sample name: sirius black tested for: western oregon … testing/rec... · 2019. 2. 18. ·...

Analytical ResultsSC Laboratories Oregon LLC ORELAP# 4133/OLCC# 1004748743D

15865 SW 74th Ave Suite 110, Tigard, OR

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Sirius Black

Western Oregon Botanicals

Laboratory ID: 19C0028-05

Matrix: Useable Marijuana

Sample Metrc ID: 1A40103000098BF000001508

Sample Name:

Tested for:

Compliance - Usable

Batch Size: 2724 (g)

Batch RFID: 1A40103000098BF000001503

Lot # 18-Feb

Strain: Sirius Black

Date Sampled: 03/08/19 10:36

Date Accepted: 03/08/19

License: 020-10021071D94

Potency Analysis

Analysis Method/SOP: Potency

* - ORELAP certified analyte

0.26

16.48

0.030.080.71

THC 0.26

THCA 16.48

CBDA 0.03

CBG 0.08

CBGA 0.71

Total: 17.55

Cannabinoids Profile

Date Extracted: 03/12/19

Date Analyzed: 03/12/19

Cannabinoids mg/g% weight LOQ (%)

Total THC ((THCA*0.877)+d9) 147.114.71 0.02

Total CBD ((CBDA*0.877)+CBD) 0.30.03 0.02

0.26d9-THC (d9-Tetrahydrocannabinol)* 2.6 0.02

< LOQd8-THC (d8-Tetrahydrocannabinol)* < LOQ 0.02

16.48THCA (d9-Tetrahydrocannabinolic Acid)* 164.8 0.03

< LOQCBD (Cannabidiol)* < LOQ 0.02

0.03CBDA (Cannabidiolic Acid)* 0.3 0.03

< LOQCBN (Cannabinol)* < LOQ 0.02

0.08CBG (Cannabigerol)* 0.8 0.02

0.71CBGA (Cannabigerolic Acid) 7.1 0.02

< LOQCBDV (Cannabidivarin)* < LOQ 0.02

< LOQCBDVA (Cannabidivarinic Acid) < LOQ 0.02

< LOQCBC (Cannabichromene)* < LOQ 0.02

< LOQTHCV (Tetrahydrocannabivarin) < LOQ 0.02

175.5Total Cannabinoids 17.55 0.02

Water Activity and Moisture

ResultAnalyte LOQ Analyzed MethodUnitsLimit

0.469 0.0300AW Water Activity03/13/2019Water Activity 0.65

9.02 0.10% Moisture03/13/2019Percent Moisture 15

Results above the action level are highlighted in red #.Cannabinoids reported as dry weight (moisture corrected)



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Terpene Analysis





Date Sampled: 03/08/19 10:36

Sample Name:

Tested for:

Sirius Black


Compliance - Usable

Lot # 18-Feb

Batch RFID: 1A40103000098BF000001503



License: 020-10021071D94

Date Extracted: 03/12/19

Date Analyzed: 03/12/19

Analysis Method/SOP: Potency

Analyte LOQ Analyte Result LOQResult (%)

alpha Pinene 0.046 0.019 Myrcene 0.634 0.019

alpha Phellandrene < LOQ 0.019 3-Carene < LOQ 0.019

alpha Terpinene < LOQ 0.019 Limonene 0.297 0.019

Terpinolene < LOQ 0.019 Linalool 0.134 0.019

Fenchol 0.049 0.019 Borneol < LOQ 0.019

Terpineol 0.047 0.019 Geraniol 0.031 0.019

alpha Humulene 0.053 0.019 beta Caryophyllene 0.169 0.019

Caryophyllene Oxide < LOQ 0.019 alpha Bisabolol 0.078 0.019

Camphene < LOQ 0.019 beta Pinene 0.070 0.019

Ocimene 0.103 0.019 Sabinene < LOQ 0.019

Camphor < LOQ 0.019 Isoborneol < LOQ 0.019

Menthol < LOQ 0.019 alpha Cedrene < LOQ 0.019

Nerolidol 0.024 0.019 R-(+)-Pulegone < LOQ 0.019

Eucalyptol < LOQ 0.019 p-Cymene < LOQ 0.019

(-)-Isopulegol < LOQ 0.019 Geranyl Acetate < LOQ 0.019

Guaiol 0.044 0.019 Valencene 0.077 0.019

Phytol 0.039 0.019 Citronellol < LOQ 0.019

gamma-Terpinene < LOQ 0.019

Total Terpenes 1.895 %



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Date Accepted: 03/08/19 11:28

Date Sampled: 03/08/19 10:36

Laboratory ID: 19C0028-05 Client/Metrc ID: 1A40103000098BF000001508

Terpene Profile

Tested for:

Sample Name:


