reports dateocdimage.emnrd.state.nm.us/imaging/filestore/santa... · pamet n&! 17444 el pasq...

REPORTS

DATE: « f / 5 / 2 0 Q o

EL PASO FIELD SERVICES

April 5, 2000 ? 4

Mr. Bill Olson New Mexico Oil Conservation Division • • . . 2040 South Pacheco Santa Fe,NM 87505

Dear Mr. Olson,

El Paso Field Services (EPFS) hereby submits the analytical report for the sampling event that occurred at the Jaquez property on February 18, 2000. The samples were collected from various locations along Citizens Ditch during a period in which the ditch had been drained for maintenance. There were six soil samples collected (SS-01 through SS-06) with one duplicate sample taken at sample point SS-06. Sample points are depicted on an enclosed site drawing.

All samples were analyzed for benzene, toluene, ethylbenzene, xylene, and Total Petroleum Hydrocarbons. All samples, with the exception of SS-05 were "non-detect" for all parameters. Sample #SS-05 indicated a low level of toluene at 0.091mg/kg. EPFS requested that the laboratory review the analytical work to confirm the presence of toluene. The laboratory has determined as documented in their letter of March 28, 2000 (enclosed), that an unidentified analyte interfered with the analysis and that toluene is not present.

If you have any questions regarding the enclosed information, please contact Scott Pope at 505/599-2124 or myself at 505/599-2141.

Sincerely,

Sandra D. Miller Environmental Manager El Paso Energy

Enclosures (3)

cc: Mr. John Jaquez, Jr. Mr. Denny Foust, NMOCD Mr. Scott Pope, El Paso Energy

El Paso Field Services Company 614 Reilly Avenue Farmington, New Mexico 87401 Phone (505) 325-2841 Fax (505) 599-2235

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JAQUEZ CAS COM Erfll RUN SS-Ofl

JAQUEZ GAS COM C#1 METER RUN

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NOTES I. tLCVATtONS AAE IN FIET WITH

RESPECT TO A STE DATUII OF 100.00 rm.

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PAMET N&! 17444

EL PASQ FIELD JAQUE7. NEW MtXICO

FIGURE 1

2709-D Pan American Freeway NE Albuquerque, New Mexico 87107 Phone (505) 344-3777 Fax (505) 344-4413

LAF^T^ir^

March 28, 2000

Ms. Sandra D. Miller 614 Reilly Avenue Farmington, NM 87401

Sandra,

We were asked to review the analytical work performed by us for Study # 002076. Specifically, whether toluene was present on sample 002076-05 (JQZ-CD-SS-05).

The original sample extract was reanalyzed and confirmed the original results. Additionally, the sample was reextracted and this extract also confirmed the original results by Method 8021.

Howver, when Pinnacle examined these extracts by EPA method 8260 (GC Mass Spectrometry), toluene was not present.

We attribute the peak to an unidentified analyte that responds to the PID and interferes with toluene analysis. Based on this work we do not believe that toluene is present.

If we can be of any further assistance, please do not hesitate to contact me.

Sincerely,

Mitch Rubenstein, Ph.D President/CEO

PHILIP SERVICES

Industrial Services Group

Central Region

February 25, 2000 Project 62800089

Mr. Scott Pope El Paso Field Services 614Reilly Ave. Farmington, NM 87499

RE: Report for Sampling the Citizens Ditch at the Jaquez Property

Dear Mr. Pope:

On February 18, 2000, El Paso Field Services (EPFS) requested Philip Environmental Services Corporation (Philip) to meet at the Jaquez property in Blanco, NM to collect and split soil samples with Denny Foust of the New Mexico Oil Conservation Division (NMOCD). The samples were collected from various locations, designated by Mr. Foust, along Citizens Ditch, which was drained for scheduled maintenance. According to Mr. Foust, the NMOCD sampling guidelines state soil samples must be collected at two feet below ground surface (bgs) unless the samples are collected from a fresh excavation. Philip collected the samples following these guidelines. A portion of the samples collected was used to perform a heated headspace screening using a photoionization detector (PID). The samples were heated inside the cab of a vehicle by turning on the floor heater and placing the samples in front of the heat ducts.

The first sample, labeled JQZ-CD-SS-01, was collected at the eastern pipeline approximately three feet from the northern edge of the ditch bank on the ditch bottom. The sample appeared to be a brown sandy clay material. The heated headspace screening result was 15 parts per million (ppm).

