sub-surface soil vapor sampling trip report - work ... · work assignment #eac00056 - sub-surface...

KMI2.9001

Lockheed Martin Technology Services Environmental Services REAC 2890 Woodbridge Avenue Building 209 Annex Edison, NJ 08837-3679 Telephone 732-321-4200 Facsimile 732-494-4021 LOCKHEED MA R T I N /

DATE: 14 March 2008

FROM:

THROUGH:

THROUGH:

TO:

Jeffrey Bradstreet, REAC Air Response Section Leader'

Christopher Gussman, REAC Task Leader JQ*"

Philip Solinski, REAC Air Team Leader(^Z^Q&^l

George Prince, U.S. EPA/ERT, Work Assignment Manager

SUBJECT: KAUFFMAN AND MINTEER, JOBSTOWN, NEW^JERSEY WORK ASSIGNMENT #EAC00056 - SUB-SURFACE SOIL VAPOR SAMPLING TRIP REPORT

BACKGROUND

Under this work assignment (WA), Response, Engineering and Analytical Contract (REAC) personnel have assisted the Environmental Protection Agency/Environmental Response Team (EPA/ERT) with the ongoing maintenance and monitoring of a phytoremediation effort utilizing hybrid poplar trees and native black willows to remove volatile organic compounds (VOCs) from contaminated soil and groundwater at the Kauffman and Minteer (K&M) Site located in Jobstown, Burlington County, New Jersey (NJ). The purpose of the June 2007 mobilization was to conduct a vapor intrusion investigation at two commercial buildings and one home for selected TO-15 chemicals including trichloroethene (TCE) and its breakdown products and benzene, toluene, ethylbenzene-and xylenes (BTEX).

The site consists of a garage/office building, a former truck wash bay area, a former collection pit area, a drainage ditch, and a former unlined lagoon. A bulk liquid transportation business once operated at the site. This business transported materials such as synthetic organics, plasticizers, resins, vegetable oils, petroleum oils, and alcohols. Wash water from tanker trucks was discharged to the unlined lagoon Since 1978, K&M has been subjected to numerous investigations by state and federal agencies. As a result, the Site was placed on the National Priorities List on March 30,1989. These investigations were documented in the Final Remedial Investigation Report and the Feasibility Study. The EPA Region II issued a Record of Decision (ROD) for the K&M Site in September 1996. The selected remedy included closure of the unlined lagoon, long-term monitoring of the contaminated shallow ground water underlying the site, andplacement of institutional controls to restrict shallow ground water use m me vicinity of the Site. I

In 1996, over 300 trees were planted at a former truck wash station in Jobstown, NJ as part of a pilot study to determine the effectiveness of phytoremediation technology at the Site. Trees were planted in a former truck wash bay area, drainage areas and in a former waste lagoon area. Soils and ground water in these areas have been shown to be contaminated with trichloroethene (TCE), dichloroethylene and associated breakdown products.

OBSERVATIONS AND ACTIVITIES

Between 17 and 19 December 2007, REAC mobilized to the Site to install sub-floor sampling ports in the Former K&M building. The building (currently occupied by the Springfield Township Emergency Squad, Station 219) is located at 7 Jobstown-Juliustown Road. The office area where the Squad operates is elevated approximately 4 inches off of the concrete slab of die building. A sub-floor sampling location is defined as a sample collected from between the plywood floor and the concrete slab. REAC also collected ambient, indoor and sub-floor air samples. Additionally, sub-slab soil gas samples were collected from ports that were installed in June of2007. Figure 1 depicts the location of the sub-slab

0056-DTR-031408 1

r 185812

KMI2.9002

sampling ports.

The sub-floor soil gas wells were installed at locations deemed clear of utilities and were chosen in consultation with the ERT Work Assignment Manager (WAM). Wells were installed flush with the basement slab and capped with a Teflon* coated fitting that was removed during sampling operations. Wells were installed in accordance with REAC standard operating procedure (SOP) #2082, Construction and Installation of Permanent Sub-Slab Soil Gas Wells.

On 17 December 2007, two sub-floor soil gas wells were installed in the former K&M building. Sub-slab soil gas weU sampling began on 18 December 2007 and were collected 24 hours later on 19 December 2007 Two ambient air samples were collected during the day of sampling in the field behind the former K&M building.

REAC personnel collected a 24-hour sample from each of the locations using a 6-liter (L) SUMMA* canister in accordance with REAC SOP #1704, SUMMA* Canister Sampling. A 4 to 5-L time-weighted average (TWA) sample was collected during a 22 to 24-hour sampling event The ambient, indoor, and sub-slab samples collected in SUMMA* canisters were properly documented and shipped to a subcontracted laboratory for analysis. Air sample analysis was performed in accordance with REAC SOP #1814 which is based on EPA Method TO-15, Determination of Volatile Organic Compounds (VOCs) in Air Collected in Specially-Prepared Canisters and Analyzed b> Gas Chromatography/Mass Spectrometry (GC/MS). The Target Compound List (TCL) included vinyl chloride 1 1 dichloroethene, trans-1,2-dichloroethene, 1,1-dichloroethane, cis-l,2-dichloroethene, 1,2-dichloroethane TCE tetochloroethene (PCE), 1,1,1-tricMoroethane, benzene, , toluene, ethylbenzene, m&p-xylene, o-xylene, me'thylene chlonde,methyl-t-butyl-ether,andchlorobenzene. mvicnc

RESULTS

A total of four sub-slab soil gas, two sub-floor, six indoor and two ambient air samples were collected and sent for VOC analysis to Columbia Analytical Services in Sun Valley, CA.

Table 1 contains the indoor and ambient air sampling results from the.December 2007 sampling event in micrograms per cubic meter (fig/m3). Table 2 contains the same results in parts per billion by volume (ppbv). Table 3 contains the sub-slab soil gas sampling results from the December 2007 sampling event in fig/iaK Table 4 contains the same results in ppby. The New Jersey Department of Environmental Protection (NJDEP) non-residential vapor intrusion screening levels (VISL) are provided m each of these tables.

Methyl tert-butyl ether (MTBE) and benzene were both detected in the indoor air of the former K&M building above the NJDEP non-residential VISL at 32 jig/m3 (9 ppbv) for MTBE and 73 /ig/m3 (2.3 ppbv) for benzene intfae Fire Department Bay. These compounds were also detected in the two sub-floor samples collected from the EMS offices at 8.2 pg/m3 (2.3 ppbv) for MTBE and 2.7 ftg/m3 (0.86 ppbv) for benzene. However, neither compound was detected in any of the sub-slab samples. • .

