

48.5

42.1

20.0 0.4 0.0

20.2 0.3 0.0

0.0

0.0

WetModerateNorth eastSlightSlight

21.0

BH1 0.00 00:06:30 0.0 21.1 0.0 0.026.40.0

20.7 0.0 0.0

20.8 0.0 0.0

66.7

55.2

20.5 0.0 0.0

20.6 0.0 0.0

104.0

81.0

20.5 0.0 0.0

20.1 0.0 0.0

126.0

142.0

20.9 0.0 0.00.0

20.7 0.1 0.0

20.8 0.0 0.0

0.0

0.0

20.6 0.2 0.0

0.0

0.0

20.4 0.2 0.0

0.4 0.0

0.0

0.0

0.4 0.0

995

BH2 0.00 00:01:30

0.00 00:00:30

BH2 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.0

BH2 0.00 00:02:00

00:02:30

BH2 0.00

BH2 0.00

BH2 0.00 00:03:00

00:03:30

0.0

0.0

0.0

0.00 00:04:00

BH2 0.00 00:04:30

BH2 0.00 00:05:00

0.0 0.00

00:01:00 0.0

0.0

0.0

2.26 0.0

BH1 0.00

BH1 0.00

0.00 -4.0

0.00 00:03:30

BH1

0.0

0.0

0.0

-4.0

-4.0

BH2

BH1

BH1 0.00 00:04:00 -3.0

BH1 0.00

00:02:00

BH1 0.00 00:00:00

00:00:30

00:01:30

BH1 0.00

BH1

BH1 0.00 00:03:00

BH1 0.00 00:02:30

0.00

00:04:30

0.0

-3.0

-4.0

0.00

0.00-4.0

0.0

0.0

0.0

0.0

0.0

0.0 19.5

0.0

0.0

0.0

19.9

0.6

19.7

18.4

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

996

0.0

0.0

0.0

0.0

0.0

0.0

Equipment Used LMSxi 1904 + Dip

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00

CO(ppm)

1.00

14/11/2013

GM

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 43: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH12.27 0.0BH1 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.3

32.4

0.00

0.0

77.9

21.1 0.1 0.0

21.3 0.00.5

78.6

78.3

0.0

0.0

78.2

78.1

78.127.9

0.0

42.4

39.2

78.9

22.0 0.0 0.0

21.0 0.0 0.0

0.0

49.8

DryCalm

CloudyNone

78.9

78.8

78.6

78.6

78.6

79.9

21.3

22.0 0.0 0.0

20.8 0.2 0.0

0.0

49.8

21.2 0.0 0.027.9

21.3 0.0 0.0

21.2 0.0 0.0

32.4

27.9

21.1 0.0 0.0

42.4

39.2

21.0 0.0 0.0

1011

BH1 0.00 00:01:30

0.00 00:00:30

BH1 0.00 00:01:00 0.000.0

0.000.0

0.000.0

BH1 0.00 00:02:00

00:02:30

BH1 0.00

BH1 0.00

BH1 0.00 00:03:00

00:03:30

0.0

0.0

0.0

0.00 00:04:00

BH1 0.00 00:04:30

BH1

0.00

0.00 00:05:00

0.0

0.0

4.92 0.0

0.0

BH2 0.00

BH2 0.00 00:01:00 0.0

0.00

0.00 00:03:30

BH2

0.5

0.5

0.5

BH1

BH2

BH2 0.00 00:04:00

00:02:00

BH2 0.00 00:00:00

00:00:30

00:01:30

BH2 0.00

BH2

BH2 0.00 00:03:00

BH2 0.00 00:02:30

0.00

00:04:30

0.4

0.0

0.0

0.00

0.00

0.00

0.0

0.0 0.0

0.0

Reading Depth

(mBGL)

0.0

0.0

0.0

0.0

9.0

9.0

10.0

11.7

1011

0.0

0.0

8.3

Equipment Used LMSxi 1904 + Dip

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

26/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 44: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

26/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

1009

0.0

0.3

0.2

0.0

0.0

0.0

0.0

0.0

0.0

0.2

0.0

0.0

Reading Depth

(mBGL)

0.1

0.0 0.2

3.4

0.0

0.0

0.0

0.00

0.0

0.00

00:05:30

BH4 0.00 00:04:00

BH4 0.00 00:03:30

00:03:00

BH4 0.00 00:01:00

00:01:30

00:02:30

BH4 0.00

BH4

BH3

BH4

BH4 0.00 00:05:00

BH4

0.0

0.0

0.0

0.00

0.00 00:04:30

0.0

BH4 0.00

BH4 0.00 00:02:00

6.73

0.0 0.00

0.00

0.00 00:00:00 0.000.0

0.0

0.00 00:04:00

BH4 0.00 00:00:30

BH4

0.0

0.0

0.0

00:03:00

00:03:30BH3 0.00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00

0.000.0

0.000.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

1010

BH3 0.00

21.3 0.0 0.0

0.0

0.0

21.2 0.0 0.0

21.3 0.0 0.00.0

22.0 0.0 0.0

1.1 4.3 0.0

0.0

0.0

1.8 4.3 0.0

3.7 3.8 0.0

0.0

1.0

94.3

93.0

7.8

77.9

78.7

78.6

78.6

DryCalm

CloudyNone

78.8

22.0 0.0 0.0

21.2 0.0 0.0

0.0

0.0

1.3

0.0

1.2

1.1

92.4

91.5

0.0

0.0

90.2

88.8

86.3

0.00 00:06:00BH4 2.7 0.01.3 86.3

10.9 2.7

0.0 10.9

0.0

77.9

4.6 3.7 0.0

3.2

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

6.1

1.3

0.00

3.4

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH32.80 0.0BH3 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 45: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 3Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH55.25 0.0BH5 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00

77.922.0 0.0 0.0

15.4 3.1 0.0

0.0

0.0

DryCalm

CloudyNone

80.2

79.6

79.7

79.619.4 0.9 0.0

19.4 0.9 0.0

0.0

0.0

18.8 1.3 0.0

19.1 1.1 0.0

0.0

0.0

18.1 1.9 0.0

0.0

0.0

17.3 2.2 0.0

1009

BH5 0.00 00:01:30

0.00 00:00:30

BH5 0.00 00:01:00 0.000.0

0.000.0

0.000.0

BH5 0.00 00:02:00

00:02:30

BH5 0.00

BH5 0.00

BH5 0.00 00:03:00

00:03:30

0.0

<<<<

<<<<

0.00 00:04:00

BH5 0.00 00:04:30

BH5 0.00 00:05:00

0.0

0.0

0.0

BH5

<<<<

0.0 0.0

>>>>

Reading Depth

(mBGL)

0.0

>>>>

>>>>

0.0

0.0

0.0

Equipment Used LMSxi 1904 + Dip

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

26/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 46: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

29/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxI 1904 + Dip

994

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

Reading Depth

(mBGL)

0.0

0.0 0.0

0.0

0.0

0.0

0.00

0.00

0.0

0.00

00:05:00

BH2 0.00 00:03:30

BH2 0.00 00:03:00

00:02:30

BH2 0.00 00:00:30

00:01:00

00:02:00

BH2 0.00

BH2

BH1

BH2

BH2 0.00 00:04:30

BH2

0.0

0.0

0.0

0.00

0.00 00:04:00

0.0

BH2 0.00

BH2 0.00 00:01:30 0.0

0.0

4.92

0.0 0.00

0.000.0

0.00 00:04:00

BH2 0.00

BH1 0.00 00:04:30

00:00:00

0.0

0.0

0.0

00:03:00

00:03:30BH1 0.00

BH1 0.00

BH1 0.00

00:02:30

BH1 0.00 00:02:00

-1.10-2.0

-1.10-2.0

-1.00-2.0

00:01:30

0.00 00:00:30

BH1 0.00 00:01:00

996

BH1 0.00

21.6 0.0 0.0

26.2

11.3

21.5 0.0 0.0

21.6 0.0 0.0

21.6 0.0 0.0

9.7

9.7

21.9 0.0 0.00.0

19.8 0.7 0.0

20.4 0.5 0.0

0.0

0.0

78.0

79.4

21.3

78.5

78.3

78.3

78.3

DryCalm

CloudyNone

79.0

21.9 0.0 0.0

20.9 0.0 0.0

0.0

49.6

0.0

0.0

0.0

0.0

79.0

78.8

0.0

0.0

78.7

78.6

78.621.3 0.00.0

78.0

20.9 0.2 0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.1

0.0

-1.10

0.1

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH12.52 -2.0BH1 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 47: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

29/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

994

0.0

3.0

2.8

1.5

1.0

1.1

1.0

0.0

0.0

0.0

Reading Depth

(mBGL)

0.0

0.0 0.0

0.0

0.0

0.3

0.4

0.00

0.2

0.00

BH4 0.00 00:04:00

BH4 0.00 00:03:30

00:03:00

BH4 0.00 00:01:00

00:01:30

00:02:30

BH4 0.00

BH4

BH3

BH4

BH4 0.00 00:05:00

0.1

0.1

0.10.00 00:04:30

0.0

BH4 0.00

BH4 0.00 00:02:00

5.87

0.0 0.00

0.00

0.00 00:00:00 0.000.0

0.0

0.00 00:04:00

BH4 0.00 00:00:30

BH4

0.0

0.0

0.0

00:03:00

00:03:30BH3 0.00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00

0.000.0

0.000.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

994

BH3 0.00

20.6 0.2 0.0

0.0

0.0

20.5 0.2 0.0

20.6 0.2 0.00.0

21.9 0.0 0.0

0.6 6.9 0.0

0.0

0.0

2.0 5.3 0.0

5.5 5.0 0.0

0.0

0.0

92.1

90.3

7.6

78.0

79.2

79.1

79.1

DryCalm

CloudyNone

79.2

21.9 0.0 0.0

20.5 0.2 0.0

0.0

0.0

0.0

0.0

0.0

88.9

87.7

0.0

87.7

87.7

78.0

8.8 4.1 0.0

4.6

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

7.6

0.0

0.00

4.6

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH32.89 0.0BH3 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 48: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 3Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

29/11/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

0.0

0.0

0.0

0.0

0.0

Reading Depth

(mBGL)

0.0

0.0 0.0

0.0

BH5

0.0

0.00.00 00:05:00

0.00 00:04:00

BH5 0.00 00:04:30

BH5

0.0

0.0

0.0

00:03:00

00:03:30BH5 0.00

BH5 0.00

BH5 0.00

00:02:30

BH5 0.00 00:02:00

0.000.0

0.000.0

0.000.0

00:01:30

0.00 00:00:30

BH5 0.00 00:01:00

994

BH5 0.00

14.2 4.6 0.0

0.0

0.0

13.4 5.1 0.0

15.2 4.0 0.0

16.3 3.3 0.0

0.0

0.0

16.3 3.3 0.00.0

81.6

81.1

80.7

80.4

80.4

DryCalm

CloudyNone

82.2

21.9 0.0 0.0

11.9 5.7 0.0

0.0

0.0

78.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH55.11 0.0BH5 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 49: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

03/12/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

21.4

21.4

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 21.9

0.0

0.0

0.0

21.6

0.0

0.0

0.00.0

0.00

0.00

0.0

0.0

0.000.0

0.00 0.00

BH3 0.00 00:02:00

BH3 0.00 00:01:30

00:01:00

BH2 0.00 00:02:30

00:00:30

BH3

BH2

BH3

0.0

0.00.00 00:02:30

BH3 0.00

BH3 0.00998 00:00:00 2.80 0.0

0.0

0.0

0.0

0.0

0.000.0

0.00 00:01:30 0.000.0

0.00 00:00:30

BH2 0.00

BH2 0.00 00:01:00

00:02:00

BH2

0.0

5.01 0.00.0

0.0

0.00

0.00

00:00:00BH2 0.00

BH1 0.00

998

00:02:30

BH1 0.00 00:02:00

-1.50 0.0-3.0

-1.50-3.0

0.0

0.0

-1.70-3.0

00:01:30

0.00 00:00:30

BH1 0.00 00:01:00

999

BH1 0.00 0.0 0.0

16.0

11.1

0.0 0.0

21.9 0.0 0.00.0

19.5 0.9 0.0

20.1 0.6 0.0

0.0

0.0

20.6 0.4 0.0

21.1 0.2 0.0

0.0

0.0

21.1 0.2 0.00.0

0.0

21.9 0.0 0.0

20.9 0.1 0.0

0.0

0.0

21.1 0.0 0.0

21.2 0.0 0.0

0.0

0.0

78.9

78.8

78.0

78.0

79.5

78.6

78.6

79.2

78.8

DryCalm

CloudyNone

78.078.5

78.5

21.4 0.0 0.0

21.4 0.0 0.0

15.1

13.6

0.0

0.0

0.0

78.7

78.6

78.6

78.5

78.3

78.5

21.3 0.0 0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.3

-10.00 0.0

0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH12.53 -30.0

0.0 0.018.3BH1 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 50: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH45.86 0.0

7.1 0.00.0BH4 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

0.6

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

20.2

0.0

0.00 0.0

0.6

91.3

90.3

88.8

20.1 0.7 0.0

79.1

79.1

0.0

79.1

79.1

0.0

0.0

0.0

87.2

5.7 5.1 0.0

8.1 4.5 0.0

0.0

0.0

DryCalm

CloudyNone

78.091.3

86.4

86.2

85.7

78.0

83.3

82.9

83.3

79.5

79.2

20.2

80.1

19.3 1.4 0.0

19.8 1.0 0.0

0.0

0.0

16.6 3.2 0.0

18.3 2.0 0.0

0.0

0.0

21.9 0.0 0.00.0

14.0 2.6 0.0

14.0 2.6 0.0

0.0

0.0

10.5 3.7 0.0

14.7 2.2 0.0

0.0

0.0

9.7 3.9 0.0

0.0

0.0

9.3 4.1 0.0

6.3 0.0

0.0

0.0

6.7 0.0

998

BH4 0.00 00:01:30

0.00 00:00:30

BH4 0.00 00:01:00 0.000.0

0.4

0.2

0.000.0

0.00 0.30.0

BH4 0.00 00:02:00

00:02:30

BH4 0.00

BH4 0.00

BH4 0.00 00:03:00

00:03:30

0.0

0.0

0.0

0.00 00:04:00

BH4 0.00

BH4 0.00 00:05:00

00:06:00

BH4 0.00 00:05:30

0.0

0.0

0.0

0.0

BH5 0.00

BH5 0.00 00:00:30 0.0

0.00 00:03:00

0.0

0.0

0.0

BH4

BH5

BH5 0.00 00:03:30

00:01:30

00:00:00

00:01:00

BH5 0.00998

BH5

BH5 0.00 00:02:30

BH5 0.00 00:02:00

0.00 0.00

0.0

0.0

0.0

0.0

0.0

0.00.0

5.29

0.00

0.00

0.00

0.1

0.2

0.0 21.9

1.8

1.8

1.0

2.9

0.0

1.8

0.8

Reading Depth

(mBGL)

0.03.0

1.8

0.6

0.2

0.3

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

Equipment Used LMSxi 1904 + Dip

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

03/12/2013

CH

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 51: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

23/12/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

1.6

0.0

0.0

7.0

6.0

5.2

Reading Depth

(mBGL)

0.01.9

2.1

0.2

0.3

0.4 4.3

1.8

1.5

1.4

6.8

0.0

0.0

0.0Dry

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH3 0.00 00:01:00

BH3 0.00 00:00:30

00:00:00

BH5 0.00 00:02:00

00:02:30BH5 0.00

BH3

BH5

BH3

BH3 0.00 00:02:00 0.0

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH5 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH5 0.00

BH5 0.00 00:00:30

00:01:30

BH5

0.3

5.36 0.00.0

00:03:00

0.00

BH4 0.00

BH4 0.00

00:02:30

BH4 0.00 00:02:00 0.000.0

0.00 0.30.0

0.000.0

0.3

0.2

0.000.0

00:01:30

0.00 00:00:30

BH4 0.00 00:01:00

BH4 0.00 6.3 0.0

0.0

0.0

6.6 0.0

0.09.2 5.6 0.0

18.9 2.9 0.0

19.2 2.6 0.0

0.0

0.0

19.6 2.3 0.0

20.0 1.7 0.0

0.0

0.0

20.5 1.2 0.0

20.9 0.7 0.0

0.0

0.0

21.2 0.1 0.00.0

18.1 0.8 0.0

18.4 0.5 0.0

0.0

0.0

81.0

19.3

78.6

84.7

78.1

78.3

78.2

78.2

78.1

78.0

WetModerateWesterlyCloudyModerate

88.687.6

85.6

7.5 6.1 0.0

8.3 5.8 0.0

0.0

0.0

0.0

0.0

0.0

0.0

81.0

80.8

0.0

0.0

80.6

80.4

80.1

0.00 00:03:00BH3 0.1 0.00.0 79.9

19.6 0.2

0.0 19.9

0.0

87.8

86.5

86.0

18.7 0.4 0.0

0.2

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

19.0

0.0

0.00 0.0

0.3

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH46.01 0.0

6.8 0.00.0BH4 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 52: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

23/12/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

0.0

0.0

0.0

0.0

0.0

0.8

0.0

0.0

1.8

19.2

18.5

Reading Depth

(mBGL)

2.52.6

2.1

0.0

0.0

0.1 18.1

1.6

1.3

1.0

19.8

0.0

0.0

BH1 0.00 00:02:00

00:02:30BH1 0.00

BH1

BH1 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH1 0.00

BH1 0.00 00:00:30

00:01:30

BH1

0.0

2.25 0.00.0

00:03:00

0.00

BH2 0.00

BH2 0.00

00:02:30

BH2 0.00 00:02:00 0.000.0

0.00 0.10.0

0.000.0

0.2

0.1

0.000.0

00:01:30

0.00 00:00:30

BH2 0.00 00:01:00

BH2 0.00 1.0 0.0

0.0

0.0

1.4 0.0

0.021.4 0.0 0.0

19.9 0.6 0.0

30.3 0.5 0.0

0.0

0.0

20.5 0.4 0.0

20.6 0.3 0.0

0.0

0.0

20.7 0.2 0.0

20.7 0.2 0.0

0.0

0.0

20.8 0.1 0.00.0 79.0

78.5

79.4

79.0

79.0

79.0

79.1

79.0

WetModerateWesterlyCloudyModerate

79.979.5

78.7

20.4 0.6 0.0

21.0 0.2 0.0

0.0

0.0

79.2

79.0

78.9

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH24.77 0.0

1.6 0.00.0BH2 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 53: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

30/12/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.9

0.0

0.0

8.4

5.9

5.8

Reading Depth

(mBGL)

1.61.5

1.9

0.2

0.2

0.5 6.1

1.3

0.8

0.7

6.3

0.0

0.0

0.04.51

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH2 0.00 00:01:00

BH2 0.00 00:00:30

00:00:00

BH3 0.00 00:02:00

00:02:30BH3 0.00

BH2

BH3

BH2

BH2 0.00 00:02:00 0.0

BH2

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH3 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH3 0.00