The second sample, labeled JQZ-CD-SS-02, was collected between the eastern pipeline and the western pipeline. The sample was collected approximately three feet from the northern edge of the ditch bank in the slope of the ditch bank. The sample appeared to be a black clay material with sand and appeared to be decaying plant matter with a slight sulfur odor. The heated headspace screening result was 0 ppm.

The third sample, labeled JQZ-CD-SS-03, was collected approximately four feet west of the western pipeline and approximately five feet from the ditch bank on the ditch bottom. The sample appeared to be a sandy-silty material and was gray to brown. The sample was saturated with water. The heated headspace screening result was 0 ppm.

Combining the Strengths of Philip Services Corp., Allwaste and Serv-Tech

4000 Monroe Road • Farmington, NM 87401 '(505) 326-2262* Fax (505) 326-2388

Mr. Scott Pope W W El Paso Field Services Page 2 of 2

The fourth sample, labeled JQZ-CD-SS-04, was collected approximately 51 feet east of the foot bridge and approximately 10 feet from the northern edge of the ditch bank on the ditch bottom. The sample appeared to be a silty-sand material and brown in color. The sample was saturated with water. The heated headspace screening result was 0 ppm.

The fifth sample, labeled JQZ-CD-SS-05, was not split with or the sample location designated by the NMOCD. The sample was collected approximately 12 feet west of the western pipeline and approximately three and a half feet from the southern edge of the ditch bank in the slope of the ditch bank. The sample was very black with a swampy odor. There appeared to be an abundance of organic material in the sample. The sample appeared to be a sandy-silt material, moist to wet with a trace of clay. The heated headspace screening result was 1 ppm.

The sixth sample, labeled JQZ-CD-SS-06, also was not split with or the sample location designated by the NMOCD. The sample was collected approximately 45 feet east of the Jaquez property fence corner. The sample was collected from the center of the ditch on the ditch bottom. The sample appeared to be a brown silty-sandy clay material and was saturated with water. The heated headspace screening result was 0 ppm.

A duplicate sample was collected from the sixth sample and was labeled JQZ-CD-SS-56.

The samples collected were shipped to Pinnacle Laboratories in Albuquerque, NM and analyzed for Total Petroleum Hydrocarbons (TPH) using U.S. Environmental Protection Agency (EPA) method 8015 modified and benzene, toluene, ethylbenzene and xylene (BTEX) using U.S. EPA method 8021. Once the analytical results are received from the laboratory, an additional letter will be sent notifying EPFS of the results.

Philip appreciates the opportunity to provide this letter report to EPFS. If you have any questions or comments, please call me at (505) 326-2262.

Respectfully submitted, PHILIP ENVIRONMENTAL SERVICES CORPORATION

Robert Thompson Project Manager

J:\62800089\Jaqz_lttr.doc


Pinnacle Lab ID number 002076 March 08, 2000

PHILIP ENVIRONMENTAL 4000 MONROE ROAD FARMINGTON, NM 87401

Project Name EPFS JAQUEZ Project Number 62800089

Attention: ROBERT THOMPSON

On 02/23/00 Pinnacle Laboratories, Inc. Inc., (ADHS License No. AZ0592 pending), received a request to analyze non-aq samples. The samples were analyzed with EPA methodology or equivalent methods. The results of these analyses and the quality control data, which follow each set of analyses, are enclosed.

If you have any questions or comments, please do not hesitate to contact us

Kimberly D. McNeill H. Mitchell Rubenstein, Ph. D. Project Manager General Manager

MR: jt

Enclosure


CLIENT : PHILIP ENVIRONMENTAL PINNACLE ID : 002076

PROJECT # : 62800089 DATE RECEIVED : 02/23/00

PROJECT NAME :EPFS JAQUEZ REPORT DATE : 03/08/00

PIN DATE

ID. # CLIENT DESCRIPTION MATRIX COLLECTED

01 JQZ-CD-SS-01 NON-AQ 02/18/00

02 JQZ-CD-SS-02 NON-AQ 02/18/00

03 JQZ-CD-SS-03 NON-AQ 02/18/00

04 JQZ-CD-SS-04 NON-AQ 02/18/00

05 JQZ-CD-SS-05 NON-AQ 02/18/00

06 JQZ-CD-SS-06 NON-AQ 02/18/00

07 JQZ-CD-SS-56 NON-AQ 02/18/00

pliJt̂ Lt

Printed: 03/08/00; 2:21 PM Confidential Fil«: '002076; COVEREP


GAS CHROMATOGRAPHY RESULTS

TEST EPA 8021 MODIFIED CLIENT PHILIP ENVIRONMENTAL PINNACLE l.D.: 002076 PROJECT # 62800089 PROJECT NAME EPFS JAQUEZ SAMPLE DATE DATE DATE DIL ID.# CLIENT l.D. MATRIX SAMPLED EXTRACTED ANALYZED FACTOR 01 JQZ-CD-SS-01 NON-AQ 02/18/00 02/23/00 02/23/00 1 02 JQZ-CD-SS-02 NON-AQ 02/18/00 02/23/00 02/23/00 1 03 JQZ-CD-SS-03 NON-AQ 02/18/00 02/23/00 02/23/00 1

