reports dateocdimage.emnrd.state.nm.us/imaging/filestore/santa... · clientproject id: gasbuggy...

3R- 3

REPORTS

DATE:

<frgroup

Wayne Price New Mexico Oil Conservation Division Environmental Bureau 2040 S. Pacheco Santa Fe, NM 87505

October 2, 2000

'IT Corporation 2621 Losee Road, Building B-l North Las Vegas, NV 89030-4129 Tel. 702.295.2033 Fax. 702.295.2025

Mailing Address: P.O. Box 93838 Las Vegas, NV 89193-3838

A Member of The IT Group

GASBUGGY SITE ANALYTICAL DATA AND WASTE DISPOSAL INFORMATION

The Department of Energy (DOE) has completed the preliminary site investigation at the Gasbuggy site in Rio Arriba County, New Mexico. At your request, the enclosed analytical data summary and complete analytical results are being forwarded to you. These data represent only the fourteen (14) waste characterization samples collected during the September 2000 field effort. Additional site characterization analytical data will be reported in the Gasbuggy preliminary site investigation data report to be published at a later date.

All Gasbuggy waste characterization samples were analyzed for the following parameters: Toxicity Characteristic Leaching Procedure (TCLP) metals (Method SW6010), TCLP volatile organic compounds (Method SW8260), TCLP semi-volatile organic compounds (Method SW8270), Total Petroleum Hydrocarbons (TPH)-gasoline (Method SW8015), TPH-diesel (Method SW8015M), and tritium (Liquid scintillation). Only constituents that were detected in the analyses are reported in the summary table; undetected constituents (given a "U" qualifier by the laboratory) are not reported, with the exception of the tritium data which is presented in its entirety. The complete analytical results for the fourteen samples used in characterizing the Gasbuggy waste are also enclosed.

As required in 40 CFR 262.11, a hazardous waste determination was completed for all investigation-derived waste (IDW) generated during the preliminary site investigation. The enclosed analytical results, coupled with knowledge of historical DOE activity at the Gasbuggy site, resulted in all IDW being characterized as non-hazardous, non-radioactive waste. As a result of this determination, all IDW will be sent off site for disposal at the RCRA-permitted Safety-Kleen Imperial Valley facility in Westmorland, California. We have scheduled transport of the waste for Wednesday, October 4, 2000. There are a total of eight drums of waste that will be sent off site: 3-30 gallon drums of soil, 3 -55 gallon drums containing personal protective gear/debris, and 2-55 gallon drums of decontamination rinsate.

I A Mi

Corporation A Member of The IT Group

In addition, copies of the historical aerial photographs of the Gasbuggy surface ground zero area that you requested during our September 7, 2000 meeting, are enclosed. Please contact Patty Gallo, of my staff, at 702-295-2310 or myself at 702-295-2501 i f you have questions or concerns regarding the enclosures.

IT CORPORATION

C. Stahl, P.E. Offsites Project Manager

cc w/enclosures: S. Afong, DOE/NV,.Las Vegas, NV D. Foust, OCD, Aztec, NM J. Kieling, NMED, Santa Fe, NM M. Sanchez, DOE/NV, Las Vegas, NV

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Method SW6010

SEPT28-00 THU 04:28 PM AGON ANALYTICS FAX NO. 70 490 1349 P. 02

TCLP ICP Metals Method SW6010-TCLP Leachate

Sample Results

Lab Name: Paragon Analytics, Inc.

Work Order Number: 0000127

Client Namo: IT Corporation Las Vegas

ClientProject ID: Gasbuggy

Fiold ID: GBPS010609

Lab ID: 00091 J M

LEACH DATE: ^20/2000

Sample Matrix: LEACHATE % Moisture: N/A

Date Collected: 14-Sep-OO Date Extractor!: 21-Sep OO Dato Analyzed: 22-Sep-00

Prep Batch: IP000921-1 QCaatchlD: 1P00092M-1

Run ID:IT000922-1A3 Cleanup: NONE

Basis: As Received

Sample Aliquot: 5G Final Volume: 50 ML Result Units: MG/L

File Name: TS00922

CASNO Target Analyte Dilut ion Resul t Report ing IDL Result EPA Target Analyte Factor Limit Qualifier Qualif ier

7*10-30-2 ARSENIC 1 0.1 0.1 0.034

• " u

7440-30-3 BARIUM 2.1 1 0.00069 ; 7C140-.13-D CAPMIlJM 1 0.05 0.05 0.0017 u 7440-4 7-3 CHROMIUM 0.00S1 f 0.1 0.0033 B

; 7439-02-1 LEAD 0.029 0.03 . . _ .

0.016 L.L_ i 7702-49-2 SELENIUM o.os; 0.05 0.026 u

i 1 7440-22-4 SILVER 1 0.1 ; o.i 0.0045 ! U

Data Package fD: IT0009127-1

Dato Printed: Wednesday, September 27. 2000 Paragon Analytics Inc. I IMS Version 1.cKS

Page 12 of 14

SEP-28-00 THU 04:28 PM EABAGON ANALYTICS FAX NO. 70 490 1349 P. 03

TCLP ICP Metals Method SW6010--TCLP Leachate

Sample Results


WorR Order Number: 0009127

Client Name: IT Corporaiion Las Vegas

ClientProjoctlD: Gasbuggy

Ploia ID: OPPS010911

Lab ID; 0009127-5

LEACH DATE: 9/20/2000


Date Collected; 14-Sep-00 Dale Extracted: 21-Sep'00 Dato Analyzed: 22-Sep-00

Prep Batch: IP000021-1 QCBatchlD:lP000921-1-1

Run ID: IT000922-1A3 Cleanup: NONE

Basis: As Received

Sample Aliquot: 5G Final Volume^ 50 ML Result Unita^G/L-•;;

File Name: TS00922

I CASNO Target Analyte Dilut ion Result Reporting IDL Result EPA

| Factor L imit Quali f ier Qualif ier

7440-3S-2 ARSCNIC 1 0.1 0.1 0 034 U

7440-39-3 BARIUM ' : ' ' ! i - • f 9 1 0.00069

74-10-43-9 CADMIUM ' "0.0019 0.05 0.0Q17 . J? .' 7440-47-3 CHROMIUM • 0:015 0,1 0.0033 5

i 7439-02-1 1

LEAD " '• '1 r 0.07 0.03 0.016

! 7782-13-2 SELENIUM 1 o.os 0.05 0.026 U

. 7440-22-4 SILVI-R 1 0 1 0.1 0.0045 U

Data Package ID; IT0009127-1

Data printed: Wednesday, September 27,2000 Paragon Analytics Inc. LIMS V.ifsiorv 1 wc

Page 14 of 14

SEP-28-00 THU 04:28 PH EARAGON ANALYTICS FAX NO. 70 490 1349 P. 04


Sample Results



Client Name: IT Corporation Las Vegas


Piflld ID. G9P3020G10

lab ID: 0000127-12

LEACH DAI E: 9/20/2000


Dato Collected: 14-Sep-OO Date Extracted: 21-Sep-00 Date Analyzed: 22-Sep-00

Prep Batch: IP000921-1 QCBatchlD:lP000921-1-1


Basis: As Received


File Name: TS00922

CASNO Target Analyte Dilution Result Reporting IDL Result EPA Factor Limit Qualifier Qualifier

I 7440-38-2 ARSENIC 1 0.1 0.1 0.034 U

| 7440-39-3 BARIUM i • 1.4 1 0.00069 ,

| 74 4 0-43-EI CADMIUM 1 o.oo; 0.05 0.0017 U

7440-47-3 CHROMIUM 1 0.1 _' _. 0 1 0.0033 . . U . . . . _ 7439-92-1, . _

LEAD 1 0.03'. 0,03 0.016 u

7782-49-2 SELENIUM 1 0.05 0.05 0.026 u 1 7440 22-4 SILVER 1 0.1 • 0.1 0.0045 u

Data Package ID: IT0009127-1

Date? Printed: Wodnesday. September 27, 2000 Paragon Analytics Inc. LIMS Vdruoo 1 H.II)

Page 1 of 14

SEP-28-0C) THU 04:28 PH AGON ANALYTICS FAX NO. 70 490 1349 P. 05


Sample Results




CliontProJoct ID: Gasbuggy

FiOld ID: CHPS03O4OC

Lrtb ID: 0009127-13



Date Collected: 1S-Scp-00 Date Extracted: 21-Sep-00 Date Analyzed: 22.Sep 00

Prop Batch: IP000921-1 QCBatchlD;IP000921-1-1

Run ID; IT0O0922-1A3 Cleanup: NONE

Basis: As Received

Sample Aliquot: 5G Final Volume: 50 ML Result Units; MG/L

File Name: TS00922

CASNO Target Analy te Di lut ion Result Report ing IDL Result EPA Target Analy te Factor L imit Qual i f ier Qualif ier

7440-38-2 ARSENIC i 0.1 0.1 0.034 U

; 7440-39-3 BARIUM 0 60 1 0.00069 B

! 7440-43-0 CADMIUM " 0 002 j 0.05 0.0017 B

' 7440-47-3 CHROMIUM 1 0012; o.i 0.0033 D

' 7439-92-1 LEAD 0 03 0.03 0.016 u

( 7782-49-2 SELENIUM 0.05 0 05 0.026 u 7440-22-4 SILVER 1

1 ' ' 0.1 0.1 0.0045 u 1


Pate Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LINKS V0l lion

Page 2 of 14

SEP-28-00 THU 04:28 PM AGON ANALYTICS FAX NO. 70 490 1349 P. 06


Sample Results

Lab Namo: Paragon Analytics, Inc.




n«ld ID: GDPS040405

LablD: 0009127-14



J Date Collected: 15-Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 22-Sep-00

Prep Batch: IP000021-1 QCBatchlD:IP000921-1-1

RunlD:IT000922-1A3 Cloanup: NONE

Basis: As Received


File Name: TS00922

CASNO Target Analy te Di lut ion Resul t Report ing IDL Resul t EPA Factor L imi t Qual i f ier Qual i f ier

'• 7440-33-2 ARSENIC 1 0.1 0.1 0,034

• 7440-39-3 HARIUM . .. . i 0.00069

7440-43-9 CADMIUM 0.051 o.os 0.0017 U

I 7440-47-3 CHROMIUM ' 1 0,0037,. 0.1 0,0033 B

I 7439-52-1 LEAD 1 0.03! 0.03 1

0.016 u \ 7782-40-2 SKLENIUM 1 o.os 0.05 0.026 U

| 7440-22-4 SILVER : 1 0.1 0,1 0.0045 u


Date Printed; Wednesday, September 27, 2000 Paragon Analy t ics Inc. P a 9 e 3 o f 1 4

l IMS Vnruton 1876

SEP-28-00 THU 04:28 PM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 07


Sample Results





F'idld ID; CRPS050408

Lab ID: 000912?-15



Date Collected: 15-Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 22-Scp-00

Prop Batch: IP000921-1 QCBatchlD:IP000921-1.1

Run ID:IT00092Z-1A3 Cleanup: NONE

Basis: As Received

Sample Aliquot: SG Final Volume: 50 ML Result Units: MG/L

File Name: TS00922

CASNO Target Analy te Di lut ion Factor

Result Report ing L imi t

IDL Result Qual i f ier

EPA Quali f ier

. 74110-311-2 ARSENIC 0.1 0.1 0.034 U

7440-39-3 BARIUM .0,97 1 0.00069 B •

74 40-43-9 CADMIUM ! 1 CHROMIUM . . . | ^

0.06 0,05 0.0017

0.0033

U

7440-47-3

CADMIUM ! 1 CHROMIUM . . . | ^ 0.008/ 0.1

0.0017

0.0033

• B

! 7430-92-1 LEAD 1 0.03 0,03 0.016 I u

7732-49-2 SELENIUM 1 0.05 0.05 0.026 U | 7440-22-4 SILVER 1 0.1; 0.1 0.0045 1 ' U


Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LtMS vernon- i B00

Page 4 of 14

SEP-28-00 THU 04:29 PM AGON ANALYTICS FAX NO.370 490 1349 P. 10


Sample Results



Client Name: IT Corporation Laa Vegas

ClienlProJectlD: Gasbuggy

Field ID: OBPSOOO608

L;ib ID: OOO0U7-3S



Date Collected: 15-Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 22-Sep-00

Prep Batch: IP0OO921-1 QCDatchID: IP000921-1-1

RunlD:lT000922-1A3 Cleanup: NONE

Basis: As Received


File Name: TS00922

CASNO Target Ana ly te Di lut ion Result Repor t ing IDL Resul t EPA Factor L imi t Qual i f ier Quali f ier

7440-33-2 ARSf-NlC i 0.1 0.1 0.034 u

• ; 7440-30-3 HARIUM 0.93 0.00069 B

• 7440-43-0 CADMIUM 1 0.051 0.05 L .

0.0017 -v " 7440-17-3 CHROMIUM 0 023 0.1 0.0033 "f" 7439 92-1 LEAD 0.03 0.03 0.016 U

7732-40-2 St'LFNIUM OOS 0.05 0.026 u 7440-22-4 SILVER .

1 0.1 0.1 0.0045


Dale printed: Wednesday. September 27, 2000 Paragon Analytics Inc. LIMS Vu tion IMC

Page 7 of 14

SEP-28-00 THU 04:29 PM RAGON ANALYTICS FAX N(Ufl70 490 1349 0^ P. 11


Sample Results


Work OrcJer Number: 0009127

Client Name; IT Corporation Las Vegas

ClientProject ID: Oasbuggy

f ield ID: ,GoPfio70608

Lab ID- 0009127-38


Sample Matrix: LEACHA'I E % Moisture: N/A

Date Collected: 15-Sep-OO Date Extracted: 21-Sep-OO Date Analyzed; ?2-Sep-00

Prep Batch: IP0OO921-1 QCBalchlD: IP000921-1-1


Basis: As Received

Sample Aliquot: 5G Final Volume; 50 ML Result Units: MG/L

File Name: TS00922

CASNO Target Ana ly to Di lut ion Factor


IDL Result Quali f ier

EPA Qualif ier

7110-38-2 ARSENIC 1 0 1 0.1 0.034 U

' 74-10-39-3 BARIUM 1 1.2 1 0.00069

7440 43-9 CADMIUM 1 0.0029 0.05 0.0017 B

7440-47-3 CHROMIUM " I 1 ' 0.01 0.1 0.0033 B

7439-92-1 LEAD I 1 . .._ . I

0.03 0.03 0.01S U .. . [ U j 7782-49-2 SELtNiUM 1 0.05 0.05 0.026

U .. . [ U

7440-22-4 SlLVHR ! 1 0.1 0.1 0.0045 u .