Sirius Black

Compliance - Usable

License: 020-10021071D94

0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7

alpha Pinene

Myrcene

alpha Phellandrene

3-Carene

alpha Terpinene

Limonene

Terpinolene

Linalool

Fenchol

Borneol

Terpineol

Geraniol

alpha Humulene

beta Caryophyllene

Caryophyllene Oxide

alpha Bisabolol

Camphene

beta Pinene

Ocimene

Sabinene

Camphor

Isoborneol

Menthol

alpha Cedrene

Nerolidol

R-(+)-Pulegone

Eucalyptol

p-Cymene

(-)-Isopulegol

Geranyl Acetate

Guaiol

Valencene

Phytol

Citronellol

gamma-Terpinene

%

These results relate only to the sample included on this report. The report may not be reproduced except in full, without

the written permission of SC Laboratories. Samples tested in accordance with Oregon Administrative Rules, TNI 2009

Standard and SC Laboratories quality assurance plan unless otherwise noted.

Page 3 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Pesticide Analysis in ppm

Date Sampled: 03/08/19 10:36






Sirius BlackSample Name:

Tested for:

Compliance - Usable


Batch RFID: 1A40103000098BF000001503

Lot # 18-Feb


License: 020-10021071D94

Date Analyzed:

Date Extracted: 03/12/19 Analysis Method/SOP: Pesticides

03/13/19 Results above the action levels are highlighed in red #.

Analyte LOQResult Action Level Analyte Result Action Level LOQ

0.5< LOQ 0.23Abamectin 0.4< LOQ 0.18Acephate

2< LOQ 0.92Acequinocyl 0.2< LOQ 0.09Acetamiprid

0.4< LOQ 0.18Aldicarb 0.2< LOQ 0.09Azoxystrobin

0.2< LOQ 0.09Bifenazate 0.2< LOQ 0.09Bifenthrin

0.4< LOQ 0.18Boscalid 0.2< LOQ 0.09Carbaryl

0.2< LOQ 0.09Carbofuran 0.2< LOQ 0.09Chlorantraniliprole

1< LOQ 0.46Chlorfenapyr 0.2< LOQ 0.09Chlorpyrifos

0.2< LOQ 0.09Clofentezine 1< LOQ 0.46Cyfluthrin

1< LOQ 0.46Cypermethrin 1< LOQ 0.46Daminozide

1< LOQ 0.46DDVP (Dichlorvos) 0.2< LOQ 0.09Diazinon

0.2< LOQ 0.09Dimethoate 0.2< LOQ 0.09Ethoprophos

0.4< LOQ 0.18Etofenprox 0.2< LOQ 0.09Etoxazole

0.2< LOQ 0.09Fenoxycarb 0.4< LOQ 0.18Fenpyroximate

0.4< LOQ 0.18Fipronil 1< LOQ 0.46Flonicamid

0.4< LOQ 0.18Fludioxonil 1< LOQ 0.46Hexythiazox

0.2< LOQ 0.09Imazalil 0.4< LOQ 0.18Imidacloprid

0.4< LOQ 0.18Kresoxim-methyl 0.2< LOQ 0.09Malathion

0.2< LOQ 0.09Metalaxyl 0.2< LOQ 0.09Methiocarb

0.4< LOQ 0.18Methomyl 0.2< LOQ 0.09Methyl parathion

0.2< LOQ 0.09MGK-264 0.2< LOQ 0.09Myclobutanil

0.5< LOQ 0.23Naled 1< LOQ 0.46Oxamyl

0.4< LOQ 0.18Paclobutrazol 0.2< LOQ 0.09Permethrins (total)

0.2< LOQ 0.09Phosmet 2< LOQ 0.46Piperonyl butoxide

0.2< LOQ 0.09Prallethrin 0.4< LOQ 0.18Propiconazole

0.2< LOQ 0.09Propoxur 1< LOQ 0.46Pyrethrins (total)

0.2< LOQ 0.09Pyridaben 0.2< LOQ 0.09Spinosad

0.2< LOQ 0.09Spiromesifen 0.2< LOQ 0.09Spirotetramat

0.4< LOQ 0.18Spiroxamine 0.4< LOQ 0.18Tebuconazole

0.2< LOQ 0.09Thiacloprid 0.2< LOQ 0.09Thiamethoxam

0.2< LOQ 0.09Trifloxystrobin



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Case Narrative

Receiving - Samples: 19C0028-01 (1504) and 19C0028-02 (1505) composited for Pesticides,

Moisture Content, and Water Activity. Samples: 19C0028-03 (1506), 19C0028-04 (1507) and

19C0028-05 (1508) composited for Pesticides, Moisture Content and Water Activity.

