site visit report · the site visit process is a sample on a particular day of an...

Site Visit Report

The site visit process is a sample on a particular day of an installation's compliance with some of its licence conditions. Where non-compliance against a particular condition has not been reported, this should not be construed to mean that there is full compliance with that condition of the licence.

Instructions and actions arising from the visit shall be addressed, or where applicable noted, by the licensee in order to ensure compliance, to improve the environmental performance of the installation and to provide clarification on certain issues.

The licensee shall take the actions specified to close out the non-compliances and observations raised in this Site Visit Report.

Licensee

Name of Installation Town of Monaghan Co-Operative Agricultural and Dairy Society

Licensee Town of Monaghan Co-Operative Agricultural and Dairy Society

Licence Register No. P0815-02

CRO Number

Site Address Coolshannagh, Monaghan, Monaghan

Site Visit Reference No. SV10489

Report Detail

Issue Date 12/10/2017

Prepared By Ken Murphy

Site Visit Detail

Date Of Inspection 23/08/2017 Announced No

Time In 09:00 Time Out 17:00

Visited by on behalf of the EPA Fitz Scientific Ltd

Licensee Personnel and Role See Report

Photo Taken No Samples Taken Yes Video Taken No

Odour Assessment No

Site Visit Report - SV10489 - Town of Monaghan Co-Operative Agricultural and Dairy Society of 43

Scope

This is a report on monitoring of emissions to air at this site. Please find the detailed technical report attached.

Media

Air

Site Areas Inspected

See Report

Documents Inspected

See Report


Town of Monaghan Co-OperativeCoolshannagh, Monaghan, Co Monaghan.

P0815-02CAR17-01

Emissions to AtmosphereReport No:

Report Date:

Fitz Scientific

Unit 35, Boyne Business Park, Drogheda, Co Louth

Phone: +353 41 98 45440

07/09/2017

Environmental Protection Agency

Industrial Emissions Licence: P0815-02

Page 1 of 39Site Visit Report - SV10489 - Town of Monaghan Co-Operative Agricultural and Dairy Society of 43

Fitz Scientific

Coolshannagh, Monaghan, Co Monaghan.

Town of Monaghan Co-Operative

Visit No: 1Year: 2017

Report for the Periodic Monitoring of Emissions to Air

Executive Summary

Licence / Permit Number:

Job Quote Number:

P0815-02

EPA17065

Operator Name:

Installation:

Phone:

Contact Name:



047 81400

Marie Mc Kenna

Monitoring Dates:

Monitoring Organisation: Fitz Scientific

Unit 35, Boyne Business Park, Drogheda, Co. Louth, Ireland

Phone: +353 41 98 45440 / Fax: +353 41 98 46171

email: [email protected]

UKAS Registration number 2802

Report Date: 07/09/2017

Signed: ____________________________ Signed: ____________________________

-1

P0815-02Industrial Emissions Licence

Report created using QRSys version

P0815-02CAR17-01

23/08/2017

Jason McGuirk

MM14 1320

Level 2

Technician

TE1, TE2, TE3, TE4

Written By:

MCERTS Reg:

Competency:

Function:

Endorsements:

Aadil Khan

MM11 1120

Level 2

Field Services Manager

TE1, TE2, TE3, TE4

Approved By:

MCERTS Reg:

Competency:

Function:

Endorsements:

3.8 August 2017


Contents

1.- Part 1

1.1.- Monitoring Objectives

1.2.- Special Monitoring Requirements

1.3.- Monitoring Results

1.4.- Operational Information

1.5.- Monitoring Deviations

1.6.- Monitoring Procedures and Deviations

2.- Part 2

Appendix 1: General Information

Appendix 2: Monitoring Information

Fitz Scientific




P0815-02Industrial Emissions LicenceP0815-02CAR17-01


Fitz Scientific





1.- Part 1

1.1.- Monitoring Objectives

1.2.- Special Monitoring Remarks

All the sampling points were obtainable Yes

All parameters were sampled Yes

Opinions and interpretations expressed in this report are outside the scope of any claimed UKAS accreditation.EPA requirements AG1 (Safety) and AG2 (Monitoring Guidance Note) were applied during the monitoring.

Additional information

NOx conversion efficiency: 95.2% tested on 04/11/2016

The monitoring was carried out at this installation as part of compliance monitoring of an Industrial Emissions Licence requirement. This Air Emissions Monitoring has been carried out by Fitz Scientific on behalf of the Environmental Protection Agency. The substances monitored at the emission points are listed below.

AE-1

Parameter Result

NOx 606.4 mg/m3

O2 5.38 %

Particulates 100.2 mg/m3

SO2 811.8 mg/m3

Volumetric flow 6134.3 m3/h


Fitz Scientific





1.3.- Monitoring Results

Analysis information

Emission Point

ReferenceSubstance to be Monitored ELV Result

Uncert (+/-) Units

Date of sampling

Start - End

Times Reference Method Accr.velocity

(m/s)LOD

AE-1 NOx 606.4 27.8 23/08/2017 13:44-14:26

BS EN 14792:2017 MCERTS9.110.04 mg/m3900 mg/m3

AE-1 O2 5.38 0.22 23/08/2017 13:44-14:26

BS EN 14789:2017 MCERTS9.110.01 %n/a

AE-1 Particulates 100.2 3.32 23/08/2017 15:15-15:45

BS EN 13284-1:2002 MCERTS9.110.1 mg/m3150 mg/m3

AE-1 SO2 811.8 75.29 23/08/2017 12:21-12:51

BS EN 14791:2017 MCERTS9.110.4 mg/m31700 mg/m3

AE-1 Volumetric flow 6134.3 180.8 23/08/2017 15:15-15:45

BS EN 16911-1:2013 MCERTS9.11n/a m3/h10000 m3/h

NOx Fitz Scientific

O2 Fitz Scientific

Particulates Fitz Scientific

SO2 Fitz Scientific

Volumetric flow Fitz Scientific

Particulates-blank <0.1 0.005 23/08/2017 15:01-15:03

BS EN 13284-1:2002 MCERTS9.110.1 mg/m3AE-1

SO2-blank <0.4 0.03 23/08/2017 12:05-12:07

BS EN 14791:2017 MCERTS9.110.4 mg/m3AE-1

Sampling stage carried out as per MCERTS requirementsNo*:


Fitz Scientific





Additional information

* The reported uncertainty is based on a standard uncertainty multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%

** Results reported at following Reference Conditions

Reference Conditions

Abatement system and process load

Emission Point Reference Temperature (K) Pressure (KPa) Moisture (%) Oxygen (%)

Monitoring Result Reference Conditions

AE-1 273 101.3 3Dry

Abatement system In Operation Fuel type and LoadLocation

None n/a As per Production demand

AE-1 Fuel-oil


Fitz Scientific





1.4.- Operating Information

Emission Point Reference Date Process Type

ProcessDuration Substance CEMS PR Units

AE-1 23/08/2017 n/a 606.4NOxCombustion Continuous mg/m3

AE-1 23/08/2017 n/a 5.38O2Combustion Continuous %

AE-1 23/08/2017 n/a 100.2ParticulatesCombustion Continuous mg/m3

AE-1 23/08/2017 n/a 811.8SO2Combustion Continuous mg/m3

AE-1 23/08/2017 n/a 6134.3Volumetric flowCombustion Continuous m3/h

* CEMS: Continuous Emission Monitoring System Results

* PR: Periodic Monitoring Results


Fitz Scientific





1.5.- Monitoring Deviations

Monitoring carried out as per Standard Methods. No deviations were recorded

Isokinetic conditions were outside the requirements of BS EN 13282-1 section 10.4.

Due to the high velocity in the duct a smaller nozzle size was used than required by BS EN 13282-1 section 5.2.4 (6mm) to carry out isokinetic sampling.

Emission monitoring point does not have required number of ports as per AG1 section 2.1/2.2 (per M1 Figure A2.5).

