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SYLLABUSOUTLINE OF PAPERS AND TESTS

FOR

B.VOC (Industrial Waste Treatment Technology) Second Year ( 3rd Semester)

2016-17,2017-2018 and 2018-19 Examinations

Code Title of Paper

Credits University Examination

Internal Assessme

nt

Max. Marks

Exam. Duration

Hours

B.VIWTT-211

Instrumentation and Techniques-I

4 60 40 100 3

B.VIWTT-212

Industrial Waste management 4 60 40 100 3

B.VIWTT-213

Instrumentation and Techniques-II

4.5 60 40 100 3

B.VIWTT-214

Basics of Chemistry-II 4.5 60 40 100 3

B.VIWTT-215

Instrumentation and Techniques:-Lab

4.5 50 50 100 3

B.VIWTT-216

Basics of Chemistry-II-Lab 4.5 50 50 100 3

B.VIWTT-217

Two week Training at industry/Lab

4 50 50 100 3

Total 30 390 310 700

1. The breakup of marks for the practicalwill be as under:i. Internal Assessment 50 Marks

ii. Viva Voce (External Evaluation) 20 Marks

iii.

Lab Record Program Development and Execution(External Evaluation)

30 Marks

2. The breakup of marks for the internal assessment for theory Subjects will be as under:i. Average of Both Mid Semester Tests / Internal Examinations 16 Marks

ii. Attendance 8 Marks

iii. Written Assignment/Project Work etc. 16 Marks

Semester III

B.VIWTT-211 : Instrumentation and Techniques-I

Max Marks: 60 Maximum Time: 3 Hrs. Min Pass Marks: 35% Lectures to be delivered: 55-65 Hrs

INSTRUCTIONS FOR THE PAPER SETTERThe question paper will consist of three sections A, B and C. Each of sections A and B

will have four questions from the respective sections of the syllabus and each question carry 9 marks. Section C will consist of one compulsory question having 12 parts of short-answer type covering the entire syllabus uniformly and each question will carry 2 marks.

INSTRUCTIONS FOR THE CANDIDATESCandidates are required to attempt two questions each from section A and B and the entire section C.

SECTION – AUnit:1 Distillation of water

Chemistry of water, physical properties, The process of distillation

Unit :2 Sterilization Techniques

Heat sterilization, Autoclave, Oven

Filter sterilization, UV sterilization

Unit:3 Preparation of solutions

Use of Balances, pH meter, Nature of acids and bases, strong and weak acids, dissociation

constant, pKa of an acid and its determination, concept of buffers, buffering capacity,

preparation of buffer, measurement of pH, working of pH meter.

SECTION – B

Unit: 4 Spectrophotometer

Principal of absorption spectroscopy, UV-Visible absorption spectroscopy, Lamberts Law,

Beer’s Law, Working and application of spectrophotometer, Working of spectrofluorimeter,

Principal of fluorescence, Intrinsic and Extrinsic fluorescence and their uses in biology.

B.VIWTT-212: Industrial Waste management

Max Marks: 60 Maximum Time: 3 Hrs.Min Pass Marks: 35% Lectures to be delivered: 55-65 Hrs




SECTION – A

Unit 1: Introduction to Industrial Pollution

Introduction, Introduction under red category, Introduction under orange category, Introduction under green category, The environment protection act 2002.

Unit: 2 Terminologies for Industrial Pollution

Various terminologies and abbreviations regarding industrial pollution

Unit: 3 Collection Preservation and Tabulation of Industrial samples

Collection and utilization of samples, BOD and DO samples, Sample for metals, Preservation of samples

SECTION – BUnit : 3 Dairy Industry

Introduction, Industrial description, causes and sources of diary industry pollution, control and treatment of dairy industry pollution.

Unit : 4 Distillery IndustryIntroduction, Industrial description, causes and sources of distillery industry pollution, effects of distillery pollution, control and treatment of distillery industry pollution.

Unit: 5 Dye and Paint Industry

Introduction, Industrial description, causes and sources of dye and paint Industry pollution, effects of dye and paint Industry pollution, control and treatment of dye and paint Industry pollution.

Reference Books:

V. K. Kudesia, N. Sharma,” Industrial Pollution” A pragati parkashan.

B.VIWTT-213: Instrumentation and Techniques-II





SECTION – A

Principal of centrifugation, basic rules of sedimentation, sedimentation coefficient, Various types of centrifuges-Table top centrifuge, Refrigerated centrifuged, Different types of motors, Differential centrifugation, Density gradient centrifugation.