Date Printed: Wednesday. September 27, 2000 Paragon Analytics Inc. LIMS V-,r™n 1 856

Page 3 Of 14

SEP-28-00 THU 04:29 PM AGON ANALYTICS FAX N0^70 490 1349 P. 12


Sample Results




ClientProject ID: Castiuggy

Fie ld ID; <iepsiOO204

Lab ID: ooooi27-37


Sample Matrix: LEACIIATC % Moisturo: N/A

Dato Collected: 16-5ep-00 Date Extracted; 21-Sop-00 Date Analyzed: 22-Sep-00

Prep Batch: IP000921-1 QCBatchlD:IP000921-1-l


Basis: As Received

Sample A l iquo t : 5 G

Final Volume: 50 ML Result Units: MG/L

File Name: TS00922

CASNO Target Ana ly te Di lut ion Resul t Report ing IDL Resul t EPA Factor L imi t Qual i f ier Qualif ier

7440-38-2 ARSENIC 1 0.1 0.1 0.034 U

7440-39-3 BARIUM 1 — ' 1 . 1 1 1 0 00069

7440-43-9 CADMIUM 1 0 05j 0.05 0.0017 u 7440-47-3 Cl IROMIUM 0.0003 0 1 0,0033 B

7439-92-1 LL'AO 1 0.03 0.03 0,016 U

7782-49-2 SiriFN.'UM 1 0.00 0.05 0.026 U

. 7440-22-4 SILVER 0.1 I .. . °'1 0.0045 U

Data P a c k a g e ID : IT000Q127-1

Dale Prinled: Wednesday. September 27, 2000 Paragon Analytics Inc. I.IMS Vivnon' 1 DOC

Page 9 of 14

SEP-28-00 THU 04:29 PH AGON ANALYTICS FAX NO.-970 490 1349 P. 13


Sample Results



Ciiunl Name: IT Corporation Las Vegas


Field ID: <SUP31102(M

U b l D ; 0009127-38



Dato Collected; 16-Sep-00 Date Extracted: 21-Sop-00 Date Analyzed: 22-Sep-00

Prep Batch: 1P000921-1 QCBatchlD:lP00092l-1-1

RuntD;IT000922-1A3 Cleanup: NONE

Basis: As Received


File Namo: TS00922

CASNO Target Analy te Di lut ion Resul t Report ing IDL Result EPA Factor L imi t Qual i f ier Qualif ier

7440-3IJ-2 ARSENIC 1 0.1 0.1 0.034 U

7440-39-3 BARIUM 1 0.92 1 j 0,00069 > ' 74 40-43. •£} CADMIUM

• 0.0016 0.05 0.0017 B

i 7440-47-3 CHROMIUM o.oosa 0.1 0.0033 B

j 7439-92-1 LCAD 0.03 0.03 0.016 U

! 7762-49-2 SFLE'NIUM 0.05 0.05 0.026 U

' 7440-22-4 SILVER 0 1 I 0.0045 !" u" J.. . . .


Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS Vcr.ion 1 &9d

Pago 10 of 14

SEP-28-00 THU 04:29 PM E£RAGON ANALYTICS FAX N0—970 490 1349 P. 14


Sample Results

Lab Namo: Paranon Analytics, Inc.




Fiftld ID;, CBPS120204

Lab ID: oooo 127-39


Sample Matrix: LEACHATF. % Moisture: N/A

Date Collected: 16-Scp-00 Dato Extracted: 21-Sep-OO Date Analyzed: 22-Sep-00

Prep Batch: IP000921-1 QCBatchID: IP000921-1-1


Basis: As Received

Sample Aliquot: 5 G Final Volume; SO ML Result Units: MG/L

File Name: TS00022

CASNO Target Ana ly te Di lut ion Factor

Result Reporting Limit

IDL Result Qualifier

EPA Qualif ier

• 7440.38-2 ARSENIC ! 1 0.1 0.1

1

0.034 u

' 7440-39-3 DARIUM 1 1.4

0.1

1 0.00069

• 7440-43-9 CADMIUM 1 0.05 0.05 0.0017

...V. i 7440-47-3 CHROMIUM i 0.0037 0.1 0.0033 B

I 7439-92-1 LEAD 1 0 03 ; 0.03 0.016 U

7782-49-2 SELCNIUM i 0.05 j 0.05 0.026 .. . u ! 74 4 0-22-4. SILVER j 1 0.1 0.1 0.0045 I u


Dato Printed: Wednesday, September 27, 2000 Paragon Ana ly t ics Inc. P a 9 e 1 1 o f 1 4

LIMS Vfcruon, 1 005

SEP-28-00 THU 04:29 PM AGON ANALYTICS FAX NO,—370 490 1349 P. 09


Sample Results

Lai? Name: Paragon Analytics, Inc.

Work Order Num ber: 0009127



Field ID:' GBPS170204

Lab ID: ooosi?7-2S

I.EACH DATE: 9/20/2000

Sample Matrix: LEACHATl£ % Moisture: N/A

Date Collected: 17-Sep-00 Date Extracted: 21-Seu-00 Dato Analyzed: 22-Sep-OO

Prep Batch: IP000921-1 QCBatchlD:|P000921-1.1


Basis: As Received

Sample Aliquot: 5 G Final Volume: 50 ML Result Units: MG/L

File Name; TS00922

CASNO Target Ana ly te Di lut ion Result Report ing IDL Resul t EPA Target Ana ly te Factor Limit Qual i f ier Qualif ier

7440-30-2

7440-30-3

7440-43-9

7440.47-3

7439- 92-1

7782-49-2

7440- 22-4

| ARSENIC

j PARIUM

J CADMIUM

j CHROMIUM

I LCAO

• SELENIUM I I SILVER I

0.1 0.1 0.034 U

- o.oj' 1 0.00069 B

0.05 0.05 0.0017 U

O.OO34! 1

0.1 0.0033 B

0.03 j 0.03 0.016 . U

D.05| 0 05 0.026 U

0.1 i 0.1 0.0045

U


Dato Printed: Wednesday, September 27, 2000 Paragon Analytics lllC. LIMS VOl'SIOd- 1 CUCr

Page 6 of 14

SEP-28-00 THU 04:29 PM P AGON ANALYTICS FAX NO. ^ 0 490 1349 P. 08


Sample Results

Lab Name: Paragon Analytics, tne.

Work Order Number: 00Q9I27



Flbld ID: GHPS1B0911

Lab ID: ooosn 77-24

LEACH DAI E: 9/20/2000


Date Collected: 17-Sep-OO Dato Extracted: 21-Sep-OO Date Analysed: 22-Sep-00

Prep Batch: IP000921-1 QcaatchlD: IP000921-1-1


Basis: As Received


File Name: TS00922

CASNO Target Analyte Dilution Result Report ing IDL Result EPA Factor Limit Qualif ier Qualif ier

7440-3U-2 ARSENIC 0,1 0,1 0.034 U

7-140-39-3 BARIUM • '' " - 1 : 1 1 0.00069

7440-43-9 CADMIUM 0 05' 0.05 0 0017 u 7440 47-3 CHROMIUM

•• I -0.0051 0.1 0.0033 B

7439-92-1 LPAD 0 03 0.03 0.010 U

7702-40-2 SELFNUJM 1 0 05. 0,05 0.026

7440-22-4 SILVER 0.1 0.1 0.0045


Data Printed: Wednesday. September 27, 2000 Paragon Analytics Inc. LIMS V.-rSiun 1

Page 5 of 14

SEP-28-00 THU 04:29 PH PARAGON ANALYTICS FAX NO. 970 490 1349 P. 15

TCLP ICP Metals Method SW6O10--TCLP Leachate

Sample Results


Work Ordor.Number: 0009127



Field ID; CBPS21020.4

LHb ID; ' 000912MO


Sample Matrix: LEACHATE % Mois tu re ; N/A

Date Collected: 19-Sep-00 Dato Extracted: 21-Sep-OO Date Analyzed: 22-Sep-OQ

Prup Batch: IP000921-1 QCBatchID: IP000921-1-1


Basis: As Received

Sample Aliquot; 5G Final Volume: 50 ML Result Units; MG/L

File Name: TS00922

CASNO Target Analy te Di lut ion Result Report ing IDL Result EPA Factor Limit Quali f ier Qualif ier

7440-38-2 ARSHNlC 1 0,1 0,1 0.034 u

7440-39-3 BARIUM 1 2.1 0.00069

j 7440 ! CADMIUM 1 0,05 a . 0 5 . 00017 u

7440-47-3 CHROMIUM i 0.0078 0.1 0 0033 . B

, 7439-92-1 LEAD 1 0.03

0.03 0.016 * U

' 7782-40-2 SELENIUM i 0.05 0.05 0.026 u

7410-22-4 SILVER 1 0.1 0 1 0 0045 U i


Dale printed: Wednesday, September 27, 2000 Paragon Analytics Inc. I.IW5 v.awnn t BOG

Page 13 of 14


TCLP MERCURY Method SW7470

Sample Results

Lab Name:

Client Ni'imo:

Client Project ID:

Work Order Number:

Paragon Analytics, Inc.

IT Corporation Las Vegas

Gasbuggy

0009127

Reporting Basis: As Received

Final Volume: 20 G

Matrix: LEACHATE

Result Units: MG/L

Cl ient Sample ID Lob ID Date

Col lec ted

Date Prepared

Date Analyzed

Percent Moisture

Di lu t ion Factor Result

Repor t ing L imi t

IDL Flag

Sample A l iquot

GBPS010C09 0000127-4 0/14/2000 8/21/2000 09/22/.'!0(l0 N/A 1 ; 0 002 0.002 0 000092 u 2 G

GBPS010911 0000127-5 3/14/2000 0/21/2000 09/22/2000 N/A i 1 i

0.002 0,002 0.000092 U 2G

CBPS020G10 0009127-12 S/14/200O 9/21/2000 09/22/2000 N/A 1 0,002 0.002 0.000092 U 2G

• GBP8O301O6

0009127-13 9/15/2O00 9/21/2000 09/22/3000 N/A 1 0.002 0.002 0.000092 . . .

u 2G

GePSn40K56 0009127-14 9/15/2000 9/21/2000 09/22/2000 N/A r 0.002 0.002 0.000092 u 2G

GDPS05U40B 0009127-15 9/15/2000 9/21/2000 09/22/2000 N/A 0.002 0.002 0.000092 u 2G

Gt.lPS1RQ911 0009127-24 9/17/2000 9/21/2000 09/22/2000 N/A 1 | 0.002 0.002 0.000002 u 2 C

G0I,31702C4 0009127-Z5 9/17/200O 9/21/2000 09/22/2000 N/A 1 | 0.002 0.002 0.000002 u 2G

GCPi->060608 0009127-35 9(15/2000 9/21/2000 09/22/2000 N/A 1 ! 0 002 0.002 -0 000092

IJ 2G

G3PSS070G08 0009127-36 9/15/2000 9/21/2000 00/22/2000 N/A 1 0.002 0.002 0 0000D2 u 2G

• GBPS1Q0204 0000127-37

9/16/2000 9/21/2000 00/22/2000 N/A ._ 0.002 0.002 . . . 0.000092

u 2G

GRPS110?Q4 0009127.33 0/16/2000 9/31/2000 os>/?a/?ooo N/A 1 0.002 0,002 0.000002 u 2G

j GBPS120204 0009127-39 9/16/2000 9/21/2000 09/22/2000 N/A 1 0.002 0.002 0 000092 u 2G

' GDPS210J04 0009127-40 9/19/2000

9/21/2000 09/22/2000 N/A 1 0.002 0.002 0 000092 u 2G

Comments:

1. ND or U a Not Delected at or above tho client requested detection limit.

Data Package ID: HG0009127-1

Onto Printed: Friday, September 22, 2000 Paragon Analytics Inc. IIMS Vois.Oil 1806

Page 1 of 1

TCLP - Volatiles

Method SW8260

-SEPv-29-00 FRI 03:45-PM PMAGON ANALYTICS FAX NO. _2JQ 490 1349 P. 04

GC/MS Volatiles Method SW8260--TCLP Leachate

Sample Results

Lab Name: Piiragon Analytics, Inc.



ClioniPiojcct ID: Gas.buggy

f jeWTpii OBPS010G09 x

•. L»;bil?:';-;ooooi27-4


Sample Matrix: LF.ACHA1 £ % Moisture: N/A

Dale Collected: 14-Sep-00 Date Extracted: 21 -Sep-00 Dale Analyzed: 21 -Sep-00

Prep Batch: VL000921-1 QCBatchID: VL000921 -1 -3

Run ID:VL000921-1A Cleanup: NONE

Basis: As Received

Sample Aliquot: 5 ML Final Volume: 5 ML Result Units: UG/L

File Name: A120S2

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Factor Limit Qualifier Qualifier

75-01-4 VINYL CHLORIDE S 50 50 2.4 u 75-35-4 1.1-DlCHl.OROETHeNS 5 j 5 25 2.8 u 70-93-3 2-BUTANONE S 100 100 31 u 67-66-3 CHLOROFORM 5 25 25 0.7 u r>0-2.3 5 CARBON TETRACI4LORIDE 5 25 25 7.5 u 107-00-2 1,2-DICHLOROETI IANE 25 25 1.5 u 71-43-2 BENZENE 5 "'ih 25 2.7 u 79-01-e TRICHLOROETHENE S 25 25 4 1 u 127-10-4 TETRACMLOROETHENE S ZS 25 4.3 u 108-90-7 CI-ILOROOCN^ENE s ' 2 S 23 2.3 u

Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike

Amoun t

Percent

Recovery

Control

Limits

450-00-4

1868-53-7

4-BROMOFLUORODENZENE

DTB'RO'MO^LUORC^ -

51 5

48,9

50

50

103

98

82-123

75-127

2037-20-6 TOLUENE-DS 50.2 50 100 8 9 - 1 1 6

0.033 t 0>o43 7 ^ ^ '

Data Package ID; VL0009127-6

Date Printed: Friday, September 29. 2000 Paragon Analytics Inc. LIMS Vofbion 1 807

Page 7 of 8

SEP-29-00 FRI 03:46 PM Pfi£AG0N ANALYTICS 3 ^ G FAX NO. MO 490 1349 P. 05


Sample Results





r(ti>ct : GBP-soiosi 1 V

': Lab ID:';:O009127-S

LEACH DATfi: 9/20/2000

Sample Matrix: LEACHATE V. Moisture: N/A

Date Collected; 14-Scp-00 Date Extracted: 21-Sup-OO Date Analyzed: 21-Scp-OO

Prep Batch: VL000921-1 QCBatchID; VL000921 -1 -3

Run ID: VL0OO921-1A Cleanup: NONE

Basis: As Received


File Name: A12053

C A S N O Target Analyte Dilution Factor


M D L Result Qualifier

EPA Qualifier

75-01-4 VINYL CHLORIDE s 50 50 2.4 u

75-35-4 1.1-DICHLOROETHENt: s 25 25 2.8 u 70-93-3 2-BUTANONE 100 100 31 u 67-ES-3 CHIOROKIRM 5 "js 25 0.7 u 56-23-5 CARBON TETRACHLORIDE 5 25 2S 7.5 u 107-OG-2 1,2-DICI ILOROETHANE S 25 25 1.5 u 71-43-2 KENZtNE 0 25 25 2.7 u 79-01-6 TRICHLOROETHENE S 25 25 4.1 u 127-18-4 TETRACHLOROETHENE 5 25 25 4.3 u