Both TCE and PCE were detected above the NJDEP indoor non-residential VISL at 6 ftg/m3 (1.1 ppbv) for TCE and 9.3 /tg/m3 (1.4 ppbv) for PCE in the Fire Department Bay. These compounds were also detected in the two sub-floor samples collected from the EMS offices at 1.9 pg/m3 (0.35 ppbv) for TCE and 15 pg/m3 (2.1 ppbv) for PCE. Both TCE and PCE were detected above the NJDEP soil gas non-residential VISL at 56000 pg/m3 (10000 ppbv) for TCE beneath the Recreation Department (Port 4) and 110000 Atg/m3 (17000 ppbv) for PCE beneath the Fire Department Bay (Port

The sub-slab soil gas concentration for cis- 1,2-dichloroethene beneath the former K&M building were detected above the NJDEP soil gas non-residential VISL at 18000 /ig/m3 (4600 ppbv) beneath the Recreation Department (Port 4) The indoor air concentrations of cis-l,2-dichloroethene were detected at 3.3 ftg/m3 (0.82 ppbv), however, were below the NJDEP indoor non-residential VISL.

0056-DTR-031408 2

KMI2.9003

Please note that due to the presence of other contaminants in high concentrations, the method reporting limit (MRL) increased for the sub-slab samples collected from beneath the EMS Bay, FD Bay and Recreation Department Bay. Therefore the MRL's were higher than the NJDEP VISL for vinyl chloride, 1,2-dichlorethane, and benzene.

Methylene chloride, benzene, toluene, ethyl benzene and xylene were present above the reporting limit in the two ambient air samples. The highest concentration was 1.6 /tg/m5 (0.43 ppbv) of toluene. PCE was also detected in the bom ambient air samples at 0.23 jtg/m3 (0.034 ppbv).

The SUMMA* Canister Analytical Report is provided in Appendix A. The Air Sampling Worksheets are provided in Appendix B.

FUTURE ACTIVITIES

No further air sampling activities are anticipated at this time.

cc: Central File WA EAC00056 (w/attachments) Electronic File: I:/Archive/REAC4/0056/D/TR/0056-DTR-031108 Dennis Miller, REAC Program Manager (cover page only)

0056-DTR-031408 3

KMI2.9004

Tables

•

Table 1

TO-15 Indoor Air Sampling Results in ug/m3

Kaufman and Minteer Site

Jobstown, NJ

March 2008

Sample Number:

Sampling Location: NJDEP

Vapor Intrussion

Screening Levels -

Indoor (Nonresid.)

ug/m3

_I_

310

9

43985

K&M Indoor 1

Crew Room

12/19/2007

43984

K&M Indoor 2

Crew Room

12/19/2007

43987

K&M Indoor 3

EMS Office

12/19/2007

43989

K&M Indoor 4

EMS Storage

12/19/2007

43991

K&M Indoor 5

EMS Bay (02)

12/19/2007

43992

K&M Indoor 6

FDBay

12/19/2007

43995

K&M

Ambient 1

12/19/2007

43996

K&M

Ambient 2

12/19/2007

ug/m3 denotes micrograms per cubic meter.

MRL denotes Method Reporting Limit

ND denotes tested but not detected.

O O

to o ©

Table 2 TO-15 Indoor Air Sampling Results in ppbv

Kaufman and Minteer Site Jobstown, NJ March 2008

Sample Number NJDEP 43985 43984 43987 43989 43991 43992 43995 43996 Sampling Location: Vapor Intrussion K&M Indoor 1 K&M Indoor 2 K&M Indoor 3 K&M Indoor 4 K&M Indoor 5 K&M Indoor 6 K&M K&M

Screening Levels - Crew Room Crew Room EMS Office EMS Storage EMS Bay (02) FDBay Ambient 1 Ambient 2 Indoor (Nonresid.) 12/19 /2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007

Parameter ppbv Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Vinyl Chloride 0̂ 5 ND 0.066 ND 0.060 ND 0.066 ND 0.060 ND 0:064 ND 0.052 ND 0.059 ND 0.048 1,1 -Dichloroethene 77 ND 0.043 . ND 0.039 ND 0.043 ND 0.039 ND 0.041 ND 0.033 ND 0.038 ND 0.031 Methylene Chloride 2 0.60 0.049 0.68 0.044 0.61 0.049 0.61 0.044 0.72 0.047 0.81 0.038 0.078 0.044 0.083 0.035 trans-1,2-Dichloroethene 26 ND 0.043 ND 0.039 ND 0.043 ND 0.039 ND 0.041 0.059 0.033 ND 0.038 ND 0.031 1,1 -Dichloroethane 180 ND 0.042 ND 0.038 ND 0.042 ND 0.038 ND 0.040 . ND 0.033 ND 0.038 ND 0.030 Methyl tert-Butyl Ether ' 1 13. 0.047 1.2 0.042 0.97 0.047 3.6 0.042 33 0.045 9 0.037 ND 0.042 ND 0.034 eis-I,2-Dichloroethene 13 ND 0.043 ND 0.039 ND 0.043 0.088 0.039 0.11 0.041 0.82 0.033 ND 0.038 ND 0.031 1,2-Dichloroethane 0.5 ND 0.042 ND 0.038 : ND 0.042 ND 0.038 ND 0.040 ND 0.033 ND 0.038 ND 0.030 1,1,1 -Trichloroethane 260 ND 0.031 ND 0.028 ND 0.031 ND 0.028 ND 0.030 0.044 0.024 ND 0.028 ND 0.023 Benzene 0.5 0.71 0.053 0.72 0.048 0.64 0.053 1.3 0.048 1J 0.051 2.3 0.041 0.22 0.048 0.25 0.039 Trichloroethene 0.5 0.14 0.031 0.14 0.028 6.13 0.031 0.20 O.028 0.23 0.030 1.1 0.025 ND 0.028 ND 0.023 Toluene 1900 3.1 0.045 3.3 0.041 2.4 0.045 8.9 0.041 8.6 0.043 . 37 0.18 0.43 0.040 0.43 0.033 Tetrachldroethene 0.5 0.30 .0.025 0.31 0.023 0.30 0.025 0.49 0.023 0.65 0.024 1.4 0.019 0.034 0.022 0.034 0.018 Chlorobenzene 16 ND 0.037 . ND 0.033 ND 0.037 ND 0.033 ND 0.035 ND 0.029 ND 0.033 ND 0.027 Ethylbenzene 340 0.30 0.039 0.32 0.035 0.24 0.039 0.83 0.035 0.79 0.038 2.7 0.030 0.055 0.035 0.05? 0.028 m&p-Xylene '35 1.3 0.078 1.4 0.070 1.1 0.078 4.0 0.070 3.8 0.075 14 0.061 0.18 0.070 0.20 0.057 o-Xylene 35 0.45 0.039 0.49 0.035 0.37 0.039 1.3 0.035 1.3 0.038 4.6 0.030 0.059 0.035 0.066 0.028

ppbv dentes parts per billion volhile. MRL denotes Method Reporting Limit ND - Analyzed but not detected.