Quality Control

Potency

Batch: B190398 - Potency/Terpenes

Blank(B190398-BLK1) Extracted - 03/12/19 9:30 Analyzed - 03/12/19 15:56

Analyte Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) < LOQ %

d8-THC (d8-Tetrahydrocannabinol) < LOQ %

THCA (d9-Tetrahydrocannabinolic Acid) < LOQ %

CBD (Cannabidiol) < LOQ %

CBDA (Cannabidiolic Acid) < LOQ %

CBN (Cannabinol) < LOQ %

CBG (Cannabigerol) < LOQ %

CBGA (Cannabigerolic Acid) < LOQ %

CBDV (Cannabidivarin) < LOQ %

CBDVA (Cannabidivarinic Acid) < LOQ %

CBC (Cannabichromene) < LOQ %

THCV (Tetrahydrocannabivarin) < LOQ %

Duplicate(B190398-DUP1) Extracted - 03/12/19 9:30 Analyzed - 03/12/19 22:22


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) 1.21 % 1.27 4.34 20

d8-THC (d8-Tetrahydrocannabinol) < LOQ % < LOQ 20

CBD (Cannabidiol) < LOQ % < LOQ 20

CBDA (Cannabidiolic Acid) 0.04 % 0.04 2.72 20

CBN (Cannabinol) < LOQ % < LOQ 20

CBG (Cannabigerol) 0.06 % 0.06 4.67 20

CBGA (Cannabigerolic Acid) 0.76 % 0.77 0.892 20

CBDV (Cannabidivarin) < LOQ % < LOQ 20

CBDVA (Cannabidivarinic Acid) < LOQ % < LOQ 20

CBC (Cannabichromene) < LOQ % < LOQ 20

THCV (Tetrahydrocannabivarin) < LOQ % < LOQ 20

LCS(B190398-BS1) Extracted - 03/12/19 9:30 Analyzed - 03/12/19 15:47


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit




Page 5 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control

Potency (Continued)

Batch: B190398 - Potency/Terpenes (Continued)



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) 0.04 % 0.0400 108 80-120

CBD (Cannabidiol) 0.04 % 0.0400 106 80-120

CBDA (Cannabidiolic Acid) 0.04 % 0.0400 100 80-120

CBN (Cannabinol) 0.04 % 0.0400 99.8 80-120




Page 6 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control

Pesticide Analysis

Batch: B190400 - Pesticide Prep



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin < LOQ ppm

Acephate < LOQ ppm

Acequinocyl < LOQ ppm

Acetamiprid < LOQ ppm

Aldicarb < LOQ ppm

Azoxystrobin < LOQ ppm

Bifenazate < LOQ ppm

Bifenthrin < LOQ ppm

Boscalid < LOQ ppm

Carbaryl < LOQ ppm

Carbofuran < LOQ ppm

Chlorantraniliprole < LOQ ppm

Chlorfenapyr < LOQ ppm

Chlorpyrifos < LOQ ppm

Clofentezine < LOQ ppm

Cyfluthrin < LOQ ppm

Cypermethrin < LOQ ppm

Daminozide < LOQ ppm

DDVP (Dichlorvos) < LOQ ppm

Diazinon < LOQ ppm

Dimethoate < LOQ ppm

Ethoprophos < LOQ ppm

Etofenprox < LOQ ppm

Etoxazole < LOQ ppm

Fenoxycarb < LOQ ppm

Fenpyroximate < LOQ ppm

Fipronil < LOQ ppm

Flonicamid < LOQ ppm

Fludioxonil < LOQ ppm

Hexythiazox < LOQ ppm

Imazalil < LOQ ppm

Imidacloprid < LOQ ppm

Kresoxim-methyl < LOQ ppm

Malathion < LOQ ppm

Metalaxyl < LOQ ppm




Page 7 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control

Pesticide Analysis (Continued)

Batch: B190400 - Pesticide Prep (Continued)



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Methiocarb < LOQ ppm

Methomyl < LOQ ppm

Methyl parathion < LOQ ppm

MGK-264 < LOQ ppm

Myclobutanil < LOQ ppm

Naled < LOQ ppm

Oxamyl < LOQ ppm

Paclobutrazol < LOQ ppm

Permethrins (total) < LOQ ppm

Phosmet < LOQ ppm

Piperonyl butoxide < LOQ ppm

Prallethrin < LOQ ppm

Propiconazole < LOQ ppm

Propoxur < LOQ ppm

Pyrethrins (total) < LOQ ppm

Pyridaben < LOQ ppm

Spinosad < LOQ ppm

Spiromesifen < LOQ ppm

Spirotetramat < LOQ ppm

Spiroxamine < LOQ ppm

Tebuconazole < LOQ ppm

Thiacloprid < LOQ ppm

Thiamethoxam < LOQ ppm

Trifloxystrobin < LOQ ppm



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 0.96 ppm 0.980 97.5 29-150

Acephate 1.01 ppm 1.00 101 48-133

Acequinocyl 0.75 ppm 1.00 75.0 48-150

Acetamiprid 0.84 ppm 1.00 83.8 45-150

Aldicarb 0.91 ppm 1.00 91.1 58-134

Azoxystrobin 0.89 ppm 1.00 89.1 25-150

Bifenazate 1.18 ppm 1.00 118 46-141

Bifenthrin 1.23 ppm 1.00 123 55-150




Page 8 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control





Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Boscalid 1.10 ppm 1.00 110 34-141