108-00-7 CHLOROBENZENE 5 25 25 2.3 u

Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Amoun t

Percent Recovery

Control Limits

4GO-00-4 4-BROMOFLUOROBENZENE 53.1 50 106 6 2 - 1 2 3

1868-53-7 DIBROMOFLUOROMETHANE 47.5 50 95 7 5 - 1 2 7

2037-2(3-5 TOLUENE-D8 52 50 104 8 9 - 1 1 6

Data Package ID: VL0009127-6

Dale Pfinied: Friday, September 29.2000 Paragon Analytics Inc. LlMS Version 1 i!)7

Page 8 of 8

SEP-29-00 FRI 03:46 PM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 06


Sample Results



Client Name: IT Corporalion Las Vegas


Field ID;.•'GHPSQ2001 o x

• • ^^ '0009127-12 "


Sample Matrix: L.FACHATE % Moisture: N/A

Date Collected: 14-Sep-00 Dale Extracted; 21-Sep-<10 Date Analyzed: 21-Scp-OO

Prep Batch: VL000921-1 QCBatchID: VL000921-1-3

RunlD:VL000921-1-A Cleanup: NONE

Basis: As Received


Fili« Name: A12056

CASNO Target Analy te Dilution Result Reporting MDL Result EPA

Factor Limit Quali f ier Qualifier

75-01-4 VINYL CHLORIDE 5 50 SO 24 u 75-35-4 LI-DICnLOROLTICNE 5 25 25 2.S u 70-93-3 2-BUTANONE 5 100 100 31 u 67-6G-3 CHLOROFORM S 0.99 25 0.7 J

56-23-5 CARBON TETRACHLORIDE G 25 25 7.5 u 107-00-2 1,2-DICI (LOROETHANE G " ' 23 25 1.5" u 71-43-2 DCNZCNE 5 25 25 2.7 u

I 79-01-6 TRICHLOROeTHIfNE 5 25 25 4.1 u 127-1M TC 1 RACHLORQe'l Ht'Nf. S 25 25 4.3 u 100-50-7 Cl iLOROBftNZENE s 25 25 2.3 u

Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Amount

Percent Recovery

Control Limits

4G0-O0-4

1868-53-7

4-BROMOFLUOROBENZENE

DIDROMOFLUOROMETHANE

51.3

46.B

50

50

103

94

82-123

75-127

2037-26-5 j TOLUENE-D8 | 51.3 SO 103 89-116


Drfia Pilntcd: Fiiday, September 29,2000 Pa ragon Ana ly t i cs Inc. P a 3 e 1 o f 8

LIMS vrrwon 1 U97

SEP-29-00 FRI 03:46 PM PARAGON ANALYTICS 3^A( FAX NO. 970 490 1349 •

P. 07


Sample Results


Work Ordor Number: 0000127


ClientProject ID ; Gasbuggy

F |jjld"it)v GEiPS03C40e y

• Lab lb:'' 001W127-13



Date Collected: 15-Sep-00 Date Extracted: 21 -Sep-00 Date Analyzed: 21-Sep-00

Piop Batch: VL00092M QCBatchlD: VL000921 -1 -3

Run ID: VL000921-1A Cleanup: NONE

Basis: As Received


File Name: A12057

CAS MO Target Analyte Dilution Factor

Result Report ing Limit

MDL Result Qualifier

EPA Qualifier

75-01-4 VINYL Cl ILORIM: s 50 50 2.4 u

75-35-4 1.1-DICHLOROeTHcNE s 25 25 2.8 u

75-93-3 2-DUTANONE 5 100 100 31 u

07-66-3 CHLOROFORM 5 25 25 0.7 U

5(3-23-5 CARBON TETRACHLORIDE 5 25 25 7.5 u

107-06-2 1,2-DICHLOROETHANE 5 25 25 1.5 u

71-43-2 BENZENE & 25 2.7 u

70-01-6 TRICHLOROETHENE 5 25 25 4.1 u

127-18-4 TETRACHLOROETHENE S 25 25 4.3 u

108-00-7 CHLOROBENZENE 5 25 25 23 u

Surrogate Recovery


Percent Recovery

Control Limits

450-00-4

1868-53-7

4 • 6ROMOFLUOROBENZENE

oierToMoT^

49.9

51.5 —-*

50

SO

100

103

62-123

75-127

5037-26-5 TOLUENE-DS j 52.6 50 105 89-116

NO 1Z/W/1 t>rvm

Data Package ID: VLOO09127-6

Dale Printed: Friday. September 29,2000 Paragon Analytics Inc. UMSVuftKM 1 Wl?

Page 2 of 8

SEPT29-00 FRI 03:46 PM PARAGON ANALYTICS P^Ai FAX NO. £70 490 1349 P. 08


Sample Results

Lab Name; Paragon Analytics, Inc.

Work Order Number: 00091 27


cilontProject ID: Gasbuggy

Fi'tfJU IP; ••• GBPS04O4D6 X

i;?tijp;.:::OQ^3i27.i/i

LEACH DATC 9/20/2000


Date Collected: 15-Sep-00 Date Extracted: 21 -Sep-00 Dale Analysed; 21 -Sep-00



Basis: As Received


File Name: A12058

C A S N O T a r g e t A n a l y t e D i l u t i o n

F a c t o r

Result R e p o r t i n g

L i m i t

M D L R e s u l t

Q u a l i f i e r

E P A

Q u a l i f i e r

75-01-4 VINYL CHLORIDE 5 50 50 2.4 U

75-35-4 1.1-DICHLOROETHENE i 25 25 2.6 U

78-<J3-3 2-BurANONfi S 100 100 31 U

67-66-3 Cl ILOROFORM s 25 25 0.7 U

50-23-5 CARBON TETRACHLORIDE s 25 25 7.5 U

107-06-2 1 ,Z-DlCHLORO£THANE 25 25 1.5 U

71-43-2 GF.NZENE """V 25 25 2.7 U

79-01 -6 TRICHLOROCTHCNE ~~ 5 25 25 4.1 U

127-18-4 TiiTRACHl-OROetHENli s 7.5 25 4.3 U

108-00-7 CHLOROBENZENE 5 25 25 2.3 U

Surrogate Recovery


Percent Recovery

Control Limits

460-00-4

U150-53-7

4' BROMOPLUOROBEN2EN6

DIBROMOFLUOROMGTIIANE

49.3

47.3

50

50

99

SS

8 2 - 1 2 3 460-00-4

U150-53-7

4' BROMOPLUOROBEN2EN6

DIBROMOFLUOROMGTIIANE

49.3

47.3

50

50

99

SS 7 5 - 1 2 7

2037-25-5 TOLUENE-D8 50 4 50 101 5 9 - 1 1 6

Data Package ID; VL0009127-6

Date Printed: Friday, September 29, 2000 Paragon Analytics Inc. LIMS Verdun 1 8 0 /

Page 3 of Q



Sample Results


Work Older Number: 0009127

Client Name: IT Corporation Laa Vegas

Clienl Project ID: Gasbuggy

Field' jb; - GDPS0S0403 V

M.ablC):.;O009i27-i&


Sample Matrix: LEACHATE Vt Moisture: N/A

Date Collected: 15-Sep 00 Date Extracted; 21-Sep-OO Date Analyzed: 21-Sep-OO


Run ID-.VL000921-1A Cleanup: NONE

Basis: Aa Received


File Name: A12059

CASNO Target Analyte Di lut ion Factor



EPA Qualifier

73-01-4 VINYL CHLORIDE 5 SO 50 2.4 U

75-35-4 1,1-DICHLOROETHENE s 25 25 2.8 U

75-93-3 2-BUTANONC s 100 100 31 u

67-6(3-3 CHLOROFORM s 25 25 0.7 u

ES-23-5 CARBON TETRACHLORIDE 5 25 25 7.5 u

107-0S-2 1,2,-OICHLOROETHANE 5 25 25 1.5 u

71-43-2 REMZENE 5 25 25 2.7 u


127-18-4 TETRACHLOROETHENE 5 25 25 4.3 u

100-90-7 cni.oRonr.N7eNe G 25 2S 2.3 u

Surrogate Recovery


Percent Recovery

Control Limits

460-00-4 4-DROMOrLUOR06c'NZeNE 50.5 50 101 82-123

13G8-53-7 DIBROMOFLUOROMETIIANE 49.7 50 99 75-127

2037-2G-5 TOLUENE-D8 49 9 50 100 89-116

Data Packatje ID: VL000D127-6

Date Printed: Friday, September 29,2000 Pa ragon Analy t ics Inc. Page 4 of 8

LIMS Vvraon: 1 697

SEP-29-00 FRI 03:47 PH PARAGON ANALYTICS FAX NO. JtfO 490 1349 P. 13


Sample Results


Work Order Number: OOOO 127


ClientProject ID: Gaobuggy

': LMb |pi-p.-00QQ127-3G

L E A C H D A T E : 9/22/2000


Date collected; 15-Sep-OO Date Extracted: 26-Sep-00 Date Analyzed: 2fi-Sep-00

Prep Batch: VLO0O926-1 QCBatchID: VL000926-1-1

RunlD:VL000926-1A Cleanup: NONE

Basis: As Received


File Name: A12087

CASNO - — —r ~ Target Analyte

Dilution Factor



EPA Qualifier

75-01-4 | VINYL CHLORIDE 1 10 10 0.48 U

75-35-4 1,1-DICHLOROETHENE 1 5 5 0.55 u

78-93-3 2-BUTANONE 1 7.3

5

20 6.2 J

67-66-3 CHLOROFORM 1

7.3

5 5 0.14 u

56-23-5 CARBON TETRACHLORIDE 1 5 5 1.5 u

107-00-2 1,2-DICI ILOROETHANS 1 5 5 0.29 u

71-43-2 PEN?ENE 1 5 5 0.53 u


127-18-4 TETRACHLOROETHENE 1 5 5 0.65 u 108-90-7 CHLOROBENZENE 1 5 5 0.45 u

Surrogate Recovery


Amoun t

Percent Recovery

Control Limits

460-00-4 4-BROMOFLUOROBENZENE 50.1 50 100 8 2 - 1 2 3

1868-53-7 DIBROMOFLUOROMETHANE 47.5 50 95 7 5 - 1 2 7

2037-26-5 TOLUEN& D8 46.7 50 93 8 9 - 1 1 6

Data Package ID: VLO0O9127-5

Dale Printed; Thursday, September 28,2000 P a r a g o n Ana ly t i cs Inc. Page 1 of 4 I.IMS Vureion 1.BSX3

SEP-29-00 FRI 03:47 PM PJfcAGON ANALYTICS P^C FAX NO. M ) 490 1349 P. 14


Sample Results Lab Mame: Paragon Analytics, Inc.



ClientPiroject ID: Gasbuggy

FkW'i&'- CBPS070G08 V

' Lab'-ID:^ 0009127-36


sample Matrix: LEACHATE % Moisture: N/A

Date Collected: 15-Scp-00 Dale Extracted: 26-Sop-00 Date Analyzed: 27-Sep-00

Prep Batch: VL000926-1 QCBatchID: VL0OO926-1 -1


Basis: As Received

Sample Aliquot: 5 ML Final Volume: S ML Result Units: UG/L

File Name: A12091




EPA Qualifier

75-01-4 ; VINYL CHLORIDE i 10 10 0.48 U

75-35-4

76 93-3

1,1-DICHLOROETHENE 5 5 0.55 U 75-35-4

76 93-3 2-BUTANONE 6.7 20 6.2 J

S7-63-3 CHI OROFORM i 0.23 5 0.14 J »

56-23-5

ToT-oeTa

CARBON TETRACHLORIDE

1.2-DICHLOROGTlMANt!

5 5 1.5 u 56-23-5

ToT-oeTa

CARBON TETRACHLORIDE

1.2-DICHLOROGTlMANt! 5 5 0.29 u 71-43-2 BENZENE 1 5 5 0.53 u 79-01-6 TRICHLOROETHENE 1 5 5 0.81 u 127-1 B-4 TETRACHLOROETHENE 1 5 5 0.B5 u 108 90-7 CHLOROBENZENE 1 5 5 0.45 u

Surrogate Recovery


Percent Recovery

Control Limits

4C0-00-4 4-BROMOFLUOROBENZENE 5 2 6 50 105 8 2 - 1 2 3

1058-53-7" DIBROMOFLUOROMETHANE 47.0 50 96 7 5 - 1 2 7

2037-20-5 TOLLIENE-D8 48 50 96 8 9 - 1 1 6

N~0 TPfTtOh PATTr-

Data Package ID: VL0009127-5 •nn • 11rr ••iiiii[MMiMi^m~MMwnrrM«M^^"«W'irrirnT^T7nrTini

Date Printed: Thursday, September 28, 2000 Paragon Analytics Inc. CIMS Version. 1 036

Page 2 of 4

SEP-/29-00 FRI 03:47 PN PARAGON ANALYTICS FAX NO, 970 490 1349 P. 15


Sample Results

Utb Nam*: Paraxon Analytics, Inc.