The ELV is such that the LOD for the analysis does not allow for the requirement of >10% ELV to be achieved (for ELV >5 mg/m3) (MID 13248-1 section 10.6)

The ELV is such that the LOD for the analysis does not allow for the requirement of >20% ELV to be achieved (for ELV <5 mg/m3) (MID 13248-1 section 10.6)

Negative flow was found (BS EN 13284-1 section 5.2 b).

The stack flow direction doesn’t meet the minimum requirement of 15 degrees with regard the axis of the stack. (BS EN 13284-1 section 5.2 a).

The ratio of highest to lowest local gas velocity is outside (higher than 3:1) of BS EN 13284-1 section 5.2 d) requirements.

Emission point does not meet the requirements of BS EN 15259:2007 Section 6.2.1 NOTE 4 and AG1 section 2.1/2.2 (per M1 Annex 1) - The measurement plane is not in a section of duct that is at least 5 hydraulic diameters of straight duct upstream of the sampling plane and 2 hydraulic diameters downtream (5 hydraulic diameters from the top of the stack)

Sampling port size is too small for velocity, temperature and pressure measurements to be carried out as per AG1 section 2.1/2.2 (M1 Annex 1).

Differential pressure lower than 5Pa measured with pitot tube (BS EN 13284-1 section 5.2 c).

SO2 Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS EN 14791:2017 section 6.6.1)

NOx calibration drift is higher than 2% of the span value. Results are corrected to drift. (TGN M22 Section 6)

The blank reading does not meet the required target of <10% of the daily limit value (for ELV >10 mg/m3) (BS EN 12384-1 section 10.6)

AE-1Emission Point NOxParameter

NOx overall uncertainty calculated is outside requirement of <10% at the daily ELV, or the lowest limit value assigned by the local authorities, expressed on dry basis before correction to O2 reference concentration as per Section 8 BS EN 14789:2017

CO overall uncertainty calculated is outside requirement of <6% at the daily ELV expressed on dry basis before correction to O2 reference concentration as per 7.3 BS EN 15058:2017.

O2 overall uncertainty calculated is outside requirement of <6% of the value expressed on dry basis, or 0.3% expressed as a volume concentration as per Section 8 BS EN 14789:2017

CO calibration drift is higher than 2% of the span value. Results are corrected to drift. (TGN M22 Section 6)

O2 calibration drift is higher than 2% of the span value. Results are corrected to drift. (EN 14789:2017 Section 9.4.2.3)

TVOC calibration drift is higher than 2% of the span value. Results are corrected to drift. (BS EN 12619:2013 Section 6.2.3)

HCl Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS EN 1911:2010 section 5.2.1.2.2)

HF Impinger efficiency is lower than the requirements of 95% total of concentration in the first impinger (BS ISO 15713:2006 section 6.4).

Homogeneity test is required for this stack as per BS EN 15259:2007 but customer did not require it in the Confirmation Form

The measurement values are invalid as the corresponding blank result is greater than the requirement identified in CEN/TS 13649:2014 section 10 (c) (must be <10% of the limit values)


Fitz Scientific




















AE-1Emission Point O2Parameter












Fitz Scientific



















AE-1Emission Point ParticulatesParameter












Fitz Scientific




















AE-1Emission Point SO2Parameter












Fitz Scientific



















AE-1Emission Point Volumetric flowParameter












Fitz Scientific





Licence / Permit Number:

Job Quote Number:

P0815-02

EPA17065

Operator Name:

Installation:

Phone:

Contact Name:



Marie Mc Kenna

047 81400

Monitoring Dates:

Monitoring Organisation: Fitz Scientific


Phone: +353 41 98 45440 / Fax: +353 41 98 46171

email: [email protected]

2.- Part 2

Supporting information

23/08/2017

Laboratory details

NOx

Address Contact email Phone Acc. Number


Geoff Fitzpatrick

[email protected] +353 41 98 45440 - ext 2

UKAS 2802Fitz Scientific

O2



Geoff Fitzpatrick



Particulates



Geoff Fitzpatrick



SO2



Fitz Scientific






Geoff Fitzpatrick



Volumetric flow



Geoff Fitzpatrick




Fitz Scientific





Appendix 1:

Sampling personnel used

Substances Monitored

Equipment Checklist References

As an accredited organisation Fitz scientific have implemented procedures to ensure that the requirements of TPS 63 (UKAS Policy on Deviating Samples) are met with regard to samples taken and tested for chemical analysis. As such all samples, when applicable, have been transported in containers, and in an environment, that meet the relevant standard requirements where applicable

Substance Fitz SOPMethod used for Monitoring

NOx BS EN 14792:2017 161

O2 BS EN 14789:2017 161

Particulates BS EN 13284-1:2002 101

SO2 BS EN 14791:2017 167

Volumetric flow BS EN 16911-1:2013 122

Stack: AE-1

EM402

n/a

n/a

Probe1

EM372

n/a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

Volumetric flowParameter:

EM402

n/a

Set C

Probe1

n/a

EM201 (a

n/a n/a

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

SO2Parameter:

EM402

Set1

Set C

Probe1

EM372

n/a

EM389 EM3297/EM3296

n/a

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

ParticulatesParameter:

23/08/2017 Technician Name Position Qualification TEs MCERTS no

Aadil Khan Team Leader Level 2 TE1, TE2, TE3, TE4

Patrick (Jamie) Rog Technician Trainee -

MM11 1120

MM16 1391


Fitz Scientific





n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

EM209

n/a

n/a

n/a n/a

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

O2Parameter:

n/a

n/a

n/a

n/a

n/a

n/a

n/a n/a

EM209

n/a

n/a

n/a EA53XU6

n/a

n/a

TCR

Nozzles

Impingers

Probe

Pitot tube

Weights

Caliper Filters

Horiba

FID

FTIR

Testo Gases

Handheld pumps

Tubes

NOxParameter:


Fitz Scientific





Appendix 2:

Monitoring Information

1

4

9.11

100.392

197.99

0.71

12979.2

7455.8

6134.3

273

101.3

-1.1

5.38

5.08

Number of Ports

Number of Points

Average Velocity v'a (m/s)

Average Pressure (KPa)

Average Temperature (ºC)

Stack Diameter (m)

Actual Moisture Flow rate (m3/h)

Moisture Flow rate at STP (m3/h)

Dry Flow rate at STP, Ref O2 (m3/h)

T reference (Deg K)

P reference (KPa)

Isokinetic condition (%)

Oxygen measured (%)

Water vapor (%)

Wet Stack (yes/no) No

Probe Temperature (°C) n/a

Impinger efficiency (%) SO2(99.9)

Size of Nozzle 10

AE-1Stack Parameter: Volumetric flow, NOx, O2, Particulates, SO2

Max Flow Rate in Licence (m3/h): 10000


Fitz Scientific





Diagram of Sampling Location (not to scale)

X

X X X

A

AE-1

Circular

1

4

ports

points

Point % of Diameter Location (cm) Velocity (m/s) Temperature (ºC)

Traverse Length 0.71 m

Line

1 6.80 4.8 7.157 151.7841

2 25.10 17.8 7.789 157.7011

3 75.10 53.3 4.459 163.2231

4 93.40 66.3 6.89 163.6861


Fitz Scientific





Monitoring result calculations and uncertainty calculations


Fitz ScientificP0815-02CAR17-01Yar: 2017 Visit no: 1________________________________________________________________________________________________________________________

Town of Monaghan Co-OperativeIndustrial Emissions Licence P0815-02

Volumetric Flowrate Correction Template BS EN 16911-1:2013Company Town of Monaghan Co-Operative Date of Test 23/08/2017Site Coolshannagh, Monaghan, Co Monaghan. Reference No P0815-02Plant Identification AE-1 Operator Id MM11 1120Test carried out by Aadil Khan TE's TE1, TE2, TE3, TE4

P0815-02CAR17-01

Stack information:

Stack dimensions

m Stack Area m2 No ports / No pointsSuitable ports

(Y/N)?

Comply with 5 Up / 2 Down?