Table 3

TO-15 Sub-Slab Soil Gas Sampling Results in ug/m3


Jobstown, NJ

March 2008

Sample Number

Sampling Location: NJDEP

Vapor Intrussion

43983

K&M Sub floor 1

43986

K&M Sub floor 2

43988

K&M Port 1

43990

K&M Port 2

43993

K&M Port 3

43994

K&M Port 4

43982

K&M

Sampling Date: Screening Levels -

Soil Gas(Nonresid.

Crew

12/19

Room

/2007

EMS Office

12/19/2007

EMS Storage

12/19/2007

EMS Bay (02)

12/19/2007

FD Bay

12/19/2007

Rec. Dept.

12/19/2007

Trip Blank

12/19/2007 Parameter ug/m3 Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Vinyl Chloride 19 ND 0.15 ND 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10

15000 ND 0.15 ND 0.16 ND 0.15 ND 21 ND 140 120 59 ND 0.10 Methylene Chloride 430 1.5 0.15 .1.3 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10 trans-1,2-Dichloroethene 5100 ND 0.15 ND 0.16 " ND 0.15 ND 21 610 140 1300 59 ND 0.10 1,1 -Dichforoethane 36000 ND . 0.15 ND 0.16 ND v 0.15 ND 21 430 140 520 59 ND 0.10 Methyl tert-Butyl Ether 180 4.7 0.15 8.2 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10 cis-1,2-Dichloroethene 2600 ND 0.15 ND 0.16 ND 0.15 ND 21 4100 140 18000 59 ND 0.10 1,2-Dichloroethane 20 ND 0.15 ND 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10 1,1,1 -Trich loroethane 72000 ND 0.15 ND. 0.16 ND 0.15 36 21 1000 140 3100 59 ND 0.10 Benzene 26 1.6 0.15 2.7 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10 Trichloroethene 27 1.7 0.15 1.9 0.16 ND 0.15 310 21 8800 140 . 56000 59 ND 0.10 Toluene 360000 13 0.15 21 0.16 1.1 0.15 ND 21 ND 140 ND 59 ND 0.10 Tetrachloroethene 36 12 0.15 15 0.16 43 0.15 18000 21 110000 140 6100 59 ND 0.10 Chlorobenzene 3600 ND 0.15 ND 0.16 ND 0.15 ND 21 ND 140 ND 59 ND 0.10 Ethylbenzene 74000 1.4 0.15 2,0 0.16 0.16 0.15 ND 21 ND 140 ND 59 ND 0.10 m&p-Xylene 7700 6.1 031 6.9 0.31 0.80 0.30 ND 41 ND 280 ND 120 ND 0.20 o-Xylene 7700 2.0 0.15 2.1 0.16 ND 0.15 ND 21 ND . 140 ND 59 ND 0.10

ug/m3 denotes micrograms per cubic meter.


ND - Analyzed but not detected.

table 4 TO-15 Sub-Slab Soil Gas Sampling Results in ppbv


Jobstown, NJ

March 2008

Sample Number: NJDEP 43983 43986 43988 43990 43993 43994 43982 Sampling Location:' Vapor Intrussion K&M Sub floor 1 K&M Sub floor 2 K&M Pott 1 K&M Port 2 K&M Port 3 K&M Port 4 K&M

Screening Levels - . Crew Room EMS Office EMS J torage EMS Bay (02) FDBay Rec. Dept. Trip Blank Sampling Date: Soil Gas(Nonresid. 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 12/19/2007 Parameter ppbv Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Result MRL Vinyl Chloride 19 ND 0.060 ND 0.061 ND 0.058 ND 8.1 ND 54 ND 23 ND 0.039 1,1-Dichloroethene 3900 ND 0.039 ND 0.040 ND 0.037 ND 5.2 ND 35 30 15 ND. 0.025 Methylene Chloride 120 0.42 0:044 0.38 0.045 ND 0.043 ND 6.0 ND 40 ND 17 ND 0.029 lrans-1,2-Dichloroethene 1300 ND 0.039 ND 0.040 ND 0.037 ND 5.2 150 35 340 15 ND 0.025 1,1-Dichloroethane' 8800 ND 0.038 ND 0.039 ND v. 0.037 ND 5.1 . 110 34 130 15 ND 0.025 Methyl tert-Butyl Ether 50 1.3 0.043 2.3 0.044 ND 0.041 ND 5.7 ND 38 ND 16 ND 0.028 cis-1,2-Dichloroethene . 640 ND 0.039 ND 0.040 ND 0.037 ND 5.2 1000 35 4600 15 ND 0.025 1,2-Dichloroethane 5 ND 0.038 ND 0.039 ND 0.037 ND 5.1 ND 34 ND 15 ND 0.025 1,1,1 -Trichloroethane 13000 ND 0.028 ND 0.029 ND 0.027 6.6 3.8 190 25 570 11 ND 0.018 Benzene 8 0.50 0.048 0.86 0M9 ND 0.046 ND 6.5 ND 43 ND 18 ND 0.031 Trichloroethene 5 0.32 0.029 0.35 0.029 ND 0.028 58 3.8 1600 26 10000 11 ND 0.019 Toluene 95000 3.5 0.041 5.6 0.042 0.28 0.039 ND 5.5 ND . 37 ND 16 ND 0.027 Tetrachloroethene 5 1.7 0.023 2.1 0.023 63 0.022 2700 3.0 17000 20 900 8.7 ND 0.015 Chlorobenzene 780 ND 0.033 . ND 0.034 ND 0.032 ND 4.5 ND 30 ND 13 ND 0.022 Ethylbenzene 17000 0.31 0.035 0.45 0.036 0.036 0.034 ND 4.8 ND 32 ND 14 ND 0.023 m&p-Xylene 1800 1.4 0.071 1.6 0.072 0.18 0.068 ND . 9.5 ND 64 ND 27 ND 0.046 o-Xylene 1800 0.47 0.035 0.49 0.036 ND 0.034 ND 4.8 ND 32 ND 14 ND 0.023

ppbv denotes parts per billion volitile


ND - Analyzed but not detected.