PARAMETER DET. LIMIT UNITS JQZ-CD-SS-01 JQZ-CD-SS-02 JQZ-CD-SS-03

BENZENE 0.025 MG/KG < 0.025 < 0.025 < 0.025 TOLUENE 0.025 MG/KG < 0.025 < 0.025 < 0.025 ETHYLBENZENE 0.025 MG/KG < 0.025 < 0.025 < 0.025 TOTAL XYLENES 0.025 MG/KG < 0.025 < 0.025 < 0.025

SURROGATE: BROMOFLUOROBENZENE (%) 112 103 103 SURROGATE LIMITS ( 6 5 - 120)

CHEMIST NOTES: N/A



TEST EPA 8021 MODIFIED CLIENT PHILIP ENVIRONMENTAL PINNACLE l.D.: 002076 PROJECT# 62800089 PROJECT NAME EPFS JAQUEZ SAMPLE DATE DATE DATE DIL. ID. # CLIENT l.D. MATRIX SAMPLED EXTRACTED ANALYZED FACTOR 04 JQZ-CD-SS-04 NON-AQ 02/18/00 02/23/00 02/23/00 1 05 JQZ-CD-SS-05 NON-AQ 02/18/00 02/23/00 02/29/00 1 06 JQZ-CD-SS-06 NON-AQ 02/18/00 02/23/00 02/23/00 1


BENZENE 0.025 MG/KG < 0.025 < 0.025 < 0.025 TOLUENE 0.025 MG/KG < 0.025 0.091 < 0.025

ETHYLBENZENE 0.025 MG/KG < 0.025 < 0.025 < 0.025 TOTAL XYLENES 0.025 MG/KG < 0.025 < 0.025 < 0.025

SURROGATE: BROMOFLUOROBENZENE (%) 107 116 111 SURROGATE LIMITS ( 65- 120 )

PIlJHACLt

CHEMIST NOTES: N/A

plNlttCLj;



TEST CLIENT PROJECT # PROJECT NAME

EPA 8021 MODIFIED PHILIP ENVIRONMENTAL 62800089 EPFS JAQUEZ

PINNACLE l.D.: 002076

SAMPLE ID. # CLIENT l.D. MATRIX

DATE SAMPLED

DATE EXTRACTED

DATE ANALYZED

DIL. FACTOR

07 JQZ-CD-SS-56 NON-AQ 02/18/00 02/23/00 02/23/00 1

PARAMETER DET. LIMIT UNITS JQZ-CD-SS-56

BENZENE TOLUENE ETHYLBENZENE TOTAL XYLENES

0.025 0.025 0.025 0.025

MG/KG MG/KG MG/KG MG/KG

< 0.025 < 0.025 < 0.025 < 0.025

SURROGATE: BROMOFLUOROBENZENE (%) SURROGATE LIMITS (65-120)

104

CHEMIST NOTES: N/A


GAS CHROMATOGRAPHY RESULTS REAGENT BLANK

TEST EPA 8021 MODIFIED PINNACLE l.D. : 002076 BLANK I. D. 022300 DATE EXTRACTED : 02/23/00 CLIENT PHILIP ENVIRONMENTAL DATE ANALYZED : 02/23/00 PROJECT # 62800089 SAMPLE MATRIX : NON-AQ

