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SCHEME AND DETAILED SYLLABUS
of
SE (Chemical Engineering)
Under Choice Based Credit & Grading System
(w.e.f. academic year 2017-18 & onwards/-)
FOUR YEAR DEGREE COURSE IN SCIENCE& TECHNOLOGY
Dr. BABASAHEB AMBEDKAR MARATHWADA UNIVERSITY,
AURANGABAD
3
Faculty of Science and Technology
Curriculum structure of S.E. (Chemical Engineering)
With effect from Academic Year: 2017-18 & onwards/-
PART-I
Sub Code Semester-I Contact Hrs/Week Examination Scheme Duration of The
Theory
Examination Subject L T P Total CT TH TW PR Total credits
BSH201 Engineering
Mathematics -III 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE202 Process Instrumentation
and Analytical
Techniques
4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE203 Mechanical Operation 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE204 Chemical Process
Calculation 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE205 Fluid Mechanics 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE221 Lab 1: Process
Instrumentation and
Analytical Techniques
-- -- 2 2 -- -- 50 -- 50 1
CHE222 Lab 2: Mechanical
Operation -- -- 2 2 -- -- -- 50 50 1
CHE223 Lab 3: Fluid Mechanics -- -- 2 2 -- -- -- 50 50 1
CHE224 Lab 4: Theory and
Drawing of Equipment -- -- 4 4 -- -- 50 -- 50 2
CHE225 Lab 5: Computer
Laboratory -- -- 2 2 -- -- -- 50 50 1
Total 20 -- 12 32 100 400 100 150 750 26
PART - II
Sub Code Semester-II Contact Hrs/Week Examination Scheme
Duration of
The Theory
Examination
Subject L T P Total CT TH TW PR Total Credits
BSH206 Engineering
Mathematics-IV 4 -- -- 4 20 80 -- -- 100 4 3 Hr
BSH207 Engineering chemistry 4 -- -- 4 20 80 -- -- 100 4 3 Hr
BSH208 Physical Chemistry and
Thermodynamics 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE209 Heat Transfer 4 -- -- 4 20 80 -- -- 100 4 3 Hr
CHE210 Strength of Material 4 -- -- 4 20 80 -- -- 100 4 3 Hr
BSH226 Lab 6: Engineering
chemistry -- -- 4 4 -- -- -- 50 50 2
BSH227 Lab 7: Physical
Chemistry and
Thermodynamics
-- -- 2 2 -- -- -- 50 50 1
CHE228 Lab 8: Heat Transfer -- -- 2 2 -- -- -- 50 50 1
CHE229 Lab 9: Strength of
Material -- -- 2 2 -- -- 50 -- 50 1
CHE230 Lab 10: Communication
Skills- I -- -- 2 2 -- -- 50 -- 50 1
Total 20 -- 12 32 100 400 100 150 750 26
Total of Semester I & II 40 24 64 200 800 200 300 1500 52
L: Lecture hours per week T: Tutorial hours per week P: Practical hours per week
CT: Class Test, TH: University Theory Examination,TW: Term Work, PR: Practical/Oral Examination
4
BSH-201: ENGINEERING MATHEMATICS-III
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test: 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
• TodevelopLogicalunderstandingofthesubject.
• Todevelopmathematical skill sothatstudentsareabletoapply
mathematicalmethods&Principle’sinsolving problemsfrom Engineeringfields.
• Toproducegraduateswithmathematicalknowledge&computationalskill.
Unit1 [8 Hrs]
LinearDifferentialEquations:
LinearDifferential Equationswithconstant coefficients Generalmethod, shortcutmethods
tofindparticularintegral,
HomogenousLineardifferentialequations(Cauchy’s&Legendre’sform),methodofvariation
ofparameters.
Unit2 [6Hrs]
Application o fL i n e a r DifferentialEquations:
Application o fL i n e a r DifferentialEquations to Electrical circuits & to Mechanical system
(Analogous study of two systems), to Civil Engineering, Free oscillations/vibrations, forced
oscillation /vibrations, Damped Free oscillations / vibrations, Damped Forced oscillations /
vibrations.
Unit3 [6Hrs]
Fourier Transform:
Fourier Transform, Fourier sine and cosine transform, Fourier integral, Fourier sine and cosine
integral.
Unit4 [8 Hrs]
Statistics&Probability: Measures of central
Tendency and Measures of Dispersion (for grouped data only), Karl Pearson’s coefficient of
skewness, Probability distribution for random variables, Binomial and Normal Distributions
Regression and Correlation.
Unit 5 [6 Hrs]
VectorDifferentiation Differentiation of
vectors, Gradient of scalar point function, Directional derivative, Divergence of vector point
function, Curl of a vector point function. Irrotational and solenoidal vector field.
Unit6: [6Hrs]
5
VectorCalculus(Integralcalculus)
The line integral, Surface integral, volume integral, Gauss Divergence theorem, Stoke’s theorem,
Green’s theorem (All theorem without proof).
Note:
SectionA:Unit1,2,3
SectionB:Unit4,5,6
Text Books:
1. P.N.WartikarandJ.N.Wartikar,“ATextBookofEngineering Mathematics”(Volume-I, II,III)
PuneVidyarthi GrihaPrakashan,Pune.