Client Name: IT Corporation las Vegas

ClientPtoject ID: Gasbuggy

Fjitcl;jp;:-GHPsiaoao4 X

; Lab |DV; oco9'i'27.37' '' '

LEACH DATE; 9/22/2000

Sample Matrix: LEACHATE % Moisture; N/A

Date Collected; 16-Sep-OO Dale Extracted: 26-Sep-00 Date Analyzed: 27-Sep-OO

Prep Batch: VL000926-1 OCBatchID; VL00O926-1-1

Run ID:VL0OO926-1A Cleanup: NONE

Basis: As Received


File Name: A12092

CASNO Target Analyte Dilution Factor



EPA Qualifier

75-01-4 VINYL CHLORIDE 1 10 10 0.48 u 75-35-4 1,1-DICHLOROETHENE J ... 5 5 0.55 u 78-93-3 2-BUTANONE 20 20 6.2 u 57-CS-3 Cl ILOROFORM 1 5 5 0.14 u 56-23-5 CARBON TETRACHLORIDE 1 5 5 1.5 u 107-00-2 1,2-DICI ILOROETHAME 1 5 S 0.29 u 71-43-2 BENiFNE '1 5 5 0.53 u 79 01-6 TRICHLOROETHENE 1 5 5 0.81 u 127-18-4 TETRACHLOROETHENE 1 5 5 0.85 u 108-90-7 CHLOROBENZENE 1 5 5 0.45 u

Surrogate Recovery


Percent Recovery

Control Limits

460-004 4-BROMOFLUOROBENZENE 47.3 50 95 8 2 - 1 2 3

1068-53-7 DIBROMOFLUOROMETHANE 46.4 io 93 7 5 - 1 2 7

2037-26-5 TOLUENE-D8 48.6 50 97 8 9 - 1 1 6

Data Package ID: VL0009127-S

Dale Printed: Thursday, September 28,2000 Paragon Analytics Inc. I IMS Vorr.ion: 1 898

Page 3 or 4


GC/MS Volatiles Method SW8260-TCLP Leachate

Sample Results





. LaVip;' :-oooai27-3B



Date Collected: 16-Qcp-00 Dale Extracted: 27-Sep-OO Dale Analysed: 27-Sep-OO

Piep Batch: VL000927-1 QCBatchID: VL000927-1 -2


Basis: As Received


File Name: A12103



MDL Result Qual i f ier

EPA Quali f ier

75 01-4

75-35-4

VINYL CHLORIDE i 10 10 0.48 U 75 01-4

75-35-4 1.1-DICHLOROE1HENE i] 5 5 0.55 U

78-03-3 2 -BUTANONE 1 6 4 20 6.2 J

67-1)0-3 ci iLorcoroRM

• 5 5 0,14 U

56-23-5 CARBON TETRACHLORIDE

• 5 5 1.5 U

107-00-:? 1.2-DICI ILOROETHANE 1 5 5 0.29 U

71-43-2 BENZENE 1 5 5 0.53 u

79-01-0 TRICHLOROETHCNE 1 5 5 0.81 u

127-10-4 TETRACHLOROcTHENF. 1 5 5 0.85 u

100-90-7 CHLOKOBfiNZENt; 1 5 5 0.45 u

Surrogate Recovery

C A S N O S u r r o g a t e A n a l y t e R e s u l t F lag S p i k e

A m o u n t P e r c e n t

R e c o v e r y

C o n t r o l

L i m i t s

4I30-00-4 4-BROMOFLUOROBENZENE 51.4 50 103 62-123

DIBROMOFLUOROMETI1ANE 50.9 50 102 75-127

2037-20-5 TOLUENE-D8 48.6 50 97 89-116

Data P a c k a g e I D : VL0009127-4

Date Printed: Tl lursday, September 28,2000 Pa ragon Analy t ics Inc. Page 1 of 2 I IM:; Vision- 1 £198

FAX NO. 970 490 1349 P. 20


Sample Results Lab Name: Paragon Analytics, Inc.




•;f,>ftllO;*G B psi202C4 y

:Lab'ipi; 0039127-13'

LEACH DATE: 9/2Z/2000


Date Collected; 16-Sep-OO Date Extracted: 27-Sep-OO Date Analyzed: 27-Sep-OO

Prep Batch: VL000927-1 QCBatchIO: VLQ00927-1-2

Run ID:VL000927-1A Cleanup: NONE

Basis; As Received


File Name; A12104

CASNO j Target Analyte Dilution R e s u l t Reporting M D L R e s u l t E P A

1 Facto? Limit Qualifier Qualifier

75-01-4 VINYL CHLORIDE i 10 10 0.48 u 75-35-4 1,1-DICHLOROETHENE 1 5 5 0.55 u 75 93 3 2-BUTANONE i 20 20 6,2 u H7-GG-3 CHLOROFORM 1 5 5 0.14 u 56-23-5 CARBON TfiTRACHLORIDE 1 5 5 1.5 u 107-00-2 1,2-DICHLOROETHANE 1 5 5 0.29 u 71-43-2 BENZENE . i 5 5 0.53 u 79-01-6 TR1CIILOROETHENE i 5 5 0.81 u 127-18-4 TETRACHLOROETHENE 1 5 5 0,85 u 10U-00-7 CHLOROBENZENE \ 5 5 0.45 u

Surrogate Recovery


Percent Recovery

Control Limits

4G0-00-4

16(50-53-7

2037-26-5

4-BROMOFLUOROBENZENE

"DIB^OMOFLUOROMGTHANE "

50.6

49.6 — ~

50

50

101

9 9 .

8 2 - 1 2 3

75 - 127~

4G0-00-4

16(50-53-7

2037-26-5 TOLUKNe-D8 45.6 J 50 91 8 9 - 1 1 6


Dale Printed: Thursday, September 28,2000 Paragon Analyt ics Inc. P a a e 2 cf 2 i IMS ViMsior 1 CMS




Worli Ordor Number: 0009127

Clie nt Name: IT Corporation Las Vegas


'jplietdip; 70304 X

. Lab ID;.:'O009I27-2&

LEACH DATC: 9/20/2000

Sample Matrix: LEACIIATE % Moisture: N/A

Date Collected: 17-Sep-OO Date Extracted: 21-Sep-00 Date Analyzed: 21 -Sep-00

Prep Batch: VL000921-1 OCBatchID: VL000921-1-3

Run ID: VLO0O921-1A Cleanup: NONE

Basis: As Received

Sample Aliquot: S ML Final Volume: 5 ML Result Units: UG/L

File Name: A12061

C A S N O Target Analyte Dilution Result Reporting MDL Result EPA Factor Limit Qualifier Qualifier

75-01 <l VINYL CHLORIDE s 50 50 2 4 U

75-35-4 1,1-DICHLORO ETHENE s 25 25 2 8 U

78-93-3 2-BUTANONG $ 100 100 31 U

07-56-3 CHLOROFORM 5 25" 25 0.7 u. 56-23-5 CAR HON TETRACHLORIDE 5 25 25 7 5 u

107-00-2 1,2-DICHLOROETI IANE 5 ?r. 25 1.5 u

71-43-2 BENZCNG S 25 25 2.7 u


127-16-4 T t fRACHLOROETHENE S 25 25 4.3 u 100-00-7 CHLOROBENZENE 5 25 25 2.3 u

Surrogate Recovery


Amount Percent

Recovery Contro l

L imits

400-00-4 4-BROMOFLUOROBENZENE 49.7 50 99 8 2 - 1 2 3

1868-53-7 DIBROMOFLUOROMETHANE 49 7 50 99 7 5 - 1 2 7

2037-26-5 TOLUCNE-DO 522 ; J .

50 104 8 9 - 1 1 8

tJO TK-mOH PA-IT)


Date Printed: Friday. September ?9.2O0O Paragon Analytics Inc. LIMS Vis ion 1 817

Page 6 of 8

SEP-29-00 FRI 03:46 PH RMAGON ANALYTICS FAX NO. ^ 0 490 1349 P. 10

GC/MS Volatiles Method SW8260-TCLP Leachate

Sample Results




ClienlProjC-ct ID: Gasbuggy

F,'Qi«ljrj.,GI3PS180911 <

L'ab.lD:::0<J09i27-24



Dale Collected: 1?-Sep-00 Date Extracted: 21-Sep-00 Date Analyzed: 21 -Sep 00

Prep Batch: VL000921-1 QCBatcbiD; VLOO0921-1 -3

Run ID: VL000921 -1A Cleanup: NONE

Basis: As Ruceivad


File Name: A12060




EPA Qualifier

75-01-4 VINYL CHLORIDE s 50 50 2.4 u 75-35-4 1,1-DlCHLOROfcTHE-NE s 25 25 2.8 u 78-93-3 2-BUTANONE 5 100 31 U

67-C6-3 CHLOROFORM 5 25 25 0.7 u 55-23-5 CARBON TETRACHLORIDE 5 25 25 7.5 u 107-06-2 1,2-DICI ILOROETHANE 5 25 25 1.5 u 71-43-2 BENZENE 5 25 25 2.7 u •" i

79-01-6 TRICHLOROETHENE 5 25 25 4.1 u 127-18-4 TETRACI1LOROCTIIENC 25 25 4.3 u

| 108-0O-7 CHLOROnrN7ENI: 5 25 25 2.3 u

Surrogate Recovery


Percent Recovery

Control Limits

460-00-4 4-BROMOFLUORODENZENE 51.2 50 102 8 2 - 1 2 3

1860-53-7 — . . . , . , „ . , „ , „ . , , . . , . , , ,

DIBROMOrLUOROMETHANG 47.9 50 06 7S-127

2037-28-8 TOLUENE-DO 53.4 50 107 6 9 - 1 1 6

Data Package ID: VL00Q9127-6

Date Printed: Friday, September 29, 2000 Paragon Analytics Inc. UMS Version 1 017

Page 5 of 8

. -29-00 FRI 03:47 PH J

PARAGON ANALYTICS P ^ FAX NO. 970 490 1349 P. 16


Sample Results





Field ID: :G[JPS210204 X

i'ab'lD':,* 0009127-40



Date Collected: 19-Sep-00 Date Extracted: 26-Sep 00 Date Analyzed: 27-Sep-OO

Prep Batch: VL0OO926-1 QCBatchID: VL000926-1 -1


Basis: As Received


File Name: A12095




EPA Qualifier

75-01-4 VINYL CHLORIDE 1 10 10 0.48 U

75-35-4 1,1-DICHLOROETHENE 1 5 5 0.55 u 78-93-3 2-BUTANONE 1 20 20 6.2 u O7-C0-3 CHLOROFORM 1 5 5 0.14 u SS-23-5 CARBON TETRACHLORIDE J 5 5 1.5 u 107-0G-2 1,2-DICHLOROETHANE .. 5 5 0.29 u 71-43-2 ElKNZtNE 1 5 5 0.53 u 79-01-6 TRICHLOROETHENE 1 S 5 0.81 u 127-18-4 TETRACHLOROETHENE 1 5 5 0.85 u 108-00-7 CHLOROBENZENE 1 5 5 0.45 u

Surrogate Recovery


Amount Percent Recovery

Control

L imi ts

450-00-4 4 euOMOI-LUOROBENZENE 48.3 50 97 8 2 - 1 2 3

1368-53-7 DIBROMOFLUOROMETHANE: 46.3 50 93 75 -127

2037-2(3-5 TOLUENE-D8 45.4 50 91 8 9 - 1 1 6

Data Package ID: VL0009127-S

Date Printed: Thursday, September 28,2000 Paragon Analytics Inc. UMS v w w 1 one

Page 4 of 4

TCLP - Semi-Volatiles

Method SW8270

SEP.-29-00 FRI 02:07 PM PMAG0N ANALYTICS FAX NO. S70 490 1349 P^AGON ANALYTICS FAX NO. ^

GC/MS Semi-volatiles Method SW8270-TCLP Leachate

Sample Results

P. 48





Field tD; CBPB010509

Lab ID; ''0000127-4



Date Collected: 14-Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 24-Sep-OO

Prep Batch: EX000921-3 QCBatchlD: EX000921-3-1

Run ID: SV000924-2 Cleanup: NONE

Basis: As Received

Sample Aliquot: 100 ML Final Volume: 1 ML Result Units: MG/L

File Name: P9793

C A S N O T a r g e t A n a l y t e D i l u t i o n

F a c t o r

R e s u l t R e p o r t i n g

L i m i t

M D L R e s u l t

Q u a l i f i e r E P A

Q u a l i f i e r

• 110-85-1 PYRIDINE 1 0.1 0.1 0.023 U

106-4 G-7 1.4-DICHLOROBENZENE 1 0.1 . . „ _ .

0.011

: 95-4 B-7 "2-MrRllYlpNCNOL 1 6.1 0.1 0.018 U

| 108-39-4 3*4"MCmYl .p i^NbT 1 0,1 0.1 0.013 U

| 67-72-1 HEXACHLORQETHANE 1 0.1 0.1 0.015 U

[ 98-05-3 NITROBENZENE » 0.1 0.1 0.011 U

! 87-68-3 HEXACHLOROCiUrADlL'NlE 1 0.1 0.1 0.014 U

I 86-QG-2

[95-05-4

2,4,0-TRICHLOROPHENbL 1 0.1 0.1 0,011 U I 86-QG-2

[95-05-4 2,4.6-1 RICIILOROPIIENOL 1 0.5 0.5 0,014 U

121-14-2 2.4-DlNlTROTOLUtlNE 1 0.1 0.1 0.012 u ' 118-74-1 HGXACHI.ORO01-N/T; NE i 0.1 0.1 0.012 U '

| B7-80-5 P ENTACHLO ROPHENOL ... Z.'."\ 0.5 0.5 0.031 I " • ...

Surrogate Recovery

CASNO S u r r o g a t e A n a l y t e Result Flag Spike A m o u n t

Percent Recovery

Control Limits

110-79-6 2 , 4 , 6 - T R I B R O M O P H E N O L 0.487 0.75 65 23 -100

321-60-8 2-FLUOROBIPHENYL 0.303 oT" 61 21 -106

3137-12-4 ZFLUOROPHGNOL 0.447 0.75

60 2 1 - 1 0 0

4165-60-0 NITROBENZENE-D5 0.33 0.5 6G 3 4 - 1 1 1

4165-62-2 PHENOL-DS 0.475 0.75 64 1 5 - 1 0 4

1718-51-0 TERPI-IENYL-D14 0,421 0.5 64 3 3 - 1 1 1

Data Package ID; SV0009127-2

Date Printed: Thursday, September 28,2000 Paragon Analyt ics Inc. P a 9 e 12 of 14 UMSV>r;inn 1 R90

SEP-29-00 FRI 02=08 PM PARAGON ANALYTICS FAX NO. 970 490 1349 PAGON ANALYTICS FAX NO. l


Sample Results

P. 49




ClionlProjcct ID: Gasbuggy

Field ID: 'GD?S010011

, Lab ID: 0009127-!}

LEACH DATE-: 9/20/2000


Date Collected: 14-Sep-00 Date Extracted: 21-Sep 00 Date Analyzed: 24-Sep-00

Prep Batch:EX000921-3 QCBatchlD: EX000921-3-1

Rim ID; SV000924-2 Cleanup: NONE

Basis: As Received


File Name: P9794


110-86-1 PYRIDINE 1 0.1 0,1 0.023 U

106-46-7 1,4- DICHLOROBENZENE 0.1 0.1 0.011 U

95-48-7 2-METHYLPHENOL „ .