BH3 0.00 00:00:30

00:01:30

BH3

0.2

Dry 0.00.0

00:03:00

0.00

BH4 0.00

BH4 0.00

00:02:30

BH4 0.00 00:02:00 0.000.0

0.00 0.30.0

0.000.0

0.4

0.3

0.000.0

00:01:30

0.00 00:00:30

BH4 0.00 00:01:00

BH4 0.00 7.3 0.0

0.0

0.0

7.6 0.0

0.07.2 6.3 0.0

19.0 0.3 0.0

19.9 0.2 0.0

0.0

0.0

20.5 0.1 0.0

20.9 0.1 0.0

0.0

0.0

21.2 0.0 0.0

21.5 0.0 0.0

0.0

0.0

21.6 0.0 0.00.0

21.4 0.0 0.0

21.2 0.2 0.0

0.0

0.0

78.5

21.1

78.3

86.2

80.6

78.4

78.9

78.7

79.8

79.3

WetModerateSoutherlyCloudyModerate

85.085.7

85.2

6.6 7.0 0.0

6.9 6.7 0.0

0.0

0.0

0.0

0.0

0.0

0.0

78.6

78.4

0.0

0.0

78.5

78.5

78.6

0.00 00:03:00BH2 0.2 0.00.0 78.6

21.1 0.2

0.0 21.1

0.0

86.1

86.0

86.1

21.2 0.3 0.0

0.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.1

0.0

0.00 0.0

0.3

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH46.06 0.0

8.0 0.00.0BH4 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 54: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

30/12/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

0.0

0.3

20.3

20.2

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 20.1

0.0

0.0

0.0

20.3

BH5 0.00

0.000:03:00

BH1 0.00

BH1 0.00

00:02:30

BH1 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH1 0.00 00:01:00

BH1 0.00 0.2 0.0

0.0

0.0

0.2 0.0

0.020.4 0.1 0.0

No access

79.4

WetModerateSoutherlyCloudyModerate

79.579.4

79.4

20.3 0.2 0.0

20.4 0.1 0.0

0.0

0.0

79.4

79.4

79.4

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH12.26 0.0

0.3 0.00.0BH1 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 55: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

03/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

988

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

1.2

18.1

17.8

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 16.5

0.0

0.0

0.0

18.0

0.0

0.0

0.02.29

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH1 0.00 00:01:00

BH1 0.00 00:00:30

00:00:00

BH2 0.00 00:02:00

00:02:30BH2 0.00

BH1

BH2

BH1

BH1 0.00 00:02:00 0.0

BH1

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH2 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH2

988

0.0

4.27 0.00.0

00:03:00

0.00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

988

BH3 0.00 0.8 0.0

0.0

0.0

0.8 0.0

0.018.5 0.7 0.0

20.8 0.0 0.0

21.3 0.0 0.0

0.0

0.0

21.1 0.1 0.0

21.1 0.0 0.0

0.0

0.0

21.1 0.0 0.0

21.2 0.0 0.0

0.0

0.0

21.2 0.0 0.00.0

19.5 0.4 0.0

19.7 0.4 0.0

0.0

0.0

80.0

20.0

78.7

80.7

79.1

78.7

78.8

78.8

78.7

78.8

DampLightSouth westerlySlightSlight

82.781.1

80.9

18.1 0.8 0.0

18.2 0.7 0.0

0.0

0.0

0.0

0.0

0.0

0.0

79.8

79.7

0.0

0.0

79.6

79.6

79.5

0.00 00:03:00BH1 0.2 0.00.0 79.5

20.1 0.3

0.0 20.2

0.0

81.0

81.1

81.0

19.9 0.3 0.0

0.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

20.0

0.0

0.00 0.0

0.3

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH3Dry 0.0

0.9 0.00.0BH3 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 56: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

03/01/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 5427 + Dip

Reading Depth

(mBGL)

00:00:00BH5 0.00

DryLightSouth westerlySlightSlight

to monitor

No access

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

Under water; unable5.77BH4 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 57: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

10/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

981

2.7

2.7

2.9

0.0

0.0

0.0

2.8

2.8

0.0

0.0

0.0

0.0

0.0

2.0

2.8

0.8

21.6

21.6

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 21.1

0.0

0.0

0.0

21.6

0.4

0.4

0.04.39

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH5 0.00 00:01:00

BH5 0.00 00:00:30

00:00:00

BH2 0.00 00:02:00

00:02:30BH2 0.00

BH5

BH2

BH5

BH5 0.00 00:02:00 0.0

BH5

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH2 0.00 00:03:00

0.4

0.3

0.4

0.4

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH2

981

0.0

4.02 0.30.0

00:03:00

0.00

BH1 0.00

BH1 0.00

00:02:30

BH1 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH1 0.00 00:01:00

981

BH1 0.00 0.1 0.0

0.0

0.0

0.3 0.0

0.021.6 0.0 0.0

2.0 6.1 0.0

2.2 6.1 0.0

0.0

0.0

1.9 6.2 0.0

1.7 6.2 0.0

0.0

0.0

1.5 6.2 0.0

1.3 6.1 0.0

0.0

0.0

1.2 6.2 0.00.0

10.1 7.8 0.0

9.8 6.6 0.0

0.0

0.0

10.1

DampModerateSouth eastCloudyNone

21.6 0.1 0.0

21.6 0.0 0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.00 00:03:00BH5 3.7 0.00.0

10.1 4.1

0.0 10.1

0.0

9.9 5.6 0.0

4.4

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

10.0

0.0

0.00 0.0

4.8

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH12.63 0.0

0.6 0.00.0BH1 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 58: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

10/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

2.1

2.2

2.2

2.2

2.2

0.0

2.1

2.1

0.0

21.6

21.4

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 21.2

0.0

0.0

0.0

21.6

0.4

0.3

BH4 0.00 00:02:00

00:02:30BH4 0.00

BH4

BH4 0.00 00:03:00

0.3

0.3

0.4

0.4

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH4 0.00

BH4 0.00 00:00:30

00:01:30

BH4

981

0.0

6.06 0.30.0

00:03:00

0.00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

981

BH3 0.00 0.0 0.0

0.0

0.0

0.0 0.0

0.021.6 0.0 0.0

2.0 6.0 0.0

2.1 5.8 0.0

0.0

0.0

2.0 5.9 0.0

1.9 5.9 0.0

0.0

0.0

1.8 5.9 0.0

1.7 5.8 0.0

0.0

0.0

1.6 5.8 0.00.0

DampModerateSoutherlyCloudyNone

21.6 0.0 0.0

21.6 0.0 0.0

0.0

0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH3Dry 0.0

0.0 0.00.0BH3 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 59: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

13/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

973

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

7.4

8.6

7.5

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 6.5

0.0

0.0

0.0

8.7

0.0

0.0

0.02.59

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH1 0.00 00:01:00

BH1 0.00 00:00:30

00:00:00

BH3 0.00 00:02:00

00:02:30BH3 0.00

BH1

BH3

BH1

BH1 0.00 00:02:00 0.0

BH1

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH3 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH3 0.00

BH3 0.00 00:00:30

00:01:30

BH3

973

0.0

Dry 0.00.0

00:03:00

0.00

BH5 0.00

BH5 0.00

00:02:30

BH5 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH5 0.00 00:01:00

973

BH5 0.00 4.6 0.0

0.0

0.0

5.3 0.0

0.09.7 3.9 0.0

21.1 0.0 0.0

21.8 0.0 0.0

0.0

0.0

21.8 0.0 0.0

21.8 0.0 0.0

0.0

0.0

21.8 0.0 0.0

21.8 0.0 0.0

0.0

0.0

21.8 0.0 0.00.0

20.6 0.5 0.0

21.5 0.4 0.0

0.5

0.4

78.8

21.5

78.1

86.3

78.8

78.1

78.1

78.1

78.1

78.1

DampCalm

CloudyNone

86.086.4

86.5

9.1 4.1 0.0

9.4 3.9 0.0

0.0

0.0

0.2

0.0

0.2

0.3

78.1

77.5

0.0

0.0

78.1

78.1

78.2

0.00 00:03:00BH1 0.2 0.00.2 78.2

21.5 0.2

0.0 21.5

0.0

86.7

86.7

86.7

22.3 0.2 0.0

0.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.5

0.3

0.00 0.0

0.3

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH54.38 0.0

6.2 0.00.0BH5 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 60: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

13/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

2.8

2.7

2.8

2.4

3.0

0.0

2.4

2.8

0.1

21.6

21.6

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 20.9

0.0

0.0

0.0

21.6

0.4

0.4

BH4 0.00 00:02:00

00:02:30BH4 0.00

BH4

BH4 0.00 00:03:00

0.4

0.4

0.3

0.4

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH4 0.00

BH4 0.00 00:00:30

00:01:30

BH4

973

0.0

5.94 0.40.0

00:03:00

0.00

BH2 0.00

BH2 0.00

00:02:30

BH2 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH2 0.00 00:01:00

973

BH2 0.00 0.0 0.0

0.0

0.0

0.0 0.0

0.021.6 0.0 0.0

1.6 5.7 0.0

2.2 5.6 0.0

0.0

0.0

1.8 5.8 0.0

1.5 5.8 0.0

0.0

0.0

1.4 5.7 0.0

1.3 5.8 0.0

0.0

0.0

1.2 5.9 0.00.0 92.4

78.3

92.2

92.3

92.1

92.4

91.8

91.8

DampCalm

CloudyNone

78.978.3

78.3

21.6 0.0 0.0

21.6 0.0 0.0

0.0

0.0

78.3

78.3

78.3

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH23.89 0.0

0.0 0.00.0BH2 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 61: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

17/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

958

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.7

20.8

20.8

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 20.3

0.0

0.0

0.0

20.8

0.0

0.0

0.0Dry

0.0

0.0

0.000.0

0.00

00:02:30

0.00

BH3 0.00 00:01:00

BH3 0.00 00:00:30

00:00:00

BH2 0.00 00:02:00

00:02:30BH2 0.00

BH3

BH2

BH3

BH3 0.00 00:02:00 0.0

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

0.00

0.00 00:01:30

BH2 0.00 00:03:00

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH

959

0.0

3.69 0.00.0

00:03:00

0.10

BH1 0.00

BH1 0.00

00:02:30

BH1 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH1 0.00 00:01:00

959

BH1 0.00 0.7 0.0

0.0

0.0

0.7 0.0

0.020.9 0.7 0.0

21.1 0.1 0.0

21.8 0.0 0.0

0.0

0.0

21.8 0.0 0.0

21.7 0.0 0.0

0.0

0.0

21.7 0.0 0.0

21.8 0.0 0.0

0.0

0.0

21.8 0.0 0.00.0

21.2 0.0 0.0

21.8 0.0 0.0

0.0

0.0

78.7

21.7

78.1

78.3

78.7

78.1

78.2

78.2

78.1

78.1

DampCalm

CloudyNone

78.978.4

78.3

20.8 0.7 0.0

20.9 0.7 0.0

0.0

0.0

0.0

0.0

0.0

0.0

78.1

78.1

0.0

0.0

78.2

78.2

78.2

0.00 00:03:00BH3 0.0 0.00.0 78.2

21.7 0.0

0.0 21.7

0.0

78.4

78.4

78.4

21.8 0.0 0.0

0.0

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

21.7

0.0

0.00 0.0

0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH12.30 0.0

0.7 0.00.0BH1 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 62: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Sheet No

Date State of Ground 2Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

17/01/2014

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3155-13

CH4(% LEL)

0.10 0.100.10

CLOUGH HALL TECHNOLOGY SCHOOL

1.00 0.10

CO(ppm)

1.00

Equipment Used LMSxi 1904 + Dip

958

0.0

0.0

0.0

8.7

0.0

0.0

2.5

0.0

6.0

0.3

0.5

Reading Depth

(mBGL)

2.02.0

2.0

0.3

0.3

0.3 1.2

2.0

2.0

2.1

0.3

0.0

0.0

0.0

0.00

BH5 0.00 00:01:30

00:02:00

00:03:00

BH5 0.00 0.0

BH5 0.00

BH5 0.00 00:02:30

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

4.18

0.00

0.00 00:00:30 0.000.0

0.0BH5 0.00

BH5 0.00 00:00:00

00:01:00

BH5

0.400:03:00

BH4 0.00

BH4 0.00

00:02:30

BH4 0.00 00:02:00 0.000.0

0.00 0.30.0

0.000.0

0.3

0.3

0.000.0

00:01:30

0.00 00:00:30

BH4 0.00 00:01:00

958

BH4 0.00 6.0 0.0

0.0

0.0

6.1 0.0

0.00.2 5.9 0.0

6.5 6.0 0.00.0

6.6 6.2 0.0

5.7 6.1 0.0

0.0

0.0

5.0 6.0 0.0

4.6 6.0 0.0

0.0

0.0

4.2 5.9 0.0

4.0 5.9 0.0

0.0

0.0 87.2

87.2

93.4

87.2

86.7

87.0

85.7

86.1

DampCalm

CloudyNone

92.492.8

93.5

0.2 6.0 0.0

0.2 5.9 0.0

0.0

0.0

93.2

93.2

93.5

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

BH45.31 0.0

6.2 0.00.0BH4 0.00 00:00:00

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03

Page 63: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Enclosure C

ENCLOSURE C

GEOTECHNICAL LABORATORY TEST RESULTS

Determination of Moisture Content and Atterberg Limits INDX 1

Particle Size Distribution Analyses PSD 1 to 21

Soil Sample Analysis ESG Scientifics Report No EFS/136829

Chemical Tests – Summary of Results CHEM 1 Determination of Moisture Content/Dry Density Relationship (Light 2.5kg Compaction) COMPL 1

Determination of Moisture Content/Moisture Condition Value MCVREL 1 to 4

Determination of California Bearing Ratio CBR 1

One Dimensional Consolidation Test OED 1 to 4 Unconsolidated Undrained Triaxial Compression Tests – Summary of Results UUSUM 1

Unconfined Compressive Strength RUCS 1

Point Load Index PLT 1

Page 64: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Name

p p d w < 425 WL WP IP p sµm

sieve

from to % % % % Mg/m3

10 1.00 DGreyish brown slightly gravelly sandy silty CLAY.

22 90 s 28 a 16 12

20 3.70 4.00 BBrown slightly sandy slightly gravelly CLAY.

27 58 s 32 a 18 14

11 1.50 1.95 UStiff grey friable slightly sandy CLAY with siltstone.

15 100 n 44 a 23 21

12 2.05 DGrey slightly sandy silty CLAY.

11 100 n 39 a 21 18

16 3.50 3.60 DDark grey sandy sliightly silty GRAVEL.

8.5

9 1.95 UBrown slightly gravelly SAND.

16 69 s 24 b NP

10 2.05 0.00 DBrown slightly sandy slightly gravelly CLAY.

19 97 s 32 a 17 15

14 3.00 3.10 DLight grey and cream slightly sandy GRAVEL.

1.6

10 1.50 1.95 UVery stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.

9.5 100 n 38 a 19 19

12 2.50 2.90 DGreyish brown slighty sandy slightly gravelly silty CLAY Gravel is siltstone.

6.1 79 s 36 a 21 15

14 3.50 3.90 DDark grey slightly gravelly silty CLAY.

8.5 69 s 40 a 22 18

3 0.25 DBrownish grey slightly gravelly silty CLAY.

18 87 s 39 a 20 19

8 2.05 DBrown slightly sandy slightly gravelly CLAY.

14 75 s 35 a 18 17

16 3.50 4.95 DGreyish brown slightly gravelly sandy silty CLAY.

1.9 73 s 37 a 20 17

20 6.15 6.20 DLight greyish brown slightly sandy SILT.

6.7

3 0.50 DGrey slightly sandy slightly gravelly CLAY.

19 90 s 40 a 20 20

10 2.50 DBrown slightly gravelly SAND.

7.3 29 s 22 b NP

14 3.00 DGreyish brown slightly gravelly sandy silty CLAY.

7.3 51 s 38 a 21 17

4 0.50 DDark brown and grey sandy gravelly CLAY.

14 39 s 29 a 17 12

7 1.10 DDark greyish brown slightly sandy slightly gravelly CLAY.

28 75 s 35 a 22 13

10 1.90 DBrown slightly gravelly very sandy CLAY.

14 78 s 25 a 15 10

14 3.50 DGrey and brown slightly sandy slightly gravelly silty CLAY.

16 81 s 36 a 18 18

15 4.00 DGreyish brown slightly gravelly sandy silty CLAY.

12 80 s 44 a 25 19

4 1.20 DDark grey slightly gravelly sandy CLAY.

16 52 s 42 b 25 17

11 4.00 DDark brown slightly sandy slightly gravelly CLAY.

26 96 s 35 a 18 17

8 1.40 DOrangish brown slightly sandy slightly gravelly CLAY.

21 91 s 34 a 13 21

11 2.60 DReddish brown slightly sandy slightly gravelly CLAY.

17 79 s 30 a 14 16

6 1.20 DLight greyish brown slightly sandy slightly gravelly silty CLAY.

6.8 66 s 41 a 21 20

8 1.80 DLight grey slightly gravelly SILT. Gravel is siltstone.

6.7

7 1.10 DLight brown slightly gravelly very clayey SAND.

11 68 s 26 a 14 12

General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.

Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density

p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar

w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer

QA Ref

WS6

WS4

WS4

WS5

WS5

WS2

WS2

WS3

WS3

WS1

WS2

WS2

WS2

BH5

BH5

TP1

WS1

BH4

BH4

BH5

BH5

BH3

BH3

BH3

BH4

BH1

BH2

BH2

BH2

CLOUGH HALL TECHNOLOGY SCHOOL

INDEX PROPERTIES - SUMMARY OF RESULTS

Soil Description

D3155-13

SLR 1Rev 91Mar 12

BH1

Hole No.

Printed:04/12/2013 14:08

Mg/m3

INDX 1

Remarks

Plasticity Index

Sample

Depth (m)No. type

Table

Page 65: Report No D3155-13 - apps2.staffordshire.gov.uk

2117

08542117

0.0048Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0354

%Passing

100756350

9593

0.0015

870.6001.18 91

9728

9796

97201410

14.3

2.65

0.063 390.150

790.425

6453

0.300

Particle density, Mg/m3

5.0

92

95

3.352.00

6.3

89

Clay

Sample Proportions

*<60mm values to aid description only

Sand

20

Silt

17 Cobbles / boulders

2521

Gravel

Remarks

854

Soil description%Passing

Brown slightly gravelly sandy CLAY.

3310010097

0.02540.01800.009537.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0494

3936

3029

PSD 1

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH1

11 B

ESGD3155-13201311040000000008

QA Ref

SLR 2,9Rev 88Aug 11

0.70

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:12

Page 66: Report No D3155-13 - apps2.staffordshire.gov.uk

118

03645118

0.0048Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0354

%Passing

100756350

7268

0.0015

520.6001.18 61

9728

8679

92201410

22.4

2.65

0.063 190.150

450.425

3527

0.300

Particle density, Mg/m3

5.0

64

74

3.352.00

6.3

56

Clay

Sample Proportions

*<60mm values to aid description only

Sand

9

Silt

7 Cobbles / boulders

1110

Gravel

Remarks

3645

Soil description%Passing

Brown sandy gravelly CLAY.

1610010099

0.02540.01810.009537.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

182

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment

0.06300.0494

1918

1513

PSD 2

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH1

13 B

ESGD3155-13201311040000000013

QA Ref

SLR 2,9Rev 88Aug 11

1.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:12

Page 67: Report No D3155-13 - apps2.staffordshire.gov.uk

116

0677116

0.0050Whole *<60mm

00.0036

0.212

Particle Size mm

Particle Size mm

0.0378

%Passing

100756350

9695

0.0016

840.6001.18 92

10028

10098

100201410

2.4

2.65

0.063 170.150

640.425

3926

0.300

Particle density, Mg/m3

5.0

94

96

3.352.00

6.3

90

Clay

Sample Proportions

*<60mm values to aid description only

Sand

6

Silt

5 Cobbles / boulders

107

Gravel

Remarks

677

Soil description%Passing

Brown gravelly clayey SAND.