SECTION – B

Basic principal of chromatography, Modes of chromatography: TLC, paper, column, Gel-filtration, Electrophoresis, Agarose gel electrophoresis, PAGE, SDS and native, IEF, Detection of nucleic acids and proteins.

B.VIWTT-214 Basics of Chemistry-II





SECTION – A

Acids and bases, Operational definition of acid and bases, Arrhenius concept of acids and

bases, Bronsted-Lowry concept of acid and bases, Lewis concept of acid and bases, Concept

of protic and aprotic solvents.

Periodic Properties: position of elements in the periodic table, effective nuclear charge and its

calculations, Atomic and ionic radii, ionization energy, electron affinity and elctronegativity

definition, trends in periodic table and applications in predicting chemical behavior.

SECTION – B

Nomenclature, Methods of preparation and basic chemical properties of alkanes, alkenes,

alkynes (No mechanism), types of reactions, Electrolphilic substation reaction of benzene (No

mechanism)

Text Books:

R.T. Morrision and R. N. boyd, Organic Chemistry, Pearson publications.

B.VIWTT – 215 Instrumentation and Techniques:-Lab

Max Marks: 50 Maximum Time: 3 Hrs.Min Pass Marks: 35%

Practical

1. Determination of pKa value of acetic acid2. Preparation of standard solutions3. Preparation of buffers4. Simple volumetric redox titrations5. Verification of Beers Law6. Estimation of protein by Lowry methods7. Separation of amino acids by paper chromatography/TLC

.

B.VIWTT – 216 Basics of Chemistry-II-Lab

Max Marks: 50 Maximum Time: 3 Hrs.Min Pass Marks: 35%

Practical

1. To determine Fe(II) ions by titrating with potassium permanganate

2. To determine surface tension of liquid by drop number method

3. To determine viscosity of liquid using Ostwald viscometer.

4. Detection of extra element (N, S, halogens) in organic compounds containing no

more than one extra element.

5. To detect the following functional groups in organic compound – alcohol, phenol,

aldehyde, ketone, carbohydrate, carboxylic acid, primary amines and amide

SYLLABUSOUTLINE OF PAPERS AND TESTS

FOR

B.VOC (Industrial Waste Treatment Technology) Second year (4th Semester) 2016-17, 2017-2018 and 2018-19 Examinations

Code Title of Paper

Credits University Examination

Internal Assessment

Max. Marks

Exam. Duration

Hours

B.VIWTT 221

Introduction to Solid Waste Management

4 60 40 100 3

B.VIWTT 222

Environmental studies and road safety awareness

4 60 40 100 3

B.VIWTT 223

Sustainable techniques in municipal solid waste

management – Case Studies

4.5 60 40 100 3

B.VIWTT 224

Basics of Chemistry-IV 4.5 60 40 100 3

B.VIWTT 225

Project work 4.5 50 50 100 3

B.VIWTT 226

Industrial Waste Management Practical

4.5 50 50 100 3

Total 26 340 260 6001. The breakup of marks for the practicalwill be as under:

i. Internal Assessment 50 Marks

ii. Viva Voce (External Evaluation) 20 Marks

iii.

Lab Record Program Development and Execution(External Evaluation)

30 Marks

2. The breakup of marks for the internal assessment for theory Subjects will be as under:i. Average of Both Mid Semester Tests / Internal Examinations 16 Marks

ii. Attendance 8 Marks

iii. Written Assignment/Project Work etc. 16 Marks

PAPER – B.VIWTT 221

Introduction to Solid Waste Management (Total Hours - 60)

M.Marks- 60 Maximum Time : 3Hrs

Internal Assesment-40

Instructions for the paper setter

The question paper will consist of three sections A, B and C. Each of section A and B will have four questions from the respective sections of the syllabus and each question carry 9 marks. Section C will consist of one compulsory question having 12 parts of short answer type covering the entire syllabus and each question will carry two marks.

Instructions for the candidate

Candidates are required to attempt two questions each from section A and B and the entire section C.

Unit - I

Introduction to Environment

Ecosystem –meaning- Types -Components- Structure – Functions, Levels of organization in nature- Food chain and Trophic structure, Biogeochemical Cycles, Energy flow.

Municipal solid waste

Definition - Sources and types of solid waste- composition and its determinants of Solid waste-factors influencing generation-quantity assessment of solid wastes-methods of sampling and characterization.

Collection and Transfer

Collection: Collection of Solid waste – collection services – collection system, equipments – time and frequency of collection – labour requirement – factors affecting collection – analysis of collection system – collection routes – preparation of master schedules.