(Y/N) Pressure kPa Temperature K Moisture % Oxygen %

Circular Stack 0.71 0.395919214 1 Yes NoReference Condition 101.3 273 0 3

Rectangular stack 0.00 0.00 0.00 4Stack Conditions 100.4 471.0 5.1 5.38

Actual Value: 0.395919214

PointVelocity m/s (v'a)

Temp degC (ta) Temp K Presssure kPa (Pa)

Flow Rate m3/sec:

Actual Flow rate m3/hr

Moisture Flow rate at STP m3/hr Moisture

Flow rate at STP, Dry m3/hr O2 %

Flow Rate at STP, Dry, Ref O2 m3/hr

1 9.11 197.985 470.985 100 3.6 12979.2 7455.8 5.1 7077.0 5.38 6134.3Volumetric flow 9.11 197.99 470.99 100.392 3.6 12979.2 7455.8 5.1 7077.0 5.38 6134.3Uncertainty 197.99 470.99 100.392 382.6 219.8 5.1 208.6 5.38 180.8

Maximum volumetric flow as per Licence 10000.0 m3/h

Report Number :

Calculation spreadsheet v.48Page 20 of 39


Fitz ScientificP0815-02CAR17-01Yar: 2017 Visit no: 1_________________________________________________________________________________________________________________________


v1.4 Oct-16Enter data in orange cells onlyConstantsGas constant 8.314 J/(K.mol)

1990 Pa0.01 Pa

2 % of value0.2 % of range between calibrations

PITOT 0.04 % of rangeSampling probe: Probe1 0.64 Pa

Pitot EM372 Water vapour me 7.44 % relativePitot coefficient, K 0.847 0.61 °C CO content meas 0.00 % relativeExpanded uncertainty (95%, k=2) 0.02 1007.11 Pa CO2 content mea 0.37 % relative

0.50 % O2 content measu 4.09 % relative

Duct dimensions Circular RectangularDiameter 0.71 m a mArea 0.4 m2 b m

Area 0.00 m2Uncertainty (%) 0.501408451 Uncertainty (%) 0.00116889

All Pressures should be entered in Pascals, Pa

Measurement Point Atmospheric Pressure, PaStack Pressure, Pa Static Pressure, Pa meas1, Pa meas2, Pa meas3, Pa meas4, Pa meas5, Pa Delta P, Pa Stack Temperature, C

Water Vapour Content, % CO, ppm CO2, % N2, % O2, % dry molecular wt, g/mol stack molecular wt, g/mol

1 100411 100392 43.753 43.75 197.99 5.08 0.00 12.06561109 82.6 5.38 30.15 29.532 5.08 0.00 12.06561109 82.6 5.38 30.15 29.533 5.08 0.00 12.06561109 82.6 5.38 30.15 29.534 5.08 0.00 12.06561109 82.6 5.38 30.15 29.535 5.08 0.00 12.06561109 82.6 5.38 30.15 29.536 5.08 0.00 12.06561109 82.6 5.38 30.15 29.537 5.08 0.00 12.06561109 82.6 5.38 30.15 29.538 5.08 0.00 12.06561109 82.6 5.38 30.15 29.539 5.08 0.00 12.06561109 82.6 5.38 30.15 29.53

10 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5311 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5312 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5313 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5314 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5315 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5316 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5317 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5318 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5319 5.08 0.00 12.06561109 82.6 5.38 30.15 29.5320 5.08 0.00 12.06561109 82.6 5.38 30.15 29.53

Mean 100411 100392 #DIV/0! 43.75 #DIV/0! #DIV/0! #DIV/0! #DIV/0! 43.75 197.99 5.08 0.0 12.1 82.6 5.4 30.15 29.53

Circular duct Rectangular ductMean velocity 9.11 m/sec Flow rate (stack conditions) 12979 m3/hour 0 m3/hour

Standard uncerta 0.12 m/sec 1.4 % of value Vol. flow rate expanded uncertain 383 m3/hour #DIV/0! m3/hour

Mean density 0.757 kg/m3 Expanded uncert 0.25 m/sec 2.7 % of value Vol. flow rate expanded uncertain 2.9 % of value #DIV/0! % of value

Developed for the STA by David Butterfield & Chris Dimopoulos, NPL

Repeatability of Delta P transducerDrift of Delta P transducerLack of fit of measurement system

Uncertainty calculation for Velocity and Volume Flow Rate Measurement by Pitot tube EN ISO 16911‐1

Characteristics of pressure sensor used for Delta PEnter uncertainties as (95%,k=2) where relevant

Range of Delta P transducerResolution of Delta P transducer

Uncertainty in duct area measurement

Dry gas basis

Uncertainty in stack gas compositionUncertainty in Delta P transducer Enter uncertainties as (95%,k=2) where relevant

Uncertainty in temperature readout systemUncertainty in atmospheric pressure transducer

Enter uncertainties as (95%,k=2) where relevant



Fitz ScientificP0815-02CAR17-01Yar: 2017 Visit no: 1_______________________________________________________________________________________________________________________


Velocity associated uncertainties

Pitot Tube CoefficientExpanded uncertainty (95%, k=2) 0.02Standard uncertainty (Dimensionless) 0.01

Table 1

Delta P Standard uncertanites^2 Measurement Point SD of the mean of the DP measurements (Standard uncertainty Delta P)^2 u2(Dpi)Velocity (m/s) Standard uncertainty velocity m/s

Sigma DP See Table 1 1 0.9 2.5 8E‐04 9.1 0.29Resolution uncertainty 0.00 2Calibration uncertainty 0.10 3Lack of fit 0.21 4Drift 5.28 5

67

Molar Mass 8u(H2O) 0.188987197 9(O2)wet 5.1 10u(O2)wet 0.11 11(CO2)wet 11.5 12u(CO2)wet 0.03 13(CO)wet 0.0 14u(CO)wet 0.00 15Oxygen sensitivity 4.00E‐05 16Water sensitivity 1.00E‐04 17CO2 sensitivity 1.60E‐04 18CO sensitivity 4.00E‐08 19

20standard uncertainty 0.000020 kg/mol 0.07 % of value Average 0.88 2.52164393 8E‐04 9.11 0.287268999

Temperaturestandard uncertainty 0.31 K 0.06 % of value

Stack static pressurestandard uncertainty 0.0 Pa #DIV/0! % of value

Stack pressurestandard uncertainty 1007.1 Pa 1.00 % of value

Stack gas densitystandard uncertainty 0.0076 kg/m3 1.01 % of value

Standard uncertainty of velocity 0.12 m/sec 1.4 % of value

Expanded uncertainty in velocity 0.25 m/sec 2.7 % of value





Volume flow rate associated uncertainties

Circular duct Rectangular ductArea uncertainty 0.01 m2 #DIV/0! m2

Flow rate standard uncertainty 191 m3/h #DIV/0! m3/h

Volume flow rate expanded uncertainty 383 m3/h #DIV/0! m3/h

Volume flow rate expanded uncertainty 2.9 % of value #DIV/0! % of value

Calculation spreadsheet v.48 Page 23 of 39Site Visit Report - SV10489 - Town of Monaghan Co-Operative Agricultural and Dairy Society of 43



Lookup tables

Factor Loading Function

Number of measurments dn2 0.8853 0.5914 0.4865 0.436 0.3957 0.378 0.3519 0.337

10 0.32511 0.31512 0.30715 0.28820 0.26825 0.25430 0.24540 0.22750 0.22260 0.21680 0.206

100 0.199




Swirl Test Record BS EN 16911-1:2013Company Town of Monaghan Co-Operative Date of Test 23/08/2017Site Coolshannagh, Monaghan, Co Monaghan. Reference No P0815-02Plant Identification AE-1 Operator Id MM11 1120Test carried out by Aadil Khan TE's TE1, TE2, TE3, TE4

Sampling Line APoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

1 4.80 31.96 151.78 7.16 0.002 17.80 37.42 157.70 7.79 0.003 53.30 11.91 163.22 4.46 0.004 66.30 28.90 163.69 6.89 0.0056789