14100100100

0.02690.01910.009937.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

28

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0532

1715

1211

PSD 3

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH1

17 B

ESGD3155-13201311040000000017

QA Ref

SLR 2,9Rev 88Aug 11

2.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:12

Page 68: Report No D3155-13 - apps2.staffordshire.gov.uk

198

02647198

0.0048Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0340

%Passing

100756350

8279

0.0015

620.6001.18 70

9628

9087

93201410

18.3

2.65

0.063 270.150

520.425

4134

0.300

Particle density, Mg/m3

5.0

74

84

3.352.00

6.3

65

Clay

Sample Proportions

*<60mm values to aid description only

Sand

10

Silt

7 Cobbles / boulders

1411

Gravel

Remarks

2647

Soil description%Passing

Brown slightly gravelly sandy CLAY.

241009997

0.02460.01770.009437.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

123

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment

0.06300.0474

2726

2119

PSD 4

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH1

19 B

ESGD3155-13201311040000000019

QA Ref

SLR 2,9Rev 88Aug 11

3.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 69: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =9

05140

9

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

6760

330.6001.18 42

9528

8779

91201410

5.80.063 90.150

260.425

1813

0.300

5.0

49

70

3.352.00

6.3

36

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

5140

Soil description%Passing

Brown very sandy GRAVEL with occasional clay pockets.

10010010037.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

44

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 5

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH3

4 B

ESGD3155-13201311040000000040

QA Ref

SLR 2,9Rev 88Aug 11

0.20

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 70: Report No D3155-13 - apps2.staffordshire.gov.uk

1215

08651215

0.0050Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0379

%Passing

100756350

9593

0.0015

880.6001.18 92

10028

9696

98201410

11.1

2.65

0.063 280.150

800.425

6041

0.300

Particle density, Mg/m3

5.0

92

95

3.352.00

6.3

90

Clay

Sample Proportions

*<60mm values to aid description only

Sand

19

Silt

14 Cobbles / boulders

2320

Gravel

Remarks

865

Soil description%Passing

Brown slightly gravelly very sandy CLAY.

25100100100

0.02690.01900.009837.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0535

2826

2424

PSD 6

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH3

13 B

ESGD3155-13201311040000000049

QA Ref

SLR 2,9Rev 88Aug 11

2.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 71: Report No D3155-13 - apps2.staffordshire.gov.uk

7017

0677017

0.0049Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0364

%Passing

100756350

9796

0.0016

920.6001.18 93

10028

9898

100201410

16.7

2.65

0.063 900.150

910.425

9190

0.300

Particle density, Mg/m3

5.0

94

97

3.352.00

6.3

92

Clay

Sample Proportions

*<60mm values to aid description only

Sand

27

Silt

13 Cobbles / boulders

6345

Gravel

Remarks

67

Soil description%Passing

Greyish brown slightly sandy slightly gravelly silty CLAY with mudstone.

79100100100

0.02580.01830.009637.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0513

9081

7876

PSD 7

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH4

8 B

ESGD3155-13201311040000000058

QA Ref

SLR 2,9Rev 88Aug 11

0.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 72: Report No D3155-13 - apps2.staffordshire.gov.uk

6727

0336727

0.0047Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0331

%Passing

100756350

9897

0.0015

970.6001.18 97

9928

9999

99201410

10.9

2.65

0.063 950.150

960.425

9696

0.300

Particle density, Mg/m3

5.0

97

98

3.352.00

6.3

97

Clay

Sample Proportions

*<60mm values to aid description only

Sand

38

Silt

22 Cobbles / boulders

7250

Gravel

Remarks

33

Soil description%Passing

Greyish brown slightly sandy slightly gravelly silty CLAY with mudstone.

89100100100

0.02350.01680.008937.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0464

9592

8683

PSD 8

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH4

13 B

ESGD3155-13201311040000000063

QA Ref

SLR 2,9Rev 88Aug 11

2.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 73: Report No D3155-13 - apps2.staffordshire.gov.uk

2222

025272424

0.0043Whole *<60mm

80.0031

0.212

Particle Size mm

Particle Size mm

0.0305

%Passing

92756350

7371

0.0014

640.6001.18 67

8928

8278

86201410

12.2

2.65

0.063 440.150

600.425

5450

0.300

Particle density, Mg/m3

5.0

69

74

3.352.00

6.3

66

Clay

Sample Proportions

*<60mm values to aid description only

Sand

25

Silt

19 Cobbles / boulders

3429

Gravel

Remarks

2325

Soil description%Passing

Brown slightly sandy slightly gravelly CLAY with one cobble.

40929290

0.02190.01560.008337.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0424

4442

3938

PSD 9

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH5

17 B

ESGD3155-13201311040000000082

QA Ref

SLR 2,9Rev 88Aug 11

4.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 74: Report No D3155-13 - apps2.staffordshire.gov.uk

5327

010105327

0.0047Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0336

%Passing

100756350

9593

0.0015

870.6001.18 88

10028

9999

100201410

2.8

2.65

0.063 810.150

860.425

8584

0.300

Particle density, Mg/m3

5.0

90

97

3.352.00

6.3

87

Clay

Sample Proportions

*<60mm values to aid description only

Sand

35

Silt

23 Cobbles / boulders

5640

Gravel

Remarks

1010

Soil description%Passing

Brown slightly sandy slightly gravelly CLAY.

75100100100

0.02410.01720.009137.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0471

8178

7166

PSD 10

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH5

19 B

ESGD3155-13201311040000000084

QA Ref

SLR 2,9Rev 88Aug 11

5.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 75: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =14

0976

15

Whole *<60mm5

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

8787

790.6001.18 85

9328

9089

92201410

9.30.063 140.150

590.425

3721

0.300

5.0

86

87

3.352.00

6.3

83

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

972

Soil description%Passing

Brown gravelly clayey SAND with one cobble.

95959537.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 11

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

TP1

6 B

ESGD3155-1320131104499609

QA Ref

SLR 2,9Rev 88Aug 11

1.00

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 76: Report No D3155-13 - apps2.staffordshire.gov.uk

1813

016531813

0.0049Whole *<60mm

10.0035

0.212

Particle Size mm

Particle Size mm

0.0367

%Passing

100756350

8685

0.0015

780.6001.18 82

9428

9290

92201410

7.8

2.65

0.063 330.150

680.425

5242

0.300

Particle density, Mg/m3

5.0

83

87

3.352.00

6.3

81

Clay

Sample Proportions

*<60mm values to aid description only

Sand

15

Silt

13 Cobbles / boulders

2016

Gravel

Remarks

1652

Soil description%Passing

Brown gravelly SAND wth frequent clay pockets.

261009694

0.02630.01870.009737.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0516

3328

2321

PSD 12

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

TP2

5 B

ESGD3155-1320131104382114

QA Ref

SLR 2,9Rev 88Aug 11

0.85

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 77: Report No D3155-13 - apps2.staffordshire.gov.uk

115

02559115

0.0050Whole *<60mm

00.0036

0.212

Particle Size mm

Particle Size mm

0.0378

%Passing

100756350

7776

0.0016

630.6001.18 73

8828

8381

86201410

14.0

2.65

0.063 160.150

490.425

3525

0.300

Particle density, Mg/m3

5.0

75

79

3.352.00

6.3

69

Clay

Sample Proportions

*<60mm values to aid description only

Sand

5

Silt

5 Cobbles / boulders

87

Gravel

Remarks

2559

Soil description%Passing

Brown very gravelly silty SAND.

131009992

0.02690.01910.010037.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

22

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: pre dried, Hydro: as BS1377 Preparation / Pretreatment

0.06300.0529

1615

1110

PSD 13

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS1

6 B

ESGD3155-13201311040000000091

QA Ref

SLR 2,9Rev 88Aug 11

0.80

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 78: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =6

02569

6

Whole *<60mm1

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

7876

600.6001.18 71

9028

8583

86201410

5.70.063 60.150

400.425

179

0.300

5.0

74

80

3.352.00

6.3

67

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

2568

Soil description%Passing

Brown very gravelly SAND with rare clay pockets.

100949437.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

3

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 14

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS1

9 B

ESGD3155-13201311040000000094

QA Ref

SLR 2,9Rev 88Aug 11

1.20

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 79: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =14

05432

14

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

5550

330.6001.18 43

8828

7266

80201410

2.80.063 140.150

260.425

2017

0.300

5.0

46

58

3.352.00

6.3

37

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

5432

Soil description%Passing

Greyish brown slightly sandy gravelly CLAY.

1001008837.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: pre dried, Preparation / Pretreatment

PSD 15

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS3

7 B

ESGD3155-13201311040000000121

QA Ref

SLR 2,9Rev 88Aug 11

2.00

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 80: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =6

0292

6

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

9999

920.6001.18 98

10028

10099

100201410

1.20.063 70.150

720.425

3513

0.300

5.0

98

99

3.352.00

6.3

96

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

292

Soil description%Passing

Brown slightly gravelly SAND with rare clay pockets.

10010010037.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

3

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 16

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS3

10 B

ESGD3155-13201311040000000124

QA Ref

SLR 2,9Rev 88Aug 11

3.50

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 81: Report No D3155-13 - apps2.staffordshire.gov.uk

97

0206497

0.0050Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0376

%Passing

100756350

8382

0.0016

750.6001.18 79

9828

9188

95201410

11.6

2.65

0.063 170.150

660.425

4933

0.300

Particle density, Mg/m3

5.0

80

84

3.352.00

6.3

77

Clay

Sample Proportions

*<60mm values to aid description only

Sand

8

Silt

7 Cobbles / boulders

109

Gravel

Remarks

2064

Soil description%Passing

Brown gravelly clayey SAND.

13100100100

0.02670.01900.009937.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

24

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0526

1715

1211

PSD 17

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS4

5 B

ESGD3155-13201311040000000131

QA Ref

SLR 2,9Rev 88Aug 11

0.70

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 82: Report No D3155-13 - apps2.staffordshire.gov.uk

2714

039202714

0.0043Whole *<60mm

00.0032

0.212

Particle Size mm

Particle Size mm

0.0283

%Passing

100756350

7166

0.0015

520.6001.18 57

9528

8882

93201410

9.5

2.65

0.063 410.150

500.425

4745

0.300

Particle density, Mg/m3

5.0

61

74

3.352.00

6.3

53

Clay

Sample Proportions

*<60mm values to aid description only

Sand

19

Silt

12 Cobbles / boulders

2822

Gravel

Remarks

3920

Soil description%Passing

Grey slightly sandy gravelly CLAY.

37100100100

0.02040.01490.008137.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0389

4139

3533

PSD 18

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS5

5 B

ESGD3155-13201311040000000148

QA Ref

SLR 2,9Rev 88Aug 11

0.60

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 83: Report No D3155-13 - apps2.staffordshire.gov.uk

5021

02455021

0.0046Whole *<60mm

00.0034

0.212

Particle Size mm

Particle Size mm

0.0327

%Passing

100756350

8078

0.0015

730.6001.18 75

10028

9490

97201410

7.7

2.65

0.063 710.150

730.425

7372

0.300

Particle density, Mg/m3

5.0

76

82

3.352.00

6.3

74

Clay

Sample Proportions

*<60mm values to aid description only

Sand

30

Silt

16 Cobbles / boulders

5540

Gravel

Remarks

245

Soil description%Passing

Grey slightly sandy slightly gravelly CLAY.

66100100100

0.02310.01650.008837.5

Sieving Sedimentation

9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

assumed

Dry mass of sample, kg

Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0461

7167

6663

PSD 19

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS5

7 B

ESGD3155-13201311040000000150

QA Ref

SLR 2,9Rev 88Aug 11

1.20

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 84: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =4

0096

4

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

100100

980.6001.18 100

10028

100100

100201410

5.60.063 40.150

880.425

6331

0.300

5.0

100

100

3.352.00

6.3

99

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

096

Soil description%Passing

Brown slightly silty SAND.

10010010037.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

3

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 20

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS6

11 B

ESGD3155-13201311040000000162

QA Ref

SLR 2,9Rev 88Aug 11

2.00

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 85: Report No D3155-13 - apps2.staffordshire.gov.uk

silt+clay =5

0194

5

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

10099

970.6001.18 99

10028

100100

100201410

3.20.063 50.150

890.425

6634

0.300

5.0

99

100

3.352.00

6.3

98

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

194

Soil description%Passing

Orangish brown slightly gravelly SAND.

10010010037.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

3

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 21

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng

Particle Size Distribution Analysis

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS6

15 B

ESGD3155-13201311040000000166

QA Ref

SLR 2,9Rev 88Aug 11

3.80

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:04/12/2013 14:13

Page 86: Report No D3155-13 - apps2.staffordshire.gov.uk

ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA

Site: Clough Hall Technology School

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 29-Nov-2013Declan Burns Operations Director

Laboratory and Analytical Business

29-Nov-2013

The 13 samples described in this report were registered for analysis by ESG on 21-Nov-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTSOIL SAMPLE ANALYSIS

Report No. EFS/136829 (Ver. 1)

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)

Tests marked '^' have been subcontracted to another laboratory.

ESG accepts no responsibility for any sampling not carried out by our personnel.

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/136829 Ver. 1

Page 87: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1329122 BH1 D 2 0.00 242 28 0.121 8.7

1329123 BH1 D 12 1.50 181 13 0.022 7.9

1329124 BH2 B 8 0.50 706 62 0.084 7.9

1329125 BH3 D 2 0.20 6200 436 0.423 9.0

1329126 BH4 D 6 0.50 1170 122 0.096 6.6

1329127 BH5 D 2 0.20 719 70 0.084 7.8

1329128 BH5 D 10 2.50 913 83 0.044 5.7

1329129 WS1 D 13 2.90 237 63 0.015 7.0

1329130 WS2 ES 4 0.50 1110 38 0.102 8.0

1329131 WS3 B 2 0.20 787 28 0.058 7.6

1329132 WS4 D 8 1.20 296 34 0.015 7.5

1329133 WS6 D 4 0.50 740 225 0.023 5.5

1329134 WS6 D 17 5.00 369 92 0.125 7.1

Contact

Date Printed

Report Number EFS/136829

Table Number 1

Fax +44 (0) 1283 554422

Soil Sample Analysis

Mr J Litten

29-Nov-2013

Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/136829 Ver. 1

Page 88: Report No D3155-13 - apps2.staffordshire.gov.uk

SOIL Analysis S136829

CustomerSiteReport No S136829

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KoneN

O3

TS

BR

E1

WS

LM43

WS

LM50

ID Number Description Sampled

Report B

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Nitrate (2:1): m

g/l

Total S

ulphur.

Chloride (W

) BS

1377

pH (B

S1377)

���� ����

CL/1329122 BH1 0.00-0.10 DCL/1329123 BH1 1.50 DCL/1329124 BH2 0.50 DCL/1329125 BH3 0.20 DCL/1329126 BH4 0.50 DCL/1329127 BH5 0.20 DCL/1329128 BH5 2.50 DCL/1329129 WS1 2.90 DCL/1329130 WS2 0.50 DCL/1329131 WS3 0.20 DCL/1329132 WS4 1.20 DCL/1329133 WS6 0.50 DCL/1329134 WS6 5.00 D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S38194

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

Clough Hall Technology School Date Logged 21-Nov-2013

Report Due 29-Nov-2013

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/136829 Ver. 1

Page 89: Report No D3155-13 - apps2.staffordshire.gov.uk

Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Air Dried Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Air Dried Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/136829

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/136829 Ver. 1

Page 90: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

END OF REPORT

Page 5 of 5Where individual results are flagged see report notes for status.

EFS/136829 Ver. 1

Page 91: Report No D3155-13 - apps2.staffordshire.gov.uk

Project No Project Name

LOI pH CO2 <2

2:1watersol.

groundwater

acidsol.

TSMgNO3

NH4

mg/Lmg/L

watersol.

acidsol.

mm

from to % g/L g/L % % % % % %

7 0.50 DDark brownish grey sandy gravelly CLAY. 2.4 c 52

10 1.40 DDark grey and black slightly sandy slightly gravelly silty CLAY.

16.7 c 100

5 0.40 DOrangish brown and grey slightly gravelly very sandy CLAY.

0.8 c 96

6 0.50 DGreyish brown slightly sandy slightly gravelly CLAY.

1.9 c 82

2 0.20 DBrown slightly sandy slightly gravelly CLAY. 3.8 c 66

13 2.90 DGreyish brown slightly sandy slightly gravelly CLAY.

6.2 c 100

4 0.50 DDark brown and grey sandy gravelly CLAY. 1.5 c 76

2 0.20 0.80 BBrown slightly sandy slightly gravelly CLAY with occasional rootlets.

2.4 c 96

2 0.30 DBrownish grey slightly sandy slightly gravelly CLAY with plant remains

1.5 c 72

13 3.00 DDark grey gravelly clayey SAND. 1.5 c 74

4 0.50 DGreyish brown slightly sandy slightly gravelly CLAY.

3.2 c 100

17 5.00 DLight brown slightly gravelly SAND. 0.5 c 100

BS 1377 : definitive method unless stated : * Sulphate tests preparation / test methods : BRE Special Digest SD1, dependent options :

Org1. BS 1377:Part 3:1990:clause 5.3 4. TRL447 - 1 water soluble sulphate TS Total Sulphur to BR279 / EN ISO15178

LOI Mass loss on ignition at 440oC 2. BS 1377:Part 3:1990:clause 5.4 5. TRL447 - 2 acid soluble sulphate Mg Soluble Magnesium to BR279, colorimetric

CO2 Carbonate content ( rapid titration ) 3. BS 1377:Part 3:1990:clause 5.5 6. BR279 - groundwater sulphate NO3 Soluble Nitrate to BR279, colorimetric

Cl Chloride content < 2mm material passing 2mm sieve NH4 qualitative

QA Ref

WS6

WS6

WS4

WS4

WS2

WS3

Sample

Depth (m)No. type

Hole No. Soil Description

Sulphate as SO4 SD1 options

Pre

para

tion/

test

*

Org

%

Chloride, Cl

Printed:04/12/2013 14:09

BH1

Remarks

Organic matter content ( s-sulphides, c-chlorides identified )

BH2

BH3

CHEMICAL TESTS - SUMMARY OF RESULTS

CHEM 1SLR 3Rev 95Aug 11

D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL

BH4

BH5

WS1

Table

Page 92: Report No D3155-13 - apps2.staffordshire.gov.uk

Soil description Derived Parameters +

Test method BS 1377:part 4:1990: clause 3.3, 2.5 kg rammer in a 1 litre mould Maximum dry density, Mg/m3

Preparation Original material was natural, single sample tested

Material > 37.5mm %

Material < 37.5mm > 20mm % Optimum moisture content, %

Particle density, Mg/m3 assumed

Remarks

1.77

16

Brown slightly sandy slightly gravelly CLAY.