Transfer and Transport: Need for transfer operation – transfer stations – types – transport means and methods – location of transport stations - Manpower requirement – collection routes: Transfer stations – selection of location, types & design requirements, operation & maintenance.

Unit - II

Processing Techniques and Recovery of Energy

Processing techniques – purposes mechanical volume reduction – necessary equipments – chemical volume reduction – incinerators – mechanical size reduction selection of equipments – components separation – methods – drying and dewatering.

Recovery of Resources, conversion products and energy recovery – recoverable materials – processing and recovery systems – incineration with heat recovery.

Disposal of Solid Wastes

Refuse disposal – various methods – incinerations – principle features of an incinerator – site selection and plant layout of an incinerator - sanitary landfill- methods of operation – advantages and disadvantages of sanitary land fill - site selection – reactions accruing in completed landfills – gas and leachate movement and control – equipments necessary.

References

1) George Techobanoglous et al,”Integrated Solid Waste Management” McGraw - Hill, 1993.

2) Techobanoglous Thiesen Ellasen; Solid Waste Engineering Principles and Management, McGraw - Hill 1997.

3) R.E.Landrefh and P.A.Rebers,” Municipal Solid Wastes-Problems & Solutions” ,Lewis, 1997.

4) Manual on Municipal 1 Solid waste Management, CPHEEO, Ministry of Urban Development, Govt. Of. India, New Delhi, 2000.

5) Blide A.D.& Sundaresan, B.B,”Solid Waste Management in Developing Countries”, INSDOC, 1993.

6) Ecology Science and Practice; Claude Fourie, Christian Ferra, Paul Medori, Tean Devaux, Oxford and IBH Publishing Co (Pvt) LTD, special Indian edition.

7) Principles of Ecology- P.S.Verma, V.K.Agarwal.S.Chand & Company (Pvt) LTD 1989.


Environment Studies and Road Safety Awareness






SECTION AIt will consist of ten short answer type questions. Candidates will be required to attempt six questions, each question carrying five marks. Answer to any of the questions should not exceed two pages.It will consist of six essay type questions. Candidates will be required to attempt three questions, each question carrying fifteen marks. Answer to any of the questions should not exceed four pages.

SECTION B

It will consist of two questions. Candidate will be required to attempt one question only. Answer to the question should not exceed 5 pages. In this section the students will be required to write on the environment of an area / ecosystem / vi1lage industry / disaster / mine/ dam agriculture field / waste management / hospital etc. with its salient features, limitations, their implications and suggestion for improvement.

1. The multidisciplinary nature of environmental studies: Definition, scope & its importance, Need for public awareness.

2. Natural resources: Natural resources and associated problems. a) Forest resources: Use of over exploitation, deforestation, case studies. Timber

extraction, mining, dams and their effects on forests and tribal people. b) Water resources: Use and over-utilization of surface and ground water, floods,

drought, conflicts over water, dams-benefits and problems. c) Mineral resources: Use and exploitation, environmental effects of extracting and

using mineral resources, case studies.d) Food resources: World food problems, change caused by agriculture and

overgrazing, effects or modern agriculture, fertilizer-pesticide problem, salinity, case studies.

e) Energy resources: Growing of energy needs, renewable and non-renewable energy resources, use of alternate energy sources, case studies.

f) Land recourses: Land as a resource, land degradation, soil erosion and desertification.

g) Role of an individual in conservation of natural resources, Equitable use of resources

for sustainable lifestyles.

3. Ecosystem:

Concept of an ecosystem, Structure and function of an ecosystem, Producers, consumers and decomposers, Energy flow in the ecosystem, Ecological succession, Food chains, food webs and ecological pyramids.Introduction, types, characteristic features, structure and function of the following ecosystems:a.Forest ecosystem b.Grassland ecosystem c.Desert ecosystemd.Aquatic ecosystems (ponds, streams, lakes, rivers, oceans, estuaries).

4. Biodiversity and its Conservation:

Definition: Genetic, species and ecosystem diversity, Biogeographical classification of India.Value of Biodiversity: Consumptive use; productive use, social, ethical, aesthetic and option values.Biodiversity of global, National and local levels, India as mega-diversity nation "Hot-spots of biodiversity.

Threats to Biodiversity: Habitat loss, poaching of wild life, man wildlife conflicts Endangered and endemic species of India.Conservation of Biodiversity: In situ and Ex-situ conservation of biodiversity.

5.Environmental Pollution:

Definition, Causes, effects and control measures of:

a) Air Pollution b) Water Pollution c) Soil Pollution d) Marine Pollutione) Noise Pollution f) Thermal Pollutiong) Nuclear Hazards Solid Waste Management: Causes, effects and control measures of urban and industrial wastes.Role of an individual in prevention of pollution.

