technical specifications - richmondgov.comtechnical specifications table of contents division 1 –...
TRANSCRIPT
DPU Standard
Table of Contents 00002-1 December 2019
TECHNICAL SPECIFICATIONS
TABLE OF CONTENTS
DIVISION 1 – GENERAL REQUIREMENTS Pages
Section 01110 – Summary of Work 01110-1 – 01110-10
Section 01111 – Construction Manager and Engineer 01111-1 – 01111-2
Section 01250 – Change Order Procedure 01250-1 – 01250-4
Section 01290 – Measurement and Payment 01290-1 – 01290-10
Section 01310 – Coordination and Meetings 01310-1 – 01310-4
Section 01325 – Progress Schedule 01325-1 – 01325-12
Section 01330 – Submittals 01330-1 – 01330-10
Section 01335 – Limitations on Sequence of Construction 01335-1 – 01335-2
Section 01422 – References 01422-1 – 01422-8
Section 01450 – Quality Control 01450-1 – 01450-6
Section 01500 – Construction Facilities and Temporary Controls 01500-1 – 1500-12
Section 01740 – Cleaning 01740-1 – 01740-2
Section 01789 – Contract Close Out 01789-1 – 01789-8
Section 01900 – Special Project Provisions 01900-1 – 01900-4
DIVISION 2 – SITE WORK
Section 02000 – Removal and Disposal of Water Treatment Residuals 02000-1 – 02000-12
DIVISION 3 THROUGH 16 (NOT USED)
SUPPLEMENT A – Contract Drawings
SUPPLEMENT B – WTR Sampling Results
SUPPLEMENT C – Summary Sheet of Lagoon Residuals Removal since 2004
SUPPLEMENT D – Construction Site Safety Plan for Contractors Working on or near Hazardous
Conditions at the Water Purification Plant
SUPPLEMENT E – Manufacturer’s Certificate of Proper Installation
DPU Standard
Table of Contents 00002-2 December 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Summary of Work 01110-1 December 2016
SECTION 01110
SUMMARY OF WORK
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Definitions
B. Description of the Work
C. Plans and Specifications
D. Work Under Other Contracts
E. Contractor's Use of Site
F. Work Sequence
G. Owner Occupancy
H. Constraints
I. Time Provisions
J. Liquidated Damages
K. Protection
L. Boundaries
1.2 DEFINITIONS
A. In addition to the definitions included in the General Conditions of the Contract, the
following words and terms, or pronouns used in their stead, shall, wherever they
appear in this Contract, be construed as follows, unless a different meaning is clear
from the context:
1. "Agents" shall mean an authorized representative of the City including but not
limited to the Engineer, Construction Manager, and other firms and their
partners, principals, members, and employees acting directly or through duly
authorized representatives.
DPU Standard
Summary of Work 01110-2 December 2016
2. "Contract Work" shall mean everything expressly or impliedly required to be
furnished and done by the Contractor by any one or more of the Contract parts
except Extra Work, as hereinafter defined; it being understood that, in case of
any inconsistency in or between any part or parts of this Contract, the
Construction Manager shall determine which shall prevail.
3. "Extra Work" shall mean work other than that required either expressly or
impliedly by the Contract in its present form.
4. "Specifications" shall mean all of the directions, requirements and standards of
performance applying to the work, as hereinafter detailed and designated as
such, or which may be issued in an addendum.
5. "Addendum" or "Addenda" shall mean the additional contract provisions issued
in writing by the Owner prior to the receipt of bids.
6. "Project" shall mean the entire improvement of which the work to be
constructed under this Contract forms a part.
7. "Site" shall mean the designated area upon or in which the Contractor's
operations are carried on and such other areas adjacent thereto as may be
required. "Site" areas may include lands owned by or leased by the Owner and
rights-of-way acquired for the construction of the project.
8. Whenever in the Contract the words "required", "permitted", "designated",
"prescribed", and words of like import are used, they shall imply the
requirement, permission, designation, or prescription of the Construction
Manager; and "approved", "acceptable", "satisfactory", "in the judgment of",
and words of like import shall mean approved by, or acceptable to, or
satisfactory to, or in the judgment of the Construction Manager.
9. “Date of substantial completion” shall be the date as certified by the
Construction Manager when the construction of the work or a specified part
thereof is sufficiently completed, in accordance with the Contract Documents,
so that the work or specified part may be beneficially occupied for the purposes
for which it was intended. Occupancy of individual structures, buildings,
facilities, or the like, being constructed under this contract, shall not constitute
Substantial Completion unless expressly provided for elsewhere in these
documents.
10. "Prevailing Standard Time" shall be construed as the time being observed in the
City of Richmond on the respective days bids are received or other documents
issued or signed, Eastern Standard Time in the winter and Eastern Daylight
Time in the summer.
DPU Standard
Summary of Work 01110-3 December 2016
11. "Final Completion": Date of final completion shall be the date as certified by
the Construction Manager when the construction of the work is complete in
accordance with the Contract Documents, such that no further work remains to
be done at the site or otherwise. The certification of final completion shall serve
as the date when the Contractor has fulfilled all requirements for final payment
as described in the General Conditions of the Contract.
12. “Change Order” is a document which is signed by Contractor and Owner and
authorizes an addition, deletion or revision in the Work and/or adjustment in the
Contract Price or the Contract Time, issued on or after the Effective Date of the
Agreement.
13. “Claim” is a demand or assertion by Contractor for a specific adjustment of
Contract Price or Contract Time or both or other relief with respect to the terms
of the Contract.
14. “Construction Manager” is a person or entity designated as a construction
manager by Owner who provides professional management services, which
contribute to the control of time and the cost and quality of a public construction
project, and who performs those services concurrent with architectural and
engineering services rendered during the design and construction phase of the
Project. This term shall apply to the Owner when the Owner acts as its own
Construction Manager.
15. “Contract Price” are the moneys payable by Owner to Contractor for completion
of the Work in accordance with the Contract Documents as stated in the General
Conditions.
16. “Contract Time” are the number of days or dates stated in Agreement to; (i)
achieve Milestones, if any, and (ii) achieve Substantial Completion.
17. “Drawings” are that part of the Contract Documents prepared or approved by
Engineer which graphically shows the scope, extent, dimensions, location and
character of the Work to be performed by Contractor. Drawings may either be
bound in the same book as the balance of the Contract Documents or bound in
separate sets, and are a part of the Contract Documents, regardless of the
method of binding. Shop Drawings and other Contractor submittals are not
Drawings as so defined.
1.3 DESCRIPTION OF THE WORK
A. General: The Work to be done under this Contract includes the hydraulic dredging,
dewatering and disposal of Water Treatment Residuals (WTR) from the OWNER’s
Water Treatment Plant Residuals Lagoon (Lagoon), maintenance of 4 surface
containment booms, and maintenance along the berm between the lagoon and the pre-
sedimentation basin, maintenance along the eastern edge of the basins, maintenance of
DPU Standard
Summary of Work 01110-4 December 2016
the dewatering pad and along the access road 100 feet west of the dewatering pad. The
anticipated total amount of WTR to be removed from the Lagoon is 8,000 dry tons.
The approximate maximum depth of the Lagoon is 15 feet.
B. The Work includes:
1. Removal and disposal of water treatment residuals (WTR) from the Residuals
Lagoon. The Contractor will be required to remove, dewater, haul, and dispose
of the WTR at an approved disposal or beneficial reuse site(s), in accordance
with all local, state, and federal requirements. It is the Contractor’s
responsibility to locate a suitable site(s) and to obtain all permits as required to
perform the Work, including permits as necessary for the selected disposal or
beneficial reuse site(s). The Contractor shall identify and obtain all permits,
easements, or agreements required for any part of the Work.
2. Maintenance of the berm between the Lagoon and the Basin, the area along the
floodwall on the east end of the Lagoon and Basin, the dewatering pad area, and
100 feet along the access road to the west of the dewatering pad to maintain
visibility for traffic. Maintenance activities include cutting grasses, cattails,
trees, and other vegetation to under 6-inches in height and removing the cuttings
from the site. The area to be maintained is approximately 2.1 acres.
Maintenance should occur as directed by CM and prior to each payment request
submission.
3. Maintenance of four permanent containment booms, as shown on the Drawings
and as specified herein. One containment boom is in the Pre-sedimentation
Basin, the North Raw Water Intake Basin, the South Raw Water Intake Basin,
and the Lagoon Decant/Overflow Structure.
4. Repairs to the dewatering pad including slope repairs, filling holes in pad and
releveling with stone, paving with asphalt, replacing the asphalt curb along the
edges of the pad, and installing a sump and drain line in the pad. These items
are to be installed prior to beginning the removal and disposal of water
treatment residuals and to be maintained throughout the duration of the project.
C. Implied and Normally Required Work: It is the intent of these Specifications to
provide the Owner with complete operable systems, subsystems and other items of
Work. Any part or item of Work which is reasonably implied or normally required to
make each installation satisfactorily and completely operable is deemed to be included
in the Work and the Contract Amount. All miscellaneous appurtenances and other
items of Work incidental to meeting the intent of these Specifications are included in
the Work and the Contract Amount even though these appurtenances may not be
specifically called for in these Specifications.
D. Quality of Work: Regard the apparent silence of the Contract Documents as to any
detail, or the apparent omission from them of a detailed description concerning any
DPU Standard
Summary of Work 01110-5 December 2016
Work to be done and materials to be furnished as meaning that only the best general
practice is to prevail and that only materials and workmanship of the best quality are to
be used. Interpretation of these specifications will be made upon this basis.
E. Compliance with Laws: Comply with all local, State and Federal laws, rules,
ordinances and regulations applicable to this Contract and to the work done hereunder,
Obtain all permits, licenses or other authorization necessary for the prosecution of the
work. The costs for all such permits shall be included in the contract price and no
separate payment will be made therefore, except for permit fees paid by the City for
this project as noted in Section 01900.
1.4 PLANS AND SPECIFICATIONS
A. Plans
1. The Plans for the work to be done under this Contract bear the general title:
Water Treatment Plant Lagoon Residuals Removal – Phase V.
2. When obtaining data and information from the Plans, use figures in preference
to scaled dimensions, and large scale plans in preference to small scale plans.
B. Supplementary Plans
1. When, in the opinion of the Engineer, it becomes necessary to explain more
fully the work to be done or to illustrate the work further or to show any
changes which may be required, plans known as Supplementary Plans, with
specifications pertaining thereto, will be prepared by the Engineer and five
paper prints thereof will be given to the Contractor.
2. The Supplementary Plans shall be binding upon the Contractor with the same
force as the Contract Plans. Where such Supplementary Plans require either less
or more than the estimated quantities of work, credit to the Owner or
compensation therefore to the Contractor shall be subject to the terms of the
Agreement.
C. Contractor to Check Contract Plans and Data
1. Verify all dimensions, quantities and details shown on the Plans, Supplementary
Plans, schedules, Specifications or other data received from the Engineer, and
notify him of all errors, omissions, conflicts, and discrepancies found therein.
Failure to discover or correct errors, conflicts or discrepancies shall not relieve
the Contractor of full responsibility for unsatisfactory work, faulty construction
or improper operation resulting therefrom nor from rectifying such conditions at
his own expense.
DPU Standard
Summary of Work 01110-6 December 2016
2. The Contractor will not be allowed to take advantage of any errors or omissions,
as full instructions will be furnished by the Engineer, should such errors or
omissions be discovered.
3. All schedules are given for the convenience of the Engineer and the Contractor
and are not guaranteed to be complete. The Contractor shall assume all
responsibility for the making of estimates of the size, kind, and quality of
materials and equipment included in work to be done under the Contract.
D. Unforeseen Physical Conditions
1. Promptly notify the Owner and the Construction Manager in writing of any
subsurface or latent physical conditions at the site or in an existing structure
differing materially from those indicated or referred to in the Contract
Documents. The Construction Manager will promptly review those conditions
and advise the Owner in writing if further investigation or tests are necessary.
Promptly thereafter, the Owner shall obtain the necessary additional
investigations and tests and furnish copies to the Construction Manager and the
Contractor.
2. If the Construction Manager finds that the results of such investigations or tests
indicate that there are subsurface or latent physical conditions which differ
materially from those intended in the Contract Documents, and which could not
reasonably have been anticipated by the Contractor, a Change Order shall be
issued incorporating the necessary revisions.
E. Specifications
1. It is hereby agreed that failure by the Contractor to advise his subcontractors
and suppliers of the necessity to review the Specifications as a whole, and not as
individual sections, to determine the work required or to be supplied, shall not
constitute a basis for a claim for additional compensation or an extension to the
Contract completion time.
F. Intent
1. All work called for in the Specifications applicable to this Contract, but not
shown on the Plans in their present form, or vice versa, shall be of like effect as
if shown or mentioned in both.
2. Work not specified in either the Plans or in the Specifications, but involved in
carrying out their intent or in the complete and proper execution of the work, is
required and shall be performed by the Contractor as though it were specifically
delineated or described.
DPU Standard
Summary of Work 01110-7 December 2016
1.5 WORK UNDER OTHER CONTRACTS
A. Contractor will be responsible for coordinating with other projects on site during the
project.
1.6 CONTRACTOR'S USE OF SITE
A. In addition to the requirements of the General Conditions, limit use of site and
premises for work and storage to allow for the following:
1. Owner occupancy and access to operate existing facilities.
2. Coordination of site use with Construction Manager.
3. Responsibility for protection and safekeeping of products under this Contract.
4. Providing additional off site storage at no additional cost to Owner as needed.
B. Noise: Contractor’s use of site shall limit noise levels to comply with current City
code requirements and any other specified requirement.
1.7 WORK SEQUENCE
A. Construct Work in stages to accommodate Owner's use of premises during
construction period and in accordance with the limitations on the sequence of
construction specified. Coordinate construction schedules and operations with
Construction Manager.
B. Coordinate Work of all subcontractors.
1.8 OWNER OCCUPANCY
A. Owner will occupy premises during entire period of construction in order to maintain
normal operations. Cooperate with Owner's representative in all construction
operations to minimize conflict, and to facilitate Owner usage.
B. Conduct operations so as to inconvenience the general public in the least. Comply with
Owner’s request to minimize impacts to the general public.
1.9 CONSTRAINTS
A. The Contract Documents are intended to allow the Contractor flexibility in
construction of the Work, however, constraints described in Section 01335, Limitation
on Sequence of Construction shall apply.
PART 2 PRODUCTS
Not Used
DPU Standard
Summary of Work 01110-8 December 2016
PART 3 EXECUTION
3.1 TIME PROVISIONS
A. Starting Work: Start Work within 10 days following the date stated in the Notice to
Proceed and execute with such progress as may be required to prevent delay to other
contractors or to the general completion of the project.
B. The Contract is a two-year contract. Fifty percent of the work shall be completed and
paid for in the first fiscal year of the Contract. The remaining fifty percent must be
completed by the end of the second year.
C. Unless the contract completion date is modified pursuant to the provisions of the
General Conditions, complete the work covered by this Contract in the number of
consecutive calendar days set forth in the Invitation for Bid. At all times, schedule and
direct the Work so that it provides an orderly progression to Substantial Completion
within the specified time for completion.
D. Milestone Dates: Complete the work no later than the dates given.
1. All Work and Contract Completion: Unless the date of completion is modified
pursuant to the General Conditions, all Work must be completed within the time
period set forth in the Invitation for Bid.
3.2 LIQUIDATED DAMAGES
A. It is agreed between the parties that time is of the essence of this Contract.
B. The amount per day set forth in the Invitation for Bid is hereby agreed upon as the
liquidated damages for each and every calendar day that the time consumed in
completing the work exceeds the time allowed in accordance with the following:
1. In the event that the date for Substantial Completion for all the work occurs
after the work as bid was to be complete or the date to which such date has been
modified by Change Order:
a. The Contractor agrees to pay the Owner liquidated damages, in the
amount per day set forth in the Invitation for Bid, for each calendar day
by which the Date of Substantial Completion exceeds the date work as
bid was to be complete or the date to which such date has been modified
by Change Order.
3.3 PROTECTION
A. During performance and until final acceptance, provide absolute protection of the
finished and unfinished work against any damage, loss, or injury. Take proper
DPU Standard
Summary of Work 01110-9 December 2016
precaution to protect the finished work from loss or damage, pending completion and
the final acceptance of all the work included in the entire Contract. Such precaution
shall not relieve the Contractor from any and all liability and responsibility for loss or
damage to the work occurring before certification of final completion by the Owner.
Such loss or damage shall be at the risk of and borne by the Contractor, whether
arising from acts or omissions of the Contractor or others. In the event of any such loss
or damage, repair, replace, and make good the work without extension of time
therefor, except as may be otherwise specified.
B. The provisions of this subsection shall not be deemed to create any new right of action
in favor of third parties against the Contractor or the Owner.
3.4 BOUNDARIES
A. Confine equipment, apparatus, storage of materials, supplies and apparatus of
workmen to the limits indicated by law, ordinances, permits, shown on the Plans,
specified or direction of the Owner.
END OF SECTION
DPU Standard
Summary of Work 01110-10 December 2016
(NO TEXT FOR THIS PAGE)
DPU Standard
Construction Manager and Engineer 01111-1 December 2016
SECTION 01111
CONSTRUCTION MANAGER AND ENGINEER
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Definitions
1.2 DEFINITIONS
A. Whitman, Requardt & Associates, LLP, 9030 Stony Point Parkway, Suite 220,
Richmond, Virginia, 23235, (804) 272-8700 who is referred to in the Contract
Documents as the Engineer, has prepared the Contract Documents for this Project.
Whitman, Requardt & Associates, LLP shall have the duties and responsibilities as
set forth for the Engineer in the Contract Documents.
B. The Project will be administrated by Construction Manager (CM) that will be
assigned to this project by the City. The CM shall have the duties and
responsibilities as set forth in the General Conditions of the Contract for the
Engineer. The CM will work with the Engineer to resolve engineering questions
concerning the project.
C. The word “Engineer” in the Specifications (Division 1 through Division 17) shall
be replaced with “Construction Manager” except as noted in the following
example. The substitution of the word “Engineer” with “Construction Manager” is
based upon the responsibilities of the “Engineer” in that particular use. As an
example, if the intent is for the Contractor to provide notice to, or submit
information to, or coordinate with Engineer, (i.e. contract administration type
issues) then “Engineer” is to be replaced with “Construction Manager.” If the
intent is for the Engineer to approve substitutions, etc. (engineering type decisions)
then the word “Engineer” shall remain as “Engineer.”
D. The printing of the word “Engineer”, or any similar term, and the substitution of
“Construction Manager” shall not serve as justification for the Contractor not
following his contractual obligations. If there is any question or confusion as to
whether “Engineer” or “Construction Manager” is appropriate, then the Contractor
shall request the Construction Manager to make a formal determination.
DPU Standard
Construction Manager and Engineer 01111-2 December 2016
E. The Owner or Engineer will not normally have direct contact or communication
with the Contractor, his subcontractors or suppliers. All communication from the
Contractor to the Owner or Engineer shall be through the Construction Manager.
To assure continuity between all parties, any communication, oral or written,
between Contractor’s personnel and either the Owner’s operation or maintenance
personnel or Engineer’s technical staff shall be deemed unofficial and non-binding
unless such communication is directed through the Construction Manager.
END OF SECTION
DPU StandardChange Order Procedure 01250-1 April 2019
SECTION 01250
CHANGE ORDER PROCEDURE
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Changes in Construction
B. Extra Work
C. Emergency Work
D. Omitted Work
E. Change Order Procedure
1.2 CHANGES IN CONSTRUCTION
A. Construction Change Orders can be made to the Contract as described in the
General Conditions of the Contract.
1.3 EXTRA WORK
A. The Owner may at any time by a written order and without notice to the sureties
require the performance of such extra work as it may find necessary or desirable.
B. An order for extra work shall be valid only if issued in writing and signed by the
Owner, and the work so ordered shall be performed by the Contractor.
1.4 EMERGENCY WORK
A. In emergencies affecting the safety of persons or the Work or property at the site or
adjacent thereto, the Contractor, without special instruction or authorization from
the Owner is obligated to act at his discretion, to prevent threatened damage, injury
or loss. He will give the Owner prompt written notice of any significant changes in
the Work or deviations from the Contract Documents caused thereby. If the
Contractor believes that additional work done by him in an emergency which arose
from causes beyond his control entitles him to an extension of the Contract
Completion Date or an increase in the Contract Price, he may make a claim
therefor as provided in the General Conditions of the Contract.
DPU StandardChange Order Procedure 01250-2 April 2019
1.5 OMITTED WORK
A. The Owner may at any time by a written order and without notice to the sureties
require the omission of such Contract work as it may find necessary or desirable.
B. An order for omission of work shall be valid only if signed by the Owner and the
work so ordered must be omitted by the Contractor. The amount by which the
Contract price shall be reduced shall be determined as follows:
1. By such applicable unit prices, if any, as are set forth in the Contract; or
2. By the appropriate lump sum price set forth in the Contract; or
3. By the fair and reasonable estimated cost to the Owner, in accordance with
the requirements of the General Conditions Section 5.4.1, Schedule of
Values or other proper costs and price documentation for any Omitted Work
as mutually agreed to by the Contractor and Construction Manager and
approved by the Owner.
1.6 CHANGE ORDER PROCEDURE
A. Initiation: Change order proposal
1. Initiated by Construction Manager or Owner: The Owner or the
Construction Manager may issue a Request for Proposal (RFP). The Request
will contain a description of the intended change with supplementary or
revised Drawings and Specifications as applicable and the projected time for
accomplishing the change.
2. Initiated by Contractor: The Contractor may propose a change in the work
by submittal of a Change Order Request (COR) to the Construction Manager
describing the proposed change with a statement of the reason for the
change and the effect on the contract time and price, along with supporting
documentation.
B. Execution of Change Order Proposal:
1. When a Proposal is requested for a change in the Work, the Contractor shall
submit his proposal within 14 days following receipt of the Request for
Proposal. The Proposal shall state the increase or decrease, if any, in the
Contract Period and/or Contract Sum.
2. The Contractor shall explain the proposal in as much detail as requested by
the Owner.
3. Any decrease in Contract Sum on account of omitted Work will include
appropriate amounts for profit and overhead.
DPU StandardChange Order Procedure 01250-3 April 2019
4. The Owner and Construction Manager will review the Proposal and may
request additional information and documentation which the Contractor
shall provide promptly.
5. If the Owner decides to proceed with the change, it will issue a Change
Order for signature first by the Contractor and then by the Owner.
6. The Contractor will promptly complete the approved change in the Work on
receipt of the executed Change Order.
C. Costs: The cost of both additive and deductive changes in the Work shall be
determined, as follows:
1. Labor: Applied labor cost, crew foreman and general foreman performing
or directly supervising the Work on the Site. Also included are travel and
subsistence, but only in the extent incurred.
2. Insurance: Net premium for Worker's Compensation Insurance, taxes
pursuant to the Federal Social Security Act, payments required under State
and Federal unemployment laws.
3. Additional Materials: Necessary extra materials, delivered at the Site
including the actual cost of consumable supplies. Consumable supplies shall
not be determined by the percentage of cost basis.
4. Plant and Equipment: Rent for plant and equipment shall be at the rental
cost for rentals from an independent firm (i.e. a firm which is not owned in
whole or in part by the Contractor). If the equipment is owned by the
Contractor or rented from a firm in which the Contractor has an interest, the
rent shall be calculated in accordance with the applicable provisions and
terms of the current "Cost Reference Guide for Construction Equipment"
published by Dataquest based on the standard monthly rental rate.
5. Subcontractor Costs: Subcontractor's costs including subtier contractors
shall be determined by items 1 through 4 in the preceding subparagraphs.
Subcontractor overhead and profit shall be limited to the percentage
amounts stipulated in the bid regardless of the number of subtier
subcontractors.
6. Overhead and Profit: Plus percentage amounts stipulated in the bid.
7. During periods of downtime, the following conditions shall also apply:
a. Payment for equipment will be on the basis of a maximum 8-hour
period during each 24 hour period.
DPU StandardChange Order Procedure 01250-4 April 2019
b. No overtime will be included.
c. No compensation for subsistence will be included.
d. The rate of overhead and profit will be 10 percent. for subcontractor labor and materials and 15% for contractor labor and material only.
e. No compensation for equipment overhaul, field repair and fuel expenses shall be included.
END OF SECTION
DPU Standard
Measurement and Payment 01290-1 November 2019
SECTION 01290
MEASUREMENT AND PAYMENT
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Measurement Authority
B. Schedule of Values
C. Application for Payment
D. Unit Quantities Specified
E. Schedule of Contract Items
F. Payment
G. Defect Assessment
H. Non-Payment for Rejected Products
1.2 MEASUREMENT AUTHORITY
A. Measurement: The Construction Manager will take all measurements and compute
quantities accordingly.
B. Assistance: Assistance to the Construction Manager in the form of necessary
equipment, and qualified personnel shall be provided by the Contractor as required for
taking measurements.
1.3 SCHEDULE OF VALUES
A. Approval of Schedule: Submit for approval a schedule of values for all the work
consistent with and generated from the cost loaded CPM schedule as indicated in
Section 01325.
B. Revisions: With each Application for Payment revise schedule to list approved
Change Orders.
DPU Standard
Measurement and Payment 01290-2 November 2019
1.4 APPLICATION FOR PAYMENT
A. The Contractor shall submit to the Construction Manager an updated copy of the cost
loaded CPM schedule as a basis for monthly progress payments to the Contractor. This
updated schedule should be submitted to the Construction Manager on or before the
5th business day of the following month for the previous month.
B. When payment for stored materials is permitted, the Contractor shall submit with the
CPM schedule update a separate schedule for Materials Stored showing line item,
description, previous value received, value incorporated into the work and present
value. Accompanying paid invoices demonstrating proof of ownership shall be
provided in conjunction with any stored material for which the Contractor is
requesting payment.
C. The Construction Manager shall update the schedule based on the Contractor's status
provided in accordance with the schedule update requirements of Section 01325 and
prepare for the Contractor's signature a partial payment request consistent with the
earned value of work as determined by the monthly CPM schedule update.
D. The Contractor shall review and if acceptable execute the partial payment request by
signature of an authorized officer of the Contractor and return to the Construction
Manager for distribution to the Owner for payment. Should the Contractor disagree
with the partial payment request as presented by the Construction Manager, the
Contractor shall respond in writing giving reasons for the areas of disagreement.
E. Retainage from Partial Payments: Retainage in the amount of five (5) percent shall be
deducted from the partial payments as stipulated in the General Conditions of the
Contract and as shown on the Partial Payment Request form.
F. The Contract is a two-year contract. Fifty percent of the work shall be completed and
paid for in the first fiscal year of the Contract. The remaining fifty percent must be
completed by the end of the second year. The Contactor may proceed with
performing more than 50% of the work in the schedule of values in the first fiscal year;
however, the Contractor may not apply for more than 50% of the total bid price in the
first year. Any additional work performed beyond 50% may be billed for in the
second fiscal year. The Contractor may also elect to store equipment onsite if 50% of
the work is completed before the end of the first year, then resume work once the
second fiscal year begins.
1.5 UNIT QUANTITIES SPECIFIED
A. Quantities: Quantities and measurements indicated in the Proposal are for bidding and
contract purposes only. Quantities and measurements supplied or placed in the Work
and verified by the Construction Manager and recorded in his daily report shall
determine the payment.
DPU Standard
Measurement and Payment 01290-3 November 2019
B. Actual Work: If the actual Work requires more or fewer quantities than those
quantities indicated, the required quantities shall be provided at the unit prices
contracted.
C. Units of Work: The intention of the unit prices is to provide a complete, functioning
unit which may include Work from several Specification Sections. All the Work which
is required or which can reasonably be inferred to be required in a unit price item to
deliver a complete, functioning unit shall be included.
1.6 SCHEDULE OF CONTRACT ITEMS
A. Contract Item 1: Mobilization and Demobilization
1. Description:
a. Under the Contract Item for Mobilization and Demobilization, the
Contractor shall provide all labor, services, specialists, material and
equipment for preparatory work and operations, including but not limited
to those necessary for the mobilizing and furnishing site equipment,
materials, supplies and incidentals; for the establishment of all offices,
buildings and other temporary facilities necessary for work on the
project; cost for prepaid bonds and insurance; and for all other work and
operations to be performed or costs incurred to begin work on the
various Contract Items.
b. The City reserves the right in case the Contractor defaults on the
Contract, to retain the use, or have used, the Contractor's plant,
equipment, tools, materials and other property for, and until, completion
of the work, in accordance with Section 7 of the General Conditions of
the Contract.
c. The Contractor is cautioned that the amount to be bid under this Contract
Item shall be as shown in the Bid Price Schedule.
2. Payment:
a. Cost of pre-paid bonds and insurance required for the Contract may be
reimbursed under this Contract Item. Proof of payment by the Contractor
for such bonds and insurance costs will be required if reimbursement is
requested prior to having 2 percent of the original Contract amount, less
the allowances, earned. The amount reimbursed for prepaid bonds and
insurance costs will be included as part of any mobilization payments
stipulated under the below listed terms and there will be no extra or
separate payment for these items.
DPU Standard
Measurement and Payment 01290-4 November 2019
b. When the monthly progress payment estimate of the total amount earned,
not including the amount earned for mobilization, is 2 percent or more of
the original Contract amount, less the allowances, the total amount
earned for mobilization shall be 35 percent of the Contract Item price for
mobilization and this amount will be included in the monthly estimate for
payment.
c. When the monthly progress payment estimate of the total amount earned,
not including the amount earned for mobilization, is 5 percent or more of
the original Contract amount, less the allowances, the total amount
earned for mobilization shall be 70 percent of the Contract Item price for
mobilization and this amount will be included in the monthly estimate for
payment.
d. When the monthly progress payment estimate of the total amount earned,
not including the amount earned for mobilization, is 90 percent or more
of the original Contract amount, less the allowances, the total amount
earned for mobilization shall be 100 percent of the Contract Item price
for mobilization and this amount will be included in the monthly estimate
for payment.
B. Contract Item 2: Removal, hauling, and disposal of Lagoon Residuals
1. Description:
a. The Contractor shall provide all labor, materials, and equipment,
including but not limited to services necessary for or incidental to the
removal, dewatering, hauling and disposal of sediments from the
Residuals Lagoon.
2. Payment:
a. Payment for Lagoon WTR sediment removal, hauling, and disposal/reuse
will be based on the unit price per dry ton of total solids as stated in the
Bid Price Schedule. The unit prices listed in the Bid Price Schedule shall
be used for determining payment for WTR removal. The Contractor shall
perform dredging operations in any portion of the Lagoon as directed by
the CM. All costs for piping and booster pumping, if required, shall be
included in the unit prices listed in the Bid Price Schedule.
b. The OWNER shall perform all sampling and analyses required for
measurement of Work performed. The Contractor shall provide access to
the CM for the collection of representative samples of WTR being hauled
from the plant. WTR and sediment sampling and testing to determine
percent total solids content (%TS) will follow established laboratory
DPU Standard
Measurement and Payment 01290-5 November 2019
procedures and testing as specified in the current edition of “Standard
Methods.” The CM will collect samples as needed.
c. The weight of WTR and sediment will be calculated on a per truckload
basis by the Contractor. The Contractor shall provide the weight of each
truck to the CM, and the CM shall conduct a visual inspection of each
truck as it is loaded and prior to leaving the site. The Contractor shall
weigh each truck at the plant site when empty and loaded. The
Contractor shall provide and use portable scales. The scales are to be
calibrated by the Contractor on a semi-annual basis. OWNER shall
approve vendor selected by the Contractor for scale calibration.
Contractor shall provide a written statement certifying calibration to the
CM. This shall be verified periodically at the OWNER’s direction to the
CM. Other means of determining the weight of WTR or sediment may
be proposed by the Contractor and requires approval by the CM.
d. The dry tonnage of WTR or sediment eligible for payment during any
period will be calculated as the sum of the dry tonnage disposed over the
Contract period. Dry tonnage will be calculated as the WTR or sediment
wet weight in each truckload multiplied by the %TS. Payment will be
determined according to the following payment formula:
[TW - EW] x C x %TS x UP = Payment to Contractor
Where:
TW = Weight of loaded truck (pounds)
EW = Weight of empty truck (pounds)
C = Conversion factor (C = 5 x 10-4)
%TS = Percent total solids as determined by the OWNER's
laboratory analysis
UP = Unit price from Bid Price Schedule (dollars per dry ton)
e. Solids Verification: If so desired, the Contractor may verify the
OWNER’s solids testing procedure through the use of an approved
independent laboratory. WTR or sediment sampling shall be arranged so
that split samples can be obtained at the same time by both the Contractor
and CM. Established sampling procedures (that is, storing, shipping, etc.)
shall be utilized to maintain the integrity of the samples. Given the
precision of the solids determination procedure, only solids content
values that deviate by more than 5 percent for the same split sample will
be taken into consideration when verifying the OWNER’s method. For
cases of greater than 5 percent variation in solids content for the same
split sample, the OWNER’s and Contractor’s values will be averaged and
the resultant mean will be used in determining the dry weight of WTR or
sediment removed for that day only.
DPU Standard
Measurement and Payment 01290-6 November 2019
f. A manifest document will be provided the Contractor to accompany each
truckload from the Water Treatment Plant to the final disposal/reuse site.
The manifest will require the following information:
(1) Project name
(2) Driver's name
(3) Subcontractor name
(4) Truck ID number
(5) Load number
(6) Date and time of truckload
(7) Tare weight
(8) Fully loaded weight
(9) Sample number for percent solids
(10) Location of disposal site
(11) Contractor Superintendent’s signature
(12) CM Inspector’s signature
(13) Truck Driver’s signature
C. Contract Item 3: Vegetative Maintenance of Berm and Dewatering Pad Area
1. Description:
a. The Contractor shall provide all labor, materials, equipment, and
incidentals for maintenance of the berm between the Lagoon and the
Basin, the area along the floodwall on the east end of the Lagoon and
Basin, the dewatering pad area, and 100 feet along the access road to the
west of the dewatering pad to maintain visibility for traffic. Maintenance
activities include cutting grasses, cattails, trees, and other vegetation to
under 6 inches and removing the cuttings from the site. The area to be
maintained is approximately 2.1 acres. Monthly berm maintenance will
be performed at the discretion of the Construction Manager.
2. Payment:
a. Payment for Maintenance Activities shall be made on the frequency as
identified in the Bid Price Schedule, payable following performance of
the work. The unit prices listed in the Bid Price Schedule shall be used
for determining payment for Vegetative Maintenance.
D. Contract Item 4: Maintain Four Containment Booms
1. Description:
a. The Contractor shall provide all labor, materials, equipment, and
incidentals for the maintenance of four spill containment booms at
locations and of approximate lengths as summarized below and shown
on the Drawings.
DPU Standard
Measurement and Payment 01290-7 November 2019
(1) Containment Boom #1: Pre-Sedimentation Basin, 600 foot length.
(2) Containment Boom #2: North Raw Water Intake Basin, 150 foot
length.
(3) Containment Boom #3: South Raw Water Intake Basin, 100 foot
length.
(4) Containment Boom # 4: Lagoon Decant/Overflow Structure, 140
foot length.
2. Payment:
a. Payment for Maintenance Activities shall be on a lump sum basis,
payable in full following completion of the work. The unit prices listed in
the Bid Price Schedule shall be used for determining payment for the
Containment Booms maintenance.
E. Contract Item 5: Repairs to Dewatering Pad Area
1. Description:
a. The Contractor shall provide all labor, materials, equipment, and
incidentals for repairs to the dewatering pad area. Repairs include slope
repairs, filling holes in pad and releveling with stone, replacing the
asphalt curb along the edges of the pad, and installing a sump and drain
line in the pad. These items are to be installed prior to beginning the
removal and disposal of water treatment residuals and to be maintained
throughout the duration of the project.
2. Payment:
a. Payment for Repair Activities shall be on a lump sum basis, payable in
full following completion of the work. The unit prices listed in the Bid
Price Schedule shall be used for determining payment for the Dewatering
Pad Repairs.
F. Contract Item 6: Site Access Delay
1. Description:
a. There is a possibility that the road access to the Lagoon could be blocked
for a work day by DPU or other DPU Contractors. Should road access to
work areas be blocked for a work day by DPU or other DPU Contractors,
as a result of other construction projects that may be in progress during
the Residuals Removal Project, the Contractor is entitled to be
reimbursed for the delay caused by blockage. Site Access Delay days
DPU Standard
Measurement and Payment 01290-8 November 2019
shall be days that have a minimum road closure time of four consecutive
hours.
b. Road blockage to the east end of the Water Treatment Plant (left turn
upon crossing the concrete access bridge) shall not constitute a site
access delay, as access to the work areas can be made by making a right
turn upon crossing the concrete access bridge.
2. Payment: Payment for the delay caused by blockage shall be made with CM
approval. The unit price listed in the Bid Price Schedule shall be used for
determining payment for Site Access Delays.
G. Contract Item 7: Allowance for Additional Site Work
1. Description:
a. Construction conditions may require that changes be made in the location
and installation of the Work, materials to be furnished, and/or other
related Work to be performed hereunder. The CM shall provide the
Contractor with a Request for Proposal form, which shall be completed
by the Contractor within 30 calendar days. When the CM and Contractor
come to agreement on costs and time, the CM will issue a Work Order.
The Contractor, when provided a signed Work Order by the CM, shall
make such adjustments and changes.
b. Use of a part or all of the Allowance will be as approved by the
OWNER.
2. Payment: The Work shall be paid for out of the Allowance, for which
Contractor will receive compensation. See the Bid Price Schedule.
H. Contract Item 8: Allowance for Replacement of Four Containment Booms
1. Description:
a. The Contractor shall provide all labor, materials, equipment, and
incidentals for the installation of four spill containment booms at
locations and of approximate lengths as summarized below and shown
on the Drawings.
(1) Containment Boom #1: Pre-Sedimentation Basin, 600 foot length.
(2) Containment Boom #2: North Raw Water Intake Basin, 150 foot
length.
(3) Containment Boom #3: South Raw Water Intake Basin, 100 foot
length.
(4) Containment Boom # 4: Lagoon Decant/Overflow Structure, 140
foot length.
DPU Standard
Measurement and Payment 01290-9 November 2019
2. Payment:
a. Payment for Installation Activities shall be on a lump sum basis, payable
in full following completion of the work. The unit prices listed in the Bid
Price Schedule shall be used for determining payment for the
Containment Booms installation.
I. Contract Item 9: Allowance for Additional Lagoon Residual Removal
1. Description:
a. The Contractor shall provide all labor, materials, and equipment,
including but not limited to services necessary for or incidental to the
removal, dewatering, hauling and disposal of additional sediments from
the Residuals Lagoon. All requirements set forth in Contract Item No. 2
will apply to this Contract Item.
b. Use of a part or all of the Allowance will be as approved by the
OWNER.
2. Payment: The Work shall be paid for out of the Allowance, for which
Contractor will receive compensation. The unit price listed in the Bid Price
Schedule for Contract Item No. 2 shall be used for determining payment for
additional lagoon residual removal.
1.7 PAYMENT
A. Payment Includes: Full compensation for all required labor, products, tools,
equipment, plant, transportation, services and incidentals; erection or application of an
Item of the Works, overhead and profit.
B. Final Payment: Final Payment for Work governed by unit prices will be made on the
basis of the actual measurements and quantities accepted by the Construction Manager
multiplied by the unit price for the Work which is incorporated in or made necessary
by the Work. Final payment will not be made until submission of Contractor’s as-built
drawings, all training has been completed and other items specified in Section 01789
have been completed.
1.8 DEFECT ASSESSMENT
A. Replace the Work, or portions of the Work, not conforming to the specified
requirements.