PROJECT NAME EPFS JAQUEZ

PARAMETER UNITS

BENZENE MG/KG <0.025

TOLUENE MG/KG O.025

ETHYLBENZENE MG/KG <0.025

TOTAL XYLENES MG/KG <0.025

SURROGATE: BROMOFLUOROBENZENE (%) 96 SURROGATE LIMITS: ( 80 - 120 ) CHEMIST NOTES: N/A


TEST

GAS CHROMATOGRAPHY QUALITY CONTROL MSMSD

EPA 8021 MODIFIED MSMSD # CLIENT PROJECT # PROJECT NAME

: 002067-01 : PHILIP ENVIRONMENTAL : 62800089 :EPFS JAQUEZ

PINNACLE l.D. DATE EXTRACTED DATE ANALYZED SAMPLE MATRIX UNITS

002076 02/22/00 02/23/00 NON-AQ MG/KG

PARAMETER SAMPLE RESULT

CONC SPIKE

SPIKED SAMPLE

% REC

DUP SPIKE

DUP % REC RPD

REC LIMITS

RPD LIMITS

BENZENE <0.025 1.00 1.09 109 1.05 105 4 ( 6 8 - 1 2 0 ) 20

TOLUENE <0.025 1.00 1.05 105 1.00 100 5 ( 6 4 - 120 ) 20

ETHYLBENZENE <0.025 1.00 1.17 117 1.11 111 5 ( 4 9 - 127) 20

TOTAL XYLENES O.025 3.00 3.34 111 3.15 105 6 ( 5 8 - 120 ) 20

CHEMIST NOTES: N/A

(Spike Sample Result - Sample Result) % Recovery = X 100

Spike Concentration

(Sample Result - Duplicate Result)

Average Result RPD (Relative Percent Difference) = X 100



TEST : EPA 8015 MODIFIED (DIRECT INJECT) CLIENT : PHILIP ENVIRONMENTAL PINNACLE l.D.: 002076 PROJECT # : 62800089 PROJECT NAME :EPFS JAQUEZ SAMPLE DATE DATE DATE DIL. ID. # CLIENT l.D. MATRIX SAMPLED EXTRACTED ANALYZED FACTOR 01 JQZ-CD-SS-01 NON-AQ 02/18/00 02/24/00 02/25/00 1 02 JQZ-CD-SS-02 NON-AQ 02/18/00 02/24/00 02/25/00 1 03 JQZ-CD-SS-03 NON-AQ 02/18/00 02/24/00 02/25/00 1


FUEL HYDROCARBONS, C6-C10 10 MG/KG < 10 < 10 < 10 FUEL HYDROCARBONS, C10-C22 10 MG/KG < 10 < 10 < 10 FUEL HYDROCARBONS, C22-C36 20 MG/KG < 20 < 20 < 20 CALCULATED SUM:

SURROGATE: O-TERPHENYL (%) SURROGATE LIMITS ( 6 6 - 1 5 1

105 106 108

CHEMIST NOTES: N/A



TEST : EPA 8015 MODIFIED (DIRECT INJECT) CLIENT : PHILIP ENVIRONMENTAL PINNACLE l.D.: 002076 PROJECT # : 62800089 PROJECT NAME :EPFS JAQUEZ SAMPLE DATE DATE DATE DIL ID. # CLIENT l.D. MATRIX SAMPLED EXTRACTED ANALYZED FACTOR 04 JQZ-CD-SS-04 NON-AQ 02/18/00 02/24/00 02/25/00 1 05 JQZ-CD-SS-05 NON-AQ 02/18/00 02/24/00 02/25/00 1 06 JQZ-CD-SS-06 NON-AQ 02/18/00 02/24/00 02/25/00 1


FUEL HYDROCARBONS, C6-C10 10 MG/KG < 10 < 10 < 10 FUEL HYDROCARBONS, C10-C22 10 MG/KG < 10 < 10 < 10 FUEL HYDROCARBONS, C22-C36 20 MG/KG < 20 < 20 < 20 CALCULATED SUM:

SURROGATE: O-TERPHENYL (%) SURROGATE LIMITS ( 6 6 - 1 5 1 )

106 110 104

CHEMIST NOTES: N/A



TEST CLIENT PROJECT # PROJECT NAME

: EPA 8015 MODIFIED (DIRECT INJECT) : PHILIP ENVIRONMENTAL : 62800089 :EPFS JAQUEZ

PINNACLE l.D.: 002076

SAMPLE ID. # CLIENT l.D.

DATE MATRIX SAMPLED

DATE EXTRACTED

DATE ANALYZED

DIL. FACTOR

07 JQZ-CD-SS-56 NON-AQ 02/18/00 02/24/00 02/25/00 1

PARAMETER DET. LIMIT UNITS JQZ-CD-SS-56

FUEL HYDROCARBONS, C6-C10 FUEL HYDROCARBONS, C10-C22 FUEL HYDROCARBONS, C22-C36 CALCULATED SUM:

10 10 20

MG/KG MG/KG MG/KG

< 10 < 10 < 20

SURROGATE: O-TERPHENYL (%) SURROGATE LIMITS ( 66-151 )

109

CHEMIST NOTES: N/A

pltfNACIj;



