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Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov, Evgeniy Statsenko, Akhmet Galeev Kazan Federal University, Kazan, Russia GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

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Page 1: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Reservoir Properties of Sandstone and Carbonate

Rocks Revealed By The Use Of X-ray micro-CT

Alexey Konovalov

Timur Zakirov, Evgeniy Statsenko, Akhmet Galeev

Kazan Federal University, Kazan, Russia

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 2: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Akhmet Galeev, Ph.D., Head of DepartmentE-mail: [email protected]: +7 (843) 233-75-60

Timur Zakirov, Ph.D.,Head of research projects: ”Digital core plug”,E-mail: [email protected]: +7-950-317-77-24

Evgeniy Statsenko, Head of Lab “X-ray CT” E-mail: [email protected]: +7-960-040-49-10

Alexey Konovalov Ph.D., ResearcherE-mail: [email protected]: +7 (843) 233-75-60http://kpfu.ru/sotrudniki-70746.html

Our Team

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 3: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Kazan Federal University (based in 1804)•31 institutes and faculties•~30000 students, •over 3000 teachers.Famous former students:

Vladimir Lenin, Lev Tolstoy,

Famous scientists:Nikolay Lobachevski, Alexandr Butlerov, Nikolay Zinin, Evgeniy Zavoiskiy

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 4: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

X-ray system for high resolution CT and 2D inspection v|tome|x s 240

• 240 kV / 320 W microfocus tube• opt. additional 180 kV /15 W nanofocus tube• 5-axis manipulation system • DXR 250RT flat panel, 1024 x 1024 pixel, 200 μm pixel size, up to 30 fps • two-fold detector shift • max. sample size: 300 mm x 400 mm • max. 3D scan size: 260 mm x 400 mm • 10 kg max. sample weight

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 5: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Our research interests :

Reservoir Properties

Archeology and Paleontology

Materials Science

Avizo Fire Edition Volume Graphics Studio SIAMS

We use:

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 6: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Reservoir Properties

X‐ray Tomography of large sized core plug

Core sample with different types of voids Voids distribution Voids larger

than 1000 mm3

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 7: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Images of sandstone

Micro-CT Nano-CT

0.5 mm 0.5 mm

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 8: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Heavy oil in sand reservoir

Scans and movie were prepared by Gerhard Zacher (GE Phoenix X-ray)

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 9: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Pore space analysis

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 10: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Pore space analysis

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 11: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Pore size distribution

Material volume: 128,8501 mm3

Void volume: 17.7075 mm3 (13.74 %)

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 12: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Visualization of pore space

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 13: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Visualization of pore space

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 14: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Reservoir properties calculation on digital core plugsSegmentation of micro-CT image

original image image after segmentation

Solid phase Pore space

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 15: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Virtual sections

Sandstone Carbonate

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 16: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Navier–Stokes and continuity equations

Stationary regime Non stationary regime

0Udiv

UU

)(1)( Pgrad

dtd

– 1 equation

– 3 equations

The unknown variables

0Udiv – 1 equation

),,,( tzyxUU xx ),,,( tzyxUU yy ),,,( tzyxUU zz

),,,( tzyxPP

),,( zyxUU xx ),,( zyxUU yy ),,( zyxUU zz

U

)(10 Pgrad– 3 equations

Velocities field

Pressure field ),,( zyxPP GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 17: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

jxj

jjxj

x PgraddS

dSUk

)()(

)(

Boundary condition

Inlet pressure

Outlet pressure

Darcy Law

j - number of cell in outlet plane

dS - area of cell edge

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 18: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

velocity field

Results of computational experimentsSandstone

pore space

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 19: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Carbonate

Results of computational experiments

velocity fieldpore space

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 20: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Porosity distribution along the length of the core

Sandstones Carbonates

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 21: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

4D reconstruction and visualization of fluid flow insandstone by SIAMS

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 22: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

4D reconstruction and visualization of fluid flow insandstone by SIAMS

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 23: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Quartz vein with inclusion of native gold

Micro-CT applications in geology

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 24: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Permonautilus

Micro-CT applications in paleontology

20 mm

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 25: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

PermonautilusMicro-CT applications in paleontology

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 26: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Nautiloid in rock

Micro-CT applications in paleontology

10 mm

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 27: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Micro-CT applications in paleontologyNautiloid in rock

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 28: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Conodont

Micro-CT applications in paleontology

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 29: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Conodont

Micro-CT applications in paleontology

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 30: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Pieces of ancient pottery

Micro-CT applications in archeology

10 mm

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 31: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

XZ-plane

Y

XY-plane

Micro-CT applications in archeology

YZ-plane

Pieces of ancient pottery

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 32: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

TextoliteMicro-CT applications in material science

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 33: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

TextoliteMicro-CT applications in material science

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 34: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Micro-CT applications in material sciencePores and mechanical properties of composites. Universal Restorative Filtek™ Z250

Virtual section of CT-scan

Pore concentration at layers boundaries

Scanning electron microscopy of layered structure of sold composite

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 35: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Micro-CT applications in material scienceMicrostructure of Cu-Fe composite

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 36: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Our future plans : Filtration measurements In-situ

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 37: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Our future plans : Filtration measurements In-situ

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 38: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Thank you for attention!

Acknowledgements:

This work is partially supported by the subsidy of the Russian Government to support the Program of competitive growth of Kazan Federal University among world class academic centers and universities.

GE GmbH

GE's 11th X-ray Forum July 7, 2015 - July 9, 2015 | Hotel Maritim Cologne City Center | Cologne, Germany

Page 39: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,
Page 40: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,
Page 41: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Терригенный коллектор

Page 42: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

Терригенный коллектор

Page 43: Reservoir Properties of Sandstone and Carbonate Rocks ... · Reservoir Properties of Sandstone and Carbonate Rocks Revealed By The Use Of X-ray micro-CT Alexey Konovalov Timur Zakirov,

3D модель порового пространства образца нефтяного коллектора