0.1 0.1 0.018 U

108-30-4 3+4-METJ IYLPHENOL " o . i 0.1 0.013 U

j 67-72-1 HftXACHLOROETHANG _.._ 1 0.1 0.1 0.015 U

! 9a -95-3 NITROBENZENE 0.1 0.1 0.011 U

87-60-3 _ . HEXACl ILOROBUTADIENE

0.1 0.1 0.014 u 88-0C-2 2,4,6-TUICHLOROPl IENOL ... 0.1 0,1 0.011 u 95-95-4 2,4,5-TRICHLOROPHENOL 0,5 0.5 0.014 u | 121-14-2 2.4-DINI7 ROTOLUENE i 0,1 0.1 0.012 u 113-74-1 HCXACIILOROBENZENE V 0.1 0.1 0.012 u 87-06-5 "PENTAC HTOROP HENOL 0.5 0,5 0.031 u

Surrogate Recovery


Percent Recovery

Control Limits

118-79-6 2,4,C-TRIBR0M0PI IENOL 0.486 0.75 65 23-100

2-FHJOROaiPH6NYL 0.305 0.5 61 21 -106

367-12-4 2-FLUOROPHENOL 0.467 0.75 62 21 -100

4165-60-0 NITROBENZENE-D5 bT34T" 0.5 68 34-111

4165-62-2 PHENOL-DS 0.494 0.75 66 15 -104

1718-51-0 TERPHENYL-D14 0.395 1

0.5 79 33-111

Data Package ID: SV0009127-2

Dale Printed: Thursday, September 28, 2000 Paragon Analytics Inc. LIMS vuiMon: 1 ass

Page 14 of 14


GC/MS Semi-volatiles Method SW8270--TCLP Leachate

Sample Results


WorK Order Number; 00013127


CliontProjcct ID: Gasbuggy

Hold ID: GBP3020G10

l.ab ID: 0009127.12 '



Date Collected: 14 Sep-00 Oate Extracted: 21-Sep-OO Date Analyzed: 24-Sep-00

Prep Batch: EX000921-3 QCBatchlD: EX000921-3-1


Basis: As Received

Samplo Aliquot: 100 ML Final Volume; 1 ML Result Units: MG/L

File Name: P9795

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Factor Limit Qualifier Qualif ier

110-66-1 PYRIDINE 0.1 0.1 0.023 u 106-4G-7 1,4-DICHLOROBENZENE ' i 0.1 0.1 0.011 U

95-48-7 2-METh IYLPHEN0L 1 0.1 o.\~ 0.018 U

108-39-4 344*MI;THYLPHE1>IOL" 0.1 0,1 0.013 U

G7-72-1 HEXACHLOROETHANE 1 0.1 0.1 0.015 U

98-95-3 NITROBENZENE 1 0.1 0.1 0.011 U

' 87-68-3 Hr5<A~CHLOROftl/rXDlENIi" " i 0.1 ""•"'"oT 0.014 u 1 88-06-2 2,4,6-TRICHLOROPHENOL i 0.1 i 0.1 0.011 U

i 95-90-4 2,4.5-TRICHlOROPHENOL i 0,6 0.5 0.014 u ' 121-14-2 2,4-DINITROTOLUENE 0.1 0.1 0.012 u 118-74-1 HCXACHLOROOCNZENC 0.1 0.012

87-D6-5 "PENTACHLOROPHI7NOL """" "0,5 0.5 ^ — _ 0.031 r« Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Percent Control Amount Recovery Limits

118-79-13 2,4,6-TRISROMOPHFNOL 0.473 0.75 63 23-100 !

321-60-8 2-rLUOUOOlPHf.NYL 0.299 0.5 GO 21 -106

367-12-4 2-FLUOROPHENOL 0.457 0.75 61 21 -100

4165-60-0 NITROD CNZIlN C-D5 . .. 0.33

0.5 66 34-111

4165-62-2 PI IENOL-D5 0.479 0.75 64 15-104

1718-51-0 TERPHENYL-D14 0.408 0.5 82 33-111


Date Printed: Thursday, September 28,2000 Paragon Analytics Inc. LIMS va non; \ BX

Page 1 of 14

SEP-29-00 FRI 02:08 PM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 51 P^AGON ANALYTICS FAX NO. ^

GC/MS Semivolatiles Method SW8270--TCLP Leachate

Sample Results Lab Name: Paragon Analytics, inc.


Client Name: IT Corporation las Vegas

ClientProject IO: Gaabuggy

Field ID: GBP503040G

Lab ID: 0009127-13



Dato Collected: IG-Sep-OO Dato Extracted: 21-Sep-OO Date Analyzed; 24-Sep-00

Prep Batch: EX000921-3 QCBatchID: EX000921-3-1

Run ID:SV000924-2 Cleanup: NONE

Basis: As Received

Sample Aliquot; 100 ML Final Volume; 1 ML Result Units: MG/L

File Name: P9796


110-CS-1 PYRIDINE 1 0.1 0.1 0.023 U I 106-46-7 1,<1-DICHLOROBENZENE ' i 0.1 0.1 0.011 u 95-48-7 2-METIIYLPIIENOL i 6.1 0.1 0.018 u 103-39-4 3i4-M£THYl PHCNOL '1 0.1 0.1 0.013 U

67-72-1 HEXACHLOROETHANE ' 1 0.1 0.1 0.015 u 00-95-3 NITROBENZENE "1 0.1 0.1 0.011 ' u 87-68-3 HEXACHLOROBUTADIENE ' i " 0.1 0.1 0.014 u 8Q-0&-2 2.4,6-T 1-llCHLOROPHQ.NOL 1 0.1 0.1 0.011 u 95-95-4 2.4,6-1 RICHI.OROPHENOL i oV 0.5 0.014 u 121-14-2 ifl-DINITRQTOLUCNF. 1 0.1 0.1 0.012 u 118-74-1 HEXACHLOROBENZENE 0.1 0.1 0.012 u 07-06-5 PL'NTACl'lLOROPI ILNOL 0.5 0.5 0031 u

Surrogate Recovery


Percent Recovery

Control Limits

118-79-6 2,4,3-TRIBROMOPHENOL 0.503 0.75 67 23-100

321-00-8 2 FLUOROBIPHENYL 0.304 0.5 51 21-10S

3C7-12-4 2-FLUOROPHENOL 0.463 0.75 62 21 -100

. , 4165-60-0

WITROBENZENE-DS "6.328 ~"6.5~ 66 34 -111

4165-62-2 PHENOL-DS 0.485 0.75 65 i

15-104

• 1718-51-0 TERPHCNYL-D14 0.434 0.5 87 33-111


Date Printed: Thursday, September 28, 2000 Paragon Analytics Inc. LIMSViT.ion. 1.00S

Page 2 of 14

SEP-29-00 FRI 02:08 PN PARAGON ANALYTICS FAX NO. JHO 490 1349 P. 52






Field ID; GBPSO4040S

Ldb ID: ;0009127-14

I. EACH DATE: 9/20/2000

Samplo Matrix; LEACHATE % Moisture: N/A

Date Collected: 15-Scp-OO Dato Extracted: 21-Sep-OO Date Analyzed: 24-Sep-OO



Basis; As Received


File Name: P9797




EPA Qualifier

110-86-1 PYRIDINE 1 0.1 0.1 0.023 u ! 106-46-7 "l.4'wCHLOf{OftFN/f:NC 0.1 0.1 0.011 U

j 95-48-7 2-METHYLPHENOL 1

._. ... 0.1 0,1 0,018 u

! 1D8-30-4 3+4-MiiTHYLPHENOL 0.1 0.1 0,013 u I 67-72-1 HFXACHLOROETHANE . ^ 6.1 0.1 0.015 u j I 98-95-3 NITROBENZENE 0.1 0.1 0.011 u ' 87-68-3 HEXACHLOROBUTADIENE i 0.1 0,1 0.014 U

. 68-0C-2 2,4,6-TRICIILOROPIIENOL 1' 0.1 0,1 0.011 u j 95-95-4 2.4,5-TRICHlOROPHCNOL 1 ~"6.5 0.5 0.014 u 121-14-2 2,40lNnRO'r6LUENC; 1 0,1 0.1 0.012 U

j 118-74-1 HEXACHLOROBENZENE 1 0.1 0.1 0.012 u I 87-8G-5 PENTACl ILOROP) l£NOL .....'..:. 0.5 0,5 0,031 u

Surrogate Recovery

CASNO Surrogate Analyte ' Result Flag Spike Percent Control Amount Recovery Limits

118-79-6 2,4,6-TRIBROMOPHENOL 0.494 0.75 66 23-100

321-G0-8 a-FLUOROQIPHENYL 0,313 0.5 63 21-106

367-12-4 2-rLUOUOPHENOL 6.485 0,75 21-100

4165-60-0 NITRO0UNZCNE-D5 0.349 70 34-111

4165-62-2 PHENOL-D5 0,506 0.75 67 15-104

1718-51-0 TERPHENYL-D14 0,439 0.5 88 33-111


Dato Printed: Thursday, September 28,2000 Paragon Analytics Inc. LIMS Version. 1.B96

Pago 3 of 14

SEP-29-00 FRI 02:08 PH PARAGON ANALYTICS P^Ai FAX NO. 970 490 1349 P. 53


Sample Results

Lata Name: Paragon Analytics, Inc.



ClientProject 10: Gasbuggy

Plftld ID" GBPSQ50-I08

Lab ID: oooai27-i&

LEACH DATfc: 9/20/2000


Date Collected; 15-Scp-00 Date Extracted: 21-Sep-OO Dato Analyzed: 24-Sop-00

Prep Batch:EX000921-3 QCBatchID: EX00097.1-3-1


Basis: As Received

Sample Aliquot: 100 ML Final Volume; 1 ML Result Units: MG/L

File Name: P979B




EPA Qualifier

110-8G-1 PYRIDINE 1 0,1 0.1 0.023 U 1

| 106-46-7 1,4-DICHLOROBENZENE 1 0.1 0.1 0.011 U .. i

j 95-43-7 2-METHYLPIIENOL 1 0.1 0.1 0.018 U

i 108-39-4 I

3*4 MLTHYLPHENOL 1 0.1 0.1 0.013 U I i

j 67-72-1 HEXACHLOROETHANE 1 6.1 0.1 0.015 U ! j

93-05-3 NlTROOCNZCNG 1 0.1 0.1 0,011 u 87-68-3 HEXACHL olwBUTArjlENlj: 'i 6.1 0.1 0.014 U

88-06-2 2,4,G-TRICHLOROPHENOL 1 0.1 0.1 0.011 u 1 95-95-4

|. .. _. ... .. 2,4,5-1 RICHLOROPHENOL 1 0.5 0.5 0.014 u

121-14-2 2,4-DINITROTOLUENE 1 0.1 0.1 0.012 u

118-74-1 HEXACIILOROBENZENE 1 0.1 0.1 0.012 u

87-80-5 PENTACIILOROPIIG.NOL Z'-.Z.T 0.5 0,5 0.031 u

Surrogate Recovery


Percent Recovery

Control Limits

118-79-6 Z.4,6 TRIBROMOPHENOL 0,472 0,75 63 23-100

321-60-8. 2-FLUOROBIPHENYL 0.311 0.5 62 21 -106

367-12-4 2-FLUOROPHENOL O.479'

0.351

0,75 64 21 -100

4160-00-0 NITROBENZENE-OS

O.479'

0.351 0.5 70 34-111

4165-C2-2 PHENOL-D5 0,501 0.75 67 15-104

1718-51-0 TERPHENYL-D14 0.4 0.5 80 ~ 33 -111


Data Printed: Thursday, September 28,2000 Paragon Analyt ics Inc. Pa9 e 4 "f 14 LIMS Vu-.1011 1.t06

SEP-29-00 FRI 02:09 PM PARAGON ANALYTICS FAX NO. 970 490 1349 P^AGON ANALYTICS FAX NO.


Sample Results

P. 56

L ib Name: Paragon Analytics, Inc.



ClioniProJect IO: Gasbuggy

Field ID: GUPSOfioriOO

Lab |D: 0009127-35

LEACH DATE;: 9/20/2000


Date Collected: 15-Sop-oo Date Extracted: 21-Sep-OO Date Analyzed: 25-Sep-00


Run ID: SVO00925-2 Cleanup: NONE

BaslsiAs Received


File Name: P9821




EPA Qualifier

110-6G-1 PYRIOINE 0.1 0.1 0.023 U

' 106-46-7 1.4 DICHl.0l'<08EN?£Ne 1 0.1 oT o.oi r u ! 95 48-7 2 METHYLPHENOL 1 0,1 0.1 0.018 u ; 108-394 3*4-MfTTHYLPHENOL 1' 0.1 0.1 0.013 u : 67-72-1 HEXACHLOROETHANE i 0.1 0.1 0.015 U

98-95-3 NITROBENZENE

11EXACHLOROBUTADIENE

1

1

0.1 0.1 0.011 u S7-C8-3

NITROBENZENE

11EXACHLOROBUTADIENE

1

1 0.1 0,1 0.014 u 8S-05-2 2.4,6-TRiCllLOROPIlENOL . 1 0.1 0.1 0.011 u 95-954 2,"n,5-TRlCHLOROPHENOL o.s 0.5 0.014 u 121-14-2 2,4-DINITROTOLUENE 0.1 0.1' 0012 u 118-74-1 IIEXACIILOROBENZENE 0.1 0.1 0.012 u

07-fl(3-5" plNfAcriLor^iTi^L ~ 1 i . . ..

0.5 0.5 0.031 u

Surrogate Recovery


Percent Recovery

Control Limits

11lS-79-fi 2,4,6-TRIBROMOPHENOL 0.42 0,75 56 23-100

321-60-0 2-rLUORODIPH£NYL 0.291 ~~6,5* 58 21 -106

367-12-4 2-FLUOROPHENOL 0.459 0.75 61 21 -100

4105-60-0 NITROBCNZF.NB-DS 0.322 0,5 T 64 . 34~111

4165-62-2 PHCNOL-DS 0.48 0.75 64 15-104

17118-51-0 TCRPIICNYL-D14 ; 0.394 0.5 79 33-111

Data Package ID; SV0009127-2

Date Printed: Thursday, September 28.2000 Paragon Analytics Inc. LIMS V««itin: 1.89S

Page 7 of 14

SEP-29-00 FRI 02:09 PM PARAGON ANALYTICS P^Al FAX NO. 970 490 1349 P. 57


Sample Results

Lab Name Paragon Analytics, Inc.



CllontProjoct ID: Gasbuggy

Field ID: C50PS070608

Lob ID: 00(19177-39



Date Collected: 15-Sop-00 Date Extracted: 21-Sep-OO DaU Analyzed: 25-Sep-00

Prop Batch: EXO00921-3 QCBatchID: EX000921-3-1


Basis: As Received


File Name: P9822

CASNO Target Analyte Di lut ion Result Report ing MDL Result EPA Factor L imi t Qual i f ier Qual i f ier

110-8G-1 PYRIDINE 1 0.1 0.1 0.023 0 106-46-7 1,4-DlCMLOROBENZENE

„ . . . . . . . . . . _ J . . - . _ . _ « . 1 0.1 0.1 0.011 U

95-4 B-7 Z-MGTIIYLPIIENOL" 1 0.1 0.1 0.018 U

! 108-39-4 aiVMbrHYLPHENOL i 0.1 0.1 _ . . 0.013 U

67-72-1 HEXACHLOROETHANE - - ~ - 0 1 - 0.015 U

50-95-3 NITROBENZENE ' ' i 6.1" 0.1 0.011 u 87-68-3 1 ILXACt ILOROBUTADIENE 1 0.1 0.1 0.014 u 88-06-2 2,4,VTriiCHt^lROpi UtNOL i" 0.1 ai" 0.011 u

'; 95-95-4 2,4,5-TRlCHLOROPHENOL 1' 0.5 0.5 0,014 u ! 121-14-2 2,4-DINITROTOLUENE 1 0.1 0.1 0.012 u J 118-74-1 HEXAOILOROBENZENE 1 0.1 0.1 0.012 u Tsr'-SS-S "pCN'rACHLORoVlTeNOL 0.5 0,5 0.031 u

Surrogate Recovery


Percent Recovery

C o n t r o l

L i m i t s

11 fl-79-S

321-60-8

367-12-4

4165-60-0

4165-62-2

1718-51-0

2.4,6-TR.IBROMOPHF-NOL

2-FIUOROOIPHE:NYL

2-FLUOROPHENOL

NITROBENZENE-OS

PHENOL-PS

TERPIIENYL-D14

0.411

0.289

6,44a

0,312

0.465

0.368

0.75

0.5

55

58-

23-100

21 -106

11 fl-79-S

321-60-8

367-12-4

4165-60-0

4165-62-2

1718-51-0

2.4,6-TR.IBROMOPHF-NOL

2-FIUOROOIPHE:NYL

2-FLUOROPHENOL

NITROBENZENE-OS

PHENOL-PS

TERPIIENYL-D14

0.411

0.289

6,44a

0,312

0.465

0.368

0,75

0.5

0.75

L . . >

60

62

62

. . . ._. ? 4 . ._.