B. If, in the opinion of the Construction Manager, it is not practical to remove and replace
the Work, the Construction Manager will direct that the defective Work may remain or
DPU Standard
Measurement and Payment 01290-10 November 2019
be partially replaced and the price will be adjusted to a new price at the discretion of
the Owner.
1.9 NON-PAYMENT FOR REJECTED PRODUCTS
A. Payment will not be made for any of the following:
1. Products wasted or disposed of in a manner that is not acceptable.
2. Products determined as unacceptable before or after placement.
3. Products not completely unloaded from the vehicle.
4. Products placed beyond the lines and grades of the required Work.
5. Contractor supplied products remaining on hand after completion of the Work.
6. Loading, hauling and disposing of rejected products.
B. Cost Loaded Schedule: No payment requests will be accepted until an approved Cost
Loaded Schedule of Values as described in Section 01325, 1.7 is received from the
Contractor. Payment requests will not be accepted until the Cost Loaded Schedule of
Values has been updated by the Contractor for work in place.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Coordination and Meetings 01310-1 June 2019
SECTION 01310
COORDINATION AND MEETINGS
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Coordination
B. Preconstruction Conference
C. Progress Meetings
1.2 COORDINATION
A. The Contractor shall keep the Construction Manager and the Owner fully advised
as to his plans for carrying out the work and obtain the Construction Manager's
approval for all phases of his operations as hereinafter specified.
B. Coordinate scheduling and submittals to assure efficient and orderly sequence of
delivery of Contract work.
C. In accordance with the requirements of section Progress Schedule, the Contractor
shall prepare and submit a comprehensive schedule of his proposed sequence of
construction included under this contract for review by the Construction Manager.
D. The schedule shall be arranged to complete the work in phases and permit
operation by the Owner of completed phases or parts thereof.
E. The Contractor is cautioned that his schedule for certain areas of the work may be
affected by work included under other Contracts. The Contractor shall coordinate
mobilization, hauling, and demobilization activities with all other contractors at the
WTP site and attend a monthly coordination meeting with the Construction
Manager.
F. Work on this Contract shall be coordinated with the work of other contracts. The
Contractor shall notify the Construction Manager of the Contractor's planned
procedures for each specific alteration of work which may effect work under other
contracts before the alteration begins. The Contractor shall not begin any alteration
until specific permission has been granted by the Construction Manager in each
case and shall provide the Construction Manager with sufficient advance notice as
not to impact the Contractor's schedule or the work of the other contracts.
DPU Standard
Coordination and Meetings 01310-2 June 2019
G. If it is necessary for the proper coordination and installation of work by Others, the
Contractor shall reschedule his operations so that his work will not conflict with
necessary operations of the other contracts. Such rescheduling shall not be cause
for a time extension except as provided for in the General Conditions of the
Contract.
H. The Construction Manager shall be the sole judge of when the Contractor's
operations are causing interference with, or delay to, the work or operations of
other contracts, and his orders and instructions shall be carried out without delay.
1.3 PRECONSTRUCTION CONFERENCE
A. General: Prior to commencement of Work at the Site, a Preconstruction
Conference shall be required. The meeting date shall be determined by the
Construction Manager. The Construction Manager will notify the attendees of the
meeting date.
B. Attendance: The conference shall be attended by the following:
1. The Contractor
2. The representatives of principal suppliers and manufacturers as appropriate
3. The Construction Manager and his resident project representative
4. The Authorized Representatives of the Engineer
5. The Authorized Representatives of the Owner
6. Governmental representatives as appropriate
7. Others, as requested by the Contractor, the Owner, or the Construction
Manager
C. Delineation of Responsibilities: The purpose of the conference is to designate
responsible personnel, to establish a working relationship among the parties and to
identify the responsibilities of the Owner, Construction Manager and the
Contractor. Matters requiring coordination will be discussed and procedures for
handling such matters, established. The agenda will include:
1. Start Work Date
2. Submittal Procedures
3. Partial Payment Procedures
4. Maintenance of Records
5. Contractor's Request for Clarification
6. Schedules, Sequences and Maintenance of Facility Operations
7. Safety and First Aid Responsibilities
8. Change Orders
9. Use of Site
10. Equipment Delivery
11. Site Access
12. Work Hours
13. Contractor Safety Plan
DPU Standard
Coordination and Meetings 01310-3 June 2019
14. Discussion of Shop Testing, Factory Testing, Functional Testing, and
Performance Testing Requirements
D. Chair and Minutes: The preconstruction conference will be scheduled and chaired
by the Construction Manager who will also arrange for the keeping and
distribution of minutes to all attendees.
1.4 PROGRESS MEETINGS
A. Meeting Frequency and Format: The Construction Manager shall schedule and
chair progress meetings. Progress Meetings shall be held once every two or four
weeks or more frequently as determined by the complexity of the Project at the
request of the Owner, Construction Manager, Engineer or Contractor. The
following topics will be reviewed at a minimum at each meeting: Distribution
Coordination, Shop Drawing Review, Requests for Clarification, Requests and
Proposals for Changes, Change Orders, Non-Conformance Notices, Progress and
Schedule, Quality Control, New Business, Shut Downs, Tie-ins and System
Impacts, Facility Outages, Permit and Inspection Status, Testing and Startup
Activities. The Contractor may invite suppliers and subcontractors as appropriate.
Minutes of the meeting will be maintained by the Construction Manager and
distributed to all parties. Draft meeting minutes shall be distributed to all parties
within seven calendar days after each meeting. The first Progress Meeting shall be
coordinated with all parties at the preconstruction conference.
B. Meeting Minutes Review: The Contractor, Engineer, and Owner shall review and
approve or propose additions or corrections to the draft meeting minutes within
seven calendar days after receiving the draft meeting notes. The Construction
Manager shall then proceed to finalize the meeting minutes and shall distribute
them to all parties.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Coordination and Meetings 01310-4 June 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Progress Schedule 01325-1 June 2019
SECTION 01325
PROGRESS SCHEDULE
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Form of Schedules
B. Working Hours
C. Scheduling Responsibilities
D. Submittals
E. Network Requirements
F. Cost Loading
G. Progress of the Work
H. Schedule Updates
I. Causes for Extensions of Time
J. Abnormal Weather
K. Approval Requests
L. Adjustment by Owner
M. Failure to Adhere to Schedule
1.2 FORM OF SCHEDULES
A. Prepare schedules in the form of Critical Path Method (CPM) as described herein.
1. Provide separate CPM networks (subnetworks) of activities for each process
or facility.
2. Each subnetwork shall be assigned a code and separate activity numbering
series.
DPU Standard
Progress Schedule 01325-2 June 2019
3. Interrelationships between subnetworks and any individual activities shall be
identified.
1.3 WORKING HOURS
A. Work Hours: Perform work between 8:00 a.m. and 5:00 p.m. on weekdays only,
except for specified after hours work. Do not perform work on Saturday, Sundays,
City holidays, or between 5:00 p.m. and 8:00 a.m. without written permission of
Owner. Extraordinary noise such as driving sheeting shall only be permitted
between 9:00 a.m. and 4:00 p.m. Comply with working hour restrictions required
by City traffic engineering department. Production may only take place while
Construction Manager is onsite.
B. Holidays: The City observes a five-day work week and the following holidays:
New Year's Day; Martin Luther King's Birthday; Washington's Birthday; Good
Friday; Memorial Day; Independence Day; Labor Day; Veterans Day;
Thanksgiving Day; the Friday after Thanksgiving; Christmas Eve and Christmas
Day. The Contractor will not be permitted to work on these holidays unless
otherwise authorized by the Construction Manager.
C. Work After Hours: Night work may be established by Contractor as regular
procedure with written permission of Owner. Such permission, however, may be
revoked at any time by Owner if Contractor fails to maintain adequate equipment
and supervision for proper prosecution and control of work at night.
D. Written Requests for Work Outside of Normal Work Hours: Written requests for
work between 5:00 p.m. and 8:00 a.m. on weekdays, and for work on Saturday,
Sundays, and City holidays shall be made in writing at least two weeks prior to
needing the work outside of normal work hours. Written approval from the Owner
shall be obtained before any Work is conducted outside normal working hours.
E. The Owner will charge Contractor for costs of Owner’s, Construction Manager’s,
and Engineer’s personnel for work outside of normal work hours as described in
Paragraph D above. Costs will be charged as a Credit to the City on the next partial
payment credit. Cumulative costs will be included in a change order which will
show credit to the Owner. The Construction Manager will record Owner’s,
Construction Manager’s, and Engineer’s hours outside of normal work hours.
F. Emergencies: In case of an emergency which may require that work be done on
Saturdays, Sundays, holidays or longer than ten hours per day, the Contractor shall
request the permission of the Construction Manager to do so. If, in the opinion of
the Construction Manager, the emergency is bona fide, he will grant permission to
the Contractor to work such hours as may be necessary. Also, if in the opinion of
the Construction Manager, a bona fide emergency exists, he may direct the
Contractor to work such hours as may be necessary whether the Contractor
requests permission to do so or not.
DPU Standard
Progress Schedule 01325-3 June 2019
1.4 SCHEDULING RESPONSIBILITIES
A. The Critical Path Method type construction schedule will be used to monitor job
progress and as a means to make monthly payments to the Contractor except for
Stored Materials which will be made in accordance with Section 6 of the General
Conditions of the Contract. Be responsible for providing all information
concerning the sequencing, logic and durations of all activities as well as providing
the initial CPM logic network diagram and tabular report data. Once the initial
logic network diagram is accepted, be responsible for providing monthly update
information on logic changes, percent complete, actual start and finish dates, and
duration changes. The Contractor will not be required to produce the monthly
computerized printout of the schedule updates. The monthly updating and report
and plot generation will be performed by the Construction Manager using
information provided by the Contractor.
B. It should be clearly understood that the initial schedule and all update information
must be provided by the Contractor, and that this information is a representation of
the best efforts of the Contractor and his subcontractors as to how they envision
the work to be accomplished. Similarly, all progress information to be provided by
and through the Contractor must be an accurate representation of his, or his
subcontractor's, or supplier's actual performance. The schedule shall at all times
remain an accurate reflection of the Contractor's actual or projected sequencing of
work. Once accepted, adherence to the established CPM schedule shall be
obligatory upon the Contractor, and his subcontractors for the work under this
Contract. The Construction Manager may require the Contractor to revise the
schedule if, in his judgment, the schedule does not accurately reflect the actual
execution of the work, or is in violation of any provision of the CPM scheduling
requirements; and the Contractor shall revise the schedule as often as is necessary
to bring the course of performance of the work without additional cost to the
Owner.
1.5 SUBMITTALS
A. General: Provide all submittals, including the following, as specified in Division
1.
B. CPM Schedule:
1. Within fifteen (15) calendar days after Notice to Proceed, submit six (6)
prints of the proposed CPM network diagrams, tabular reports for the entire
Contract duration and include both procurement and construction activities.
Sort the tabular reports by total float and activity number. They shall also
contain a predecessor/successor resource loading report, and project
calendar. This logic diagram shall be drawn as described herein and will be
the subject of a schedule review meeting with the Contractor, the Owner,
and Owner's representatives within two (2) weeks of its submission.
DPU Standard
Progress Schedule 01325-4 June 2019
2. Submit network diagrams and reports, Microsoft Project or Primavera
schedules in digital format on CD.
3. If a review of the submitted CPM Schedule indicates a work plan which will
not complete the work within the Contract Time stated in the Contract,
revise the CPM Schedule as required and resubmit it until it is acceptable.
Failure to submit an acceptable schedule may, at the Owner's sole discretion,
be cause for the withholding of any partial payment(s) otherwise due under
the Contract.
4. Acceptance of the schedule shall not constitute a representation by the
Owner or Construction Manager that the work can be completed as shown
on the schedule.
C. Submittals Schedule:
1. In addition to the above scheduling requirements, submit a complete and
detailed listing of anticipated submittals during the course of the Contract.
Coordinate submittals with those of subcontractors and suppliers, and
identify each submittal as specified. Indicated the anticipated submission
date for each submittal along with the date on which its return is anticipated.
Review time for submittal shall be as provided for in Section 01330 -
Submittals. Durations shown for review shall be to share available float for
that path. Submittals and the review time, of which are on the critical path,
shall be clearly marked in red with the words "Critical Path" by the
Contractor at the time of submission.
2. Submit the Submittal Schedule within fifteen (15) working days from the
Notice to Proceed. The Submittal Schedule will then be accepted or revised
as required, and the Contractor will incorporate the dates and review
durations into his CPM Schedule.
1.6 NETWORK REQUIREMENTS
A. The network diagram shall show the interdependence of activities, and the
sequence in which the work is to be accomplished as planned by the Contractor.
The basic concept of the network analysis diagram is to show how the start of a
given activity is dependent on the completion of preceding activities, and its
completion restricts the start of succeeding activities. A time scaled precedence
format will be followed. The detailed network diagram will be time scaled
showing a continuous flow from left to right.
B. The Schedule Activities shall be developed into three major groups:
1. Procurement Activities: Procurement Activities shall include at a minimum:
a. Permits
DPU Standard
Progress Schedule 01325-5 June 2019
b. Easements
c. Program(s)
d. Submittal Items
e. Approval of Submittal Items
f. Fabrication and Delivery of Submittal Items
Permits, easements, and fabrication and delivery items shall be tied logically
to the correct construction activity in the overall CPM construction
schedule.
2. Construction Activities: Construction activities will be physical work
activities that describe how the job will be constructed.
3. Close-out: CPM activities for this group shall include all work required to
satisfy to appropriate specification sections and meet the requirements of
substantial and final completion.
C. Break the work into activities, with durations of one to twenty (1 to 20) working
days each, except for non-construction activities (such as procurement of materials
and delivery of equipment), and other activities which may require longer
durations. To the extent feasible, activities related to a specific physical area of the
project shall be grouped on the network for ease of understanding and
simplification. The selection and number of activities shall be subject to the review
of the Construction Manager.
D. Each activity on the network shall have indicated for it the following:
1. A single duration, no longer than 20 days (i.e., the single best estimate of the
expected elapsed time considering the scope of work involved in the
activity) expressed in working days. City holidays and weather delays shall
be included. One critical path shall be shown for the schedule.
2. An activity I.D. number will be assigned to each activity. The I.D. number
will be numeric with a maximum of ten (10) digits.
3. A brief description of the activity will be included. If this description is not
definitive, a separate listing of each activity and a descriptive narrative may
be required.
4. Each activity (except for procurement activities and unit price activities)
shall be cost loaded to indicate the total estimated costs of the activity. No
activity shall exceed $60,000 except if an equipment item. Material costs
shall be assigned to delivery activities.
5. Each construction activity shall be man-hour loaded with the estimated man-
hours to be expended on each activity.
DPU Standard
Progress Schedule 01325-6 June 2019
E. When preparing the CPM construction schedule, consider all construction
sequence and critical construction activities requirements.
F. Failure to include on a network any element of work required for the performance
of this Contract shall not excuse the Contractor from completing all work required
within the applicable Contract Time, notwithstanding Construction Manager's
network review.
G. A CPM schedule which shows a completion of any portion of the construction
work (not including testing and start-up) prior to the Contract Time dates may be
accepted but in no event shall be acceptable as a basis for a claim for delay against
the Owner by the Contractor.
H. The schedule calendar shall be a 5 day work week with holidays corresponding to
those observed by the City of Richmond's Department of Public Utilities.
1.7 COST LOADING
A. Schedule of Values:
1. Each activity for Work-in-Place on the construction schedule shall be
allocated a dollar value in accordance with paragraph 1.6.D.4 above. Each
activity's assigned cost shall consist of labor, equipment, and materials costs,
and a prorated contribution to overhead and profit. The sum of the activities
costs shall be equal to the total contract price. Activities not directly related
to Work-in-Place including Stored Materials, preparation and submittal of
Shop or Working Drawings, or other required submittal or equipment and
material procurement shall not be cost loaded. In submitting cost data the
Contractor certifies that they are not unbalanced, and that the value assigned
to each activity represents the Contractor's estimate of the actual costs of
performing that activity. The listing of cost loaded CPM activities will
become the Schedule of Values, and will serve as the basis for payments to
the Contractor for non-unit price items.
2. The accepted schedule of values shall represent a fair, reasonable and
equitable dollar cost allocation for each activity on the Contractor's
construction schedule.
B. Documentation: If it is determined that the cost data do not meet the requirements
for a balanced bid breakdown, provide documentation substantiating any cost
allocation on the cost data. Cost allocations shall be considered unbalanced if an
activity on the construction schedule has been assigned a disproportionate
allocation of direct costs, overhead and profit.
DPU Standard
Progress Schedule 01325-7 June 2019
1.8 PROGRESS OF THE WORK
A. The work shall be started on the date indicated in the Notice to Proceed and shall
be executed with such progress as may be required to prevent delay to other
contractors or to the general completion of the project. The work shall be executed
at such times and in or on such parts of the project, with such forces, material and
equipment, as to assure completion of the work in the time established by the
Contract. Additionally, schedule and direct the work so that it provides an orderly
progression of the work to completion within the specified Contract Time. Fifty
percent of the work shall be completed and billed for during the first year of the
contract and fifty percent shall be completed by the end of the two year contract.
B. Whenever it becomes apparent from the current monthly CPM Schedule update
that delays to the critical path have resulted; and these delays are through no fault
of the Owner, or Owner's representatives, and hence, that the Contract completion
date will not be met, or when so directed by the Construction Manager, take some
or all of the following actions at no additional cost to the Owner.
1. Increase construction manpower in such quantities and crafts as will
substantially eliminate the backlog of work.
2. Increase the number of working hours per shift; shifts per working day, or
days, per week; the amount of construction equipment; the forms for
concrete work; etc., or any combination of the foregoing to substantially
eliminate the backlog of work.
3. Schedule activities to achieve maximum practical concurrence of
accomplishment of activities, and comply with the revised schedule.
C. Submit for review a written statement of the steps to be taken to remove, or arrest
the delay to the schedule. If the Contractor fails to submit a written statement of
the steps he intends to take or fails to take such steps as required by the Contract;
the Owner may direct the level of effort in manpower and trades, equipment, work
schedule and overtime to remove or arrest the delay to the critical path in the
accepted schedule, and the Contractor shall promptly provide such level of effort at
no additional cost to the Owner. In addition, should schedule delays persist, the
Contractor's bond agent will be asked to attend meetings to update the schedule.
D. Failure of the Contractor to comply with the requirements of this provision shall
subject him to, at the Owner's sole discretion, withholding, in partial or in total,
payments otherwise due the Contractor for work performed under this Contract.
The Contractor agrees that any withholding of moneys is not a penalty for
noncompliance, but is an assurance for the Owner that funds will be available to
implement these requirements should the Contractor fail to do so, since failure of
the Contractor to comply with these requirements shall mean that the Contractor
failed to execute the work with such diligence as to ensure its completion within
the time for completion.
DPU Standard
Progress Schedule 01325-8 June 2019
1.9 SCHEDULE UPDATES
A. Monthly Meetings: A monthly Schedule Update Meeting will be held on the first
week of each month, at the construction site to review and update the CPM
Schedule for the previous month. The Schedule Update Meeting will be chaired by
the Construction Manager and attended by the Owner and the Contractor. Actual
progress of the previous month will be recorded and future activities will be
reviewed. The duration of activities and their logical connections may be revised
as needed. Decisions made at these meetings and agreed to by all parties are
binding with the exception that no contract completion dates will be modified
without formal written requests and acceptance as specified herein. In either case,
provide the following information for each update at a minimum:
1. Actual start and finished dates for all completed activities.
2. Actual start dates for all started but incomplete activities including
remaining durations and/or percent completes.
B. Withholding of Payments: Failure to provide specified updated information or
failure to attend progress meetings may result in the withholding of progress
payments.
1.10 CAUSES FOR EXTENSIONS OF TIME
A. The Contract completion time will be adjusted only for causes specified in this
Contract. In the event the Contractor requests an extension of any contract
completion date, he shall furnish justification and supporting evidence per the
General Conditions, and provide a detailed CPM Schedule delay analysis based on
the most current updated CPM Schedule. The Construction Manager will after
receipt of such justification and supporting evidence, make findings of fact and
will advise the Contractor in writing thereof. If the Construction Manager finds
that the Contractor is entitled to an extension of the Contract completion date
under the provisions of the Contract, the Construction Manager's determination as
to the total number of days extension shall be based upon the current accepted and
updated CPM schedule and on all data relevant to the extension. Such data shall be
included in the next monthly updating of the schedule. The Contractor
acknowledges and agrees that actual delays in activities, which according to the
CPM schedule, do not affect any contract completion date shown by the critical
path in the network, do not have any effect on the Contract completion date or
dates, and therefore will not be the basis for a change in Contract completion time.
1.11 ABNORMAL WEATHER
A. The Contract Period will be adjusted to account for unusually severe weather
conditions which prevent or inhibit the Contractor's performance of the Work and
lengthen the critical path indicated on the Schedule (such unusually severe weather
DPU Standard
Progress Schedule 01325-9 June 2019
conditions referred to herein as "Inclement Weather"). It is the intent of this
provision to offset the impact of Inclement Weather with unusually favorable
weather conditions which immediately precede and/or follow the occurrence of
Inclement Weather.
B. The Contractor shall notify the Construction Manager in writing of the occurrence
of Inclement Weather within two days after the onset of such Inclement Weather
and shall describe in reasonable detail the type of Inclement Weather encountered
by the Contractor and the Work thereby interfered with or interrupted.
C. This provision specifies the procedure for the determination of time extensions for
unusually severe weather. In order for the Construction Manager to award a time
extension under this clause, the following conditions must be satisfied:
1. The weather experienced at the project site during the contract period must
be found to be unusually severe, that is, more severe than the adverse
weather anticipated for the project location during any given month.
2. The unusually severe weather must actually cause a delay to the completion
of the project. The delay must be beyond the control and without the fault or
negligence of the Contractor.
D. Schedule: The following Schedule of Monthly Anticipated Adverse Weather
Delays is based on National Oceanic and Atmospheric Administration (NOAA) or
similar data for the project location and will constitute the base line for monthly
weather time evaluations. The Contractor's progress schedule must reflect these
anticipated adverse weather delays in all-weather dependent activities.
SCHEDULE OF MONTHLY ANTICIPATED ADVERSE WEATHER DELAYS
WORK DAYS BASED ON (5) DAY WORK WEEK
JAN FEB MAR APR MAY JUN JUL AUG SEP OCT NOV DEC
City of
Richmond10 9 9 6 8 7 8 7 6 5 7 9
E. Records: Upon acknowledgement of the Notice to Proceed and continuing
throughout the contract, the Contractor will record daily, and submit to the
Construction Manager, the occurrence of adverse weather and resultant impact to
normally scheduled work. Actual adverse weather delay days must prevent work
on critical activities for 50 percent or more of the Contractor's scheduled work day.
F. Impacted Days: The number of actual adverse weather days shall include days
impacted by actual adverse weather (even if adverse weather occurred in previous
month), be calculated chronologically from the first to the last day in each month,
and be recorded as full days. If the number of actual adverse weather delay days
exceeds the number of days anticipated in the Schedule of Monthly Anticipated
Adverse Weather Delays, above, the Construction Manager will convert any
DPU Standard
Progress Schedule 01325-10 June 2019
qualifying delays to calendar days, giving full consideration for equivalent fair
weather work days, and issue a modification in accordance with Section 01250 -
Change Order Procedure.
G. CONTRACTOR shall be responsible for providing the necessary provisions to
maintain operations during cold weather conditions, as may be required. OWNER
shall not be responsible for any delays or additional costs associated with cold
weather operations.
1.12 APPROVAL REQUESTS
A. From time to time, as the work progresses and in the sequence indicated by the
accepted progress schedule, the Contractor must submit to the Construction
Manager a specific request, in writing, for each item of information or approval
required of him by the Contract. These requests must be submitted sufficiently in
advance of the date upon which the information or approval is actually required by
the Contractor to allow for the time the Construction Manager may take to act
upon such submissions or resubmissions.
B. The Contractor shall not have any right to an extension of time on account of
delays due to his failure to submit his requests for the required information or the
required approval in accordance with these requirements.
1.13 ADJUSTMENT BY OWNER
A. From time to time it may be necessary for the Contract schedule and/or Contract
Times to be adjusted by the Owner due to the effects of job conditions, acts or
omissions of other contractors not directly associated with this contract, weather,
technical difficulties, strikes, unavoidable delays on the part of the Owner or his
representatives, and other enforceable conditions which may indicate schedule
adjustments and/or completion time extension. Under such conditions, the
Construction Manager shall direct the Contractor to reschedule the work to reflect
the changed conditions, and the Contractor shall revise his schedule accordingly.
Schedule extensions affecting the Contract Times shall be granted only by the
Owner in writing. It is specifically pointed out that the use of available total float
in the CPM schedule may be used by the Owner and his representatives, as well as,
by the Contractor.
B. Without obligation to extend the Contract Times or any intermediate completion
dates set out in the CPM network, the Owner may initiate changes to the Contract
work that absorb float time only. Owner-initiated changes that affect the critical
path on the CPM network shall be the sole grounds for extending or shortening the
Contract Times. Contractor initiated changes that encroach on the float time,
identified in the CPM network, may be accomplished with the Owner's
concurrence. Such changes, however, shall give way to Owner-initiated changes
competing for the same float time.
DPU Standard
Progress Schedule 01325-11 June 2019
1.14 FAILURE TO ADHERE TO SCHEDULE
A. If the Contractor fails to adhere to the schedule, the City may withhold partial
payments until such time as the Work is at least within 90% of the projected
schedule in accordance with the General Conditions of the Contract.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Progress Schedule 01325-12 June 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Submittals 01330-1 June 2019
SECTION 01330
SUBMITTALS
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Description of Requirements
B. Submittal Procedures
C. Specific Submittal Requirements
D. Action on Submittals
E. Approval by the Contractor
F. Review of Shop Drawings by the Construction Manager and Engineer
G. Resubmittals
H. Forms
1.2 DESCRIPTION OF REQUIREMENTS
A. This section specifies procedural requirements for Shop Drawings, product data,
samples, and other miscellaneous Work-related submittals.
B. Electronic Submittals: Submittals and other documents shall be made in
electronic, PDF, format to the Construction Manager.
1. Additional hard paper copies of pages larger than 11x17 inches shall be
submitted and include eight (8) copies which shall be in addition to the one
(1) electronic copy.
2. Detailed procedures for handling electronic submittals will be discussed at
the preconstruction conference.
3. Submittals will be returned to the Contractor from the Construction Manager
in electronic format.
C. Procedures concerning items such as listing of manufacturers, suppliers,
subcontractors, construction progress schedule, schedule of Shop Drawing
DPU Standard
Submittals 01330-2 June 2019
submissions, bonds, payment applications, insurance certificates, and schedule of
values are specified elsewhere.
D. Work-Related Submittals:
1. Shop Drawings: Includes technical data and drawings specially prepared for
this Project, including fabrication and installation drawings, software
programming, diagrams, actual performance curves, data sheets, schedules,
templates, patterns, reports, storage instructions, design mix formulas,
measurements, and similar information not in standard printed form.
a. Standard information prepared without specific reference to the
Project is not considered a Shop Drawing.
2. Product Data: Includes standard printed information on manufactured
products, and systems that has not been specially prepared for this Project,
including manufacturer's product specifications, equipment storage,
handling and installation instructions, catalog cuts, standard wiring
diagrams, printed performance curves, mill reports, standard color charts,
and recommended spare parts.
3. Samples: Includes both fabricated and manufactured physical examples of
materials, products, and units of work, partial cuts of manufactured or
fabricated work, swatches showing color, texture, and pattern, and units of
work to be used for independent inspection and testing.
4. Miscellaneous Submittals: Work-related submittals that do not fit in the
previous categories, such as guarantees, warranties, certifications,
experience records, maintenance agreements, Operating and Maintenance
Manuals, workmanship bonds, survey data and reports, physical work
records, quality testing and certifying reports, copies of industry standards,
record drawings, field measurement data, and similar information, devices,
and materials applicable to the Work.
1.3 SUBMITTAL PROCEDURES
A. Scheduling:
1. Submit for approval, a preliminary schedule of shop drawings and samples
submittals, in duplicate, within 15 days after the date stated as the date to
proceed at the Preconstruction Conference.
2. Prepare and transmit each submittal to Construction Manager sufficiently in
advance of scheduled performance of related work and other applicable
activities. Allow a minimum of 14 days for Construction Manager and
Engineer's review of normal submittals and all of a minimum of 30 days for
Engineer's review of software programming submittals.
DPU Standard
Submittals 01330-3 June 2019
B. Coordination:
1. Coordinate preparation and processing of submittals with performance of
work. Coordinate each submittal with other submittals and related activities
such as testing, purchasing, fabrication, delivery, and similar activities that
require sequential activity.
2. Coordinate submission of different units of interrelated work so that one
submittal will not be delayed by Construction Manager and Engineer's need
to review a related submittal. Construction Manager and Engineer may
withhold action on any submittal requiring coordination with other
submittals until related submittals are forthcoming.
C. Submittal Preparation:
1. Stamp and sign each submittal certifying to review of submittal, verification
of products, coordination of information within submittal with requirements
of the Work and the Contract Documents, and verification that product will
fit in space provided.
2. Stock or standard drawings will not be accepted for review unless full
identification and supplementary information is shown thereon in ink or
typewritten form.
3. A submittal shall not encompass more than one paragraph of the
Specifications.
4. Submit one (1) electronic copy and eight (8) hard copies of all pages larger
than 11x17 niches for all submittals and resubmittals accompanied by a
letter of transmittal. The form of the letter of transmittal which shall be used
is as shown at the end of this section. The letter of transmittal shall contain
the following information.
a. Identification of the Contractor, subcontractor or supplier.
b. Project title, project number and division, and contract number.
c. Submittal number comprised of specification chapter number,
paragraph number and suffix.
d. Drawing sheet, and detail number as appropriate.
e. Contractor's stamp or certification the products have been reviewed
and are in accordance with the requirements of the Work and the
Contract Documents.
DPU Standard
Submittals 01330-4 June 2019
f. Listing of variations from Contract Documents and any limitations
which may be detrimental to the Work.
5. Shop Drawing Numbering:
a. All shop drawing submittals shall be numbered as follows:
(A) - (B) __
(Specification Section No.) (Consecutive No. / Submittal Rev.)
where:
(A) = Specification Section Number
(B) = Consecutive submittal number for the specification
section number listed in (A) with an alphabetic suffix
identifying the revision number.
Example: 01300-001A - indicates the initial submission
of submittal number 001 for
Specification Section 01300.
01300-001B - indicates the first revision of
submittal number 001 for
Specification Section 01300.
01300-002A - indicated the initial submission
of submittal number 002 for
Specification section 01300.
b. When an item is resubmitted for any reason, transmit under a new
letter of transmittal and with the same submittal number indicated
revised by an alphabetic suffix. List the previous transmittal number
and date.
D. Resubmittal Preparation:
1. Comply with the requirements described in Submittal Preparation. In
addition:
a. Make any corrections or changes in submittals required by
Construction Manager and Engineer's notations on returned submittal.
DPU Standard
Submittals 01330-5 June 2019
b. Respond to Engineer's notations:
(1) On the transmittal or on a separate page attached to
Contractor's resubmission transmittal, answer or acknowledge
in writing all notations or questions indicated by Construction
Manager and Engineer on Construction Manager and
Engineer's transmittal form returning review submission to
Contractor.
(2) Identify each response by question or notation number
established by Construction Manager and Engineer.
(3) If Contractor does not respond to each notation or question,
resubmission will be returned without action by Construction
Manager and Engineer until Construction Manager and
Contractor provides a written response to all Engineer's
notations or questions.
1.4 SPECIFIC SUBMITTAL REQUIREMENTS
A. Specific submittals required for individual elements of work are specified in the
individual Specification sections. Except as otherwise indicated in Specification
sections, comply with requirements specified herein for each indicated type of
submittal.
B. Shop Drawings:
1. Submit newly prepared information, with graphic information at accurate
scale. Indicate name of manufacturer or supplier (firm name). Show
dimensions and clearly note which are based on field measurement; identify
materials and products which are included in the Work; identify revisions.
Indicate compliance with standards and notation of coordination
requirements with other work. Highlight, encircle or otherwise indicate
variations from Contract Documents or previous submittals.
2. Include on each drawing or page:
a. Submittal date and revision dates.
b. Project name, division number and descriptions.
c. Detailed specifications section number and page number.
d. Identification of equipment, product or material.
e. Name of Contractor and Subcontractor.
DPU Standard
Submittals 01330-6 June 2019
f. Name of Supplier and Manufacturer.
g. Standards or Industry Specification references.
h. Identification of deviations from the Contract Documents.
i. Contractor's stamp, initialed or signed, dated and certifying to review
of submittal, certification of field measurements and compliance with
Contract.
j. Physical location and location relative to other connected or attached
material at which the equipment or materials are to be installed.
3. Distribution:
a. Do not proceed with fabrication of equipment until copy of applicable
product data showing only approved information is in possession of
installer.
C. Miscellaneous Submittals:
1. Inspection and Test Reports:
a. Classify each inspection and test report as being either "Shop
Drawings" or "product data", depending on whether report is specially
prepared for Project or standard publication of workmanship control
testing at point of production. Process inspection and test reports
accordingly.
2. Guarantees, Warranties, Maintenance Agreements, and Workmanship
Bonds:
a. Refer to Specification sections for specific requirements. Submittal is
final when returned by Construction Manager marked "Approved" or
"Approved as Noted".
b. Provide copies where required for maintenance data.
3. Certifications:
a. Refer to Specification sections for specific requirement on submittal
of certifications. Certifications are submitted for review of
conformance with specified requirements and information. Submittal
is final when returned by Construction Manager marked "Approved".
Include copies of all certifications in the Operation and Maintenance
Manual.
DPU Standard
Submittals 01330-7 June 2019
4. Closeout Submittals:
a. Refer to Specification sections and section titled "Contract Close Out"
for specific requirements on submittal of closeout information.
D. General Distribution:
1. Unless required elsewhere, provide distribution of submittals to
subcontractors, suppliers, governing authorities, and others as necessary for
proper performance of work.
1.5 ACTION ON SUBMITTALS
A. Engineer's Action:
1. General: Except for submittals for record and similar purposes, where
action and return on submittals are required or requested, Engineer will
review each submittal, mark with appropriate action, and return. Where
submittal must be held for coordination, Engineer will also advise
Contractor without delay. Engineer will review each submittal with uniform,
self-explanatory action, appropriately marked on the submittal transmittal
form.
2. Action:
a. Approved: Where submittals are marked "Approved", Work covered
by submittal may proceed provided it complies with contract
documents. Acceptance of Work will depend upon that compliance.
b. Approved Subject to Corrections Noted: When submittals are marked
"Approved Subject to Corrections Noted", Work covered by submittal
may proceed provided it complies with both Engineer's notations or
corrections on submittal and with Contract Documents. Acceptance of
Work will depend on that compliance.
c. Revise and Resubmit: When submittals are marked "Revise and
Resubmit", do not proceed with Work covered by submittal. Do not
permit Work covered by submittal to be used at Project site or
elsewhere where Work is in progress. Revise submittal or prepare
new submittal in accordance with Engineer's notations in accordance
with this section. Resubmit submittal without delay. Repeat if
necessary to obtain different action marking. Any additional time
necessary to make corrections to the submittals, or loss of materials,
equipment and time of manufacturing, or labor costs, or any other
costs of any nature as a direct consequence of the non-conformity of
the Contractor's document or non-compliance with the specifications,
DPU Standard
Submittals 01330-8 June 2019
shall not be cause for extension of contract time or increase to the
Contract cost.
d. Not Reviewed: Submittals marked “Not Reviewed” are not needed
and is being returned without being reviewed.
e. For Information Only: Submittals marked "For Information Only" do
not require further action unless noted otherwise on submittal. Such
submittals include guarantees, warranties, maintenance agreements,
workmanship bonds, and calculations by a licensed professional
engineer.
1.6 APPROVAL BY THE CONTRACTOR
A. The Contractor shall check and approve all shop drawings before transmitting
them to the Construction Manager to determine that they comply with the
requirements of the Contract Documents. Drawings which are not complete or not
in compliance with the Contract Documents shall not be submitted. All shop
drawing submittals, regardless of origin, shall be stamped with the approval of the
Contractor and identified with the Contractor's name and references to applicable
specification paragraphs and Contract Drawings. Each shop drawing submittal
shall indicate the intended use of the item in the Work. When catalog pages are
submitted, applicable items shall be clearly identified. The current revision, issue
number, and date shall be indicated on all shop drawings and other descriptive
data. The Contractor's stamp of approval shall constitute a representation to the
Owner, the Construction Manager, and the Engineer that the Contractor accepts
full responsibility for determining and verifying all quantities, dimensions, field
construction criteria, materials, catalog numbers, and similar data; that he has
reviewed or coordinated each submittal with the requirements of the Work and the
Contract Documents; and that the submittal fully meets the requirements of the
Contract Documents.
1.7 REVIEW OF SHOP DRAWINGS BY THE CONSTRUCTION MANAGER
AND ENGINEER
A. Deviations from Contract Requirements: If the shop drawings show deviations
from the Contract requirements, the Contractor shall make specific mention thereof
as previously specified in this Section. Review of such submittals shall not
constitute approval of the deviation unless the deviations are identified. Review of
the shop drawings shall constitute review of the subject matter thereof only and not
of any structure, material, equipment, or apparatus shown or indicated. Such
submittals shall, as pertinent to the deviation, indicate essential details of all
changes proposed by the Contractor (including modifications to other facilities that
may be a result of the deviation) and all required piping and wiring diagrams, all in
accordance with the General Requirements.
DPU Standard
Submittals 01330-9 June 2019
B. Completeness of Shop Drawings: The Contractor shall accept full responsibility
for the completeness of each submittal, and, in the case of a resubmittal, shall
verify that all exceptions previously noted by the Engineer have been taken into
account. Costs associated with the review by the Engineer of any third and
subsequent submittals shall be borne by the Contractor which may be deducted
from any progress payments due the Contractor by the Owner.
C. Accuracy of Drawings: The review of shop drawings will be general and shall not
relieve the Contractor of responsibility for the accuracy of such drawings, or for
the furnishing of materials or Work required by the Contract and not indicated on
the shop drawings. Approval is intended on for compliance with the information
given in the Contract Documents. The Contractor is also responsible for
information that pertains solely to the fabrication processes.
1.8 RESUBMITTALS
A. Resubmittals Within 20 Days: Resubmittals shall be made within 20 days of the
date of the Construction Manager transmittal returning the material to be modified
or corrected, unless within 7 days the Contractor submits an acceptable request for
an extension of the stipulated time period, listing the reasons the resubmittal
cannot be completed within that time.
B. Additional Resubmittals: Any need for more than one resubmittal or any other
delay in obtaining the Engineer's review of submittals will not entitle the
Contractor to an extension of time unless a delay of the Work is directly caused by
an authorized change in the Work or by the Engineer's failure to return any
submittal.
1.9 FORMS
A. An example of the Contractor Submittal Form is furnished at the end of this
section and will be provided to the Contractor in electronic format.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
DPU Standard
Submittals 01330-10 June 2019
CONTRACTOR'S SUBMITTAL TRANSMITTAL FORM
TO: SITE:
PROJECT NAME:
SPEC. REF. NO.
ATTN: PLAN REF. NO.