Pollution case studies Disaster Management: Floods, Earthquake, Cyclone and Landslides

6. Social Issues and Environment:

*From unsustainable to sustainable development *Urban problems related to energy*Water conservation, rain water harvesting, watershed management*Resettlement and rehabilitation of people; its problems and concerns. Case studies *Environmental ethics: Issues and possible solutions.*Climate change, global warning, acid rain, ozone layer depletion, nuclear accidents and

holocause. Case studies.*Wasteland reclamation *Consumerism and waste products *Environmental Protection Act

*Air (Prevention and Control of Pollution) Act *Water (Prevention and Control of Pollution) Act

*Wildlife Protection Act

*Forest Conservation Act*Issues involved in enforcement of environmental legislation *Public awareness7. Human population and the environment

*Population growth, variation among nations *Population explosion-Family welfare programme

*Environment and human health

*Human rights *Value education *HIV / AIDS

*Women and child welfare


Sustainable Techniques in Municipal Solid Waste Management Plan- Case Studies

(Total Hours – 60)






Candidates are required to attempt two questions each from section A and B and the entire section C

Unit – I

Sustainable Techniques for MSWM

Introduction - Segregation-Sorting-Composting-Vermi composting- Home composting- Recycling and Reuse- Incineration method-Scientific Land filling-Energy development

Composting, Incineration and Land filling

Definition and concepts-Palacode Model-Namakkal Model -Thudiyalur Model -Anthiyur Model -Mohanur Model – Exnora Method –CEE method in Bangalore- Coimbatore Corporation Model in Vellalore-Bio medical system in Coimbatore

Unit – II

Reuse and Recycling Techniques

Need for the concept-Various Types - Hand made Paper production –Reuse of materials-Recycle of materials

PPP Model

Definition, Concept and need- Tiruppur model-IWMUST Model in Udumalai-Erode-Pollachi-Coonur Model-Bangalore Model 13

Energy Development

Chennai Koyambedu Model- Oodandurai Town Panchayat Model - Developed countries model

References

1) J. Glynn Henry and Gary. W. Heinke, “Environmental Science and Engineering”, Pretice Hall of India, 2004.

2) A. D.Bhide and B.B.Sundaresan, “Solid Waste Management – Collection, Processing and disposal” Mudrashilpa Offset Printers, Nagpur, 2001.

3) Techobanoglous Thiesen Ellasen; Solid Waste Engineering Principles and Management, McGraw - Hill 1997.


Basics of Chemistry-IV

(Total Hours – 60)







Unit-1

Alkyl halides

Nomenclature and classes of alkyl halides, structural isomerism in alkyl halides, physical properties, Methods of formation, Chemical reactions (without mechanism)

Aryl halides

Nomenclature and classes of aryl halides, physical properties, Methods of formation, Chemical reactions (without mechanism), Reason of low reactivity of aryl halides.

Unit-II

Alcohol and Phenols

Nomenclature, structure and bonding, preparation of alcohols and phenols, physical properties and acidic character, Comparative acidic strength of alcohols and phenols, stabilization of phenoxide ion, Phenols electrophilic substitution reactions (without mechanism).

Carboxylic acids

Nomenclature, structure and bonding, physical properties and acidic character, Reactions of carboxylic acids, Synthesis of acid chlorides, esters and amides. Reduction of carboxylic acids, method of formation and chemical reactions of unsaturated monocarboxylic acids. Dicarboxylic acids, methods of their formation and effect of heat and hydrating agents without mechanism). (without mechanism).


Project Work

List of Experiments

1) Determination of pH of MSW

2) Determination of Total Solids, fixed solids and volatile solids

3) Determination of nutrient value (NPK)

4) Lab scale study on vermin composting

5) Lab scale study of aerobic and anaerobic digesting of solid wastes (Both industrial & Municipal)

List of Practical

6) A Visit to the Hazardous waste Generation or disposal site.

7) Practical knowledge and working of incinerators

8) Visit to Industries.

9) Ecology baseline and impact of waste – disposal on vegetation

10) Preparation of Project report based on a case study of one hospital

Study of the source, generation rates and characteristics of hazardous wastes and their regulation, handling, treatment, and disposal. Special emphasis is placed on process design of waste handling, treatment and disposal systems.

Any one of the above practical can be chosen by the candidate.


Industrial Waste Management Practical

M. Marks- 60 Maximum Time : 3Hrs






Industrial waste management in any of the two industries

1. Dairy2. Distilleries3. Paper 4. Food 5. Dye and Paint6. Leather

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