KMI2.9009

Figures

J — : — : 1 1 1 |

' ' 1 1 1

EMS STORAGE

• p o r t l

EMS BAY

Port 2 •

—I U_ Ul or

CM O

1 1

4 1

FIRE DEPARTMENT

BAY

• Port 3

RECREATION DEPARTMENT

BAY

• Port 4

EMS OFFICE

Sub Floor 2

• 1

CREW L ROOM

r SUb

Floor 1 J

WC

MC

r

i U

TIL

ITY

RA

MP

EMS BAY

Port 2 •

—I U_ Ul or

CM O

1 1

4 1

FIRE DEPARTMENT

BAY

• Port 3

RECREATION DEPARTMENT

BAY

• Port 4

20 Feet (Approximate)

U.S. EPA ENVIRONMENTAL RESPONSE TEAM RESPONSE ENGINEERING AND ANALYTICAL CONTRACT

EP-C-04-032 WA# 0-056

FIGURE SAMPLE LOCATIONS

KAUFFMAN & MINTEER SITE JOBSTOWN, NJ

DECEMBER 2007

KMI2.9011

Appendix A

KMI2.9013

Lockheed Martin Technology Services Environmental Services REAC 2890 Woodbridge Avenue Building 209 Annex Edison, NJ 08837-3679 Telephone 732-321-4200 Facsimile 732-494-4021 LOCKHEED MA R T I N

DATE:

TO:

FROM:

SUBJECT:

February 8, 2008

R. Singhvi, EPA/ERT Analytical Work Assignment Manager

V. Kansal, REAC Analytical Section Leader ( U ^ > ^

DOCUMENT TRANSMITTAL UNDER wfc>RK ASSIGNMENT # 0-056

Attached please find the following document prepared under this work assignment:

Kauffman and Minteer Site - Analytical Report

G. Prince Work Assignment Manager (w/o attachment) P. Solinski Air Response Group Leader (w/o attachment) C. Gussman Task Leader (w/o attachment) J. Soroka Data Validation and Report Writing Group Leader (w/o attachment) Central File WA # 0-056 (w/attachment)

KMI2.9014

ANALYTICAL REPORT

Prepared by LOCKHEED MARTIN, Inc.

Kauffman and Minteer Site Jobstown, NJ

February 2008

EPA Work Assignment No. 0-056 LOCKHEED MARTIN Work Order EAC0056

EPA Contract No. EP-C-04-032

Submitted to G. Prince EPA-ERT

Analysis by: Columbia

Prepared by: Y.Mehra

DTMiller | Date Program Manager

Reviewed by: J. Soroka

0056-DAR-020808

KMI2.9015

Table of Contents

Topic

Introduction Case Narrative Summary of Abbreviations

Section I

Results of the Analysis for VOC (ppbv) in Air Table I . la Results of the Analysis for VOC fag/m3) in Air Table 1.1 b

Section II

Results of the LCS Analysis for VOC in Air Table 2.1 Results of the Duplicate Analysis for VOC in Air Table 2.2

Section III

Correspondence Chains of Custody

Appendices

Appendix A Data for VOC in Air T02S

The appendix will be furnished on request.

0056-DAR-020808

KMI2.9016

Introduction

REAC personnel, in response to WA 0-056, provided analytical support for environmental samples collected from the Kauffman and Minteer Site, located in Jobstown, NJ as described in the following table. The support also included QA/QC, data review and preparation of an analytical report containing a summary of the analytical and the QAJQC results.

coc# Number of

Sample

Sampling Date

Date Received

Matrix Analysis/ Method

Laboratory Data Package

EAC00056-12/|l9/07-0001 4 12/19/07 12/22/07 Air VOC/ Columbia T028 EAC00O56-12/19/07-O0O2 4 TO-15 Analytical

EAC00056-12/19/07-0003 1 Services'

2 Soil Gas EAC00056-12/19/07-0004 4

Columbia Analytical Services is NELAC certified for VOC TO-15 analysis;

Case Narrative

The laboratory reported the data to two significant figures and the data was also validated to two significant figures. Any other representation of the data is the responsibility of the user. Values less than the reporting limits have not bjeen reported. At the request of the WAM, results for 17 compounds (14 chlorinated and three aromatic compounds) were reported and validated.

VOC in Air Package T 028

The data package was examined and found to be acceptable.

0056-DAR-020808 01

KMI2.9017

Summary of Abbreviations

BFB C CLP COC cone cont CRDL CRQL D Dioxin DFTPP EMPC GC/MS IS LCS LCSD MDA MS (BS) MSD (BSD) MW NA NAD NC NR NS %D %REC SOP ppbv ppm pptv PQL QA/QC QL REAC RL RPD RSD SIM Sur TIC TCLP VOC *

Bromofluorobenzene Centigrade Contract Laboratory Program Chain of Custody concentration continued Contract Required Detection Limit Contract Required Quantitation Limit (Surrogate Table) value is from a diluted sample and was not calculated Polychlorinated dibenzo-p-dioxins (PCDD) and Polychlorinated dibenzofurans (PCDF) Decafluorotriphenylphosphine Estimated maximum possible concentration Gas Chromatography/Mass Spectrometry Internal Standard Laboratory Control Sample Laboratory Control Sample Duplicate Minimum Detectable Activity Matrix Spike (Blank Spike) Matrix Spike Duplicate (Blank Spike Duplicate) Molecular Weight Not Applicable or Not Available Normalized Absolute Difference Not Calculated Not Requested/Not Reported Not Spiked Percent Difference Percent Recovery / Standard Operating Procedure parts per billion by volume parts per million parts per trillion by volume Practical Quantitation Limit Quality Assurance/Quality Control Quantitation Limit Response Engineering and Analytical Contract Reporting Limit Relative Percent Difference Relative Standard Deviation '* ' Selected Ion Monitoring Surrogate Tentatively Identified Compound Toxicity Characteristic Caching Procedure Volatile Organic Compound Value exceeds the acceptable QC limits.

m

ng

J J+ J-

cubic meter microgram nanogram

g uL Pg

gram. microliter picogram

kg kilogram mg milligram pCi picocurie

L liter mL milliliter s sigma

Data Validation Flags .

Value is estimated jR Value is estimated high (metals only) U Value is estimated low (metals only) UJ

Value is unusable Notdetected Not detected and RL is estimated

Rev. 01/10/08

0056-DAR-020808 02

KMI2.9018

Method TO-15

Sample No. Location Sublocation

AnaMe

Table 1.1a Results of the Analysis for VOC (ppbv) h Air WA * 0-056 Kauffman S Minteer Site

1/3/2008 Method Blank

43982 Field/Trip Blank

43984 K and M Building

Indoor 2 - Crew Room


Ambient 1

Page 1 oi2


Ambient 2

Vinyl Chloride 1,1-Oichloroelhene (1,1-OCE)

. Oichloromelhane (Methylene Chloride) trans-1,2-OkMoroethene 1.1-Oichloroethana (1;1-0CA) Mathyl lert-Butyl Ether ds-1.2-Oiehkxoethene 1.2- Oichioroe(hane | 1.1.1-Tncnloroethane (TCA) Benzene TricMoroethene (TCE) Toluene Tetrachloroalhene (PCE) Chlorobenzena Ethylbenzene m.p-Xylenes o-Xylene

Result RL Result RL _Epbv ppbv DObv ppp»