SYSTEM:
FROM: SUBCONTRACTOR:
SUPPLIER:
DATE:
1. The following submittals are forwarded for your review:
No. of
Repros/CopiesManufacturer Description Dwg. No. Date
/
/
/
/
/
2. Will item submitted for review fit in space
provided in the Contract Documents? ______ Yes ______ No
3. Has work indicated in this submittal been
coordinated with all trades: ______ Yes ______ No
4. Is work by all trades being provided as
necessary to accommodate this submittal? ______ Yes ______ No
5. Contractor has approved submittal and has
affixed his certification stamp? ______ Yes ______ No
6. Contractor's description and justification for deviations from Contract Documents. (Use additional
sheet, if necessary)
7. Remarks:
Signature:
END OF SECTION
DPU Standard
Limitations on Sequence of Construction 01335-1 June 2019
SECTION 01335
LIMITATIONS ON SEQUENCE OF CONSTRUCTION
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Operation of Existing Facilities
B. Limitations of Sequence of Construction
1.2 RELATED SECTIONS
A. Section 01325 - Progress Schedule
1.3 OPERATION OF EXISTING FACILITIES
A. The work shall be so conducted that the existing facilities will be maintained in full
operation at all times except for operation interruptions provided for under this section.
B. The Contractor shall keep the Construction Manager fully advised as to his plans for
carrying out the work and obtain the Construction Manager's approval for all phases of
his operations as hereinafter specified.
C. It is mutually agreed that the existing facilities shall not be shut down.
D. Any temporary structures, connections, piping, and other work necessary to maintain
service during the construction period shall be made as a part of the work.
E. All work shall be performed to avoid damage to existing structures and equipment.
Before starting work on any modifications to existing facilities, the Contractor shall
submit a schedule to the Construction Manager for approval, comprising a detailed
sequence of operations for these modifications which demonstrates that operation of
these existing facilities will be maintained. All construction shall be in accordance with
the approved schedule. At no time shall the service performed by any operating
system, pipeline, equipment or structures be interrupted from providing its intended
operation, function and service without specific prior approval of the Construction
Manager.
F. Temporary facilities and equipment shall be provided as required and directed to
maintain pipelines, equipment, systems, processes, auxiliaries, appurtenances and
structures in service. Any temporary work not required after completion of the work
shall be promptly removed.
DPU Standard
Limitations on Sequence of Construction 01335-2 June 2019
G. All costs associated with maintaining the existing facilities in operation shall be
included in the lump sum Contract Item for Structures and Equipment and no separate
payment will be made therefore.
1.4 LIMITATIONS ON SEQUENCE OF CONSTRUCTION
A. In accordance with the requirements of Section 01325, Progress Schedule, the
Contractor shall prepare and submit a comprehensive schedule of his proposed
sequence of construction for review by the Construction Manager.
B. The Contractor is cautioned that his schedule for certain areas of the work may be
affected by work included under the other Contracts. Refer to Section 01310 -
Coordination and Meetings.
C. Work on this Contract shall be coordinated with the operation of the facilities. The
Contractor shall notify the Construction Manager of the Contractor's planned
procedures for each specific alteration of existing facilities before the alteration begins.
The Contractor shall not begin any alteration until specific permission has been
granted by the Construction Manager with sufficient advance notice as not to impact
the Contractor's schedule. The making of connections to existing facilities or other
operations that interfere with the operation of the existing equipment shall be
completed as quickly as possible and with as little delay as possible.
D. Authorized Owner personnel will perform all changes to the operational functions of
the existing facilities identified as necessary to facilitate the Work of the Contractor.
E. If it is necessary for proper operation or maintenance of the facilities, the Contractor
shall reschedule his operations so that his work will not conflict with necessary
operation or maintenance of the Water Treatment Plant. Such rescheduling shall not be
cause for a time extension except as provided for in the General Conditions.
F. The Contractor shall maintain safe passage through all access roads to the existing
facilities and to all parts of the existing Water Treatment Plant. Travel routes in the
plant are at the discretion of the City and may be altered at any time.
G. The Construction Manager shall be the sole judge of when the Contractor's operations
are causing interference with the existing facilities operations, and his orders and
instructions shall be carried out without delay.
H. The Construction Manager shall be the sole judge of when the Contractor's operations
are causing interference with the existing facilities operations, and his orders and
instructions shall be carried out without delay.
PART 2 PRODUCTS (NOT USED)
PART 3 EXECUTION (NOT USED)
END OF SECTION
DPU Standard
References 01422-1 June 2019
SECTION 01422
REFERENCES
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Reference Abbreviations
B. Abbreviations
C. Reference Standards
D. Definitions
1.2 RELATED SECTIONS
A. Information provided in this section is used where applicable in individual
Specification Sections, Divisions 1 through 16.
1.3 REFERENCE ABBREVIATIONS
A. Reference to a technical society, trade association or standards setting
organization, may be made in the Specifications by abbreviations in accordance
with the following list:
AABC Associated Air Balance Council
AAMA Architectural Aluminum Manufacturers Association
AASHTO American Association of State Highway and Transportation Officials
AATCC American Association of Textile Chemists and Colorists
ACI American Concrete Institute
ADC Air Diffusion Council
AFBMA Anti-friction Bearing Manufacturers Association
AGA American Gas Association
AGMA American Gear Manufacturers Association
AHA Association of Home Appliance Manufacturers
AISC American Institute of Steel Construction
AISI American Iron and Steel Institute
AMCA Air Movement and Control Association, Inc.
ANSI American National Standards Institute
APA American Plywood Association
ARI American Refrigeration Institute
ASCE American Society of Civil Engineers
DPU Standard
References 01422-2 June 2019
ASHRAE American Society of Heating, Refrigerating and Air Conditioning
Engineers
ASME American Society of Mechanical Engineers
ASSE American Society of Sanitary Engineers
ASTM American Society for Testing and Materials
AWI Architectural Woodwork Institute
AWPA American Wood Preservers Association
AWS American Welding Society
AWWA American Water Works Association
BHMA Builders' Hardware Manufacturers Association
BIA Brick Institute of American
CABO Council of American Building Officials
CAGI Compressed Air and Gas Institute
CISPI Cast Iron Soil Pipe Institute
CMAA Crane Manufacturers Association of America
CRD U.S. Corps of Engineers Specifications
CRSI Concrete Reinforcing Steel Institute
CTI Cooling Tower Institute
DHI Door and Hardware Institute
DOH Department of Health
DOT Department of Transportation
Fed. Spec. Federal Specifications
FGMA Flat Glass Marketing Association
FM Factory Mutual
HMI Hoist Manufacturing Institute
HPMA See HPVA
HPVA Hardwood Plywood Veneer Association
ICEA Insulated Cable Engineers Association
IEEE Institute of Electrical and Electronics Engineers
IFI Industrial Fasteners Institute
MIL Military Specifications
MSS Manufacturer's Standardization Society
NAAMM National Association of Architectural Metal Manufacturers
NACM National Association of Chain Manufacturers
NBS National Bureau of Standards, See NIST
NEBB National Environmental Balancing Bureau
NEC National Electrical Code
NEMA National Electrical Manufacturers Association
NETA National Electrical Testing Association
NFPA National Fire Protection Association
NFPA National Forest Products Association
NFPA National Fluid Power Association
NIST National Institute of Standards and Technology
NLMA National Lumber Manufacturers Association
NSF National Sanitation Foundation
OSHA Occupational Safety and Health Act
PCI Prestressed Concrete Institute
DPU Standard
References 01422-3 June 2019
PDI Plumbing and Drainage Institute
SAE Society of Automotive Engineers
SCPRF Structural Clay Products Research Foundation
SMACNA Sheet Metal and Air Conditioning Contractors' National Association
SPI Society of the Plastics Industry
SSPC Steel Structures Painting Council
STI Steel Tank Institute
TCA Tile Council of American
TIMA Thermal Insulation Manufacturers' Association
UL Underwriters' Laboratories, Inc.
USBR U. S. Bureau of Reclamation
USBS U. S. Bureau of Standards, See NIST
1.4 ABBREVIATIONS
A. Abbreviations which may be used in individual Specification Sections Divisions 1
through 16 are as follows:
DPU Standard
References 01422-4 June 2019
alternating current.................................... ac
American wire gauge.......................... AWG
ampere(s) ............................................... amp
ampere-hour(s)....................................... AH
annual...................................................... ann
Ampere Interrupting
Capacity ............................................... AIC
atmosphere(s).......................................... atm
average.................................................... avg
biochemical oxygen demand ................BOD
Board Foot ........................................... FBM
brake horsepower.................................... bhp
Brinell Hardness .................................... BH
British thermal unit(s)............................. Btu
calorie (s) ................................................. cal
carbonaceous biochemical
oxygen demand............................... CBOD
Celsius (centigrade) .................................. C
Center to Center................................. C to C
centimeter(s) ........................................... cm
chemical oxygen demand .....................COD
coefficient, valve flow ............................. Cv
condensate return .....................................CR
cubic......................................................... cu
cubic centimeter(s).................................... cc
cubic feet per day..................................... cfd
cubic feet per hour ................................... cfh
cubic feet per minute ..............................cfm
cubic feet per minute,
standard conditions ............................ scfm
cubic feet per second ............................... cfs
cubic foot (feet)......................................cu ft
cubic inch(es)........................................ cu in
cubic yard(s) ........................................ cu yd
decibels .................................................... dB
decibels (A scale)....................................dBa
degree(s) ................................................. deg
dewpoint temperature ..............................dpt
diameter ................................................... dia
direct current............................................. dc
dissolved oxygen .................................... DO
dissolved solids........................................DS
dry-bulb temperature ...............................dbt
efficiency ..................................................eff
elevation ................................................... el
entering water temperature ......................ewt
entering air temperature............................eat
equivalent direct radiation ....................... edr
face area..................................................... fa
face to face.............................................f to f
Fahrenheit .................................................. F
feet per day .............................................. fpd
feet per hour............................................. fph
feet per minute........................................fpm
feet per second......................................... fps
foot (feet) ....................................................ft
foot-candle................................................. fc
foot-pound ............................................. ft-lb
foot-pounds per minute................... ft-lb/min
foot-pounds per second.................... ft-lb/sec
formazin turbidity unit(s) ......................FTU
frequency ................................................freq
fuel oil...................................................... FO
fuel oil supply........................................FOS
fuel oil return .........................................FOR
gallon(s)................................................... gal
gallons per day........................................ gpd
gallons per day per
cubic foot ...................................... gpd/cu ft
gallons per day per
square foot .................................... gpd/sq ft
gallons per hour ..................................... gph
gallons per minute ................................. gpm
gallons per second ...................................gps
gas chromatography and
mass spectrometry ..........................GC-MS
gauge .........................................................ga
grain(s).......................................................gr
gram(s)........................................................ g
grams per cubic centimeter..................gm/cc
Heat Transfer Coefficient .......................... U
height ....................................................... hgt
Hertz ........................................................ Hz
horsepower .............................................. hp
horsepower-hour...................................hp-hr
hour(s) ...................................................... hr
humidity, relative...................................... rh
DPU Standard
References 01422-5 June 2019
hydrogen ion concentration ..................... pH
inch(es) ...................................................... in
inches per second..................................... ips
inside diameter..........................................ID
Jackson turbidity unit(s) ........................ JTU
kelvin ........................................................ K
kiloamperes.............................................. kA
kilogram(s)................................................ kg
kilometer(s)..............................................km
kilovar (kilovolt-amperes
reactive) ...............................................kvar
kilovolt(s)................................................. kV
kilovolt-ampere(s)................................. kVA
kilowatt(s) ............................................... kW
kilowatt-hour(s) .................................... kWh
linear foot (feet) .................................... lin ft
liter(s)..........................................................L
megavolt-ampere(s) .............................MVA
meter(s) ......................................................m
micrograms per liter............................ ug/L
miles per hour ........................................mph
milliampere(s)........................................ mA
milligram(s) ............................................ mg
milligrams per liter ............................. mg/L
milliliter(s) ............................................. mL
millimeter(s) .......................................... mm
million gallons ....................................... MG
million gallons per day ......................... mgd
millisecond(s) ......................................... ms
millivolt(s) ............................................. mV
minute(s) ................................................ min
mixed liquor suspended
solids.................................................MLSS
nephelometric turbidity
unit ......................................................NTU
net positive suction head.....................NPSH
noise criteria.............................................. nc
noise reduction coefficient....................NRC
number ...................................................... no
ounce(s)..................................................... oz
outside air ..................................................oa
outside diameter.......................................OD
parts per billion...................................... ppb
parts per million.................................... ppm
percent .................................................... pct
phase (electrical).................................. . . ph
pound(s).................................................... lb
pounds per cubic foot ............................. pcf
pounds per cubic foot
per hour..............................................pcf/hr
pounds per day...................................lbs/day
pounds per day per
cubic foot ................................ lbs/day/cu ft
pounds per day per
square foot ...............................lbs/day/sq ft
pounds per square foot............................ psf
pounds per square foot
per hour..............................................psf/hr
pounds per square inch ............................ psi
pounds per square inch
absolute.................................................psia
pounds per square inch
gauge ....................................................psig
power factor..............................................PF
pressure drop or
difference................................................ dp
pressure, dynamic
(velocity)................................................. vp
pressure, vapor.................................... vap pr
quart(s)....................................................... qt
Rankine...................................................... R
relative humidity........................................ rh
resistance ................................................. res
return air .................................................... ra
revolution(s) ........................................... rev
revolutions per minute............................rpm
revolutions per second............................ rps
root mean squared.................................. rms
safety factor .............................................. sf
second(s)................................................. sec
shading coefficient.................................. SC
sludge density index .............................. SDI
Sound Transmission
DPU Standard
References 01422-6 June 2019
Coefficient .......................................... STC
specific gravity..................................... sp gr
specific volume................................. Sp Vol
sp ht at constant pressure ........................ Cp
square....................................................... sq
square centimeter(s).............................sq cm
square foot (feet).................................... sq ft
square inch (es) ..................................... sq in
square meter(s)..................................... sq m
square yard(s)....................................... sq yd
standard................................................... std
static pressure......................................... st pr
supply air .............................................. . . sa
suspended solids ...................................... SS
temperature .......................................... temp
temperature difference ............................ TD
temperature entering ............................... TE
temperature leaving ................................ TL
thousand Btu per hour.......................... Mbh
thousand circular mils......................... kcmil
thousand cubic feet ............................... Mcf
threshold limit value ............................ TLV
tons of refrigeration ............................... tons
torque ................................................... TRQ
total dissolved solids............................ TDS
total dynamic head............................... TDH
total kjeldahl nitrogen .......................... TKN
total oxygen demand............................ TOD
total pressure........................................... TP
total solids............................................... TS
total suspended solids ........................... TSS
total volatile solids............................... TVS
vacuum................................................... vac
viscosity ................................................. visc
volatile organic chemical ..................... VOC
volatile solids ...........................................VS
volatile suspended solids ...................... VSS
volt(s)........................................................ V
volts-ampere(s) ...................................... VA
volume .................................................... vol
watt(s) ...................................................... W
watthour(s)............................................. Wh
watt-hour demand ............................... WHD
watt-hour demand meter ..................WHDM
week(s) ................................................... wk
weight ...................................................... wt
wet-bulb................................................. WB
wet bulb temperature .......................... WBT
yard(s)....................................................... yd
year(s) ........................................................yr
DPU Standard
References 01422-7 June 2019
B. Use ASME Y1.1-1989, “Abbreviations for use on Drawings and in Text” for
abbreviations for units of measure not included herein in Paragraph 1.4.
1.5 REFERENCE STANDARDS
A. Latest Edition: Construe references to furnishing materials or testing, which
conform to the standards of a particular technical society, organization, or body, to
mean the latest standard, code, or specification of that body, adopted and published
as of the date of bidding this Contract. Standards referred to herein are made a part
of these Specifications to the extent which is indicated or intended.
B. Precedence: The duties and responsibilities of the Owner, Contractor or
Construction Manager, or any of their consultants, agents or employees are set
forth in the Contract Documents, and are not changed or altered by any provision
of any referenced standard specifications, manuals or code, whether such standard
manual or code is or is not specifically incorporated by reference in the Contract
Documents. Any duty or authority to supervise or direct the furnishing or
performance of the Work or any duty or authority, to undertake responsibility
contrary to the powers of the Construction Manager as set forth in the Contract
Documents cannot be assigned to the Construction Manager or any of the
Construction Manager's consultants, agents or employees.
1.6 DEFINITIONS
A. In these Contract Documents the words furnish, install and provide are defined as
follows:
1. Furnish (materials): to supply and deliver to the project ready for
installation and in operable condition.
2. Install (services or labor): to place in final position, complete, anchored,
connected in operable condition.
3. Provide: to furnish and install complete. Includes the supply of specified
services. When neither furnish, install or provide is stated, provide is
implied.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
References 01422-8 June 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Quality Control 01450-1 June 2019
SECTION 01450
QUALITY CONTROL
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Submittals
B. Inspection Services
C. Quality Control
D. Costs of Inspection
E. Failure to Comply with Contract
1.2 RELATED SECTIONS
A. Section 01330 - Submittals: Specific Submittal Requirements
1.3 SUBMITTALS
A. General: Provide all submittals, including the following, as specified in Section
01330 - Submittals.
B. Certificate Submittals: Furnish the Engineer authoritative evidence in the form of
Certificates of Manufacture that the materials and equipment to be used in the
Work have been manufactured and tested in conformity with the Contract
Documents. Include copies of the results of physical tests and chemical analyses,
where necessary, that have been made directly on the product or on similar
products of the manufacturer.
1.4 INSPECTION SERVICES
A. Owner's Access: At all times during the progress of the Work and until the date of
final completion, afford the Owner, Construction Manager, and Engineer every
reasonable, safe, and proper facility for inspecting the Work at the site. The
observation and inspection of any work will not relieve the Contractor of any
obligations to perform proper and satisfactory work as specified. Replace work
rejected due to faulty design, inferior, or defective materials, poor workmanship,
improper installation, excessive wear, or nonconformity with the requirements of
the Contract Documents, with satisfactory work at no additional cost to the Owner.
Replace as directed, finished or unfinished work found not to be in strict
DPU Standard
Quality Control 01450-2 June 2019
accordance with the Contract, even though such work may have been previously
approved and payment made therefor.
B. Rejection: The Owner and the Owner's Authorized Representatives have the right
to reject materials and workmanship which are defective or require correction.
Promptly remove rejected work and materials from the site.
C. Inferior Work Discoveries: Failure or neglect on the part of the Owner or the
Owner's Authorized Representatives to condemn or reject bad or inferior work or
materials does not imply an acceptance of such work or materials. Neither is it to
be construed as barring the Owner or the Owner's Authorized Representatives at
any subsequent time from recovering damages or a sum of money needed to build
anew all portions of the Work in which inferior work or improper materials were
used.
D. Removal for Examination: Should it be considered necessary or advisable by the
Owner or the Owner's Authorized Representatives, at any time before final
acceptance of the Work, to make examinations of portions of the Work already
completed, by removing or tearing out such portions, promptly furnish all
necessary facilities, labor, and material, to make such an examination. If such
Work is found to be defective in any respect, defray all expenses of such
examination and of satisfactory reconstruction. If, however, such work is found to
meet the requirements of the Contract, the cost of examination and restoration of
the Work will be considered a change in the Work and Contractor may request
compensation in accordance with applicable provisions of the Contract.
E. Operation Responsibility: Assume full responsibility for the proper operation of
equipment during tests and instruction periods. Make no claim for damage which
may occur to equipment prior to the time when the Owner accepts the Work.
F. Rejection Prior to Warrantee Expiration: If at any time prior to the expiration of
any applicable warranties or guarantees, equipment is rejected by the Owner, repay
to the Owner all sums of money received for the rejected equipment on progress
certificates or otherwise on account of the Contract lump sum prices, and upon the
receipt of the sum of money, Owner will execute and deliver a bill of sale of all its
rights, title, and interest in and to the rejected equipment. Do not remove the
equipment from the premises of the Owner until the Owner obtains from other
sources, equipment to take the place of that rejected. The Owner hereby agrees to
obtain other equipment within a reasonable time and the Contractor agrees that the
Owner may use the equipment furnished by the Contractor without rental or other
charge until the other new equipment is obtained.
1.5 QUALITY CONTROL
A. Testing
1. Field and Laboratory
DPU Standard
Quality Control 01450-3 June 2019
a. Provide personnel to assist the Construction Manager in performing
the following periodic observation and associated services.
(1) Soils: Observe and test excavations, placement and
compaction of soils. Determine suitability of excavated
material. Observe subgrade soils and foundations.
(2) Concrete: Observe forms and reinforcement; observe concrete
placement; witness air entrainment tests, facilitate concrete
cylinder preparation and assist with other tests performed by
Construction Manager.
(3) Masonry: Sample and test mortar, bricks, blocks and grout;
inspect brick and block samples and sample panels; inspect
placement of reinforcement and grouting.
b. When specified in Divisions 2 through 16 of the Contract Documents,
provide an independent laboratory testing facility to perform required
testing. Qualify the laboratory as having performed previous
satisfactory work. Prior to use, submit to the Construction Manager
for approval.
c. Cooperate with the Construction Manager and laboratory testing
representatives. Provide at least 24 hours notice prior to when
specified testing is required. Provide labor and materials, and
necessary facilities at the site as required by the Construction
Manager and the testing laboratory.
d. Provide an independent testing agency, a member of the National
Electrical Testing Association, to perform inspections and tests
specified in Division 16 of these Specifications.
2. Equipment: Coordinate and demonstrate test procedures as specified in the
Contract Documents or as otherwise required during the formal tests.
3. Pipeline and Other Testing: Conform to test procedures and requirements
specified in the appropriate Specification Section.
B. Reports
1. Certified Test Reports: Where transcripts or certified test reports are
required by the Contract Documents, meet the following requirements:
a. Before delivery of materials or equipment submit and obtain approval
of the Construction Manager for all required transcripts, certified test
DPU Standard
Quality Control 01450-4 June 2019
reports, certified copies of the reports of all tests required in
referenced specifications or specified in the Contract Documents.
b. Perform all testing in an approved independent laboratory or the
manufacturer's laboratory. Submit for approval reports of shop
equipment tests within thirty days of testing.
c. Transcripts or test reports are to be accompanied by a notarized
certificate in the form of a letter from the manufacturer or supplier
certifying that tested material or equipment meets the specified
requirements and the same type, quality, manufacture and make as
specified. The certificate shall be signed by an officer of the
manufacturer or the manufacturer's plant manager.
2. Certificate of Compliance: At the option of the Construction Manager, or
where not otherwise specified, submit for approval a notarized Certificate of
Compliance. The Certificates may be in the form of a letter stating the
following:
a. Manufacturer has performed all required tests
b. Materials to be supplied meet all test requirements
c. Tests were performed not more than one year prior to submittal of the
certificate
d. Materials and equipment subjected to the tests are of the same quality,
manufacture and make as those specified
e. Identification of the materials
1.6 COSTS OF INSPECTION
A. Owner's Obligation: Initial inspection and testing of materials furnished under this
Contract will be performed by the Owner or his authorized Representatives or
inspection bureaus without cost to the Contractor, unless otherwise expressly
specified. If subsequent testing is necessary due to failure of the initial tests or
because of rejection for noncompliance, reimburse the Owner for expenditures
incurred in making such tests.
B. Contractor's Obligation: Include in the Contract Price, the cost of all shop and
field tests of equipment and other tests specifically called for in the Contract
Documents. Contractor shall be responsible for obtaining all necessary permits and
inspections from City of Richmond Building Inspections.
C. Reimbursements to Owner:
DPU Standard
Quality Control 01450-5 June 2019
1. Materials and equipment submitted by the Contractor as the equivalent to
those specifically named in the Contract may be tested by the Owner for
compliance. Reimburse the Owner for expenditures incurred in making such
tests on materials and equipment which are rejected for noncompliance.
2. Reimburse Owner for the costs of jobsite inspection on weekends and
holidays, and between the hours of 5:00 p.m. and 8:00 a.m. on workdays
unless the weekend, holiday or after-hours work is specifically required by
the Owner to minimize operational impact or traffic disruption. Jobsite
inspection costs for weekend, holidays or after-hours work, if authorized,
solely to make up schedule slippage shall be reimbursable.
3. Reimbursement to Owner shall be by a credit Change Order to the lump sum
contract items issued at the end of the project.
1.7 FAILURE TO COMPLY WITH CONTRACT
A. Unacceptable Materials: If it is ascertained by testing or inspection that the
material or equipment does not comply with the Contract, do not deliver said
material or equipment, or if delivered remove it promptly from the site or from the
Work and replace it with acceptable material without additional cost to the Owner.
Fulfill all obligations under the terms and conditions of the Contract even though
the Owner or the Owner's Authorized Representatives fail to ascertain
noncompliance or notify the Contractor of noncompliance.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Quality Control 01450-6 June 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Construction Facilities and Temporary Controls 01500-1 June 2019
SECTION 01500
CONSTRUCTION FACILITIES AND TEMPORARY CONTROLS
PART 1 GENERAL
1.1 SECTION INCLUDES
A. References
B. General Requirements
C. Temporary Utilities
D. Temporary Construction
E. Barricades and Enclosures
F. Fences
G. Protection of Property, Utilities and Structures
H. Temporary Controls
I. Traffic Regulation
J. Field Offices and Sheds
K. Hoists and Cranes
L. WTP Site Security
1.2 REFERENCES
A. Codes and standards referred to in this section are:
1. Virginia Department of Transportation Road and Bridge Specifications
2. OSHA Regulations
1.3 GENERAL REQUIREMENTS
A. Plant and Facilities: Furnish, install, maintain and remove all false work,
scaffolding, ladders, hoistways, braces, pumping plants, shields, trestles, roadways,
sheeting, centering forms, barricades, drains, flumes, control equipment, and the
like, any of which may be needed in the construction of any part of the Work and
DPU Standard
Construction Facilities and Temporary Controls 01500-2 June 2019
which are not herein described or specified in detail. Accept responsibility for the
safety and efficiency of such works and for any damage to the Work or Owner
equipment, buildings and structures that may result from their failure or from their
improper construction, maintenance or operation.
B. First Aid: Maintain a readily accessible, completely equipped first aid kit at each
location where work is in progress.
C. Safety Responsibility: Accept sole responsibility for safety and security at the site.
Indemnify and hold harmless the Owner and the Owner's Authorized
Representatives, including the Engineer and Construction Manager, for any safety
violation, or noncompliance with governing bodies and their regulations, and for
accidents, deaths, injuries, or damage at the site during occupancy or partial
occupancy of the site by Contractor's forces while performing any part of the
Work. Provide the Construction Manager with a copy of the Contractor Safety
Plan for this project which includes all proposed Work planned.
D. Hazard Communication: Furnish two copies of the Contractor's Hazard
Communication Program required under OSHA regulations before beginning on
site activities. Furnish two copies of amendments to Hazard Communications
Program as they are prepared.
E. Confined Space: Portions of the existing facilities are considered Confined Spaces
by the Owner. These generally include but are not limited to: Storage Tanks,
Sewers, Dry Wells, Underground Vaults, Boilers, Digesters, Manholes, Tunnels,
Ventilation or Exhaust Ducts, Wet Wells, Open Top Pits, Lagoons, and Vats and
Vessels. These areas may be considered Permit Required Confined Spaces because
of the potential to contain a hazardous atmosphere, the potential of engulfment,
and because of its internal configuration. Permit Required Confined Spaces are
posted and identified with signs. Concurrent entry into any permit required
confined space by Contractor and Owner’s personnel shall be coordinated.
F. Fuel Storage: Contractor shall develop proposed procedures for refueling
equipment for review by the CM. Procedures should detail proposed fuel storage
and transport measures. Contractor shall also maintain documentation of fuel
quantities stored on site, including storage location.
G. General Requirement Costs: All costs associated with the general requirements
shall be included in the contract items and no separate payments will be made
therefore.
1.4 TEMPORARY UTILITIES
A. Water: Provide all necessary facilities and required water without additional cost
to the Owner, unless otherwise specified. If necessary, provide and lay water lines
to the place of use; secure all necessary permits; pay for all taps to water mains and
hydrants and for all water used at the established rates.
DPU Standard
Construction Facilities and Temporary Controls 01500-3 June 2019
B. Lighting: Provide without additional cost to the Owner temporary lighting
facilities required for the proper construction and inspection of the Work. If, in the
Construction Manager's opinion, these facilities are inadequate, do NOT proceed
with any portion of the Work affected thereby. Maintain temporary lighting until
the Work is accepted.
C. Electrical:
1. An existing 900A, 480V, 3-phase service (via a NEMA 3R fused disconnect
switch) is available on site for the Contractor’s use. The existing fused
disconnect switch is located adjacent to the Floodwall in the area of the
Dewatering Pad. Contractor is responsible for providing all temporary
wiring and electrical power panels needed for the Contractor’s equipment.
The Owner will provide electrical power at no cost.
2. The Contractor is responsible to obtain electrical permits (with a copy to be
submitted to the Owner and CM), and to meet all electrical code
requirements.
D. Heat: Provide temporary heat, whenever required, for work being performed
during cold weather to prevent freezing of concrete, water pipes, and other damage
to the Work or existing facilities.
E. Sanitary Facilities:
1. The Contractor shall provide and maintain sanitary facilities, preferably a
green color and hidden from neighbors, for his employees and his
subcontractors' employees that will comply with the regulations of the local
and state health departments. Service, clean, and maintain facilities and
enclosures.
2. The Contractor shall provide chemical toilets of suitable types and maintain
them in a sanitary condition at all times, conforming to code requirements
and acceptable to the health authorities. They shall be of watertight
construction so that no contamination of the area can result from their use.
Make arrangements for frequent emptying of toilets. Upon completion of the
work, remove toilets and restore area to original condition.
F. Connections to Existing Utilities:
1. Unless otherwise specified or indicated, make all necessary connections to
existing facilities including structures, drain lines, and utilities such as water,
sewer, gas, telephone, and electricity. In each case, obtain permission from
the Owner or the owning utility prior to undertaking connections. Protect
facilities against deleterious substances and damage.
DPU Standard
Construction Facilities and Temporary Controls 01500-4 June 2019
2. Thoroughly plan in advance all connections to existing facilities. Have on
hand at the time of undertaking the connections, all material, labor and
required equipment. Proceed continuously to complete connections in
minimum time. Arrange for the operation of valves or other appurtenances
on existing utilities, under the direct supervision of the owning utility.
G. Telephone Service:
1. The Contractor shall arrange and provide onsite telephone service for
Contractor's use during construction at no cost to the Owner.
2. No incoming calls allowed to Owner's telephone system.
1.5 TEMPORARY CONSTRUCTION
A. Bridges:
1. If required, design and place suitable temporary bridges where necessary for
the maintenance of vehicular and pedestrian traffic. Assume responsibility
for the sufficiency and safety of all such temporary work or bridges and for
any damage which may result from their failure or their improper
construction, maintenance, or operation. Indemnify and save harmless the
Owner and the Owner's representatives, including Engineer and
Construction Manager, from all claims, suits or actions, and damages or
costs of every description arising by reason of failure to comply with the
above provisions.
1.6 BARRICADES AND ENCLOSURES
A. Protection of Workmen and Public: Effect and maintain at all times during the
prosecution of the Work, barriers and lights necessary for the protection of
Workmen and the Public. Provide suitable barricades, lights, "danger" or "caution"
or "street closed" signs and watchmen at all places where the Work causes
obstructions to normal traffic, excavation sites, or constitutes in any way a hazard
to the public.
B. Barricades and Lights:
1. Protect all streets, roads, highways, excavations and other public
thoroughfares which are closed to traffic; use effective barricades which
display acceptable warning signs. Locate barricades at the nearest public
highway or street on each side of the blocked section.
2. Statutory Requirements: Install and maintain all barricades, signs, lights,
and other protective devices within highway rights-of-way in strict
conformity with applicable statutory requirements by the authority having
jurisdiction.
DPU Standard
Construction Facilities and Temporary Controls 01500-5 June 2019
1.7 FENCES
A. Existing Fences: Obtain written permission from the Owner prior to relocating or
dismantling fences which interfere with construction operations. Reach agreements
with the fence owner as to the period the fence may be left relocated or dismantled.
Install adequate gates where fencing must be maintained. Keep gates closed and
locked at all times when not in use.
B. Restoration: Restore all fences to their original or better condition and to their
original location on completion of the Work.
1.8 PROTECTION OF PROPERTY, UTILITIES AND STRUCTURES
A. Preservation of Property:
1. Preserve from damage, all property along the line of the Work, in the
vicinity of or in any way affected by the Work, the removal or destruction of
which is not called for by the Drawings. Preserve from damage, public
utilities, trees, lawn areas, building monuments, fences, pipe and
underground structures, existing station security system, and public streets.
Tree protection within public street right-of-ways, parks, and other City
public spaces shall be provided in accordance with the City of Richmond
Arborist requirements. Note: Normal wear and tear of streets resulting from
legitimate use by the Contractor are not considered as damage. Whenever
damages occur to such property, immediately restore to its original
condition. Costs for such repairs are incidental to the Contract.
2. In case of failure on the part of the Contractor to restore property or make
good on damage or injury, the Owner may, upon 24 hours written notice,
proceed to repair, rebuild, or otherwise restore such property as may be
deemed necessary, and the cost thereof will be deducted from any moneys
due or which may become due the Contractor under this Contract. If
removal, repair or replacement of public or private property is made
necessary by alteration of grade or alignment authorized by the Owner and
not contemplated by the Contract Documents, the Contractor will be
compensated, in accordance with the General Conditions, provided that such
property has not been damaged through fault of the Contractor or the
Contractor's employees.
3. A residential neighborhood is adjacent to the Water Treatment Plant. The
CONTRACTOR shall be required to abate any contribution to air, water, or
land pollution including such nuisances as odors, noise, surface or
groundwater contamination, or other conditions resulting from the WTR and
sediment removal and hauling operations. An 8-foot, wooden privacy fence
(submit for approval) shall be constructed around the CONTRACTOR’s
DPU Standard
Construction Facilities and Temporary Controls 01500-6 June 2019
trailer, sanitary facilities, and storage area to keep out of sight of
neighboring residents.
B. Public Utility Installations and Structures:
1. Public utility installations and structures include all poles, tracks, pipes,
wires, conduits, vaults, ductbanks, manholes, and other appurtenances and
facilities, whether owned or controlled by public bodies or privately owned
individuals, firms or corporations, used to serve the public with
transportation, gas, electricity, telephone, storm and sanitary sewers, water,
or other public or private utility services. Facilities appurtenant to public or
private property which may be affected by the Work are deemed included
hereunder.
2. The Contract Documents contain data relative to existing public utility
installations and structures above and below the ground surface. Existing
public utility installations and structures are indicated on the Drawings only
to the extent such information was made available to, or found by, the
Engineer in preparing the Drawings. These data are not guaranteed for
completeness or accuracy, and the Contractor is responsible for making
necessary investigations to become fully informed as to the character,
condition, and extent of all public utility installations and structures that may
be encountered and that may affect the construction operations.
3. Contact utility locating service sufficiently in advance of the start of
construction to avoid damage to the utilities and delays to the completion
date.
4. Remove, replace, relocate, repair, rebuild, and secure any public utility
installations and structures damaged as a direct or indirect result of the Work
under this Contract. Costs for such work are incidental to the Contract. Be
responsible and liable for any consequential damages done to or suffered by
any public utility installations or structures. Assume and accept
responsibility for any injury, damage, or loss which may result from or be
consequent to interference with, or interruption or discontinuance of, any
public utility service.
5. Repair or replace any water, electric, sewer, gas, or other service connection
or equipment damaged during the Work with no addition to the Contract
price.
6. At all times in performance of the Work, employ proven methods and
exercise reasonable care and skill to avoid unnecessary delay, injury,
damage, or destruction to public utility installations and structures. Avoid
unnecessary interference with, or interruption of, public utility services.
Cooperate fully with the owners thereof to that end.
DPU Standard
Construction Facilities and Temporary Controls 01500-7 June 2019
7. Give written notice to the owners of all public utility installations and
structures affected by proposed construction operations, sufficiently in
advance of breaking ground in any area or on any unit of the Work, to obtain
their permission before disrupting the lines and to allow them to take
measures necessary to protect their interests. Advise the Chiefs of Police,
Fire and Rescue Services of any excavation in public streets or the
temporary shut-off of any water main. Provide at least 24 hours notice to all
affected property owners whenever service connections are taken out of
service.
C. Miscellaneous Structures: Assume and accept responsibility for all injuries or
damage to culverts, building foundations and walls, retaining walls, or other
structures of any kind met with during the prosecution of the Work. Assume and
accept liability for damages to public or private property resulting therefrom.
Adequately protect against freezing all pipes carrying liquid.
D. Protection of Trees and Lawn Areas:
1. Protect with boxes, trees and shrubs, except those shown to be removed. Do
not place excavated material so as to cause injury to such trees or shrubs.
Replace trees or shrubs destroyed by accident or negligence of the
Contractor or Contractor's employees with new stock of similar size and age,
at the proper season, at no additional cost to the Owner.
2. Leave lawn areas in as good condition as before the start of the Work.
Restore areas where sod has been removed by seeding or sodding.
1.9 TEMPORARY CONTROLS
A. During Construction:
1. Keep the site of the Work and adjacent premises free from construction
materials, debris, and rubbish. Remove this material from any portion of the
site if such material, debris, or rubbish constitutes a nuisance or is
objectionable.
2. Remove from the site all surplus materials and temporary structures when
they are no longer needed.
3. Neatly stack construction materials such as concrete forms and scaffolding
when not in use. Promptly remove splattered concrete, asphalt, oil, paint,
corrosive liquids, and cleaning solutions from surfaces to prevent marring or
other damage.
4. Properly store volatile wastes in covered metal containers and remove from
the site daily.
DPU Standard
Construction Facilities and Temporary Controls 01500-8 June 2019
5. Do not bury or burn on the site or dispose of into storm drains, sanitary
sewers, streams, or waterways, any waste material. Remove all wastes from
the site and dispose of in a manner complying with applicable ordinances
and laws.
B. Smoke Prevention:
1. Strictly observe all air pollution control regulations.
2. Open fires will be allowed only if permitted under current ordinances.
C. Noise Control:
1. Provide acoustical barriers so noise emanating from tools or equipment will
not exceed legal noise levels.
2. The maximum allowable noise level at the property line of neighborhood
residences is 60 dBA for CONTRACTOR operations from 7:00 a.m. to
6:00 p.m., local time. The maximum allowable noise level at the property
line of neighborhood residences is 55 dBA for CONTRACTOR operations
from 6:00 p.m. to 7:00 a.m., local time.
3. Noise Control Plan: Propose plan to mitigate construction noise and to
comply with noise control ordinances, including method of construction,
equipment to be used, and acoustical treatments.
D. Hours of Operation:
1. Operation of construction equipment between the hours of 5:00 p.m. and
8:00 a.m. the following day is prohibited. For operation of this equipment
during this period obtain written consent from the Owner.
2. Do not carry out nonemergency work, including equipment moves, on
Saturdays, Sundays or City observed holidays without prior written
authorization by the Owner.
E. Dust Control:
1. Take measures to prevent unnecessary dust. Keep earth surfaces exposed to
dusting moist with water or a chemical dust suppressant. Cover materials in
piles or while in transit to prevent blowing or spreading dust.
2. Adequately protect buildings or operating facilities which may be affected
adversely by dust. Protect machinery, motors, instrument panels, or similar
equipment by suitable dust screens. Include proper ventilation with dust
screens.
DPU Standard
Construction Facilities and Temporary Controls 01500-9 June 2019
F. Temporary Drainage Provisions:
1. Provide for the drainage of stormwater and any water applied or discharged
on the site in performance of the Work. Provide adequate drainage facilities
to prevent damage to the Work, the site, and adjacent property.
2. Supplement existing drainage channels and conduits as necessary to carry all
increased runoff from construction operations. Construct dikes as necessary
to divert increased runoff from entering adjacent property (except in natural
channels), to protect the Owner's facilities and the Work, and to direct water
to drainage channels or conduits. Provide ponding as necessary to prevent
downstream flooding.