2. B.S.Grewal,“Higher EngineeringMathematics,”Khanna Publications,NewDelhi.
3. H. K.Das,“AdvancedEngineeringMathematics,” S.Chand&Company.
ReferenceBooks:
1. B.V.Ramana,“HigherEngineeringMathematics,”(Tata McGraw- Hill).
2. ErwinKreyszig, “AdvancedEngineeringMathematics,”Wiley EasternLtd.
3. RavishR Singh,MukulBhat,“EngineeringMathematics,”ATutorial Approach,McGrawHill
4. S.C. Gupta and V.K. Kapoor,“Fundamentals of Mathematical Statistics” byS. Chand and
Sons
PatternofQuestionPaper:
Theunitsinthesyllabusshallbedividedintwoequalsections.Questionpapershallbesethavingtwosectio
nsAandB.SectionAquestionsshallbeset onfirstthreeunits(1,2,3)
andSectionBquestionsonremainingthreeunits(4,5,6). Questionpapershouldcovertheentiresyllabus.
For80marksPaper:
1. Minimumtenquestions
2. Fivequestionsineachsection
3. Question no1and6bemadecompulsoryandshouldhaveatleast EIGHTbits
oftwomarksoutofwhichFIVEtobesolved.
4. Twoquestionsfromremainingquestionsfromeachsectionbe
askedtosolvehavingweightageof15marks.
6
CHE-202: PROCESS INSTRUMENTATION AND ANALYTICAL TECHNIQUES
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test: 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop understanding of the principles of measurement.
2) To understand the instruments and analytical method using in process industries.
Unit I [6 Hrs]
Principles of measurement, elements of instruments, static and dynamic characteristics, response
of first and second order instruments. Process Instrumentation. Recording, indicating, signaling
instruments. Principles of transductions, Transducers & their classification. Elastic, Resistance,
Capacitive & Inductive transducers for temperature, level, flow and pressure measurements.
Instrumentation diagrams.
UnitII [8 Hrs]
Constructional details, working principles and response characteristics of, temperature measuring
instruments like expansion thermometers, thermocouples,thermister, resistance thermometer,
pyrometers, etc.
Unit III [6 Hrs]
Constructional details, working principles and response characteristics of, pressure and vacuum
measuring devices (instruments) like pressure gauge, McLeod gauge, etc. Head and Level
measuring devices. Review of flow meters (orifice meter, venturi meter, rotameter.
Unit IV [8 Hrs]
Importance, scope & methods of sampling of solids, liquids, gaseous materials, industrial &
laboratory techniques. Tools of the analyst, general procedures, preliminaries to the analyst.
Theory of indicators. Gas analysis,Introduction theory, instrumentation and application of
Visible Spectrophotometry, Colorimetry, Infrared Spectroscopy, Conductometry &
conductometric titration, Potentiometry.
Unit V [6 Hrs]
Introduction theory, instrumentation and application of Flame Photometry, Polarography,
Amperometric titration, Coulometric technique & titration.
Unit VI [6 Hrs]
Introduction theory, instrumentation and application of Karl-Fischer titrimetry, Gas
chromatography, thin layer chromatography.
7
Reference Book:
1. Industrial Instrumentation by Donald P. Eckrnan, Wiley Eastern Ltd.
2. Principles of Industrial Instrumentation by D. Patranabis, Tata -McGraw Hill Co.
3. Instrumental Methods in Chemical Analysis by G.W.Ewing, Mc Graw Hill Co.
4. Instrumental Methods in Chemical Analysis by Chatwal and Anand.
5. Instrumental Methods in Chemical Analysis by B.K.Sharma
6. Quantitative Inorganic Analysis by A. I. Vogel
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6) Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out of
which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve
havingweightage of 15 marks
8
CHE-203: MECHANICAL OPERATIONS
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test: 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop understanding of the principles of unit operations.
2) To understand calculations and principles related to chemical processes.
Unit 1 [6 Hrs]
Size Reduction:
Law of Size reduction, types of equipment used and their selection. Open and Closed Circuit
Operation, Crushers, Ball Mill, Rod Mill etc. Energy relationship in size reduction.
Unit 2 [8 Hrs]
Particle size analysis and Separation:
Methods of representation of size analysis, sub sieve methods of analysis, surface area
determination. Theory of screening and size distribution, different type of screening equipments,
mesh number, cumulative screening, effectiveness factor, screening effectiveness.
Unit 3 [6 Hrs]
Storage and Transportation of Solids:
Storage of solids; Bunkers, Silos, Bins, Hoppers and handling of solids. Transportation of solids,
conveying, types of conveyors and performances.
Unit 4 [8 Hrs]
Sorting:
Separation of solids, Gravity concentrationmethods. Jigging, Principles of jigging, types of jiggs,
their performances, characteristics. Froth flotation- Principles and Theories of collection,
flotation cell, typical circuits, magnetic and electrical separation.
Unit 5 [10 Hrs]
Solid-Liquid Separation:
Filtration- filtration theory, equipments for filtration, constant pressure and constant rate
filtration, optimum cycle, use of filter aids, equipment for liquid solid filtration. Agitated
Nutsche filters. Micro and ultrailtration, reverse osmosis. Centrifugal separations - Principle.
Thickening - Batch and Continuous thickeners Classification, types of classifiers, mechanical
and non mechanical, pneumatic, Cyclone separation, theory, principle.
Unit 6 [4 Hrs]
Mixing :
Mixers & mixing, Agitators & agitation, Flow patters in agitated vessels, flow numbers, power
consumption and mixing index.
9
Reference Books:
1. Unit Operations of Chemical Engineering, W. L. McCabe & J.M. Smith, et al McGraw Hill
Publication.
2. Chemical Engineering Vol.-I & II, J. F. Richardson J. M. Coulson, Pergamon Press
Publication.
3. Introduction to Chemical Engineering, W. L. Badger and J. T. Banchero McGraw Hill
Publication.