TEST BLANK l.D. CLIENT PROJECT # PROJECT NAME

REAGENT BLANK EPA 8015 MODIFIED (DIRECT INJECT) 022400 PHILIP ENVIRONMENTAL 62800089 EPFS JAQUEZ

PINNACLE l.D. DATE EXTRACTED DATE ANALYZED SAMPLE MATRIX

002076 02/24/00 02/24/00 NON-AQ

PARAMETER UNITS FUEL HYDROCARBONS, C6-C10 FUEL HYDROCARBONS, C10-C22 FUEL HYDROCARBONS, C22-C36

MG/KG MG/KG MG/KG

< 10 < 10 < 20

SURROGATE: O-TERPHENYL (%) SURROGATE LIMITS (80-151 )

107

CHEMIST NOTES: N/A


TEST

GAS CHROMATOGRAPHY QUALITY CONTROL MSMSD

EPA 8015 MODIFIED (DIRECT INJECT) MSMSD # : 002081-01 PINNACLE l.D. 002076 CLIENT : PHILIP ENVIRONMENTAL DATE EXTRACTED 02/24/00 PROJECT # : 62800089 DATE ANALYZED 02/25/00 PROJECT NAME :EPFS JAQUEZ SAMPLE MATRIX

UNITS NON-AQ MG/KG

SAMPLE CONC SPIKED % DUP DUP REC RPD PARAMETER RESULT SPIKE SAMPLE REC SPIKE % REC RPD LIMITS LIMITS

FUEL HYDROCARBONS <10 200 220 110 219 110 0 ( 5 6 - 148) 20

CHEMIST NOTES: N/A

(Spike Sample Result - Sample Result) % Recovery = X 100

Spike Concentration

(Sample Result - Duplicate Result) RPD (Relative Percent Difference) =

Average Result X 100

PHILIP IfSailEBJilffl.

Chain of Custody Record 4000 Monroe Road Farmington, NM 87401

(505) 326-2262 Phone (505) 326-2388 FAX COC Serial No. C 2 4 9 4

Project Name £PF£> .XtACcUt-Z-

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Sample Number (and depth) Date Time Matrix

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Relinquished by: Received By: Signature Date Time

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Samples Iced: £3, Yes • No Preservatives (ONLY for Water Samples)

G Cyanide Sodium hyroxlde (NaOH)

• Volatile Organic Analysis Hydrochloric acid (HCI)

• Metals Nitric acid (HNO3)

• TPH (418.1) Sulfuric acid (H2SO4)

• Other (Specify)

• Other (Specify)

Carrier: Airbill No. fl/J HfiQ I t l t S O W 8

Shipping and Lab Notes:

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002076-01

EVENTS.E

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EVENTS.E

Feb 28 14:32 2000

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C:\HPCHEM\2\METHODS\NM102799.M (Chemstation Integrator: NM 3015 Wed Nov 10 11:29:39 1999 Mult i p l e Level Calibration NM102799.M

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EVENTS.E

Quant Time: Mar 1 16:06 2000 Quant Resul ts F i l e : NM102799.RES

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C:\HPCIW\2\DATA\111299\FID003.D 12 Nov 1999 11:21 gasoline at 200ug/mL EVENTS.E

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Q u a n t i t a t i o n Report

C: \HP^M\2\DATA\110899\FID004 . D1

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EVENTS.E

Quant Time: Nov 12 13:54 1999

V i a l : 4 Opera tor : CFF I n s t : F I D - 1 M u l t i p l r : 1.00

Quant Resul ts F i l e : NM102799.RES

Quant Method T i t l e Las t Update Response v i a DataAcq Meth

C:\HPCHEM\2\METHODS\NM102799.M (Chemstation I n t e g r a t o r ) NM 8015 Wed Nov 10 11:29:39 1999 M u l t i p l e Leve l C a l i b r a t i o n NM102799.M

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FID004.D NM102799.M F r i Nov 12 13:54:18 1999 Page

iliJilill̂ cEAMLYSis, INC UU 6701 Aberdeen Avenue, Suite 9 4725 Ripley Avenue, Suite A

Lubbock, Texas 79424 800-378-1296 806-794-1296 El Paso, Texas 79922 888-588-3443 915-585-3443

E-Mail: [email protected]

FAX 806-794-1298 FAX 915-585-4944

Analytical and Quality Control Report

Denny Foust 0 C D Report Date: 2/23/00 1000 Rio Brazos Rd. Aztec, NM 87410

Project Number: Project Name: Project Location:

N/A Jaquez Blanco,NM

Order ID Number: A00021907

Enclosed are the Analytical Results and Quality Control Data Reports for the following samples submitted to TraceAnalysis, Inc. for analysis:

Date Time Date Sample Number Sample Description Matrix Taken Taken Received

140974 #1 143002182000 Soil 2/18/00 14:30 2/19/00

140975 #2 141002182000 Soil 2/18/00 14:10 2/19/00

140976 #3 140002182000 Soil 2/18/00 14:00 2/19/00

140977 #4 144002182000 Soil 2/18/00 14:40 2/19/00

These results represent only the samples received in the laboratory. The Quality Control Report is generated on a batch basis. All information contained in this report is for the analytical batch(es) in which your sample(s) were analyzed.