101112

Average 27.55 159.10 6.57 0.00Min 11.91 151.78 4.46 0.00Max 37.42 163.69 7.79 0.00

Sampling Line BPoint Distance to duct (m) Diff. Pressure (Pa) Temp oC Velocity (m/s) Angle of Swirl

123456789

101112

Average #DIV/0! #DIV/0! #DIV/0! #DIV/0!Min 0 0 0 0Max 0 0 0 0

Calculation spreadsheet v.48 Page 25 of 39




Moisture Content BS EN 14790:2017Company Town of Monaghan Co-Operative 23/08/2017Site Coolshannagh, Monaghan, Co Monaghan. P0815-02Plant Identification AE-1 MM11 1120Test carried out by Aadil Khan TE1, TE2, TE3, TE4Report Number : P0815-02CAR17-01

Dry at Gas Meter: (Vg) 0.07 m3Gas Meter Temperature: (tg) 21.318 294.318 K TCR EM No. Volume:orrection Fact Calibration Date:Ambient Pressure Measured:(Pa) 100.399 kPa EM036 0.5 0.9976 22/02/2017Gas Volume STP (Vgn) 0.06435226 m3 1 1.0020Gas Volume Factor Correction: 0.9791 taken from this table --> 1.5 1.0098Corrected Volume STP 0.063007298 m3 2 1.0151

2.5 1.0258Before EM003 0.5 1.0051 08/05/2017

Readings: Line Impinger 1 Impinger 2 Impinger 3 Impinger 4 Sum: 1 1.01161 261.9 505.3 513.7 355.0 601.7 2237.6 1.5 1.01972 261.9 505.3 513.7 355.0 601.8 2237.7 2 1.02873 262.0 505.4 513.7 355.0 601.8 2237.9 2.5 1.03824 262.0 505.4 513.7 355.0 601.8 2237.9 EM207 0.5 0.9958 17/01/20175 262.0 505.4 513.7 355.0 601.8 2237.9 1 0.98686 262.0 505.4 513.7 355.0 601.8 2237.9 1.5 0.98977 262.0 505.4 513.7 355.0 601.8 2237.9 2 0.99388 262.0 505.4 513.7 355.0 601.8 2237.9 2.5 1.00329 262.0 505.4 513.7 355.0 601.8 2237.9 EM402 0.72 0.9791 27/09/2016

10 262.0 505.4 513.8 355.0 601.8 2238 1.44 0.9824Standard Deviation: 0.0 0.0 0.0 0.0 0.0 0.1 2.16 0.9865

Average: 262.0 505.4 513.7 355.0 601.8 2237.9 2.88 0.9963.6 0.9996

After:Readings: Line Impinger 1 Impinger 2 Impinger 3 Impinger 4 Sum:

1 262.6 505.9 513.8 355.0 603.2 2240.52 262.6 505.9 513.8 355.0 603.2 2240.53 262.7 505.9 513.9 355.0 603.2 2240.74 262.7 505.9 513.9 355.0 603.1 2240.65 262.7 505.9 513.9 355.0 603.1 2240.66 262.7 505.9 513.9 355.0 603.1 2240.67 262.7 505.9 513.9 355.0 603.1 2240.68 262.7 505.9 513.9 355.0 603.1 2240.69 262.7 505.9 513.9 355.0 603.0 2240.5

10 262.7 505.9 513.9 355.0 603.0 2240.5Standard Deviation: 0.0 0.0 0.0 0.0 0.1 0.1

Average: 262.7 505.9 513.9 355.0 603.1 2240.6

Difference in weigh of impingers after and before measurements: 2.7 g

43.01 g/m3

3 %5.38 %

5.1 %5.9 %

Weights: Before Sampling: After Sampling: Difference:Silca trap: 601.8 603.1 1.32 g

Efficiency: 99.8 %

Correction Factors for Volume:

TE's

Date of TestReference NoOperator Id

Corrected to O2ref:

Referenced oxygen:Meas oxygen:

Water vapour content on STP basis:

Water vapour content in % on wet basis:

Calculation spreadsheet v.48

Page 26 of 39




Moisture Uncertainty Calculations

Measured concentration 5.1 % (at STP)

Measured Quantities Symbol Value Standard uncertainty UnitsSampled Volume Vm 0.063007298 uVm 0.001 m3Sampled gas Temperature Tm 470.985 uTm 2 kSampled gas Pressure ρm 100.392 uρm 1 kPaEfficiency Ɛ 99.78 %Oxygen content O2,m 5.38 uO2,m 0.1 % by volumeWater collected in condensation stage 601.80Water collected in adsorption stage 1.32Wate collected in addidional unit 1.32Water collected in trapping m 603.12 um 0.00 gIntermediate calculationsVwc 106.30073 ^2

0.0 0.0 Efficiency uncertain 0.00-0.1 0.0 support 0.00-1.2 1.5 calculations -0.17

√water in trapping unit 24.6

water in adsorption stage 1.1Uncertainty Efficiency^2 0.2Volume ^2 0.3Sensityvity coefficiency 0.4Uncertainty efficiency 0.03

Repatability standard devWeight in the field st 0.1 0.1Sampled Volume 0.002 0.0Sampled gas Temperature 0.02 0.0Sampled gas Pressure 0.3 0.2

Combined measurement uncertainty 0.19 %

Expanded uncertainty as percentage of measured value 7.44 % measured of value expressed with a level of confidence of 95%(Using a coverage factor k=2)

Expanded uncertainty in units of measuremen 0.38 % of water vapour

Overall uncertainty should be less than +/-20% of the measured concentration.


Page 27 of 39




Flue gases O2 BS EN 14789:2017, NOx BS EN 14792:2017, CO BS EN 15058:2017, CO2 ISO 12039:2001Company Town of Monaghan Co-Operative Date of TestSite Coolshannagh, Monaghan, Co Monaghan. Reference NoPlant Identification AE-1 Operator IdTest carried out by Aadil Khan TE'sReport Number : P0815-02CAR17-01

No. O2 % CO2 % CO ppm NOx ppm SO2 ppm1 5.38 12.07 - 256.38 -

Flue Gas parameter Concentration UnitRef O2 Value 3 % If no correction for oxygen use the same value as for measured oxygen.Meas O2 Value O2 5.38 % Deviation?Uncertainty 0.22 % FALSENOx 256.38 ppmConvert to NO2 mg/Nm3 525.6 Nmg/m3Corrected to ref. O2 % NOx 606.4 Nmg/m3 Deviation?Uncertainty 27.8 Nmg/m3 FALSEMass concentration STP, dry, Ref O2 3.7 kg/hrUncertainty 0.0 kg/hrCO #VALUE! ppmConvert to mg/m3 #VALUE! Nmg/m3Corrected to ref. O2 % CO #VALUE! Nmg/m3 Deviation?Uncertainty #REF! Nmg/m3 #REF!Mass concentration STP, dry, Ref O2 #VALUE! kg/hrUncertainty #REF! kg/hrSO2 #VALUE! ppmConvert to mg/Nm3 #VALUE! Nmg/m3Corrected to ref. O2 % SO2 #VALUE! Nmg/m3Uncertainty #REF! Nmg/m3Mass concentration STP, dry, Ref O2 #VALUE! kg/hrUncertainty #REF! kg/hrCO2Meas CO2 Value CO2 12.1 %Uncertainty 3.0 %

Flow Rate STP,dry,RefO2 6134.32 m3/hr

Calibration Cylinder No: Concentration ppm Concentration mg/m3NO EA53XU6 200.76 411.558CO - - #VALUE!SO2 - - #VALUE!