0 0.039 U 0.039 U 0.025 U 0.025 u 0.029 u 0.029 u 0.025 u 0.025 u 0.025 u 0.025 u 0.028 u 0.028 u 0.025 u 0.025 u 0.025 u 0.025 u 0.018 u 0.018 u 0.031 u 0.031 u 0.019 u 0.019 u 0.027 u 0.027 u 0.015 u 0.015 u 0.022 u 0.022

u O.023 u 0.023 u 0.046 u 0.046 u 0.023 u 0.023

Result ppbv

RL ppbv

Result RL

U 0.060 U 0.059 U 0.039 U 0.038

0.68 0.044 0.078 0.044 U 0.039 U 0.038 U 0.038 U 0.038

1.2 0.042 U 0.042 U 0.039 U 0.038 U 0.038 U 0.038 U 0.028 U 0.028

0.72 0.046 022 0.048 0.14 0.028 U 0.028

3.3 0.041 0.43 0.040 0.31 0.023 0.034 0.022

U 0.033 U 0.033 0.32 0.035 0.055 0.035 1.4 0070 0.18 0.070

0.49 0.035 0.059 0.035

Result RL PPbv oobv

U U

0.083 U 0 U U U U

0.25 U

0.43 0.034

U 0.058 0.20

0.066

0.048 0.031 0.035 0.031 0.030 0.034 0.031 0.030 0.023 0.039 0.023 0.033 0.018 0.027 0.028 0.057 0.028

Method TO-15


AnaMe

Table 1.1 a (cant) Results of the Analysis for VOC (ppbv) In Air WA # 0456/Kauffman & Minteer Site



Result RL ppbv ppbv


Indoor 3 - EMS Office

Result RL

43983 43989 4399, K ^ M Building KandM Building K and M Building

Indoor 4-EMS Storage Indoor 5 - EMS Bay (02) Sub Floor 1 - Crew Room

Result RL PPbv ppbv ppbv ppbv

U 0.066 U 0.060 U 0.043 U 0.039

0.61 0.049 0.61 0.044 U 0.043 U 0.039 U 0.042 U 0.038

0.97 0.047 3.6 0.042 U O.043 0.088 0.039 U 0.042 U 0.038 U 0.031 u 0.028

0.64 0.053 1.3 0.048 0.13 0.031 0.20 0.028 2.4 0.045 8.9 0.041

0.30 0.025 0.49 0.023 U 0.037 .0 0.033

0.24 0.039 0.83 0.035 1.1 0.078 4.0 0.070

0.37 0.039 1.3 0.035

Result RL

Vinyl Chloride | g 0 066 1,1-Olchloroethene (1,1-OCE) U 0.043 Oichloromethane (Methylene Chloride) 0.60 o'o49 trans-1,2-Olchloroethene I (j 0 043 1.1-Oichloroethane (1,1-OCA) U 0.042 Methyl tert-Butyl Ether 1.2 0.047 ds-1 ,2-Dichloroetnene U 0043 1.2-Olchloroethane U 0042* l.l.l-TnehtoroeinanerrCA) U 0.031 Benzene 0.71 0.053 Trichloroethene (TCE) 014 0031 toluene 0.045 Tetraohloroethene (PCE) 0.30 0.025 Chlorobenzene u 0037 Ethylbenzene 0.30 0.039 m,p-Xylene» ) 3 0.078 c-Xylene 0.45 0.039

oebv

U

PPbv

0.064

ppbv

U

ppbv

0.060 U 0.041 U 0.039

0.72 0.047 0.42 0.044 U 0.041 U 0.039 U 0.040 u 0.038

3.3 0.045 ' 1.3 0.043 0.11 0.041 * U 0.039

U 0.040 U 0.038 U 0.030 U 0.028

1.3 0.051 0 5 0 0.048 0.23 0.030 . 0.32 0.029 8.6 0.043 3.S 0.041

0.65 0.024 1.7 0.023 U 0.035 U 0.033

0.79 0.038 0.31 0.035 3.8 0.075 1.4 0.071 1.3 0.038 0.47 0.035

0056-DAR-020808 03

KMI2.9019

Method TO-15

Sample No, Location Sublocation

Table 1.1a (cent) Result* of the Analysis for VOC (ppbv) in Air WA * O056 Kauffman & Minteer Site

43986 K a n d M Building

Sub Floor2-EMS Office

Result RL

43992 K and M Buiiding Indoor 6- FD Bay

Pag*2of2

Vinyl Chloride 1.1-Oichloroethene (1,1-OCE) Oichloromethane (Methylene Chloride) lrans-1,2-Oichloroe(hene 1.1- Oichloroelhane (1.1-OCA) Methyl tert-Butyl Efher ois-1,2-Oichloroethene 1.2- Oichloroethane 1,1,1-Trichloroe<hane (TCA) Benzene Trichloroethene (TCE) Toluene Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m.p-XvtenM o-Xylene

u 0.061 U 0.052 u 0.040 U 0.033

0.38 0.045 0.81 0.038 0 0.040 0.059 0.033 U 0.039 U 0.033

2.3 0.044 9.0 0.037 U 0.040 0.82 0.033 U 0.039 U 0.033 u O.029 0.044 0.024

0.88 0.049 2.3 0.041 0.35 0.029 1.1 0.025

5.6 0.042 37 018 2.1 0.023 1.4 0.019

U 0.034 U 0.029 0.45 0.036 2.7 0.030

1.6 0.072 14 0.061 0.49 0.036 4.6 0.030

Method TO-15


Table 1.1 a (cont) Results of the Analysis for VOC (ppbv) in Air WA # 0056 Kauffman & Minteer Site


Result RL

43988 KandM Building

Port 1 - EMS Storage

43990 K a n d M Building

Port 2 - EMS Bay (02)

43993 K a n d M Building Port3-FOBay


Port 4 - Roc Oopt Bay

Vinyl Chloride 1,1-Oichloroelhene (1,1-OCE) Oichloromethane (Methylene Chloride) trans-1,2-Oichlaroelhene 1.1-Oichloroethane (1,1-OCA) Methyl tert-Butyl Ether ds-1,2-Olehtoroetfiene 1.2-Ofchloroethane 1.1,1-Trichkxoethane (TCA) Benzene Trichloroethene (TCE) Toluene Tetrachloroethene (PCE) Chlorobenzene Elhybenzene m.pJCytenss o-Xylene

U

U U U U U U U U U U U U

U 0.039 U 0.025

0.029 U 0.025 U 0.025

0.028 0.025 0.025 0.018 0.031 0.019 0.027 0.01S 0.022 0.023 0.046 0.023

u 0.058 U 8.1 u 0.037 U 5.2 u 0.043 U 6 0 u 0.037 U 5.2 u 0.037 U £ 1 u 0.041 . U 6.7 u 0.037 U 5.2 u 0.037 U 5.1 u 0.027 6.6 3.8 u 0.046 U as u 0.028 58 3.8