This report consists of a total of 7 pages and shall not be reproduced except in its entirety, without written approval of TraceAnalysis, Inc. j £

Dr. Blair Leftwich, Director

Report Date: 2/23/00

N/A


Jaquez

Page Number: 2 of 7

Blanco,NM

Analytical Results Report

Sample Number: 140974 Description: #1 143002182000

Analytical Date Date Prep QC Param Result Dilution Method Prepared Analyzed Analyst Batch # Batch # RDL

BTEX (mg/Kg) Benzene 0.054 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Toluene 0.056 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Ethylbenzene <0.05 50 S802IB 2/21/00 2/21/00 RC PB00849 QC01022 0.001 M,P,0-Xylene 0.212 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Total BTEX 0.322 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 * Test Comments - LCS/LCSD WERE USED TO CALCULATE RPD AND EA, DUE TO POOR PREP OF THE MS/MSD.

Spike % % Rec. Prep QC Surrogate (mg/Kg) Result Dilution Amount Rec. Limit Analyst Batch # Batch #

TFT 4.15 1 0.1 83 72-128 RC PB00849 QC01022 4-BFB 4.3 1 0.1 86 72 - 128 RC PB00849 QC01022

TPH DRO (mg/Kg) DRO <50 1 Mod. 8015B 2/20/00 2/20/00 MA PB00827 QC00999

TPH GRO (mg/Kg) GRO <5 1 8015B 2/22/00 2/22/00 RC PB00874 QC01058



BTEX (mg/Kg) Benzene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Toluene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Ethylbenzene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 M,P,0-Xylene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Total BTEX <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 * Test Comments - LCS/LCSD WERE USED TO CALCULATE RPD AND EA, DUE TO POOR PREP OF THE MS/MSD.

i Spike % % Rec. Prep QC Surrogate (mg/Kg) Result Dilution Amount Rec. Limit Analyst Batch # Batch #

TFT 4.66 1 0.1 93 72-128 RC PB00849 QC01022

4-BFB 5.03 1 0.1 101 72- 128 RC PB00849 QC01022

TPH DRO (mg/Kg) DRO <50 1 Mod. 8015B 2/20/00 2/20/00 MA PB00827 QC00999 50

TPH GRO (mg/Kg) GRO <5 1 8015B 2/22/00 2/22/00 RC PB00874 QC01058 0.1



BTEX (mg/Kg) Benzene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001

Toluene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001

Ethylbenzene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001


N/A


Jaquez

Page Number: 3 of 7

Blanco,NM

M,P,0-Xylene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 Total BTEX <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 * Test Comments - LCS/LCSD WERE USED TO CALCULATE RPD AND EA, DUE TO POOR PREP OF THE MS/MSD.

Surrogate (mg/Kg) Spike % % Rec. Prep QC

Surrogate (mg/Kg) Result Dilution Amount Rec. Limit Analyst Batch # Batch # TFT 5.03 1 0.1 101 72-128 RC PB00849 QC01022 4-BFB 5.49 1 0.1 110 72 - 128 RC PB00849 QC01022


TPH GRO (mg/Kg) GRO <5 1 8015B 2/22/00 2/22/00 RC PB00874 QC01058



BTEX (mg/Kg) Benzene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Toluene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Ethylbenzene <0.05 50 S8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 M,P,0-Xylene <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001 Total BTEX <0.05 50 S 8021B 2/21/00 2/21/00 RC PB00849 QC01022 0.001

* Test Comments - LCS/LCSD WERE USED TO CALCULATE RPD AND EA, DUE TO POOR PREP OF THE MS/MSD,

Spike % % Rec. Prep QC Surrogate (mg/Kg) Result Dilution Amount Rec. Limit Analyst Batch § Batch #

TFT 4.28 1 0.1 86 72- 128 RC PB00849 QC01022

4-BFB 4.38 1 0.1 88 72- 128 RC PB00849 QC01022


TPH GRO (mg/Kg) GRO <5 1 8015B 2/22/00 2/22/00 RC PB00874 QC01058 0.1

Report Date: 2/23/00 Order ID Number: A00021907 w Page Number: 4 of 7

N/A Jaquez Blanco.NM

Quality Control Report Method Blanks Blank Reporting Date Prep QC

Param Flag Result Limit Analyzed Batch # Batch #

Benzene (mg/Kg) <0.05 0.05 2/21/00 PB00849 QC01022 Toluene (mg/Kg) <0.05 0.05 2/21/00 PB00849 QC01022