Concentration%CO2 EA53XU6 15.02O2 Ambient Air 20.9Drift Calculations NO ppm CO ppm SO2 ppm O2 % CO2

Sampling time 30 30 30 30 30Span expected Value 200.76 - - 20.9 15.02Zero expected result 0 0 0 0 0Zero reading before 1 0 - - 0 0Span reading before measurement 201.66 - - 20.92 15.04Zero reading before 2 0 - - -0.01 0.04Zero reading after 0 - - 0.05 0.02Span reading after measurement 200 - - 20.94 14.96

Span adjustment 0.996 #VALUE! #VALUE! 0.999 0.999Span Check 1.004 #VALUE! #VALUE! 1.000 1.005Deviation 0.008 #VALUE! #VALUE! 0.001 0.007Drift/Min 0.000275432 #VALUE! #VALUE! 4.7824E-05 0.00022282

Zero adjustment 1 0 #VALUE! #VALUE! 0 0Zero Adjustment 2 0 #VALUE! #VALUE! 0.00999044 -0.0399468Zero check 1 0 #VALUE! #VALUE! -0.0500239 -0.0201071Zero Check 2 0 #VALUE! #VALUE! -0.0500239 -0.0201071Deviation 1 0 #VALUE! #VALUE! 0.05002393 0.0201071Deviation 2 0 #VALUE! #VALUE! 0.06001437 -0.0198397Drift/min 1 0 #VALUE! #VALUE! 0.00166746 0.00067024Drift/min 2 0 #VALUE! #VALUE! 0.00200048 -0.0006613Drift 0.826295745 #VALUE! #VALUE! 0.43062221 0.53636532Actual measured Concentration 256.38 #DIV/0! #DIV/0! 5.38 12.07Corrected concentration for drift 256.38 #VALUE! #VALUE! 5.38 12.07Deviation FALSE #VALUE! #VALUE! FALSE FALSE

TE1, TE2, TE3, TE4

23/08/2017P0815-02

MM11 1120

If the span or zero are higher than 2% of the span value, it is necessary to correct result for

zero and span drifts. The results shal be rejected if the drift in zero or span gas is higher

than 5%


Page 28 of 39




Uncertainty calculation for Gaseous Measurement Oxygen EN14789V2.2 Jul-08

Limit value n/a %vol Calibration gas 20.9 %volMeasured concentration 5.38 %vol Full Scale 25 %vol

Performance characteristic Value specificationResponse time 56 seconds < 200 sLogger sampling interval 15 seconds 0.00 % volMeasurement period 30 minutes 0.00 % valueNumber of readings in measurement 30 Assuming 1 minute collected over 1 hourRepeatability at zero 0.03 % by volume stdev <0.2 % rangeRepeatability at span level 0.02 % by volume stdev <0.4 % rangeDeviation from linearity 0.1 % vol +/- <0.3 % volumeZero drift (during measurement period) 4.7824E-05 % vol at zero level +/- <2% of volume / 24hrSpan drift (during measurement period) 4.7824E-05 % vol at span level +/- <2% volume/24hr min max value at calibvolume or pressure flow dependence 0.1 % of fs / 10l/h +- 5 l/h <1% range flow 5 15 10 l/hatmospheric pressure dependence 0.19 % of fs/kPa +- 2kPa < 1.5 % range pressure 99.00 101 100 kPaambient temperature dependence -0.21 % by volume /10K +- 15K <0.3% volume 10 K temp 280 285 285 KCO2 (% vol) 15 0.07 % by volume per 15 CO2 range 8 15 0 % volNO (mg/m3) 300 0.02 % by volume per 300 NO range 100 150 0 mg/m3NO2 (mg/m3) 30 0 % by volume per 30 NO2 range 5 7.5 0 mg/m3Combined interference 0.56 % range <2% range Voltage 105 115 110 VDependence on voltage 0.02 % by volume /10V +- 5% < 0.1%vol /10 voltLosses in the line (leak) 0.27 % of value < 2% of valueUncertainty of calibration gas 0.5 % of value

Performance characteristic Uncertainty Value of uncertainty quantity % volStandard deviation of repeatability at zero ur0 for mean Only use rep at spanStandard deviation of repeatability at span level urs for mean 0.00Lack of fit ufit 0.06Drift u0dr 0.00volume or pressure flow dependence uspres 0.01atmospheric pressure dependence uapres 0.03ambient temperature dependence utemp -0.06CO2 0.05 Use largest of sum of all positive or all negative influencesNO 0.01 0.06 all +ves CriteriaNO2 0.00 0 all -ves sum <2% valueCombined interference (from mcerts) 0.08 0.06 largest 0.107686dependence on voltage uvolt 0.01 Value to use for intereference uncertaintylosses in the line (leak) uleak 0.01 unit 0.06Uncertainty of calibration gas ucalib 0.02

Measurement uncertainty 5.38 %volCombined uncertainty 0.11 %vol% of value 2.05 %Coverage factor k = 2Expanded uncertainty expressed with a level of confidence of 95% 4.09 % of valueExpanded uncertainty expressed with a level of confidence of 95% 0.22 % vol

Requirement for SRM is that Uncertaitny should be < 6% of value, on a dry gas basis, or 0.3% expressed as a volume concentration

Effect of drift

range of variation from conditions at calibration


Page 29 of 39




Uncertainty calculation for Gaseous Measurement NOxv4

Limit value 900 mg.m-3 (corrected) NOGas NO Correction for reference conditionsFull Scale 250 ppm O2, % Moisture, %Pressure, Temperature, K

Measured concentration 256.38 ppm Cal gas conc 200.76 ppm ref 3 0.00 101.30 273.00Measured concentration 525.59 mg.m-3 (273K, 101.3kPConversion 2.05 measured 5.38 5.08 100.39 470.99Ratio NO/NO2 5.00 Full Scale 512.5 mg.m-3 (NO2) Factors 1.15 1.05 1.01 1.73

Cal gas conc 411.558 mg.m-3 (NO2) Correction Factor 2.12

Performance characteristic Value specification Effect of driftResponse time 55 seconds 180.000 0.00 mg/m3Number of readings in measurement 120 0.00 % valueRepeatability at zero 0 % full scale 0.200Repeatability at span level 0.1 % full scale 2.000Deviation from linearity 0.75 % of value 2.000 rangesZero drift 0 % full scale 2.000 min max value at calibSpan drift 0.000275432 % full scale 2.000 flow 0.3 0.5 0.4volume or pressure flow dependence 0.02 % of full scale/kPa 0.033 pressure 101.30 101.5 101.3atmospheric pressure dependence 0.1 % of value/kPa 0.750 temp 283 289 283ambient temperature dependence 0.01 % full scale/10K 0.300 NH3 range 0 0 0NH3 (20 mg/m3) 1.2 mg/m3 CO2 range 0 0.5 0CO2 (15%) 1.2 % by vol H2O range 0 0.5 0H2O (30%) 1.2 % by vol 4.000 Instrument Voltage Rating 110dependence on voltage -0.23 % full scale/10V 2%fs/10V Voltage 104.5 115.5 110converter efficiency 95 % 95%losses in the line (leak) 0.29 % of value 2% of valueUncertainty of calibration gas 2 % of value

Measurement performance related to stationary conditionsPerformance characteristic UncertaintyStandard deviation of repeatability at zero ur0 for mean use rep at spanStandard deviation of repeatability at span level urs for mean 0.01 Use largest negative or positive interferent effectLack of fit ufit 2.22 0 0.00Drift u0dr 0.00 0 0.02volume or pressure flow dependence uspres 0.00 0 0.01atmopsheric pressure dependence uapres 0.06 0 0.03ambient temperature dependence utemp 0.00 Interference uncertainty 0.03NH3 (20 mg/m3) uinterf 0.00CO2 (15%) 0.02H2O (30%) 0.01

Dependence on voltage uvolt -0.07Converter efficiency uceff 0.76losses in the line (leak) uleak 0.88Uncertainty of calibration gas ucalib 6.07

Measurement uncertainty Result 525.59 mg/m3

Combined uncertainty 6.57 mg/m3

Expanded uncertainty k = 2 13.13 mg/m3

Uncertainty corrected to std conds 27.79 mg.m-3 (corrected)Expanded uncertainty expressed with a level of confidence of 95% 3.09 % ELVExpanded uncertainty expressed with a level of confidence of 95% 27.79 mg.m-3 at ELV