4. Principles of Unit Operations, A. S. Foust et al John Wiley & Sons Publications.
5. Chemical Engineers Hand book, R. H. Perry, McGraw Hill Publication.
6. Chemical Engineering mechanical operations by Hiramath and A.P. Kulkarni.
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6) . Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out of
which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
10
CHE-204: CHEMICAL PROCESS CALCULATIONS
Teaching Scheme Examination Scheme
Lectures 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop Logical understanding of the subject
2) To understand fundamental calculations and principles related to chemical processes.
3) To produce graduates with knowledge of making basic chemical engineering calculations.
UNIT 1 [6 Hrs]
Introduction to Process Calculations. Basic & derived units, Stoichiometric relations, different
ways of expressing the composition of mixtures and solutions. Properties of Gases Liquids &
Solids: Ideal & real gas laws. Critical properties, properties of mixtures & solution, phase
Equilibria, phase rule. Laws of Dalton & Amagat and their applications. Vapor pressure:
vaporization, effect of temperature on vapor pressure, vapor pressure plot, Estimation of critical
properties. vapor pressure of immiscible liquids solutions, Raoult’s law.
UNIT 2 [6 Hrs]
Humidity & Saturation:Humidity, Saturation, Dew point, Vaporization & Condensation
processes, Wet & Dry bulb thermometry. Psychometric chart, Solubility diagrams. Thermo
physics: Heat capacity of gases, liquids, solids & solutions. Kopp’s rule, Latent heats, heat of
fusion & vaporization.
UNIT 3 [6 Hrs]
Material Balance: Concepts of limiting & excess reactants, recycle, purging, bypass in batch,
stage wise & continues operations in systems with & without chemical reaction in unit operation.
UNIT 4 [6 Hrs]
Thermo chemistry: Heats of formation, combustion, reaction, neutralization and their
applications. Heats of mixing solution. Dilution, the effect of pressure & temperature on them.
Temperature of reaction. Use of enthalpy concentration charts. Energy balances for system with
& without chemical reaction. Process efficiency.
UNIT 5 [8 Hrs]
Fuels and Combustion: Basic concepts. Types of fuels, heating values of fuels, theoretical &
excess air. Material and Energy balances- heat & combustion calculations.
UNIT 6 [6 Hrs]
Applications: Application of material and energy balance to typical chemical industrial
processes. Unsteady material balance & energy balances & its applications. (06 Hr)
11
Reference Books
1. Stoichiometry by Bhat B I & Vora S.M, Tata McGraw Hill Co. Ltd.
2. Basic Principles & Calculations in Chemical Engineering by Himmelblau D M. Prentice Hall
of India Ltd.
3. Chemical Process Principles Part I by Hougen D A & Watson K M John Wiley & Sons.
4. Chemical Engineering Vol 6, by Richardson & Coulson
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out of
which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
12
CHE-205: FLUID MECHANICS
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test: 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop Logical understanding of the subject.
2) To understand fundamental calculations and principles related to fluid flow in chemical
processes.
3) To produce graduates with knowledge of dynamics of fluid flow.
Unit 1 [8 Hrs]
Fluid Statics: Nature and properties of fluids, static fluid properties, hydrostatic equation,
barometric equation, hydrostatic equation in centrifugal fields, hydrostatic forces on plane and
curved surfaces, Buoyancy. Measurement of fluid pressure – manometers, Fluid flow
phenomenon: Types of fluid flow–shear stress and shear rate fields, viscosity and momentum
flux. Viscosity of gases and liquids, eddy viscosity.
Unit 2 [4 Hrs]
Flow of compressible fluids: Continuity equation, Total energy balance equation, mechanical
energy balance equation, Ideal gas equation, Velocity of sound, Sonic velocity, Mach Number.
Unit 3 [8 Hrs]
Basic equations of fluid flow: Basic equations of incompressible flow- conservation of mass
momentum and energy. Turbulence and nature of turbulence, Reynolds number, flow in
boundary layers. Boundary layer formation in straight tubes/ pipes, Boundary layer separation &
wake formation. One-dimensional flow, Euler’s equation and Bernoulli equation. Application of
basic equations of fluid flow.
Unit 4 [8 Hrs]
Flow of fluids: Flow of incompressible fluids through circular conduits, shear stress distribution,
and relation between skin friction and wall shear. The friction factor, relation between skin
friction parameters, laminar flow in pipes. Laminar and turbulent flow equations – average
velocity kinetic, energy correction factor. Hagen– Poiseuille equation. Turbulent flow in pipes
and closed channel, velocity distribution equation for laminar, sub layer, buffer layer and
turbulent core. Maximum and average velocity. Effect of roughness parameter. The friction
factor chart (Mood’s diagram), friction factor in flow through channels of non-circular cross
section, friction from changes in velocity or direction, effect of fittings and valves. Flow through
coils. Non –Newtonian fluid flow.
Unit 5 [6 Hrs]
Flow past immersed bodies: Boundary layer formation -Laminar and turbulent boundary layers.
Types of drag, drag coefficient and stream lining. Flow through solids, Ergun’s equation,
Kozney- Carmen equation, Blake Plummer equation. Mechanism of fluidization, types of
13
fluidization, minimum fluidization velocity. Applications of fluidization, Motion of particles
through fluids- free and hindered settling. Measurement of fluid flow by pitot tube, orifice meter,
venturimeter, rotameter
Unit 6 [6 Hrs]
Fluid flow machinery: Developed head, power requirement, suction lift & cavitation, NPSH.
Pumps & Compressors for chemical plants- reciprocating, rotary, centrifugal, airlift pumps,
blowers (their performance & characteristics. Pipeline in series and parallel flow problems.