Ethylbenzene (mg/Kg) <0.05 0.05 2/21/00 PB00849 QC01022

M,P,0-Xylene (mg/Kg) <0.05 0.05 2/21/00 PB00849 QC01022

Total BTEX (mg/Kg) <0.05 0.05 2/21/00 PB00849 QC01022

Surrogate Spike % % Rec. QC

Surrogate Result Amount Rec. Limit Batch # TFT (mg/Kg) 4.86 0.1 97 72 - 128 QC01022 4-BFB (mg/Kg) 5.16 0.1 103 72- 128 QC01022

Blank Reporting Date Prep QC Param Flag Result Limit Analyzed Batch # Batch #

DRO (mg/Kg) <50 50 2/20/00 PB00827 QC00999

Blank Reporting Date Prep QC Param Flag Result Limit Analyzed Batch # Batch #

GRO (mg/Kg) <5 0.1 2/22/00 PB00874 QC01058


N/A


Jaquez

Page Number: 5 of 7

Blanco,NM

Qualify Control Report Matrix Spike and Matrix Duplicate Spike

Spike Matrix Sample Amount Spike % % Rec. RPD QC

Standard Param Result Dil . Added Result Rec. RPD Limit Limit Batch #

MS DRO (mg/Kg) * <50 1 250 226 90 70-130 0-20 QC00999 * DRO - MS/MSD OUT OF RANGE DUE TO MATRIX INTERFERENCES USE LCS/LCSD.

MSD DRO (mg/Kg) * <50 1 250 157 63 36 70-130 0-20 QC00999 * DRO - MS/MSD OUT OF RANGE DUE TO MATRIX INTERFERENCES USE LCS/LCSD.

Spike Matrix Sample Amount Spike % % Rec. RPD QC

Standard Param Result Dil . Added Result Rec. RPD Limit Limit Batch #

MS Benzene (mg/Kg) <0.05 50 0.1 5.52 110 9 80- 120 0-20 QC01022

MS Toluene (mg/Kg) 0.064 50 0.1 5.66 112 9 80- 120 0-20 QC01022

MS Ethylbenzene (mg/Kg) <0.05 50 0.1 5.65 113 6 80- 120 0-20 QC01022

MS M,P,0-Xylene (mg/Kg) 0.124 50 0.3 16.7 111 5 80-120 0-20 QC01022

Spike % % Rec. Prep QC Standard Surrogate Result Dil. Amount Analyst Rec. Limit Batch # Batch # MS TFT (mg/Kg) 4.4 50 0.1 RC 88 72- 128 PB00849 QC01022

MS 4-BFB (mg/Kg) 4.77 50 0.1 RC 95 72- 128 PB00849 QC01022

MSD Benzene (mg/Kg) <0.05 50 0.1 5.6 112 1 80- 120 0-20 QC01022

MSD Toluene (mg/Kg) 0.064 50 0.1 5.84 116 3 80- 120 0-20 QC01022

MSD Ethylbenzene (mg/Kg) <0.05 50 0.1 6.01 120 6 80- 120 0-20 QC01022

MSD M,P,0-Xylene (mg/Kg) 0.124 50 0.3 18 119 8 80 - 120 0-20 QC01022

Spike % % Rec. Prep QC Standard Surrogate Result Dil. Amount Analyst Rec. Limit Batch # Batch # MSD TFT (mg/Kg) 4.7 50 0.1 RC 94 72- 128 PB00849 QC01022

MSD 4-BFB (mg/Kg) 5.52 50 0.1 RC 110 72- 128 PB00849 QC01022


N/A Order ID Number: A00021907

Jaquez Page Number: 6 of 7

Blanco/NM

Quality Control Report Lab Control Spikes and Duplicate Spike

Spike Matrix Blank Amount Spike % % Rec. RPD QC

Param Result Dil . Added Result Rec. RPD Limit Limit Batch #

LCS MTBE (mg/Kg) <0.05 50 0.1 5.6 112 80- 120 0-20 QC01022

LCS Benzene (mg/Kg) <0.05 50 0.1 5.26 105 80-120 0-20 QC01022

LCS Toluene (mg/Kg) <0.05 50 0.1 5.38 108 80- 120 0-20 QC01022

LCS Ethylbenzene (mg/Kg) <0.05 50 0.1 5.33 107 80-120 0-20 QC01022

LCS M,P,0-Xylene (mg/Kg) <0.05 50 0.3 15.6 104 80- 120 0-20 QC01022

Spike % % Rec. QC Standard Surrogate Dil. Amount Result Rec. Limit Batch # LCS TFT (mg/Kg) 50 0.1 4.48 90 72- 128 QC0I022 LCS 4-BFB (mg/Kg) 50 0.1 4.9 98 72 - 128 QC01022