2.65

0

3

COMPL 1

DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH5

0.25

5 B

ESGD3155-13201311040000000070

QA Ref

SLD 4, 3.3/4Rev 66Aug 11

1.4

1.5

1.6

1.7

1.8

1.9

2.0

2.1

2.2

0 4 8 12 16 20 24 28 32

MOISTURE CONTENT %

DR

Y D

EN

SIT

Y M

g/m

3

----- zero, 5% and 10% air voids

Spec Ref

Figure

� Printed:04/12/2013 14:10

Page 93: Report No D3155-13 - apps2.staffordshire.gov.uk

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Characteristics of calibration line (determined using linear regression)

25.7

-0.52

1.93

Intercept

Slope

Method of interpretation of MCV

-0.95

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

MCVREL 1

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH4

0.10

4 B

ESGD3155-13201311040000000052

QA Ref

SLD 4, 5.5Rev 72Aug 11

MCV CALIBRATION

0

5

10

15

20

25

30

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 94: Report No D3155-13 - apps2.staffordshire.gov.uk

Test No * ineffective / invalid point 1 2 3 4

%

sheet 2 of 2

1.75

18.7

2.182.08

12.1 10.5 17.2

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

5.8

Soil description

19.8 19.7 16.4

14.2

18.7

1.87

2.03 2.04

1.69 1.70

Mg/m³

Mg/m³

% Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test

Reddish brown sandy gravelly CLAY.

Remarks

%

MCVREL 1

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH4

0.10

4 B

ESGD3155-13201311040000000052

QA Ref

SLD 4, 5.5Rev 72Aug 11

Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 95: Report No D3155-13 - apps2.staffordshire.gov.uk

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Characteristics of calibration line (determined using linear regression)

15.7

-0.36

2.82

Intercept

Slope

Method of interpretation of MCV

-1.00

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

MCVREL 2

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS1

0.20

4 B

ESGD3155-13201311040000000089

QA Ref

SLD 4, 5.5Rev 72Aug 11

MCV CALIBRATION

0

4

8

12

16

20

24

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 96: Report No D3155-13 - apps2.staffordshire.gov.uk

Test No * ineffective / invalid point 1 * 2 3 4 5

%

sheet 2 of 2

1.84

16.6

12.2

9.9

2.01

2.222.15

2.7 4.6 6.7

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

33.7

Soil description

2.25

14.7 14.2 13.3

#N/A

16.6

1.96

2.18 2.18

1.90 1.91

Mg/m³

Mg/m³

% Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test

Brown sandy gravelly CLAY with two cobbles.

Remarks

%

MCVREL 2

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS1

0.20

4 B

ESGD3155-13201311040000000089

QA Ref

SLD 4, 5.5Rev 72Aug 11

Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 97: Report No D3155-13 - apps2.staffordshire.gov.uk

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Characteristics of calibration line (determined using linear regression)

22.2

-0.67

1.50

Intercept

Slope

Method of interpretation of MCV

-0.99

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

MCVREL 3

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS4

0.40

4 B

ESGD3155-13201311040000000129

QA Ref

SLD 4, 5.5Rev 72Aug 11

MCV CALIBRATION

0

4

8

12

16

20

24

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 98: Report No D3155-13 - apps2.staffordshire.gov.uk

Test No * ineffective / invalid point 1 2 3 4 5

%

sheet 2 of 2

1.80

16.4

13.9

12.6

1.89

2.032.09

6.9 10.5 5.0

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

24.2

Soil description

2.15

17.8 15.4 19.1

7.9

16.4

1.70

2.06 2.12

1.75 1.84

Mg/m³

Mg/m³

% Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test

Brown slightly sandy slightly gravelly CLAY with two cobbles.

Remarks

%

MCVREL 3

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS4

0.40

4 B

ESGD3155-13201311040000000129

QA Ref

SLD 4, 5.5Rev 72Aug 11

Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 99: Report No D3155-13 - apps2.staffordshire.gov.uk

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Characteristics of calibration line (determined using linear regression)

12.0

-0.31

3.25

Intercept

Slope

Method of interpretation of MCV

-1.00

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

MCVREL 4

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS6

0.20

3 B

ESGD3155-13201311040000000154

QA Ref

SLD 4, 5.5Rev 72Aug 11

MCV CALIBRATION

0

4

8

12

16

20

24

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 100: Report No D3155-13 - apps2.staffordshire.gov.uk

Test No * ineffective / invalid point 1 2 3 4

%

sheet 2 of 2

2.16

9.1

2.232.36

6.2 13.7 0.8

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

25.2

Soil description

10.2 7.9 11.8

9.1

9.1

1.99

2.27 2.37

2.06 2.20

Mg/m³

Mg/m³

% Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test

Dark brown slightly sandy clayey GRAVEL.

Remarks

%

MCVREL 4

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

WS6

0.20

3 B

ESGD3155-13201311040000000154

QA Ref

SLD 4, 5.5Rev 72Aug 11

Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:04/12/2013 14:11

Page 101: Report No D3155-13 - apps2.staffordshire.gov.uk

%

Notes :

Soil description

%

Mg/m³

17

2.02

17

18

Test Conditions

Sample Retained on 20 mm sieve

Sample Conditions

%

%

BASETOP

1.73Mg/m³

CBR Values %

Moisture Content - BASE

Bulk Density

Dry Density

mm

Method of Compaction

days 6Soaking PeriodPre

para

tion

3

Recompacted - Rammer compaction with specified effort ( 2.5kg )

Soaked test

2.61.8

5.0 2.2 3.30

0

2.2

Amount of Swell 0.19

Brown slightly sandy slightly gravelly CLAY.

Initial Moisture Content

Moisture Content - TOP

YES

Penetration mm

Accepted CBR % 3.3

kgSurcharge applied

2.5

kPa

CBR 1

0.00

0.10

0.20

0.30

0.40

0.50

0.60

0.70

0.80

0.90

1.00

0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5

Penetration - mm

For

ce o

n P

lung

er -

kN

TOPBASE

California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH5

0.25

5 B

ESGD3155-13201311040000000070

QA Ref

SLR 4.7Rev 89Aug 11

Spec Ref

Figure

� Printed:04/12/2013 14:10

Page 102: Report No D3155-13 - apps2.staffordshire.gov.uk

Soil description

Preparation

Index properties 44 23( if available )

Specimen detailsParticle density Mg/m3

Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3

Dry density Mg/m3

Saturation %Average temperature for test oC

Swelling pressure kPa

Notes :

Specimen taken 20 mm from base of sample

0.1371824

m2/MN

0.3888330.3737

kPa

Applied

PressureMv

Cv

( t50, log )Cv

( t90, root )Voids ratio

m2/year m2/year

3060

2.00

17.89

13

2.65 assumed

74.99

960

240480

120

18.850.395

122.141.9083

0.152 46 49

18

31221716- -

0.28280.095

0.325

2.2660

0.059

19

0.3247

0.35110.181

0.036

0.3204

Stiff grey friable slightly sandy CLAY with siltstone.

Undisturbed

>30

Liquid limit % Plastic limit %

0.3952

105

Initial Final

0.200

0.220

0.240

0.260

0.280

0.300

0.320

0.340

0.360

0.380

0.400Applied pressure kPa

Voi

ds r

atio

ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details:

Hole No

Depth (m BGL)

Samp No Type

ID

BH2

1.50

11 U

ESGD3155-13201311040000000031

QA Ref

SLR 5.3Rev 140Mar 12

00.00

10.00

20.00

30.00

40.00

50.00

1 10 100 1000 10000Applied pressure kPa

Cv

m2 /y

ear

( lo

g t )

Log pressure / voids ratio

Log pressure / Cv

Spec Ref

OED 1

Figure

� Printed:04/12/2013 14:10

Page 103: Report No D3155-13 - apps2.staffordshire.gov.uk

Soil description

Preparation

Index properties 24 NP( if available )

Specimen detailsParticle density Mg/m3

Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3

Dry density Mg/m3

Saturation %Average temperature for test oC

Swelling pressure kPa

Notes :

Specimen taken 40 mm from base of sample

0.032--

m2/MN

0.5846-0.5825

kPa

Applied

PressureMv

Cv

( t50, log )Cv

( t90, root )Voids ratio

m2/year m2/year

020

1.68

18.85

17

2.65 assumed

75.02

320

80160

40

19.030.590

171.941.6775

0.168 - -

-

----- -

0.57450.020

0.575

1.9620

0.014

19

0.5752

0.58050.066

0.001

0.5780

Brown slightly gravelly SAND.

Undisturbed

not measured

Liquid limit % Plastic limit %

0.5899

77

Initial Final

Insufficient movement after intial settlement to interpret t50 and t90, hence no Cv's.

0.570

0.572

0.574

0.576

0.578

0.580

0.582

0.584

0.586

0.588

0.590Applied pressure kPa

Voi

ds r

atio

ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details:

Hole No

Depth (m BGL)

Samp No Type

ID

BH3

1.95

9 U

ESGD3155-13201311040000000045

QA Ref

SLR 5.3Rev 140Mar 12

00.00

00.02

00.04

00.06

00.08

00.10

1 10 100 1000 10000Applied pressure kPa

Cv

m2 /y

ear

( lo

g t )

Log pressure / voids ratio

Log pressure / Cv

Spec Ref

OED 2

Figure

� Printed:04/12/2013 14:11

Page 104: Report No D3155-13 - apps2.staffordshire.gov.uk

Soil description

Preparation

Index properties 38 19( if available )

Specimen detailsParticle density Mg/m3

Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3

Dry density Mg/m3

Saturation %Average temperature for test oC

Swelling pressure kPa

Notes :

Specimen taken 0 mm from base of sample

0.0711928

m2/MN

0.3249170.3088

kPa

Applied

PressureMv

Cv

( t50, log )Cv

( t90, root )Voids ratio

m2/year m2/year

60120

2.10

18.07

10

2.65 assumed

75.01

1920

480960

240

19.030.332

112.211.9987

0.083 47 50

19

16231817- -

0.22530.048

0.264

2.32120

0.026

19

0.2643

0.28650.101

0.018

0.2570

Very stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.

Undisturbed

>60

Liquid limit % Plastic limit %

0.3315

105

Initial Final

0.140

0.160

0.180

0.200

0.220

0.240

0.260

0.280

0.300

0.320

0.340Applied pressure kPa

Voi

ds r

atio

ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details:

Hole No

Depth (m BGL)

Samp No Type

ID

BH4

1.50

10 U

ESGD3155-13201311040000000060

QA Ref

SLR 5.3Rev 140Mar 12

00.00

10.00

20.00

30.00

40.00

50.00

1 10 100 1000 10000Applied pressure kPa

Cv

m2 /y

ear

( lo

g t )

Log pressure / voids ratio

Log pressure / Cv

Spec Ref

OED 3

Figure

� Printed:04/12/2013 14:11

Page 105: Report No D3155-13 - apps2.staffordshire.gov.uk

Soil description

Preparation

Index properties( if available )

Specimen detailsParticle density Mg/m3

Diameter mmHeight mmVoids ratioMoisture content %Bulk density Mg/m3

Dry density Mg/m3

Saturation %Average temperature for test oC

Swelling pressure kPa

Notes :

Specimen taken 0 mm from base of sample

0.2701325

m2/MN

0.40389.70.4001

kPa

Applied

PressureMv

Cv

( t50, log )Cv

( t90, root )Voids ratio

m2/year m2/year

010

1.92

18.61

15

2.65 assumed

75.00

160

4080

20

19.040.411

142.151.8893

0.536 7.9 8.2

20

9.5231218- -

0.36970.180

0.380

2.2010

0.116

19

0.3800

0.39260.264

0.050

0.3826

Firm greyish brown slightly sandy slightly gravelly CLAY.

Undisturbed

not measured

Liquid limit % Plastic limit %

0.4114

101

Initial Final

0.365

0.370

0.375

0.380

0.385

0.390

0.395

0.400

0.405

0.410

0.415Applied pressure kPa

Voi

ds r

atio

ONE DIMENSIONAL CONSOLIDATION TESTBS 1377 : Part 5 : 1990 : clause 3

Project No

Project Name

D3155-13

CLOUGH HALL TECHNOLOGY SCHOOL

Sample Details:

Hole No

Depth (m BGL)

Samp No Type

ID

BH5

3.50

13 U

ESGD3155-13201311040000000079

QA Ref

SLR 5.3Rev 140Mar 12

00.00

05.00

10.00

15.00

20.00

25.00

1 10 100 1000 10000Applied pressure kPa

Cv

m2 /y

ear

( lo

g t )

Log pressure / voids ratio

Log pressure / Cv

Spec Ref

OED 4

Figure

� Printed:04/12/2013 14:11

Page 106: Report No D3155-13 - apps2.staffordshire.gov.uk

w Test Dia. ó3

bulk drytype Axial

strain ó1 - ó3 c u

from to % mm kPa % kPa kPa

11 1.50 1.95 UStiff grey friable slightly sandy CLAY with siltstone. 2.13 1.86 15 UUM

102.4 102.4 102.4

20 40 80

3.0 4.5 8.9

69 89

125

35 45 63

B

9 1.95 UBrown slightly gravelly SAND.

2.14 1.85 16 UU 101.9 20 13.5 263 132 C

10 1.50 1.95 UVery stiff grey slightly sandy slightly gravelly CLAY. Gravel is mudstone.

2.33 2.13 9.5 UUM102.6 102.6 102.6

30 60 90

3.5 4.9 6.9

230 240 256

115 120 128

B

7 1.50 1.95 UStiff yellowish brown slightly sandy slightly gravelly CLAY with mudstone.

1.93 1.60 21 UUM103.7 103.7 103.7

15 30 60

3.5 4.9 8.4

196 211 248

98 106 124

B

13 3.50 3.95 UFirm greyish brown slightly sandy slightly gravelly CLAY. 2.14 1.84 17 UU 103.1 35 19.8 84 42 C

General notes: Tests carried out in accordance with BS1377: Part 7: 1990, clause 8 for single stage, clause 9 for multistage tests. Specimens nominally 2:1 height

diameter ratio and tested at a rate of strain of 2%/minute, unless annotated otherwise. See individual test reports for further details.

Legend UU - single stage test ( may be in sets of specimens ) ó3 cell pressure Mode of failure P plastic

UUM - multistage test on a single specimen ó1 - ó3 deviator stress B brittle

suffix R - remoulded or recompacted c u undrained shear strength C compound

QA Ref

UNCONSOLIDATED UNDRAINED TRIAXIAL COMPRESSION TESTS WITHOUT MEASUREMENT OF PORE PRESSURE - SUMMARY OF RESULTS

Project No

D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL

Project Name

UUSUM 1Printed:04/12/2013 14:09

RemarksMODE

At failure / end of stage

BH2

SLR 2Rev 71Mar 12

BH3

BH4

BH5

BH5

DensitySample

Depth (m)No. type

Hole No. Soil Description

Mg/m3

Table

Page 107: Report No D3155-13 - apps2.staffordshire.gov.uk

Dia. Height H/DLoad Rate

Time to failure

Mode of failure

UCS

from to mm mm Mg/m3 % kN/min secs MPa

24 14.91 15.27 CS SILTSTONE 86.8 221.0 2.5 2.60 2.5 7.5 254 S 5.35

27 22.96 23.29 CS SILTSTONE 86.1 162.9 1.9 2.61 1.6 10 407 SMS 11.7Outside ISRM Specification

17 5.16 5.34 CSSANDSTONE/SILTSTONE

86.8 140.7 1.6 2.57 1.8 80 449 MS 101Outside ISRM Specification

21 21.26 21.54 CS SILTSTONE 86.3 172.8 2.0 2.60 2.0 10 345 AC 9.83Outside ISRM Specification

17 9.10 9.28 CS SILTSTONE 86.1 115.3 1.3 2.61 1.7 20 304 S 17.4

Notes : Test Specification : International Society for Rock Mechanics, The complete ISRM suggested methods for Rock Characterization Testing and Monitoring, 2007

1 ISRM p87 test 1, water content at 105 ± 3 oC, specimen as received at the laboratory

2 ISRM p86 clause (vii), Caliper method used for determination of bulk volume and derivation of bulk density Mode of failure :

3 ISRM p153 part 1, determination of Uniaxial Compressive Strength ( UCS ) of Rock Materials S - Single shear MS - multiple shear

above notes apply unless annotated otherwise in the remarksAC - Axial cleavage F - Fragmented

Ref

BH1

BH2

BH2

BH4

UNIAXIAL COMPRESSIVE STRENGTH OF ROCK - SUMMARY OF RESULTS

D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL

BH1

RemarksRock Type

Project NameProject No

Specimen

Dimensions2 Bulk

Density2

Sample

Depth (m)No. type

Hole No.

RLR 2Rev 16Aug 11

Water

Content1

Uniaxial Compression3

RUCS 1

Table

Printed:04/12/2013 14:14

Page 108: Report No D3155-13 - apps2.staffordshire.gov.uk

LOADP

Typ

e(D

, A, I

, B)

Dire

ctio

n(L

, P o

r U

)

Lnemm

Wmm

Dpsmm

Dps'mm

kN Is Is(50)

BH110.25 - 10.42

22 CS MUDSTONE A U Y 86.6 36.0 34.0 1.50 61.23 0.40 0.44

BH115.94 - 16.24

25 CS MUDSTONE A U Y 86.2 41.0 38.0 2.20 64.58 0.53 0.59

BH119.30 - 19.50

26 CS MUDSTONE A U Y 86.4 43.0 41.0 1.50 67.16 0.33 0.38

BH125.42 - 25.57

28 CS MUDSTONE A U Y 86.6 44.0 41.0 3.50 67.24 0.77 0.88

BH129.08 - 29.24

29 CS MUDSTONE A U Y 86.3 43.0 42.0 3.60 67.93 0.78 0.90

BH26.10 - 6.26

18 CS MUDSTONE A L N 86.7 46.0 44.0 4.00 69.69 0.82 0.96 Laminated

BH218.88 - 19.06

20 CS MUDSTONE A U Y 85.8 42.0 43.0 4.50 68.54 0.96 1.10

BH224.11 - 24.25

22 CS MUDSTONE A U Y 85.7 42.0 41.0 1.20 66.89 0.27 0.31

BH49.10 - 9.28

17 CS SILTSTONE I P Y 43.0 86.4 55.0 53.0 3.40 76.36 0.58 0.71

BH413.32 - 13.44

19 CS MUDSTONE A L N 86.2 41.0 38.0 1.40 64.58 0.34 0.38 Laminated

All specimens tested at as received water content unless shown otherwise

Test TypeD - Diametral, A - Axial, I - Irregular Lump, B - BlockDirection ( U = unknown or random )L - parallel to planes of weaknessP - perpendicular to planes of weaknessDimensions Dps - Distance between platens ( platen separation )Dps' - at failure ( see ISRM note 6 )Lne - Length from platens to nearest free endW - Width of shortest dimension perpendicular to load, P

Point Load IndexMPa

F = (De/50)0.45

De

equi

vale

nt d

iam

eter

,m

m

Fai

lure

Val

id (

Y/N

)

Dimensions

Sam

ple

Typ

e

Sam

ple

Ref

Test Typesee ISRM

Fig 5 and 8

Rock typeRemarks

Spe

cim

en R

ef

Bor

ehol

e

Dep

th, m

Spe

cim

en D

epth

Point Load Index TestISRM:1985

Project No Project Name

D3155-13 CLOUGH HALL TECHNOLOGY SCHOOL

QA Ref

RLR 104Rev 65May 12

PLT 1

Figure

� Printed:04/12/2013 14:12

Dps

P

Lne

Diametral

P

WDps

Axial

P

W

Lne Dps

Block/irregular lump

Page 109: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Enclosure D

ENCLOSURE D

GEOENVIRONMENTAL LABORATORY TEST RESULTS

ESG Scientifics Report EFS/136756M

ESG Scientifics Report EFS/136757M

ESG Scientifics Report EFS/136819M

ESG Scientifics Report EXR/167084

ESG Scientifics Report EXR/167086

ESG Scientifics Report EXR/167224

ESG Scientifics Report EXR/169647

Page 110: Report No D3155-13 - apps2.staffordshire.gov.uk

ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA

Site: Clough Hall Technology School

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 02-Dec-2013Declan Burns Operations Director

Laboratory and Analytical Business

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

ESG accepts no responsibility for any sampling not carried out by our personnel.