3. Maintain excavations free of water. Provide, operate, and maintain pumping
equipment.
G. Erosion Control: Provide erosion control in accordance with the Virginia Erosion
and Sediment Control law and regulations.
H. Pollution:
1. The CONTRACTOR’s operations shall in no way contribute to air, water, or
land pollution. This includes such nuisances as odors, insects, noise, surface
or groundwater contamination, or any other condition that would have a
detrimental effect on the environment. The CONTRACTOR’s operations
shall meet all local, state, and federal regulations for handling and
disposal/beneficial reuse of the WTR and sediment.
2. The CONTRACTOR shall minimize air pollution from operations. Burning
of waste materials, rubbish, or other debris will not be permitted on or
adjacent to the site. Give streets, roads, detours, or haul roads used in the
area a dust-preventive treatment or periodically water to prevent dust.
Strictly adhere to applicable environmental regulations for dust prevention.
3. Prevent the pollution of drains and watercourses by sanitary wastes,
sediment, debris, and other substances resulting from construction activities.
Do not permit sanitary wastes to enter any drain or watercourse other than
sanitary sewers. Do not permit sediment, debris, or other substances to enter
sanitary sewers. Take reasonable measures to prevent such materials from
entering any drain or watercourse.
I. Odors
1. The CONTRACTOR shall be responsible and take necessary precautions to
prevent nuisance odors from leaving the plant site during WTR removal
operations.
DPU Standard
Construction Facilities and Temporary Controls 01500-10 June 2019
1.10 TRAFFIC REGULATION
A. Site Access:
1. The CONTRACTOR must travel on Douglasdale Road through a residential
neighborhood in order to enter and exit the plant. The road is narrow and the
grade is steep. The existing concrete bridge to the plant at the end of
Douglasdale Road has a HS-20 live load limit. It shall be the
CONTRACTOR’s responsibility to inspect and document the condition of
the road, and plan the Work as required to accommodate the road condition.
2. Access to the Dewatering Pad is via a road that runs along the plant’s
Sedimentation Basins.
3. At no time will access be allowed through the Science Museum of Virginia
Property (except as dictated by the easement agreement), the CSXT Railroad
property (except by use of the existing railroad underpass) or any other 3rd
party landowner without express written permission from said landowner.
Cost for any additional access agreements will be at the CONTRACTOR’s
expense.
4. The CONTRACTOR shall be responsible for repairing any damage to
Douglasdale Road, the plant entrance road, the roadway along the Plant
Sedimentation Basins, the access road along the Basin, and other areas that
is caused by the CONTRACTOR’s operations at no additional cost to the
OWNER.
5. The CONTRACTOR shall comply with all traffic regulations outside of the
plant site, as well as all requirements established by the CM for on-site
traffic.
6. No construction equipment will be allowed in the James River and Kanawha
Canal at anytime.
7. It shall be the CONTRACTOR’s responsibility to determine the condition of
the site as required to accommodate the CONTRACTOR’s WTR and
sediment removal and hauling operations, as described in the General
Conditions. Any damage to the site caused by the CONTRACTOR’s
operations shall be repaired at no additional cost to the OWNER.
8. CONTRACTOR shall thoroughly wash and clean trucks carrying any
material other than the OWNER’s WTR and/or sediment prior to entering
the WTP.
B. Work-in-Street Permit: All work in City streets shall comply with the
requirements of the Work-in-Street permit obtained by the Contractor.
DPU Standard
Construction Facilities and Temporary Controls 01500-11 June 2019
C. Traffic and Speeding Requirements: Adhere to all local traffic and speeding
requirements.
1.11 MATERIAL SHEDS AND TEMPORARY STRUCTURES
A. Material Sheds and Temporary Structures: Provide material sheds and other
temporary structures of sturdy construction and neat appearance.
B. Location: Coordinate location of material sheds and temporary structures with
Construction Manager and Owner.
1.12 HOISTS AND CRANES
A. Contractor shall NOT use any hoists or cranes belonging to the Owner, for the
performance of the work, without first submitting a written request to the
Construction Manager. The request shall describe how the Contractor intends to
use the hoist or crane, the weight of the items being lifted, and how long the
Contractor intends to use the hoist or crane. If the request is approved, the
Construction Manager will provide written authorization to the Contractor.
B. Contractor’s use of hoist/crane, upon receiving written approval, shall be in
accordance with the unit’s operation and maintenance procedures and all
applicable regulations.
C. Prior to using the hoist/crane, the Contractor shall pay for an independent certified
inspection of the hoist/crane by an inspector approved by the Construction
Manager. Submit copies of the report to the Construction Manager.
D. Upon completion of the work, the Contractor shall pay for a second certified
inspection of the hoist/crane, by the approved inspector. Submit copies of the
report to the Construction Manager. The report shall be submitted prior to
substantial completion.
E. Any unusual wear or damage to the hoist/crane, its appurtenances, or any
components, found by this second inspection, shall be repaired or replaced prior to
substantial completion, to the satisfaction of the Owner and Construction Manager,
at the expense of the Contractor.
1.13 WTP SITE SECURITY
A. The Contractor shall only use the Douglasdale Road WTP access gate for this
project.
B. Contractor shall issue photo ID badges that shall be worn at all times when
Contractor and Subcontractor personnel are on site. Photo ID badges shall be 2” x
3” approximately, PVC, and include employee photo, ID number, name of
contractor, project name, and be color coded.
DPU Standard
Construction Facilities and Temporary Controls 01500-12 June 2019
C. The Contractor shall have a supervisor on the WTP site during all work periods
that will be responsible for construction personnel site security.
D. No private vehicles are allowed on the WTP site. All Contractor and Subcontractor
vehicles shall be labeled.
E. No Contractor or Subcontractor personnel are allowed in other areas of WTP site
apart from the project work area. Contractor or Subcontractor personnel discovered
in other areas of the WTP site without prior authorization by the City shall be
removed from the project and shall not be allowed access to the WTP site.
F. The Contractor shall provide the Construction Manager with a list of employees,
subcontractors, and subcontractor employees who will be accessing the WTP for
the project for approval by the Construction Manager. Only personnel approved by
the Construction Manager shall be allowed on the plant site. The list shall be
updated monthly or as needed.
G. Notify the Construction Manager of material deliveries to the WTP site including a
description of material to be delivered, date and time, and delivery company.
H. Notify the Construction Manager or Owner if any suspicious activity is noted
around or near the WTP site.
I. The employee ID badges will be checked by the plant security guard periodically
and the name on the badge shall match the name on the employee list.
J. The CONTRACTOR will be required to provide a lock on the chain link gates in
the Floodwall. The CONTRACTOR lock shall not prevent OWNER employees
from using OWNER gate locks. The gates shall be locked during non-working
hours.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Cleaning 01740-1 June 2019
SECTION 01740
CLEANING
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Final Cleaning
B. Final Inspection
1.2 FINAL CLEANING
A. Requirements: At the completion of work and immediately prior to final
inspection, clean the entire project as follows:
1. Leave the structures and site in a complete and finished condition to the
satisfaction of the Construction Manager.
2. Remove all temporary structures and all debris, including dirt, sand, gravel,
rubbish and waste material.
3. Should the Contractor not remove rubbish or debris or not clean the
buildings and site as specified above, the Owner reserves the right to have
the cleaning done at the expense of the Contractor.
B. Employ experienced workers, or professional cleaners, for final cleaning.
C. Repair, patch, and touch up marred surfaces to specified finish, to match adjacent
surfaces.
D. Handle materials in a controlled manner with as few handlings as possible. Do not
drop or throw materials from heights.
E. Schedule cleaning operations so that dust and other contaminants resulting from
cleaning process will not fall on wet, newly-painted surfaces.
F. Broom clean exterior paved surfaces; rake clean other surfaces of the grounds.
G. Remove erection plant, tools, temporary structures and other materials.
H. Remove and dispose of all water, dirt, rubbish or any other foreign substances.
DPU Standard
Cleaning 01740-2 June 2019
1.3 FINAL INSPECTION
A. After cleaning is complete the final inspection may be scheduled. The inspection
will be done with the Owner and Construction Manager.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Contract Close Out 01789-1 June 2019
SECTION 01789
CONTRACT CLOSE OUT
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Submittals
B. Record Drawings
C. Warranties and Bonds
D. Substantial Completion
E. Final Cleaning
F. Final Inspection
G. Certificate of Final Completion.
1.2 RELATED SECTIONS
A. Section 01450 - Quality Control
1.3 SUBMITTALS
A. Contractor shall submit to the CM a CD with photographs, video, and other
records documenting the condition of the Lagoon and existing roads (plant roads
and Douglasdale Road), and other structures in the vicinity of the Work, as
applicable, which might be damaged by Contractor operations. This shall include
aerial photographs of the Lagoon before and after the project.
B. Contractor shall provide a written Statement that all requirements of the contract
have been met while complying with all federal, state and local regulations.
C. Project Record Documents: Project record documents required by this Section
shall be submitted prior to beginning the Substantial Completion Inspection.
D. Prior to Final Inspection:
1. Provide submittals to the Owner that are required by governing or other
authorities.
DPU Standard
Contract Close Out 01789-2 June 2019
2. Submit Bonds, Warranties, Guarantees and similar documents.
3. Submit evidence of compliance with requirement of governing authorities.
E. Upon receipt of the Certificate of Final Completion submit Final Application for
Payment identifying total adjusted Contract Sum, previous payments, and sum
remaining due.
F. Submit to the Owner, with the Final Application for Payment, a sworn affidavit
that all labor, service, materials, and Subcontractors have been paid and that there
are no suits pending in connection with the Work done or labor and materials
furnished under the Contract.
1.4 RECORD DRAWINGS
A. At the site keep and maintain one record copy of the following Contract
Documents, reference documents and all technical documents.
1. Drawings.
2. Specifications.
3. Addenda.
4. Change Orders and other modifications to the Contract.
5. Reviewed Shop Drawings, Product Data, and Samples.
6. Manufacturer's instructions for assembly, installation, and adjusting.
B. Using drafting symbols and standards consistent with the original documents,
annotate Contract Drawings neatly and clearly in color to show all changes made
during the construction period.
C. Store record documents separate from documents used for construction.
D. On Record Drawings, legibly mark each item to record actual construction,
including:
1. Measure horizontal location of building, concrete pads, fencing and other
project facilities. Locations shall be referenced to Virginia State Plane
Coordinate System.
2. Field changes of dimensions and details.
3. Details not on original drawings.
4. Any other variations between the work actually provided and that shown on
the Contract Drawings.
5. Change Order Work.
DPU Standard
Contract Close Out 01789-3 June 2019
E. Annotated drawings are to be made available to Construction Manager for
reference at all times. Provide annotated drawings to be reviewed monthly at the
time of payment application. Contractor partial payments will be withheld if this
data is not provided within four weeks of the new work being placed into service
to perform its design functions. Copies so provided will be retained by the
Construction Manager. Should the annotated drawings be found not current with
the work, an additional retainage of one percent of the total application amount
will be deducted from the monthly payment. Such additional retainage will be
released in future payments if the drawings are brought current.
F. At completion of the Contract and before final payment is made, deliver to the
Construction Manager one set of clearly readable, reproducible Contract Drawings
reflecting all changes made during construction. Mark each drawing "Record
Drawing" in ink. Include copies of the Record Drawings in the Operation and
Maintenance Manuals. Also provide a complete set of the field measured pipeline,
fitting and valve location drawings and as-built site survey drawings.
1.5 WARRANTIES AND BONDS
A. Prior to Final Inspection deliver to the Owner the original and one copy of all
bonds, warranties, guarantees and similar documents, including those customarily
provided by manufacturers and suppliers which cover a period greater than one
year. Show Owner as beneficiary of these documents. Begin warranty periods from
the Date of Substantial Completion or the Date of Final Completion when
Substantial Completion is not required by the Owner.
1.6 SUBSTANTIAL COMPLETION
A. The Work will be considered substantially complete when 8,000 dry tons of Water
Treatment Residuals are removed from the Lagoon in accordance with the
Contract Documents. When the Work is sufficiently completed, the Contractor
shall, in writing to the Owner and Construction Manager, certify that the entire
work is substantially complete and request that the Construction Manager issue a
Certificate of Substantial Completion. Within a reasonable time thereafter, the
Owner, the Contractor and Construction Manager shall make an inspection of the
work to determine the status of completion. If the Construction Manager does not
consider the work substantially complete, the Construction Manager will notify the
Contractor in writing giving his reasons therefor. If the Construction Manager
considers the work substantially complete, the Construction Manager will prepare
and deliver to the Owner a Certificate of Substantial Completion which shall fix
the date of Substantial Completion. The certificate shall include the project
equipment and any special warranty periods that apply to the project work. There
shall be attached to the certificate a list of tentative items to be completed or
corrected before final payment. This list shall be identified as the PUNCH LIST
OF OPEN ITEMS and may be added to at the Owner's discretion for work not
completed in conformance with the Contract Documents. This tentative PUNCH
LIST OF OPEN ITEMS shall be cost loaded as determined by the Owner based on
DPU Standard
Contract Close Out 01789-4 June 2019
the estimated value of work involved to complete the associated items. This
retained value shall be reduced monthly as a basis for payment to the Contractor
based on the difference between outstanding retained value during the invoice
period and the value of the PUNCH LIST OF OPEN ITEMS provided record
drawings have been received in accordance with the General Conditions of the
Contract. No payment made therefor shall be less than one thousand dollars
($1,000.00) except for final payment. When it has been determined by the Owner
that all items identified in the PUNCH LIST OF OPEN ITEMS are complete in
accordance with the Contract Documents, final payment shall be made.
B. Inspection
1. General: The work shall be subjected to continuous inspection and in
addition to the formal Substantial Completion inspections for each Phase of
the work requiring Substantial Completion. Each inspection shall be
performed by the Contractor in the presence of the Construction Manager.
The inspection shall be conducted in accordance with the requirement of
Section 01450 - Quality Control and field testing check lists completed for
all equipment and systems provided. All required labor, materials,
equipment, instruments, lubricants and incidentals necessary to perform
these inspections shall be furnished by the Contractor. Before proceeding to
the next inspection, all discrepancies and deficiencies observed during each
inspection shall be noted and corrected and, if directed by the Construction
Manager, the inspection shall be rescheduled and repeated at no additional
cost to the Owner.
a. Notification: When the Contractor considers the Work ready for each
inspection, the Contractor shall so notify the Construction Manager in
writing for each inspection. Each inspection shall be performed by the
Construction Manager within 10 days after receipt of the request.
2. Substantial Completion Inspection:
a. Perform a SUBSTANTIAL COMPLETION INSPECTION to fully
demonstrate to the Construction Manager that all major site work has
been brought to final configurations and restoration initiated.
b. The Construction Manager will prepare a LIST OF DEFICIENT
ITEMS to be accomplished prior to performing the Final Inspection.
1.7 FINAL CLEANING
A. Removal of Contractor's Materials: At the conclusion of the Work, promptly take
away all erection plant, tools, temporary structures and materials belonging to the
Contractor. Remove and promptly dispose of all water, dirt, rubbish or any other
foreign substances.
DPU Standard
Contract Close Out 01789-5 June 2019
B. Cleaning Materials and Equipment: Thoroughly clean all materials installed and
clean all existing structures, materials or equipment soiled during construction and
deliver over such materials and equipment undamaged in a bright, clean and
polished condition.
1.8 FINAL INSPECTION
A. When the Contractor considers the entire work complete in accordance with the
Contract Documents, the Contractor shall, in writing to the Owner and
Construction Manager, certify that the entire work is complete and request that the
Construction Manager issue a Certificate of Final Completion for all work
included in the Contract Documents. Within ten calendar days thereafter, the
Owner, the Contractor and Construction Manager shall make a FINAL
INSPECTION of the work to determine the status of completion. If the
Construction Manager considers the work complete, the Construction Manager
will prepare and deliver to the Owner a Certificate of Final Completion which shall
fix the Date of Final Completion for all work identified in the Contract
Documents.
B. If the Construction Manager does not consider the work complete, the
Construction Manager will issue to the Contractor a LIST OF DEFICIENT ITEMS
to be completed in accordance with the Contract Documents to achieve Final
Completion. This list identified as the LIST OF DEFICIENT ITEMS may be
added to at the Owner's discretion for work not completed in conformance with the
contract documents and shall include all incomplete work items previously
identified in the LIST OF DEFICIENT ITEMS issued with the Certificate of
Substantial Completion for the entire work.
C. The LIST OF DEFICIENT ITEMS shall be cost loaded as determined by the
Owner based on the estimated value of work involved to complete the associated
items. This retained value shall be reduced monthly as a basis for payment to the
Contractor based on the difference between the outstanding retained value during
the invoice period and the value of the LIST OF DEFICIENT ITEMS provided
record drawing have been received in accordance with the General Conditions of
the Contract. No payment made therefor shall be less than one thousand dollars
($1,000.00) except for final payment. When the Contractor verifies to the Owner's
and Construction Manager's satisfaction that all items identified in the LIST OF
DEFICIENT ITEMS have been corrected in accordance with the Contract
Documents final payment shall be made. This inspection shall demonstrate that all
elements of the project are ready to be placed in operation and all work has been
completed in accordance with the Contract Documents.
1.9 CERTIFICATE OF FINAL COMPLETION
A. The Work will be deemed complete as of the date set by the Contractor if, upon
Final Inspection, the Construction Manager determines that no further work,
physical or otherwise, is required to complete the Work in accordance with the
DPU Standard
Contract Close Out 01789-6 June 2019
Contract Documents. Upon determination that all Work is completed, the
Construction Manager will issue a Certificate of Final Completion. This Certificate
of Final Completion shall serve as Contractor’s authorization to generate a
requisition for final payment. The Certificate of Final Completion shall include the
project, equipment and any special warranty periods.
B. However, if such inspection, in the opinion of the Construction Manager, reveals
items of Work still to be performed, the Contractor shall promptly perform them
and then request a reinspection. In the event the Construction Manager then
determines that the Work is complete, the date of final completion shall be deemed
to be the last day of such reinspection.
C. The Owner may at its sole discretion issue a Certificate of Final Completion for
signature by the Owner, Construction Manager and Contractor; following the
expiration of the time fixed for completion in the Contract or the time for
completion as modified through a change order to the contract even though such
items of work as identified in the LIST OF DEFICIENT ITEMS are not complete
in accordance with the Contract Documents. Any items identified on the LIST OF
DEFICIENT ITEMS which have not been completed in accordance with the
contract documents within the time fixed for completion in the Contract or the time
for completion as modified through a change order to the contract shall be
identified on the Certificate of Final Completion as incomplete and shall be
credited to the Owner based solely on the Owner's determination of the cost of
such items; and, an adjustment to the total contract value shall be made via a
change order to the contract at the Owner's discretion.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
3.1 CONTRACT CLOSE OUT CHECK LIST
A. Table 01789-1 is a contract close out check list that will be used to coordinate
contract close out activities.
END OF SECTION
DPU Standard
Contract Close Out 01789-7 June 2019
Table 01789-1
PROJECT CLOSE OUT CHECK LIST
Item RequirementDate
to CM
Date
Approved
Date
Completed
Date Provided
to City
Coded
Notes
1. Completed Permits
2. Tapes, Pictures and Videos
3. Substantial Completion
4. Preliminary Punch List
5. Final Punch List
6. Contractor Notice of Completion
7. Final Inspection
8. Final Completion
9. Record Drawings
10. Final MBE-3 Form
11. Final Payment Request for Close Out
12. Project Close Out Recommendation (CM)
13. Project Close Out Recommendation (Engineer)
14. Miscellaneous Close Out Support Information
15. Release of Claims from Contractor
16. Final Affidavit of Payment of Claims
17. Final Affidavit of Release of Liens
18. Contractor Performance Evaluation
19. Close Out Letter to City Procurement Services
20. Contract Close Out Notice
DPU Standard
Contract Close Out 01789-8 June 2019
(NO TEXT FOR THIS PAGE)
DPU Standard
Special Project Provisions 01900-1 June 2019
SECTION 01900
SPECIAL PROJECT PROVISIONS
PART 1 GENERAL
1.1 SECTION INCLUDES
A. Subcontracts and Assignments
B. Contractor's Employees
C. Clarification Requests
D. Area of Operations
E. Work Adjacent to Existing Facilities
F. Existing Facilities Shown on Contract Drawings
G. Relocation of Existing Facilities
H. Photographs or Video Recording
I. Fire Protection
1.2 RELATED SECTIONS
A. Section 01325 - Progress Schedule
B. Section 01330 - Submittals
C. Section 01789 - Contract Close Out
1.3 SUBCONTRACTS AND ASSIGNMENTS
A. If the Owner finds that the proposed subcontractor is qualified, the Contractor will
be notified in writing. The Owner may revoke approval of any subcontractor when
such subcontractor evidences an unwillingness or inability to perform his work in
strict accordance with these Contract Documents. Notice of such revocation of
approval will be given in writing to the Contractor.
B. The Contractor shall promptly, upon request, file with the Owner a conformed copy
of the subcontract. The Contractor shall cause appropriate provisions to be inserted
in all subcontracts relative to the work to bind subcontractors to the Contractor by
the terms of these Contract Documents, insofar as applicable to the work of
subcontractors, and to give the Contractor the same power as regards terminating
any subcontract that the Owner may exercise over the Contractor under provisions
of these Contract Documents.
C. Each subcontract and each lower tier subcontract shall include appropriate
provisions to bind all subcontracting tiers to the requirements of this Contract.
D. No assignment will receive approval unless the instrument of assignment contains a
clause to the effect that it is agreed that the funds to be paid the assignee under the
DPU Standard
Special Project Provisions 01900-2 June 2019
assignment are subject to a prior lien for services rendered or materials supplied for
the performance of the work called for in the Contract in favor of all persons, firms,
or corporations rendering such services or supplying such materials.
1.4 CONTRACTOR'S EMPLOYEES
A. Character and Competency: The Contractor and his subcontractors shall employ
upon all parts of the work herein contracted for only competent, skillful, and
trustworthy employees. Should the Owner at any time give notice, in writing, to the
Contractor or his duly authorized representative on the work that any employee in
his opinion is incompetent, disorderly, careless, unobservant of instructions, or in
any way a detriment to the satisfactory progress of the work, such employee shall
immediately be dismissed and not again allowed upon the "Site".
1.5 CLARIFICATION REQUESTS
A. During the work the Contractor may request clarification of the information
presented of the Contract Documents. Such requests for information shall be in
writing on a Clarification Request Form. The final format for the Clarification
Request Form will be provided to the Contractor at the preconstruction meeting.
1.6 AREA OF OPERATIONS
A. The Contractor shall limit his operations generally to the area around the facilities
included in the Contract.
B. Access or work required in other areas of the site shall be arranged and coordinated
with the Construction Manager.
1.7 WORK ADJACENT TO EXISTING FACILITIES
A. All existing facilities, construction or adjacent property shall be adequately
protected, to the satisfaction of the Engineer, during all work under the Contract.
Such facilities include but are not limited to structure, building, utilities, process
pipelines, plant yard piping, storm and sanitary sewerage, excavations, ditches, tress,
conduits and electrical systems, any existing facilities and any appurtenances
thereto.
B. Any existing facilities, construction or adjacent property which are damaged,
disturbed, destroyed or otherwise, in the opinion of the Construction Manager, have
their usefulness or operation impaired by work under this Contract shall be replaced
by new and equal items or restored, all to the satisfaction of the Construction
Manager, by the Contractor at his own expense and no separate payment will be
made therefor.
DPU Standard
Special Project Provisions 01900-3 June 2019
1.8 EXISTING FACILITIES SHOWN ON CONTRACT DRAWINGS
A. The Contract Drawings are considered to be substantially complete and accurate
with respect to the types and locations of existing facilities, but are not guaranteed
to be absolutely so.
B. It is the Contractor's responsibility to make his own investigations to fully inform
himself of the location, character, condition and extent of all existing facilities as
may be encountered and as may affect the construction operations.
1.9 RELOCATION OF EXISTING FACILITIES
A. The work shall include all labor, materials, equipment and all work necessary to
relocate any existing facilities (including lights, ductwork, electrical conduit and
wiring, small piping and the like), whether shown or not, that interfere with the
proper installation of the new and relocated piping and equipment as required.
1.10 PHOTOGRAPHS OR VIDEO RECORDING
A. Examination: After Effective Date of the Agreement and before Work at site is
started, Contractor, CM, and Owner shall make thorough examination of pre-
existing conditions including existing roads (plant roads and Douglasdale Road),
structures, and other improvements in vicinity of Work, as applicable, which might
be damaged by Contractor operations. Periodic reexamination shall be jointly
performed, but not less than once per year of the contract term.
B. Documentation: Contractor shall submit two copies of photographs, video, and
other records documenting examination to the CM. The CM will review, sign, and
return one record copy of every observation document to Contractor to be kept on
file in Contractor's field office as site records. These observation documents are
intended for use as indisputable evidence in ascertaining whether and to what extent
damage occurred as a result of Contractor's operations, and are for protection of
adjacent property owners, Contractor, and Owner. Contractor shall also provide this
documentation each time a crane is employed.
C. From time to time during progress of the work, photographs or video record of the
work will be taken by the Construction Manager, the Owner or their authorized
representatives at no expense to the Contractor. The Contractor shall, however,
furnish access to the work at all times for this purpose and shall furnish such
assistance as may be required.
D. The photographs or video recording thus taken shall be the property of the Owner.
Nothing herein outlined shall be construed as prohibiting the taking of photographs
or videotapes by the Contractor or his agents provided it is done at no expense to the
Owner.
DPU Standard
Special Project Provisions 01900-4 June 2019
E. Aerial photographs shall be taken before Work at site is started, six months after
start of work and after date of Substantial Completion. A minimum of seven (7) still
views: an overall still taken directly above encompassing the entire Residuals
Lagoon area and several stills (6) taken at the four corners and one at each of the
two midpoints to adequately document the entire site. Obtain and transfer copyright
usage rights from photographer to Owner for unlimited reproduction of
photographic documentation. Provide images in JPG format, produced by a digital
camera with minimum sensor size of 12 megapixels, and at an image resolution of
not less than 4,000 by 3,000 pixels or better.
1.11 FIRE PROTECTION
A. The Contractor shall furnish and maintain on site adequate firefighting equipment
capable of extinguishing incipient fires. The Contractor shall comply with applicable
parts of the National Fire Prevention Standard for Safeguarding Building
Construction Operations (NFPA No. 241).
1.12 FLOOD EVENT
A. The 100-year flood level is approximately at elevation 108.5-ft. The Contractor shall
relocate equipment at no expense to the Owner in case of a flood event. Flood-
damaged material or equipment shall be replaced at the Contractor’s cost and Owner
shall be reimbursed for any damage to City property caused by the Contractor’s
personnel, material, or equipment.
PART 2 PRODUCTS
Not Used
PART 3 EXECUTION
Not Used
END OF SECTION
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-1 June 2019
SECTION 02000
REMOVAL AND DISPOSAL OF WATER TREATMENT RESIDUALS
PART 1 GENERAL
1.1 SUMMARY
A. The Contractor shall provide all labor, materials, and equipment, including but not
limited to services necessary for or incidental to the removal, dewatering, hauling and
disposal of water treatment residuals (WTR) from the Residuals Lagoon.
B. The method of sediment removal shall be by use of a hydraulic dredge. The anticipated
total amount of WTR to be removed from the Lagoon is 8,000 dry tons. The
approximate maximum depth of the Lagoon is 15 feet. Field conditions will determine
the actual quantities and locations to be removed, as directed by the CM. The
Contractor shall have no claim against the Owner if the actual amount of WTR and
sediment removed differs from the anticipated amount.
C. The Work includes hauling and disposing of the WTR and sediment to an approved
disposal or beneficial reuse site(s) in accordance with all local, state, and federal
requirements. It is the Contractor’s responsibility to locate a suitable site(s) and to
dewater the WTR and sediment as necessary for the selected site(s). The Contractor is
responsible for obtaining and paying all charges and fees for any permits, easements,
or agreeme4
D. The Contractor shall provide all equipment and temporary piping required for WTR
removal and dewatering. All costs for piping and booster pumping, if required, shall
be included in the unit prices listed in the Bid Form. The Contractor shall not use any
Owner equipment or facilities.
E. The Contractor shall provide all temporary piping and pumping required to return the
filtrate or concentrate to the Lagoon. The Contractor shall not discharge filtrate or
concentrate to the sanitary sewer system, Pre-Sedimentation Basin, Kanawha Canal, or
James River.
F. It shall be the Contractor’s responsibility to determine the condition of the site as
required to accommodate the Contractor’s WTR and sediment removal and hauling
operations. Any damage to the site caused by the Contractor’s operations shall be
repaired at no additional cost to the Owner.
G. Maintain four spill containment booms at locations and of approximate lengths as
summarized below and shown on the Drawings.
1. Containment Boom #1: Pre-Sedimentation Basin, 600 foot length.
2. Containment Boom #2: North Raw Water Intake Basin, 150 foot length.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-2 June 2019
3. Containment Boom #3: South Raw Water Intake Basin, 100 foot length.
4. Containment Boom # 4: Lagoon Decant/Overflow Structure, 140 foot length.
1.2 SUBMITTALS
A. The Contractor shall submit a detailed Work Plan showing the layout of the dredging
and dewatering operation. Plan shall show:
1. Location of all equipment throughout the duration of the operation.
2. The location of all piping used for dredging, dewatering, and return of filtrate
to the Lagoon.
3. Storage location for all materials.
4. Access routes, truck turn around, and truck staging points.
5. A narrative detailing dredge placement into and removal from the Lagoon,
including movement of all equipment through the plant to the worksite.
Contractor shall satisfy himself that there is adequate room to maneuver
equipment and materials through the plant to the worksite and adjust his plan
accordingly prior to submission.
6. Plan shall be submitted to the CM for approval prior to mobilizing any
materials or equipment. Any changes to the Work Plan shall be submitted in
advance to the CM for approval.
B. Prior to commencing Work on the site, the Contractor shall submit:
1. The Contractor shall provide the CM a listing of the areas where the WTR is to
be disposed/reused in accordance with all local, state, and federal requirements.
a. If the Contractor plans to dispose of WTR in a municipal or private
landfill, the Contractor shall submit documentation that the landfill meets
the requirements of the Resource Conservation and Recovery Act
(RCRA) and applicable state regulations.
b. If the Contractor plans to beneficially reuse WTR, the Contractor shall
submit documentation certifying compliance with all federal, state, and
local guidelines or requirements.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-3 June 2019
2. The Contractor shall submit confirmation that the roads and bridges on the
specified hauling route are designed for the loaded truck weights. Routes to
each disposal site and estimated round trip duration shall be provided.
3. Overall schedule covering all Work to be performed. The overall schedule shall
indicate the sequence of Work and the time of starting and completion of each
part. It shall include, but not be limited to, the following items:
a. Material and equipment delivery and setup.
b. Operational testing for WTR dewatering to determine filtrate quality and
quantity.
c. WTR removal, dewatering, and hauling.
d. Final cleaning.
4. Spill Containment Contingency Plan, including identification of all materials
and equipment required to be maintained on site in case of a spill event.
5. Plan to abate nuisance noise, lights, and odors resulting from the site activities.
6. Safety Plan.
7. Fuel Storage and Equipment Refueling Plan and Procedures.
8. Hazard communication information including product information on polymer
and other chemicals to be used. Include material safety data sheets and NSF
certification.
9. Permits required for hauling and disposal of WTR and sediment.
1.3 SPECIAL REQUIREMENTS
A. The Contractor shall not add any material to the WTR for the purpose of increasing
solids content. Such material includes, but is not limited to, fly ash, sawdust, and lime.
This requirement shall not apply to substances used solely for the purpose of
dewatering conditioners.
B. The Contractor shall route all sediment pipes and hoses or provide containment
protection such that a rupture will not cause sediments to spill into the Kanawha Canal
or the James River.
C. The Contractor shall provide special protective measures for utilities in load limited
areas (if applicable). This shall include, but not be limited to, the Raw Water Access
Bridge at the Kanawha Canal intake.
D. For the control of fuels, oils, and fluids that may be used by dredge or other equipment,
the Contractor shall maintain on-site a spill control kit and all materials necessary to
clean up and remove fuel, oil, or fluid spills.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-4 June 2019
1.4 MATERIALS TO BE REMOVED
A. The Owner recently collected samples and performed analyses of the WTR in the
Residuals Lagoon. See results on Supplement B of the Technical Specifications.
B. The WTR in the Lagoon are a byproduct of the sedimentation and filtration treatment
processes of water from the James River to produce potable water. Most of the
sediments are produced through using aluminum sulfate. WTR have accumulated in
the Lagoon over the last five (5) years. Supplement C, Summary Sheet of Lagoon
Residuals Removal since 2004, includes the dewatered residuals average percent Total
Solids and average residuals removed per truck.
C. The Contractor shall satisfy himself to the existing condition of the materials to be
removed. If a Bidder wishes to take additional WTR samples he shall submit a completed
Right of Entry and Indemnification Agreement, Contractor Safety Plan and their method of
collecting samples to the City for authorization. Bidders must submit the completed
information as described in the IFB Statement of Work.
1.5 LIMITS OF WORK AREA FOR SEDIMENTS REMOVAL
A. Limits of the work area for sediment removal are shown on the Drawings and will be
strictly enforced to protect utilities, structures, etc.
B. The Contractor shall submit a written request for any deviation from the work area shown
and receive written approval of the CM prior to proceeding with work in any revised
work areas.
C. Sediments removed by hydraulic dredging shall be processed, dewatered, and loaded into
transport vehicles within the Dewatering Pad Area.
1.6 DISPOSAL SITES AND PERMITS
A. The Contractor shall obtain all appropriate permits to excavate, dredge, dewater,
transport, and dispose of WTR. Permits include but may not be limited to: VPDES and
Disposal Permit/Agreement if required for disposal site.
B. All expenses in obtaining the site(s), obtaining necessary permits from local, State, and
Federal jurisdictions, preparing the site(s), and protecting the environment, before,
during, and after the operation shall be borne by the Contractor.
C. Off-site temporary storage of the WTR shall be acceptable, if is in accordance with all
local, state, and federal requirements. Approved submittal is required for offsite
temporary storage of WTR. All temporary stored WTR shall be finally hauled to the
permitted permanent disposal site. All costs for temporary storage and transportation
of WTR’s shall be at Contractor’s expense.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-5 June 2019
1.7 SPILL CONTAINMENT CONTINGENCY PLAN
A. The Contractor shall take precautions to prevent spillage of oil, fuel, chemicals, and
WTR into the James River, Kanawha Canal, Basin, and Lagoon during removal and
dewatering operations, as well as, into residential neighborhoods and other areas
during hauling operations to the disposal site(s).
1. The Contractor shall use food grade oil for all equipment operating within the
Lagoon, Basin, and Channel.
2. The Contractor shall be responsible for any spills that occur as a result of his
WTR or sediment removal and hauling operations. A Spill Containment
Contingency Plan shall be developed, and shall include response procedures
for potential oil, fuel, chemical, and WTR spills. Contractor shall maintain
on-site at all times a sufficient quantity of oil absorbers and other appropriate
response materials as may be required to mitigate the full magnitude of spills
that could occur. All spills shall be immediately addressed at the time the
incident occurs.
3. Notify CM and Owner immediately upon occurrence and remove spilled
substance(s) immediately and complete cleanup work the same day that the
spill occurs. Cleanup of spilled substance(s) left unresolved for more than
24 hours or considered a public nuisance may be performed or contracted by
the Owner on an emergency basis and the cost will be withheld from the
Contractor’s payment. This in no way will relieve the Contractor of
responsibility for the spill or subsequent results of the spill.
4. The Contractor shall properly document all spill events and mitigation actions
taken. Cleanup procedures and documentation thereof shall comply with all
applicable federal and state requirements.
5. The Contractor is responsible to compensate the Owner for any additional
expenses that the Owner incurs as a result from remediating a spill event.
1.8 SAFETY
A. The Contractor shall initiate, maintain, and supervise all safety precautions and
programs in connection with the Work. The Contractor shall take all necessary
precautions for the safety of, and provide the necessary protection to prevent damage,
injury, or loss to:
1. All persons on the Work site or who may be affected by the Work.
2. All the Work and materials and equipment to be incorporated therein, whether
in storage on or off the site.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-6 June 2019
3. Other property at the site or adjacent thereto, including trees, shrubs, lawns,
walks, pavements, roadways, structures, utilities and Underground Facilities not
designated for removal, relocation or replacement in the course of the Work.
4. Contractor shall meet all safety requirements for working over and around water.
B. Safety Plan:
1. Before any Work at the site is started, the Contractor shall prepare a written plan
for Project-specific safety precautions and programs, complete with respect to
procedures and actions that the Contractor intends Contractor and all others to
follow in order for Contractor and all others to comply with all applicable Laws
and Regulations, as well as specific site requirements.
2. The Contractor shall make available the following items for review: OSHA-
200 Log for the past five years, current safety program, training program, and
experience with other related processes. Documented evidence showing
compliance with lockout/tagout, emergency response, and safe work practices
are required. The Contractor must comply with the applicable safe work
practices and controls outlined in Supplement D: Construction Site Safety Plan
for Contractors Working on or near Hazardous Conditions at the Water
Purification Plant.
3. The Contractor shall revise plan for safety precautions and programs at
appropriate times to reflect changes in construction conditions, the Work, means,
methods, techniques, sequences and procedures of construction.
C. Safety Representative: The Contractor shall designate a qualified and experienced
safety representative at the site whose duties and responsibilities shall be the prevention
of accidents and the maintaining and supervising of safety precautions and programs.
D. Hazard Communication Programs: The Contractor shall be responsible for
coordinating any exchange of material safety data sheets or other hazard
communication information required to be made available to or exchanged between
or among employers at the site in accordance with Laws or Regulations.
E. Wildlife: Species of wildlife are present in the area of the project site and may be
encountered by the Contractor during the course of the Work. Contractor shall be
solely responsible for ensuring the safety of its personnel, and shall comply with
applicable federal and state laws, when dealing with potentially dangerous species.
The OWNER shall not be responsible for any delays or costs resulting from wildlife
present at the project site.
F. Emergencies: In emergencies affecting the safety or protection of persons or the Work
or property at the site or adjacent thereto, Contractor, without special instruction or
authorization from OWNER or CM, is obligated to act to prevent threatened damage,
injury or loss. Contractor shall give CM prompt written notice if Contractor believes
that any significant changes in the Work or variations from the Contract Documents
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-7 June 2019
have been caused thereby. If the CM determines that a change in the Contract
Documents is required because of the action taken by Contractor in response to such an
emergency, a Change Order will be issued to document the consequences of such action.
G. The CONTRACTOR shall keep CM informed of accidents on and off the site and
related claims in a timely manner. A written accident report shall be submitted with 72
hours.
PART 2 – PRODUCTS
2.1 DREDGE PIPING
A. Pipe shall be ASTM D3350, high density polyethylene, maximum allowable hoop
stress 800 psi at 73.4 degrees F to be joined by thermal butt-fusion. Polyethylene
resins shall conform to Type PE 3408 or better. Protection shall be provided against
ultraviolet light degradation using carbon black, not less than 2 percent well dispersed
in the resin. Pipe wall thickness shall reflect the required SDR and diameter, as
shown in Table 8, ASTM F714. C.
B. Fittings shall be same as pipe, butt fusion joined, conforming to ASTM D3350. All
fittings shall have same pressure rating as pipe, unless otherwise noted.