Requirement in standard is for uncertainty to be < 10% at ELV, or the lowest limit value assigned by the local authorities, expressed on a dry basis before correction to O2 reference concentration

Value of uncertainty quantity


Page 30 of 39




Uncertainty calculation for Gaseous Measurement CO2V2.2 Jul-08

Limit value n/a %vol Calibration gas 15.02 %volMeasured concentration 12.07 %vol Full Scale 25 %vol

Performance characteristic Value specificationResponse time 60 seconds < 200 sLogger sampling interval 60 seconds 0.00 % volMeasurement period 30 minutes 0.01 % valueNumber of readings in measurement 30 Assuming 1 minute collected over 1 hourRepeatability at zero 0 % by volume stdev <0.2 % rangeRepeatability at span level 0.1 % by volume stdev <0.4 % rangeDeviation from linearity 0.13 % vol +/- <0.3 % volumeZero drift (during measurement period) 0.000670237 % vol at zero level +/- <2% of volume / 24hrSpan drift (during measurement period) 0.000222818 % vol at span level +/- <2% volume/24hr min max value at calibvolume or pressure flow dependence 0 % of fs / 10l/h +- 5 l/h <1% range flow 5 15 10 l/hatmospheric pressure dependence 0.3 % of fs/kPa +- 2kPa < 1.5 % range pressure 99.00 101 100 kPaambient temperature dependence -0.07 % by volume /10K +- 15K <0.3% volume 10 K temp 280 285 285 KCO2 (% vol) 15 0.07 % by volume per 15 CO2 range 8 15 0 % volNO (mg/m3) 300 0.02 % by volume per 300 NO range 100 150 0 mg/m3NO2 (mg/m3) 30 0 % by volume per 30 NO2 range 5 7.5 0 mg/m3Combined interference 0.56 % range <2% range Voltage 105 115 110 VDependence on voltage 0.1 % by volume /10V +- 5% < 0.1%vol /10 voltLosses in the line (leak) 2 % of value < 2% of valueUncertainty of calibration gas 0.5 % of value

Performance characteristic Uncertainty Value of uncertainty quantity % volStandard deviation of repeatability at zero ur0 for mean Only use rep at spanStandard deviation of repeatability at span level urs for mean 0.02Lack of fit ufit 0.08Drift u0dr 0.00volume or pressure flow dependence uspres 0.00atmospheric pressure dependence uapres 0.04ambient temperature dependence utemp -0.02CO2 0.05 Use largest of sum of all positive or all negative influencesNO 0.01 0.06 all +ves CriteriaNO2 0.00 0 all -ves sum <2% valueCombined interference (from mcerts) 0.08 0.06 largest 0.241312dependence on voltage uvolt 0.03 Value to use for intereference uncertaintylosses in the line (leak) uleak 0.14 unit 0.06Uncertainty of calibration gas ucalib 0.03

Measurement uncertainty 12.07 %volCombined uncertainty 0.18 %vol% of value 1.52 %Coverage factor k = 2Expanded uncertainty expressed with a level of confidence of 95% 3.04 % of valueExpanded uncertainty expressed with a level of confidence of 95% 0.37 % vol

Requirement for SRM is that Uncertaitny should be < 6% of value, on a dry gas basis

range of variation from conditions at calibration

Effect of drift


Page 31 of 39




Date / Time NOx (ppm) O2 (%)23/08/2017 13:44 13.06 256.33 4.3623/08/2017 13:44 12.63 262.33 4.7423/08/2017 13:44 10.39 227.67 7.4923/08/2017 13:45 12.58 258.00 4.8823/08/2017 13:45 12.80 293.67 4.5223/08/2017 13:45 13.09 317.33 4.1123/08/2017 13:45 13.09 327.00 4.0923/08/2017 13:46 13.08 331.33 4.0923/08/2017 13:46 13.14 331.00 4.0223/08/2017 13:46 13.05 328.00 4.1123/08/2017 13:46 13.00 318.33 4.1823/08/2017 13:47 12.70 302.67 4.5323/08/2017 13:47 12.50 274.67 4.8123/08/2017 13:47 10.13 228.67 7.5623/08/2017 13:47 10.60 226.67 7.3223/08/2017 13:56 10.41 229.00 7.4723/08/2017 13:56 12.62 259.00 4.8323/08/2017 13:56 12.69 290.33 4.6423/08/2017 13:56 12.46 288.00 4.9023/08/2017 13:57 12.21 265.33 5.1123/08/2017 13:57 9.67 211.67 8.3523/08/2017 13:57 11.83 244.00 5.8123/08/2017 13:57 12.80 257.67 4.5223/08/2017 13:58 12.99 257.67 4.2523/08/2017 13:58 13.20 263.00 3.9423/08/2017 13:58 13.10 267.00 4.0423/08/2017 13:58 12.65 263.33 4.6023/08/2017 13:59 11.96 256.33 5.4723/08/2017 13:59 11.80 251.33 5.7223/08/2017 13:59 12.02 254.00 5.4523/08/2017 13:59 11.79 253.67 5.6923/08/2017 14:00 11.71 250.00 5.8523/08/2017 14:00 10.90 246.00 6.7123/08/2017 14:00 9.86 214.67 8.1823/08/2017 14:00 9.05 206.33 9.1623/08/2017 14:01 10.85 216.00 7.1723/08/2017 14:01 10.74 232.67 6.8223/08/2017 14:01 10.75 224.33 7.2223/08/2017 14:01 11.96 250.67 5.6023/08/2017 14:02 12.21 255.67 5.2423/08/2017 14:02 12.52 259.00 4.8523/08/2017 14:02 12.51 259.67 4.8423/08/2017 14:02 10.81 247.67 6.7623/08/2017 14:03 8.90 201.33 9.4223/08/2017 14:03 12.97 238.00 4.5023/08/2017 14:03 14.29 259.33 2.5823/08/2017 14:03 12.94 247.33 4.1523/08/2017 14:04 12.78 267.00 4.4623/08/2017 14:04 11.56 251.67 5.7823/08/2017 14:04 8.78 196.67 9.5323/08/2017 14:04 10.51 226.67 7.4123/08/2017 14:05 12.56 246.67 4.8923/08/2017 14:05 11.11 240.33 6.3723/08/2017 14:05 10.61 221.00 7.3523/08/2017 14:05 11.37 239.00 6.3323/08/2017 14:06 12.88 268.33 4.4523/08/2017 14:06 12.82 291.33 4.4623/08/2017 14:06 12.47 274.67 4.8723/08/2017 14:06 11.05 238.00 6.5423/08/2017 14:07 11.82 243.00 5.8023/08/2017 14:07 12.37 256.00 5.0223/08/2017 14:07 12.73 259.33 4.5723/08/2017 14:07 13.04 260.67 4.1523/08/2017 14:08 13.04 265.00 4.1323/08/2017 14:08 11.60 248.00 5.89