02-Dec-2013

The 4 samples described in this report were registered for analysis by ESG on 19-Nov-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTSOIL SAMPLE ANALYSIS

Report No. EFS/136756M (Ver. 1)

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 7)Table of PCB Congener (12) Results (Page 8)Table of GRO Results (Page 9)Table of TPH (Si) banding (std) (Page 10)GC-FID Chromatograms (Pages 11 to 18)Table of VOC (HSA) Results (Pages 19 to 22)Table of Asbestos Screening Results (Page 23)Analytical and Deviating Sample Overview (Pages 24 to 25)Table of Additional Report Notes (Page 26)Table of Method Descriptions (Page 27)Table of Report Notes (Page 28)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 1 of 28

Page 111: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL

Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 16 1 0.1 36Accreditation Code: UM U UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

1328802 WS4 ES 6 0.80 Req <0.5 0.4 5 <0.20 11.6 12.9 12.0 <0.5 0.8 12.0 0.8 30.7 101 0.78 16400

1328803 WS4 ES 14 3.70 Req 1.6 5.7 33.0 0.57 45.5 389.5 961.9 <0.51 5.2 45.6 1 190.9 202 1.11 140000

1328804 WS5 ES 2 0.10 Req <0.5 1 8.5 1.75 13.2 39.9 51.8 <0.50 2.4 19.4 1.5 80.6 478 1.2 22700

1328805 WS5 ES 4 0.60 Req <0.5 0.4 8.0 0.33 13.6 24.1 24.5 <0.5 0.6 29.4 0.8 70.9 266 1.07 45900

Contact

Date Printed

Report Number EFS/136756M

Table Number 1

Fax +44 (0) 1283 554422

Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

02-Dec-2013

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 2 of 28

Page 112: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg mg/kg µg/kg % % M/M mg/kgMethod Codes : ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 ICPMSS KONECR PCBUSECDAR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 10 0.5 0.5 0.2 10 0.5 0.6 0.1 0.005 0.02Accreditation Code: UM UM UM U U U N N N N N

LAB

ID N

umber C

L/

Client Sample Description

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

^Asbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Chrom

ium (III)

Vanadium

(MS

)

Chrom

ium vi:

PC

B-12 C

ongeners Analysis

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1328802 WS4 ES 6 0.80 197 8.0 <0.6 <0.6 NAIIS 11.1 Req Req <11.6 15.8 <0.1 Req 0.110 3.48 Req

1328803 WS4 ES 14 3.70 1060 5.3 <0.6 <0.6 NAIIS 19.2 Req Req <45.5 96.6 <0.1 Req 0.562 >25 Req

1328804 WS5 ES 2 0.10 456 8.5 <0.5 <0.5 NAIIS 8.3 Req Req <13.2 25.6 <0.1 0.915 5.69 Req

1328805 WS5 ES 4 0.60 480 6.9 <0.6 <0.6 NAIIS 9.6 Req Req <13.6 18.6 <0.1 0.436 3.04 Req

Contact

Date Printed

Report Number EFS/136756M

Table Number 1

Fax +44 (0) 1283 554422

Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

02-Dec-2013

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 3 of 28

Page 113: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS4 ES 6 0.80 Job Number: S13_6756MLIMS ID Number: CL1328802 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13

Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.22 0.15 92 UMPyrene 129-00-0 7.52 0.13 99 UMBenzo[a]anthracene 56-55-3 9.24 0.09 79 UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.80 0.10 85 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.55 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 115 2-Fluorobiphenyl 109Acenaphthene-d10 112 Terphenyl-d14 76Phenanthrene-d10 114Chrysene-d12 109Perylene-d12 114

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 4 of 28

Page 114: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS4 ES 14 3.70 Job Number: S13_6756MLIMS ID Number: CL1328803 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13

Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.83 0.30 97 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 7.22 0.35 97 UMPyrene 129-00-0 7.52 0.31 80 UMBenzo[a]anthracene 56-55-3 9.23 0.27 99 UMChrysene 218-01-9 9.29 0.26 96 UMBenzo[b]fluoranthene 205-99-2 10.79 0.32 79 UMBenzo[k]fluoranthene 207-08-9 10.83 0.14 82 UMBenzo[a]pyrene 50-32-8 11.22 0.21 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.63 0.17 75 UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 12.96 0.14 94 UMTotal (USEPA16) PAHs - - < 3.06 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 111 2-Fluorobiphenyl 110Acenaphthene-d10 110 Terphenyl-d14 76Phenanthrene-d10 109Chrysene-d12 110Perylene-d12 118

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 5 of 28

Page 115: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS5 ES 2 0.10 Job Number: S13_6756MLIMS ID Number: CL1328804 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13

Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2213PAH.GC5\ Matrix: SoilDilution: 5.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 3.38 1.37 98 UMAcenaphthylene 208-96-8 4.43 1.60 99 UAcenaphthene 83-32-9 4.55 3.69 99 UMFluorene 86-73-7 4.95 3.00 85 UMPhenanthrene 85-01-8 5.83 41.10 99 UMAnthracene 120-12-7 5.88 20.40 93 UFluoranthene 206-44-0 7.22 178.00 98 UMPyrene 129-00-0 7.51 158.00 99 UMBenzo[a]anthracene 56-55-3 9.23 86.50 96 UMChrysene 218-01-9 9.28 66.70 99 UMBenzo[b]fluoranthene 205-99-2 10.78 88.50 99 UMBenzo[k]fluoranthene 207-08-9 10.82 35.10 95 UMBenzo[a]pyrene 50-32-8 11.22 76.60 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.62 46.30 89 UMDibenzo[a,h]anthracene 53-70-3 12.65 8.02 95 UMBenzo[g,h,i]perylene 191-24-2 12.94 43.00 99 UMTotal (USEPA16) PAHs - - 857.84 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 111 2-Fluorobiphenyl 98Acenaphthene-d10 110 Terphenyl-d14 72Phenanthrene-d10 120Chrysene-d12 142Perylene-d12 146

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 6 of 28

Page 116: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS5 ES 4 0.60 Job Number: S13_6756MLIMS ID Number: CL1328805 Date Booked in: 19-Nov-13QC Batch Number: 130923 Date Extracted: 21-Nov-13

Quantitation File: Initial Calibration Date Analysed: 22-Nov-13Directory: 2113PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.43 0.20 94 UAcenaphthene 83-32-9 4.55 0.38 98 UMFluorene 86-73-7 4.94 0.35 95 UMPhenanthrene 85-01-8 5.83 6.58 98 UMAnthracene 120-12-7 5.88 3.88 96 UFluoranthene 206-44-0 7.22 27.90 98 UMPyrene 129-00-0 7.51 24.20 100 UMBenzo[a]anthracene 56-55-3 9.23 14.20 96 UMChrysene 218-01-9 9.28 10.06 98 UMBenzo[b]fluoranthene 205-99-2 10.78 11.80 98 UMBenzo[k]fluoranthene 207-08-9 10.82 4.21 94 UMBenzo[a]pyrene 50-32-8 11.22 10.82 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.61 6.36 89 UMDibenzo[a,h]anthracene 53-70-3 12.65 1.04 96 UMBenzo[g,h,i]perylene 191-24-2 12.95 4.77 98 UMTotal (USEPA16) PAHs - - < 126.84 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 109 2-Fluorobiphenyl 105Acenaphthene-d10 110 Terphenyl-d14 74Phenanthrene-d10 114Chrysene-d12 120Perylene-d12 136

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 7 of 28

Page 117: Report No D3155-13 - apps2.staffordshire.gov.uk

Customer and Site Details: ESG Southam: Clough Hall Technology School Matrix:Job Number: S13_6756M Date Booked in:QC Batch Number: 130280 Date Extracted:Directory: 1122PCB.GC8 Date Analysed:Method: UltrasonicAccreditation code: N

Concentration, (µg/kg)

Sample ID Customer ID PCB 81 PCB 77 PCB 123 PCB 118 PCB 114 PCB 105 PCB 126 PCB 167 PCB 156 PCB 157 PCB 169 PCB 189* CL1328802 WS4 ES 6 0.80 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6* CL1328803 WS4 ES 14 3.70 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2 <6.2

25-Nov-13

Polychlorinated Biphenyls (congeners)

Soil19-Nov-1321-Nov-13

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 8 of 28

Page 118: Report No D3155-13 - apps2.staffordshire.gov.uk

Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: Soil

Job Number: s13_6756 Date Booked in: 19-Nov-13

Directory: D:\TES\DATA\Y2013\1127HSA_GC12\112713 2013-11-27 13-49-22\035F3501.D Date extracted: 26-Nov-13

Method: Headspace GCFID Date Analysed: 28-Nov-13, 00:59:12Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredit ed.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1328802 WS4 ES 6 0.80 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328803 WS4 ES 14 3.70 <0.012 0.038 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328804 WS5 ES 2 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328805 WS5 ES 4 0.60 <0.011 0.244 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 9 of 28

Page 119: Report No D3155-13 - apps2.staffordshire.gov.uk

ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: SoilJob Number: S13_6756 Separation: Silica gel Date Booked in: 19-Nov-13QC Batch Number: 130923 Eluents: Hexane, DCM Date Extracted: 21-Nov-13Directory: D:\TES\DATA\Y2013\02\1122TPH_GC3\066B1201.D Date Analysed: 22-Nov-13Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1328802 WS4 ES 6 0.80 <4 <4 <4 <4 <4 <4 <4 <4 <9.85 <9.85 <22 <22

CL1328803 WS4 ES 14 3.70 <5 <5 <5 <5 <5 <5 <5 5.9 40.6 31.2 47.8 42.7

CL1328804 WS5 ES 2 0.10 <4 <4 <4 <4 18.3 34.7 44.8 482 133 2240 253 2900

CL1328805 WS5 ES 4 0.60 <4 <4 <4 <4 8.84 12.8 9.52 88.6 <9.69 312 32.9 427

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 10 of 28

Page 120: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328802ALI Job Number: S13_6756MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 6 0.80Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\013F0901.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1122TPH_GC3\013F0901.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 11 of 28

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328802ARO Job Number: S13_6756MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 6 0.80Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\063B0901.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID2 B, (1122TPH_GC3\063B0901.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 12 of 28

Page 122: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328803ALI Job Number: S13_6756MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 14 3.70Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\014F1001.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1122TPH_GC3\014F1001.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 13 of 28

Page 123: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328803ARO Job Number: S13_6756MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 14 3.70Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\064B1001.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

700

FID2 B, (1122TPH_GC3\064B1001.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 14 of 28

Page 124: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328804ALI Job Number: S13_6756MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 2 0.10Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\015F1101.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (1122TPH_GC3\015F1101.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 15 of 28

Page 125: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328804ARO Job Number: S13_6756MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 2 0.10Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\065B1101.D

min0 1 2 3 4 5

pA

0

500

1000

1500

2000

2500

3000

FID2 B, (1122TPH_GC3\065B1101.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 16 of 28

Page 126: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328805ALI Job Number: S13_6756MMultiplier: 15.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\016F1201.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1122TPH_GC3\016F1201.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 17 of 28

Page 127: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328805ARO Job Number: S13_6756MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 22-Nov-13Datafile: D:\TES\DATA\Y2013\02\1122TPH_GC3\066B1201.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1122TPH_GC3\066B1201.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 18 of 28

Page 128: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS4 ES 6 0.80 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328802 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 13

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 4 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 11 88 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 10 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 92 Toluene-d8 98

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 89Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 801,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 64m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 52Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 19 of 28

Page 129: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS4 ES 14 3.70 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328803 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 14

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 62 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 11 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 87 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 80 Toluene-d8 97

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 62Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 461,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 10Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 20 of 28

Page 130: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 2 0.10 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328804 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 15

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 9 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 13 M UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 11 90 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 23 61 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 85 Dibromofluoromethane 1091,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 84 Toluene-d8 88

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 63Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.98 491,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 36m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 13Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 21 of 28

Page 131: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 4 0.60 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328805 Date Analysed: 27-Nov-13 Multiplier: 1Job Number: S13_6756M Operator: TP Position: 16

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.79 3 M UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 2.17 6 M UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 6 M UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 4.31 3 M UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 33 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 650 97 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 92 86 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 73 Dibromofluoromethane 1071,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 66 Toluene-d8 84

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 36Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 201,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 13m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.26 4Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 22 of 28

Page 132: Report No D3155-13 - apps2.staffordshire.gov.uk

Page 1 of 1

Report No:

Report Date: 28/11/2013Project Number:

Sample Number

Sample Date

Sample Location Test DateTotal Sample Dry Weight

(g)

Weight of <2mm

Fraction (g)

Asbestos(g) in >8mm+>2mm

Asbestos(g) in <2mm

% Asbestos by weight of Total Dried Sample

CL/1328802 WS4 0.80 28/11/2013 Screen OnlyCL/1328803 WS4 3.70 28/11/2013 Screen OnlyCL/1328804 WS5 0.10 28/11/2013 Screen OnlyCL/1328805 WS5 0.60 28/11/2013 Screen Only

Name: Louise JamesAuthorised Signatory:

Position: Lab Project Manager

Sampling has been carried out by a third party

For the attention of:

Address:

ESG Environmental Chemistry

ANO-0488-07139Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent

Client:

Detection limit of Method SCI-ASB-020 is 0.001%

ESG Asbestos Limited Certificate of Analysis for Asbestos in Soils

ESG Southam

Asbestos Fibre Types Identified

ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS

S136756Clough Hall Technology SchoolSite Address:

NAIISNAIIS

NAIISNAIIS

The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.

NAACR = Not Analysed at Clients Request NAIIS = No As bestos Identified in Sample (Screens Only)

NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys

1089

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 23 of 28

Page 133: Report No D3155-13 - apps2.staffordshire.gov.uk

SOIL Analysis S136756

CustomerSiteReport No S136756

MethodID

CA

LC_C

R3

CE

N Leachate

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PC

BU

SE

CD

AR

ID Number Description Sampled

Chrom

ium (III)

CE

N Leac(P

)1

Report B

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

PC

B-12 C

ongeners Analysis

���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����

CL/1328802 WS4 0.80 DCL/1328803 WS4 3.70 DCL/1328804 WS5 0.10 DCL/1328805 WS5 0.60 D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

Clough Hall Technology School Date Logged 19-Nov-2013

Report Due 29-Nov-2013

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S37808

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 24 of 28

Page 134: Report No D3155-13 - apps2.staffordshire.gov.uk

SOIL Analysis S136756

CustomerSiteReport No S136756

MethodID

PH

SO

IL

SF

AP

I

Sub002a

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

^Asbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

���� ���� ���� ���� ���� ���� ����

CL/1328802 WS4 0.80 DCL/1328803 WS4 3.70 DCL/1328804 WS5 0.10 DCL/1328805 WS5 0.60 D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

Clough Hall Technology School Date Logged 19-Nov-2013

Report Due 29-Nov-2013

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S37808

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 25 of 28

Page 135: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Number : EFS/136756

Method Code

Sample IDThe following information should be taken into consideration when using the

data contained within this report

VOCHSAS CL/1328803

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328804

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328805

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

Additional Report Notes

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136756M Ver. 1Page 26 of 28

Page 136: Report No D3155-13 - apps2.staffordshire.gov.uk

Matrix MethodID Analysis Basis

Method Description

Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS

Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PCBUSECDAR As Received Determination of Polychlorinated Biphenyl (PCB) congeners/aroclors by hexane/acetone extraction followed by GCECD detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/136756

Method Descriptions

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 27 of 28

Page 137: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.EFS/136756M Ver. 1Page 28 of 28

Page 138: Report No D3155-13 - apps2.staffordshire.gov.uk

Client : ESG Southam

Site : Clough Hall Technology School

Report Number : S13_6756M

Note: major constituent in upper case

Lab ID Number Client ID

CL/1328802 WS4 ES 6 0.80CL/1328803 WS4 ES 14 3.70CL/1328804 WS5 ES 2 0.10CL/1328805 WS5 ES 4 0.60

Sample Descriptions

Grey Stone SILT Grey Stone SILT

Description

Brown Stone SILT Grey Stone SILT

Appendix A Page 1 of 1 END OF REPORT

Page 139: Report No D3155-13 - apps2.staffordshire.gov.uk

ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA

Site: Clough Hall Technology School

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 02-Dec-2013Declan Burns Operations Director

Laboratory and Analytical Business

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

ESG accepts no responsibility for any sampling not carried out by our personnel.