Reference Books
1. Unit operations in Chemical Engineering by McCabe W L & Smith J C McGraw Hill Co.
2. Chemical Engineering Vol I by Richardson & Coulson
3. Fluid and Particle mechanics by Michele S J
4. Fluid Mechanics by A K Jain Khanna Publication
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out
of which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
14
CHE221 LAB-I PROCESS INSTRUMENTATION AND ANALYTICAL TECHNIQUES
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Term work: 50 Marks
Credit: 01
Term Work:
Term work shall consist of a Journal containing record of any eight experiments, at least four
from each section, performed from the following list of suggested experiments:
Section-A
1. Characteristics of thermocouple
2.Calculation of time constant of thermometer.
3. Characteristics of thermister
4. Characteristics of Resistance Temperature Detector.
5. Calculation of time constant of single liquid level tank.
6. Characteristic of Pressure gauge.
Section-B
1.Detennination of iron/ nickel spectrophotometrically.
2. Determination of sodium / calcium / potassium by flame photometer. ,
3. Determination of KMnO4 or acetic acid potentiometrically.
4. Identification and quantification of cadmium in a mixture by polarigraphy.
5. Separation of some amines by TLC or paper chromatography.
6. Identification and quantification of an organic compound by gas chromatography.
7. Determination of moisture content by Karl-fisher apparatus.
8. Determination of percentage of sugar / camphor / lactic acid in a solution by polarometer.
9. Analysis of fertilizer / drugs / milk by colorimeter.
15
CHE222 LAB-II MECHANICAL OPERATIONS
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Practical: 50 Marks
Credit: 01
Practical Work
Minimum eight experiments, based on the syllabus, should be conducted during the course and
record (Journal) for the same shall be submitted.
The practical examination shall consist of performing an experiment based on the practical work
done during the course, the record of the experiments to be submitted by the candidate and viva-
voce based on the syllabus.
Suggested List of Experiments:
1. The experiment be based on following list:
1. Sieve analysis.
2. Double deck Vibrating Screen.
3. Jaw crusher.
4. Pulveriser.
5. Ball mill.
6. Plate and frame filter.
7. Vacuum filter.
8. Batch settling.
9. Cyclone Separator.
10. Sigma mixer.
16
CHE223 LAB-III FLUID MECHANICS
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Practical: 50 Marks
Credit: 01
The term work syllabus consists of a record of minimum eight (laboratory experiments)
performed & completed during the term
Suggested list of experiments/studies:
1. To perform an experiment on venturimeter.
2. To perform an experiment on orifice meter.
3. To perform an experiment on flow of water through pipe.
4. To perform an experiment on flow of water through helical coil.
5. To perform an experiment on flow of water through spiral coil
6. To study the characteristics of centrifugal pump.
7. To study the characteristics of reciprocating pump.
8. To determine reflux time of a tank and funnel.
9. To study the velocity profile of fluid in pipe/duct.
10. To study flow of fluid through packed bed.
11. To study flow of fluid through fluidized bed.
12. Determination of viscosity
13. Verification of Bernoulli's theorem
17
CHE224 LAB-IV THEORY AND DRAWING OF EQUIPMENT
Teaching Scheme Examination Scheme
Practical: 4 Hrs/Week Term work: 50 Marks
Credit: 02
Note:
1. The theoretical concepts and design in this subject is to be taught in the practical class.
2. The practical classes are to be conducted in a drawing hall.
3. The duration for each batch of students attending the practical class is 04 (four) hours, out of
which 01(one) hour is to be spent on teaching the theoretical concepts and 03 (three) hours
are to be given to the students to complete the drawings on a drawing sheet.
4. Along with the theory & design, drawing of simple parts of machines and ability of supply
additional views is expected.
5. Stress should be given with reference to chemical industry applications.
List of Practical:
Total five sheets should be completed based on the following topics.
1. Standard equipment symbol
2. Standard instrumentation symbol
3. Process flow-sheet based on 1.and 2.
4. Pipe joints and pipe fittings.
5. Types of valves – Gate valve, Globe valve, etc.
6. Types of Joints
7. Types of threads and fastenings
8. Keys and Coupling
The practical examination shall consist of a viva-voce based on theory and drawing work done
during the course and on the syllabus.
18
CHE225 LAB-IV COMPUTER LABORATORIES
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Practical: 50 Marks
Credit: 01
Term work shall consist of a record of minimum eight executable programming assignments
using C or C++ language dedicated to "Applications in Chemical Engineering" and based on
following numerical techniques.
1. Root finding methods (bisection, secant, regular-false, Newton Raphson), for algebraic and
transcendental equations.
2. Interpolation and extrapolation.
3. Numerical Integration and differentiation.
4. Curve fitting.
5. Matrix operations (Addition, subtraction, multiplication, inverse) for solution of
simultaneous linear algebraic equation arising in chemical engineering.
Emphasis is to be given on numerical techniques. Students should be made aware of advantages
and disadvantages of One method over other, wherever possible.
The term work will be a continuous assessment based on: 1. Program compiled by the student in
the computer laboratory. 2. The record of the experiments submitted by the student. 3. An oral
examination / viva-voce (conducted internally) on the syllabus and the term work mentioned
above.
The practical examination shall consist of a viva-voce based on numerical techniques done
during the course and on the syllabus.
Reference Books
For Numerical Methods:
1. Computer oriented numerical methods by Rajaraman V.
2. Numerical methods by Balchandra R.S.
3. Numerical methods with C++ programming by Somasundaram R.M.
4. Numerical methods for Engineering problems by Krishna R.N.
5. Lean Lapidus. "Digital Computation for Chemical Engineers". McGrawHill Publication,
1962.