LCSD MTBE (mg/Kg) <0.05 50 0.1 5.19 104 8 80-120 0-20 QC01022

LCSD Benzene (mg/Kg) <0.05 50 0.1 4.81 96 9 80 - 120 0-20 QC01022

LCSD Toluene (mg/Kg) O.05 50 0.1 4.94 99 9 80- 120 0-20 QC01022

LCSD Ethylbenzene (mg/Kg) <0.05 50 0.1 5.02 100 6 80-120 0-20 QC01022

LCSD M,P,0-Xylene (mg/Kg) <0.05 50 0.3 14.8 99 5 80- 120 0-20 QC01022

Spike % % Rec. QC Standard Surrogate Dil. Amount Result Rec. Limit Batch # LCSD TFT (mg/Kg) 50 0.1 4.24 85 72- 128 QC01022

LCSD 4-BFB (mg/Kg) 50 0.1 4.75 95 72- 128 QC01022



LCS DRO (mg/Kg) <50 1 250 238 95 70- 130 0-20 QC00999

LCSD DRO (mg/Kg) <50 1 250 242 97 2 70- 130 0-20 QC00999



LCS GRO (mg/Kg) <5 1 1 0.924 92 80- 120 0-20 QC01058

LCSD GRO (mg/Kg) <5 1 1 0.892 89 4 80- 120 0-20 QC01058

' Report Date: 2/23/00 N/A

Order ID Number: A00021907 Jaquez

Page Number: 7 of 7

BIanco,NM

Quality Control Report Continuing Calibration Verification Standard

Standard Param Flag

CCVs TRUE Cone.

CCVs Found Cone.

CCVs Percent

Recovery

Percent Recovery

Limits

Date Analyzed

QC Batch #

ICV Benzene (mg/Kg) 0.1 0.103 103 80 - 120 2/21/00 QC01022 ICV Toluene (mg/Kg) 0.1 0.105 105 80 - 120 2/21/00 QC01022 ICV Ethylbenzene (mg/Kg) 0.1 0.109 109 80 - 120 2/21/00 QC01022 ICV M,P,0-Xylene (mg/Kg) 0.3 0.321 107 80 - 120 2/21/00 QC01022

CCV 1 Benzene (mg/Kg) 0.1 0.101 101 80-120 2/21/00 QC01022 CCV 1 Toluene (mg/Kg) 0.1 0.103 103 80- 120 2/21/00 QC01022 CCV 1 Ethylbenzene (mg/Kg) 0.1 0.102 102 80- 120 2/21/00 QC01022 CCV 1 M,P,0-Xylene (mg/Kg) 0.3 0.298 99 80- 120 2/21/00 QC01022

CCV 2 Benzene (mg/Kg) 0.1 0.098 98 80- 120 2/21/00 QC01022 CCV 2 Toluene (mg/Kg) 0.1 0.102 102 80 - 120 2/21/00 QC01022

CCV 2 Ethylbenzene (mg/Kg) 0.1 0.1 100 80 - 120 2/21/00 QC01022

CCV 2 M,P,0-Xylene (mg/Kg) 0.3 0.296 99 80 - 120 2/21/00 QC01022

Standard Param Flag

CCVs TRUE Cone.

CCVs Found Cone.

CCVs Percent

Recovery

Percent Recovery

Limits

Date Analyzed

QC Batch #

ICV DRO (mg/Kg) 250 298 119 70- 130 2/20/00 QC00999

CCV 1 DRO (mg/Kg) 250 270 108 70- 130 2/20/00 QC00999

CCV 2 DRO (mg/Kg) 250 202 81 70- 130 2/20/00 QC00999

Standard Param Flag

CCVs TRUE Cone.

CCVs Found Cone.

CCVs Percent

Recovery

Percent Recovery

Limits

Date Analyzed

QC Batch #

ICV GRO (mg/Kg) 1 0.889 89 80 - 120 2/22/00 QC01058

CCV 1 GRO (mg/Kg) 1 1.07 107 80 - 120 2/22/00 QC01058

Page / of /

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