02-Dec-2013

The 15 samples described in this report were registered for analysis by ESG on 19-Nov-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTSOIL SAMPLE ANALYSIS

Report No. EFS/136757M (Ver. 1)

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 18)Table of PCB Congener (12) Results (Page 19)Table of GRO Results (Page 20)Table of TPH (Si) banding (std) (Page 21)GC-FID Chromatograms (Pages 22 to 51)Table of VOC (HSA) Results (Pages 52 to 66)Table of Asbestos Screening Results (Page 67)Analytical and Deviating Sample Overview (Pages 68 to 69)Table of Additional Report Notes (Page 70)Table of Method Descriptions (Page 71)Table of Report Notes (Page 72)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 1 of 72

Page 140: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL

Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 16 1 0.1 36Accreditation Code: UM U UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

1328806 BH2 ES 7 0.5 Req 0.6 0.6 6.5 0.33 12.4 18.7 25.5 <0.53 0.6 20.9 <0.5 69.3 665 1.23 42000

1328807 BH2 ES 13 2.0 Req <0.5 0.2 1.3 <0.2 13.8 15.9 9.5 <0.50 <0.5 22.0 <0.5 50.1 250 0.95 34600

1328808 BH4 ES 3 0.2 Req <0.5 1.5 14.8 0.37 35.1 63.7 79.8 <0.50 4.9 23.6 <0.5 32.4 338 1.14 134000

1328809 BH5 ES 4 0.5 Req <0.5 0.4 7.3 <0.21 17.9 20.3 23.4 <0.53 0.7 17.3 <0.5 58.3 152 1.09 64600

1328810 BH5 ES 9 2.0 Req <0.5 0.4 6.9 <0.21 17.0 23.5 33.2 <0.52 0.5 26.6 0.5 71.9 153 1.16 45900

1328811 BH5 ES 12 3.0 Req <0.5 0.4 8.1 <0.21 14.8 16.9 15.4 <0.5 <0.5 28.4 <0.5 61.4 890 0.97 48700

1328812 TP1 ES 2 0.25 Req 0.9 0.4 7.0 1.11 16.2 19.1 25.9 <0.52 0.6 28.4 0.7 90.4 205 0.93 25800

1328813 TP1 ES 4 0.7 Req <0.6 0.3 5.9 1.52 15.8 16.8 26.0 <0.6 <0.6 16.2 0.8 65.8 225 0.87 20100

1328814 TP2 ES 2 0.2 Req 0.8 1.2 5.4 0.89 39.0 31.2 21.6 <0.5 0.9 12.6 1 78.4 177 1.25 13800

1328815 TP2 ES 4 0.55 Req 2 0.4 6.7 0.29 15.8 14.8 17.7 <0.5 0.9 15.5 2.3 53.0 241 1.90 20000

1328816 WS1 ES 3 0.2 Req <0.5 0.6 12.4 <0.2 15.3 13.2 30.8 <0.5 0.8 15 <0.5 62 133 0.45 29000

1328817 WS2 ES 2 0.2 Req <0.5 0.4 6.8 1.88 17.1 23 21.7 <0.51 2.2 27.9 0.9 117.9 237 0.66 17700

1328818 WS2 ES 6 1.0 Req <0.5 0.8 24.1 0.30 21.1 30.9 37.3 <0.5 2.5 19.8 0.9 47.0 540 0.65 22100

1328819 WS3 ES 1 0.2 Req <0.5 0.8 10.3 0.57 18.0 18.7 38.9 <0.51 1.2 16.1 0.6 75.7 185 0.6 20700

1328820 WS3 ES 5 1.8 Req 0.9 1.1 36.2 0.33 16.2 42.1 45.2 0.52 1.7 48.2 2.4 81 521 1.19 17900

Contact

Date Printed

Report Number EFS/136757M

Table Number 1

Fax +44 (0) 1283 554422

Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

02-Dec-2013

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 2 of 72

Page 141: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg mg/kg µg/kg % % M/M mg/kgMethod Codes : ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 ICPMSS KONECR PCBUSECDAR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 10 0.5 0.5 0.2 10 0.5 0.6 0.1 0.005 0.02Accreditation Code: UM UM UM U U U N N N N N

LAB

ID N

umber C

L/

Client Sample Description

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

^Asbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Chrom

ium (III)

Vanadium

(MS

)

Chrom

ium vi:

PC

B-12 C

ongeners Analysis

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1328806 BH2 ES 7 0.5 344 8.1 <0.6 <0.6 NAIIS 18.0 Req Req <12.4 21.3 <0.1 0.069 2.25 Req

1328807 BH2 ES 13 2.0 613 7.2 <0.5 <0.5 NAIIS 7.6 Req Req <13.8 15.6 <0.1 0.089 1.26 Req

1328808 BH4 ES 3 0.2 356 8.6 <0.6 <0.6 CH 10.3 Req Req <35.1 78.1 <0.1 0.182 2.09 Req

1328809 BH5 ES 4 0.5 114 7.8 <0.6 <0.6 NAIIS 17.5 Req Req <17.9 26.8 <0.1 0.033 1.44 Req

1328810 BH5 ES 9 2.0 159 6.3 <0.6 <0.6 NAIIS 15.7 Req Req <17.0 22.5 <0.1 0.026 1.42 Req

1328811 BH5 ES 12 3.0 231 6.2 <0.6 <0.6 NAIIS 15.7 Req Req <14.8 20.2 <0.1 0.039 1.19 Req

1328812 TP1 ES 2 0.25 349 8.3 <0.6 <0.6 NAIIS 16.3 Req Req <16.2 21.0 <0.1 Req 0.075 2.38 Req

1328813 TP1 ES 4 0.7 193 8.4 <0.6 <0.6 NAIIS 20.4 Req Req <15.8 18.3 <0.1 0.060 1.79 Req

1328814 TP2 ES 2 0.2 567 8.4 <0.6 <0.6 NAIIS 9.8 Req Req <39.0 32.2 <0.1 Req 0.198 2.78 Req

1328815 TP2 ES 4 0.55 2390 8.6 <0.6 <0.6 NAIIS 15.9 Req Req <15.8 19.9 <0.1 0.516 3.15 Req

1328816 WS1 ES 3 0.2 188 8.4 <0.6 <0.6 NAIIS 14.5 Req Req <15.3 21 <0.1 0.040 1.86 Req

1328817 WS2 ES 2 0.2 204 8.6 <0.6 <0.6 NAIIS 13.2 Req Req <17.1 30.0 <0.1 0.328 7.03 Req

1328818 WS2 ES 6 1.0 152 7.5 <0.6 <0.6 NAIIS 22.0 Req Req <21.1 24.3 <0.1 0.163 7.31 Req

1328819 WS3 ES 1 0.2 104 7.9 <0.6 <0.6 NAIIS 9.8 Req Req <18.0 22.1 <0.1 0.072 3.68 Req

1328820 WS3 ES 5 1.8 242 7.9 <0.6 <0.6 NAIIS 9.8 Req Req <16.2 28.0 <0.1 0.303 12.50 Req

Contact

Date Printed

Report Number EFS/136757M

Table Number 1

Fax +44 (0) 1283 554422

Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

02-Dec-2013

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 3 of 72

Page 142: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH2 ES 7 0.5 Job Number: S13_6757MLIMS ID Number: CL1328806 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.56 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 100 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 74Phenanthrene-d10 98Chrysene-d12 106Perylene-d12 115

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 4 of 72

Page 143: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH2 ES 13 2.0 Job Number: S13_6757MLIMS ID Number: CL1328807 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.18 97 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 102Acenaphthene-d10 101 Terphenyl-d14 74Phenanthrene-d10 99Chrysene-d12 106Perylene-d12 113

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 5 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH4 ES 3 0.2 Job Number: S13_6757MLIMS ID Number: CL1328808 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.39 0.43 98 UAcenaphthene 83-32-9 4.51 0.86 97 UMFluorene 86-73-7 4.91 0.90 92 UMPhenanthrene 85-01-8 5.78 12.00 99 UMAnthracene 120-12-7 5.83 4.18 97 UFluoranthene 206-44-0 7.16 27.00 98 UMPyrene 129-00-0 7.46 24.60 100 UMBenzo[a]anthracene 56-55-3 9.17 16.00 95 UMChrysene 218-01-9 9.22 12.00 98 UMBenzo[b]fluoranthene 205-99-2 10.72 18.20 100 UMBenzo[k]fluoranthene 207-08-9 10.76 6.56 96 UMBenzo[a]pyrene 50-32-8 11.15 16.30 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.55 11.00 89 UMDibenzo[a,h]anthracene 53-70-3 12.58 2.08 93 UMBenzo[g,h,i]perylene 191-24-2 12.87 9.52 99 UMTotal (USEPA16) PAHs - - < 161.74 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 100 Terphenyl-d14 73Phenanthrene-d10 101Chrysene-d12 114Perylene-d12 129

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 6 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 4 0.5 Job Number: S13_6757MLIMS ID Number: CL1328809 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.55 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 102Acenaphthene-d10 99 Terphenyl-d14 75Phenanthrene-d10 98Chrysene-d12 105Perylene-d12 116

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 7 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 9 2.0 Job Number: S13_6757MLIMS ID Number: CL1328810 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.52 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 98Chrysene-d12 107Perylene-d12 115

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 8 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: BH5 ES 12 3.0 Job Number: S13_6757MLIMS ID Number: CL1328811 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.52 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 102 2-Fluorobiphenyl 102Acenaphthene-d10 101 Terphenyl-d14 75Phenanthrene-d10 99Chrysene-d12 107Perylene-d12 116

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 9 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP1 ES 2 0.25 Job Number: S13_6757MLIMS ID Number: CL1328812 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.37 97 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 7.17 0.11 95 UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.82 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 99Chrysene-d12 107Perylene-d12 115

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 10 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP1 ES 4 0.7 Job Number: S13_6757MLIMS ID Number: CL1328813 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.18 95 UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.68 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 105Acenaphthene-d10 99 Terphenyl-d14 77Phenanthrene-d10 97Chrysene-d12 105Perylene-d12 113

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 11 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP2 ES 2 0.2 Job Number: S13_6757MLIMS ID Number: CL1328814 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.16 0.17 95 UMPyrene 129-00-0 7.46 0.23 97 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.72 0.16 77 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.16 0.09 83 UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.71 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 102Acenaphthene-d10 100 Terphenyl-d14 75Phenanthrene-d10 100Chrysene-d12 110Perylene-d12 127

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 12 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: TP2 ES 4 0.55 Job Number: S13_6757MLIMS ID Number: CL1328815 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.52 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 102Acenaphthene-d10 98 Terphenyl-d14 73Phenanthrene-d10 93Chrysene-d12 94Perylene-d12 108

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 13 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS1 ES 3 0.2 Job Number: S13_6757MLIMS ID Number: CL1328816 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 4.51 0.11 99 UMFluorene 86-73-7 4.91 0.11 84 UMPhenanthrene 85-01-8 5.78 1.02 98 UMAnthracene 120-12-7 5.84 0.32 88 UFluoranthene 206-44-0 7.17 1.01 97 UMPyrene 129-00-0 7.46 0.75 100 UMBenzo[a]anthracene 56-55-3 9.18 0.37 96 UMChrysene 218-01-9 9.23 0.28 96 UMBenzo[b]fluoranthene 205-99-2 10.73 0.27 79 UMBenzo[k]fluoranthene 207-08-9 10.76 0.13 93 UMBenzo[a]pyrene 50-32-8 11.16 0.20 93 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.14 76 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.89 0.13 70 UMTotal (USEPA16) PAHs - - < 5.13 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 91 2-Fluorobiphenyl 104Acenaphthene-d10 93 Terphenyl-d14 73Phenanthrene-d10 89Chrysene-d12 89Perylene-d12 102

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 14 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS2 ES 2 0.2 Job Number: S13_6757MLIMS ID Number: CL1328817 Date Booked in: 19-Nov-13QC Batch Number: 0 Date Extracted: 00-Jan-00

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2913PAHMS14\ Matrix: SoilDilution: 5.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 3.41 2.20 96 UMAcenaphthylene 208-96-8 4.46 0.86 98 UAcenaphthene 83-32-9 4.59 4.12 96 UMFluorene 86-73-7 4.98 3.68 98 UMPhenanthrene 85-01-8 5.84 56.80 99 UMAnthracene 120-12-7 5.89 16.80 99 UFluoranthene 206-44-0 7.20 136.00 95 UMPyrene 129-00-0 7.49 119.00 91 UMBenzo[a]anthracene 56-55-3 9.17 56.10 98 UMChrysene 218-01-9 9.22 49.20 100 UMBenzo[b]fluoranthene 205-99-2 10.70 56.80 97 UMBenzo[k]fluoranthene 207-08-9 10.73 23.30 96 UMBenzo[a]pyrene 50-32-8 11.13 48.70 95 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.50 32.00 91 UMDibenzo[a,h]anthracene 53-70-3 12.53 5.10 91 UMBenzo[g,h,i]perylene 191-24-2 12.81 28.70 96 UMTotal (USEPA16) PAHs - - 639.24 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 93Acenaphthene-d10 100 Terphenyl-d14 64Phenanthrene-d10 99Chrysene-d12 97Perylene-d12 100

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 15 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS2 ES 6 1.0 Job Number: S13_6757MLIMS ID Number: CL1328818 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 5.78 0.76 98 UMAnthracene 120-12-7 5.84 0.18 90 UFluoranthene 206-44-0 7.16 1.05 98 UMPyrene 129-00-0 7.46 0.81 100 UMBenzo[a]anthracene 56-55-3 9.17 0.59 92 UMChrysene 218-01-9 9.23 0.47 98 UMBenzo[b]fluoranthene 205-99-2 10.73 0.50 90 UMBenzo[k]fluoranthene 207-08-9 10.76 0.19 94 UMBenzo[a]pyrene 50-32-8 11.16 0.41 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.29 94 UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.21 70 UMTotal (USEPA16) PAHs - - < 5.99 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 103Acenaphthene-d10 99 Terphenyl-d14 76Phenanthrene-d10 100Chrysene-d12 112Perylene-d12 129

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 16 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS3 ES 1 0.2 Job Number: S13_6757MLIMS ID Number: CL1328819 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.64 98 UMAnthracene 120-12-7 5.84 0.16 88 UFluoranthene 206-44-0 7.16 1.43 98 UMPyrene 129-00-0 7.46 1.19 99 UMBenzo[a]anthracene 56-55-3 9.17 0.71 92 UMChrysene 218-01-9 9.23 0.58 96 UMBenzo[b]fluoranthene 205-99-2 10.73 0.80 93 UMBenzo[k]fluoranthene 207-08-9 10.76 0.29 94 UMBenzo[a]pyrene 50-32-8 11.16 0.63 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.55 0.49 100 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.38 97 UMTotal (USEPA16) PAHs - - < 7.73 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 100 2-Fluorobiphenyl 101Acenaphthene-d10 101 Terphenyl-d14 74Phenanthrene-d10 102Chrysene-d12 115Perylene-d12 132

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 17 of 72

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Clough Hall Technology SchoolSample Details: WS3 ES 5 1.8 Job Number: S13_6757MLIMS ID Number: CL1328820 Date Booked in: 19-Nov-13QC Batch Number: 130939 Date Extracted: 27-Nov-13

Quantitation File: Initial Calibration Date Analysed: 29-Nov-13Directory: 2713PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 3.33 0.40 97 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.78 0.94 98 UMAnthracene 120-12-7 5.84 0.12 87 UFluoranthene 206-44-0 7.16 0.72 98 UMPyrene 129-00-0 7.46 0.62 98 UMBenzo[a]anthracene 56-55-3 9.17 0.42 94 UMChrysene 218-01-9 9.23 0.34 97 UMBenzo[b]fluoranthene 205-99-2 10.72 0.43 76 UMBenzo[k]fluoranthene 207-08-9 10.76 0.16 79 UMBenzo[a]pyrene 50-32-8 11.16 0.29 96 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.56 0.20 96 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 12.88 0.17 99 UMTotal (USEPA16) PAHs - - < 5.23 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 100Acenaphthene-d10 100 Terphenyl-d14 72Phenanthrene-d10 101Chrysene-d12 114Perylene-d12 127

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 18 of 72

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Customer and Site Details: ESG Southam: Clough Hall Technology School Matrix:Job Number: S13_6757M Date Booked in:QC Batch Number: 130282 Date Extracted:Directory: 1122PCB.GC8 Date Analysed:Method: UltrasonicAccreditation code: N

Concentration, (µg/kg)

Sample ID Customer ID PCB 81 PCB 77 PCB 123 PCB 118 PCB 114 PCB 105 PCB 126 PCB 167 PCB 156 PCB 157 PCB 169 PCB 189* CL1328812 TP1 ES 2 0.25 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0* CL1328813 TP1 ES 4 0.7 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 <6.3

25-Nov-13

Polychlorinated Biphenyls (congeners)

Soil19-Nov-1322-Nov-13

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 19 of 72

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Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: Soil

Job Number: s13_6757 Date Booked in: 19-Nov-13

Directory: D:\TES\DATA\Y2013\1127HSA_GC12\112713 2013-11-27 13-49-22\026F2601.D Date extracted: 26-Nov-13

Method: Headspace GCFID Date Analysed: 27-Nov-13, 22:07:01Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredit ed.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1328806 BH2 ES 7 0.5 <0.012 0.141 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328807 BH2 ES 13 2.0 <0.011 0.132 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328808 BH4 ES 3 0.2 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328809 BH5 ES 4 0.5 <0.012 0.022 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328810 BH5 ES 9 2.0 <0.012 0.033 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328811 BH5 ES 12 3.0 <0.012 0.058 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328812 TP1 ES 2 0.25 <0.012 0.016 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328813 TP1 ES 4 0.7 <0.013 0.021 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3

CL1328814 TP2 ES 2 0.2 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328815 TP2 ES 4 0.55 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328816 WS1 ES 3 0.2 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328817 WS2 ES 2 0.2 <0.012 0.022 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328818 WS2 ES 6 1.0 <0.013 <0.013 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3

CL1328819 WS3 ES 1 0.2 <0.011 0.080 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1328820 WS3 ES 5 1.8 <0.011 0.251 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 20 of 72

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ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Southam : Clough Hall Technology School Matrix: SoilJob Number: S13_6757 Separation: Silica gel Date Booked in: 19-Nov-13QC Batch Number: 130939 Eluents: Hexane, DCM Date Extracted: 27-Nov-13Directory: D:\TES\DATA\Y2013\02\1128TPH_GC3\088B4401.D Date Analysed: 28-Nov-13Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1328806 BH2 ES 7 0.5 <5 <5 <5 <5 <5 <5 <5 <5 <10.68 <10.68 <24 <24

CL1328807 BH2 ES 13 2.0 <4 <4 <4 <4 <4 5.45 <4 8.38 <9.48 17 <22 33.8

CL1328808 BH4 ES 3 0.2 <4 <4 <4 <4 <4 8.09 4.85 97.4 19.6 485 28.2 633

CL1328809 BH5 ES 4 0.5 <5 <5 <5 <5 <5 <5 <5 <5 <10.62 <10.62 <24 <24

CL1328810 BH5 ES 9 2.0 <5 <5 <5 <5 <5 <5 <5 <5 <10.39 <10.39 <24 <24

CL1328811 BH5 ES 12 3.0 <5 <5 <5 <5 <5 <5 <5 <5 <10.39 <10.39 <24 <24

CL1328812 TP1 ES 2 0.25 <5 <5 <5 <5 <5 <5 <5 <5 <10.47 <10.47 <24 <24

CL1328813 TP1 ES 4 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <11.01 <11.01 <25 <25

CL1328814 TP2 ES 2 0.2 <4 <4 <4 <4 <4 <4 17.3 11.4 324 284 404 360

CL1328815 TP2 ES 4 0.55 <5 <5 <5 <5 <5 <5 <5 <5 <10.42 23.1 <24 33.2

CL1328816 WS1 ES 3 0.2 <5 <5 <5 <5 <5 <5 <5 <5 <10.25 <10.25 <23 <23

CL1328817 WS2 ES 2 0.2 <5 <5 <5 <5 11.1 32 53.9 515 619 2590 904 3440

CL1328818 WS2 ES 6 1.0 <5 <5 <5 <5 <5 <5 <5 11.8 <11.23 47.7 <26 67.7

CL1328819 WS3 ES 1 0.2 <4 <4 <4 <4 <4 <4 <4 8.39 <9.71 35.9 <22 50.8

CL1328820 WS3 ES 5 1.8 <4 <4 <4 <4 <4 13.2 <4 22.1 <9.71 51.6 <22 90.7

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 21 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328806ALI Job Number: S13_6757MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 7 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\018F2401.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\018F2401.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 22 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328806ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 7 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\074B3001.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\074B3001.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 23 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328807ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 13 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\019F2501.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\019F2501.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 24 of 72

Page 163: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328807ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 13 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\075B3101.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\075B3101.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 25 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328808ALI Job Number: S13_6757MMultiplier: 15.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\020F2601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

FID1 A, (1128TPH_GC3\020F2601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 26 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328808ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\076B3201.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

700

FID2 B, (1128TPH_GC3\076B3201.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 27 of 72

Page 166: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328809ALI Job Number: S13_6757MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 4 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\021F2701.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\021F2701.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 28 of 72

Page 167: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328809ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 4 0.5Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\077B3301.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\077B3301.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 29 of 72

Page 168: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328810ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 9 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\022F2801.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

FID1 A, (1128TPH_GC3\022F2801.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 30 of 72

Page 169: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328810ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 9 2.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\078B3401.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\078B3401.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 31 of 72

Page 170: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328811ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 12 3.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\023F2901.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\023F2901.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 32 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328811ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 12 3.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\079B3501.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\079B3501.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 33 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328812ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 2 0.25Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\024F3001.D

min0 1 2 3 4 5

pA

0

100

200

300

400

FID1 A, (1128TPH_GC3\024F3001.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 34 of 72