21-100

34 -111

15 -104

^ 33 -111


Date Printed: Thursday, September 28,2000 Paragon Analyt ics Inc. Page 8 of 14 LIMS V ^ i u r t 1.BQ8

SEP-29-00 FRI 02:09 PH PARAGON ANALYTICS FAX NO. 970 490 1349 GON ANALYTICS FAX NO.


Sample Results

P. 58

t ab Name: Paragon Analytics. Inc.




Bold ID: GBPS1002C4

'Lab ID: '0009127.37


Sample Matrix: LEACHATE % Moisturo: N/A

Date Collected: 16-Sep-00 Date Extracted: 21-Sep-OO Oate Analyzed: 25-Sep-OO

Prop Batch:EX000921-3 QCBatchID: EX000921-3-1

RunlD:SV000925-2 Cleanup: NONE

Basis: As Received

Sample Aliquot; 100 ML Final Volume: 1 ML Result Units: MG/L

File Name: P9823

[ CASNO Target Analyte Dilution Factor



EPA Quali f ier

110-66-1 PYRIDINE

10G--4G-7 1,4-DICHLOROBENZENE

96-13-7 2-METI IYLPI IENOL

105-39-4 3+I1-METHYLPHENOL

57-72-1 HEXACHLOROETHANE

90-95-3 NITROBENZENE

87-68-3 1 lEXACHLOROBUTADIENE

88-06-2 2,4.6-TKICI ILOROPI IENOL

95-95-4 2,4.5-1 liiCHLOROPl IliNOL

121-14-2 2,4-DIN|TRQT0LUIAN£

118-74-1 1IEXACIILOROBENZENE

87-86^5 PENTACHLOROPHCNOL

0.1

0.1

0,1

0.1

0.1

0.1

0.1

0.1

0.5

J3.1

0.1

0.5

Surrogate Recovery

0.1

0J ai 0.1

0.1

0.1

0.1

0.1

0.5

0.1

0.1

0.5

0.023

0 011

0.018

0.013

0.015

0.011

0.014

0.011

0.014

0.012

0.012

0.031 U

U

U

U

U

U

U

U

U

U

U

U


Percent Recovery

Control Limits

118-79-6 2,4,6-TRIBROMOPHENOL 0.426 j 0.75 57 23 -100

321-60-8 2-FLUOR06IPHENYL 0.29 0.5 58 21-106 .

367-12-4 2-FLUOROPHENOL 0.461 0.75 62 21 -100

4165-60-0 NUROBENJlF.NE-Ds 0.311 0.5 62 34-11?

4105-62-2 PHL-NOL-DS 0.474 0.75 63 15-104

1718-51-0 TCRP1IENYL-D14 0.557 0.5 71 33-111

Dafa Package ID; SV0009127-2

Dale Printed:Thursday, September 28, 2000 Paragon Analytics Inc. LIMS Vision, vbye

Page 9 of 14

SEP-29-00 FRI 02:09 PH PARAGON ANALYTICS FAX NO. 970 490 1349 ^AGON ANALYTICS FAX NO. ^


Sample Results

P. 59


Work Order Number; 0009127



Field ID: GBPSI10204

Lab ID: 0003127-38

LEACH DATE: 9/20/200O


Date Collected: 1G-Sep-0O Date Extracted: 21-Sep-00 Date Analyzed; 25-Sep-00

Prep Batch: EX000921-3 QCBatchID: EX0O0921-3-1


Basis: As Received


File Name; P9B24

CASNO T a r g e t A n a l y t e Dilution Factor

R e s u l t Reporting Limit

MDL Result Qualifior

EPA Qualifier

110-85-1 PYRIDINE 1 0.1 0.1 0.023 U

106-46-7 M-olcHLORo'oENZeNE 1 0.1 0.1 0 011 U 1

95-48-7 2-METHYLPHEKOl 1 0.1 0.1 0.018 U

i 103-39-4 3i4-Mr.rrlYLPHGNOL i 0.1 0.1 0.013 U 1

! 67-72-1 HEXACHLOROETHAN5 1 0.1 0.1 0.015 U

j 90-95-3 NITROBENZENE 1 O.'l 0.1 0.011 u

j 87-60-3 1 (EXACIILOROBUTADIENE 1 0.1 0.1 0.014 u

j 88-06-2

I 95-95-4 [ . , „ . . _

2,4,8-TRlCHLOROPI IENOL i 0.1 0.1 0.011 U •[ j 88-06-2

I 95-95-4 [ . , „ . . _

2.4.5-1 RICHLOROP1IENOL 1 0.5 0.5 0.014 L l "

! 121-14-2 2,4 nTNITRoToIuENE' . ... 0.1 0.1 0.012 U •

118-74-1 HEXACHLOROBENZENE 1 0.1 0.1 0.012

f 07-66-5 PENTACHLOROPHENOL 1 0.5' 0.5 0,031 u

Surrogate Recovery


Amount

Percent

Recovery

Control

Limits

118-79-6 2,4,6-TRIBROMOPHENOL 0.414 0.75 55 23-100

321-60-8 2-FLUOROBlPHENYL 0.277 0.5 55 21 - 1 0 6

3C/-12-4 ZFLUOROPHENOL 0.43 0.75 57 21 - 100

4165-CO-O NIVROriFN?e.NC:-DS 0.305 0 5 61 34 - 111

41(55-62-2 PHCN0L-D5 0.4S2 .. 0.75 60 1 5 - 1 0 4

1718-51-0 TERPIICNYL-D14 0.39

• 0.5 78 | 3 3 - 1 1 1

DaUi Package ID: SV0009127-2

Date Printed: Thursday. September 28. 2000 Paragon Analytics Inc. LIMS Vision. 1.095

Page 10 of 14



Sample Results

Lob Name: Paragon Analytics, Inc.


Clicnit Name: IT Corporation Las Vegas

CliontProjoct ID: Gasbuggy

PiOldID; GBPS120204

Lab ID: 0009127-39



Date Collected: 16 -Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 25-Sep-00

Prep Batch: EX000921-3 QCBatchID: EXO00921-3-1


Basis: As Received


File Name: P9825




EPA Qualifier

110-86-1 PYRIDINE 1 0.1 0.1 0.023 U

106-46-7 1,4-0ICIILORODrN2ENC 0.1 0.1 0.011 U I \

95-48-7 2 METHYLF~HgNOL 0,1 0.1 j 0,018 U I 108-39-4 3 r4-METHYl PHENOL " 0,1 ai'' 0.013 U j

67-72-1 HEXACHLOR0ETI-IANE i 0.1 0.1 0.015 U i

98-95-3 I

NITROBENZENE .. .. 0 1 0,1 0,011

u '< 87-68-3 HEXACHLo'ROEru'rADlENl; 1 0.1 0.1 0.014 u 88-06-2 2,4,6-TRICHLOROPHENOL 1 0.1 0.1 0.011 I u

(J5-95-4 2,4,5-TRICHLOROPH ENOL " ' " 1 0.5| 0.5 0.014 u -•

121-14-2 2.4-DINlTROrOLU£NE " " ' " V 0.1 0.1 0.012 u

118-74-1 Hr-XACHLOROOeNEENG V ai 0.1 0.012 u 87-86-5 PENTACHLOROPHENOL 1 0,5 0.5 0.031 u

Surrogate Recovery


Percent Recovery

Control Limits

118-79-6 2,4,G-TRiBROMOPHENOL 0,429 0.75 57 23-100 ^

321-60-6 Z FLUORODIPHCNYL 0.294 0.5 59 21 -106

367-12-4

4165-60-0

2-FLUOROPHENOL 6.46 0.75 61 21-100 367-12-4

4165-60-0 NITROBENZENE-D5 0~32 0.5~ 64 34-111

4165-62-2 PHFN0L-D5 0.477 0.75 64 15-104

1713-51-0 TERPHENYL-D14 0.368 0.5 74 33-111


Date Printed: Thursday, September 28, 2000 Paragon Analytics Inc. LIMS Vi-rwon-

Page 11 of 14

SEP-29-00 FRI 02:09 PM PARAGON ANALYTICS 'A^( FAX NO. 970 490 1349 P. 55

GC/MS Semivolatiles Method SW8270--TCLP Leachate

Sample Results

Lnb Namo: Paragon Analytics, Inc.



ClientProject IO: Gasbuggy

F-icId |D: .OBPS170204

t.itb ID: ' 0003127-25



Date Collected: 17-Sop-00 Date Extracted: 21-Sep-00 Date Analyzed: 25-Sep-00

Prep Batch: EX000921-3 QCBatchID: EX00O921-3-1

Run ID: SVQ00924-2 Cleanup: NONE

Basis: As Received


File Name: P9801

CASNO T a r g e t A n a l y t e Dilution Factor



EPA Qualifier

110-86-1 PYRIDINE i 0.1 0.1 0.023 U

10G-4G-7 1,4-DICHLOROBENZENE 1 0.1 0.1 0,011 U

95-48-7 2-MnTHYLPHCNOL 1 0.1 0.1 0,018 u 108-30-4 3i4MF.THYLPHENOL 0.1 0.1 0.013 U

67-72-1 HEXACHLOROETHANE 0.1 0.1 0.015 U

98-95-3 NITROBENZENE 1 0.1 0.1 0.011 U 1 87-C8-3 HEXACHLOROBUTADIENE 0.1 0.014 U

t

88-00-2

i 95-05-4

2,4,6-TRICHLOROPHENOL i ' 0.1 0.1 0.011 U 88-00-2

i 95-05-4 2,4,6-TRICHI,OROPHCNOL 0.5 0.5 0.014 U

| 121-14-2 2,4-DINITROTOLUENE 0-1 0.1 0.012 U

j 118-74-1 IIEXACHLOROBENZENE 0.1 0.1 0.012 U

I 87-86-5 PENTACIILOROPIIENOL " 0.5 0.5 0.031 ~u

Surrogate Recovery


Percent Recovery

Control Limits

1161-79-6 2,4,6-TRIBROMOPI IENOL 0.462

• 0.75 02 23 -100

321-60-8 2-FLUOROBIPHENYL 0.288 0.5 58 21 - 106

367-12-4 2-FLUOROPHENOL 0.45 0.75 - - - - -

60 21 - 1 0 0

4165-60-0 N1TROBEN7.ENE-D5 0,323 65 ' " 3 4 - 1 1 1

416562-2 PHENOL-OS 0.476 "b.75" 63' 15-104

1718-51-0 TERPIICNYL-OU 0.38 0.5 76 33-111

Data Package- ID; SV0009127-2

Date Printed; Thursday, September 26, 2000 Paragon Analytics Inc. L!MSV>!ii,lon. 1 096

Page 6 of 14

SEP-29-00 FRI 02:08 PM PARAGON ANALYTICS FAX NO. 3J0 490 1349 P. 54


Sample Results





Held ID: <30PS1B0911

Lab ID. 0OCW127-2V



Dato Collected: 17-Sep-OO Date Extracted: 21-Sep-OO Dato Analyzed: 24-Sep-00


Run ID: SV000924-2 Cleanup; NONE

Basis: As Received


File Namo: P9800


Resul t Reporting Limit


EPA Qualif ier

, 110-E6-1 PYRIDINE 1 0.1 0.1 0.023 U

, 105-46-7 1,4 DICHLOROBENZENE 1 0.1 0.1 0.011 u \ 95-48-7 2-METl IYLPI IENOL 1 " 0.1' 0.018 u ...j 108-39-4 " sT^M^THYLplHENOi. " " _

1 0.1 0.1 0.013 u

07-72-1 HEXACIILOROETIIANE 1 0.1 0.1 0.015 u 90-DS-3 ' NiTRoheN/cNrs " " " ' 0 1 0.1 0.011 u B7-SB-3 HEXACHLOROBUTADIENE 1 0.1 0.1 0.014 u 88' 06-2 2,<l,6 TRICHLOROPHENOL 1 0.1 0.1 0.011 u 05-95.-4 2,4,5-TRICHLOROPHENOL 0.5 0.5 0.014 u 121-14-2 2,4-DINITROTOLUENE 1 0.1 0.1 0.012 u 118-7-1-1 HEXACHLOROBENZENE 1 0.1 0.1 0.012 u 87-80-5 PCNrACHloROPT-iCNOL 1 0.5 0.5 0.031 _ . . _

Surrogate Recovery


Percent Recovery

Control Limits

118-79-6 2.4.0-TRIBROMOPHENOL 0.472 0.75 63 23-100

321-60-8 2-FLUOROSIPHENYL 0.307 0.5 61 21 - 106

3G7-12-4 2-FLUOROPHENOL 0.452 0.75 60 21-100

' 4165-60-0 NITROBENZENE-D3 0.338 0.5 68 34-111

i 41C5-62-2 PHENOl-DS ' "0,492 ~ 0,75 15-104

1718-51-0 TERPHENYL-D14 0.41 0.5 | 82 33-111 1


Date Printed: Thursday, September 28,2000 Pa ragon Analy t ics Inc. Page 5 of 14 LIMSVi i i iun 1.656

SEP-29-00 FRI 02:10 PH PARAGON ANALYTICS FAX NO. 970 490 1349 P. 61


Sample Results

Lob Namo: Paragon Analytics, Inc.