28 0.039 U 5.5 8.3 0.022 2700 3.0 U 0.032 U 4.5

U 54

0.036 0.034 0.18 0.068 U 0.034

U 4.8 U 9.5 U 4.8

u 35

u 40 150 35 110 34

U 38 1000 35

U 34 190 25

U 43 1600 26

U 37 17000 20

U 30 U 32 U 64 U 32

U 23 30 15 U 17

. 340 15 • 130 15 - 0 16 4600 15 0 IS

S70 11 U 18

10000 11 U 16

900 17 U 13 U 14 U 27 U 14

0056-DAR-020808 0 4

KMI2.9020

Method TO-15


Table 1.1b Results of the Analysis for VOC (ug/m *) in Air WA * 0-056 Kauffman & Minteer Site


Result RL

43982 Field/Trip Blank


Indoor 2-Crew Room


Ambient 1

Result RL j


Ambient 2

Result RL

Vinyl Chloride 1.1-OlchlorOethene (1,1-OCE) Oichloromethane (Methylene Chloride) trans-1,2-Dichloroethene | 1.1-Oichforoethane (1.1-OCA) Methyl tert-Butyl Ether ets-1,2-Oichloroethene 1 ̂ -Dichloroethane 1.1.1-Trichloraethane (TCA) Benzene Trichloroethene (TCE) Toluene Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m,p-Xylenes o-Xylene

U U U U U U

. U U U U U U U U U U U

0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.20 0.10

u u u u u u u u u u u u u u u u u

0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.10 0.20 0.10

u u

2.4 u u

4.4 u u u

2.3 0.78

12 Z1

U 1.4 6.2 2.1

0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.31 0.15

u 0.15 u 0.15

0.27 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15

0.72 0.15 U 0.15

1.6 0.15 0.23 0.15

U 0.15 0.24 0.15 0.79 0.30 0.28 0.15

U 0.12 U 0.12

029 0.12 U 0.12 U 0.12 U 0.12 U 0.12 U 0.12 U 0:12

0.79 0.12 U 0.12

1.6 0.12 0.23 0.12

U 0.12 0.25 0.12 0.85 0.25 0.29 0.12

Method TO-15


Table 1.1b (cont) Result of the Analysis for VOC (ug/m ^ in Air WA # 0056 Kauffman & Minteer Site



Result RL „ 3 I u . l L - >


Indoor 3-EMS Office

Result RL


Indoor 4 - EMS Storage

Result RL

Vinyl Chloride 1,1-Olchloroethene (1,1-OCE) Oichloromethane (Methylene Chloride) trans-1.2-OfcMoreethene 1,1-Oichloroethane (1,1-OCA) Methyl tert-Butyl Ether

. els-1^-Oichloroethene l^-Ofchloroettjane 1.1,1-Trichloroethane (TCA) Benzene Trichloroethene (TCE) Toluene Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m,p-Xylenes b-Xylerie

43991 43983 KandM Building K and M Building

Indoor 5 - EMS Bay (02) Sub Floor 1 - Crew Room

Result RL

U U

2.1 U U

4.4 U U U

2.3 0.73

12 2.0

U 1.3 5.9 2.0

0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 034 0.17

U U

2.1 U U

3.5 U U U

2.0 0.71 9.2 2.0 U

1.1 4.7 1.6

0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.34 0.17

0056-DAR-020808

u 0.15 U u 0.15 U

2.1 0.15 2JS U 0.15 U U 0.15 U

13 0.15 12 0.35 0.15 0.42

U 0.15 U U 0.15 (J

4.2 0.15 4.2 1.1 0.15 1.3 33 0.15 32

3.3 0.15 4.4 U 0.15 U

3.6 0.15 3.4 17 0.31 17

5.8 0.15 5.6

0.18 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.33 0.16

• U - U

1.5 u u

4.7 U U U

1.6 1.7 13 12 U

1.4 6.1 2.0

0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.15 0.31 0.15

05

KMI2.902I

Table 1.1b (conO Result of the Analysis for VOC (ug/m in Air WA * 0-058 Kauffman 4 Minteer Site

Method TO-15

Sample No. 43986 43992 Location K and. M Building K and M Building Sublocation Sub Floor 2 - EMS Office Indoor 6- FD Bay

Result RL Result RL AnaMe uaAn' uoAn' UflAn* U0/m

Vinyl Chloride U 0.16 U 0.13 1.1-Oichloreelhene (1,1-OCE) U 0.16 U 0.13 Oichloromethane (Methylene Chloride) 1.3 0.16 2.8 0.13 tran»-1,2-Dichloroethene U 0.16- 0.23 0.13 1,1-Oichloroethane (1.1-OCA) U 0.16 U 0.13 Methyl tert-Butyl Ether 8.2 0.16 32 0.13 cis-1,2-Oichloroethene U 0.18 3.3 0.13 1.2-Olchloroethane U 0.16 U 0.13 1,1.1-Trlchloroethane (TCA) U 0.16 0.24 0.13 Benzene 2.7 0.16 7.3 0.13 Trichloroethene (TCE) 1.9 0.16 6.0 0.13 Toluene 21 0.18 ' 140 0.86 Tetrachloroethene (PCE) 15 0.16 9.3 0.13 Chlorobenzene U 0.16 U 0.13 Ethylbenzene 2.0 0.16 12 0.13 m,p-Xylenes • 6.9 0.31 61 0.26 o-Xylene 2.1 0.16 20 0.13

Method TO-15

Table 1.1 b (cent) Result of the Analysis for VOC (ug/m *) In Air WA # 0-056 Kauffman & Minteer Site


Anarvte


Result RL ug/m' uoVm1


Port 1 - EMS Storage

Result RL ua/m' unrni'


Port2-EMS Bay(02)

Result RL uoAn' uaAn'

43993 K and M Building Port 3 - FD Bay

Result RL HO*"3 ua/m'


Port 4 - Rec Dept Bay

Result RL uaAn' uaAn'

Vinyl Chloride 1 ,!-Dlehloroethene(1,1-DCE) Oichloromethane (Methylene Chloride) trans-1,2-Olehloroethene 1,1-Oichloroethane (1,1-OCA) Methyl. tert-Butyl Ether ds-1,2-Oichloroethene 1 ̂ -Dichloroethane 1,1,1-Trichloroefhane (TCA) Benzene' Trichloroethene (TCE) Toluene Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene ' mp-Xylenee o-Xylene