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328812ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 2 0.25Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\080B3601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID2 B, (1128TPH_GC3\080B3601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 35 of 72

Page 174: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328813ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 4 0.7Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\025F3101.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\025F3101.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 36 of 72

Page 175: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328813ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP1 ES 4 0.7Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\081B3701.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\081B3701.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 37 of 72

Page 176: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328814ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\026F3201.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (1128TPH_GC3\026F3201.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 38 of 72

Page 177: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328814ARO Job Number: S13_6757MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\082B3801.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\082B3801.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 39 of 72

Page 178: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328815ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 4 0.55Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\027F3301.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (1128TPH_GC3\027F3301.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 40 of 72

Page 179: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328815ARO Job Number: S13_6757MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP2 ES 4 0.55Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\083B3901.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\083B3901.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 41 of 72

Page 180: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328816ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\028F3401.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

FID1 A, (1128TPH_GC3\028F3401.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 42 of 72

Page 181: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328816ARO Job Number: S13_6757MMultiplier: 11.68 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 3 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\084B4001.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\084B4001.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 43 of 72

Page 182: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328817ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\029F3501.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (1128TPH_GC3\029F3501.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 44 of 72

Page 183: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328817ARO Job Number: S13_6757MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\085B4101.D

min0 1 2 3 4 5

pA

0

500

1000

1500

2000

FID2 B, (1128TPH_GC3\085B4101.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 45 of 72

Page 184: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328818ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 6 1.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\030F3601.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

FID1 A, (1128TPH_GC3\030F3601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 46 of 72

Page 185: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328818ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 6 1.0Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\086B4201.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\086B4201.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 47 of 72

Page 186: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328819ALI Job Number: S13_6757MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\031F3701.D

min0 1 2 3 4 5

pA

50

100

150

200

250

300

350

400

FID1 A, (1128TPH_GC3\031F3701.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 48 of 72

Page 187: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328819ARO Job Number: S13_6757MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.2Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\087B4301.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\087B4301.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 49 of 72

Page 188: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1328820ALI Job Number: S13_6757MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 5 1.8Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\032F3801.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (1128TPH_GC3\032F3801.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 50 of 72

Page 189: Report No D3155-13 - apps2.staffordshire.gov.uk

Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1328820ARO Job Number: S13_6757MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Clough Hall Technology SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 5 1.8Acquisition Date/Time: 28-Nov-13Datafile: D:\TES\DATA\Y2013\02\1128TPH_GC3\088B4401.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (1128TPH_GC3\088B4401.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 51 of 72

Page 190: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 128VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 7 0.5 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328806 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 14

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 6 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 59 92 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 33 83 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1111,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 93 Toluene-d8 94

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 84Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 721,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 60m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 31Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 52 of 72

Page 191: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 13 2.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328807 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 26

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 2.12 4 M UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 3 M UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 4.31 1 M UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 15 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 393 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 26 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 63 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 57 Toluene-d8 84

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 35Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 251,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 15m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 53 of 72

Page 192: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH4 ES 3 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328808 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 27

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 2 M UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.26 27 M UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 81 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 78 Toluene-d8 95

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 67Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 42m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 22Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 54 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 4 0.5 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328809 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 28

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 12 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 82 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 82 Toluene-d8 96

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 76Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 691,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 67m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 49Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 55 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 9 2.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328810 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 29

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 19 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 56 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 17 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 74 Dibromofluoromethane 1131,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 71 Toluene-d8 92

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 61Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 41m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 56 of 72

Page 195: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 12 3.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328811 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 30

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 1 M UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 19 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 50 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 17 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 76 Dibromofluoromethane 1161,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 74 Toluene-d8 95

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 67Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 43m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 57 of 72

Page 196: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP1 ES 2 0.25 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328812 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 31

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 4.06 16 M UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 35 90 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 80 Dibromofluoromethane 1051,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 75 Toluene-d8 91

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 401,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 11Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 58 of 72

Page 197: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP1 ES 4 0.7 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328813 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 32

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 5 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 40 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 9 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 75 Toluene-d8 92

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 65Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.97 551,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 47m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 59 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP2 ES 2 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328814 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 1

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 4.31 3 M UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 20 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 22 91 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 18 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 71 Dibromofluoromethane 1101,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 72 Toluene-d8 87

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 421,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 30m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 14Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 60 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: TP2 ES 4 0.55 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328815 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 2

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 4.31 5 M UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 12 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 11 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 10 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 921,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 72 Toluene-d8 95

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 66Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 541,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 47m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 27Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 61 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS1 ES 3 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328816 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 3

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 5.07 6 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 82 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 81 Toluene-d8 96

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 74Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 681,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 62m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 40Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 62 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 2 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328817 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 4

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 9 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 13 M UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 29 89 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 16 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 69 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 68 Toluene-d8 84

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 46Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 311,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 23m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 63 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 6 1.0 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328818 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 5

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 75 Dibromofluoromethane 1201,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 73 Toluene-d8 94

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 55Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.97 391,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 31m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 8Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 64 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 1 0.2 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328819 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 6

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.79 6 M UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 6 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 160 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 23 M UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 64 Dibromofluoromethane 1281,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 62 Toluene-d8 91

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 45Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 331,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 21m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 7Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 65 of 72

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Clough Hall Technology School Directory/Quant file: 127VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 5 1.8 Date Booked in: 19-Nov-13 Method: HeadspaceLIMS ID Number: CL1328820 Date Analysed: 28-Nov-13 Multiplier: 1Job Number: S13_6757M Operator: TP Position: 7

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 5.78 3 M UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 2.14 7 M UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 4 M UM

Chloroform 67-66-3 4.07 1 M UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 4.31 1 M UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** 7.18 20 M N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 5.07 533 96 UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 5.28 51 83 UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 42 Dibromofluoromethane 1301,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 41 Toluene-d8 81

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 23Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 151,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 9m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.26 2Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 66 of 72

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Page 1 of 1

Report No:

Report Date: 02/12/2013Project Number:

Sample Number

Sample Date

Sample Location Test DateTotal Sample Dry Weight

(g)

Weight of <2mm

Fraction (g)

Asbestos(g) in >8mm+>2mm

Asbestos(g) in <2mm

% Asbestos by weight of Total Dried Sample

CL/1328806 BH2 0.50 29/11/2013 Screen OnlyCL/1328807 BH2 2.00 29/11/2013 Screen OnlyCL/1328808 BH4 0.20 29/11/2013 Screen & IDCL/1328809 BH5 0.50 29/11/2013 Screen OnlyCL/1328810 BH5 2.00 29/11/2013 Screen OnlyCL/1328811 BH5 3.00 29/11/2013 Screen OnlyCL/1328812 TP1 0.25 29/11/2013 Screen OnlyCL/1328813 TP1 0.70 29/11/2013 Screen OnlyCL/1328814 TP2 0.20 29/11/2013 Screen OnlyCL/1328815 TP2 0.55 29/11/2013 Screen OnlyCL/1328816 WS1 0.20 02/12/2013 Screen OnlyCL/1328817 WS2 0.20 02/12/2013 Screen OnlyCL/1328818 WS2 1.00 02/12/2013 Screen OnlyCL/1328819 WS3 0.20 02/12/2013 Screen OnlyCL/1328820 WS3 1.80 02/12/2013 Screen Only

Name: Louise JamesAuthorised Signatory:

Position: Lab Project Manager

Sampling has been carried out by a third party

For the attention of:

Address:

ESG Environmental Chemistry

ANO-0488-07141Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent

Client:

Detection limit of Method SCI-ASB-020 is 0.001%

ESG Asbestos Limited Certificate of Analysis for Asbestos in Soils

ESG Southam

Asbestos Fibre Types Identified

ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS

S136757Clough Hall Technology School

NAIISNAIIS

Site Address:

NAIISNAIIS

Chrysotile(Free Fibres)NAIISNAIIS

NAIISNAIIS

NAIISNAIISNAIISNAIIS

NAIISNAIIS

The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.

NAACR = Not Analysed at Clients Request NAIIS = No As bestos Identified in Sample (Screens Only)

NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys

1089

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 67 of 72

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SOIL Analysis S136757

CustomerSiteReport No S136757

MethodID

CA

LC_C

R3

CE

N Leachate

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PC

BU

SE

CD

AR

ID Number Description Sampled

Chrom

ium (III)

CE

N Leac(P

)1

Report B

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

PC

B-12 C

ongeners Analysis

���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����

CL/1328806 BH2 0.50 DCL/1328807 BH2 2.00 DCL/1328808 BH4 0.20 DCL/1328809 BH5 0.50 DCL/1328810 BH5 2.00 DCL/1328811 BH5 3.00 DCL/1328812 TP1 0.25 DCL/1328813 TP1 0.70 DCL/1328814 TP2 0.20 DCL/1328815 TP2 0.55 DCL/1328816 WS1 0.20 DCL/1328817 WS2 0.20 DCL/1328818 WS2 1.00 DCL/1328819 WS3 0.20 DCL/1328820 WS3 1.80 D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

Clough Hall Technology School Date Logged 19-Nov-2013

Report Due 29-Nov-2013

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S37808.01

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 68 of 72

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SOIL Analysis S136757

CustomerSiteReport No S136757

MethodID

PH

SO

IL

SF

AP

I

Sub002a

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

^Asbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

���� ���� ���� ���� ���� ���� ����

CL/1328806 BH2 0.50 DCL/1328807 BH2 2.00 DCL/1328808 BH4 0.20 DCL/1328809 BH5 0.50 DCL/1328810 BH5 2.00 DCL/1328811 BH5 3.00 DCL/1328812 TP1 0.25 DCL/1328813 TP1 0.70 DCL/1328814 TP2 0.20 DCL/1328815 TP2 0.55 DCL/1328816 WS1 0.20 DCL/1328817 WS2 0.20 DCL/1328818 WS2 1.00 DCL/1328819 WS3 0.20 DCL/1328820 WS3 1.80 D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

Clough Hall Technology School Date Logged 19-Nov-2013

Report Due 29-Nov-2013

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S37808.01

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 69 of 72

Page 208: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Number : EFS/136757

Method Code

Sample IDThe following information should be taken into consideration when using the

data contained within this report

VOCHSAS CL/1328807

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328812

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328814

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328818

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328819

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1328820

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

Additional Report Notes

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/136757M Ver. 1Page 70 of 72

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Matrix MethodID Analysis Basis

Method Description

Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS

Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PCBUSECDAR As Received Determination of Polychlorinated Biphenyl (PCB) congeners/aroclors by hexane/acetone extraction followed by GCECD detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/136757

Method Descriptions

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 71 of 72

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.EFS/136757M Ver. 1Page 72 of 72

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Client : ESG Southam

Site : Clough Hall Technology School

Report Number : S13_6757M

Note: major constituent in upper case

Lab ID Number Client ID

CL/1328806 BH2 ES 7 0.5CL/1328807 BH2 ES 13 2.0CL/1328808 BH4 ES 3 0.2CL/1328809 BH5 ES 4 0.5CL/1328810 BH5 ES 9 2.0CL/1328811 BH5 ES 12 3.0CL/1328812 TP1 ES 2 0.25CL/1328813 TP1 ES 4 0.7CL/1328814 TP2 ES 2 0.2CL/1328815 TP2 ES 4 0.55CL/1328816 WS1 ES 3 0.2CL/1328817 WS2 ES 2 0.2CL/1328818 WS2 ES 6 1.0CL/1328819 WS3 ES 1 0.2CL/1328820 WS3 ES 5 1.8

Sample Descriptions

Grey Stone SILT

Grey SILT Brown Stone SILT Grey Stone SILT Grey Stone SILT

Brown Stone SILT

Brown SILT Grey Stone SILT

Grey Stone SILT Brown Stone CLAY Brown Stone CLAY Brown Stone SILT Brown Stone CLAY

Description

Brown Stone CLAY Grey SILT

Appendix A Page 1 of 1 END OF REPORT

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ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA

Site: D3155-13 Clough Hall Technology School

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 20-Jan-2014Declan Burns Operations Director

Laboratory and Analytical Business

20-Jan-2014

The 3 samples described in this report were registered for analysis by ESG on 07-Jan-2014. This report supersedes any versions previously issued by the laboratory.

TEST REPORTWATER SAMPLE ANALYSIS

Report No. EXR/169647 (Ver. 1)

Table 1 Main Analysis Results (Pages 2 to 5)Table of PAH (MS-SIM) (10) Results (Pages 6 to 8)Table of GRO Results (Page 9)Table of TPH (Si) banding (0.01) (Page 10)Table of VOC (HSA) Results (Pages 11 to 13)Table of Subcontracted Analysis Results (Pages 14 to 24)Analytical and Deviating Sample Overview (Pages 25 to 26)Table of Additional Report Notes (Page 27)Table of Method Descriptions (Page 28)Table of Report Notes (Page 29)

Tests marked '^' have been subcontracted to another laboratory.

ESG accepts no responsibility for any sampling not carried out by our personnel.

Page 1 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 213: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : pH units mg/l mg/l mg/l mg/l µg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF VOCHSAW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW

Method Reporting Limits : 0.01 7 1 0.1 1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/

Client Sample Description

Sam

ple Date

pH units w

Chrom

ium (III)

Total H

ardness as CaC

O3

Chloride as C

l w

Fluoride as F

a

VO

C H

SA

-GC

MS

o

Total S

ulphur as SO

4 (Dissolved) a

Calcium

as Ca (D

issolved) a

Magnesium

as Mg (D

issolved) a

Barium

as Ba (D

issolved) a

Sodium

as Na (D

issolved) a

Nickel as N

i (Dissolved)

Chrom

ium as C

r (Dissolved)

Cadm

ium as C

d (Dissolved)

PA

H G

C-M

S (16) o

Copper as C

u (Dissolved)

1453767 BH1 W 03-Jan-14 8.3 <0.01 308 65 0.2 Req 38 77 28 0.75 28 0.001 0.004 <0.0001 Req <0.001

1453768 BH2 W 03-Jan-14 8.3 <0.01 329 67 0.2 Req 42 84 29 0.59 30 0.005 0.004 <0.0001 Req <0.001

1453769 BH4 W 03-Jan-14 8.0 <0.01 319 19 0.2 Req 54 93 21 0.19 18 0.01 0.003 <0.0001 Req <0.001

Contact

Date Printed

Report Number EXR/169647

Table Number 1

Fax +44 (0) 1283 554422

Water Sample Analysis

Mr J Litten

20-Jan-2014

D3155-13 Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam

Page 2 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 214: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAS

Method Reporting Limits : 0.001 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.05UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/

Client Sample Description

Sam

ple Date

Lead as Pb (D

issolved)

Zinc as Z

n (Dissolved)

Manganese as M

n (Dissolved)

Iron as Fe (D

issolved) a

Arsenic as A

s (Dissolved)

Boron as B

(Dissolved) a

Mercury as H

g (Dissolved)

Selenium

as Se (D

issolved)

Vanadium

as V (D

issolved)

Molybdenum

as Mo (D

issolved)

Antim

ony as Sb (D

issolved)

Am

moniacal N

itrogen as N

Nitrate as N

Chrom

ium V

I as Cr

Cyanide (T

otal) as CN

Sulphide as S

1453767 BH1 W 03-Jan-14 <0.001 0.01 0.371 <0.01 <0.001 0.1 <0.0001 <0.001 0.001 <0.001 <0.001 0.5 <0.2 <0.01 <0.02 <0.05

1453768 BH2 W 03-Jan-14 <0.001 0.006 0.43 <0.01 <0.001 0.09 <0.0001 <0.001 0.001 <0.001 <0.001 0.4 <0.2 <0.01 <0.02 <0.05

1453769 BH4 W 03-Jan-14 <0.001 0.012 0.583 <0.01 0.002 0.02 <0.0001 <0.001 0.001 0.002 <0.001 0.3 <0.2 <0.01 <0.02 1.41

Contact

Date Printed

Report Number EXR/169647

Table Number 1

Fax +44 (0) 1283 554422

Water Sample Analysis

Mr J Litten

20-Jan-2014

D3155-13 Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam

Page 3 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 215: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : mg/l ug/l mg/l µg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/lMethod Codes : TPHFID-Si Sub045 ICPWATVAR Sub045 GROHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW

Method Reporting Limits : 0.01 5 0.01 0.1 5 5 5 15 10 5 1 1 1 2 1UKAS Accredited : Yes No No No No Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/

Client Sample Description

Sam

ple Date

TP

H by G

C(S

i) o

^Cyanide (F

ree) 5ug/l

Beryllium

as Be (D

issolved) a

^VO

C Low

Level

GR

O-H

SA

(AA

)

Ethyl B

enzene

Benzene

Toluene

Xylenes

m/p X

ylenes

o Xylene

Benzene

Toluene

Ethyl B

enzene

Xylenes

m/p X

ylenes

1453767 BH1 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 3 <1 4 3

1453768 BH2 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 <1 <1 <2 <1

1453769 BH4 W 03-Jan-14 Req <0.005 <0.01 Req Req <5 <5 <5 <15 <10 <5 <1 <1 <1 <2 <1

Contact

Date Printed

Report Number EXR/169647

Table Number 1

Fax +44 (0) 1283 554422

Water Sample Analysis

Mr J Litten

20-Jan-2014

D3155-13 Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam

Page 4 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 216: Report No D3155-13 - apps2.staffordshire.gov.uk

Units : µg/l mg/l mg/l mg/l mg/lMethod Codes : VOCHSAW PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL

Method Reporting Limits : 1 0.0005 0.0005 0.0005 0.0005UKAS Accredited : Yes No No No No

LAB

ID N

umber E

X/

Client Sample Description

Sam

ple Date

o Xylene

Phenol

Cresols

Dim

ethylphenols

Trim

ethylphenols

1453767 BH1 W 03-Jan-14 1 <0.0005 <0.0005 <0.0005 <0.0005

1453768 BH2 W 03-Jan-14 <1 <0.0005 <0.0005 <0.0005 <0.0005

1453769 BH4 W 03-Jan-14 <1 <0.0005 <0.0005 <0.0005 <0.0005

Contact

Date Printed

Report Number EXR/169647

Table Number 1

Fax +44 (0) 1283 554422

Water Sample Analysis

Mr J Litten

20-Jan-2014

D3155-13 Clough Hall Technology School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam

Page 5 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 217: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH1 W Job Number: W16_9647LIMS ID Number: EX1453767 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14

Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 10.0 Ext Method: Bottle

UKAS accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit(min) ug/l

Naphthalene 91-20-3 3.50 14.300 98Acenaphthylene 208-96-8 4.56 0.299 MAcenaphthene 83-32-9 4.68 0.873 80Fluorene 86-73-7 5.08 5.310 94Phenanthrene 85-01-8 5.97 14.900 99Anthracene 120-12-7 6.02 1.060 98Fluoranthene 206-44-0 7.36 4.460 74Pyrene 129-00-0 7.66 3.510 73Benzo[a]anthracene 56-55-3 9.37 1.820 97Chrysene 218-01-9 9.42 1.980 99Benzo[b]fluoranthene 205-99-2 10.91 1.950 80Benzo[k]fluoranthene 207-08-9 10.95 0.761 80Benzo[a]pyrene 50-32-8 11.34 1.550 86Indeno[1,2,3-cd]pyrene 193-39-5 12.74 1.160 74Dibenzo[a,h]anthracene 53-70-3 - < 0.100 -Benzo[g,h,i]perylene 191-24-2 13.08 1.280 53Total (USEPA16) PAHs - - < 55.313 -

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 81 2-Fluorobiphenyl 71Acenaphthene-d10 77 Terphenyl-d14 54Phenanthrene-d10 78Chrysene-d12 78Perylene-d12 83