Carbaryl 1.10 ppm 1.00 110 67-125

Carbofuran 0.81 ppm 1.00 81.0 71-128

Chlorantraniliprole 0.90 ppm 1.00 89.9 43-138

Chlorfenapyr 1.18 ppm 1.00 118 45-150

Chlorpyrifos 1.17 ppm 1.00 117 36-150

Clofentezine 1.24 ppm 1.00 124 59-135

Cyfluthrin 1.33 ppm 1.00 133 33-150

Cypermethrin 1.12 ppm 1.00 112 47-148

Daminozide 0.72 ppm 1.00 72.1 18-116

DDVP (Dichlorvos) 1.16 ppm 1.00 116 65-150

Diazinon 1.15 ppm 1.00 115 60-130

Dimethoate 1.09 ppm 1.00 109 65-131

Ethoprophos 1.04 ppm 1.00 104 52-150

Etofenprox 0.81 ppm 1.00 81.2 60-139

Etoxazole 0.94 ppm 1.00 94.2 59-122

Fenoxycarb 1.23 ppm 1.00 123 39-146

Fenpyroximate 0.85 ppm 1.00 84.9 44-147

Fipronil 1.24 ppm 1.00 124 40-143

Flonicamid 1.73 ppm 1.00 173 50-142

Fludioxonil 0.54 ppm 1.00 54.0 49-150

Hexythiazox 1.00 ppm 1.00 100 41-142

Imazalil 1.16 ppm 1.00 116 61-127

Imidacloprid 0.82 ppm 1.00 82.2 36-150

Kresoxim-methyl 0.93 ppm 1.00 93.4 53-131

Malathion 0.96 ppm 1.00 95.7 55-134

Metalaxyl 1.06 ppm 1.00 106 64-127

Methiocarb 0.98 ppm 1.00 98.5 53-144

Methomyl 1.40 ppm 1.00 140 47-141

Methyl parathion 1.09 ppm 1.00 109 48-142

MGK-264 0.81 ppm 0.630 129 38-150

Myclobutanil 1.23 ppm 1.00 123 45-146

Naled 0.81 ppm 1.00 80.5 28-113

Oxamyl 1.00 ppm 1.00 99.9 48-133

Paclobutrazol 1.26 ppm 1.00 126 37-150




Page 9 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control





Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Permethrins (total) 1.24 ppm 46-150

Phosmet 1.17 ppm 1.00 117 48-137

Piperonyl butoxide 0.93 ppm 1.00 93.5 43-142

Prallethrin 1.16 ppm 1.00 116 48-144

Propiconazole 0.98 ppm 1.00 97.8 52-136

Propoxur 0.83 ppm 1.00 83.4 61-131

Pyrethrins (total) 0.88 ppm 24-150

Pyridaben 0.90 ppm 1.00 89.8 40-150

Spinosad 0.65 ppm 0.820 78.9 42-148

Spiromesifen 0.98 ppm 1.00 97.5 38-150

Spirotetramat 0.93 ppm 1.00 92.7 37-132

Spiroxamine 0.58 ppm 0.550 105 49-136

Tebuconazole 1.15 ppm 1.00 115 46-142

Thiacloprid 0.84 ppm 1.00 83.9 48-150

Thiamethoxam 1.51 ppm 1.00 151 46-138

Trifloxystrobin 0.80 ppm 1.00 80.0 44-144

Matrix Spike(B190400-MS1) Extracted - 03/12/19 9:31 Analyzed - 03/13/19 3:32


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 1.91 ppm 1.76 109 15-150< LOQ

Acephate 1.85 ppm 1.80 103 45-130< LOQ

Acequinocyl 1.00 ppm 1.80 55.8 31-146< LOQ

Acetamiprid 1.44 ppm 1.80 80.2 39-150< LOQ

Aldicarb 1.54 ppm 1.80 85.7 47-143< LOQ

Azoxystrobin 1.60 ppm 1.80 89.2 21-150< LOQ

Bifenazate 2.12 ppm 1.80 118 31-150< LOQ

Bifenthrin 0.85 ppm 1.80 47.1 23-132< LOQ

Boscalid 2.29 ppm 1.80 127 41-141< LOQ

Carbaryl 1.94 ppm 1.80 108 60-125< LOQ

Carbofuran 1.33 ppm 1.80 74.1 57-136< LOQ

Chlorantraniliprole 1.67 ppm 1.80 92.8 32-145< LOQ

Chlorfenapyr 2.04 ppm 1.80 114 29-150< LOQ

Chlorpyrifos 2.09 ppm 1.80 116 29-146< LOQ

Clofentezine 1.88 ppm 1.80 105 48-128< LOQ

Cyfluthrin 2.40 ppm 1.80 134 16-150< LOQ




Page 10 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control





Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Cypermethrin 1.91 ppm 1.80 106 22-150< LOQ