C. Flanges shall be Van Stone type, cast ASTM A536 (65/45/12), ductile iron backing
ring, IPP Deltaflex convoluted design or equal for bolting to ANSI B16.1, Class 125;
ANSI B16.5, Class 150; and AWWA C207, Class E. Pressure performance of the
backing ring equal to SDR rating of the pipe with safety factor of two. Stub ends
same grade HDPE and pressure rating as pipe. Bolts and Washers shall be stainless
steel, ASTM A193/A193M Grade B8M studs and ASTM A194/A194M Grade 8M
hex head nuts. Gaskets shall be flat ring, 1/8-inch ethylene propylene rubber (EPR).
2.2 TREATMENT CHEMICALS
A. Polymer or other dewatering treatment chemicals shall be suitable for use in potable
water supply. The Contractor shall provide NSF certification of the treatment
chemical to the CM to verify the acceptability of the chemical for potable water use.
The use of chemicals that add weight to the solids are not allowed (e.g., lime).
2.3 CONTAINMENT BOOMS
A. Maintain or replace as needed four spill containment booms at locations and of
approximate lengths as summarized below and shown on the Drawings.
1. Containment Boom #1: Pre-Sedimentation Basin, 600 foot length.
2. Containment Boom #2: North Raw Water Intake Basin, 150 foot length.
3. Containment Boom #3: South Raw Water Intake Basin, 100 foot length.
4. Containment Boom #4: Lagoon Decant/Overflow Structure, 140 foot length.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-8 June 2019
B. Spill containment booms shall be designed for deployment at permanent sites.
Containment booms shall have 18” overall height and shall be manufactured in
modular section lengths.
1. Freeboard: 8 inch.
2. Draft: 10 inch.
3. Section lengths: 50 or 100 foot.
4. Weights: Hot galvanized steel 11 oz.
5. Flotation: Molded polyethylene UV inhibited shell filled with Coast
Guard approved marine grade closed cell foam.
6. Fabric: 175 oz PVC belting with UV and marine inhibitors.
7. Color: Black belting with orange floats.
8. Connector: 18” ASTM serrated slide universal connectors wit zinc anodes.
9. Anchor Points Handles: On each connector end.
C. Provide complete anchoring system, to include, but not limited to, land anchors,
chain, and shackles, as designed and supplied by containment boom manufacturer.
Anchoring system components and materials shall be suitable for installation
conditions specific to each containment boom.
D. Submit product information, storage and handling instructions, and installation
procedures for approval. Coordinate proposed boom installation and anchor point
locations with CM prior to submitting.
E. Submit manufacturer’s recommended maintenance procedures, and furnish OWNER
with any special tools, materials, or supplies that may be necessary for future
maintenance.
F. Provide minimum one year manufacturer’s warranty.
G. Manufacturer and Products: SpillMaster SuperFlex Permanent Oil Spill Containment
Boom as manufactured by Parker Systems, Inc. Chesapeake, VA, or approval equal.
PART 3 – EXECUTION
3.1 GENERAL
A. The Contractor shall use caution when operating near any structure, including the flood
wall, CSXT railroad, and gate works. The Contractor shall be responsible for the repair
of any damage caused to any structure.
B. Any type of anchoring device shall be temporary and removed by the Contractor upon
completion of the Work. Damage caused by placement of anchors shall be repaired by
the Contractor in-kind.
C. Inspection of containment booms in the Pre-sedimentation Basin, and North and South
Raw Water Intake Basins, shall be complete prior to starting dredging of the Lagoon.
Inspection and maintenance will be required throughout the project.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-9 June 2019
3.2 DREDGE PIPING INSTALLATION
A. The Contractor shall use the dredge pipe material specified herein. Securely support
the piping on top of the Lagoon berm using supports and thrust restraints approved by
the Owner.
B. In locations where a filtrate or sludge pipe will cross an area requiring vehicular access
the pipe should be supported and a ramp installed to prevent damage to the pipe and
allow vehicular access.
3.3 LAGOON WTR REMOVAL
A. WTR shall be removed by means of a floating, hydraulic dredge.
B. Control of fuels, oils, and fluids that may be used by dredge or other equipment. The
Contractor shall maintain on-site a spill control kit and all materials necessary to
clean up and remove fuel, oil, or fluid spills.
C. The Contractor shall provide all equipment and temporary piping required for WTR
removal and dewatering. All costs for piping and booster pumping, if required, shall
be included in the unit prices listed in the Bid Form. The Contractor shall not use any
Owner equipment or facilities.
D. The Contractor shall conduct his WTR removal operations to prevent damage to the
Lagoon, Basin, and Berm.
E. A maximum of one day’s production of dewatered WTR may be stored or stockpiled
at the Dewatering Pad. The stockpile must be protected from the weather. All storage
areas must comply with the Virginia Erosion and Sediment Control Law,
Regulations, and Certification Regulations.
F. Virginia Department of Health (VDH) guidelines for Lagoon overflow are less than
1.0 mg/l of aluminum; less than 10 mg/L of TSS; and less than 10 NTU of turbidity.
The Contractor is required to maintain these values below the VDH levels. The CM
shall obtain daily samples of the overflow from the Lagoon to the Basin to monitor
compliance.
G. The Contractor shall be responsible for removing and disposing of any debris found
in the Lagoon including, but not limited to, rocks, cattails, and other vegetation.
Remove all vegetation that is dislodged in the removal operation and is floating on
the surface of the Lagoon, at no additional cost to Owner.
H. The Contractor shall dewater the removed WTR on site to the maximum extent
practicable and as required by the disposal site selected by the Contractor.
I. Filtrate or concentrate shall be drained back to the Residuals Lagoon.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-10 June 2019
J. Vehicle for use on Berm for dredge re-fueling operations (if needed):
1. Must be approved for all-terrain use.
2. Adhere to a 5 mph speed limit.
3. Fuel tank for refueling must be double-walled with a spill proof cap and
securely fastened to the vehicle.
4. Fuel tank size when filled with fuel combined with operator shall not exceed
the vehicle load limit.
5. Vehicle shall be stored out of sight when not in use.
6. Vehicle use is restricted to refueling activities only.
7. Build-up Berm soft spots and around tree stumps as necessary for safe travel
with gravel fill.
8. Submit proposed color and noise data of Vehicle for approval.
9. Submit proposed method of fuel transfer between Vehicle tank and dredge for
approval.
K. Booster Pump (if needed):
1. Submit pump size, type, catalog data, and method of control.
2. Submit sketch of proposed location for pump.
3. Submit method of securing booster pump to site.
4. Submit color and noise data for operating booster pump.
5. Submit a visual and sound barrier and proposed color.
6. Submit method to be utilized to transport pump to location on site.
7. Submit spill control/contingency measures at booster pump location.
3.4 WTR HAULING
A. The Contractor shall be responsible for hauling the WTR from the Owner’s plant site
to the disposal/reuse site and shall obtain and pay for any permits or fees required.
B. Dewatered WTR shall be transported in watertight containers.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-11 June 2019
C. The Contractor is responsible for providing any special measures for traffic control,
including flaggers, signs, or detours.
D. The Contractor is responsible for ensuring proper signage is located on trucks
entering and exiting the WTP. Labeling on the trucks should be approved by the CM
and the Owner.
E. The Contractor shall obey all laws, regulations, and requirements of the agencies
having jurisdiction of the haul routes.
F. The Owner may stop Work if the roads are not maintained clean during WTR
hauling.
3.5 WTR DISPOSAL
A. The Contractor shall dispose of the WTR as documented in the Contractor’s Work
Plan and comply with all local, state, and federal requirements or guidelines.
B. The Contractor shall provide the CM a copy of the uniform manifest document that
accompanies each truckload if requested.
C. The Contractor shall notify the CM immediately of any problems encountered during
WTR disposal/reuse.
D. If land-applying, determination of the WTR application rate and method of
application are the Contractor’s responsibility. The application rate must be designed
to meet all local, state and federal requirements for the site.
E. All requirements for buffer zones, incorporation of WTR, land use limitations,
loading rates, storing or stockpiling of WTR, and all other guidelines or requirements
must be complied with.
F. At the completion of the Work, the Contractor shall provide the CM written
certification that the WTR were disposed/reused in accordance with all local, state,
and federal requirements. The Contractor shall also provide the CM a written report
that lists the areas where the WTR were disposed/reused, the quantities of WTR
disposed/reused, and all monitoring information required by local, state, and federal
regulatory agencies.
3.6 CONTAINMENT BOOMS
A. If the containment booms are replaced, a manufacturer’s representative shall provide
installation assistance and shall inspect and certify each completed containment boom
installation.
B. If the containment booms are replaced, a Manufacturer’s representative shall complete
and submit form “Manufacturer’s Certificate of Proper Installation” located in
Supplement E.
DPU Standard
Removal and Disposal of Water Treatment Residuals 02000-12 June 2019
C. The CONTRACTOR shall immediately address any issues associated with the
containment boom installations to ensure proper function is maintained. The Owner
may restrict other work activities until necessary repairs are made.
3.7 INSPECTION
A. The Contractor shall furnish, at the request of the CM and at no additional cost to the
Owner, boats, boatmen, laborers, and materials necessary for inspecting and
supervising the Work. When requested, the Contractor shall provide transportation for
the CM to and from the dredging or work area.
3.8 SUPPLEMENTS
A. The supplements listed below, following “END OF SECTION,” are part of this
Specification.
1. Supplement A – Contract Drawings
2. Supplement B – WTR Sampling Results
3. Supplement C – Summary Sheet of Lagoon Residuals Removal since 2004
4. Supplement D – Construction Site Safety Plan for Contractors Working on or
near Hazardous Conditions at the Water Purification Plant
5. Supplement E – Manufacturer’s Certificate of Proper Installation
6. Supplement F – Right of Entry and Indemnification Agreement
END OF SECTION
Supplement A Contract Drawings
Supplement B WTR Sampling Results
MEMORANDUM
City of Richmond – Water Treatment Plant Pre-Sediment Basin and Residual Lagoon Sediment Sampling
Date: 4/12/2017
To: Edward Alleyne, City of Richmond Work Order Number: 46510-003
From: Kevin T. Roberts
Subject: City of Richmond Residual Lagoon and Pre-Sedimentation Basin Sediment Sampling
Project: City of Richmond Water Purification Plant Residual Lagoon Sediment Sampling
CC: Joe Felton, Dan Seli, Kevin Alvarado
Introduction
The City of Richmond is proposing to dredge the bottom of the Residual Lagoon at the Water Purification Plant located at 3998 Douglasdale Road in Richmond, Virginia. The “site” is defined as two manmade ponds, a Pre-Sediment Basin and Residual Lagoon containing post-treatment sediment. The City of Richmond has tasked WRA to conduct sediment characterization study to determine the contents of the sediment prior to the proposed dredging efforts. This investigation describes the methodology and analytical results of the environmental sediment sampling to characterize accumulated sediment to assist the City of Richmond with addressing the following items: health and safety plan, handling procedures, material management and disposal. The results of the sampling and this report are to be used by contractors planning to submit bids for the Water Treatment Plant Lagoon Residuals Removal, Phase IV.
Environmental Sediment Sampling & Methodology
On March 21 and 23, 2017, WRA was onsite to perform sediment sampling within both the Pre-Sediment Basin and the Residual Lagoon located at the Richmond Water Purification Plant. Environmental sediment sampling was performed by WRA using a combination of a hand-held sediment coring device (AMS® sludge and sediment sampler kit) specifically designed to retain undisturbed samples from non-cohesive materials in streams and shallow lakes and a PVC sediment extractor. Continuous sampling was performed from the top of the sediment and advanced to a depth approximately 10 feet below sediment surface or to refusal. Due to the depth of accumulate sediment on the southern end of the Residual Lagoon, sediment was sampled from the bank. In order to collect representative sediment samples from middle of the lagoon sample locations were accessed by boat.
Methodology
10 discreet sample points were selected within the Residual Lagoon to provide representation of the accumulated sediment. For background comparison, three sample points were also selected within the Pre-sedimentation Basin where accumulated sediment was visible. Samples were comprised of composite sediment collected from 0-10 feet below sediment surface in the Residual Lagoon and the Pre-Sediment Basin. Sample locations are depicted in the Sample Location Plan included in Appendix A.
Once retrieved, samples were immediately placed in their respective sample containers and retained on ice until they were submitted under chain of custody to Air, Water and Soil Laboratories for analytical testing for the following parameters:
• Priority Pollutant List (PPL) Metals by methods 6010B/ 7471A
• Hexavalent Chromium by method SW7916
• Toxicity Characteristic Leaching Procedure (TCLP) Metals by method 7470
• Volatile Organic Compounds (VOCs) by method 8260B
• Semi-Volatile Organic Compounds (SVOCs) by method 8270
• Total Petroleum Compounds Gasoline Range Organics (TPH-GRO) by method 8015
• Total Petroleum Compounds Diesel Range Organics (TPH-DRO) by method 8015
4/12/2017 Page 2 46510-003
Representative samples RL-S-1 to RL-S-4 (combined) and Sample RL-S-53A & RL-S-53B were provided to determine the sample composition via wet chemistry analysis. These samples were collected in areas where the majority of dredging will occur. Sample composition, including total percent moisture, total percent solids, and total percent volatile solids (organics), was calculated via methods SM18 2540G and SM22 2540G-2011.
Analytical Data Results Summary
The accumulated sediment has revealed detections of select contaminants. Analytical results for detected compounds are summarized in Table 1 included as Appendix B in this report. For discussion purposes, the results are compared the Environmental Protection Agency’s (EPA) Regional Screening Levels (RSLs) for Residential and Industrial Soil, the Virginia Department of Environmental Quality (DEQ) TPH Clean Fill Limits and Voluntary Remediation Program’s (VRP) Tier II Sediment Screening Concentrations (Residential). Additionally, metals were compared to the United States Geological Survey (USGS) Geochemical and Mineralogical Maps for Soils of the Conterminous United States background values (Retrieved 5 April, 2016, from http://pubs.usgs.gov/of/2014/1082/pdf/ofr2014-1082.pdf). The laboratory analytical report is included in Appendix C. VOCs
Two VOC compounds were reported in the analytical results. Acetone and 2-Butanone (Methyl Ethyl Ketone (MEK)) were reported in concentrations below the EPA RSLs and DEQ Sediment Screening Concentrations. SVOCs
Two SVOCs were reported in the analytical results. Acetophenone was reported in concentrations below the EPA RSL and DEQ Sediment Screening Concentration. Pyridine was reported in concentrations below the EPA RSL; there is no DEQ Sediment Screening Concentration established for pyridine. TPH
TPH-DRO was detected above the reporting limits in RL-S-6A+6B (11.4 mg/kg) but was below the DEQ TPH clean fill limit of 50 ppm (9 VAC20-80-700: Soil Contaminated with Petroleum Products). Metals
Arsenic was detected at a concentration above the EPA RSLs (3.27 mg/kg) but were below the DEQ Sediment Screening Concentrations and USGS background value in PSB-3 (Pre-Sediment Basin location). Also in PSB-3, cadmium was detected at a concentration exceeding the USGS background value (1.22 mg/kg) but was below the EPA RSL and DEQ Sediment Screening Concentration. TCLP Metals
No TCLP metal concentrations were reported. Sample Composition Samples RL-S-1 to RL-S-4 were reported to be 93.5% moisture and 6.46% solids. Of the 6.46% solids reported, approximately 31.9% of the volume was determined to be volatile solids (organics). Samples RL-S-53A and RL-S-53B were reported to be 89.5% moisture and 10.5% solids. Of the 10.5% solids reported, approximately 27.7% of the volume was determined to be volatile solids (organics).
Discussion and Recommendations The purpose of this investigation is to evaluate sediment conditions in the Water Purification Plant Residual Lagoon and Pre - sedimentation Basin to assist the City of Richmond with addressing health and safety, material handling/management and potential disposal options for the accumulated sediment. Composite soil samples were collected from 10 sample locations and three sample locations within the Pre-Sediment Basin. Samples were collected continuously to sampler refusal. No staining, sheens or petroleum odors were observed during the sampling event. DEQ TPH Clean Fill Limits and Voluntary Remediation Program’s Tier II Sediment Screening Concentration (Residential) and the USGS background values were used as sources of analytical comparison for the area. These
4/12/2017 Page 3 46510-003
comparisons are to assist with worker safety and disposal considerations during the dredging efforts (it should be noted that these are not cleanup levels, they are levels based upon human health risk and in in the case for metals, naturally occurring background ranges). According to the analytical results for the sediment, TPH-DRO was detected in one sample location but was below the DEQ clean fill limit for TPH. Two VOCs (acetone and 2-Butanone) were detected but were below the EPA RSL and DEQ Sediment Screening Concentration. Two SVOCs (acetophenone and pyridine) were detected at concentrations below the EPA RSL and DEQ Sediment Screening Concentration. In one location, arsenic was detected in a concentration above the EPA RSL and cadmium was detected in concentrations above the USGS background range; however, arsenic was below the DEQ Sediment Screening Concentration established for residential settings. Cadmium was detected at a concentration that exceeded the naturally occurring background range but was within the EPA RSLs and the DEQ Sediment Screening Concentration. Additionally, both exceedances were detected in the PSB-3 sample location, located in the Pre-Sediment Basin and not in the Residual Lagoon. With regard to sample composition, a large percentage of each sample was represented by moisture (~90%). Of the remaining solids (>10% of total volume), approximately 30% consisted of volatile solids (organic material). This information should be taken into consideration during the sediment removal process. The laboratory results from this investigation provide a basic characterization of the sediment located in the Residual Lagoon and the Pre-sediment Basin. Overall, the contaminant detections reported in the Residual Lagoon are minor and do not exceed established values for soil or sediment in residential or industrial settings. The only exceedances were reported in sediment from sample location PSB-3, located in the Pre-Sediment Basin. Furthermore, these exceedances were metals which were slightly above their respective background range or respective EPA RSL. These values are not cleanup levels but are included for comparison purposes. No TCLP metal detections were reported. With regard to sample composition, a large percentage of each sample was represented by moisture (~90%). Of the remaining solids (>10% of total volume), approximately 30% consisted of volatile solids (organic material).Prior to dredging efforts, WRA recommends that the City of Richmond (or the contractor performing the work) pre-select several solid waste facilities to be considered for potential disposal of sediment material, including the City Landfill. Each disposal facility has specific acceptance requirements based on their respective solid waste permit and may require additional analytical data (i.e. Toxicity Characteristic Leaching Procedure, EPA paint filter liquid testing for moisture content).
_________________________________________ Kevin T. Roberts Project Environmental Scientist
MEMORANDUM
City of Richmond – Water Treatment Plant Pre-Sediment Basin and Residual Lagoon Sediment Sampling
Appendix A
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
PSB-3
PSB-2
PSB-1
RL-S-5
RL-S-4
RL-S-3
RL-S-2
RL-S-1
RL-S-7A+7B
RL-S-6A+6B
RL-S-51A+51B
RL-S-52A+52B
RL-S-53A+53B
© OpenStreetMap (and) contributors, CC-BY-SA, Source: Esri,DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA,USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and the GISUser Community
Source:
Figure: City of Richmond Residiual Lagoon
& Pre-Sedimentation Basin Sediment Sampling
WRA Project No.:
Date:
City of Richmond, VirginiaSample Location
Map
Title:
1 inch = 600 feet
©Client:46510.003
City of Richmond
04/17/2017
Hydrologic Unit Code: 02080205 (Middle James-Willis)
LegendProject Study Area
!. Sample Location (Approx.)
Pre-Sedimentation Basin
Residual Lagoon
4/12/2017 Page 5 46510-003
Appendix B
Appendix B Table 1: Residual Lagoon and Pre-Sedimentation Basin Sediment Sampling – Analytical Data Results Summary
Composite Sample ID: RL-S-1 RL-S-2 RL-S-3 RL-S-4 RL-S-5 RL-S-51A
+ 51B
RL-S-52A
+ 52B
RL-S-53A
+ 53B
RL-S-6A +
6B
RL-S-7A +
7B PSB-1 PSB-2 PSB-3
Depth 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft. 0-10 ft.
Analyte / Test Method Units DEQ TPH Clean
Fill Limit
EPA
Regional
Screening
Levels (RSLs)
Residential
EPA Regional
Screening
Levels (RSLs)
Industrial
DEQ VRP Tier
II Sediment
Screening
Concentration
(Residential)
TPH-DRO / 3546 mg/kg 50 NA NA NA ND ND ND ND ND ND ND ND 11.4 ND ND ND ND
TPH-GRO / 8015 mg/kg 50 NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND
VOCs / 8260 mg/kg
Acetone mg/kg 61,000 670,000 61,000 0.028 0.0255 0.0425 0.059 0.0813 0.059 0.0287 0.03 0.0183 ND 0.0213 0.0154 0.0223
2-Butanone (MEK) mg/kg 27,000 190,000 27,000 ND ND ND ND 0.00979 0.00704 ND 0.00556 ND 0.00995 ND ND ND
SVOCs / 8270
Acetophenone mg/kg 7,800 120,000 7,800 0.117 ND ND ND ND ND ND ND ND 0.114 ND ND ND
Pyridine mg/kg 78 1,200 NA 0.148 ND ND ND ND ND ND ND ND ND ND ND ND
Metals / 6000 / 7000 USGS
Background Ranges
Arsenic mg/kg 0.6-4.3 0.68 3.0 34 ND 1.07 1.21 1.07 1.96 2.66 ND 1.99 1.25 1.35 2.36 2.10 3.27
Cadmium mg/kg <0.1-1 71 980 70 ND ND ND ND 0.234 0.423 ND 0.214 ND 0.299 0.584 0.904 1.22
Chromium (Trivalent III) mg/kg 30-35 120,000 1,800,000 30 14.2 9.84 11.8 9.63 9.71 11.7 8.09 8.05 7.17 7.55 12.8 10.7 15.5
Chromium (Hexavalent VI) mg/kg -- 0.31 6.3 NA ND ND ND ND ND ND ND ND ND ND ND ND ND
Copper mg/kg 17.1-280 3,100 47,000 3,100 13.3 12.1 19.6 9.29 85.9 69.2 12.1 51.6 19.3 29.6 18.4 43.3 62.7
Lead mg/kg 20-24.1 400 800 400 ND ND ND ND 3.09 4.48 0.635 2.85 1.56 2.42 4.32 8.32 ND
Mercury mg/kg 0.03-0.05 11 46 9.4 ND ND 0.011 ND 0.016 0.031 ND 0.014 0.019 0.024 0.025 0.036 0.086
Nickel mg/kg 11.2-18.3 1,500 22,000 150,000 1.02 0.852 1.12 0.930 1.87 2.71 0.963 2.22 1.51 2.61 4.56 6.06 8.69
Zinc mg/kg 76-977 2,300 23,000 23,000 6.10 5.10 6.94 5.85 12.9 21.8 8.74 13.8 12.9 28.5 29.1 40.7 56.2
TCLP Metals / 6000 / 7000 mg/L RCRA Limits NA NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND
Sample Composition / 2540
Combined RL-S-1 through 4 RL-S-53A
+ 53B
Moisture % 93.5 89.5
Solid % 6.46 10.5
*Volatile Solid (Organics) % 31.9 27.7
Notes: ND: Non-detect: NS: Not sampled NA: Not applicable Red Bolded: values indicate exceedance of soil standard
*Volatile Solids (Organics) represents a % of the total SOLID volume of the sample. For example: Of the 10.5% solids reported for sample RL-S-53A + 53B, approximately 27.7% of the volume of SOLIDS was determined to be volatile solids (organics).
4/12/2017 Page 6 46510-003
Appendix C
1941 Reymet Road l Richmond, Virginia 23237 l Tel: (804)-358-8295 Fax: (804)-358-8297
Laboratory Order ID 17C0754
Certificate of Analysis
Client Name:
Enclosed are the results of analyses for samples received by the laboratory on 03/22/2017 11:57. If you have
any questions concerning this report, please feel free to contact the laboratory.
Sincerely,
Ted Soyars
Laboratory Manager
Richmond, VA 23235
9030 Stony Point Parkway, Suite 220
Purchase Order:
46510-003Project Number:
Date Issued:
Date Received:
Submitted To:
Client Site I.D.:
March 29, 2017 16:36
March 22, 2017 11:57Whitman, Requardt & Associates, LLP - Richmond
Joe Felton
End Notes:
The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.
Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen,
temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely
short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler
included in the Certificate of Analysis are done so at the client�s request and are not included in the laboratory�s fields of certification
nor have they been audited for adherence to a reference method or procedure.
The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified.
For a complete list of the Laboratory�s NELAC certified parameters please contact customer service.
This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air
Water & Soil Laboratories, Inc.
COR WPP Feeder Channel Sediment Testing
Final Report
Page 1 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
ANALYTICAL REPORT FOR SAMPLES
Laboratory Order ID 17C0754
MatrixSample ID Laboratory ID Date Sampled Date Received
RL-S-1 17C0754-01 03/22/2017 11:57Soil 03/21/2017 13:00
RL-S-2 17C0754-02 03/22/2017 11:57Soil 03/21/2017 13:30
RL-S-3 17C0754-03 03/22/2017 11:57Soil 03/21/2017 13:45
RL-S-4 17C0754-04 03/22/2017 11:57Soil 03/21/2017 14:00
RL-S-5 17C0754-05 03/22/2017 11:57Soil 03/21/2017 14:15
Page 2 of 81Page 2 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 101 03/22/17 13:27 03/23/17 13:04Silver
SW6010C CWO<1.98 mg/kg 1.98 201RE2 03/22/17 13:27 03/24/17 13:52Arsenic
SW6010C CWO<0.200 mg/kg 0.200 101 03/22/17 13:27 03/23/17 13:04Beryllium
SW6010C CWO<0.200 mg/kg 0.200 101 03/22/17 13:27 03/23/17 13:04Cadmium
SW6010C 14.2 mg/kg CWO0.500 101 03/22/17 13:27 03/23/17 13:04Chromium
SW6010C 13.3 mg/kg CWO2.50 101 03/22/17 13:27 03/23/17 13:04Copper
SW7471B RCV<0.008 mg/kg 0.008 101 03/22/17 13:27 03/22/17 14:58Mercury
SW6010C 1.02 mg/kg CWO0.500 101 03/22/17 13:27 03/23/17 13:04Nickel
SW6010C CWO<0.500 mg/kg 0.500 101 03/22/17 13:27 03/23/17 13:04Lead
SW6010C CWO<5.00 mg/kg 5.00 101 03/22/17 13:27 03/23/17 13:04Antimony
SW6010C CWO<2.50 mg/kg 2.50 101 03/22/17 13:27 03/23/17 13:04Selenium
SW6010C CWO<2.50 mg/kg 2.50 101 03/22/17 13:27 03/23/17 13:04Thallium
SW6010C 6.10 mg/kg CWO0.500 101 03/22/17 13:27 03/23/17 13:04Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 101 03/23/17 10:00 03/24/17 12:36TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 101 03/23/17 10:00 03/24/17 12:36TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 101 03/23/17 10:00 03/24/17 12:36TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 101 03/23/17 10:00 03/24/17 12:36TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 101 03/23/17 10:00 03/24/17 12:36TCLP Chromium
SW7470A RCV<0.008 mg/L 0.008 101 03/23/17 09:00 03/24/17 11:41TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 101 03/23/17 10:00 03/24/17 12:36TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 101 03/23/17 10:00 03/24/17 12:36TCLP Selenium
SW1311 1 # RCV-- 101 03/22/17 15:59 03/23/17 08:33TCLP Extraction Fluid,
Metals
Page 3 of 81Page 3 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.50 mg/kg 0.50 101 03/23/17 13:22 03/23/17 13:22TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:591,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:592,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:592-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:592-Chlorotoluene
Page 4 of 81Page 4 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:592-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:594-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:594-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:594-Methyl-2-pentanone (MIBK)
SW8260B 28.0 ug/kg LAO10.0 101 03/22/17 13:59 03/22/17 13:59Acetone
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Benzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Bromoform
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Chloroform
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 101 03/22/17 13:59 03/22/17 13:59Ethanol
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 101 03/22/17 13:59 03/22/17 13:59Ethyl-t-butyl ether (ETBE)
Page 5 of 81Page 5 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Styrene
SW8260B LAO<10.0 ug/kg 10.0 101 03/22/17 13:59 03/22/17 13:59TAA
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59TAEE
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59TAME
SW8260B LAO<100 ug/kg 100 101 03/22/17 13:59 03/22/17 13:59TBA
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Toluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 101 03/22/17 13:59 03/22/17 13:59Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 101 03/22/17 13:59 03/22/17 13:59Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 101 03/22/17 13:59 03/22/17 13:59Xylenes, Total
Page 6 of 81Page 6 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Volatile Organic Compounds by GCMS
80-120102 %Surr: 1,2-Dichloroethane-d4 LAO01 SW8260B 03/22/17 13:59 03/22/17 13:59
85-12099.0 %Surr: 4-Bromofluorobenzene LAO01 SW8260B 03/22/17 13:59 03/22/17 13:59
78-119105 %Surr: Dibromofluoromethane LAO01 SW8260B 03/22/17 13:59 03/22/17 13:59
85-115102 %Surr: Toluene-d8 LAO01 SW8260B 03/22/17 13:59 03/22/17 13:59
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:201-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Naphthylamine
Page 7 of 81Page 7 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:203,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:203-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:203-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg C 83.3 101 03/24/17 10:14 03/24/17 19:204-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:204-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:207,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Acenaphthylene
SW8270D 117 ug/kg SKS83.3 101 03/24/17 10:14 03/24/17 19:20Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Aniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Benzyl alcohol
Page 8 of 81Page 8 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:202,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Chrysene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Fluorene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Isophorone
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Naphthalene
Page 9 of 81Page 9 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Phenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Pronamide
SW8270D SKS<83.3 ug/kg 83.3 101 03/24/17 10:14 03/24/17 19:20Pyrene
SW8270D 148 ug/kg SKS83.3 101 03/24/17 10:14 03/24/17 19:20Pyridine
35-12558.3 %Surr: 2,4,6-Tribromophenol SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
45-10557.8 %Surr: 2-Fluorobiphenyl SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
35-10563.7 %Surr: 2-Fluorophenol SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
35-10061.5 %Surr: Nitrobenzene-d5 SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
40-10063.2 %Surr: Phenol-d5 SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
30-12567.0 %Surr: p-Terphenyl-d14 SKS01 SW8270D 03/24/17 10:14 03/24/17 19:20
Page 10 of 81Page 10 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:00Date/Time Sampled:
RL-S-1 Laboratory Sample ID:Sample I.D. 17C0754-01
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 101 03/23/17 15:28 03/28/17 15:15TPH-Semi-Volatiles (DRO)
40-16068.2 %Surr: Pentacosane CVH01 SW8015C 03/23/17 15:28 03/28/17 15:15
Wet Chemistry Analysis
SW7196A CMB<0.20 mg/kg 0.20 101 03/24/17 15:30 03/24/17 15:30Chromium, Hexavalent
Page 11 of 81Page 11 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 102 03/22/17 13:27 03/23/17 13:06Silver
SW6010C 1.07 mg/kg CWO1.00 102 03/22/17 13:27 03/23/17 13:06Arsenic
SW6010C CWO<0.200 mg/kg 0.200 102 03/22/17 13:27 03/23/17 13:06Beryllium
SW6010C CWO<0.200 mg/kg 0.200 102 03/22/17 13:27 03/23/17 13:06Cadmium
SW6010C 9.84 mg/kg CWO0.500 102 03/22/17 13:27 03/23/17 13:06Chromium
SW6010C 12.1 mg/kg CWO2.50 102 03/22/17 13:27 03/23/17 13:06Copper
SW7471B RCV<0.008 mg/kg 0.008 102 03/22/17 13:27 03/22/17 15:00Mercury
SW6010C 0.852 mg/kg CWO0.500 102 03/22/17 13:27 03/23/17 13:06Nickel
SW6010C CWO<0.500 mg/kg 0.500 102 03/22/17 13:27 03/23/17 13:06Lead
SW6010C CWO<5.00 mg/kg 5.00 102 03/22/17 13:27 03/23/17 13:06Antimony
SW6010C CWO<2.50 mg/kg 2.50 102 03/22/17 13:27 03/23/17 13:06Selenium
SW6010C CWO<2.50 mg/kg 2.50 102 03/22/17 13:27 03/23/17 13:06Thallium
SW6010C 5.10 mg/kg CWO0.500 102 03/22/17 13:27 03/23/17 13:06Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 102 03/23/17 10:00 03/24/17 12:40TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 102 03/23/17 10:00 03/24/17 12:40TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 102 03/23/17 10:00 03/24/17 12:40TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 102 03/23/17 10:00 03/24/17 12:40TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 102 03/23/17 10:00 03/24/17 12:40TCLP Chromium