Work Order Numbor: O0O9127


ClientProject ID; Gasbuggy

F i«".d ID: GBPS2102CM

Lab ID: 0003127-40 '



Date Collected: 19 Sep-00 Date Extracted: 21-Sep-00 Date Analyzed: 25-Sep-00

Prep Batch: EXOQ0921-3 QCBatchID: EX000921-3-1

Run ID; SVO0O925-2 Cleanup: NONE

Basis: As Received

Sample Aliquot: 10OML Final Volume: 1 ML Result Units: MG/L

File Name: P9626

I CASNO Target Analyte Dilution Result Reporting MDL Result EPA

I Factor Limit Qualifier Qualifier

! 110-86-1 PYRIDINE 1 0,1 0.1 0.023 U

106-46-7 1.4-DlCHLOROBEN2£Ne r 0.1 0.1 0.011 U . _. j I 95 43-7 2-ME7IIYLPHENOL 1 6.1 0.1 0,018 U

1108-39 4 j 3 M METHYLPHENOL i 0.1 0.1 0.013 U " • 67-72-1 1 lEXACHLOROF.THANE 1 0.1! ' " " " 0.1 0.015 U

— , - „ . . . . _ .. . . i i 98-95-3 NH ROBENZENE 0.1 o!on U

i B7-60-3 HEXACHLORORUTADKNE 1 0.1 0.1 0.014 U j 88-06-2 2,4.6-TRlCHLOROPHENbL 1 0.1 0.1 0.011 U 1 95-95-4 2,4,5-TRICHLOROPHENOL " 1 0.5 0.5 0.014 U 1

j 121-14-2 2.4-blw"mOTOLUENE 1 0.1 o.i 0.012 u "1 i 118-74-1 HI'XACl ILOROBENZENE 1 0.1 0.1 0.012 U i ' 87-86-5 PEN! ACHLOROPI IENOL 1 0.5 0.5 0.031 u

Surrogate Recovery


118-79-6 2.4.6-7 RIBROMOPHENOL 0.414 0.76 55 23-100

321-<50-8 2-FLUOROBIPHENYL 0.298 0.5 " "'"io"""' 21 - 106

367-12-4 2-FLUOROPHF.NOL " " ' 0.459 0.75 61 21 - 100

4165-60-0 NITROBEN^LNC-05 0.318 0.5 64 34 -111

4165-62-2 PHENOL-DS 0.48 0.75 64 15-104

1718-51-0 TERPHENYL-D14 0.346 0.5 69 33-111


Date Printed.: Thursday, September 26, 2000 Paragon Analytics Inc. UMSVu.v.on: 1.8<K5

Page 13 of 14

Diesel Range Organics

Method SW8015M

SER-29-00 FRI 08:47 AM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 02

Diesel Range Organics Method SW801SM

Sample Results





F(okl ID: G0PS010SQ9

Lab ID'. 0000127-2

Sample Matrix: SOIL % Moisture: 14.9

Date Collected: 14-Sep-00 Date Extracted: 21-Scp-00 Date Analyzed: 2B Sep-00


Run ID: HCD000927-1 Cleanup: NONE

Basis; Dry Weight

Sample Aliquot: 20 G Final Volume: 5 ML Result Units: MG/KG

File Name: D0927S13




EPA Qualifier

. 60334-30-5 Diesel Range Organics 2 2100 . . . . " 1.2 i

Surrogate Recovery

CASNO Surrogate Analyte Result | Flag Spike

Amount

Percent Recovery

Control

Limits

630-01-3 N-IIEXACOSANE .116 i . : 7.34 , . . . 1 7 1

54 - 146

The chromatogram indicates the presence of hydrocarbons In ilia range of C8-C32.

Pata Package ID: HCD0009127-1

Dato Printed: Thursday, September 28, 2000 Paragon Analytics Inc. LIMS V:.'5iOi\ 1.6H6

Page 5 of 14

SEP-29-00 FRI 08:47 AH PARAGON ANALYTICS FAX NO. 970 490 1349 P. 03

Diesel Range Organics Method SW8015M

Sample Results


Woik Order Number: 000912*/


ClientProject ID: Gasbugoy

FWsltUD-. GBPS010011

Lab ID: ,0(109127-3

Sample Matrix: SOIL % Moisture: 15,5

Date Collected: 14-Sep 00 Date Extracted: 21-Sep-00 Date Analyzed: 24-Sep-OO

Prep Batch: EX0O0921-2 QCBatchID: EX000921-2-1


Basis: Dry Weight


File Name: D0922S56

CASNO Target Analy te Dilution Factor



EPA Qualifier

• 60334-30-S I Diesel Rang'; Organics 1 270' 5.9 1

0.61

Surrogate Recovery


Percent Recovery

Control Limits

630.01-3 N-HEXACOSANG 10.2 7.4 137 _

54 - 146

Tho dtromatogram indicates the presence of hydrocarbons in Vie rango of C10-C22.

Dala Package ID: HCD0009127-1

Data Printed; Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS Vccjiorv 1 69S

Page 7 of 11

SEP-29-00 FRI 08:47 AH PARAGON ANALYTICS A^G FAX NO. 970 490 1349 P. 04


Sample Results


Work Order Numbor: 0009127

Client Name: IT Corporation Lao Vegas


Field ID: 6RPS020010

Lab ID' 0009127-7

Sample Matrix: SOU. % Moisture: 12.8

Date Collected: 14-Sep-00 Dato Extracted: 21-Sop-00 Date Analyzed: 27-Sep-OO

Prep Batch:EX000921-2 QCBatchID: EX000921-2-1

Run |D:MCD000927.1 Cleanup: NONE

Basis: Dry Weight

Sample Aliquot: 20 G Final Volume; 5 ML Result Units: MG/KG

File Name: D0927S11

CASNO

• Target Analyte

Dilution Factor



EPA Qualif ier

' 6S334-30-5 Diesel Range C^amca i 300;, 5 7 0.59

• Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Percent Control Surrogate Analyte Amount Recovery Limits

630-01-3 N-1 IEXACOSANE 8.62 - .

7.17 120 54-146 . . .

The chromatogram indicates the presence of hydrocarbons in the range of C8-C3S.

Data Package ID: HCD0009127-1

Dale Printed: Thursday, September 26, 20Q0 Paragon Analytics Inc. LIMS Vision. 1 D!X3

Page 13 of 14



Sample Results





FVlUl IO: CBPS;03040e

Lab ID: 0OQ9 i?7-£)


Date Collected: 15-Scp-00 Date Extracted: 21-Sep-OO Date Analyzed: 27-Sep-OO



Basis: Diy Weight

Sample Aliquot: 20 G Final Volume: S ML Result Units: MG/KG

File Namo: D0927S12

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Target Analyte Factor Limit Qualifier Qualifier

J 68334-30-5 Dieaal Ranga Organics 1 720 • 5.8 0.6 . . . . I Surrogate Recovery


Percent Recovery

Control Limits

630- 01-3 N-HEXACOSANC 14 j - 7.21 ! 194 54 -146

The chromatogiam indicates the presence of hydrocarbons in the range of C8-C36.


Date Printed:Thursday, September 28. 2000 Paragon Analytics Inc. UMSVCtiiOl 1WG

Page 14 of 14

SEPr29-00 FRI 08:47 AM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 06 3A^l

Diesel Range Organics Method SW8015M Sample Results



Client Name.* IT Corporation Las Vegas


Field ID: GRPS04040G

Lab ID; ' 0000127-10

Sample Matrix: SOIL % Moisture: 12

Date Collected: 15-Sep-00 Dato Extracted: 21-Sep-OO Date Analyzed: 24-Sep-00


Run ID:HCD000922-1 Cleanup: NONE

Basis: Dry Weight


File Name: D0922S59




EPA Qualifier

68334-30-5 j Diesel Range Oigunics 1 6,7 6,7 • 0.59 | U

Surrogate Recovery


Amount

Percent

Recovery

Control

Limits

630-01-3 N-1 lEXACOSANE 6.79 7.1 124 54 - 146

Data Package ID: HCD0Q09127-1

Date Printed: Wednesday, September 27. 2000 Paragon Analytics Inc. UMSV.rn.ion. 1806

Page 1 of 11

SEP-29-00 FRI 08:47 AM PARAGON ANALYTICS A^G FAX NO. 970 490 1349 P. 07




Client Name: IT Coiporation Las Vegas


Field ID: GBPS050400

LdbID- 0009127-11


Dato Collected: 15-Sep-OO Date Extracted: 21-Sep <00 Dato Analyzed: 24-Sep-00



Basis: Dry Weight


File Name: D0922S60


68334-30-5 Dlcaol Rouge Organics 1 58 5.8 0.59 U

Surrogate Recovery


Percent

Recovery

Control

Limits

630-01-3 NI-IEXACOSANE 9.08 . ...

7.19 126 54 - 146


Dote Printed; Wednesday, September 27,2000 Paragon Analytics Inc. LIMS Vvr.icn 1 SW

page 2 of 11







.Field ID: •GBPS060608

> Lab ID: Qfi09 (27-27


Date Collected: 15-Sep-00 Date Extracted: 21-Sep-OO Date Analyzod: 25-Sep-OO



Basis: Dry Weight


File Name: D0922S65

CASNO Target Analy te Di lut ion Result Reporting MDL Result EPA Factor Limit Qualifier Qualif ier

: 68334-30-5 Diusel Range Organics 1 . a.2 5.2 0.54

Surrogate Recovery


Percent Recovery

Control Limits

630-01-3 N HtXACOSANE 7.86 6.53 120 54 - 146

The chromatogram Indicates the presence of hydrocarbons in the range of C10-C32.


Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMSVun'On- 1 SflCi

Page 5 of 11

SEP-29-00 FRI 08:48 AN PARAGON ANALYTICS A^G FAX NO. 970 490 1349 P. 11


Lab Name, parayon Analytics, Inc.




FioldlD: CBPJ;070G03

Lab ID: 'boO!)1?7-?B


Date Collected: 15-Sep-00 Date Extracted: 21-Sep-00 Dato Analyzed: 25'Sep-00

Prop Batch: EX000921-2 QCBatchID: EX000921-2-1


Basis: Dry Weight


File Name: D0922S05

j CASNO Target Analyte Dilution Factor



EPA Qualifier

• 63334-30-5 3.7 5.7 0.58 i . . . .

J I

Surrogate Recovery


Percent Recovery

Control Limits

630-Ol-3 N Hf-.XACOSANE 9 7.07 127 54 - 146


Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS Vision- 1.UDC

Page 6 of 11

SEP--29-00 FRI 08:48 All PAEAGON ANALYTICS A G FAX NO. 490 1349 P. 12





ClientProject ID; Gasbuggy

Field ID: GGPS100204

Lab ID: 0009127-30


Date Collected: 16-Sep-00 •ate Extracted: 21-Sep-OO Dato Analyzed: 25-Sep-00



Basis: Dry Weight


File Name: D0922S67



MDL Result Qualif ier

EPA Qualifier

j 08334-30-5 I Diesel Range Organics i 5.S 5.6 | 0.58 j U . . . . . . . . .

Surrogate Recovery


Percent Recovery

Control Limits

630-01-3 NIILXACOSANE 6.98 6.96 129 54-146

Data Package ID: HCD0009127~1

Date Printed: Wednesday, September 27.2000 Paragon Analytics Inc. UMSVorsioir. 11>')6

Page 8 of 11

SEP-29-00 FRI 08:48 AM PARAGON ANALYTICS A^G FAX NO. 970 490 1349 P. 13




Client Name: IT Corporation Las Vogas


Fit-Id ID- GBPSl 10204

Lab ID' 0009127-31


Date collected: 16-Scp-00 Date Extractod: 21 -Sep-00 Date Analyzed: 25-Sep-00



Basis: Dry Weight


File Name: D0922S69




EPA Qualif ier

• C8334-30-5 j DiesBl Ranoe Organics ' -• • - 1 0.7 S.5 0.56 J

Surrogate Recovery


630 01-3 NHCXACOSANE 8.03 6.82 127 54 - 146

Data Package ID; HCD0009127-1

Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS Vrnworv 1

Page 9 of 11

SEP-29-00 FRI 08:48 All PARAGON ANALYTICS A^G FAX NO. 970 490 1349 P. 14



Woi'K Ordor Number: 0009127



Picld ID: GBPS120204

Lab ID: 0009127-32


Date Collected: 16-Sep-00 Date Extracted: 21-Sep-00 Date Analyzed: 25-Scp-00


Run ID:HCD000922-1 Cleanup: NONE

Basis: Dry Weight


File Name: D0922S70




EPA Qualifier

68334 30-5 Dlosct Ranyo Organics - i I 1 5.5 0.57 J

Surrogate Recovery


630-01-3 N HEXACOSANE a.72 6.94 126 54-146

Data Package ID; HCD0009127-1

Date Printed: Wednesday, September 27, 2000 Paragon Analy t ics Inc. P a 9 e 10 of I.IMS VI.T.JOII 1.806

SEP-29-00 FRI 08:47 AM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 09


Sample Results




ClicnlProjoct ID: Gasbuggy

FUildID: CBPS1 70204

Lab ID: 0000127-18

Sample Matrix: SOIL % Moisture: S.I

Date Collected: 17-Sep-00 Date Extracted: 21-Sep-OO Dato Analyzed: 25-Sep-OO



Basis: Dry Weight


File Name: D0922S64


; 6&334-30-5 Diesel Range Organics 1 5.3 5.3 0.54 U

Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Percent Control Amoun t Recovery Limits

630-01-3 N-HFJCACOSANE 8.34 6.59 127 54 -146


Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMSWiion 1,0%

Page 4 of 11

SEP-29-00 FRI 08:47 AM PARAGON ANALYTICS A G FAX NO. 970 490 1349 P. 08





CliontProJoct ID: Gasbuggy

I".old ID: GCPKiangii

Lab ID; 0000127-17


Date Collected: 17-Sep-00 Date Extracted: 21-Sep-OO Date Analyzed: 24-Sep-00



Basis: Dry Weight


File Name: D0922S63

CASNO Target Analyte Dilution | Result Factor I

Report ing Limit


EPA Qualifier

68334-30-5 .Dices! Range Organics 1 [ 10;' 6.8 0.7

Surrogate Recovery


Percent Recovery

Control Limits

630-01-3 NHEXACOSANE 10.2 8.46 121 54 - 146

The chromatogram indicates the presence of hydrocarbons in the range of C10-C32.

Data Package ID: HCDO009127-1

Date Printed: Wednesday, Soptombcr 27. 2000 Paragon Analytics Inc. UMS VvrJion 1 l-TA

Page 3 of 11

SEP-29-00 FRI 08:48 AM PARAGON ANALYTICS FAX NO. 970 490 1349 P. 15



Wark Order Number: 0009127

Client Nfirne: IT Corporation Las Vegas

ClienlProJect ID: Gasbuggy

Field ID: G0PS2I0204

' Lab ID: 000912/-34


Date Collected: 19-SepOO Date Extracted: 21-Sep-OO Date Analyzed: 25-Sep-00



Basis; Dry Weight


File Name: D0922S71

j^CASNO Target Analyte Dilution Factor



EPA Qualifier

I G8334-30-5 Diesel Range Organics 1 5.5 5.5 0.57 U

Surrogate Recovery


630-01-3 NHEXACOSANE 8,57 ...

6.85 125 i

54 -146


Date Printed: Wednesday, September 27, 2000 Pa ragon Ana ly t ics Inc. P a 3 e 1 1 o M 1

LIMS Vision- 1 8'jr.