For C Programming:
1. Let us C by Yeshwant Kanitkar
2. The C programming language by Karnighan B.W.
3. Programming in C by Stepken G. Kochan
For C++ Programming:
1. The complete reference in C++ 3rd
edition by Herbert Schidlt, Tata McGraw hill.
2. Object oriented programming in turbo C++ by Robert Lafore.
19
BSH-251: ENGINEERING MATHEMATICS-IV
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
• To develop Logical understanding of the subject
• To developmathematical skill so that students are able to apply mathematical methods &
Principal’s in solving problems from Engineering fields
• To produce graduates with mathematical knowledge & computational skill.
Unit1 [6 Hrs]
Laplace Transform:
Definition,Transfor
mofelementaryfunctions, Properties& theorems of Laplace transforms (without proof),
transforms of periodic function,
Heavisideunitstepfunction,displacedunitstepfunction,Diracdeltafunction,errorfunction,
Bessel’functionofzeroorder.
Unit2 [6 Hrs]
InverseLaplace TransformanditsApplications:
Inverse Laplace transforms by using (i) properties, ii) partial fractions, iii) Convolution theorem,
Applications to solve linear differential equations with constant coefficients (Initial value
problems), Simultaneous Linear differential equations.
Unit3 [8 Hrs]
Z Transform:
Definition,Ztransformofelementaryfunctions,propertiesofZ transform,InverseZtransform by
using partial fraction and residues theorem,SolutionofdifferenceequationbyZtransform.
Unit4 [8 Hrs]
NumericalMethods and Curve Fitting:
Solution of transdental equations by Newton Raphson method, Gauss Seidel method to solve
simultaneous linear equations, Lagranges interpolation formula for unequal intervals, numerical
differentiation: Newton’s forward and Newton’s Backward difference formulae, Solution of
ordinary differential equation by Eular modified Method and Runge-Kutta IVth order method,
Curve fitting: Principle of least squares, Fitting of linear curve, parabola, exponential curve.
Unit5 [6 Hrs]
FunctionofComplexVariable(Differentialcalculus):
Introduction,AnalyticfunctionCauchy Riemann equationsinCartesian andPolarform,Harmonic
function,Laurent’sseries (withoutproof),Conformalmapping: Translation, Magnification,
Rotation and inversionbilinear transformation.
20
Unit6 [6 Hrs]
Function ofComplex Variable(Integral calculus):
Line integral, contour
integral:Cauchy’sintegraltheorem,Cauchy’sintegralformulaResidues,Cauchy’sresiduetheorem(Al
l theorems withoutproof).
Note:
SectionA:Unit1,2,3
SectionB:Unit4,5,6
Text Books:
1. P.N.WartikarandJ.N.Wartikar,“ATextBookofEngineering Mathematics(Volume-I, II,III)
PuneVidyarthi GrihaPrakashan,Pune.
2. B.S.Grewal,“HigherEngineeringMathematics,”Khanna Publications,NewDelhi.
3. H. K.Das,“AdvancedEngineeringMathematics,” S.Chand&Company.
ReferenceBooks:
1. B.V.Ramana,“HigherEngineeringMathematics,”(Tata McGraw-Hill).
2. Erwin Kreyszig,“AdvancedEngineeringMathematics,”WileyEastern Ltd.
3. RavishR Singh, Mukul Bhat, “Engineering MathematicsATutorial
Approach,”by,McGrawHill
PatternofQuestionPaper:
Theunitsinthesyllabusshallbedividedintwoequalsections.Questionpapershallbesethavingtwosectio
nsAandB.SectionAquestionsshallbesetonfirstthreeunits(1,2,3)andSectionBquestionsonremaining
threeunits(4,5,6).Questionpapershouldcoverthe entiresyllabus.
For80marksPaper:
1. Minimumtenquestions
2. Fivequestionsineachsection
3. Questionno1and6bemadecompulsoryandshouldhaveatleastEIGHTbitsoftwomarksout
ofwhichFIVEtobesolved.
4. Twoquestionsfromremainingquestionsfromeachsectionbeaskedtosolvehaving weightageof
15marks
21
BSH-207: ENGINEERING CHEMISTRY
Teaching Scheme Examination Scheme
Lectures: 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test: 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop understanding related to synthesis of organics
2) To produce graduates with knowledge of reaction mechanism & synthetic chemistry.
Unit 1 [8 Hrs]
AromaticHydrocarbons:
Preparation, Properties and uses of Benzene, Naphthalene and Anthracene, Structure
determination of benzene. Heterocyclic Compounds: Preparation, properties and uses of: Pyrrole,
Thiophene, Furan, Pyridine and Quinolene.
Unit 2 [8 Hrs]
Carbohydrates & Dyes:
Manufacture of Sucrose and Glucose, their reaction and structure determination and industrial
use.Dyes: Introduction, dyeing, isolation, constitution, synthesis and properties of (1) Indigotin
(2) Methyl Orange, (3) Alizarin. (4) Congored.
Unit3 [6 Hrs]
Amines:
Mono, Di and Tri amines, their general preparations, separations and reactions. Aniline and
diazotization reaction. General properties of diazonium salts.
Unit 4 [8 Hrs]
Study of the following unit processes: Nitration:
Nitrating agents, Mechanism of nitration of aromatics, process equipments typical nitration
process for making nitrobenzene and chloronitrobenzene Sulphonation: Reagents for
sulphonation, mechanism of sulphonation of aromatics, preparation of aliphatic and aromatic
sulphonates and sulphates. Sulphonation of lauryl alcohol, dimethyl ether etc. Halogenation:
Reagents for halogenation, mechanism of halogenations of aromatics, preparation of
chlorobenzene, DDT, BHC etc. Uses of LiAIH4 and peracids.