Date / Time NOx (ppm) O2 (%)23/08/2017 14:08 12.66 259.33 4.6423/08/2017 14:08 12.05 258.67 5.2923/08/2017 14:09 10.53 225.00 7.3023/08/2017 14:09 12.07 241.33 5.4923/08/2017 14:09 12.59 260.67 4.6123/08/2017 14:09 9.74 215.33 8.2223/08/2017 14:10 9.42 208.00 8.7623/08/2017 14:10 11.04 219.00 6.9123/08/2017 14:10 12.61 261.67 4.7323/08/2017 14:10 11.84 247.67 5.5723/08/2017 14:11 11.59 236.33 6.1123/08/2017 14:11 12.63 262.00 4.6523/08/2017 14:11 12.41 261.33 4.9523/08/2017 14:11 11.52 242.00 6.0423/08/2017 14:12 12.16 247.67 5.3623/08/2017 14:12 12.77 268.00 4.5123/08/2017 14:12 12.53 281.67 4.7823/08/2017 14:12 12.44 261.33 4.8923/08/2017 14:13 11.74 245.33 5.7623/08/2017 14:13 12.66 255.33 4.6723/08/2017 14:13 12.54 277.67 4.7623/08/2017 14:13 12.50 264.00 4.8523/08/2017 14:14 11.92 247.00 5.5423/08/2017 14:14 12.13 253.33 5.3123/08/2017 14:14 12.72 257.33 4.5723/08/2017 14:14 12.22 265.67 5.1723/08/2017 14:15 12.88 258.33 4.3623/08/2017 14:15 11.69 243.33 5.8023/08/2017 14:15 12.55 255.00 4.7923/08/2017 14:15 12.17 264.67 5.2523/08/2017 14:16 12.24 251.00 5.1123/08/2017 14:16 12.61 254.67 4.7123/08/2017 14:16 12.43 276.33 4.8823/08/2017 14:16 12.37 259.33 5.0123/08/2017 14:17 12.09 248.00 5.3123/08/2017 14:17 12.32 255.33 5.0523/08/2017 14:17 12.64 258.33 4.6423/08/2017 14:17 12.00 260.33 5.3923/08/2017 14:18 12.53 256.33 4.8323/08/2017 14:18 12.47 265.00 4.8123/08/2017 14:18 12.06 265.00 5.3623/08/2017 14:18 12.10 260.67 5.3423/08/2017 14:19 13.49 258.33 3.6623/08/2017 14:19 13.56 256.33 3.4523/08/2017 14:19 12.94 259.67 4.2123/08/2017 14:19 12.92 288.00 4.3123/08/2017 14:20 12.29 280.00 5.0523/08/2017 14:20 12.03 254.67 5.4023/08/2017 14:20 12.14 249.00 5.3223/08/2017 14:20 12.51 259.33 4.8223/08/2017 14:21 12.61 258.33 4.7023/08/2017 14:21 12.46 274.33 4.8723/08/2017 14:21 12.20 271.33 5.1723/08/2017 14:21 11.88 247.00 5.5923/08/2017 14:22 12.53 258.33 4.84

Average 12.07 256.38 5.38




Particulates BS EN 13284-1:2002Company Town of Monaghan Co-Operative Date of Test 23/08/2017Site Coolshannagh, Monaghan, Co Monaghan. Reference No P0815-02Plant Identification AE-1 Operator Id MM11 1120Test carried out by Aadil Khan TE's TE1, TE2, TE3, TE4

Report Number: P0815-02CAR17-01

Particulate ConcentrationsLab Results g Certificate Number: Laboratory: Accreditation status: Analytical Method Date of AnalysisFilter #1 0.07915 5790/625/05 Fitz Scientific MCERTS Gravimetry 30/08/2017Rinse 0.00078 5790/625/06 Fitz Scientific MCERTSFilter Blank 0.00006 5790/625/07 Fitz Scientific MCERTSRinse Blank 0.00005 5790/625/08 Fitz Scientific MCERTSLOD Filter 0.00006 n/aLOD Nozzle Wash 0.00005 n/aTotal Particulate g mg Deviation?LOD 0.00011 0.11 Nozzle 10 FALSERun 0.07993 79.93 Isokinetic Ratio -1.1 FALSEBlank 0.00011 0.11 5 up / 2 down (Y/N?) No TRUE

No of ports 1 TRUERequirements:

Dry at Gas Meter: (Vg) 1.02400 m3 Blank < 10% ELV FALSEGas Meter Temperature: (tg) 22.88700 295.887 K ELV>5mg/m3 --> LOD<10%ELV FALSEAmbient Pressure Measured:(Pa) 100.41100 KPa ELV<=5mg/m3 --> LOD<20%ELV FALSEGas Volume STP (Vgn) 0.936501691 m3Gas Volume Factor Correction: 0.98240Corrected Volume STP 0.920019262 m3

Resultsmg/Nm3 @ STP Dry Gas

mg/Nm3 @ STP Dry Gas Ref Oxygen Uncertainty mg/m3 kg/h Uncertainty Kg/h

LOD 0.1 0.1 n/a 0.001 n/aRun 86.9 100.2 3.317 0.615 0.02035Blank 0.1 0.1 0.005 0.001 0.00003

O2 meas = 5.384305552 %O2 Reference = 3 %

Flow Rate as reference conditions 6134.32 m3/hr

Before Blank : After Blank: Before Sample After SampleLeak Test Results: 0 0 0.1 0.15 cc/min


Page 34 of 39




Run CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14 Measurement EquationLimit value (ELV) 150 mg.m-3 Reference oxygen 3 % by volumeMeasured concentration 100.2 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.920019262 uVm 0.001 m3 0.11 <=2%Sampled gas Temperature Tm 470.985 uTm 2 k 0.42 <=1%Sampled gas Pressure ρm 100.392 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 5.080532585 uHm 1 % by volume 19.68 <=1%Oxygen content O2,m 5.384305552 uO2,m 0.1 % by volume 1.86 <=5%Mass particulate m 79.93 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0.0008152 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.55uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.51

Corrected volume V 0.50 uV 0.008 m3 1.52

Factor for O2 correction fc 1.15uncertainty components symbol sensitivity coeff u

O2,m 0.07 0.007Factor for O2 Correction ufc 1.15 0.007 0.64

Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume (standard V 0.50 m3 199.80 1.53 mg.m-3 1.52 %Mass m 79.93 mg 1.25 0.00 mg.m-3 0.00 %Factor for O2 Correction fc 1.15 86.88 0.65 mg.m-3 0.64 %Leak L 0.00 mg.m-3 1.00 0.00 mg.m-3 0.00 %Uncollected mass UCM 0.00 mg 1.25 0.00 mg.m-3 0.00 %Combined measurement uncertainty 1.66 mg.m-3


Expanded uncertainty in units of measurement 3.32 mg.m-3

Expanded uncertainty as percentage of limit value 2.2 % ELV

Requirement in standard is for uncertainty to be < 30% at ELV at standard conditions

sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


Page 35 of 39




Blank CalculationsUncertainty calculation for EN 13284 Determination of low range mass concentration of dust, Manual Gravimetric Methodv14

Measurement EquationLimit value (ELV) 15 mg.m-3 Reference oxygen 3 % by volumeMeasured concentration 0.1 mg.m-3 (at reference conditions)

Measured Quantities Symbol Value Standard uncertainty Units Uncertainty as percentage Uncertainty aRequirement of stdSampled Volume Vm 0.920019262 uVm 0.001 m3 0.11 <=2%Sampled gas Temperature Tm 470.985 uTm 2 k 0.42 <=1%Sampled gas Pressure ρm 100.392 uρm 1 kPa 1.00 <=1%Sampled gas Humidity Hm 5.080532585 uHm 1 % by volume 19.68 <=1%Oxygen content O2,m 5.384305552 uO2,m 0.1 % by volume 1.86 <=5%Mass particulate m 0.11 um 0.00 mg 0.00 0.00 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meterLeak L 0 % 0.00 <=2%Uncollected Mass UCM 0 mg 0 <=10%(Instack filter - no rinse)Intermediate calculationsFactor for std conds fs 0.55uncertainty components symbol sensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.51


Factor for O2 correction fc 1.15uncertainty components symbol sensitivity coeff u

O2,m 0.07 0.007Factor for O2 Correction ufc 1.15 0.007 0.64

Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume (standard V 0.50 m3 0.27 0.00 mg.m-3 0.00 %Mass m 0.11 mg 1.25 0.00 mg.m-3 0.00 %Factor for O2 Correction fc 1.15 0.12 0.00 mg.m-3 0.00 %Leak L 0.00 mg.m-3 1.00 0.00 mg.m-3 0.00 %Uncollected mass UCM 0.00 mg 1.25 0.00 mg.m-3 0.00 %Combined measurement uncertainty 0.00 mg.m-3