Gasoline Range Organics

Method SW8015


Gasoline Range Organics Method SW8015

Sample Results


WorK Order Number: 0009127



Field ID: G0PS01OCO9

Lab ID: 0000127-2


Date Collected: 14-Sep-OO Dato Extracted: 21 -Sep-00 Date Analyzed: 21-Sep-00

Prep Batch; HCG000921 -1 QCBatchID: HCG000921-1-1

Run ID:HCG000921-1G Cleanup: NONE

Basis: Dry Weight

Sample Aliquot; SG Final Volume: 5G Result Units: MG/KG

File Name; G0921S09

CASNO Targot Analyte Dilution Factor

Rosult Reporting Limit

MDL Rasult Qualifier

EPA Qualifier

9006-61-9 GASOLINE - ? — - _. . 6 • .7 3.1 2.9 0.12 ..

._ I Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,4-TRlFLUOROTOLUCNf: 0.566 0.588 96 69-119

Data Package ID; HCG0009127-1

Date Printed: Tuesday, September 26,2000 Pa ragon Analy t ics Inc. P a 9 e 4 o f 9

LIMS Version: 1 C'«

SEP-28-00 THU 04:33 PM PARDON ANALYTICS FAX NO. 9711 490 1349 P. 36

Gasoline Range Organics Method SW8015 Sample Results

L ab Name: Paragon Analytics, Inc.


Client Name: I f Coiporation Las Vegas


Field ID: GHPS010Q11

Lab ID; 0000127-3


Date Collected: 14-Sep-OO Dato Extracted: 22-Sep-OO Date Analyzed: 22-Sep-00

Prep Batch: HCG000922-1 QCBatchID; HCG000922-1-1

Run ID:HCG000922-1G Claanup: NONE

Basis: Dry Weight

Sample Aliquot: 5G Final Volume: 5G Result Units; MG/KG

File Name: G0922S10


8005-61-0: " GASOUNE 1 ; 1.6" 0.59 0.024 j

Surrogate Recovery


Amount

Percont

Recovery

Control Limits

13-10-5 2,3.4-1 RlFLUOROTOLUENE 0.114 0.11a 96 69-119

Data Package ID: HCG0009127-2

Dale Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS vun.on • 0'W

Page 3 of 5

SEP-28-00 THU 04:33 PN PARAGON ANALYTICS FAX NO. 91a 490 1349 P. 37




Client Namo: IT Corporation l.ss Vegas


Field ID: <~,iir'.so20bio

l .db |D: 0000127-7


Dale Collected: 14-Sep-00 Date Extracted: 22-Sep-OO Date Analyzed; 22-Sep-OO

Prop Batch: HCG000922-1 QCBatchID: HCG000922-1-1


Basis: Dry Weight

Sample Aliquot; SG Final Volume: 5G Result Units; MG/KG

File Name: G0922S06

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Target Analyte Factor Limit Qual i f ier Qualifier

I 8006-131-9 ' GASOLINE : 1 0,p41 0.57 0.023 J

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 JArt-TRIFLUOROTOLUENE 0.0907 0.115 79 | 69-119

Data Package JD: HCG0009127-2

Dale Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LlMi vwsiorv 1 COO

Page 5 of 5

SEP-28-00 THU 04:33 PM PARAGON ANALYTICS FAX NO. 92D 490 1349 9^ P. 38






Field ID: GBPStwoioe

U h ID: ' 0009127-0



Prep Batch: HCG000921-1 QCBatchID: HCG000921-1-1

RunlD:HCG00092l-1G Cleanup: NONE

Basis: Dry Woight

Sample Aliquot: 5 G Final Volume: 5G Result Units: MG/KG

File Namo: G0921S07

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Target Analyte Factor Limit Qualifier Qualifier

5006-61-9 GASOLINE i 0.53 0.5a 0.023 U

Surrogate Recovery

CASNO Surrogate Analyte Result Flag Spike Percent Control Surrogate Analyte Amount Recovery Limits

13-10-5

. . 2,3,1-TRIFLUOROTOLUENE 0.102 [ _ 0.115

.. . . 8 8 . . _ . 6 9 - 1 1 9


D;*te Printed: Tuesday, September 26, 2000 Paragon Analytics Inc. LIMS Vunon: 1,60(1

Page S of 8

SEP-28-00 THU 04:33 Ptl PARAGON ANALYTICS FAX NO. 910 490 1349 9^ P. 39

Gasoline Range Organics Method SW8015

Sample Results





Field ID: GRPS0404QB

LSblp: 0000127-10

Sample Matrix: SOIL % Moisture: 12




Basis: Dry Weight

Sample Aliquot: 5G Final Volume: 5 G Result Units: MG/KG

File Name: G0921S08




EPA Quali f ier

8003-61-9 CASOLINE j 1 0.57 0.57 0.023 . 4_ J Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 .

2,3,i1-TRlFLU0ROrOLL)F.NE 0.0969 0.114 85 69-119

Dafa Package ID: HCG0009127-1

Date Printed: Tuesday, September 26, 2000 Paragon Analytics Inc. UMBVcraon 1090

Page 1 of 8

SEP-28-00 THU 04:33 PM PARAGON ANALYTICS FAX NO. 910 490 1349 9^ P. 40


Lab Name: Paragon Analytics. Inc.


Cliuiit Namo: IT Corporation Las Vegas


pibldlD; GBPS050400

, Lab ID: 000912M1

Sample Matrix: SOIL % Moisture; 13.1

Dato Collected: 15-3ep-0Q Date Extracted: 22-Sep-OO Dato Analyzed: 22-Sep-OO

Prop Batch: HCG000922-1 QCBatchID: HCG000922-1-1

Run ID;I1CG000922-1G Cleanup: NONE

Basis: Dry Weight

Sample Aliquot: 5G Final Volume: 5G Result Units: MG/KG

File Name: G0922S07




EPA Qualifier

3006-61-9 GASOUNG . . .

1 0.56 0.58 0.023 U

Surrogate Recovery


Percent Recovory

Control Limits

13-10-5 2.3,<1-TRlFLUOROrOLUIi:NI-: 0.102 0.115 89 69-119


Dato Printed: Wednesday, September 27,2000 Paragon Analytics Inc. LIMS Voi 1 K'Jti

Page 1 of 5

SEP-28-00 THU 04:34 PM PARDON ANALYTICS FAX NO. 9^ 490 1349 P. 43


|,ab Name: Paragon Analytics, Inc.


Ciient Name; IT Corporation Las Vegas


Field ID: COPSneosos

f.abID; 0000127-27


Date Collected; 15-Scp-OO Date Extracted: 22-Sep-OO Date Analyzed: 22-Sep-OO

Prep Batch: HCG000922-1 QCBatchID: HCG000922-1 -1

Run ID:HCG000922-1G Cleanup; NONE

Basis: Dry Weight


File Namo: G0922S14

CASNO Target Analyte Dilution Result Reporting MDL Result EPA Target Analyte Factor

" * Limit Qualifier Qualifier

8006-51 -9 GASOLINE 1 0.52 0.62 0.021 L. U .

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 I 2,3,4-TRIFLUOROTOLUENG 0.0844 I 0.104 I 81 69-119


Date printud: Wednesday, Snptomber 27, 2000 Paragon Analytics Inc. LIMS wr.'f>n 11>%

Page 2 of 5







Fmld ID: CBPS070600

Lab ID: .000912^-26

Sample Matrix: SOIL % Moisture; 11.6



Run 1D;HCG000925-1G Cloanup:NONE

Basis: Dry Weight

Sample Aliquot: SG Final Volume: 5G Result Units: MG/KG

File Name: B0925S05

I CASNO Target Analyto Dilution Result Reporting MDL Result EPA Factor Limit Qualifier Qualifier

: 8006-61-9 GASOLINE 1 0.57 0.57 0.023 u

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2.3,<1-TRIFLUOR0"[0lUENI= 0.0906 0.113 80 69-119


Date Printed: Wednesday, September 27, 2000 Paragon Analy t ics Inc. P a s e 1 of 1 LIMS Version: 1 DOR

SEP-28-00 THU 04:34 PM PAMON ANALYTICS FAX NO. 92a 490 1349 P. 45




Client Name: IT Corporation LasVegas


Field ID: .(SBPS100204

LabJD; 0O09127-3O


Date Collected: 16-Sep-0o Date Extracted: 21-Sep-OO Date Analyzod: 21-Sep-00

Prep Batch: HCG000921-1 QCBatchID: HCG000921 -1 -1


Basis: Dry Weight


File Namo: G0921S16




EPA Qualifier

800S-G1-9 | GASOLINE 1 0.56 0.56 0.023 u

i

Surrogate Recovery


Amount

Percent

Recovery Control

Limits

13-10-5 2,3,4-TRIFLUOROTOLUENE 0.0926 j 0.112 83 69-119

Data Package ID: HCGQ009127-1

Dato Printed: Tuesday. September 26, 2000 Paragon Analyt ics Inc. p a 9 e 5 Q f 8

UMSVuiiiorr 1.836

SEP-28-00 THU 04:34 PH PARAGON ANALYTICS FAX NO. 910 490 1349 9^. P. 46

Gasoline Range Organics Method SW801S Sample Results

Lob Numc: Paragon Analytics, Inc.




Field Ip ; ' G0PS110204

Lab ID' 0000127-31

Samplo Matrix: SOIL % Moisture: S.3

Date Collected: 16-Sop-00 Dato Extracted: 21-Sep-OO Date Analyzed: 21-Sep-OO


Run 1D:HCG000921-1G Cleanup: NONE

Basis: Dry Weight

Sample Aliquot: SG Final Volume: 5G Result Units: MG/KG

File Name: G0921519

CASNO Target Analyte Dilution Result Report ing MDL Result EPA Factor Limit Qualifier Qualifier

S006-61-9 i

GASOLINE 1 0.55 0.55 0.022 U

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,4-TRin.UOROTOLUENLt 0.0771 . . .

0.109 71 69-119


Date Printed:Tuesday, September 26, 2000 Pa ragon Analy t ics Inc. P s - e 6 o f 8

1 IMS V/,!i Iran 1.096

SEP-28-00 THU 04:34 PH PARAGON ANALYTICS FAX NO. 920 490 1349 9^ P. 47




Client Namo: IT Corporation Las Vogas


Field ID: GBP5120204

' Lab ID. 000912/-32


Dato Collected: 16-Sep-OO Date Extracted: 21-Sep-OO Dale Analyzed; 21-Scp-00



Basis: Dry Weight


File Name: G0921S20


Result Reporting I MDL Limit |

Result Qualifier

EPA Qualifier

: 8006-G1-9 i

GASOLINE 1 0.55 0.55 j 0.022 U

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,4-TRIFLUOROTOLUENE 0.0971 0.111 07 69-119


Date Printed: Tuesday, September 26, 2000 Pa ragon Analy t ics Inc. P a 9 e 7 o f 8 l IMSVi- fmn: 185,9

SEP-28-00 THU 04:34 PM PARAGON ANALYTICS R O FAX NO. 970 490 1349 1^4 P. 42





ClientProject IP: Gasbuggy

FmUlID-. GfiPSi7020i

' U b ID; 0000127-18


Date Collected: 17-Scp-00 Dato Extracted: 21-Sep-OO Date Analyzed: 21-Sep-OO

Prep Batch: HCG000921-1 QCBatchID; HCG000921-1-1


Basis: Dry Weight

Sample Aliquot: 5 G Final Voiume: 5G Result Units: MG/KG

File Namo: G0921S15




EPA Qualifier

8006-61-9 GASOLINE 1 0.53 0.53 0.021 u

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,1-TRIFLUOROTOLUl£Ne 0.0925 0.105 88 69-119


Date Printed: Tuesday, September 26, 2000 Paragon Analytics Inc. UMSVo.Mon 1.C9E

Page 3 of 6

SEP-28-00 THU 04:34 PH PARAGON ANALYTICS FAX NO. 971L490 1349 P. 41

Gasoline Range Organics Method SW8015 Sampte Results

Lab Name - Paragon Analytics, Inc.

Work Order Number. 0009127



Field ID; 'fiBPSi80Dii

Lab ID: oo'oni27-i7

Samplo Matrix: SOIL % Moisture: 26.1

Date Collected: 17-Sep-00 Date Extracted: 21-Sop-OO Date Analyzed: 21-Sep-OO


Run ID: HCG000921-1G Cleanup: NONE

Basis: Dry Weight


File Name: G0921S14


8000-61-9 GASOlINn * •'• ' 1 0.68 0.68 0.027 U

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,4-YRIFLUOROTOLUENE 0.124 0.135 91 69-119


Date Printed; Tuesday, September 26,2000 Paragon Analyt ics Inc. p a 9 c 2 o f 8

LIMS Vur&ion. LKOri

SEP-28-00 THU 04:34 PM PARAGON ANALYTICS |AG( FAX NO. 970 490 1349

I P. 48




Client Name: IT Corporation I as Vegas

ClientProject IO: Gasbuggy

Field ID: 6UPS3102fi4

Lab'lD: 0009127-31



Prep Batch: HCG000922-1 QCBatchID: HCG000922-M

Run ID: HCG000922-1G Cleanup: NONE

Basis: Dry Weight


FileNama:G0922S18

I CASNO Target Analyte Dilution Result Reporting MDL Result EPA

j Factor Limit Qualifier Qualifier

| 8000-61-9 GASOLINE 1 0.65 0.55 0.022 j U

Surrogate Recovery


Percent Recovery

Control Limits

13-10-5 2,3,4-TRIFLUOROTOLUENE 0.102 0.11 93 69-119

Data Package ID: HCGO009127-2

Date Printed: Wednesday, September 27, 2000 Paragon Analytics Inc. LIMS Vuiiiwi. 1 006

Page 4 of 5

Tritium

Liquid Scintillation

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Surface Ground Zero Photographs

Price, Wayne

From: Afong, Scotty[SMTP:[email protected]] Sent: Friday, September 15, 2000 6:58 PM To: 'Catron, Mark'; 'Hooley, Camela'; 'Ketterman, Lorri'; 'Kieling.John'; Price, Wayne Cc: 'Chapman.Jenny'; Sanchez, Monica L; Stahl, David(IT); 'Young, John' Subject: Update for Gasbuggy Field Work (Week of September 11)

The following is an update on subject matter.

The New Mexico Oil and Conservation Division approved our proposed site ground disturbing activities (i.e., sampling of the site) and included conditions requiring additional chemical analysis (i.e. target analyte list, Radium 226/228, cyanide, nitrate, fluoride, uranium, boron, molybdenum, chloride, PCB). Direct push sampling was started on September 13 and is expected to be completed by September 25. A cultural survey of site areas, where these surveys have not previously been done, is scheduled the week of September 18. Our Public Affairs Information Office received a citizen inquiry on what we were doing at the site and the citizen was told that we were doing some preliminary site characterization work. Unfortunately, we were not able to obtain a contractor to purge our EPNG 10-36 well so all previously proposed work (purge well, video log the casing, sample aquifer) will not be accomplished.

For your information, I will be out of the office from September 18 to 29. For the September 18 report, I plan to fax you it. If you have any issues, please contact the project manager, Monica Sanchez, via e-mail (shown as copy addressee) or by calling (702) 295-0160.

Scotty Afong

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