Unit 5 [6 Hrs]
Reactions, mechanisms and Industrial applications:
Knoevanagel's reaction, Gatterman Koch reaction, Claisen rearrangement, Pinacol-Pinacolone
rearrangement, Michel reaction, Deckmann Condensation, Benzil-Benzilic acid rearrangement,
Beckmann Rearrangement.
22
Unit 6 [4 Hrs]
Chemistry of Natural products:
Simple turpines. General methods of extraction and separation, their physical and chemical
properties, Geranial and alpha-pinene
Reference Books:
1. Organic chemistry Vol-I & II by Finar IL
2. Text book of organic chemistry by Soni PI.
3. Unit processes in synthesis by Groggin P.H.
4. Organic chemistry by Morrison and Boyd.
5. Textbook on quantitative and qualitative organic chemistry by Vogel A. I
6. Organic Chemistry by O.P. Agrawal.
7. Pitter Sykes, Organic reactions and mechanism, Orient Longman-1986
8. Reaction, rearrangements and reagents by S.N. Sanyal
9. Chemistry of Organic natural products Vol-I & II by O.P. Agrawal.
10. Heterocyclic chemistry by Raj K. Bansal.
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3)and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out
of which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
23
BSH-208: PHYSICAL CHEMISTRY AND THERMODYNAMICS
Teaching Scheme Examination Scheme
Lectures 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) Physical Chemistry is the base of all the Chemical Industries.
2) To develop practical skill which helps the students in Chemical Industries?
Unit 1 [6 Hrs]
Electrolyte:
Conductance, Ionic mobility’s, Galvanic Cells, Classification of electrodes, determination of
Standard EMF, and its application, Cell reaction, Thermodynamics of electrolytes solutions,
Dehye and Hackle theory.
Unit 2 [10 Hrs]
Colloidal state, Adsorption,Molecular structure & properties:
Relation between molecular structure and properties such as surface tension, viscosity,
refractivity and dipole moments. Introduction, Types of colloidal states. Classification,
preparation, properties of colloidal Systems (hydrophobic & hydrophilic). Emulsifiers, gels,
foams, etc. and their applications.Adsorption Heat of adsorption, factors influencing adsorption,
adsorption isobar and adsorption isotherms Langmuir's umimolecular adsorption and limitations.
BET Theory and verification of BET equation and related problems
Unit 3 [4 Hrs]
Photochemistry:
Laws of photochemistry, quantum efficiency, kinetics of photochemical reactions.
Photochemical equilibrium, photosensitized reactions, photochemical phenomena. Radiation
chemistry, ionization radiation and electron impact process.
Unit 4 [6 Hrs]
Introduction:
Basic concepts of work., energy, heat, internal energy. The first law of thermodynamics,
thermodynamic state & state functions. Enthalpy, the steady state flow process. Equilibrium,
the reversible process. Heat capacities & specific heat. Numerical based on the above.
Unit 5 [10 Hrs]
The Phase rule:
Phase, degree of freedom of a system, the phase rule & its thermodynamic derivation.
Application of phase rule to one and two component systems. Numerical based on the above.
Volumetric properties of pure fluids: The PVT behavior. The Virial equations & its applications.
Ideal gas, Cubic equations of state, Accentric factor. The behavior of liquids. Numerical based
on the above.
24
Unit 6 [4 Hrs]
The Second law of Thermodynamic:
The Second law of Thermodynamic, heat engines, the thermodynamic temperature scale. The
concept of entropy. Entropy changes & irreversibility. The third law of thermodynamics.
Numerical based on the above.
Reference Books:
1. Principles of Physical Chemistry by Puri & Sharma
2. Physical Chemistry by Peter Atkin.
3. Advanced Physical Chemistry by Gurdeep, Raj.
4. Introduction to Chemical Engineering Thermodynamics by J M Smith & Van Ness
5. Chemical Engineering Thermodynamics, T. E. Daubert McGraw Hill Publication.
6. Chemical Process Principles Part - II O. A. Hougen et al John Wiley Publication.
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out
of which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
25
CHE-209: HEAT TRANSFER
Teaching Scheme Examination Scheme
Lectures 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test 20 Marks
Duration of Theory paper: 3Hrs
Objectives:
1) To develop understanding of the principles and modes of heat transfer.
2) To understand calculations and principles related to heat transfer in chemical processes.
Unit 1 [6 Hrs]
Heat Transfer Media and Conduction:
Heat Transfer Media: Characteristic properties, classification, selection and application. Nature
of heat flow, modes of heat transfer, Fourier’s Law, steady state and unsteady state conduction in
plane wall, cylindrical wall, spherical wall, multilayer walls, lumped parameter analysis,
transient heat flow in a semi-infinite solid.
Unit 2 [8 Hrs]
Insulation, Fins and Heat Transfer Augmentation:
Thermal insulation, types and selection, optimum and economic thickness of insulation for high
and low temperatures. Heat transfer in extended surfaces,effectiveness of fins, areas of
application. Heat transfer by convection, concept, of film and overall heat transfer coefficient,
resistance concept, coefficients for scale deposits, Augmentation Techniques.
Unit 3 [6 Hrs]
Convection:
Convective heat transfers for flow through and outside pipes, laminar heat transfer on a flat plate,
dimensionless numbers in heat transfer. Dittus-Boltzer Equation, Sieder-Tate Equation, Colburn
Equation. Natural convection, fluid flow and heat transfer across cylinders and spheres.