Daminozide 2.27 ppm 1.80 126 34-150< LOQ

DDVP (Dichlorvos) 1.81 ppm 1.80 101 55-133< LOQ

Diazinon 1.94 ppm 1.80 108 54-126< LOQ

Dimethoate 1.95 ppm 1.80 109 60-129< LOQ

Ethoprophos 1.81 ppm 1.80 101 40-150< LOQ

Etofenprox 0.84 ppm 1.80 46.7 25-135< LOQ

Etoxazole 1.59 ppm 1.80 88.5 26-149< LOQ

Fenoxycarb 2.17 ppm 1.80 121 37-145< LOQ

Fenpyroximate 1.86 ppm 1.80 103 27-150< LOQ

Fipronil 1.82 ppm 1.80 101 27-150< LOQ

Flonicamid 3.21 ppm 1.80 178 46-139< LOQ

Fludioxonil 1.65 ppm 1.80 91.7 31-150< LOQ

Hexythiazox 2.17 ppm 1.80 121 32-150< LOQ

Imazalil 2.12 ppm 1.80 118 44-142< LOQ

Imidacloprid 1.51 ppm 1.80 83.9 23-150< LOQ

Kresoxim-methyl 1.63 ppm 1.80 90.7 49-130< LOQ

Malathion 1.70 ppm 1.80 94.6 25-150< LOQ

Metalaxyl 1.90 ppm 1.80 106 49-141< LOQ

Methiocarb 1.70 ppm 1.80 94.6 44-146< LOQ

Methomyl 2.52 ppm 1.80 140 44-136< LOQ

Methyl parathion 1.79 ppm 1.80 99.8 15-150< LOQ

MGK-264 1.34 ppm 1.13 118 22-150< LOQ

Myclobutanil 2.18 ppm 1.80 121 34-150< LOQ

Naled 1.70 ppm 1.80 94.5 38-142< LOQ

Oxamyl 1.80 ppm 1.80 100 40-132< LOQ

Paclobutrazol 2.13 ppm 1.80 118 29-147< LOQ

Permethrins (total) 1.46 ppm 27-104< LOQ

Phosmet 2.04 ppm 1.80 114 35-150< LOQ

Piperonyl butoxide 1.62 ppm 1.80 90.3 34-143< LOQ

Prallethrin 2.03 ppm 1.80 113 33-150< LOQ

Propiconazole 1.70 ppm 1.80 94.7 46-138< LOQ

Propoxur 1.40 ppm 1.80 78.1 50-138< LOQ

Pyrethrins (total) 1.32 ppm 21-150< LOQ

Pyridaben 1.24 ppm 1.80 69.1 39-150< LOQ




Page 11 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control





Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Spinosad 1.12 ppm 1.47 76.3 31-150< LOQ

Spiromesifen 1.72 ppm 1.80 95.4 27-141< LOQ

Spirotetramat 1.73 ppm 1.80 96.4 31-141< LOQ

Spiroxamine 1.10 ppm 0.989 112 57-139< LOQ

Tebuconazole 1.90 ppm 1.80 106 32-140< LOQ

Thiacloprid 1.44 ppm 1.80 80.0 45-150< LOQ

Thiamethoxam 2.71 ppm 1.80 151 40-141< LOQ

Trifloxystrobin 1.40 ppm 1.80 77.6 30-137< LOQ

Matrix Spike Dup(B190400-MSD1) Extracted - 03/12/19 9:31 Analyzed - 03/13/19


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 1.81 ppm 1.79 101 15-150< LOQ 7.35 40