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Page 6 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 218: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH2 W Job Number: W16_9647LIMS ID Number: EX1453768 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14

Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle

UKAS accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit(min) ug/l

Naphthalene 91-20-3 3.50 0.340 86Acenaphthylene 208-96-8 4.55 0.010 MAcenaphthene 83-32-9 4.68 0.082 90Fluorene 86-73-7 5.08 0.109 MPhenanthrene 85-01-8 5.97 0.100 97Anthracene 120-12-7 6.01 0.012 97Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3 - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.753 -

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 79 2-Fluorobiphenyl 80Acenaphthene-d10 74 Terphenyl-d14 66Phenanthrene-d10 75Chrysene-d12 70Perylene-d12 70

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Page 7 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 219: Report No D3155-13 - apps2.staffordshire.gov.uk

1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: D3155-13 Clough Hall Technology SchoolSample Details: BH4 W Job Number: W16_9647LIMS ID Number: EX1453769 Date Booked in: 07-Jan-14QC Batch Number: 140021 Date Extracted: 09-Jan-14

Quantitation File: Initial Calibration Date Analysed: 11-Jan-14Directory: 110MS10.PAH\ Matrix: WaterDilution: 1.4 Ext Method: Bottle

UKAS accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit(min) ug/l

Naphthalene 91-20-3 3.51 3.700 90Acenaphthylene 208-96-8 4.56 0.106 MAcenaphthene 83-32-9 4.68 0.703 81Fluorene 86-73-7 5.08 1.180 89Phenanthrene 85-01-8 5.97 1.730 97Anthracene 120-12-7 6.01 0.216 96Fluoranthene 206-44-0 7.36 0.612 91Pyrene 129-00-0 7.66 0.870 97Benzo[a]anthracene 56-55-3 9.37 0.389 88Chrysene 218-01-9 9.42 0.387 90Benzo[b]fluoranthene 205-99-2 10.91 0.531 75Benzo[k]fluoranthene 207-08-9 10.95 0.235 76Benzo[a]pyrene 50-32-8 11.34 0.450 99Indeno[1,2,3-cd]pyrene 193-39-5 12.74 0.306 98Dibenzo[a,h]anthracene 53-70-3 - < 0.014 -Benzo[g,h,i]perylene 191-24-2 13.08 0.352 59Total (USEPA16) PAHs - - < 11.781 -

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 79 2-Fluorobiphenyl 79Acenaphthene-d10 76 Terphenyl-d14 60Phenanthrene-d10 77Chrysene-d12 77Perylene-d12 78

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Page 8 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 220: Report No D3155-13 - apps2.staffordshire.gov.uk

Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Southam : D3155-13 Clough Hall Technology School Matrix: Water

Job Number: w16_9647 Date Booked in: 07-Jan-14

Directory: D:\TES\DATA\Y2014\0112HSA_GC12\011214 2014-01-12 11-42-47\128B2801.D Date extracted: 10-Jan-14

Method: Headspace GCFID Date Analysed: 12-Jan-14, 21:45:10

y * Sample data with an asterisk are not UKAS accredit ed.

Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

* EX1453767 BH1 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

* EX1453768 BH2 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

* EX1453769 BH4 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Page 9 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 221: Report No D3155-13 - apps2.staffordshire.gov.uk

ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Southam : D3155-13 Clough Hall Technology School Matrix: WaterJob Number: W16_9647 Separation: Silica gel Date Booked in: 07-Jan-14QC Batch Number: 140021 Eluents: Hexane, DCM Date Extracted: 09-Jan-14Directory: D:\TES\DATA\Y2014\011314TPH_GC16\011314 2014-01-13 10-20-12\058B0801.D Date Analysed: 13-Jan-14, 12:33:57Method: Bottle

Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

EX1453767 BH1 W 0.039 0.043 0.038 0.067 0.069 0.226 0.116 0.289 1.24 0.852 1.75 1.63

EX1453768 BH2 W <0.01 <0.01 <0.01 0.014 <0.01 0.036 <0.01 0.012 <0.01 0.013 <0.01 0.08

EX1453769 BH4 W <0.01 <0.01 0.095 0.115 1.09 0.566 1.9 0.662 0.778 0.286 3.88 1.65

Page 10 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 222: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

UKAS accredited?: NoCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH1 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453767 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 28

Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l

Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -

Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 5.47 6 M2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 - < 1 -Chloroform 67-66-3 3.31 4 86 sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 4.41 3 82trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 57 Dibromofluoromethane 120Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.78 67 Toluene-d8 70

Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.93 29 Bromofluorobenzene 581,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.74 6m and p-Xylene 108-38-3/106-42-3 5.02 3 Mo-Xylene 95-47-6 5.15 1 MNote: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.

Page 11 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 223: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

UKAS accredited?: YesCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH2 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453768 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 29

Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l

Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -

Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 - < 1 -2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 - < 1 -Chloroform 67-66-3 - < 1 - sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 - < 1 -trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 100 Dibromofluoromethane 109Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.77 100 Toluene-d8 99

Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.92 99 Bromofluorobenzene 1011,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.72 93m and p-Xylene 108-38-3/106-42-3 - < 1 -o-Xylene 95-47-6 - < 1 -Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.

Page 12 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 224: Report No D3155-13 - apps2.staffordshire.gov.uk

Volatile Organic Compounds by HSA-GCMS

UKAS accredited?: YesCustomer and Site Details: ESG Southam: D3155-13 Clough Hall Technology School Directory/Quant file: 0110VOC.MS8\ Initial Calibration Matrix: WaterSample Details: BH4 W Date Booked in: 07-Jan-14 Method: HeadspaceLIMS ID Number: EX1453769 Date Analysed: 10-Jan-14 Multiplier: 1Job Number: W16_9647 Operator: PR Position: 30

Target Compounds CAS # R.T. Concentration % Fit Target Compounds CAS # R.T. Concentration % Fit(min.) µg/l (min.) µg/l

Dichlorodifluoromethane 75-71-8 * - < 1 - Styrene 100-42-5 - < 1 -Chloromethane 74-87-3 - < 1 - Bromoform 75-25-2 - < 1 -Vinyl Chloride 75-01-4 - < 1 - iso-Propylbenzene 98-82-8 - < 1 -

Bromomethane 74-83-9 * - < 5 - 1,1,2,2-Tetrachloroethane 79-34-5 - < 1 -Chloroethane 75-00-3 - < 5 - Propylbenzene 103-65-1 - < 1 -Trichlorofluoromethane 75-69-4 - < 1 - Bromobenzene 108-86-1 - < 1 -1,1-Dichloroethene 75-35-4 - < 1 - 1,2,3-Trichloropropane 96-18-4 - < 1 -trans 1,2-Dichloroethene 156-60-5 - < 1 - 2-Chlorotoluene 95-49-8 - < 1 -1,1-Dichloroethane 75-34-3 - < 1 - 1,3,5-Trimethylbenzene 108-67-8 - < 1 -2,2-Dichloropropane 594-20-7 * - < 1 - 4-Chlorotoluene 106-43-4 - < 1 -cis 1,2-Dichloroethene 156-59-2 - < 1 - tert-Butylbenzene 98-06-6 - < 1 -Bromochloromethane 74-97-5 - < 1 - 1,2,4-Trimethylbenzene 95-63-6 5.59 1 88Chloroform 67-66-3 - < 1 - sec-Butylbenzene 135-98-8 - < 1 -1,1,1-Trichloroethane 71-55-6 - < 1 - p-Isopropyltoluene 99-87-6 - < 1 -Carbon Tetrachloride 56-23-5 - < 1 - 1,3-Dichlorobenzene 541-73-1 - < 1 -1,1-Dichloropropene 563-58-6 - < 1 - 1,4-Dichlorobenzene 106-46-7 - < 1 -Benzene 71-43-2 - < 1 - n-Butylbenzene 104-51-8 - < 1 -1,2-Dichloroethane 107-06-2 - < 1 - 1,2-Dichlorobenzene 95-50-1 - < 5 -Trichloroethene 79-01-6 * - < 5 - 1,2-Dibromo-3-chloropropane 96-12-8 - < 5 -1,2-Dichloropropane 78-87-5 - < 1 - 1,2,4-Trichlorobenzene 120-82-1 - < 5 -Dibromomethane 74-95-3 - < 1 - Hexachlorobutadiene 87-68-3 - < 5 -Bromodichloromethane 75-27-4 - < 1 - Naphthalene 91-20-3 - < 5 -cis 1,3-Dichloropropene 10061-01-5 * - < 1 - 1,2,3-Trichlorobenzene 87-61-6 - < 5 -Toluene 108-88-3 - < 1 -trans 1,3-Dichloropropene 10061-02-6 - < 1 - Compounds marked * are not UKAS accredited1,1,2-Trichloroethane 79-00-5 - < 1 - "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 5 -1,3-Dichloropropane 142-28-9 - < 1 -Dibromochloromethane 124-48-1 - < 1 - Internal standards R.T. Area % Surrogates % Rec1,2-Dibromoethane 106-93-4 - < 1 - Pentafluorobenzene 3.42 102 Dibromofluoromethane 108Chlorobenzene 108-90-7 - < 1 - 1,4-Difluorobenzene 3.77 104 Toluene-d8 98

Ethylbenzene 100-41-4 - < 1 - Chlorobenzene-d5 4.92 104 Bromofluorobenzene 991,1,1,2-Tetrachloroethane 630-20-6 - < 1 - 1,4-Dichlorobenzene-d4 5.72 100m and p-Xylene 108-38-3/106-42-3 - < 1 -o-Xylene 95-47-6 - < 1 -Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 14 days of sampling.

Page 13 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 225: Report No D3155-13 - apps2.staffordshire.gov.uk

Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

Louise SmithEnvironmental Scientifics Group

ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ

Dear Louise

Please find attached the results for the batch of 3 samples described below.

Samples Registered on: 09-Jan-2014

Analysis Started on: 10-Jan-2014

Analysis Completed on: 14-Jan-2014

Results for Batch Number 20060742

Your Purchase Order Number: 56037 BEC

You will be invoiced shortly by our accounts department.

If we can be of further assistance then please do not hesitate to contact us.

Yours sincerely

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and

performance data are available on request. The date of sample analysis is available on request.

The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no

knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were

representative of the need for which the information was required.

The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on

the basis of the analysis or advice or interpretation provided.

William FardonCustomer Services Team Manager

Tel: (0113) 231 [email protected]

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Page 1 of 11

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Analytical Report

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Batch description: W169647Reported on:

14-Jan-2014

Environmental Scientifics Group Cyanide AnalysisClient: Project:

1

CC Environmental Scientifics GroupSample Point Name:

Folder No: 002686163 Sampled on: 3-Jan-14 @ (Time not supplied)

Comments: W1453767 - BH1

Quote No: 10242 Matrix: Freshwater

Lab ID Result Units TestcodeAnalyte MRV AccredFlag

Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l

1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,4-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

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1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

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Page 3 of 11

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Report ID - 20060742 - 1

Analytical Report

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Batch description: W169647Reported on:

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Hexachloroethane SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Naphthalene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

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Page 4 of 11

Page 229: Report No D3155-13 - apps2.staffordshire.gov.uk

Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

Environmental Scientifics Group Cyanide AnalysisClient: Project:

1

CC Environmental Scientifics GroupSample Point Name:

Folder No: 002686165 Sampled on: 3-Jan-14 @ (Time not supplied)

Comments: W1453768 - BH2

Quote No: 10242 Matrix: Freshwater

Lab ID Result Units TestcodeAnalyte MRV AccredFlag

Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l

1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,4-Trimethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

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Report ID - 20060742 - 1

Analytical Report

0754

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Batch description: W169647Reported on:

14-Jan-2014

1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

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Report ID - 20060742 - 1

Analytical Report

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Batch description: W169647Reported on:

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Hexachloroethane SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Naphthalene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 7 of 11

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Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

Environmental Scientifics Group Cyanide AnalysisClient: Project:

1

CC Environmental Scientifics GroupSample Point Name:

Folder No: 002686166 Sampled on: 3-Jan-14 @ (Time not supplied)

Comments: W1453769 - BH4

Quote No: 10242 Matrix: Freshwater

Lab ID Result Units TestcodeAnalyte MRV AccredFlag

Cyanide : Free as CN SX<0.00500 UKAS0.005 183mg/l

1,1,1,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,1-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2,2-Tetrachloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1,2-Trichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trichloropropane SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,3-Trimethylbenzene SX4.06 UKAS0.1 1296ug/l DB, DC

1,2,4-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2,4-Trimethylbenzene SX1.42 UKAS0.1 1296ug/l DB, DC

1,2-Dibromo-3-chloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dibromoethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloroethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,2-Dimethylbenzene :- {o-Xylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trichlorobenzene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3-Dichlorobenzene SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

1,3-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 8 of 11

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Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

1,4-Dichlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2,2-Dichloropropane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Benzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromochloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromodichloromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Bromoform :- {Tribromomethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon Disulphide SX<0.5 None0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Carbon tetrachloride :- {Tetrachloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorobenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chlorodibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloroform :- {Trichloromethane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Chloromethane :- {Methyl Chloride} SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dibromomethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dichloromethane :- {Methylene Dichloride} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<1 UKAS0.2 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethyl tert-butyl ether :- {ETBE} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Ethylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Hexachlorobutadiene SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Hexachloroethane SX<3 None0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 9 of 11

Page 234: Report No D3155-13 - apps2.staffordshire.gov.uk

Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

Isopropylbenzene SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

MTBE :- {Methyl tert-butyl ether} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Naphthalene SX4.33 None0.5 1296ug/l DB, DC

n-ButylBenzene :- {1-Phenylbutane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

n-Propylbenzene :- {1-phenylpropane} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Styrene :- {Vinylbenzene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Amyl methyl ether :- {TAME} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Tetrachloroethylene :- {Perchloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Toluene :- {Methylbenzene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<3 UKAS0.5 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichloroethylene :- {Trichloroethene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Trichlorofluoromethane SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

Vinyl Chloride :- {Chloroethylene} SX<0.5 UKAS0.1 1296ug/l DB, DC

ELEVATED_MRV : Matrix interference

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 10 of 11

Page 235: Report No D3155-13 - apps2.staffordshire.gov.uk

Report ID - 20060742 - 1

Analytical Report

0754

Final Report

Batch description: W169647Reported on:

14-Jan-2014

Method Description Summary for all samples in batch Number 20060742SX I Cyanide - (free) - determined colorimetrically by CF analyser 183

SX O Volatiles - direct aqueous injected; determined by P and T GCMS 1296

Laboratory Site Manager

Simon Padley

All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are

necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be

quoted and will be above the MRV.

Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"

sample was used.

Key to Results Flags:

DB Samples received outside analysis holding times. It is possible that the results may be compromised.

DC Analysis started outside of specified holding time. It is possible that the results may be compromised.

The analysis start date specified is the date of the first test, dates for other analysis are available on request.

Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless

otherwise agreed with Customer Services

Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated

Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard

for testing of soils, none = Methodology not accredited

Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions

END OF TEST REPORT

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 11 of 11

Page 236: Report No D3155-13 - apps2.staffordshire.gov.uk

WATER Analysis W169647

CustomerSiteReport No W169647

MethodID

BT

EX

HS

A

Calc_C

R3

Calc_H

D

CU

ST

SE

RV

GR

OH

SA

ICP

MS

W

ICP

WA

TV

AR

ID Number Description Sampled

BT

EX

-HS

A A

nalysis

Chrom

ium (III) (C

ALC

)

Total H

ardness as CaC

O3 (C

ALC

)

Report A

GR

O-H

SA

GC

FID

(AA

)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Sodium

as Na (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����

EX/1453767 BH1 03/01/14EX/1453768 BH2 03/01/14EX/1453769 BH4 03/01/14

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No W64308

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

D3155-13 Clough Hall Technology School Date Logged 07-Jan-2014

Report Due 13-Jan-2014

Page 25 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 237: Report No D3155-13 - apps2.staffordshire.gov.uk

WATER Analysis W169647

CustomerSiteReport No W169647

MethodID

ICP

WA

TV

AR

ISE

F

KO

NE

NS

PA

HM

SW

PH

EH

PLC

VL

SF

AP

I

SF

AS

Sub045

TP

HF

ID-S

i

VO

CH

SA

W

WS

LM3

ID Number Description Sampled

Beryllium

as Be (D

issolved) VA

R

Fluoride as F

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

Nitrate as N

(Kone calc)

Chrom

ium V

I. as Cr (K

one)

PA

H G

C-M

S (16)

Phenols by H

PLC

(Low Level)

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

^Cyanide (F

ree) 5ug/l

^VO

C Low

Level

TP

H by G

C(S

i)

BT

EX

Analysis H

SA

GC

-MS

Benzene (µg/l)

Toluene (µg/l)

Ethyl B

enzene (µg/l)

Xylenes (µg/l)

m/p X

ylenes (µg/l)

o Xylene (µg/l)

VO

C H

SA

-GC

MS

pH units

���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����

EX/1453767 BH1 03/01/14EX/1453768 BH2 03/01/14EX/1453769 BH4 03/01/14

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No W64308

Accredited to ISO17025

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

D3155-13 Clough Hall Technology School Date Logged 07-Jan-2014

Report Due 13-Jan-2014

Page 26 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 238: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Number : W/EXR/169647

Method Code

Sample IDThe following information should be taken into consideration when using the

data contained within this report

VOCHSAW EX1453767Due to the matrix effect on the internal standards and surrogates, the sample has been reported as non-UKAS.

Additional Report Notes

Page 27 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 239: Report No D3155-13 - apps2.staffordshire.gov.uk

Matrix MethodID Analysis Basis

Method Description

Water BTEXHSA As Received Benzene, Toluene, Ethylbenzene, & Xylenes by headspace extraction GCFID quantitation

Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI

Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons

(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using

ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using

ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective

Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane

extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with

colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Water TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in

water by GCFIDWater VOCHSAW As Received Determination of Volatile Organics Compounds by Headspace

GCMSWater WSLM3 As Received Determination of the pH of water samples by pH probe

Report Number: W/EXR/169647

Method Descriptions

Page 28 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 240: Report No D3155-13 - apps2.staffordshire.gov.uk

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

END OF REPORT

Page 29 of 29Where individual results are flagged see report notes for status.

EXR/169647 Ver. 1

Page 241: Report No D3155-13 - apps2.staffordshire.gov.uk

January 2014 Report No D3155-13 Issue 3.0 Enclosure E

ENCLOSURE E

PHOTOGRAPHS

Rotary Core BH1, BH2 and BH4

Page 242: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH1

Core Photographs

Page 243: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH1

Core Photographs

Page 244: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH1

Core Photographs

Page 245: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH1

Core Photographs

Page 246: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH1

Core Photographs

Page 247: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH2

Core Photographs

Page 248: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH2

Core Photographs

Page 249: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH2

Core Photographs

Page 250: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH2

Core Photographs

Page 251: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH2

Core Photographs

Page 252: Report No D3155-13 - apps2.staffordshire.gov.uk

Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH4

Core Photographs

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Notes: CLOUGH HALL TECHNOLOGY SCHOOL

D3155-13Education Funding Agency

Project

Project No.Carried out for

Figure

BH4

Core Photographs

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January 2014 Report No D3155-13 Issue 3.0 Enclosure F

ENCLOSURE F

DRAWINGS

Site Location Plan 1

Site Plan 2

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