Unit 4 [6 Hrs]
Convection with Phase Change and Analogy:
Heat transfer with phase change, heat transfer in boiling liquids and condensation of vapors.
Reynolds Analogy between Heat Transfer and Momentum Transfer, Colburn’s Analogy in
convective flow. Heat Transfer in Packed Bed and Fluidized Bed Systems.
Unit 5 [6 Hrs]
Radiation:
Heat transfer by radiation, Absorptivity, Reflectivity, Transimitivity, Kickoff’s Law, Stefan
Boatman’s Law, Black and Gray body radiations, Opaque Body, view factors, radiant heat
exchange between non-black surfaces. Radiation between different surfaces, radiation shield,
radiation from flames and gases. Combined heat transfers by conduction-convection and
radiation.
26
Unit 6 [8 Hrs]
Heat Transfer Equipment:
Heat transfer equipments, double pipe heat exchangers, single and multi-pass shell and tube heat
exchangers, LMTD and effectiveness-NTU method. Spiral coil and plate type heat exchangers,
heat transfer in evaporators – single and multiple effects, heat transfer in agitated vessels, coils,
jacketed vessels, transient heating and cooling, Heat pipe.
Reference Books:
1. Unit Operations of Chemical Engineering, W. L. McCabe & J.M. Smith, et al McGraw Hill
Publication.
2. Process Heat Transfer, D. Q. Kern McGraw Hill Publication.
3. Chemical Engineering Vol.-I J. F. Richardson J. M. Coulson, Pergamon Press Publication.
4. Heat Transfer by J P Holman, McGraw Hill Publication.
5. Fundamentals of Heat Transfer F. Krieth, M. S. Bohn et al Harper & Row Publishers, New
York.
6. Heat Transmission W. H. Mc Adams McGraw Hill Publication.
7. Engineering Heat Transfer Gupta and Prakash.
8. Heat and Mass Transfer:Fundamentals & Applications by Yunus Cengel, McGraw Hill
Publication
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out
of which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
27
CHE-210:STRENGTH OF MATERIAL
Teaching Scheme Examination Scheme
Lectures 4 Hrs/week Theory: 80 Marks
Credits: 04 Class Test 20 Marks
Duration of Theory paper: 3Hrs
Unit 1 [10 Hrs]
Shear force & Bending moment:
Relation between load intensity, shear force and bending moment. Shear force & Bending
moment diagrams for simply supported, cantilever & overhanging beams with point loads &
UDL. Theory of simple bending & bending stress distribution. Shear stresses & shear stress
distribution in beam sections
Unit 2 [6 Hrs]
Simple Stresses & Strain:
Simple stress & strain due to tension, compression and. shear. Temperature stresses for section
of one material & more than one material.
Unit 3 [4 Hrs]
Principle Stresses & Strain:
Principle stresses & planes. Analysis of stresses on different planes in a material, two-
dimensional stress system. Mohr’s circle diagram for stress.
Unit 4 [6 Hrs]
Eccentric Loading:
Bending combined with axial loads. Eccentrically loaded short columns & chimneys. Axially
loaded long & short columns with different support conditions. Euler’s & Ranking’s method.
Unit 5 [8 Hrs]
Theory of Torsion:
Circular shafts subjected to torque- stress distribution & power transmission. Torsion combined
with bending & axial force. Strain Energy: Strain energy due to axial loads, bending, shear,
torsion & axial impact load.
Unit 6 [6 Hrs]
Thin & Thick Cylinders & Spheres:
Thin cylinders & spheres subjected to internal fluid pressure. Lame’s theory, design of thick
cylinders & spheres.
Reference Books
1. Mechanics of structure vol I by S. B. Junnarkar
2. Strength of materials by Singer F L
3. Strength of materials by Ramamurtham
4. Strength of materials by B C Punmia
5. Elements of strength of materials by Timoshenko & Young
28
Pattern of Question Paper:
The units in the syllabus shall be divided in two equal sections. Question paper shall be set
having two sections A and B. Section A questions shall be set on first three units (1,2,3) and
Section B questions on remaining three units (4,5,6). Question paper should cover the entire
syllabus.
For 80 marks Paper:
1. Minimum ten questions
2. Five questions in each section
3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out
of which FIVE to be solved.
4. Two questions from remaining questions from each section be asked to solve having
weightage of 15 marks
29
BSH226LAB-VI ENGINEERING CHEMISTRY
Teaching Scheme Examination Scheme
Practical: 4 Hrs/Week Practical: 50 Marks
Credit: 02
Practical Work
Minimum ten experiments, based on the syllabus, should be conducted during the course and
record (Journal) for the same shall be submitted.
The practical examination shall consist of performing an experiment based on the practical work
done during the course, the record of the experiments submitted by the candidate and viva-voce
based on the syllabus.
Suggested List of Experiments:
The experiment be based onfollowing list:
1. Identification of organic compounds based on functional group analysis. Physical
constants and derivatives. (at least 4 compounds)
2. Preparation of organic compounds (any three)
a) Preparation of acetanilide from aniline.
b) Preparation of meta-dinitrobenzene from benzene.
c) Preparation of iodoform from acetone.
d) Preparation of benzoic acid from benzaldehyde.
e) Preparation of aspirin form salicylic acid.
3. Estimation of following compounds (any three)
a) Carboxylic acid by titration method. Acetic acid.
b) Phenol by bromination.
c) Glucose by iodiometry method.
d) Esters by hydrolysis (ethyl acetate)
e) Aniline by bromination
f) Amide by hydrolysis (amide group) (acetamide)
30
BSH227 LAB-VII PHYSICAL CHEMISTRY AND THERMODYNAMICS
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Practical: 50 Marks
Credit: 01
Practical Work
Minimum eight experiments, based on the syllabus, should be conducted during the course and
record (Journal) for the same shall be submitted.