Acephate 1.89 ppm 1.83 103 45-130< LOQ 0.224 26

Acequinocyl 1.20 ppm 1.83 65.5 31-146< LOQ 16.1 50

Acetamiprid 1.59 ppm 1.83 86.9 39-150< LOQ 8.07 21

Aldicarb 1.68 ppm 1.83 91.7 47-143< LOQ 6.81 30

Azoxystrobin 1.50 ppm 1.83 81.7 21-150< LOQ 8.67 21

Bifenazate 2.06 ppm 1.83 112 31-150< LOQ 4.64 20

Bifenthrin 0.82 ppm 1.83 44.8 23-132< LOQ 4.92 30

Boscalid 2.09 ppm 1.83 114 41-141< LOQ 10.8 20

Carbaryl 1.93 ppm 1.83 105 60-125< LOQ 2.57 20

Carbofuran 1.46 ppm 1.83 79.6 57-136< LOQ 7.17 24

Chlorantraniliprole 1.56 ppm 1.83 85.0 32-145< LOQ 8.77 20

Chlorfenapyr 1.79 ppm 1.83 97.9 29-150< LOQ 14.8 50

Chlorpyrifos 2.05 ppm 1.83 112 29-146< LOQ 3.43 24

Clofentezine 1.92 ppm 1.83 105 48-128< LOQ 0.302 20

Cyfluthrin 2.33 ppm 1.83 127 16-150< LOQ 4.86 50

Cypermethrin 1.81 ppm 1.83 98.8 22-150< LOQ 6.98 30

Daminozide 2.39 ppm 1.83 131 34-150< LOQ 3.53 30

DDVP (Dichlorvos) 1.98 ppm 1.83 108 55-133< LOQ 7.51 30

Diazinon 2.02 ppm 1.83 110 54-126< LOQ 1.93 20

Dimethoate 1.99 ppm 1.83 108 60-129< LOQ 0.126 20

Ethoprophos 1.75 ppm 1.83 95.9 40-150< LOQ 5.07 29

Etofenprox 0.82 ppm 1.83 44.6 25-135< LOQ 4.60 24

Etoxazole 1.55 ppm 1.83 84.7 26-149< LOQ 4.30 30




Page 12 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



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Quality Control



Matrix Spike Dup(B190400-MSD1) Extracted - 03/12/19 9:31 Analyzed - 03/13/19


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Fenoxycarb 2.10 ppm 1.83 115 37-145< LOQ 5.14 23

Fenpyroximate 1.75 ppm 1.83 95.9 27-150< LOQ 7.45 20

Fipronil 1.74 ppm 1.83 94.9 27-150< LOQ 6.69 28

Flonicamid 3.25 ppm 1.83 178 46-139< LOQ 0.333 29

Fludioxonil 1.19 ppm 1.83 64.8 31-150< LOQ 34.4 30

Hexythiazox 2.09 ppm 1.83 114 32-150< LOQ 5.73 28

Imazalil 2.07 ppm 1.83 113 44-142< LOQ 4.24 25

Imidacloprid 1.51 ppm 1.83 82.5 23-150< LOQ 1.61 30

Kresoxim-methyl 1.66 ppm 1.83 90.5 49-130< LOQ 0.192 20

Malathion 1.65 ppm 1.83 90.0 25-150< LOQ 5.02 21

Metalaxyl 1.86 ppm 1.83 101 49-141< LOQ 3.98 20

Methiocarb 1.63 ppm 1.83 89.0 44-146< LOQ 6.08 20

Methomyl 2.58 ppm 1.83 141 44-136< LOQ 0.490 30

Methyl parathion 1.84 ppm 1.83 100 15-150< LOQ 0.541 50

MGK-264 1.31 ppm 1.15 113 22-150< LOQ 4.44 24

Myclobutanil 2.12 ppm 1.83 116 34-150< LOQ 4.33 23

Naled 1.64 ppm 1.83 89.4 38-142< LOQ 5.53 25

Oxamyl 1.83 ppm 1.83 100 40-132< LOQ 0.154 30

Paclobutrazol 2.05 ppm 1.83 112 29-147< LOQ 5.10 20

Permethrins (total) 1.48 ppm 27-104< LOQ 30

Phosmet 1.96 ppm 1.83 107 35-150< LOQ 6.09 20

Piperonyl butoxide 1.53 ppm 1.83 83.5 34-143< LOQ 7.79 21

Prallethrin 2.02 ppm 1.83 110 33-150< LOQ 2.34 25

Propiconazole 1.73 ppm 1.83 94.7 46-138< LOQ 0.0143 20

Propoxur 1.51 ppm 1.83 82.7 50-138< LOQ 5.77 28

Pyrethrins (total) 1.27 ppm 21-150< LOQ 28

Pyridaben 1.20 ppm 1.83 65.5 39-150< LOQ 5.32 23

Spinosad 1.13 ppm 1.50 75.6 31-150< LOQ 0.878 30

Spiromesifen 1.67 ppm 1.83 91.5 27-141< LOQ 4.17 30

Spirotetramat 1.64 ppm 1.83 89.6 31-141< LOQ 7.33 25

Spiroxamine 1.00 ppm 1.01 99.6 57-139< LOQ 11.3 20

Tebuconazole 1.95 ppm 1.83 106 32-140< LOQ 0.513 20

Thiacloprid 1.59 ppm 1.83 86.7 45-150< LOQ 7.99 21

Thiamethoxam 2.75 ppm 1.83 150 40-141< LOQ 0.249 30

Trifloxystrobin 1.37 ppm 1.83 74.9 30-137< LOQ 3.51 29




Page 13 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis

Batch: B190399 - Potency/Terpenes



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

alpha Pinene < LOQ %

Myrcene < LOQ %

alpha Phellandrene < LOQ %

3-Carene < LOQ %

alpha Terpinene < LOQ %

Limonene < LOQ %

Terpinolene < LOQ %

Linalool < LOQ %

Fenchol < LOQ %

Borneol < LOQ %

Terpineol < LOQ %

Geraniol < LOQ %

alpha Humulene < LOQ %

beta Caryophyllene < LOQ %

Caryophyllene Oxide < LOQ %

alpha Bisabolol < LOQ %

Camphene < LOQ %

beta Pinene < LOQ %

Ocimene < LOQ %

Sabinene < LOQ %

Camphor < LOQ %

Isoborneol < LOQ %

Menthol < LOQ %

alpha Cedrene < LOQ %

Nerolidol < LOQ %

R-(+)-Pulegone < LOQ %

Eucalyptol < LOQ %

p-Cymene < LOQ %

(-)-Isopulegol < LOQ %

Geranyl Acetate < LOQ %

Guaiol < LOQ %

Valencene < LOQ %

Phytol 0.305 %

Citronellol < LOQ %

gamma-Terpinene < LOQ %




Page 14 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis (Continued)




Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

alpha Ocimene < LOQ % < LOQ 20

alpha Terpineol 0.063 % 0.070 11.4 20

beta Ocimene < LOQ % < LOQ 20

beta Terpineol < LOQ % < LOQ 20

cis-Nerolidol 0.040 % 0.044 8.96 20

Phytol 1 < LOQ % < LOQ 20

Phytol 2 0.044 % 0.053 18.3 20

trans-Nerolidol 0.096 % 0.107 10.2 20

alpha Pinene 0.059 % 0.065 10.3 20

Myrcene 0.502 % 0.564 11.5 20

alpha Phellandrene < LOQ % < LOQ 20

3-Carene < LOQ % < LOQ 20

alpha Terpinene < LOQ % < LOQ 20

Limonene 0.725 % 0.796 9.24 20

Terpinolene 0.025 % 0.028 12.0 20

Linalool 0.172 % 0.187 8.46 20

Fenchol 0.062 % 0.068 9.20 20

Borneol 0.023 % 0.026 11.4 20

Terpineol 0.063 % 0.070 11.4 20

Geraniol 0.042 % 0.048 12.2 20

alpha Humulene 0.159 % 0.177 10.5 20

beta Caryophyllene 0.480 % 0.536 11.0 20

Caryophyllene Oxide 0.019 % 0.020 6.80 20

alpha Bisabolol 0.044 % 0.050 12.4 20

Camphene 0.019 % 0.020 4.68 20

beta Pinene 0.109 % 0.121 10.1 20

Ocimene < LOQ % < LOQ 20

Sabinene < LOQ % < LOQ 20

Camphor < LOQ % < LOQ 20

Isoborneol < LOQ % < LOQ 20

Menthol < LOQ % < LOQ 20

alpha Cedrene < LOQ % < LOQ 20

Nerolidol 0.137 % 0.151 9.86 20

R-(+)-Pulegone 0.023 % 0.022 2.72 20

Eucalyptol < LOQ % < LOQ 20




Page 15 of 18 03/14/2019 16:21

Brian Weigel

Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis (Continued)




Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

p-Cymene < LOQ % < LOQ 20

(-)-Isopulegol < LOQ % < LOQ 20

Geranyl Acetate 0.021 % 0.022 6.41 20

Guaiol < LOQ % < LOQ 20

Valencene 0.101 % 0.105 3.97 20

Phytol 0.044 % 0.053 18.3 20

Citronellol < LOQ % < LOQ 20

gamma-Terpinene < LOQ % < LOQ 20

Batch: B190401 - Gravimetric



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Percent Moisture 10.0 % 10.0 0.0996 20

Batch: B190402 - Water Activity



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Water Activity 0.544 AW 0.550 1.10 20




Page 16 of 18 03/14/2019 16:21

Brian Weigel

Lab Director

Client: Western Oregon Botanicals Client License: 02010021071d94 Date Sampled: 3/8/2019 Thermometer ID: T014

Address Where

Sampled:Requestor: Abdullah Naimi Event ID: 19C0028 Balance ID: SAMP_BAL_02

Sampler Signature

Sampling SOP & Rev.

#:SC-OR-SAMP-003 Sampler: Scott Forster Transporter: Scott Forster Hygrometer ID: Anemometer_02

Lab ORELAP ID: 4133 Weight used (g) Weight Set IDAcceptance

CriteriaInitial Measured Initial P/F Final Measured Final P/F

Lab OLCC ID: 1004748743D 0.5 SAMP_CAL_02 ±2.5% 0.5 0.5

200 ±2.5% 200 200

Container Type METRC Harvest/Processing Lot ID #: Product Type Client Sample Name Product Date Batch Size (g)

storage tubs 43514 Usable Marijuana Super Glue 2/18/2019 4540

METRC Batch IDProduct Temp

(°C)Humidity (%) # of Containers Sampling Media # Zones # of Inc.