Expanded uncertainty as percentage of limit value 0.0 % ELVNote:

sm fVV

m

refc O

Of

,2

,2

2121

3.101273

100)100( m

m

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Hf

cfVmc


Page 36 of 39




SO2 BS EN 14791:2017Company: Town of Monaghan Co-Operative Date of test: 23/08/2017Site: Coolshannagh, Monaghan, Co Monaghan. Reference No: P0815-02Plant Identification AE-1 Operator Id MM11 1120Test Carried out by: Aadil Khan TE's TE1, TE2, TE3, TE4Report Number: P0815-02CAR17-01

Run Laboratory Results: mgSO4/L Cert Number: Laboratory Accredtation Analytical MethDate of AnalysisLOQ 0.1 Fitz Scientific MCERTS IC 01/09/2017Impinger 1 365.600 5790/625/01 Fitz Scientific MCERTSImpinger 2 0.236 5790/625/02 Fitz Scientific MCERTS

BlankImpinger 1 0.100 5790/625/03 Fitz Scientific MCERTSImpinger 2 0.100 5790/625/04 Fitz Scientific MCERTS

Run BlankSample Volumes

ml L ml L181.8 0.1818 130.0 0.13144.6 0.1446 124.1 0.1241

0.063007298 Nm3

SO4 mgmgSO2/m3 at

STP,Dry

mgSO2/m3 at Reference Conditions

Uncertainty mgSO2/m3 SO2 kg/hr

Uncertainty SO2 kg/hr

LOQ 0.03 0.3 0.4 n/a 0.002444084 n/aRun 66.50 703.6 811.8 75.29 4.979536679 0.461823786Blank 0.03 0.3 0.3 0.03 0.001902701 0.000176465

3 %5.4 %

6134.32 m3/hr

DeviationAbsorption efficiency(Impinger 1 should absorb 95% of total sulphate): 99.9 % Deviation FALSEor result in second absorber should be <LOQ

Sampled Volume corrected to reference conditionsSTP, Dry

Flow Rate at reference conditions

Reference oxygen:Measured oxygen:


Page 37 of 39




Uncertainty calculation for EN 14791 Determination of mass concentration of sulphur dioxide, Reference methodV2RunLimit value (ELV) 1700 mg.m-3 Reference oxygen 3 % by volumeMeasured concen 811.8 mg.m-3 (at reference conditions)

Measured QuantitSymbol Value Standard uncertainty Units Uncertainty as percUncertainty at lv Requirement of stdSampled Volume Vm 0.063007298 uVm 0.001 m3 1.59 <=2%Sampled gas Tem Tm 470.985 uTm 2 k 2.00 <2.5 kSampled gas Pres ρm 100.392 uρm 1 kPa 1.00 <=1%Sampled gas Hum Hm 5.080532585 uHm 1 % by volume 19.68 <=1%Oxygen content O2,m 5.38 uO2,m 0.1 % by volume 1.86 <=5%Concentration in C 365.8 uC 10.97508 mg/l 3.00 <5%Impinger solution VS 326.4 uVS 0.001 l 0.00 <1%Mass SO2 m 66.5 um 2.00 mg 3.00 1.43 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meteLeak L 2 % 2.00 <=2%

Intermediate calculationsFactor for std con fs 0.55uncertainty comp symbolsensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.51


Factor for O2 cor fc 1.15uncertainty comp symbolsensitivity coeff u

O2,m 0.07 0.007Factor for O2 Cor ufc 1.15 0.007 0.64

Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume V 0.03 m3 23628.24 26.62 mg.m-3 3.28 %Mass m 66.50 mg 12.21 24.35 mg.m-3 3.00 %Factor for O2 Corre fc 1.15 703.62 5.23 mg.m-3 0.64 %Leak L 9.37 mg.m-3 1.00 9.37 mg.m-3 1.15 %

Combined uncertainty 37.64 mg.m-3



Expanded uncertainty as percentqge of limit value 4.4 % ELV

sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


Page 38 of 39




Uncertainty calculation for EN 14791 Determination of mass concentration of sulphur dioxide, Reference methodBlank

Limit value (ELV) 170 mg.m-3 Reference oxygen 3 % by volumeMeasured concen 0.3 mg.m-3 (at reference conditions)

Measured QuantitSymbol Value Standard uncertainty Units Uncertainty as percUncertainty at lv Requirement of stdSampled Volume Vm 0.1 uVm 0.001 m3 1.59 <=2%Sampled gas Tem Tm 470.985 uTm 2 k 2.00 <2.5 kSampled gas Pres ρm 100.392 uρm 1 kPa 1.00 <=1%Sampled gas Hum Hm 5.080532585 uHm 1 % by volume 19.68 <=1%Oxygen content O2,m 5.38 uO2,m 0.1 % by volume 1.86 <=5%Concentration in C 0.2 uC 0.006 mg/l 3.00 <5%Impinger solution VS 254.1 uVS 0.001 l 0.00 <1%Mass SO2 m 0.0 um 0.00 mg 3.00 0.01 <5% of limit valueNote - Sampled gas humidity, temperature and pressure are values at the gas meteLeak L 2 % 2.00 <=2%

Intermediate calculationsFactor for std con fs 0.55uncertainty comp symbolsensitivity coeff u (in units of fs)

ρm 0.005 0.005Hm 0.006 0.006Tm 0.001 0.002ufs 0.008 1.51


Factor for O2 cor fc 1.15uncertainty comp symbolsensitivity coeff u

O2,m 0.07 0.007Factor for O2 Cor ufc 1.15 0.007 0.64

Parameter Value Units Sensitivity coeff Uncertainty contribution Uncertainty as %Corrected Volume V 0.03 m3 9.03 0.01 mg.m-3 3.28 %Mass m 0.03 mg 12.21 0.01 mg.m-3 3.00 %Factor for O2 Corre fc 1.15 0.27 0.00 mg.m-3 0.64 %Leak L 0.00 mg.m-3 1.00 0.00 mg.m-3 1.15 %

Combined uncertainty 0.01 mg.m-3



Expanded uncertainty as percentqge of limit value 0.0 % ELV

sm fVV

m

refc O

Of

,2

,2

2121

cfVmc

3.101273

100)100( m

m

ms T

Hf


Page 39 of 39


Summary

FOLLOW-UP ACTIONS

You are required to complete the instructions and actions, as outlined in this report, within the specified timeframe. Where required, you shall respond to actions specified in Compliance Investigations within the required timeframe.The licensee shall maintain documentary evidence, for review by the EPA, that the prescribed corrective actions were completed within the required timeframe.

(i) Compliance Investigations

You are not required to respond directly to items contained in this EPA site visit report; where an issue requires a direct response, the EPA will generate a Compliance Investigation through the EDEN system. You will receive notification when a Compliance Investigation instruction or action is generated.

(ii) Publication of reports and licensee response.

Please note that this Site Visit Report will be made available for public viewing via the EPA’s Licence Enforcement Access Portal within one day of the issue date and will be published on the Licence Details Page of the EPA’s website, www.epa.ie, that relates to your licence 60 calendar days after the issue date.

You may if you choose submit, within 45 calendar days of the issue date of this Site Visit Report, a Licensee Public Response that will be published alongside the Site Visit Report. This Response, should you wish to avail of it, provides you with an opportunity to inform the public about how you are implementing the actions set out in the report, activities underway, timescales and target completion dates. Please be aware that the content of your Licensee Public Response must be factual and should not breach the EPAs stated online publication standards.

If you wish to submit a Licensee Public Response to an EPA Site Visit Report, you should do this by clicking on the ‘Make a Response’ link on the Site Visits page in EDEN. A .pdf document containing your response can be attached and submitted from here.

(iii) Response to Site visit report

Where you do wish to respond directly to a site visit report, you should do this by generating a ‘Licensee Return’ of the type ‘Site Updates/Notifications’ and the sub-type ‘Response to EPA Report’ in EDEN.

Please note that you are required to comply with the conditions of your licence at all times, and where noncompliance occurs you must restore compliance within the shortest possible time. These actions will be verified during subsequent EPA visits.

Please quote the above Inspection Reference Number in any future correspondence in relation to this Report.


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