The practical examination shall consist of performing an experiment based on the practical work
done during the course, the record of the experiments submitted by the candidate and viva-voce
based on the syllabus.
Suggested list of experiments/studies
To determine the viscosity of the liquid.
1. To determine the specific and molecular refractions of unknown liquid by refractrometer.
2. To determine the normality of acetic acid and hydrochloric acid.
3. To determine the dissociation constants of acetic acids by pH meter.
4. To verify the Lambert-Beer law for Potassium dichromate, Potassium per magnet
and to prove the principal of additives.
5. To determine the energy of activation of liquid phase reaction.
6. To determine the unknown composition of Acetic acid in three-component system.
7. To determine the red ox potential in Ferrous-ferric system using potentiometer
8. Hydrolysis of ester in presence of hydrochloric acid.
9. Saponification of ester by sodium hydroxide.
10. Determination of rate of reaction in Zero order kinetics.
31
CHE228 LAB-VIII HEAT TRANSFER
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Practical: 50 Marks
Credit: 01
Practical Work
Minimum eight experiments, based on the syllabus, should be conducted during the course and
record (Journal) for the same shall be submitted.
The practical examination shall consist of performing an experiment based on the practical work
done during the course, the record of the experiments submitted by the candidate and viva-voce
based on the syllabus.
Suggested List of Experiments:
The experiment be based onfollowing list:
1. Thermal conductivity of composite wall.
2. Pin fins.
3. Forced convection apparatus.
4. Natural convective apparatus.
5. Emmisivity of test plate.
6. Dropwise and filmwise condensation
6. Stefan Boltzman apparatus.
7. Parallel flow /counter flow heat exchanger.
8. Pool boiling phenomena and critical heat flux.
9. Heat transfer on evaporator.
10. Thermal conductivity of insulating material.
11. Temperature profile in a metal rod.
12. Heat Transfer in Agitated Vessel.
13. Heat Transfer through Shell and Tube heat exchanger.
32
CHE229 LAB-IX: STRENGTH OF MATERIAL
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Term work: 50 Marks
Credit: 01
The term work will consist of a record of laboratory experiments and studies on following:
Part A (Any Five)
1. Tension test on ductile materials.
2. Bending test.
3. Shear test.
4. Torsion test.
5. Hardness test - Brinell & Rockwell.
6. Impact test.
Part B: Two exercises (each) on following
1. Shear Force & Bending Moment Diagram
2. Theory of bending.
3. Mohr’s circle for principal stresses.
4. Deflection of beams.
The term work will be a continuous assessment based on the experiments performed by the
student in the laboratory. The record of the experiments submitted by the student.
33
BSH 275: COMMUNICATION SKILLS-I
Teaching Scheme Examination Scheme
Practical: 2Hrs/Week Term work/Oral: 50 Marks
Credit: 01
The teacher shall explain in detail, the gist and techniques involved in the following work units
to the students. The teacher shall subsequently formulate the exercises to adjudge the skill sets
acquired by the students.
Unit 1 [04 Hrs]
Time Management:
Value of time, Diagnosing Time Management, Weekly Planner to do list and Prioritizing work.
Unit 2 [08 Hrs]
Grammar and Usage:
Overview of basic Mid-level English Grammar, Parts of speech, Preparations and Conditions,
Tense and Concept of time, Sentence Construction (Concord), Vocabulary: Words, Idioms,
Phrases, Antonyms and Synonyms
Unit 3 [08 Hrs]
Speaking Skills:
Training in Sound Recognition, the speech process, message, audience, speech style, feedback,
conversation and oral skills, fluency and self-expression body language phonetics and spoken
English, speaking techniques, word stress, correct stress patterns, voice quality, correct tone,
types of tones, Presentation skills-planning, preparation, organization, Stress and Intonation
pattern in spoken communication, Sound Recording Exercise (Language Lab Exercise),
Communication Errors in English
Unit 4 [08 Hrs]
Listening and Reading Skills:
Active and Passive Listening, the reading process, purpose, different kinds of texts, reference
material, scientific and technical texts, active and passive reading, strategies-vocabulary skills,
eye reading and visual perception, Skimming and scanning reading, drawing inferences and
conclusions, comprehension of technical material- scientific and technical texts, instructions and
technical manuals, graphic information. Note making- tool for study skills.
Unit 5 [06 Hrs]
Writing Skills:
Identification of different writing styles (Four Writing Style), Types of reports, information and
analytical reports, oral and written reports, formal and non-formal reports, printed forms, letter
and memo format, manuscript format, proposals, technical articles, journal articles and
conference papers, Drafting: Memo, Circulars, Notices, agendas etc. E-mails, Business Memos /
Letters, Employment Communication- resume design, resume style.
34
Unit 6 [08 Hrs]
Developing Skills and Presentations:
Developing key traits 1: creativity, critical thinking and problem solving. Effective
Presentations- Gathering Information and Building Presentation. Presentation by students in
team.
Text Books:
1. ‘Effective Technical Communication’ by M Ashraf Rizvi, Tata McGraw Hill Publishing
Company Ltd.
2. ‘Basic Managerial Skills for all’ E. H. McGrath, Eastern Economy Edition, Prentice
hall India.
3. ‘Developing Communication Skills’ Krishna Mohan, Meera Banerji, McMillan India Ltd.
4. Skills’ Krishna Mohan, Meera Banerji, McMillan India Ltd.
Term Work:
Term work marks should be given on the basis of online test conducted internally at college level.