SW7470A RCV<0.008 mg/L 0.008 102 03/23/17 09:00 03/24/17 11:49TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 102 03/23/17 10:00 03/24/17 12:40TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 102 03/23/17 10:00 03/24/17 12:40TCLP Selenium
SW1311 1 # RCV-- 102 03/22/17 15:59 03/23/17 08:33TCLP Extraction Fluid,
Metals
Page 12 of 81Page 12 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.50 mg/kg 0.50 102 03/23/17 13:44 03/23/17 13:44TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:251,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:252,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:252-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:252-Chlorotoluene
Page 13 of 81Page 13 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:252-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:254-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:254-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:254-Methyl-2-pentanone (MIBK)
SW8260B 25.5 ug/kg LAO10.0 102 03/22/17 14:25 03/22/17 14:25Acetone
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Benzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Bromoform
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Chloroform
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 102 03/22/17 14:25 03/22/17 14:25Ethanol
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 102 03/22/17 14:25 03/22/17 14:25Ethyl-t-butyl ether (ETBE)
Page 14 of 81Page 14 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Styrene
SW8260B LAO<10.0 ug/kg 10.0 102 03/22/17 14:25 03/22/17 14:25TAA
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25TAEE
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25TAME
SW8260B LAO<100 ug/kg 100 102 03/22/17 14:25 03/22/17 14:25TBA
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Toluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 102 03/22/17 14:25 03/22/17 14:25Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 102 03/22/17 14:25 03/22/17 14:25Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 102 03/22/17 14:25 03/22/17 14:25Xylenes, Total
Page 15 of 81Page 15 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Volatile Organic Compounds by GCMS
80-120102 %Surr: 1,2-Dichloroethane-d4 LAO02 SW8260B 03/22/17 14:25 03/22/17 14:25
85-120102 %Surr: 4-Bromofluorobenzene LAO02 SW8260B 03/22/17 14:25 03/22/17 14:25
78-119102 %Surr: Dibromofluoromethane LAO02 SW8260B 03/22/17 14:25 03/22/17 14:25
85-115103 %Surr: Toluene-d8 LAO02 SW8260B 03/22/17 14:25 03/22/17 14:25
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:551-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Naphthylamine
Page 16 of 81Page 16 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:553,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:553-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:553-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg C 83.3 102 03/24/17 10:14 03/24/17 19:554-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:554-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:557,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Aniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Benzyl alcohol
Page 17 of 81Page 17 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:552,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Chrysene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Fluorene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Isophorone
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Naphthalene
Page 18 of 81Page 18 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Phenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Pronamide
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/24/17 10:14 03/24/17 19:55Pyridine
35-12542.0 %Surr: 2,4,6-Tribromophenol SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
45-10543.1 %Surr: 2-Fluorobiphenyl S SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
35-10551.8 %Surr: 2-Fluorophenol SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
35-10046.5 %Surr: Nitrobenzene-d5 SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
40-10046.8 %Surr: Phenol-d5 SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
30-12549.0 %Surr: p-Terphenyl-d14 SKS02 SW8270D 03/24/17 10:14 03/24/17 19:55
Page 19 of 81Page 19 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:30Date/Time Sampled:
RL-S-2 Laboratory Sample ID:Sample I.D. 17C0754-02
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 102 03/23/17 15:28 03/28/17 15:41TPH-Semi-Volatiles (DRO)
40-16081.7 %Surr: Pentacosane CVH02 SW8015C 03/23/17 15:28 03/28/17 15:41
Wet Chemistry Analysis
SW7196A CMB<0.20 mg/kg 0.20 102 03/24/17 15:30 03/24/17 15:30Chromium, Hexavalent
Page 20 of 81Page 20 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 103 03/22/17 13:27 03/23/17 13:07Silver
SW6010C 1.21 mg/kg CWO1.00 103RE1 03/22/17 13:27 03/24/17 13:12Arsenic
SW6010C CWO<0.200 mg/kg 0.200 103 03/22/17 13:27 03/23/17 13:07Beryllium
SW6010C CWO<0.200 mg/kg 0.200 103 03/22/17 13:27 03/23/17 13:07Cadmium
SW6010C 11.8 mg/kg CWO0.500 103 03/22/17 13:27 03/23/17 13:07Chromium
SW6010C 19.6 mg/kg CWO2.50 103 03/22/17 13:27 03/23/17 13:07Copper
SW7471B 0.011 mg/kg RCV0.008 103 03/22/17 13:27 03/22/17 15:02Mercury
SW6010C 1.12 mg/kg CWO0.500 103 03/22/17 13:27 03/23/17 13:07Nickel
SW6010C CWO<0.500 mg/kg 0.500 103 03/22/17 13:27 03/23/17 13:07Lead
SW6010C CWO<5.00 mg/kg 5.00 103 03/22/17 13:27 03/23/17 13:07Antimony
SW6010C CWO<2.50 mg/kg 2.50 103 03/22/17 13:27 03/23/17 13:07Selenium
SW6010C CWO<2.50 mg/kg 2.50 103 03/22/17 13:27 03/23/17 13:07Thallium
SW6010C 6.94 mg/kg CWO0.500 103 03/22/17 13:27 03/23/17 13:07Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 103 03/23/17 10:00 03/24/17 12:51TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 103 03/23/17 10:00 03/24/17 12:51TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 103 03/23/17 10:00 03/24/17 12:51TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 103 03/23/17 10:00 03/24/17 12:51TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 103 03/23/17 10:00 03/24/17 12:51TCLP Chromium
SW7470A RCV<0.008 mg/L 0.008 103 03/23/17 09:00 03/24/17 11:51TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 103 03/23/17 10:00 03/24/17 12:51TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 103 03/23/17 10:00 03/24/17 12:51TCLP Selenium
SW1311 1 # RCV-- 103 03/22/17 15:59 03/23/17 08:33TCLP Extraction Fluid,
Metals
Page 21 of 81Page 21 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.47 mg/kg 0.47 103 03/23/17 14:07 03/23/17 14:07TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:501,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:502,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:502-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:502-Chlorotoluene
Page 22 of 81Page 22 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:502-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:504-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:504-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:504-Methyl-2-pentanone (MIBK)
SW8260B 42.5 ug/kg LAO10.0 103 03/22/17 14:50 03/22/17 14:50Acetone
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Benzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Bromoform
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Chloroform
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 103 03/22/17 14:50 03/22/17 14:50Ethanol
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 103 03/22/17 14:50 03/22/17 14:50Ethyl-t-butyl ether (ETBE)
Page 23 of 81Page 23 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Styrene
SW8260B LAO<10.0 ug/kg 10.0 103 03/22/17 14:50 03/22/17 14:50TAA
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50TAEE
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50TAME
SW8260B LAO<100 ug/kg 100 103 03/22/17 14:50 03/22/17 14:50TBA
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Toluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 103 03/22/17 14:50 03/22/17 14:50Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 103 03/22/17 14:50 03/22/17 14:50Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 103 03/22/17 14:50 03/22/17 14:50Xylenes, Total
Page 24 of 81Page 24 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Volatile Organic Compounds by GCMS
80-12098.6 %Surr: 1,2-Dichloroethane-d4 LAO03 SW8260B 03/22/17 14:50 03/22/17 14:50
85-12096.9 %Surr: 4-Bromofluorobenzene LAO03 SW8260B 03/22/17 14:50 03/22/17 14:50
78-119104 %Surr: Dibromofluoromethane LAO03 SW8260B 03/22/17 14:50 03/22/17 14:50
85-115103 %Surr: Toluene-d8 LAO03 SW8260B 03/22/17 14:50 03/22/17 14:50
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:291-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Naphthylamine
Page 25 of 81Page 25 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:293,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:293-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:293-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg C 83.3 103 03/24/17 10:14 03/24/17 20:294-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:294-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:297,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Aniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Benzyl alcohol
Page 26 of 81Page 26 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:292,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Chrysene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Fluorene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Isophorone
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Naphthalene
Page 27 of 81Page 27 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Phenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Pronamide
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/24/17 10:14 03/24/17 20:29Pyridine
35-12542.1 %Surr: 2,4,6-Tribromophenol SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
45-10540.7 %Surr: 2-Fluorobiphenyl S SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
35-10550.4 %Surr: 2-Fluorophenol SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
35-10045.4 %Surr: Nitrobenzene-d5 SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
40-10046.1 %Surr: Phenol-d5 SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
30-12547.4 %Surr: p-Terphenyl-d14 SKS03 SW8270D 03/24/17 10:14 03/24/17 20:29
Page 28 of 81Page 28 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 13:45Date/Time Sampled:
RL-S-3 Laboratory Sample ID:Sample I.D. 17C0754-03
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 103 03/23/17 15:28 03/28/17 16:08TPH-Semi-Volatiles (DRO)
40-16056.7 %Surr: Pentacosane CVH03 SW8015C 03/23/17 15:28 03/28/17 16:08
Wet Chemistry Analysis
SW7196A CMB<0.20 mg/kg 0.20 103 03/24/17 15:30 03/24/17 15:30Chromium, Hexavalent
Page 29 of 81Page 29 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 104 03/22/17 13:27 03/23/17 13:08Silver
SW6010C 1.07 mg/kg CWO1.00 104 03/22/17 13:27 03/23/17 13:08Arsenic
SW6010C CWO<0.200 mg/kg 0.200 104 03/22/17 13:27 03/23/17 13:08Beryllium
SW6010C CWO<0.200 mg/kg 0.200 104 03/22/17 13:27 03/23/17 13:08Cadmium
SW6010C 9.63 mg/kg CWO0.500 104 03/22/17 13:27 03/23/17 13:08Chromium
SW6010C 9.29 mg/kg CWO2.50 104 03/22/17 13:27 03/23/17 13:08Copper
SW7471B RCV<0.008 mg/kg 0.008 104 03/22/17 13:27 03/22/17 15:04Mercury
SW6010C 0.930 mg/kg CWO0.500 104 03/22/17 13:27 03/23/17 13:08Nickel
SW6010C CWO<0.500 mg/kg 0.500 104 03/22/17 13:27 03/23/17 13:08Lead
SW6010C CWO<5.00 mg/kg 5.00 104 03/22/17 13:27 03/23/17 13:08Antimony
SW6010C CWO<2.50 mg/kg 2.50 104 03/22/17 13:27 03/23/17 13:08Selenium
SW6010C CWO<2.50 mg/kg 2.50 104 03/22/17 13:27 03/23/17 13:08Thallium
SW6010C 5.85 mg/kg CWO0.500 104 03/22/17 13:27 03/23/17 13:08Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 104 03/23/17 10:00 03/24/17 12:52TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 104 03/23/17 10:00 03/24/17 12:52TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 104 03/23/17 10:00 03/24/17 12:52TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 104 03/23/17 10:00 03/24/17 12:52TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 104 03/23/17 10:00 03/24/17 12:52TCLP Chromium
SW7470A RCV<0.008 mg/L 0.008 104 03/23/17 09:00 03/24/17 11:53TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 104 03/23/17 10:00 03/24/17 12:52TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 104 03/23/17 10:00 03/24/17 12:52TCLP Selenium
SW1311 1 # RCV-- 104 03/22/17 15:59 03/23/17 08:33TCLP Extraction Fluid,
Metals
Page 30 of 81Page 30 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.50 mg/kg 0.50 104 03/23/17 14:29 03/23/17 14:29TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:131,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:132,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:132-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:132-Chlorotoluene
Page 31 of 81Page 31 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:132-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:134-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:134-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:134-Methyl-2-pentanone (MIBK)
SW8260B 59.0 ug/kg LAO10.0 104 03/22/17 15:13 03/22/17 15:13Acetone
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Benzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Bromoform
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Chloroform
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 104 03/22/17 15:13 03/22/17 15:13Ethanol
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 104 03/22/17 15:13 03/22/17 15:13Ethyl-t-butyl ether (ETBE)
Page 32 of 81Page 32 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Styrene
SW8260B LAO<10.0 ug/kg 10.0 104 03/22/17 15:13 03/22/17 15:13TAA
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13TAEE
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13TAME
SW8260B LAO<100 ug/kg 100 104 03/22/17 15:13 03/22/17 15:13TBA
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Toluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 104 03/22/17 15:13 03/22/17 15:13Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 104 03/22/17 15:13 03/22/17 15:13Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 104 03/22/17 15:13 03/22/17 15:13Xylenes, Total
Page 33 of 81Page 33 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Volatile Organic Compounds by GCMS
80-12097.3 %Surr: 1,2-Dichloroethane-d4 LAO04 SW8260B 03/22/17 15:13 03/22/17 15:13
85-120101 %Surr: 4-Bromofluorobenzene LAO04 SW8260B 03/22/17 15:13 03/22/17 15:13
78-119105 %Surr: Dibromofluoromethane LAO04 SW8260B 03/22/17 15:13 03/22/17 15:13
85-115102 %Surr: Toluene-d8 LAO04 SW8260B 03/22/17 15:13 03/22/17 15:13
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:031-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Naphthylamine
Page 34 of 81Page 34 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:033,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:033-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:033-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg C 83.3 104 03/24/17 10:14 03/24/17 21:034-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:034-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:037,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Aniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Benzyl alcohol
Page 35 of 81Page 35 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:032,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Chrysene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Fluorene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Isophorone
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Naphthalene
Page 36 of 81Page 36 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Phenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Pronamide
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/24/17 10:14 03/24/17 21:03Pyridine
35-12554.1 %Surr: 2,4,6-Tribromophenol SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
45-10552.6 %Surr: 2-Fluorobiphenyl SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
35-10561.5 %Surr: 2-Fluorophenol SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
35-10056.8 %Surr: Nitrobenzene-d5 SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
40-10056.2 %Surr: Phenol-d5 SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
30-12561.6 %Surr: p-Terphenyl-d14 SKS04 SW8270D 03/24/17 10:14 03/24/17 21:03
Page 37 of 81Page 37 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-4 Laboratory Sample ID:Sample I.D. 17C0754-04
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 104 03/23/17 15:28 03/28/17 16:34TPH-Semi-Volatiles (DRO)
40-16059.9 %Surr: Pentacosane CVH04 SW8015C 03/23/17 15:28 03/28/17 16:34
Wet Chemistry Analysis
SW7196A CMB<0.20 mg/kg 0.20 104 03/24/17 15:30 03/24/17 15:30Chromium, Hexavalent
Page 38 of 81Page 38 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 105 03/22/17 13:27 03/23/17 13:10Silver
SW6010C 1.96 mg/kg CWO1.00 105 03/22/17 13:27 03/23/17 13:10Arsenic
SW6010C CWO<0.200 mg/kg 0.200 105 03/22/17 13:27 03/23/17 13:10Beryllium
SW6010C 0.234 mg/kg CWO0.200 105 03/22/17 13:27 03/23/17 13:10Cadmium
SW6010C 9.71 mg/kg CWO0.500 105 03/22/17 13:27 03/23/17 13:10Chromium
SW6010C 85.9 mg/kg CWO2.50 105 03/22/17 13:27 03/23/17 13:10Copper
SW7471B 0.016 mg/kg RCV0.008 105 03/22/17 13:27 03/22/17 15:12Mercury
SW6010C 1.87 mg/kg CWO0.500 105 03/22/17 13:27 03/23/17 13:10Nickel
SW6010C 3.09 mg/kg CWO0.500 105 03/22/17 13:27 03/23/17 13:10Lead
SW6010C CWO<5.00 mg/kg 5.00 105 03/22/17 13:27 03/23/17 13:10Antimony
SW6010C CWO<2.50 mg/kg 2.50 105 03/22/17 13:27 03/23/17 13:10Selenium
SW6010C CWO<2.50 mg/kg 2.50 105 03/22/17 13:27 03/23/17 13:10Thallium
SW6010C 12.9 mg/kg CWO0.500 105 03/22/17 13:27 03/23/17 13:10Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 105 03/23/17 10:00 03/24/17 12:53TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 105 03/23/17 10:00 03/24/17 12:54TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 105 03/23/17 10:00 03/24/17 12:54TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 105 03/23/17 10:00 03/24/17 12:54TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 105 03/23/17 10:00 03/24/17 12:54TCLP Chromium
SW7470A RCV<0.008 mg/L 0.008 105 03/23/17 09:00 03/24/17 11:56TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 105 03/23/17 10:00 03/24/17 12:54TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 105 03/23/17 10:00 03/24/17 12:54TCLP Selenium
SW1311 1 # RCV-- 105 03/22/17 15:59 03/23/17 08:33TCLP Extraction Fluid,
Metals
Page 39 of 81Page 39 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.49 mg/kg 0.49 105 03/23/17 14:52 03/23/17 14:52TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:371,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:372,2-Dichloropropane
SW8260B 9.79 ug/kg LAO5.00 105 03/22/17 15:37 03/22/17 15:372-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:372-Chlorotoluene
Page 40 of 81Page 40 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:372-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:374-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:374-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:374-Methyl-2-pentanone (MIBK)
SW8260B 81.3 ug/kg LAO10.0 105 03/22/17 15:37 03/22/17 15:37Acetone
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Benzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Bromoform
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Chloroform
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 105 03/22/17 15:37 03/22/17 15:37Ethanol
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 105 03/22/17 15:37 03/22/17 15:37Ethyl-t-butyl ether (ETBE)
Page 41 of 81Page 41 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Styrene
SW8260B LAO<10.0 ug/kg 10.0 105 03/22/17 15:37 03/22/17 15:37TAA
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37TAEE
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37TAME
SW8260B LAO<100 ug/kg 100 105 03/22/17 15:37 03/22/17 15:37TBA
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Toluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 105 03/22/17 15:37 03/22/17 15:37Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 105 03/22/17 15:37 03/22/17 15:37Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 105 03/22/17 15:37 03/22/17 15:37Xylenes, Total
Page 42 of 81Page 42 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Volatile Organic Compounds by GCMS
80-120104 %Surr: 1,2-Dichloroethane-d4 LAO05 SW8260B 03/22/17 15:37 03/22/17 15:37
85-120101 %Surr: 4-Bromofluorobenzene LAO05 SW8260B 03/22/17 15:37 03/22/17 15:37
78-119104 %Surr: Dibromofluoromethane LAO05 SW8260B 03/22/17 15:37 03/22/17 15:37
85-115103 %Surr: Toluene-d8 LAO05 SW8260B 03/22/17 15:37 03/22/17 15:37
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:371-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Naphthylamine
Page 43 of 81Page 43 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:373,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:373-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:373-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg C 83.3 105 03/24/17 10:14 03/24/17 21:374-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:374-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:377,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Aniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Benzyl alcohol
Page 44 of 81Page 44 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:372,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Chrysene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Fluorene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Isophorone
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Naphthalene
Page 45 of 81Page 45 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Phenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Pronamide
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/24/17 10:14 03/24/17 21:37Pyridine
35-12557.7 %Surr: 2,4,6-Tribromophenol SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
45-10557.5 %Surr: 2-Fluorobiphenyl SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
35-10550.6 %Surr: 2-Fluorophenol SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
35-10060.3 %Surr: Nitrobenzene-d5 SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
40-10060.7 %Surr: Phenol-d5 SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
30-12567.7 %Surr: p-Terphenyl-d14 SKS05 SW8270D 03/24/17 10:14 03/24/17 21:37
Page 46 of 81Page 46 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17C0754
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:15Date/Time Sampled:
RL-S-5 Laboratory Sample ID:Sample I.D. 17C0754-05
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 105 03/23/17 15:28 03/29/17 10:31TPH-Semi-Volatiles (DRO)
40-16073.9 %Surr: Pentacosane CVH05 SW8015C 03/23/17 15:28 03/29/17 10:31
Wet Chemistry Analysis
SW7196A CMB<0.20 mg/kg 0.20 105 03/24/17 15:30 03/24/17 15:30Chromium, Hexavalent
Page 47 of 81Page 47 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Analytical Summary
Preparation Method:
Preparation Method:
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
17C0754-01 BAC0653 SAC0654SW7196A AC70129100 g / 100 mL
17C0754-02 BAC0653 SAC0654SW7196A AC70129100 g / 100 mL
17C0754-03 BAC0653 SAC0654SW7196A AC70129100 g / 100 mL
17C0754-04 BAC0653 SAC0654SW7196A AC70129100 g / 100 mL
17C0754-05 BAC0653 SAC0654SW7196A AC70129100 g / 100 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW1311 MetalsPreparation Method:TCLP Metals by 6000/7000 Series Methods
17C0754-01 BAC0574 SAC0579SW1311 100 g / 2000 mL
17C0754-02 BAC0574 SAC0579SW1311 100 g / 2000 mL
17C0754-03 BAC0574 SAC0579SW1311 100 g / 2000 mL
17C0754-04 BAC0574 SAC0579SW1311 100 g / 2000 mL
17C0754-05 BAC0574 SAC0579SW1311 100 g / 2000 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3010APreparation Method:TCLP Metals by 6000/7000 Series Methods
17C0754-01 BAC0592 SAC0635SW6010C AC7012410.0 mL / 50.0 mL
17C0754-02 BAC0592 SAC0635SW6010C AC7012410.0 mL / 50.0 mL
17C0754-03 BAC0592 SAC0635SW6010C AC7012410.0 mL / 50.0 mL
17C0754-04 BAC0592 SAC0635SW6010C AC7012410.0 mL / 50.0 mL
17C0754-05 BAC0592 SAC0635SW6010C AC7012410.0 mL / 50.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3050BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
17C0754-01 BAC0552 SAC0605SW6010C AC701141.01 g / 50.0 mL
17C0754-01RE1 BAC0552 SAC0636SW6010C AC701241.01 g / 50.0 mL
Page 48 of 81Page 48 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
17C0754-01RE2 BAC0552 SAC0636SW6010C AC701241.01 g / 50.0 mL
17C0754-02 BAC0552 SAC0605SW6010C AC701141.08 g / 50.0 mL
17C0754-03 BAC0552 SAC0605SW6010C AC701141.09 g / 50.0 mL
17C0754-03RE1 BAC0552 SAC0636SW6010C AC701241.09 g / 50.0 mL
17C0754-04 BAC0552 SAC0605SW6010C AC701141.04 g / 50.0 mL
17C0754-05 BAC0552 SAC0605SW6010C AC701141.08 g / 50.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3550CPreparation Method:Semivolatile Organic Compounds by GCMS
17C0754-01 BAC0635 SAC0647SW8270D AC7007330.0 g / 1.00 mL
17C0754-02 BAC0635 SAC0647SW8270D AC7007330.6 g / 1.00 mL
17C0754-03 BAC0635 SAC0647SW8270D AC7007331.5 g / 1.00 mL
17C0754-04 BAC0635 SAC0647SW8270D AC7007330.9 g / 1.00 mL
17C0754-05 BAC0635 SAC0647SW8270D AC7007331.5 g / 1.00 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW5030BPreparation Method:Volatile Organic Compounds by GCMS
17C0754-01 BAC0584 SAC0584SW8260B AC700235.01 g / 5.00 mL
17C0754-02 BAC0584 SAC0584SW8260B AC700235.03 g / 5.00 mL
17C0754-03 BAC0584 SAC0584SW8260B AC700235.00 g / 5.00 mL
17C0754-04 BAC0584 SAC0584SW8260B AC700235.09 g / 5.00 mL
17C0754-05 BAC0584 SAC0584SW8260B AC700235.01 g / 5.00 mL
SW5030BPreparation Method:Volatile Hydrocarbons by GC
17C0754-01 BAC0617 SAC0617SW8015C AC701181.00 g / 5.00 mL
17C0754-02 BAC0617 SAC0617SW8015C AC701181.01 g / 5.00 mL
17C0754-03 BAC0617 SAC0617SW8015C AC701181.06 g / 5.00 mL
17C0754-04 BAC0617 SAC0617SW8015C AC701181.01 g / 5.00 mL
17C0754-05 BAC0617 SAC0617SW8015C AC701181.03 g / 5.00 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW7470APreparation Method:TCLP Metals by 6000/7000 Series Methods
Page 49 of 81Page 49 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
17C0754-01 BAC0580 SAC0638SW7470A AC701221.00 mL / 20.0 mL
17C0754-02 BAC0580 SAC0638SW7470A AC701221.00 mL / 20.0 mL
17C0754-03 BAC0580 SAC0638SW7470A AC701221.00 mL / 20.0 mL
17C0754-04 BAC0580 SAC0638SW7470A AC701221.00 mL / 20.0 mL
17C0754-05 BAC0580 SAC0638SW7470A AC701221.00 mL / 20.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW7471APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
17C0754-01 BAC0538 SAC0556SW7471B AC701080.551 g / 20.0 mL
17C0754-02 BAC0538 SAC0556SW7471B AC701080.570 g / 20.0 mL
17C0754-03 BAC0538 SAC0556SW7471B AC701080.538 g / 20.0 mL
17C0754-04 BAC0538 SAC0556SW7471B AC701080.514 g / 20.0 mL
17C0754-05 BAC0538 SAC0556SW7471B AC701080.558 g / 20.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW8100Preparation Method:Semivolatile Hydrocarbons by GC
17C0754-01 BAC0614 SAC0728SW8015C AC7010450.5 g / 1.00 mL
17C0754-02 BAC0614 SAC0728SW8015C AC7010450.9 g / 1.00 mL
17C0754-03 BAC0614 SAC0728SW8015C AC7010451.8 g / 1.00 mL
17C0754-04 BAC0614 SAC0728SW8015C AC7010450.2 g / 1.00 mL
17C0754-05 BAC0614 SAC0750SW8015C AC7010450.2 g / 1.00 mL
Page 50 of 81Page 50 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0538 - SW7471A
Blank (BAC0538-BLK1) Prepared & Analyzed: 03/22/2017
0.008 mg/kg<0.008 mg/kgMercury
LCS (BAC0538-BS1) Prepared & Analyzed: 03/22/2017
0.008 0.0940 80-12096.1mg/kg0.090 mg/kg mg/kgMercury
LCS Dup (BAC0538-BSD1) Prepared & Analyzed: 03/22/2017
0.008 0.0998 2080-12097.6 7.56mg/kg0.097 mg/kg mg/kgMercury
Matrix Spike (BAC0538-MS1) Prepared & Analyzed: 03/22/2017Source: 17C0728-01
0.008 0.0877 80-120108mg/kg0.094 mg/kg <0.008 mg/kgMercury
Matrix Spike Dup (BAC0538-MSD1) Prepared & Analyzed: 03/22/2017Source: 17C0728-01
0.008 0.0924 2080-120102 0.355mg/kg0.094 mg/kg <0.008 mg/kgMercury
Batch BAC0552 - SW3050B
Blank (BAC0552-BLK1) Prepared: 03/22/2017 Analyzed: 03/23/2017
2.50 mg/kg<2.50 mg/kgSelenium
0.500 mg/kg<0.500 mg/kgLead
0.200 mg/kg<0.200 mg/kgBeryllium
2.50 mg/kg<2.50 mg/kgThallium
0.500 mg/kg<0.500 mg/kgChromium
0.200 mg/kg<0.200 mg/kgCadmium
0.500 mg/kg<0.500 mg/kgNickel
5.00 mg/kg<5.00 mg/kgAntimony
2.50 mg/kg<2.50 mg/kgCopper
1.00 mg/kg<1.00 mg/kgArsenic
0.500 mg/kg<0.500 mg/kgZinc
0.500 mg/kg<0.500 mg/kgSilver
Page 51 of 81Page 51 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0552 - SW3050B
LCS (BAC0552-BS1) Prepared: 03/22/2017 Analyzed: 03/23/2017
2.50 98.0 80-120105mg/kg103 mg/kg mg/kgCopper
0.500 98.0 80-120102mg/kg99.9 mg/kg mg/kgChromium
5.00 98.0 80-12099.2mg/kg97.2 mg/kg mg/kgAntimony
2.50 98.0 80-12096.4mg/kg94.5 mg/kg mg/kgThallium
0.500 98.0 80-120102mg/kg100 mg/kg mg/kgNickel
0.500 98.0 80-120103mg/kg101 mg/kg mg/kgLead
2.50 98.0 80-12098.4mg/kg96.5 mg/kg mg/kgSelenium
0.500 98.0 80-120100mg/kg98.3 mg/kg mg/kgZinc
0.500 4.90 80-12098.8mg/kg4.84 mg/kg mg/kgSilver
0.200 98.0 80-12098.5mg/kg96.6 mg/kg mg/kgBeryllium
0.200 98.0 80-120101mg/kg99.0 mg/kg mg/kgCadmium
1.00 98.0 80-12098.9mg/kg96.9 mg/kg mg/kgArsenic
LCS Dup (BAC0552-BSD1) Prepared: 03/22/2017 Analyzed: 03/23/2017
5.00 98.5 2080-12098.9 0.217mg/kg97.5 mg/kg mg/kgAntimony
0.200 98.5 2080-12099.3 1.31mg/kg97.8 mg/kg mg/kgBeryllium
0.500 98.5 2080-120102 0.414mg/kg101 mg/kg mg/kgLead
1.00 98.5 2080-12098.2 0.144mg/kg96.8 mg/kg mg/kgArsenic
0.500 4.93 2080-120100 1.92mg/kg4.93 mg/kg mg/kgSilver
0.500 98.5 2080-120103 0.835mg/kg101 mg/kg mg/kgNickel
2.50 98.5 2080-12098.0 0.111mg/kg96.6 mg/kg mg/kgSelenium
2.50 98.5 2080-120102 6.13mg/kg100 mg/kg mg/kgThallium
0.500 98.5 2080-120103 1.24mg/kg101 mg/kg mg/kgChromium
0.200 98.5 2080-120102 1.18mg/kg100 mg/kg mg/kgCadmium
0.500 98.5 2080-120101 1.12mg/kg99.5 mg/kg mg/kgZinc
2.50 98.5 2080-120106 1.21mg/kg104 mg/kg mg/kgCopper
Matrix Spike (BAC0552-MS1) Prepared: 03/22/2017 Analyzed: 03/23/2017Source: 17C0728-01
0.500 97.6 75-12588.3mg/kg186 mg/kg 99.6 mg/kgZinc
2.50 97.6 75-125101mg/kg113 mg/kg 15.1 mg/kgCopper
0.500 4.88 75-12597.2mg/kg4.74 mg/kg <0.500 mg/kgSilver
2.50 97.6 75-12593.9mg/kg91.6 mg/kg <2.50 mg/kgThallium
Page 52 of 81Page 52 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0552 - SW3050B
Matrix Spike (BAC0552-MS1) Prepared: 03/22/2017 Analyzed: 03/23/2017Source: 17C0728-01
0.500 97.6 75-12599.5mg/kg101 mg/kg 3.89 mg/kgLead
0.500 97.6 75-12596.6mg/kg108 mg/kg 13.9 mg/kgNickel
1.00 97.6 75-12597.5mg/kg99.2 mg/kg 4.11 mg/kgArsenic
0.200 97.6 75-125101mg/kg99.7 mg/kg 1.23 mg/kgCadmium
0.500 97.6 75-12598.7mg/kg137 mg/kg 40.8 mg/kgChromium
0.200 97.6 75-12599.9mg/kg97.5 mg/kg <0.200 mg/kgBeryllium
5.00 97.6 75-12532.0mg/kg36.2 mg/kg <5.00 mg/kgAntimony M
2.50 97.6 75-12599.4mg/kg97.0 mg/kg <2.50 mg/kgSelenium
Matrix Spike Dup (BAC0552-MSD1) Prepared: 03/22/2017 Analyzed: 03/23/2017Source: 17C0728-01
2.50 98.0 2075-125101 8.03mg/kg99.3 mg/kg <2.50 mg/kgThallium
2.50 98.0 2075-125106 5.06mg/kg119 mg/kg 15.1 mg/kgCopper
0.200 98.0 2075-125109 8.18mg/kg108 mg/kg 1.23 mg/kgCadmium
0.200 98.0 2075-125108 8.35mg/kg106 mg/kg <0.200 mg/kgBeryllium
5.00 98.0 2075-12540.1 20.1mg/kg44.3 mg/kg <5.00 mg/kgAntimony M, P
0.500 98.0 2075-125111 11.2mg/kg113 mg/kg 3.89 mg/kgLead
0.500 98.0 2075-125107 9.43mg/kg119 mg/kg 13.9 mg/kgNickel
0.500 4.90 2075-125104 7.59mg/kg5.12 mg/kg <0.500 mg/kgSilver
1.00 98.0 2075-125110 12.3mg/kg112 mg/kg 4.11 mg/kgArsenic
2.50 98.0 2075-125111 11.1mg/kg108 mg/kg <2.50 mg/kgSelenium
0.500 98.0 2075-12597.1 0.784mg/kg136 mg/kg 40.8 mg/kgChromium
0.500 98.0 2075-12592.2 2.28mg/kg190 mg/kg 99.6 mg/kgZinc
Page 53 of 81Page 53 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0574 - SW1311 Metals
Blank (BAC0574-BLK1) Prepared: 03/22/2017 Analyzed: 03/23/2017
0 #1 #Extraction Fluid, Metals
Batch BAC0580 - SW7470A
Blank (BAC0580-BLK1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.008 mg/L<0.008 mg/LMercury
LCS (BAC0580-BS1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.008 0.0500 80-120106mg/L0.053 mg/L mg/LMercury
LCS Dup (BAC0580-BSD1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.008 0.0500 2080-120107 0.938mg/L0.054 mg/L mg/LMercury
Matrix Spike (BAC0580-MS1) Prepared: 03/23/2017 Analyzed: 03/24/2017Source: 17C0754-01
0.008 0.0500 80-120110mg/L0.055 mg/L <0.008 mg/LMercury
Matrix Spike Dup (BAC0580-MSD1) Prepared: 03/23/2017 Analyzed: 03/24/2017Source: 17C0754-01
0.008 0.0500 2080-120107 2.35mg/L0.054 mg/L <0.008 mg/LMercury
Batch BAC0592 - SW3010A
Blank (BAC0592-BLK1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.100 mg/L<0.100 mg/LArsenic
5.00 mg/L<5.00 mg/LBarium
0.0400 mg/L<0.0400 mg/LCadmium
0.100 mg/L<0.100 mg/LChromium
0.100 mg/L<0.100 mg/LLead
0.250 mg/L<0.250 mg/LSelenium
0.100 mg/L<0.100 mg/LSilver
Page 54 of 81Page 54 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0592 - SW3010A
LCS (BAC0592-BS1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.100 2.50 80-120109mg/L2.73 mg/L mg/LArsenic
5.00 2.50 80-120109mg/L<5.00 mg/L mg/LBarium
0.0400 2.50 80-120107mg/L2.67 mg/L mg/LCadmium
0.100 2.50 80-120104mg/L2.60 mg/L mg/LChromium
0.100 2.50 80-120102mg/L2.55 mg/L mg/LLead
0.250 2.50 80-120103mg/L2.58 mg/L mg/LSelenium
0.100 0.500 80-12099.8mg/L0.499 mg/L mg/LSilver
LCS Dup (BAC0592-BSD1) Prepared: 03/23/2017 Analyzed: 03/24/2017
0.100 2.50 2080-120109 0.657mg/L2.71 mg/L mg/LArsenic
5.00 2.50 2080-120112 2.48mg/L<5.00 mg/L mg/LBarium
0.0400 2.50 2080-120109 1.66mg/L2.71 mg/L mg/LCadmium
0.100 2.50 2080-120106 1.80mg/L2.65 mg/L mg/LChromium
0.100 2.50 2080-120105 2.38mg/L2.62 mg/L mg/LLead
0.250 2.50 2080-120108 4.77mg/L2.71 mg/L mg/LSelenium
0.100 0.500 2080-120104 4.11mg/L0.520 mg/L mg/LSilver
Matrix Spike (BAC0592-MS1) Prepared: 03/23/2017 Analyzed: 03/24/2017Source: 17C0754-01
0.100 2.50 75-125101mg/L2.53 mg/L <0.100 mg/LArsenic
5.00 2.50 75-125107mg/L<5.00 mg/L <5.00 mg/LBarium
0.0400 2.50 75-12598.7mg/L2.47 mg/L <0.0400 mg/LCadmium
0.100 2.50 75-125100mg/L2.51 mg/L <0.100 mg/LChromium
0.100 2.50 75-12596.6mg/L2.42 mg/L <0.100 mg/LLead
0.250 2.50 75-12597.4mg/L2.44 mg/L <0.250 mg/LSelenium
0.100 0.500 75-12592.6mg/L0.463 mg/L <0.100 mg/LSilver