1° Sample Size

(g)Sample Name

1a40103000098bf000001499 16.3 44.9 1 mylar bag 4 9 2.7 Super Glue Primary

Container ID Increment ZoneSampling

Media Wt. (g)Wt. Inc+Media (g)

Increment

Weight (g)Sample METRC ID#

19C0028-01 Super Glue-1 A1 0 2.7 2.7 1504

19C0028-01 Super Glue-1 A1 2.7 5.4 2.7 1504

19C0028-01 Super Glue-1 A1 5.4 8.1 2.7 1504

19C0028-01 Super Glue-1 A2 8.1 10.8 2.7 1504

19C0028-01 Super Glue-1 A2 10.8 13.5 2.7 1504

19C0028-01 Super Glue-1 A3 13.5 16.2 2.7 1504

19C0028-01 Super Glue-1 A4 16.2 18.9 2.7 1504

19C0028-01 Super Glue-1 A4 18.9 21.6 2.7 1504

19C0028-01 Super Glue-1 A4 21.6 24.47 2.87 1504

Totals:Minimum Sample Size = 22.7g (Usable

Marijuana Only)9 Total Sample Mass = 24.47

Batch # Equipment Cont. Types/Sizes Uniform Plant Colors Shape and Size Sampling Plan ID & Rev. Date

Observations and Abnormalities:

.


storage tubs 43514 Usable Marijuana PGSC 2/18/2019 2270



1° Sample Size

(g)Sample Name

1a40103000098bf000001500 16.3 44.9 4 mylar bag 4 8 1.6 PGSC Primary



Increment


19C0028-02 PGSC-1 A2 0 1.6 1.6 1505

19C0028-02 PGSC-1 A2 1.6 3.2 1.6 1505

19C0028-02 PGSC-2 B2 3.2 4.8 1.6 1505

19C0028-02 PGSC-2 B3 4.8 6.4 1.6 1505

19C0028-02 PGSC-2 B4 6.4 8 1.6 1505

19C0028-02 PGSC-3 C2 8 9.6 1.6 1505

19C0028-02 PGSC-3 C4 9.6 11.2 1.6 1505

19C0028-02 PGSC-4 D2 11.2 12.84 1.64 1505

P P

18270 SW Benton Rd Sherwood OR

Lab Sample ID

Lab Sample ID

Sampling Report Page 1 of 4

Form Page 1 of 1SC-OR-SAMP-010, Rev. 1.00

Issued by DoQA of 07/05/2018





.


storage tubs 43514 Usable Marijuana AJ 2/18/2019 1362



1° Sample Size

(g)Sample Name

1a40103000098bf000001501 16.3 44.9 1 mylar bag 4 7 1 AJ Primary



Increment


19C0028-03 AJ-1 A1 0 1 1 1506

19C0028-03 AJ-1 A2 1 2 1 1506

19C0028-03 AJ-1 A2 2 3 1 1506

19C0028-03 AJ-1 A2 3 4 1 1506

19C0028-03 AJ-1 A3 4 5 1 1506

19C0028-03 AJ-1 A4 5 6 1 1506

19C0028-03 AJ-1 A4 6 7.14 1.14 1506

Totals:Minimum Sample Size = 7g (Usable




.


storage tubs 43514 Usable Marijuana 9lb Hammer 2/18/2019 2724



1° Sample Size

(g)Sample Name

Lab Sample ID




1a40103000098bf000001502 16.3 44.9 1 mylar bag 4 8 1.9 9lb Hammer Primary



Increment


19C0028-04 9lb Hammer-1 A1 0 1.9 1.9 1507

19C0028-04 9lb Hammer-1 A1 1.9 3.8 1.9 1507

19C0028-04 9lb Hammer-1 A2 3.8 5.7 1.9 1507

19C0028-04 9lb Hammer-1 A2 5.7 7.6 1.9 1507

19C0028-04 9lb Hammer-1 A3 7.6 9.5 1.9 1507

19C0028-04 9lb Hammer-1 A4 9.5 11.4 1.9 1507

19C0028-04 9lb Hammer-1 A4 11.4 13.3 1.9 1507

19C0028-04 9lb Hammer-1 A4 13.3 15.45 2.15 1507





.


storage tubs 43514 Usable Marijuana Sirius Black 2/18/2019 2724



1° Sample Size

(g)Sample Name

1a40103000098bf000001503 16.3 44.9 1 mylar bag 4 8 1.9 Sirius Black Primary



Increment


19C0028-05 Sirius Black-1 A1 0 1.9 1.9 1508

19C0028-05 Sirius Black-1 A1 1.9 3.8 1.9 1508

19C0028-05 Sirius Black-1 A1 3.8 5.7 1.9 1508

19C0028-05 Sirius Black-1 A1 5.7 7.6 1.9 1508

19C0028-05 Sirius Black-1 A1 7.6 9.5 1.9 1508

19C0028-05 Sirius Black-1 A2 9.5 11.4 1.9 1508

19C0028-05 Sirius Black-1 A3 11.4 13.3 1.9 1508

19C0028-05 Sirius Black-1 A4 13.3 15.44 2.14 1508




Lab Sample ID

Lab Sample ID





.




sample name: sirius black tested for: western oregon … testing/rec... · 2019. 2. 18. ·...

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