U U U U U U U

U U U U U U

0.10 0.10 0.10 0.10 0.10 0.10 0.10

U 0.10 U 0.10 U 0.10 U 0.10

0.10 0.10 0.10 0.10 0.20 0.10

U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15 U 0.15

i.1 0.15 43 0.15 U 0.15

0.16 0.15 0.80 0.30

U 0.15

U 21 U 21 U U U U U U

36 U

310 U

16000 u u u u

21 21 21 21 21 21 21 21 21 21 21 21 21 41 21

U U U 140

610 140

140 140

430 U

4100 U

1000 U

8600 U

110O00 U U . U U

140 140 140 140 140 140 140 140 140 140 140 280 140

U 59 ' 120 59 * U 59

1300 59 520 59

U 59 18000 59

U 59 3100 59

U 59 56000 59

U 59 6100 59

U 59 U 59 U 120 U 59

0056-DAR-020808 06

Table 2.1 Results of the LCS Analysis for VOC in Air WA # 0-056 Kauffman & Minteer Site

Sample No: LCS 0//03/08

Analyte

LCS Spike

Added LCS

Result LCS % Recovery

Vinyl Chloride 1,1-DicHloroethene (1,1-DCE) Dichloromethane (Methylene Chloride) trans-1,2-Dichloroethene 1.1- Dichloroethane (1,1-DCA) Methyl tert-Butyl Ether cis-1,2-Dichloroethene 1.2- Dichlproethane 1,1,1 -Trichloroethane (TCA) Benzene| Trichloroethene (TCE) Toluene I Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m.p-Xylenes o-Xylene

QC Limits % Recovery

24.8 21.1 85 27.8 24.2 87 27.8 22.0 79 26.5 23.5 89 26.8 21.9 82 26.8 27.4 102 27.0 23.7 88 26.3 24.4 93 26.8 24.5 91 27.0 22.8 64 27.3 24.2 89 26.5 25.5 96 26.0 25.8 99 26.5 25.5 96 26.3 25.9 98 62.5 63.8 102 29.8 29.1 98

Sample No. LCS 01/07/08

Analyte

LCS Spike

Added "3

LCS Result

"9 ,.. LCS

% Recovery

Vinyl Chloride 1.1- Dichloroethene (1,1-DCE). Dichlorometriane (Methylene Chloride) trans-1,2-Dichloroethene 1,1 -Dichloroethane (1,1 -DCA) Methyl tert-Butyl Ether cis-1,2-Dichloroethene 1.2- Dlchloroethane 1,1,1-Trichloroethane (TCA) Benzene | Trichloroethene (TCE) Toluene I Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m.p-Xyienes o-Xylene

0056-DAR-020808

24.8 27.8 27.8 26.5 26.8 26.6 27.0 26.3 26.8 27.0 27.3 26.5 26.0 26.5 26.3 62.5 29.8

20.4 22.4 20.4 22.0 20.9 21.8 22.5 22.8 22.7 22.2 24.1 24.8 24.9 25.2 25.4 62.7 28.7

82 81 73 83 78 81 83 87 85 82 88 94 95 95 97 100 96

07

6M27 77- 116 71- 113 74-118 74-118 72- 119 74-117 72- 117 78- 114 73- 111 80-116 76- 116 77- 118 78- 117 79- 116 80- 117 80-116

QC Limits % Recovery

61-127 77-116 71- 113 74-118 74-118 72- 119 74-117 72- H7 78-114 73- 111 80-116 76- 116 77- 118 78- 117 79- 116 80- 117 80-116

Lockheed Martin Technology Services Environmental Services R£AC 2890 Woodbridge Avenue Building 209 Annex Edison, NJ 08837-3679 Telephone 732 32M200 Facsimile 732-494-4021

Columbia Analytical Services 2665 Park Center Dr. STE A Simi Valley, CA 93065

*• O C K M E E D

Attn: Kate Aguilera January 2,2008

S S ^ & S , ' ™ ^ < * * * ™ - P r oJeC 0 * * . p f e a s e a o ^ e

Analysis/Method

VOA/TO-15 SIM(0.070 ppbv) See attached compound list

Data packaoe: Package with niskette Delrvemhto

samples. n» iompfete d a t e m V s T S d i ^ l t a S ? £ , ^ S ^ ' " ' " • V alter receipt J &|

Sincerely. / /

/inodKansal Analytical Section Leader Lockheed Martin / REAC Project

vTCIm Attachments

cc R. Singhvi G. Prince 0056\non\mem\0801\sub\0056Con

V. Kansal Subcontracting File J. Soroka

J. Tapkas C. Gussman P. Solinski

•

0056-DAR-020808 09

o o cn o> i

O >

<S M O CO o CO

Page 1 od

CHAIN OF CUSTODY RECORD

SltettEACOOOM Contact Name: John Johnson Contact Phono: 732-321-4248

No: EAC00056-12/19/07-0001

Lab: Columbia Analytical Services

NJ

O NJ

Special Instructions: Vdc'a bvTn I K T « ~ . Z •

Items/Reason

•<\ f t K

Relinquished by Date

"Id Receh/edby'

SAMPLES TRANSFERRED FROM

CHATN~6F"C1J8TODY #

Date Time Items/Reason Relinquished By Date B Received by Date Time

1

•

o o a? —ai i o >

<S NJ O CD o oo

CO

1 Of 1

Lab* Sample

43983

43986

43992

Location

KandM" Building KandM Building

K and wT Building

CHAIN OF CUSTODY RECORD Sit8#:EACO0Q5e

Contact Name: John Johnson Contact Phone: 732-321-4248

Sub Location

No: EAC00056-12/19/07-0003

Lab: Columbia Analytical Service,

Sub FlwM-Ciew" Room

Sub Floor 2 - EMS Office

Indoor 6-FD Bay -

Analyse

VOC's-TOIS SIM

VOC's-T015~ SIM

VOC8-T015 SIM

Matrix Collecte Id

Soil Gas Soli Gas

Air

12/19/200 7

Container

Summa Canister

12/19/200 7

12/19/200 7

Sample Time

Summa Canister Summa Canister

10:18

ibTlY"

10:37

Pumpf

AC01502

AC01127

OrtflcalD

FC00550"

AC00540

FC00291

rc66o3T

Special Inatructlons' VOC's bv Tn 1 - ~ ' —>

Start Pretsu

re

-30

-30

-29.5

Stop Pressu

re

-6.5

-6.5

"-'£5

Volum

4.8

~4~7

Vol Unite

5.3

t. .-j!g^s/?W8'orr"" Rellnqulsjiqrj by Date ...-^gggy^by l Date J E T


CHAIN "OF CUSTODY*

"ate | Time Hems/Reason Relinquished By Date Received by Date Time

Appendix B

KMI2.9027

APPENDIX B Sampling Work Sheets/Chain of Custody Record

Kauffinan and Minteer Site Jobstown, NJ March 2008

0056-DTR-03I408 5

of 1


Slte#:EAC00056 Contact Name: John Johnson Contact Phone: 732-321-4248

No: EAC00056-12/19/07-0001


e t h y l e n e , m*>xy1ene. o-xylene. i « 3 « « ^ ^ • * « . tetrachloroethene, SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #


S!te#;EAC00056 Contact Name: John Johnson Contact Phone: 732-321-4248

No: EAC00056-12/19/07-0003


ethylbenzene. m ^ e n e , o-xylene, methylene c h . S K « K b ~ - « « * ^

Items/Reason i h

Relinquished by


CHAIN OF CUSTODY*

Date Received by Date Time Items/Reason Relinquished By Date Received by Date Time

KMI2.9030

Site: K & M

Sampler Solinski

EPA/Environmental Response Team Response Engineering Analytical Contract

SUMMA® Sampling Work Sheet

Lockheed Martin Corp., Edison, NJ EPA Contract No. EP-C-04-032

Page __v o f

R«powEroin««ci^c^AroMt^Cc<i r ror t i

WA#: EAC000S6

EPA/ERT WAM: Prince

Date: 12/18/2007

Sample #

Location

Unit#

Summa #

Orifice*

Picture*

Analysis/Method

Total Time

% Initial Pressure

REAC Task Leaden Gussman

43983 43984 43985

Q(1*ciuj /term.

I

• 43986

^ - C ^ / < -2.-7

43987

tcr?fC=,

F < ^ c o S " 7 2 _

-5o ' JO - T O

Post Pressure •"5 . £7-3

(Stan Flow Rate (Start) - 3LS

Sample Volume f/.1 W. 3

MET Station on Site?: I Y / N Atmospheric Pressure (Local): Ambient Sampling Temperature:

KMI2.9031




Page ' 3 of 3

Hwponn Engirwwtno and AnoyHcol Contract

Site: K & M WA#: EAC00056

Sampler Soltnski EPA/ERT WAM: Prince

Date: 12/18/2007 REAC Task Leaden Gussman

Sample *

Location

43993 43995 L/»Wt PaC^fr T~tZ7^\ f**Tlf W-t+\

43996 • 43982

Unit*

Summa*

Orifice* p c - o o ^ C S ^ o o 5 Y 3 fF^go^otf

Picture* 1

Analysis/Method

Date/Time (Start)

Date/Time (Stop)

Total Time

Initial Pressure -so

Post Pressure

Flow Rate (Start)

V - 3o

Sample Volume

MET Station on Site?: Y / N 1 v- lj Atmospheric Pressure (local): Ambient Sampling Temperature?

KMI2.9032

Site: K & M




Page ^-of 3

(mponm EnefciMrina and AnoMcd Contract

, WA*:_EAC00056

P a g e ^ ^


S!teftEAC00058 Contact Name: John Johnson Contact Phone: 732-321-4248

No: EAC00056-12/19/07-0004


Items/Reason Relinquished by


CHAIN OF CUSTODY*

Date Received by Date Items/Reason

of 1


Site ft EAC00056 Contact Name: John Johnson Contact Phone: 732-321-4248

No: EAC000S6-12/19/07-0002


o o

83 I o > 6 ho o CO o CO

# e l o f l

CHAIN OF CUSTODY RECORD SIte#:EAC0005e


r No: EAG00056-12/19/or-0004

Lab: Columbia Analytical Servfces

Special Instructions' VOC'a bvTO us

Items/Reason JTHSSE^SS^y-

I


CHAIN OF CUSTODY #

Date Time Items/Reason Relinquished By Date Received by Date Time o

o o

o

o 00 O CD

CHAIN OF CUSTOuC RECORD Slte#; EAC00056


No: EAC00056-12/1o/07-0002 | N vc

Lab: Columbia Analytical Services S •o

Sample

43985

"43987"

43989

43991

Location

KandM Building

K and M :

Building

KandM Building KanofM Building

Sub Location


Indoor 3 - EMS Office

Indoor 4 - EMS Storage

Indoor 5 - EMS Bay (02)

Analyses

V0CS-T015 SIM

V0CB-T015 SIM

V0CS-T015 SIM

VOC8-T015 SIM

Matrix

Air

Air

Air

Air

Collects d

12/19/200 7

12/19/200 7

12/19/200 7

12/19/200 7

Container

Summa Canlster

Sumrna Canister

Summa Canister

Summa Canister

/ ._ : — ^

Sample Time

10:18

10:18

10:30

10:35

Pump#

AC01101

AC00796

AC01312

AC00661

OrlflcelD

£C00403_

FC00572

FC00189

FC00360

Start Pressu

re

-30-

-29.5

-30

-29.5

Stop Pressu

re

-8

-8.5

-7

-8

Volum o

—'4:4

4.3

4.6

4.4

Vol Units

Items/Reason


CHAIN OF CUSTODY *

Relinquished By Date Received by Date Time

KMI2.9037

TO-15 Compound List for Project 0056 Reporting

Limit (ppbv)

vinyl Chloride 0.070 1,1-Dichloroether»e(1,1-DCE) 0.070 Oichloromethane (Methylene Chloride) 0.070 trans-1,2-Dtchloroethene 0.070 1.1- Dichloroethane(1,1-OCA) 0.070 Methyl tert-Buryl Ether 0.070 cis-1,2-Dfchloroetfiene - o.070 1.2- Dfchloroethane 0.070 1.1.1 -Trichloroethane (TCA) 0.070 Benzene 0.070 Trichloroethene (TCE) 0.070 Toluene 0.070 Tetrachloroethene (PCE) 0.070 Chlorobenzene 0.070 m,p-Xylenes 0070 o-Xylene 0.070 Ethyl benzene - 0.070

* After normal diftinon rate of 1-2x

0056-DAR-020808 0 1 0

KMI2.9038

r Table 2.2 Results of the Duplicate Analysis for VOC in Air

WA # 0-056 Kauffman & Minteer Site

Sample No. 43996

Initial Analysis Duplicate Analysis QC ppbv ppbv RPD RPD Limits

U U NC 25 U U NC 25

0.0829 0.0790 5 25 U U NC 25 U U NC 25 U U NC 25 U U NC 25 U U NC 25 U U NC 25

0.249 0.231 7 25 U U NC 25

0.426 0.419 2 25 0.0341 0.0377 10 25

U U NC '25' 0.0575 0.0547 5 25 0.196 0.203 3 25

0.0660 0.0601 9 25

Vinyl Chloride 1,1-Dichloroethene (1,1-DCE) Dichloromethane (Methylene Chloride) trans-1,2-Dichloroethene 1.1- Dichloroethane (1,1-DCA) Methyl tert-Butyl | Ether cis-1,2-Dichloroethene 1.2- Dichloroethahe 1.1.1 -Trichloroethane (TCA) Benzene | Trichloroethene (TCE) Toluene | Tetrachloroethene (PCE) Chlorobenzene Ethylbenzene m.p-Xylenes o-Xylene

0056-DAR-020808 08

sub-surface soil vapor sampling trip report - work ... · work assignment #eac00056 - sub-surface...

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