Matrix Spike Dup (BAC0592-MSD1) Prepared: 03/23/2017 Analyzed: 03/24/2017Source: 17C0754-01
0.100 2.50 2075-12596.9 4.49mg/L2.42 mg/L <0.100 mg/LArsenic
5.00 2.50 2075-125106 1.26mg/L<5.00 mg/L <5.00 mg/LBarium
0.0400 2.50 2075-12596.3 2.45mg/L2.41 mg/L <0.0400 mg/LCadmium
0.100 2.50 2075-12596.7 3.71mg/L2.42 mg/L <0.100 mg/LChromium
0.100 2.50 2075-12592.5 4.36mg/L2.31 mg/L <0.100 mg/LLead
0.250 2.50 2075-12592.3 5.44mg/L2.31 mg/L <0.250 mg/LSelenium
Page 55 of 81Page 55 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0592 - SW3010A
Matrix Spike Dup (BAC0592-MSD1) Prepared: 03/23/2017 Analyzed: 03/24/2017Source: 17C0754-01
0.100 0.500 2075-12590.1 2.70mg/L0.451 mg/L <0.100 mg/LSilver
Page 56 of 81Page 56 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0617 - SW5030B
Blank (BAC0617-BLK1) Prepared & Analyzed: 03/23/2017
0.10 mg/kg<0.10 mg/kgTPH-Volatiles (GRO)
LCS (BAC0617-BS1) Prepared & Analyzed: 03/23/2017
0.10 1.00 70-13089.5mg/kg0.90 mg/kg mg/kgTPH-Volatiles (GRO)
Matrix Spike (BAC0617-MS1) Prepared & Analyzed: 03/23/2017Source: 17C0754-01
0.50 5.00 70-13084.4mg/kg4.22 mg/kg <0.50 mg/kgTPH-Volatiles (GRO)
Matrix Spike Dup (BAC0617-MSD1) Prepared & Analyzed: 03/23/2017Source: 17C0754-01
0.50 5.00 2070-13090.2 6.71mg/kg4.51 mg/kg <0.50 mg/kgTPH-Volatiles (GRO)
Page 57 of 81Page 57 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Blank (BAC0584-BLK1) Prepared & Analyzed: 03/22/2017
5.00 ug/kg<5.00 ug/kg1,1,1,2-Tetrachloroethane
5.00 ug/kg<5.00 ug/kg1,1,1-Trichloroethane
5.00 ug/kg<5.00 ug/kg1,1,2,2-Tetrachloroethane
5.00 ug/kg<5.00 ug/kg1,1,2-Trichloroethane
5.00 ug/kg<5.00 ug/kg1,1-Dichloroethane
5.00 ug/kg<5.00 ug/kg1,1-Dichloroethylene
5.00 ug/kg<5.00 ug/kg1,1-Dichloropropene
5.00 ug/kg<5.00 ug/kg1,2,3-Trichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2,3-Trichloropropane
5.00 ug/kg<5.00 ug/kg1,2,4-Trichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2,4-Trimethylbenzene
5.00 ug/kg<5.00 ug/kg1,2-Dibromo-3-chloropropane (DBCP)
5.00 ug/kg<5.00 ug/kg1,2-Dibromoethane (EDB)
5.00 ug/kg<5.00 ug/kg1,2-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2-Dichloroethane
5.00 ug/kg<5.00 ug/kg1,2-Dichloropropane
5.00 ug/kg<5.00 ug/kg1,3,5-Trimethylbenzene
5.00 ug/kg<5.00 ug/kg1,3-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg1,3-Dichloropropane
5.00 ug/kg<5.00 ug/kg1,4-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg2,2-Dichloropropane
5.00 ug/kg<5.00 ug/kg2-Butanone (MEK)
5.00 ug/kg<5.00 ug/kg2-Chlorotoluene
5.00 ug/kg<5.00 ug/kg2-Hexanone (MBK)
5.00 ug/kg<5.00 ug/kg4-Chlorotoluene
5.00 ug/kg<5.00 ug/kg4-Isopropyltoluene
5.00 ug/kg<5.00 ug/kg4-Methyl-2-pentanone (MIBK)
10.0 ug/kg<10.0 ug/kgAcetone
5.00 ug/kg<5.00 ug/kgBenzene
5.00 ug/kg<5.00 ug/kgBromobenzene
5.00 ug/kg<5.00 ug/kgBromochloromethane
Page 58 of 81Page 58 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Blank (BAC0584-BLK1) Prepared & Analyzed: 03/22/2017
5.00 ug/kg<5.00 ug/kgBromodichloromethane
5.00 ug/kg<5.00 ug/kgBromoform
5.00 ug/kg<5.00 ug/kgBromomethane
5.00 ug/kg<5.00 ug/kgCarbon disulfide
5.00 ug/kg<5.00 ug/kgCarbon tetrachloride
5.00 ug/kg<5.00 ug/kgChlorobenzene
5.00 ug/kg<5.00 ug/kgChloroethane
5.00 ug/kg<5.00 ug/kgChloroform
5.00 ug/kg<5.00 ug/kgChloromethane
5.00 ug/kg<5.00 ug/kgcis-1,2-Dichloroethylene
5.00 ug/kg<5.00 ug/kgcis-1,3-Dichloropropene
5.00 ug/kg<5.00 ug/kgDibromochloromethane
5.00 ug/kg<5.00 ug/kgDibromomethane
5.00 ug/kg<5.00 ug/kgDichlorodifluoromethane
5.00 ug/kg<5.00 ug/kgDi-isopropyl ether (DIPE)
80.0 ug/kg<80.0 ug/kgEthanol
5.00 ug/kg<5.00 ug/kgEthylbenzene
25.0 ug/kg<25.0 ug/kgEthyl-t-butyl ether (ETBE)
5.00 ug/kg<5.00 ug/kgHexachlorobutadiene
5.00 ug/kg<5.00 ug/kgIodomethane
5.00 ug/kg<5.00 ug/kgIsopropylbenzene
5.00 ug/kg<5.00 ug/kgm+p-Xylenes
5.00 ug/kg<5.00 ug/kgMethylene chloride
5.00 ug/kg<5.00 ug/kgMethyl-t-butyl ether (MTBE)
5.00 ug/kg<5.00 ug/kgNaphthalene
5.00 ug/kg<5.00 ug/kgn-Butylbenzene
5.00 ug/kg<5.00 ug/kgn-Propylbenzene
5.00 ug/kg<5.00 ug/kgo-Xylene
5.00 ug/kg<5.00 ug/kgsec-Butylbenzene
5.00 ug/kg<5.00 ug/kgStyrene
10.0 ug/kg<10.0 ug/kgTAA
Page 59 of 81Page 59 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Blank (BAC0584-BLK1) Prepared & Analyzed: 03/22/2017
5.00 ug/kg<5.00 ug/kgTAEE
5.00 ug/kg<5.00 ug/kgTAME
100 ug/kg<100 ug/kgTBA
5.00 ug/kg<5.00 ug/kgtert-Butylbenzene
5.00 ug/kg<5.00 ug/kgTetrachloroethylene (PCE)
5.00 ug/kg<5.00 ug/kgToluene
5.00 ug/kg<5.00 ug/kgtrans-1,2-Dichloroethylene
5.00 ug/kg<5.00 ug/kgtrans-1,3-Dichloropropene
5.00 ug/kg<5.00 ug/kgTrichloroethylene
5.00 ug/kg<5.00 ug/kgTrichlorofluoromethane
10.0 ug/kg<10.0 ug/kgVinyl acetate
5.00 ug/kg<5.00 ug/kgVinyl chloride
10.0 ug/kg<10.0 ug/kgXylenes, Total
50.0 80-120Surr: 1,2-Dichloroethane-d4 98.749.3 ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10150.6 ug/kg
50.0 78-119Surr: Dibromofluoromethane 10150.6 ug/kg
50.0 85-115Surr: Toluene-d8 10150.7 ug/kg
LCS (BAC0584-BS1) Prepared & Analyzed: 03/22/2017
5 50.0 75-125104ug/L51.8 ug/L ug/L1,1,1,2-Tetrachloroethane
5 50.0 70-135114ug/L57.0 ug/L ug/L1,1,1-Trichloroethane
5 50.0 55-130100ug/L50.0 ug/L ug/L1,1,2,2-Tetrachloroethane
5 50.0 60-125109ug/L54.7 ug/L ug/L1,1,2-Trichloroethane
5 50.0 75-125117ug/L58.4 ug/L ug/L1,1-Dichloroethane
5 50.0 65-135116ug/L57.8 ug/L ug/L1,1-Dichloroethylene
5 50.0 70-135114ug/L57.1 ug/L ug/L1,1-Dichloropropene
5 50.0 60-135102ug/L50.9 ug/L ug/L1,2,3-Trichlorobenzene
5 50.0 65-13099.0ug/L49.5 ug/L ug/L1,2,3-Trichloropropane
5 50.0 65-130104ug/L52.2 ug/L ug/L1,2,4-Trichlorobenzene
5 50.0 65-135105ug/L52.6 ug/L ug/L1,2,4-Trimethylbenzene
5 50.0 40-13594.9ug/L47.5 ug/L ug/L1,2-Dibromo-3-chloropropane (DBCP)
Page 60 of 81Page 60 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
LCS (BAC0584-BS1) Prepared & Analyzed: 03/22/2017
5 50.0 70-125106ug/L53.2 ug/L ug/L1,2-Dibromoethane (EDB)
5 50.0 75-12097.3ug/L48.6 ug/L ug/L1,2-Dichlorobenzene
5 50.0 70-135103ug/L51.6 ug/L ug/L1,2-Dichloroethane
5 50.0 70-120112ug/L55.9 ug/L ug/L1,2-Dichloropropane
5 50.0 65-135102ug/L51.2 ug/L ug/L1,3,5-Trimethylbenzene
5 50.0 70-125101ug/L50.4 ug/L ug/L1,3-Dichlorobenzene
5 50.0 75-125108ug/L54.0 ug/L ug/L1,3-Dichloropropane
5 50.0 70-125101ug/L50.6 ug/L ug/L1,4-Dichlorobenzene
5 50.0 65-135126ug/L63.2 ug/L ug/L2,2-Dichloropropane
5 50.0 30-160123ug/L61.3 ug/L ug/L2-Butanone (MEK)
5 50.0 70-130104ug/L52.2 ug/L ug/L2-Chlorotoluene
5 50.0 45-145119ug/L59.6 ug/L ug/L2-Hexanone (MBK)
5 50.0 75-125100ug/L50.2 ug/L ug/L4-Chlorotoluene
5 50.0 75-135102ug/L51.1 ug/L ug/L4-Isopropyltoluene
5 50.0 45-145120ug/L59.8 ug/L ug/L4-Methyl-2-pentanone (MIBK)
10 50.0 20-160114ug/L57.0 ug/L ug/LAcetone
5 50.0 75-125116ug/L58.0 ug/L ug/LBenzene
5 50.0 65-120101ug/L50.5 ug/L ug/LBromobenzene
5 50.0 70-125109ug/L54.3 ug/L ug/LBromochloromethane
5 50.0 70-130116ug/L58.2 ug/L ug/LBromodichloromethane
5 50.0 55-135100ug/L50.1 ug/L ug/LBromoform
5 50.0 30-160104ug/L51.9 ug/L ug/LBromomethane
5 50.0 45-160153ug/L76.5 ug/L ug/LCarbon disulfide
5 50.0 65-135106ug/L52.9 ug/L ug/LCarbon tetrachloride
5 50.0 75-125101ug/L50.4 ug/L ug/LChlorobenzene
5 50.0 40-155105ug/L52.5 ug/L ug/LChloroethane
5 50.0 70-125108ug/L54.0 ug/L ug/LChloroform
5 50.0 50-13092.3ug/L46.2 ug/L ug/LChloromethane
5 50.0 65-125110ug/L54.8 ug/L ug/Lcis-1,2-Dichloroethylene
5 50.0 70-125106ug/L53.0 ug/L ug/Lcis-1,3-Dichloropropene
5 50.0 65-130115ug/L57.3 ug/L ug/LDibromochloromethane
Page 61 of 81Page 61 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
LCS (BAC0584-BS1) Prepared & Analyzed: 03/22/2017
5 50.0 75-130112ug/L56.1 ug/L ug/LDibromomethane
5 50.0 35-13587.3ug/L43.7 ug/L ug/LDichlorodifluoromethane
5 50.0 75-125107ug/L53.4 ug/L ug/LEthylbenzene
5 50.0 55-14098.4ug/L49.2 ug/L ug/LHexachlorobutadiene
5 50.0 75-130108ug/L54.0 ug/L ug/LIsopropylbenzene
5 100 80-125105ug/L105 ug/L ug/Lm+p-Xylenes
5 50.0 55-140103ug/L51.6 ug/L ug/LMethylene chloride
5 50.0 65-125117ug/L58.4 ug/L ug/LMethyl-t-butyl ether (MTBE)
5 50.0 40-125106ug/L52.8 ug/L ug/LNaphthalene
5 50.0 65-140105ug/L52.6 ug/L ug/Ln-Butylbenzene
5 50.0 65-135107ug/L53.7 ug/L ug/Ln-Propylbenzene
5 50.0 75-125103ug/L51.5 ug/L ug/Lo-Xylene
5 50.0 65-13099.0ug/L49.5 ug/L ug/Lsec-Butylbenzene
5 50.0 75-125104ug/L52.0 ug/L ug/LStyrene
5 50.0 65-130106ug/L52.8 ug/L ug/Ltert-Butylbenzene
5 50.0 65-140155ug/L77.6 ug/L ug/LTetrachloroethylene (PCE) L
5 50.0 70-125112ug/L55.8 ug/L ug/LToluene
5 50.0 65-135118ug/L58.8 ug/L ug/Ltrans-1,2-Dichloroethylene
5 50.0 65-125119ug/L59.4 ug/L ug/Ltrans-1,3-Dichloropropene
5 50.0 75-125115ug/L57.7 ug/L ug/LTrichloroethylene
5 50.0 25-185101ug/L50.4 ug/L ug/LTrichlorofluoromethane
5 50.0 60-130105ug/L52.3 ug/L ug/LVinyl chloride
50.0 80-120Surr: 1,2-Dichloroethane-d4 95.447.7 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10150.3 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 10250.8 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 10250.8 ug/kg ug/kg
Matrix Spike (BAC0584-MS1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 75-12586.2ug/L43.1 ug/L <5 ug/L1,1,1,2-Tetrachloroethane
5 50.0 70-13595.6ug/L47.8 ug/L <5 ug/L1,1,1-Trichloroethane
5 50.0 55-13080.9ug/L40.4 ug/L <5 ug/L1,1,2,2-Tetrachloroethane
Page 62 of 81Page 62 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Matrix Spike (BAC0584-MS1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 60-12591.9ug/L45.9 ug/L <5 ug/L1,1,2-Trichloroethane
5 50.0 75-125101ug/L50.7 ug/L <5 ug/L1,1-Dichloroethane
5 50.0 65-13593.6ug/L46.8 ug/L <5 ug/L1,1-Dichloroethylene
5 50.0 70-13594.2ug/L47.1 ug/L <5 ug/L1,1-Dichloropropene
5 50.0 60-13559.5ug/L29.8 ug/L <5 ug/L1,2,3-Trichlorobenzene M
5 50.0 65-13075.5ug/L37.8 ug/L <5 ug/L1,2,3-Trichloropropane
5 50.0 65-13060.6ug/L30.3 ug/L <5 ug/L1,2,4-Trichlorobenzene M
5 50.0 65-13580.0ug/L40.0 ug/L <5 ug/L1,2,4-Trimethylbenzene
5 50.0 40-13562.0ug/L31.0 ug/L <5 ug/L1,2-Dibromo-3-chloropropane (DBCP)
5 50.0 70-12584.4ug/L42.2 ug/L <5 ug/L1,2-Dibromoethane (EDB)
5 50.0 75-12071.3ug/L35.7 ug/L <5 ug/L1,2-Dichlorobenzene M
5 50.0 70-13582.6ug/L41.3 ug/L <5 ug/L1,2-Dichloroethane
5 50.0 70-12093.7ug/L46.8 ug/L <5 ug/L1,2-Dichloropropane
5 50.0 65-13578.7ug/L39.3 ug/L <5 ug/L1,3,5-Trimethylbenzene
5 50.0 70-12573.7ug/L36.9 ug/L <5 ug/L1,3-Dichlorobenzene
5 50.0 75-12588.7ug/L44.4 ug/L <5 ug/L1,3-Dichloropropane
5 50.0 70-12575.9ug/L38.0 ug/L <5 ug/L1,4-Dichlorobenzene
5 50.0 65-135105ug/L52.7 ug/L <5 ug/L2,2-Dichloropropane
5 50.0 30-16084.3ug/L42.2 ug/L <5 ug/L2-Butanone (MEK)
5 50.0 70-13082.4ug/L41.2 ug/L <5 ug/L2-Chlorotoluene
5 50.0 45-14575.8ug/L37.9 ug/L <5 ug/L2-Hexanone (MBK)
5 50.0 75-12577.4ug/L38.7 ug/L <5 ug/L4-Chlorotoluene
5 50.0 75-13573.8ug/L36.9 ug/L <5 ug/L4-Isopropyltoluene M
5 50.0 45-14578.9ug/L39.5 ug/L <5 ug/L4-Methyl-2-pentanone (MIBK)
10 50.0 20-16073.4ug/L95.8 ug/L 59.0 ug/LAcetone
5 50.0 75-12593.8ug/L46.9 ug/L <5 ug/LBenzene
5 50.0 65-12079.0ug/L39.5 ug/L <5 ug/LBromobenzene
5 50.0 70-12593.3ug/L46.6 ug/L <5 ug/LBromochloromethane
5 50.0 70-13093.7ug/L46.8 ug/L <5 ug/LBromodichloromethane
5 50.0 55-13578.3ug/L39.2 ug/L <5 ug/LBromoform
5 50.0 30-16078.8ug/L39.4 ug/L <5 ug/LBromomethane
Page 63 of 81Page 63 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Matrix Spike (BAC0584-MS1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 45-160130ug/L65.7 ug/L <5 ug/LCarbon disulfide
5 50.0 65-13587.9ug/L44.0 ug/L <5 ug/LCarbon tetrachloride
5 50.0 75-12581.4ug/L40.7 ug/L <5 ug/LChlorobenzene
5 50.0 40-15583.9ug/L42.0 ug/L <5 ug/LChloroethane
5 50.0 70-12592.3ug/L46.2 ug/L <5 ug/LChloroform
5 50.0 50-13078.2ug/L39.1 ug/L <5 ug/LChloromethane
5 50.0 65-12591.1ug/L45.5 ug/L <5 ug/Lcis-1,2-Dichloroethylene
5 50.0 70-12582.0ug/L41.0 ug/L <5 ug/Lcis-1,3-Dichloropropene
5 50.0 65-13090.8ug/L45.4 ug/L <5 ug/LDibromochloromethane
5 50.0 75-13089.8ug/L44.9 ug/L <5 ug/LDibromomethane
5 50.0 35-13572.9ug/L36.4 ug/L <5 ug/LDichlorodifluoromethane
5 50.0 75-12588.3ug/L44.1 ug/L <5 ug/LEthylbenzene
5 50.0 55-14047.3ug/L23.7 ug/L <5 ug/LHexachlorobutadiene M
5 50.0 75-13088.4ug/L44.2 ug/L <5 ug/LIsopropylbenzene
5 100 80-12585.8ug/L85.8 ug/L <5 ug/Lm+p-Xylenes
5 50.0 55-14089.9ug/L44.9 ug/L <5 ug/LMethylene chloride
5 50.0 65-12591.3ug/L45.7 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 40-12562.9ug/L31.5 ug/L <5 ug/LNaphthalene
5 50.0 65-14072.1ug/L36.0 ug/L <5 ug/Ln-Butylbenzene
5 50.0 65-13583.8ug/L41.9 ug/L <5 ug/Ln-Propylbenzene
5 50.0 75-12583.0ug/L41.5 ug/L <5 ug/Lo-Xylene
5 50.0 65-13074.5ug/L37.3 ug/L <5 ug/Lsec-Butylbenzene
5 50.0 75-12576.5ug/L38.2 ug/L <5 ug/LStyrene
5 50.0 65-13078.5ug/L39.3 ug/L <5 ug/Ltert-Butylbenzene
5 50.0 65-140114ug/L56.8 ug/L <5 ug/LTetrachloroethylene (PCE)
5 50.0 70-12589.5ug/L44.7 ug/L <5 ug/LToluene
5 50.0 65-135100ug/L50.2 ug/L <5 ug/Ltrans-1,2-Dichloroethylene
5 50.0 65-12590.2ug/L45.1 ug/L <5 ug/Ltrans-1,3-Dichloropropene
5 50.0 75-12588.2ug/L44.1 ug/L <5 ug/LTrichloroethylene
5 50.0 25-18583.1ug/L41.5 ug/L <5 ug/LTrichlorofluoromethane
5 50.0 60-13059.4ug/L29.7 ug/L <5 ug/LVinyl chloride M
Page 64 of 81Page 64 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Matrix Spike (BAC0584-MS1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
50.0 80-120Surr: 1,2-Dichloroethane-d4 99.149.5 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10753.5 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 10452.1 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 99.649.8 ug/kg ug/kg
Matrix Spike Dup (BAC0584-MSD1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 3075-12579.1 8.65ug/L39.5 ug/L <5 ug/L1,1,1,2-Tetrachloroethane
5 50.0 3070-13589.5 6.62ug/L44.7 ug/L <5 ug/L1,1,1-Trichloroethane
5 50.0 3055-13073.1 10.1ug/L36.5 ug/L <5 ug/L1,1,2,2-Tetrachloroethane
5 50.0 3060-12583.8 9.21ug/L41.9 ug/L <5 ug/L1,1,2-Trichloroethane
5 50.0 3075-12593.7 7.82ug/L46.8 ug/L <5 ug/L1,1-Dichloroethane
5 50.0 3065-13590.9 2.84ug/L45.5 ug/L <5 ug/L1,1-Dichloroethylene
5 50.0 3070-13589.1 5.63ug/L44.5 ug/L <5 ug/L1,1-Dichloropropene
5 50.0 3060-13551.9 13.8ug/L25.9 ug/L <5 ug/L1,2,3-Trichlorobenzene M
5 50.0 3065-13068.7 9.43ug/L34.4 ug/L <5 ug/L1,2,3-Trichloropropane
5 50.0 3065-13053.2 13.0ug/L26.6 ug/L <5 ug/L1,2,4-Trichlorobenzene M
5 50.0 3065-13573.9 7.95ug/L37.0 ug/L <5 ug/L1,2,4-Trimethylbenzene
5 50.0 3040-13556.9 8.57ug/L28.5 ug/L <5 ug/L1,2-Dibromo-3-chloropropane (DBCP)
5 50.0 3070-12576.4 9.93ug/L38.2 ug/L <5 ug/L1,2-Dibromoethane (EDB)
5 50.0 3075-12066.9 6.44ug/L33.4 ug/L <5 ug/L1,2-Dichlorobenzene M
5 50.0 3070-13579.0 4.47ug/L39.5 ug/L <5 ug/L1,2-Dichloroethane
5 50.0 3070-12090.1 3.89ug/L45.1 ug/L <5 ug/L1,2-Dichloropropane
5 50.0 3065-13573.1 7.29ug/L36.6 ug/L <5 ug/L1,3,5-Trimethylbenzene
5 50.0 3070-12567.7 8.47ug/L33.9 ug/L <5 ug/L1,3-Dichlorobenzene M
5 50.0 3075-12584.2 5.24ug/L42.1 ug/L <5 ug/L1,3-Dichloropropane
5 50.0 3070-12567.8 11.3ug/L33.9 ug/L <5 ug/L1,4-Dichlorobenzene M
5 50.0 3065-13599.0 6.21ug/L49.5 ug/L <5 ug/L2,2-Dichloropropane
5 50.0 3030-16046.3 58.2ug/L23.2 ug/L <5 ug/L2-Butanone (MEK) M
5 50.0 3070-13076.4 7.60ug/L38.2 ug/L <5 ug/L2-Chlorotoluene
5 50.0 3045-14526.0 97.9ug/L13.0 ug/L <5 ug/L2-Hexanone (MBK) M
5 50.0 3075-12571.0 8.73ug/L35.5 ug/L <5 ug/L4-Chlorotoluene M
Page 65 of 81Page 65 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Matrix Spike Dup (BAC0584-MSD1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 3075-13566.5 10.4ug/L33.2 ug/L <5 ug/L4-Isopropyltoluene M
5 50.0 3045-14528.4 94.3ug/L14.2 ug/L <5 ug/L4-Methyl-2-pentanone (MIBK) M
10 50.0 3020-16061.4 6.49ug/L89.7 ug/L 59.0 ug/LAcetone
5 50.0 3075-12591.6 2.41ug/L45.8 ug/L <5 ug/LBenzene
5 50.0 3065-12072.7 8.32ug/L36.4 ug/L <5 ug/LBromobenzene
5 50.0 3070-12583.6 10.9ug/L41.8 ug/L <5 ug/LBromochloromethane
5 50.0 3070-13090.9 3.00ug/L45.4 ug/L <5 ug/LBromodichloromethane
5 50.0 3055-13569.1 12.5ug/L34.5 ug/L <5 ug/LBromoform
5 50.0 3030-16064.2 20.5ug/L32.1 ug/L <5 ug/LBromomethane
5 50.0 3045-16050.1 86.8ug/L25.9 ug/L <5 ug/LCarbon disulfide M
5 50.0 3065-13581.2 7.88ug/L40.6 ug/L <5 ug/LCarbon tetrachloride
5 50.0 3075-12575.7 7.22ug/L37.9 ug/L <5 ug/LChlorobenzene
5 50.0 3040-15582.6 1.65ug/L41.3 ug/L <5 ug/LChloroethane
5 50.0 3070-12587.5 5.39ug/L43.7 ug/L <5 ug/LChloroform
5 50.0 3050-13070.5 10.3ug/L35.2 ug/L <5 ug/LChloromethane
5 50.0 3065-12585.4 6.42ug/L42.7 ug/L <5 ug/Lcis-1,2-Dichloroethylene
5 50.0 3070-12578.9 3.79ug/L39.5 ug/L <5 ug/Lcis-1,3-Dichloropropene
5 50.0 3065-13085.2 6.43ug/L42.6 ug/L <5 ug/LDibromochloromethane
5 50.0 3075-13085.1 5.45ug/L42.5 ug/L <5 ug/LDibromomethane
5 50.0 3035-13571.7 1.62ug/L35.9 ug/L <5 ug/LDichlorodifluoromethane
5 50.0 3075-12581.8 7.58ug/L40.9 ug/L <5 ug/LEthylbenzene
5 50.0 3055-14039.0 19.3ug/L19.5 ug/L <5 ug/LHexachlorobutadiene M
5 50.0 3075-13080.8 9.03ug/L40.4 ug/L <5 ug/LIsopropylbenzene
5 100 3080-12579.2 7.98ug/L79.2 ug/L <5 ug/Lm+p-Xylenes M
5 50.0 3055-14082.8 8.13ug/L41.4 ug/L <5 ug/LMethylene chloride
5 50.0 3065-12587.3 4.48ug/L43.7 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 3040-12555.3 12.8ug/L27.7 ug/L <5 ug/LNaphthalene
5 50.0 3065-14062.8 13.8ug/L31.4 ug/L <5 ug/Ln-Butylbenzene M
5 50.0 3065-13576.8 8.61ug/L38.4 ug/L <5 ug/Ln-Propylbenzene
5 50.0 3075-12579.1 4.82ug/L39.6 ug/L <5 ug/Lo-Xylene
5 50.0 3065-13065.8 12.4ug/L32.9 ug/L <5 ug/Lsec-Butylbenzene
Page 66 of 81Page 66 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0584 - SW5030B
Matrix Spike Dup (BAC0584-MSD1) Prepared & Analyzed: 03/22/2017Source: 17C0754-04
5 50.0 3075-12569.0 10.3ug/L34.5 ug/L <5 ug/LStyrene M
5 50.0 3065-13071.8 8.96ug/L35.9 ug/L <5 ug/Ltert-Butylbenzene
5 50.0 3065-140104 8.81ug/L52.0 ug/L <5 ug/LTetrachloroethylene (PCE)
5 50.0 3070-12586.6 3.32ug/L43.3 ug/L <5 ug/LToluene
5 50.0 3065-13593.8 6.82ug/L46.9 ug/L <5 ug/Ltrans-1,2-Dichloroethylene
5 50.0 3065-12584.9 6.04ug/L42.5 ug/L <5 ug/Ltrans-1,3-Dichloropropene
5 50.0 3075-12588.3 0.111ug/L44.2 ug/L <5 ug/LTrichloroethylene
5 50.0 3025-18579.6 4.29ug/L39.8 ug/L <5 ug/LTrichlorofluoromethane
5 50.0 3060-13055.9 6.00ug/L28.0 ug/L <5 ug/LVinyl chloride M
50.0 80-120Surr: 1,2-Dichloroethane-d4 96.248.1 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10250.9 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 10251.0 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 10150.7 ug/kg ug/kg
Page 67 of 81Page 67 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0635 - SW3550C
Blank (BAC0635-BLK1) Prepared & Analyzed: 03/24/2017
83.3 ug/kg<83.3 ug/kg1,2,4,5-Tetrachlorobenzene
83.3 ug/kg<83.3 ug/kg1,2,4-Trichlorobenzene
83.3 ug/kg<83.3 ug/kg1,2-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1,2-Diphenylhydrazine
83.3 ug/kg<83.3 ug/kg1,3-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1,4-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1-Chloronaphthalene
83.3 ug/kg<83.3 ug/kg1-Naphthylamine
83.3 ug/kg<83.3 ug/kg2,3,4,6-Tetrachlorophenol
83.3 ug/kg<83.3 ug/kg2,4,5-Trichlorophenol
83.3 ug/kg<83.3 ug/kg2,4,6-Trichlorophenol
83.3 ug/kg<83.3 ug/kg2,4-Dichlorophenol
83.3 ug/kg<83.3 ug/kg2,4-Dimethylphenol
83.3 ug/kg<83.3 ug/kg2,4-Dinitrophenol
83.3 ug/kg<83.3 ug/kg2,4-Dinitrotoluene
83.3 ug/kg<83.3 ug/kg2,6-Dichlorophenol
83.3 ug/kg<83.3 ug/kg2,6-Dinitrotoluene
83.3 ug/kg<83.3 ug/kg2-Chloronaphthalene
83.3 ug/kg<83.3 ug/kg2-Chlorophenol
83.3 ug/kg<83.3 ug/kg2-Methylnaphthalene
83.3 ug/kg<83.3 ug/kg2-Naphthylamine
83.3 ug/kg<83.3 ug/kg2-Nitroaniline
83.3 ug/kg<83.3 ug/kg2-Nitrophenol
83.3 ug/kg<83.3 ug/kg3,3'-Dichlorobenzidine
83.3 ug/kg<83.3 ug/kg3-Methylcholanthrene
83.3 ug/kg<83.3 ug/kg3-Nitroaniline
83.3 ug/kg<83.3 ug/kg4,6-Dinitro-2-methylphenol
83.3 ug/kg<83.3 ug/kg4-Aminobiphenyl
83.3 ug/kg<83.3 ug/kg4-Bromophenyl phenyl ether
83.3 ug/kg<83.3 ug/kg4-Chloroaniline
83.3 ug/kg<83.3 ug/kg4-Chlorophenyl phenyl ether
Page 68 of 81Page 68 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0635 - SW3550C
Blank (BAC0635-BLK1) Prepared & Analyzed: 03/24/2017
83.3 ug/kg<83.3 ug/kg4-Nitroaniline
83.3 ug/kg<83.3 ug/kg4-Nitrophenol
83.3 ug/kg<83.3 ug/kg7,12-Dimethylbenz (a) anthracene
83.3 ug/kg<83.3 ug/kgAcenaphthene
83.3 ug/kg<83.3 ug/kgAcenaphthylene
83.3 ug/kg<83.3 ug/kgAcetophenone
83.3 ug/kg<83.3 ug/kgAniline
83.3 ug/kg<83.3 ug/kgAnthracene
83.3 ug/kg<83.3 ug/kgBenzidine
83.3 ug/kg<83.3 ug/kgBenzo (a) anthracene
83.3 ug/kg<83.3 ug/kgBenzo (a) pyrene
83.3 ug/kg<83.3 ug/kgBenzo (b) fluoranthene
83.3 ug/kg<83.3 ug/kgBenzo (g,h,i) perylene
83.3 ug/kg<83.3 ug/kgBenzo (k) fluoranthene
83.3 ug/kg<83.3 ug/kgBenzoic acid
83.3 ug/kg<83.3 ug/kgBenzyl alcohol
83.3 ug/kg<83.3 ug/kgbis (2-Chloroethoxy) methane
83.3 ug/kg<83.3 ug/kgbis (2-Chloroethyl) ether
83.3 ug/kg<83.3 ug/kg2,2'-Oxybis (1-chloropropane)
83.3 ug/kg<83.3 ug/kgbis (2-Ethylhexyl) phthalate
83.3 ug/kg<83.3 ug/kgButyl benzyl phthalate
83.3 ug/kg<83.3 ug/kgChrysene
83.3 ug/kg<83.3 ug/kgDibenz (a,h) anthracene
83.3 ug/kg<83.3 ug/kgDibenz (a,j) acridine
83.3 ug/kg<83.3 ug/kgDibenzofuran
83.3 ug/kg<83.3 ug/kgDiethyl phthalate
83.3 ug/kg<83.3 ug/kgDimethyl phthalate
83.3 ug/kg<83.3 ug/kgDi-n-butyl phthalate
83.3 ug/kg<83.3 ug/kgDi-n-octyl phthalate
83.3 ug/kg<83.3 ug/kgDiphenylamine
83.3 ug/kg<83.3 ug/kgEthyl methanesulfonate
Page 69 of 81Page 69 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0635 - SW3550C
Blank (BAC0635-BLK1) Prepared & Analyzed: 03/24/2017
83.3 ug/kg<83.3 ug/kgFluoranthene
83.3 ug/kg<83.3 ug/kgFluorene
83.3 ug/kg<83.3 ug/kgHexachlorobenzene
83.3 ug/kg<83.3 ug/kgHexachlorobutadiene
83.3 ug/kg<83.3 ug/kgHexachlorocyclopentadiene
83.3 ug/kg<83.3 ug/kgHexachloroethane
83.3 ug/kg<83.3 ug/kgIndeno (1,2,3-cd) pyrene
83.3 ug/kg<83.3 ug/kgIsophorone
83.3 ug/kg<83.3 ug/kgm+p-Cresols
83.3 ug/kg<83.3 ug/kgMethyl methanesulfonate
83.3 ug/kg<83.3 ug/kgNaphthalene
83.3 ug/kg<83.3 ug/kgNitrobenzene
83.3 ug/kg<83.3 ug/kgn-Nitrosodimethylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodi-n-butylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodi-n-propylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodiphenylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosopiperidine
83.3 ug/kg<83.3 ug/kgo+m+p-Cresols
83.3 ug/kg<83.3 ug/kgo-Cresol
83.3 ug/kg<83.3 ug/kgp-(Dimethylamino) azobenzene
83.3 ug/kg<83.3 ug/kgp-Chloro-m-cresol
83.3 ug/kg<83.3 ug/kgPentachloronitrobenzene (quintozene)
83.3 ug/kg<83.3 ug/kgPentachlorophenol
83.3 ug/kg<83.3 ug/kgPhenacetin
83.3 ug/kg<83.3 ug/kgPhenanthrene
83.3 ug/kg<83.3 ug/kgPhenol
83.3 ug/kg<83.3 ug/kgPronamide
83.3 ug/kg<83.3 ug/kgPyrene
83.3 ug/kg<83.3 ug/kgPyridine
3010 35-125Surr: 2,4,6-Tribromophenol 63.91920 ug/kg
1510 45-105Surr: 2-Fluorobiphenyl 66.0993 ug/kg
Page 70 of 81Page 70 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0635 - SW3550C
Blank (BAC0635-BLK1) Prepared & Analyzed: 03/24/2017
3010 35-105Surr: 2-Fluorophenol 71.42150 ug/kg
1510 35-100Surr: Nitrobenzene-d5 68.21030 ug/kg
3010 40-100Surr: Phenol-d5 68.62070 ug/kg
1510 30-125Surr: p-Terphenyl-d14 78.11180 ug/kg
LCS (BAC0635-BS1) Prepared & Analyzed: 03/24/2017
83.3 3330 44-14271.3ug/kg2380 ug/kg ug/kg1,2,4-Trichlorobenzene
83.3 3330 20-12476.0ug/kg2530 ug/kg ug/kg1,4-Dichlorobenzene
83.3 3330 15-14073.6ug/kg2450 ug/kg ug/kg4-Nitrophenol
83.3 3330 45-11076.4ug/kg2550 ug/kg ug/kgAcenaphthene
83.3 3330 40-11593.1ug/kg3100 ug/kg ug/kgn-Nitrosodi-n-propylamine
83.3 3330 25-12082.2ug/kg2740 ug/kg ug/kgPentachlorophenol
83.3 3370 40-10069.1ug/kg2330 ug/kg ug/kgPhenol
83.3 3330 45-12574.2ug/kg2470 ug/kg ug/kgPyrene
3330 35-125Surr: 2,4,6-Tribromophenol 76.72560 ug/kg ug/kg
1670 45-105Surr: 2-Fluorobiphenyl 76.61280 ug/kg ug/kg
3330 35-105Surr: 2-Fluorophenol 79.42650 ug/kg ug/kg
1670 35-100Surr: Nitrobenzene-d5 80.81350 ug/kg ug/kg
3330 40-100Surr: Phenol-d5 82.22740 ug/kg ug/kg
1670 30-125Surr: p-Terphenyl-d14 74.51240 ug/kg ug/kg
Matrix Spike (BAC0635-MS1) Prepared & Analyzed: 03/24/2017Source: 17C0754-05
83.3 3150 44-14254.4ug/kg1720 ug/kg <83.3 ug/kg1,2,4-Trichlorobenzene
83.3 3150 20-12456.1ug/kg1770 ug/kg <83.3 ug/kg1,4-Dichlorobenzene
83.3 3150 15-14058.3ug/kg1840 ug/kg <83.3 ug/kg4-Nitrophenol
83.3 3150 45-11059.5ug/kg1880 ug/kg <83.3 ug/kgAcenaphthene
83.3 3150 40-11578.3ug/kg2470 ug/kg <83.3 ug/kgn-Nitrosodi-n-propylamine
83.3 3150 25-12060.4ug/kg1910 ug/kg <83.3 ug/kgPentachlorophenol
83.3 3190 40-10056.9ug/kg1810 ug/kg <83.3 ug/kgPhenol
83.3 3150 45-12560.3ug/kg1900 ug/kg <83.3 ug/kgPyrene
3150 35-125Surr: 2,4,6-Tribromophenol 61.81950 ug/kg ug/kg
Page 71 of 81Page 71 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0635 - SW3550C
Matrix Spike (BAC0635-MS1) Prepared & Analyzed: 03/24/2017Source: 17C0754-05
1580 45-105Surr: 2-Fluorobiphenyl 58.4922 ug/kg ug/kg
3150 35-105Surr: 2-Fluorophenol 68.62160 ug/kg ug/kg
1580 35-100Surr: Nitrobenzene-d5 64.31010 ug/kg ug/kg
3150 40-100Surr: Phenol-d5 64.92050 ug/kg ug/kg
1580 30-125Surr: p-Terphenyl-d14 60.7958 ug/kg ug/kg
Matrix Spike Dup (BAC0635-MSD1) Prepared & Analyzed: 03/24/2017Source: 17C0754-05
83.3 3260 2044-14235.4 39.4ug/kg1150 ug/kg <83.3 ug/kg1,2,4-Trichlorobenzene M, P
83.3 3260 2020-12436.7 38.8ug/kg1190 ug/kg <83.3 ug/kg1,4-Dichlorobenzene P
83.3 3260 2015-14036.8 42.2ug/kg1200 ug/kg <83.3 ug/kg4-Nitrophenol P
83.3 3260 2045-11035.5 47.4ug/kg1160 ug/kg <83.3 ug/kgAcenaphthene M, P
83.3 3260 2040-11539.6 62.6ug/kg1290 ug/kg <83.3 ug/kgn-Nitrosodi-n-propylamine M, P
83.3 3260 2025-12041.0 35.2ug/kg1330 ug/kg <83.3 ug/kgPentachlorophenol P
83.3 3290 2040-10038.9 34.6ug/kg1280 ug/kg <83.3 ug/kgPhenol M, P
83.3 3260 2045-12544.1 27.9ug/kg1440 ug/kg <83.3 ug/kgPyrene M, P
3260 35-125Surr: 2,4,6-Tribromophenol 42.71390 ug/kg ug/kg
1630 45-105Surr: 2-Fluorobiphenyl 38.0619 ug/kg ug/kg S
3260 35-105Surr: 2-Fluorophenol 45.91500 ug/kg ug/kg
1630 35-100Surr: Nitrobenzene-d5 44.1719 ug/kg ug/kg
3260 40-100Surr: Phenol-d5 46.41510 ug/kg ug/kg
1630 30-125Surr: p-Terphenyl-d14 46.6759 ug/kg ug/kg
Page 72 of 81Page 72 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0614 - SW8100
Blank (BAC0614-BLK1) Prepared: 03/23/2017 Analyzed: 03/28/2017
10.0 mg/kg<10.0 mg/kgTPH-Semi-Volatiles (DRO)
5.00 40-160Surr: Pentacosane 81.44.07 mg/kg
LCS (BAC0614-BS1) Prepared: 03/23/2017 Analyzed: 03/28/2017
10.0 97.7 40-16069.5mg/kg67.8 mg/kg mg/kgTPH-Semi-Volatiles (DRO)
4.96 40-160Surr: Pentacosane 69.13.43 mg/kg mg/kg
Matrix Spike (BAC0614-MS1) Prepared: 03/23/2017 Analyzed: 03/28/2017Source: 17C0808-01
10.0 99.4 40-16064.9mg/kg64.5 mg/kg <10.0 mg/kgTPH-Semi-Volatiles (DRO)
5.05 40-160Surr: Pentacosane 65.33.30 mg/kg mg/kg
Matrix Spike Dup (BAC0614-MSD1) Prepared: 03/23/2017 Analyzed: 03/28/2017Source: 17C0808-01
10.0 98.6 2040-16047.0 32.7mg/kg46.4 mg/kg <10.0 mg/kgTPH-Semi-Volatiles (DRO) P
5.01 40-160Surr: Pentacosane 54.22.72 mg/kg mg/kg
Page 73 of 81Page 73 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Wet Chemistry Analysis - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0653 - No Prep Wet Chem
Blank (BAC0653-BLK1) Prepared & Analyzed: 03/24/2017
0.005 mg/kg<0.005 mg/kgChromium, Hexavalent
LCS (BAC0653-BS1) Prepared & Analyzed: 03/24/2017
0.05 0.100 80-12099.0mg/kg0.10 mg/kg mg/kgChromium, Hexavalent
Matrix Spike (BAC0653-MS1) Prepared & Analyzed: 03/24/2017Source: 17C0754-05
0.20 0.100 80-120mg/kg<0.20 mg/kg <0.20 mg/kgChromium, Hexavalent M
Matrix Spike Dup (BAC0653-MSD1) Prepared & Analyzed: 03/24/2017Source: 17C0754-05
0.20 0.100 2080-120mg/kg<0.20 mg/kg <0.20 mg/kgChromium, Hexavalent M
Page 74 of 81Page 74 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
SW1311 in Solids
Extraction Fluid, Metals VELAP
SW6010C in Non-Potable Water
Arsenic VELAP,WVDEP
Barium VELAP,WVDEP
Cadmium VELAP,WVDEP
Chromium VELAP,WVDEP
Lead VELAP,WVDEP
Selenium VELAP,WVDEP
Silver VELAP,WVDEP
SW6010C in Solids
Antimony VELAP
Arsenic VELAP
Beryllium VELAP
Cadmium VELAP,WVDEP
Chromium VELAP
Copper VELAP
Lead VELAP,WVDEP
Nickel VELAP
Selenium VELAP,WVDEP
Silver VELAP,WVDEP
Thallium VELAP
Zinc VELAP
SW7196A in Solids
Chromium, Hexavalent VELAP
SW7470A in Non-Potable Water
Mercury VELAP,WVDEP
SW7471B in Solids
Mercury VELAP,WVDEP
SW8015C in Solids
TPH-Semi-Volatiles (DRO) VELAP,NC,WVDEP
TPH-Volatiles (GRO) VELAP,NC,WVDEP
SW8260B in Solids
1,1,1,2-Tetrachloroethane NC,VELAP,WVDEP
1,1,1-Trichloroethane NC,VELAP,WVDEP
1,1,2,2-Tetrachloroethane NC,VELAP,WVDEP
Page 75 of 81Page 75 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
1,1,2-Trichloroethane NC,VELAP,WVDEP
1,1-Dichloroethane NC,VELAP,WVDEP
1,1-Dichloroethylene NC,VELAP,WVDEP
1,1-Dichloropropene NC,VELAP,WVDEP
1,2,3-Trichlorobenzene NC,VELAP,WVDEP
1,2,3-Trichloropropane NC,VELAP,WVDEP
1,2,4-Trichlorobenzene NC,VELAP,WVDEP
1,2,4-Trimethylbenzene NC,VELAP,WVDEP
1,2-Dibromo-3-chloropropane (DBCP) NC,VELAP,WVDEP
1,2-Dibromoethane (EDB) NC,VELAP,WVDEP
1,2-Dichlorobenzene NC,VELAP,WVDEP
1,2-Dichloroethane NC,VELAP,WVDEP
1,2-Dichloropropane NC,VELAP,WVDEP
1,3,5-Trimethylbenzene NC,VELAP,WVDEP
1,3-Dichlorobenzene NC,VELAP,WVDEP
1,3-Dichloropropane NC,VELAP,WVDEP
1,4-Dichlorobenzene NC,VELAP,WVDEP
2,2-Dichloropropane NC,VELAP,WVDEP
2-Butanone (MEK) NC,VELAP,WVDEP
2-Chlorotoluene NC,VELAP,WVDEP
2-Hexanone (MBK) NC,VELAP,WVDEP
4-Chlorotoluene NC,VELAP,WVDEP
4-Isopropyltoluene NC,VELAP,WVDEP
4-Methyl-2-pentanone (MIBK) NC,VELAP,WVDEP
Acetone NC,VELAP,WVDEP
Benzene NC,VELAP,WVDEP
Bromobenzene NC,VELAP,WVDEP
Bromochloromethane NC,VELAP,WVDEP
Bromodichloromethane NC,VELAP,WVDEP
Bromoform NC,VELAP,WVDEP
Bromomethane NC,VELAP,WVDEP
Carbon disulfide NC,VELAP,WVDEP
Carbon tetrachloride NC,VELAP,WVDEP
Chlorobenzene NC,VELAP,WVDEP
Chloroethane NC,VELAP,WVDEP
Chloroform NC,VELAP,WVDEP
Chloromethane NC,VELAP,WVDEP
cis-1,2-Dichloroethylene NC,VELAP,WVDEP
Page 76 of 81Page 76 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
cis-1,3-Dichloropropene NC,VELAP,WVDEP
Dibromochloromethane NC,WVDEP
Dibromomethane NC,VELAP,WVDEP
Dichlorodifluoromethane NC,VELAP,WVDEP
Di-isopropyl ether (DIPE) NC,VELAP,WVDEP
Ethanol NC,VELAP,WVDEP
Ethylbenzene NC,VELAP,WVDEP
Ethyl-t-butyl ether (ETBE) NC,VELAP,WVDEP
Hexachlorobutadiene NC,VELAP,WVDEP
Iodomethane NC,VELAP,WVDEP
Isopropylbenzene NC,VELAP,WVDEP
m+p-Xylenes NC,VELAP,WVDEP
Methylene chloride NC,VELAP,WVDEP
Methyl-t-butyl ether (MTBE) NC,VELAP,WVDEP
Naphthalene NC,VELAP,WVDEP
n-Butylbenzene NC,VELAP,WVDEP
n-Propylbenzene NC,VELAP,WVDEP
o-Xylene NC,VELAP,WVDEP
sec-Butylbenzene NC,VELAP,WVDEP
Styrene NC,VELAP,WVDEP
TAA NC,VELAP,WVDEP
TAEE NC,VELAP,WVDEP
TAME NC,VELAP,WVDEP
TBA NC,VELAP,WVDEP
tert-Butylbenzene NC,VELAP,WVDEP
Tetrachloroethylene (PCE) NC,VELAP,WVDEP
Toluene NC,VELAP,WVDEP
trans-1,2-Dichloroethylene NC,VELAP,WVDEP
trans-1,3-Dichloropropene NC,VELAP,WVDEP
Trichloroethylene NC,VELAP,WVDEP
Trichlorofluoromethane NC,VELAP,WVDEP
Vinyl acetate NC,VELAP,WVDEP
Vinyl chloride NC,VELAP,WVDEP
Xylenes, Total NC,VELAP,WVDEP
Dibromofluoromethane VELAP
SW8270D in Solids
1,2,4,5-Tetrachlorobenzene NC,VELAP,WVDEP
Page 77 of 81Page 77 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
1,2,4-Trichlorobenzene NC,VELAP,WVDEP
1,2-Dichlorobenzene NC,VELAP,WVDEP
1,2-Diphenylhydrazine NC,VELAP,WVDEP
1,3-Dichlorobenzene NC,VELAP,WVDEP
1,4-Dichlorobenzene NC,VELAP,WVDEP
1-Chloronaphthalene NC,VELAP,WVDEP
1-Naphthylamine NC,VELAP,WVDEP
2,3,4,6-Tetrachlorophenol NC,VELAP,WVDEP
2,4,5-Trichlorophenol NC,VELAP,WVDEP
2,4,6-Trichlorophenol NC,VELAP,WVDEP
2,4-Dichlorophenol NC,VELAP,WVDEP
2,4-Dimethylphenol NC,VELAP,WVDEP
2,4-Dinitrophenol NC,VELAP,WVDEP
2,4-Dinitrotoluene NC,VELAP,WVDEP
2,6-Dichlorophenol NC,VELAP,WVDEP
2,6-Dinitrotoluene NC,VELAP,WVDEP
2-Chloronaphthalene NC,VELAP,WVDEP
2-Chlorophenol NC,VELAP,WVDEP
2-Methylnaphthalene NC,VELAP,WVDEP
2-Naphthylamine NC,VELAP,WVDEP
2-Nitroaniline NC,VELAP,WVDEP
2-Nitrophenol NC,VELAP,WVDEP
3-Methylcholanthrene NC,VELAP,WVDEP
3-Nitroaniline NC,VELAP,WVDEP
4,6-Dinitro-2-methylphenol NC,VELAP,WVDEP
4-Aminobiphenyl NC,VELAP,WVDEP
4-Bromophenyl phenyl ether NC,VELAP,WVDEP
4-Chloroaniline NC,VELAP,WVDEP
4-Chlorophenyl phenyl ether NC,VELAP,WVDEP
4-Nitroaniline NC,VELAP,WVDEP
4-Nitrophenol NC,VELAP,WVDEP
7,12-Dimethylbenz (a) anthracene NC,VELAP,WVDEP
Acenaphthene NC,VELAP,WVDEP
Acenaphthylene NC,VELAP,WVDEP
Acetophenone NC,VELAP,WVDEP
Aniline NC,VELAP,WVDEP
Anthracene NC,VELAP,WVDEP
Benzidine NC,VELAP,WVDEP
Page 78 of 81Page 78 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Benzo (a) anthracene NC,VELAP,WVDEP
Benzo (a) pyrene NC,VELAP,WVDEP
Benzo (b) fluoranthene NC,VELAP,WVDEP
Benzo (g,h,i) perylene NC,VELAP,WVDEP
Benzo (k) fluoranthene NC,VELAP,WVDEP
Benzoic acid NC,VELAP,WVDEP
Benzyl alcohol NC,VELAP,WVDEP
bis (2-Chloroethoxy) methane NC,VELAP,WVDEP
bis (2-Chloroethyl) ether NC,VELAP,WVDEP
2,2'-Oxybis (1-chloropropane) NC,VELAP,WVDEP
bis (2-Ethylhexyl) phthalate NC,VELAP,WVDEP
Butyl benzyl phthalate NC,VELAP,WVDEP
Chrysene NC,VELAP,WVDEP
Dibenz (a,h) anthracene NC,VELAP,WVDEP
Dibenz (a,j) acridine NC,VELAP,WVDEP
Dibenzofuran NC,VELAP,WVDEP
Diethyl phthalate NC,VELAP,WVDEP
Dimethyl phthalate NC,VELAP,WVDEP
Di-n-butyl phthalate NC,VELAP,WVDEP
Di-n-octyl phthalate NC,VELAP,WVDEP
Diphenylamine NC,VELAP,WVDEP
Ethyl methanesulfonate NC,VELAP,WVDEP
Fluoranthene NC,VELAP,WVDEP
Fluorene NC,VELAP,WVDEP
Hexachlorobenzene NC,VELAP,WVDEP
Hexachlorobutadiene NC,VELAP,WVDEP
Hexachlorocyclopentadiene NC,VELAP,WVDEP
Hexachloroethane NC,VELAP,WVDEP
Indeno (1,2,3-cd) pyrene NC,VELAP,WVDEP
Isophorone NC,VELAP,WVDEP
m+p-Cresols NC,VELAP,WVDEP
Methyl methanesulfonate NC,VELAP,WVDEP
Naphthalene NC,VELAP,WVDEP
Nitrobenzene NC,VELAP,WVDEP
n-Nitrosodimethylamine NC,VELAP,WVDEP
n-Nitrosodi-n-butylamine NC,VELAP,WVDEP
n-Nitrosodi-n-propylamine NC,VELAP,WVDEP
n-Nitrosodiphenylamine NC,VELAP,WVDEP
Page 79 of 81Page 79 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
n-Nitrosopiperidine NC,VELAP,WVDEP
o+m+p-Cresols NC,VELAP,WVDEP
o-Cresol NC,VELAP,WVDEP
p-(Dimethylamino) azobenzene NC,VELAP,WVDEP
p-Chloro-m-cresol NC,VELAP,WVDEP
Pentachloronitrobenzene (quintozene) NC,WVDEP
Pentachlorophenol NC,VELAP,WVDEP
Phenacetin NC,VELAP,WVDEP
Phenanthrene NC,VELAP,WVDEP
Phenol NC,VELAP,WVDEP
Pronamide NC,VELAP,WVDEP
Pyrene NC,VELAP,WVDEP
Pyridine NC,VELAP,WVDEP
Code Description Lab Number Expires
341 12/31/2017Maryland DE Drinking WaterMdDOE
495 12/31/2017North Carolina DENRNC
001 10/31/2017NELAC-PennsylvaniaPADEP
460021 06/15/2017NELAC-Virginia Certificate #8886VELAP
350 11/30/2017West Virginia DEPWVDEP
Page 80 of 81Page 80 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Summary of Data Qualifiers
C Continuing calibarion verification response for this analyte is outside specifications.
L LCS recovery is outside of established acceptance limits
M Matrix spike recovery is outside established acceptance limits
P Duplicate analysis does not meet the acceptance criteria for precision
S Surrogate recovery was outside acceptance criteria
Relative Percent DifferenceRPD
QualifersQual
Denotes sample was re-analyzed-RE
Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F.
TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library .
A TIC spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations are estimated
and are calculated using an internal standard response factor of 1.
PCBs, Total Total PCBs are defined as the sum of detected Aroclors 1016, 1221, 1232, 1248, 1254, 1260, 1262, and 1268.
Page 81 of 81Page 81 of 83
Page 82 of 83
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/29/2017 16:36
COR WPP Feeder Channel Sediment Testing
Final Report
Samples Received at: 0.20°C
How were samples received?
NA
Sample Conditions Checklist
NA
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Walk In
Were Custody Seals used? If so, were they received intact?
Are the custody papers filled out completely and correctly?
Do all bottle labels agree with custody papers?
Is the temperature blank or representative sample within acceptable limits? (above freezing to 6°C) or received on ice and
recently taken?
Are all samples within holding time for requested laboratory tests?
Is a sufficient amount of sample provided to perform the tests included?
Are all samples in appropriate containers for the analyses requested?
Were volatile organic containers received?
Are all volatile organic and TOX containers free of headspace?
Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011, EPA504, EPA8260, EPA624,
EPA8015 GRO, EPA8021, EPA524, and RSK-175.
Are all samples received appropriately preserved? Note that metals containers do not require field preservation but lab
preservation may delay analysis.
Page 83 of 83
1941 Reymet Road l Richmond, Virginia 23237 l Tel: (804)-358-8295 Fax: (804)-358-8297
Laboratory Order ID 17C0845
Certificate of Analysis
Client Name:
Enclosed are the results of analyses for samples received by the laboratory on 03/24/2017 12:07. If you
have any questions concerning this report, please feel free to contact the laboratory.
Sincerely,
Ted Soyars
Laboratory Manager
Richmond, VA 23235
9030 Stony Point Parkway, Suite 220
Purchase Order:
46510-003Project Number:
Date Issued:
Date Received:
Submitted To:
Client Site I.D.:
March 31, 2017 15:28
March 24, 2017 12:07Whitman, Requardt & Associates, LLP - Richmond
Joe Felton
End Notes:
The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.
Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen,
temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely
short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler
included in the Certificate of Analysis are done so at the client�s request and are not included in the laboratory�s fields of certification
nor have they been audited for adherence to a reference method or procedure.
The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified.
For a complete list of the Laboratory�s NELAC certified parameters please contact customer service.
This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air
Water & Soil Laboratories, Inc.
COR Water Purification Plant Feeder Channel
Final Report
Page 1 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
ANALYTICAL REPORT FOR SAMPLES
Laboratory Order ID 17C0845
MatrixSample ID Laboratory ID Date Sampled Date Received
RL-S-7A+7B 17C0845-01 03/24/2017 12:07Soil 03/23/2017 13:00
RL-S-6A+6B 17C0845-02 03/24/2017 12:07Soil 03/23/2017 13:45
RL-S-51A+51B 17C0845-03 03/24/2017 12:07Soil 03/23/2017 14:20
RL-S-52A+52B 17C0845-04 03/24/2017 12:07Soil 03/23/2017 14:45
RL-S-53A+53B 17C0845-05 03/24/2017 12:07Soil 03/23/2017 15:15
PSB-1 17C0845-06 03/24/2017 12:07Soil 03/23/2017 16:30
PSB-2 17C0845-07 03/24/2017 12:07Soil 03/23/2017 16:55
PSB-3 17C0845-08 03/24/2017 12:07Soil 03/23/2017 17:35
Page 2 of 109Page 2 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 101 03/27/17 08:50 03/27/17 13:26Silver
SW6010C 1.35 mg/kg CWO1.00 101 03/27/17 08:50 03/27/17 13:26Arsenic
SW6010C CWO<0.200 mg/kg 0.200 101 03/27/17 08:50 03/27/17 13:26Beryllium
SW6010C 0.299 mg/kg CWO0.200 101 03/27/17 08:50 03/27/17 13:26Cadmium
SW6010C 7.55 mg/kg CWO0.500 101 03/27/17 08:50 03/27/17 13:26Chromium
SW6010C 29.6 mg/kg CWO2.50 101 03/27/17 08:50 03/27/17 13:26Copper
SW7471B 0.024 mg/kg RCV0.008 101 03/27/17 08:20 03/27/17 11:32Mercury
SW6010C 2.61 mg/kg CWO0.500 101 03/27/17 08:50 03/27/17 13:26Nickel
SW6010C 2.42 mg/kg CWO0.500 101 03/27/17 08:50 03/27/17 13:26Lead
SW6010C CWO<5.00 mg/kg 5.00 101 03/27/17 08:50 03/27/17 13:26Antimony
SW6010C CWO<2.50 mg/kg 2.50 101 03/27/17 08:50 03/27/17 13:26Selenium
SW6010C CWO<2.50 mg/kg 2.50 101 03/27/17 08:50 03/27/17 13:26Thallium
SW6010C 28.5 mg/kg CWO0.500 101 03/27/17 08:50 03/27/17 13:26Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 101 03/28/17 09:54 03/28/17 14:43TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 101 03/28/17 09:54 03/28/17 14:44TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 101 03/28/17 09:54 03/28/17 14:44TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 101 03/28/17 09:54 03/28/17 14:44TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 101 03/28/17 09:54 03/28/17 14:44TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 101 03/28/17 09:30 03/28/17 14:12TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 101 03/28/17 09:54 03/28/17 14:44TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 101 03/28/17 09:54 03/28/17 14:44TCLP Selenium
SW1311 1 # BG-- 101 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 3 of 109Page 3 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.47 mg/kg 0.47 101 03/27/17 13:00 03/27/17 13:00TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:091,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:092,2-Dichloropropane
SW8260B 9.95 ug/kg LAO5.00 101 03/28/17 16:09 03/28/17 16:092-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:092-Chlorotoluene
Page 4 of 109Page 4 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:092-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:094-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:094-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:094-Methyl-2-pentanone (MIBK)
SW8260B LAO<10.0 ug/kg 10.0 101 03/28/17 16:09 03/28/17 16:09Acetone
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Benzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Bromoform
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Chloroform
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 101 03/28/17 16:09 03/28/17 16:09Ethanol
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 101 03/28/17 16:09 03/28/17 16:09Ethyl-t-butyl ether (ETBE)
Page 5 of 109Page 5 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Styrene
SW8260B LAO<10.0 ug/kg 10.0 101 03/28/17 16:09 03/28/17 16:09TAA
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09TAEE
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09TAME
SW8260B LAO<100 ug/kg 100 101 03/28/17 16:09 03/28/17 16:09TBA
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Toluene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 101 03/28/17 16:09 03/28/17 16:09Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 101 03/28/17 16:09 03/28/17 16:09Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 101 03/28/17 16:09 03/28/17 16:09Xylenes, Total
Page 6 of 109Page 6 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Volatile Organic Compounds by GCMS
80-12094.3 %Surr: 1,2-Dichloroethane-d4 LAO01 SW8260B 03/28/17 16:09 03/28/17 16:09
85-12099.5 %Surr: 4-Bromofluorobenzene LAO01 SW8260B 03/28/17 16:09 03/28/17 16:09
78-11992.2 %Surr: Dibromofluoromethane LAO01 SW8260B 03/28/17 16:09 03/28/17 16:09
85-115101 %Surr: Toluene-d8 LAO01 SW8260B 03/28/17 16:09 03/28/17 16:09
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:351-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Naphthylamine
Page 7 of 109Page 7 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:353,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:353-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:353-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:354-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:357,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Acenaphthylene
SW8270D 114 ug/kg SKS83.3 101 03/28/17 09:03 03/29/17 00:35Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Aniline
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Benzyl alcohol
Page 8 of 109Page 8 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:352,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Chrysene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Fluorene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 101 03/28/17 09:03 03/29/17 00:35Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Isophorone
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Naphthalene
Page 9 of 109Page 9 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Phenol
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Pronamide
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Pyrene
SW8270D SKS<83.3 ug/kg 83.3 101 03/28/17 09:03 03/29/17 00:35Pyridine
35-12547.1 %Surr: 2,4,6-Tribromophenol SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
45-10546.7 %Surr: 2-Fluorobiphenyl SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
35-10557.6 %Surr: 2-Fluorophenol SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
35-10053.1 %Surr: Nitrobenzene-d5 SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
40-10056.5 %Surr: Phenol-d5 SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
30-12568.0 %Surr: p-Terphenyl-d14 SKS01 SW8270D 03/28/17 09:03 03/29/17 00:35
Page 10 of 109Page 10 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:00Date/Time Sampled:
RL-S-7A+7B Laboratory Sample ID:Sample I.D. 17C0845-01
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 101 03/27/17 13:33 03/29/17 15:21TPH-Semi-Volatiles (DRO)
40-16051.4 %Surr: Pentacosane CVH01 SW8015C 03/27/17 13:33 03/29/17 15:21
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 101 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 11 of 109Page 11 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 102 03/27/17 08:50 03/27/17 13:30Silver
SW6010C 1.25 mg/kg CWO1.00 102RE1 03/27/17 08:50 03/27/17 14:18Arsenic
SW6010C CWO<0.200 mg/kg 0.200 102 03/27/17 08:50 03/27/17 13:30Beryllium
SW6010C <0.200 mg/kg CWO0.200 102 03/27/17 08:50 03/27/17 13:30Cadmium
SW6010C 7.17 mg/kg CWO0.500 102 03/27/17 08:50 03/27/17 13:30Chromium
SW6010C 19.3 mg/kg CWO2.50 102 03/27/17 08:50 03/27/17 13:30Copper
SW7471B 0.019 mg/kg RCV0.008 102 03/27/17 08:20 03/27/17 11:34Mercury
SW6010C 1.51 mg/kg CWO0.500 102 03/27/17 08:50 03/27/17 13:30Nickel
SW6010C 1.56 mg/kg CWO0.500 102 03/27/17 08:50 03/27/17 13:30Lead
SW6010C CWO<5.00 mg/kg 5.00 102 03/27/17 08:50 03/27/17 13:30Antimony
SW6010C CWO<2.50 mg/kg 2.50 102 03/27/17 08:50 03/27/17 13:30Selenium
SW6010C CWO<2.50 mg/kg 2.50 102 03/27/17 08:50 03/27/17 13:30Thallium
SW6010C 12.9 mg/kg CWO0.500 102 03/27/17 08:50 03/27/17 13:30Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 102 03/28/17 09:54 03/28/17 14:45TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 102 03/28/17 09:54 03/28/17 14:45TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 102 03/28/17 09:54 03/28/17 14:45TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 102 03/28/17 09:54 03/28/17 14:45TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 102 03/28/17 09:54 03/28/17 14:45TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 102 03/28/17 09:30 03/28/17 14:14TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 102 03/28/17 09:54 03/28/17 14:45TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 102 03/28/17 09:54 03/28/17 14:45TCLP Selenium
SW1311 1 # BG-- 102 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 12 of 109Page 12 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.44 mg/kg 0.44 102 03/27/17 13:23 03/27/17 13:23TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:321,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:322,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:322-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:322-Chlorotoluene
Page 13 of 109Page 13 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:322-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:324-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:324-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:324-Methyl-2-pentanone (MIBK)
SW8260B 18.3 ug/kg LAOC 10.0 102 03/28/17 16:32 03/28/17 16:32Acetone
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Benzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Bromoform
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Chloroform
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 102 03/28/17 16:32 03/28/17 16:32Ethanol
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 102 03/28/17 16:32 03/28/17 16:32Ethyl-t-butyl ether (ETBE)
Page 14 of 109Page 14 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Styrene
SW8260B LAO<10.0 ug/kg 10.0 102 03/28/17 16:32 03/28/17 16:32TAA
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32TAEE
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32TAME
SW8260B LAO<100 ug/kg 100 102 03/28/17 16:32 03/28/17 16:32TBA
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Toluene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 102 03/28/17 16:32 03/28/17 16:32Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 102 03/28/17 16:32 03/28/17 16:32Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 102 03/28/17 16:32 03/28/17 16:32Xylenes, Total
Page 15 of 109Page 15 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Volatile Organic Compounds by GCMS
80-12098.4 %Surr: 1,2-Dichloroethane-d4 LAO02 SW8260B 03/28/17 16:32 03/28/17 16:32
85-12097.8 %Surr: 4-Bromofluorobenzene LAO02 SW8260B 03/28/17 16:32 03/28/17 16:32
78-11995.5 %Surr: Dibromofluoromethane LAO02 SW8260B 03/28/17 16:32 03/28/17 16:32
85-115103 %Surr: Toluene-d8 LAO02 SW8260B 03/28/17 16:32 03/28/17 16:32
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:101-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Naphthylamine
Page 16 of 109Page 16 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:103,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:103-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:103-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:104-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:107,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Aniline
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Benzyl alcohol
Page 17 of 109Page 17 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:102,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Chrysene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Fluorene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 102 03/28/17 09:03 03/29/17 01:10Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Isophorone
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Naphthalene
Page 18 of 109Page 18 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Phenol
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Pronamide
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Pyrene
SW8270D SKS<83.3 ug/kg 83.3 102 03/28/17 09:03 03/29/17 01:10Pyridine
35-12543.7 %Surr: 2,4,6-Tribromophenol SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
45-10546.1 %Surr: 2-Fluorobiphenyl SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
35-10542.1 %Surr: 2-Fluorophenol SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
35-10049.8 %Surr: Nitrobenzene-d5 SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
40-10052.3 %Surr: Phenol-d5 SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
30-12569.7 %Surr: p-Terphenyl-d14 SKS02 SW8270D 03/28/17 09:03 03/29/17 01:10
Page 19 of 109Page 19 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 13:45Date/Time Sampled:
RL-S-6A+6B Laboratory Sample ID:Sample I.D. 17C0845-02
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C 11.4 mg/kg CVH10.0 102 03/27/17 13:33 03/29/17 15:47TPH-Semi-Volatiles (DRO)
40-16090.0 %Surr: Pentacosane CVH02 SW8015C 03/27/17 13:33 03/29/17 15:47
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 102 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 20 of 109Page 20 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 103 03/27/17 08:50 03/27/17 13:32Silver
SW6010C 2.66 mg/kg CWO1.00 103 03/27/17 08:50 03/27/17 13:32Arsenic
SW6010C CWO<0.200 mg/kg 0.200 103 03/27/17 08:50 03/27/17 13:32Beryllium
SW6010C 0.423 mg/kg CWO0.200 103 03/27/17 08:50 03/27/17 13:32Cadmium
SW6010C 11.7 mg/kg CWO0.500 103 03/27/17 08:50 03/27/17 13:32Chromium
SW6010C 69.2 mg/kg CWO2.50 103 03/27/17 08:50 03/27/17 13:32Copper
SW7471B 0.031 mg/kg RCV0.008 103 03/27/17 08:20 03/27/17 11:36Mercury
SW6010C 2.71 mg/kg CWO0.500 103 03/27/17 08:50 03/27/17 13:32Nickel
SW6010C 4.48 mg/kg CWO0.500 103 03/27/17 08:50 03/27/17 13:32Lead
SW6010C CWO<5.00 mg/kg 5.00 103 03/27/17 08:50 03/27/17 13:32Antimony
SW6010C CWO<2.50 mg/kg 2.50 103 03/27/17 08:50 03/27/17 13:32Selenium
SW6010C CWO<2.50 mg/kg 2.50 103 03/27/17 08:50 03/27/17 13:32Thallium
SW6010C 21.8 mg/kg CWO0.500 103 03/27/17 08:50 03/27/17 13:32Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 103 03/28/17 09:54 03/28/17 14:47TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 103 03/28/17 09:54 03/28/17 14:47TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 103 03/28/17 09:54 03/28/17 14:47TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 103 03/28/17 09:54 03/28/17 14:47TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 103 03/28/17 09:54 03/28/17 14:47TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 103 03/28/17 09:30 03/28/17 14:17TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 103 03/28/17 09:54 03/28/17 14:47TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 103 03/28/17 09:54 03/28/17 14:47TCLP Selenium
SW1311 1 # BG-- 103 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 21 of 109Page 21 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.40 mg/kg 0.40 103 03/27/17 13:45 03/27/17 13:45TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:561,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:562,2-Dichloropropane
SW8260B 7.04 ug/kg LAO5.00 103 03/28/17 16:56 03/28/17 16:562-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:562-Chlorotoluene
Page 22 of 109Page 22 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:562-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:564-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:564-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:564-Methyl-2-pentanone (MIBK)
SW8260B 59.0 ug/kg LAOC 10.0 103 03/28/17 16:56 03/28/17 16:56Acetone
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Benzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Bromoform
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Chloroform
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 103 03/28/17 16:56 03/28/17 16:56Ethanol
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 103 03/28/17 16:56 03/28/17 16:56Ethyl-t-butyl ether (ETBE)
Page 23 of 109Page 23 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Styrene
SW8260B LAO<10.0 ug/kg 10.0 103 03/28/17 16:56 03/28/17 16:56TAA
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56TAEE
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56TAME
SW8260B LAO<100 ug/kg 100 103 03/28/17 16:56 03/28/17 16:56TBA
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Toluene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 103 03/28/17 16:56 03/28/17 16:56Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 103 03/28/17 16:56 03/28/17 16:56Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 103 03/28/17 16:56 03/28/17 16:56Xylenes, Total
Page 24 of 109Page 24 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Volatile Organic Compounds by GCMS
80-12097.1 %Surr: 1,2-Dichloroethane-d4 LAO03 SW8260B 03/28/17 16:56 03/28/17 16:56
85-12097.7 %Surr: 4-Bromofluorobenzene LAO03 SW8260B 03/28/17 16:56 03/28/17 16:56
78-11994.5 %Surr: Dibromofluoromethane LAO03 SW8260B 03/28/17 16:56 03/28/17 16:56
85-115102 %Surr: Toluene-d8 LAO03 SW8260B 03/28/17 16:56 03/28/17 16:56
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:441-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Naphthylamine
Page 25 of 109Page 25 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:443,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:443-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:443-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:444-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:447,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Aniline
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Benzyl alcohol
Page 26 of 109Page 26 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:442,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Chrysene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Fluorene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 103 03/28/17 09:03 03/29/17 01:44Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Isophorone
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Naphthalene
Page 27 of 109Page 27 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Phenol
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Pronamide
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Pyrene
SW8270D SKS<83.3 ug/kg 83.3 103 03/28/17 09:03 03/29/17 01:44Pyridine
35-12550.8 %Surr: 2,4,6-Tribromophenol SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
45-10546.1 %Surr: 2-Fluorobiphenyl SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
35-10553.4 %Surr: 2-Fluorophenol SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
35-10051.3 %Surr: Nitrobenzene-d5 SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
40-10052.0 %Surr: Phenol-d5 SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
30-12576.9 %Surr: p-Terphenyl-d14 SKS03 SW8270D 03/28/17 09:03 03/29/17 01:44
Page 28 of 109Page 28 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:20Date/Time Sampled:
RL-S-51A+51B Laboratory Sample ID:Sample I.D. 17C0845-03
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 103 03/27/17 13:33 03/29/17 16:14TPH-Semi-Volatiles (DRO)
40-16067.7 %Surr: Pentacosane CVH03 SW8015C 03/27/17 13:33 03/29/17 16:14
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 103 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 29 of 109Page 29 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 104 03/27/17 08:50 03/27/17 13:33Silver
SW6010C CWO<1.00 mg/kg 1.00 104 03/27/17 08:50 03/27/17 13:33Arsenic
SW6010C CWO<0.200 mg/kg 0.200 104 03/27/17 08:50 03/27/17 13:33Beryllium
SW6010C CWO<0.200 mg/kg 0.200 104 03/27/17 08:50 03/27/17 13:33Cadmium
SW6010C 8.09 mg/kg CWO0.500 104 03/27/17 08:50 03/27/17 13:33Chromium
SW6010C 12.1 mg/kg CWO2.50 104 03/27/17 08:50 03/27/17 13:33Copper
SW7471B RCV<0.008 mg/kg 0.008 104 03/27/17 08:20 03/27/17 11:38Mercury
SW6010C 0.963 mg/kg CWO0.500 104 03/27/17 08:50 03/27/17 13:33Nickel
SW6010C 0.635 mg/kg CWO0.500 104 03/27/17 08:50 03/27/17 13:33Lead
SW6010C CWO<5.00 mg/kg 5.00 104 03/27/17 08:50 03/27/17 13:33Antimony
SW6010C CWO<2.50 mg/kg 2.50 104 03/27/17 08:50 03/27/17 13:33Selenium
SW6010C CWO<2.50 mg/kg 2.50 104 03/27/17 08:50 03/27/17 13:33Thallium
SW6010C 8.74 mg/kg CWO0.500 104 03/27/17 08:50 03/27/17 13:33Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 104 03/28/17 09:54 03/28/17 14:48TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 104 03/28/17 09:54 03/28/17 14:49TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 104 03/28/17 09:54 03/28/17 14:49TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 104 03/28/17 09:54 03/28/17 14:49TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 104 03/28/17 09:54 03/28/17 14:49TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 104 03/28/17 09:30 03/28/17 14:24TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 104 03/28/17 09:54 03/28/17 14:49TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 104 03/28/17 09:54 03/28/17 14:49TCLP Selenium
SW1311 1 # BG-- 104 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 30 of 109Page 30 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.50 mg/kg 0.50 104 03/28/17 14:27 03/28/17 14:27TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:191,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:192,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:192-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:192-Chlorotoluene
Page 31 of 109Page 31 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:192-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:194-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:194-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:194-Methyl-2-pentanone (MIBK)
SW8260B 28.7 ug/kg LAOC 10.0 104 03/28/17 17:19 03/28/17 17:19Acetone
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Benzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Bromoform
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Chloroform
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 104 03/28/17 17:19 03/28/17 17:19Ethanol
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 104 03/28/17 17:19 03/28/17 17:19Ethyl-t-butyl ether (ETBE)
Page 32 of 109Page 32 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Styrene
SW8260B LAO<10.0 ug/kg 10.0 104 03/28/17 17:19 03/28/17 17:19TAA
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19TAEE
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19TAME
SW8260B LAO<100 ug/kg 100 104 03/28/17 17:19 03/28/17 17:19TBA
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Toluene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 104 03/28/17 17:19 03/28/17 17:19Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 104 03/28/17 17:19 03/28/17 17:19Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 104 03/28/17 17:19 03/28/17 17:19Xylenes, Total
Page 33 of 109Page 33 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Volatile Organic Compounds by GCMS
80-120102 %Surr: 1,2-Dichloroethane-d4 LAO04 SW8260B 03/28/17 17:19 03/28/17 17:19
85-120100 %Surr: 4-Bromofluorobenzene LAO04 SW8260B 03/28/17 17:19 03/28/17 17:19
78-11995.7 %Surr: Dibromofluoromethane LAO04 SW8260B 03/28/17 17:19 03/28/17 17:19
85-115101 %Surr: Toluene-d8 LAO04 SW8260B 03/28/17 17:19 03/28/17 17:19
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:181-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Naphthylamine
Page 34 of 109Page 34 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:183,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:183-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:183-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:184-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:187,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Aniline
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Benzyl alcohol
Page 35 of 109Page 35 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:182,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Chrysene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Fluorene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 104 03/28/17 09:03 03/29/17 02:18Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Isophorone
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Naphthalene
Page 36 of 109Page 36 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Phenol
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Pronamide
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Pyrene
SW8270D SKS<83.3 ug/kg 83.3 104 03/28/17 09:03 03/29/17 02:18Pyridine
35-12543.7 %Surr: 2,4,6-Tribromophenol SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
45-10546.4 %Surr: 2-Fluorobiphenyl SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
35-10560.3 %Surr: 2-Fluorophenol SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
35-10051.3 %Surr: Nitrobenzene-d5 SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
40-10054.0 %Surr: Phenol-d5 SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
30-12569.1 %Surr: p-Terphenyl-d14 SKS04 SW8270D 03/28/17 09:03 03/29/17 02:18
Page 37 of 109Page 37 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 14:45Date/Time Sampled:
RL-S-52A+52B Laboratory Sample ID:Sample I.D. 17C0845-04
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 104 03/27/17 13:33 03/29/17 16:40TPH-Semi-Volatiles (DRO)
40-16068.5 %Surr: Pentacosane CVH04 SW8015C 03/27/17 13:33 03/29/17 16:40
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 104 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 38 of 109Page 38 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 105 03/27/17 08:50 03/27/17 13:34Silver
SW6010C 1.99 mg/kg CWO1.00 105 03/27/17 08:50 03/27/17 13:34Arsenic
SW6010C CWO<0.200 mg/kg 0.200 105 03/27/17 08:50 03/27/17 13:34Beryllium
SW6010C 0.214 mg/kg CWO0.200 105 03/27/17 08:50 03/27/17 13:34Cadmium
SW6010C 8.05 mg/kg CWO0.500 105 03/27/17 08:50 03/27/17 13:34Chromium
SW6010C 51.6 mg/kg CWO2.50 105 03/27/17 08:50 03/27/17 13:34Copper
SW7471B 0.014 mg/kg RCV0.008 105 03/27/17 08:20 03/27/17 11:46Mercury
SW6010C 2.22 mg/kg CWO0.500 105 03/27/17 08:50 03/27/17 13:34Nickel
SW6010C 2.85 mg/kg CWO0.500 105 03/27/17 08:50 03/27/17 13:34Lead
SW6010C CWO<5.00 mg/kg 5.00 105 03/27/17 08:50 03/27/17 13:34Antimony
SW6010C CWO<2.50 mg/kg 2.50 105 03/27/17 08:50 03/27/17 13:34Selenium
SW6010C CWO<2.50 mg/kg 2.50 105 03/27/17 08:50 03/27/17 13:34Thallium
SW6010C 13.8 mg/kg CWO0.500 105 03/27/17 08:50 03/27/17 13:34Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 105 03/28/17 09:54 03/28/17 14:56TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 105 03/28/17 09:54 03/28/17 14:57TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 105 03/28/17 09:54 03/28/17 14:57TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 105 03/28/17 09:54 03/28/17 14:57TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 105 03/28/17 09:54 03/28/17 14:57TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 105 03/28/17 09:30 03/28/17 14:26TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 105 03/28/17 09:54 03/28/17 14:57TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 105 03/28/17 09:54 03/28/17 14:57TCLP Selenium
SW1311 1 # BG-- 105 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 39 of 109Page 39 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.49 mg/kg 0.49 105 03/28/17 14:50 03/28/17 14:50TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:431,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:432,2-Dichloropropane
SW8260B 5.56 ug/kg LAO5.00 105 03/28/17 17:43 03/28/17 17:432-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:432-Chlorotoluene
Page 40 of 109Page 40 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:432-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:434-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:434-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:434-Methyl-2-pentanone (MIBK)
SW8260B 30.0 ug/kg LAOC 10.0 105 03/28/17 17:43 03/28/17 17:43Acetone
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Benzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Bromoform
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Chloroform
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 105 03/28/17 17:43 03/28/17 17:43Ethanol
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 105 03/28/17 17:43 03/28/17 17:43Ethyl-t-butyl ether (ETBE)
Page 41 of 109Page 41 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Styrene
SW8260B LAO<10.0 ug/kg 10.0 105 03/28/17 17:43 03/28/17 17:43TAA
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43TAEE
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43TAME
SW8260B LAO<100 ug/kg 100 105 03/28/17 17:43 03/28/17 17:43TBA
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Toluene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 105 03/28/17 17:43 03/28/17 17:43Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 105 03/28/17 17:43 03/28/17 17:43Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 105 03/28/17 17:43 03/28/17 17:43Xylenes, Total
Page 42 of 109Page 42 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Volatile Organic Compounds by GCMS
80-120104 %Surr: 1,2-Dichloroethane-d4 LAO05 SW8260B 03/28/17 17:43 03/28/17 17:43
85-12098.3 %Surr: 4-Bromofluorobenzene LAO05 SW8260B 03/28/17 17:43 03/28/17 17:43
78-11993.6 %Surr: Dibromofluoromethane LAO05 SW8260B 03/28/17 17:43 03/28/17 17:43
85-115102 %Surr: Toluene-d8 LAO05 SW8260B 03/28/17 17:43 03/28/17 17:43
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:521-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Naphthylamine
Page 43 of 109Page 43 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:523,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:523-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:523-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:524-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:527,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Aniline
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Benzyl alcohol
Page 44 of 109Page 44 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:522,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Chrysene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Fluorene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 105 03/28/17 09:03 03/29/17 02:52Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Isophorone
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Naphthalene
Page 45 of 109Page 45 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Phenol
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Pronamide
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Pyrene
SW8270D SKS<83.3 ug/kg 83.3 105 03/28/17 09:03 03/29/17 02:52Pyridine
35-12541.8 %Surr: 2,4,6-Tribromophenol SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
45-10552.5 %Surr: 2-Fluorobiphenyl SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
35-10563.8 %Surr: 2-Fluorophenol SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
35-10054.8 %Surr: Nitrobenzene-d5 SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
40-10054.9 %Surr: Phenol-d5 SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
30-12565.6 %Surr: p-Terphenyl-d14 SKS05 SW8270D 03/28/17 09:03 03/29/17 02:52
Page 46 of 109Page 46 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 15:15Date/Time Sampled:
RL-S-53A+53B Laboratory Sample ID:Sample I.D. 17C0845-05
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 105 03/27/17 13:33 03/29/17 17:07TPH-Semi-Volatiles (DRO)
40-16070.8 %Surr: Pentacosane CVH05 SW8015C 03/27/17 13:33 03/29/17 17:07
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 105 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 47 of 109Page 47 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 106 03/27/17 08:50 03/27/17 13:36Silver
SW6010C 2.36 mg/kg CWO1.00 106 03/27/17 08:50 03/27/17 13:36Arsenic
SW6010C CWO<0.200 mg/kg 0.200 106 03/27/17 08:50 03/27/17 13:36Beryllium
SW6010C 0.584 mg/kg CWO0.200 106 03/27/17 08:50 03/27/17 13:36Cadmium
SW6010C 12.8 mg/kg CWO0.500 106 03/27/17 08:50 03/27/17 13:36Chromium
SW6010C 18.4 mg/kg CWO2.50 106 03/27/17 08:50 03/27/17 13:36Copper
SW7471B 0.025 mg/kg RCV0.008 106 03/27/17 08:20 03/27/17 11:48Mercury
SW6010C 4.56 mg/kg CWO0.500 106 03/27/17 08:50 03/27/17 13:36Nickel
SW6010C 4.32 mg/kg CWO0.500 106 03/27/17 08:50 03/27/17 13:36Lead
SW6010C CWO<5.00 mg/kg 5.00 106 03/27/17 08:50 03/27/17 13:36Antimony
SW6010C CWO<2.50 mg/kg 2.50 106 03/27/17 08:50 03/27/17 13:36Selenium
SW6010C CWO<2.50 mg/kg 2.50 106 03/27/17 08:50 03/27/17 13:36Thallium
SW6010C 29.1 mg/kg CWO0.500 106 03/27/17 08:50 03/27/17 13:36Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 106 03/28/17 09:54 03/28/17 14:58TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 106 03/28/17 09:54 03/28/17 14:58TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 106 03/28/17 09:54 03/28/17 14:58TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 106 03/28/17 09:54 03/28/17 14:58TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 106 03/28/17 09:54 03/28/17 14:58TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 106 03/28/17 09:30 03/28/17 14:29TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 106 03/28/17 09:54 03/28/17 14:58TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 106 03/28/17 09:54 03/28/17 14:58TCLP Selenium
SW1311 1 # BG-- 106 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 48 of 109Page 48 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.49 mg/kg 0.49 106 03/28/17 15:13 03/28/17 15:13TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:061,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:062,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:062-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:062-Chlorotoluene
Page 49 of 109Page 49 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:062-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:064-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:064-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:064-Methyl-2-pentanone (MIBK)
SW8260B 21.3 ug/kg LAOC 10.0 106 03/28/17 18:06 03/28/17 18:06Acetone
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Benzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Bromoform
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Chloroform
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 106 03/28/17 18:06 03/28/17 18:06Ethanol
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 106 03/28/17 18:06 03/28/17 18:06Ethyl-t-butyl ether (ETBE)
Page 50 of 109Page 50 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Styrene
SW8260B LAO<10.0 ug/kg 10.0 106 03/28/17 18:06 03/28/17 18:06TAA
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06TAEE
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06TAME
SW8260B LAO<100 ug/kg 100 106 03/28/17 18:06 03/28/17 18:06TBA
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Toluene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 106 03/28/17 18:06 03/28/17 18:06Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 106 03/28/17 18:06 03/28/17 18:06Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 106 03/28/17 18:06 03/28/17 18:06Xylenes, Total
Page 51 of 109Page 51 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Volatile Organic Compounds by GCMS
80-12099.4 %Surr: 1,2-Dichloroethane-d4 LAO06 SW8260B 03/28/17 18:06 03/28/17 18:06
85-12098.3 %Surr: 4-Bromofluorobenzene LAO06 SW8260B 03/28/17 18:06 03/28/17 18:06
78-11996.6 %Surr: Dibromofluoromethane LAO06 SW8260B 03/28/17 18:06 03/28/17 18:06
85-115103 %Surr: Toluene-d8 LAO06 SW8260B 03/28/17 18:06 03/28/17 18:06
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:261-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Naphthylamine
Page 52 of 109Page 52 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:263,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:263-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:263-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:264-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:267,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Aniline
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Anthracene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzidine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Benzyl alcohol
Page 53 of 109Page 53 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:262,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Chrysene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Fluorene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 106 03/28/17 09:03 03/29/17 03:26Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Isophorone
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Naphthalene
Page 54 of 109Page 54 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Phenol
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Pronamide
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Pyrene
SW8270D SKS<83.3 ug/kg 83.3 106 03/28/17 09:03 03/29/17 03:26Pyridine
35-12540.2 %Surr: 2,4,6-Tribromophenol SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
45-10543.4 %Surr: 2-Fluorobiphenyl S SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
35-10556.1 %Surr: 2-Fluorophenol SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
35-10047.5 %Surr: Nitrobenzene-d5 SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
40-10049.7 %Surr: Phenol-d5 SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
30-12560.8 %Surr: p-Terphenyl-d14 SKS06 SW8270D 03/28/17 09:03 03/29/17 03:26
Page 55 of 109Page 55 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:30Date/Time Sampled:
PSB-1 Laboratory Sample ID:Sample I.D. 17C0845-06
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 106 03/27/17 13:33 03/29/17 17:33TPH-Semi-Volatiles (DRO)
40-16068.6 %Surr: Pentacosane CVH06 SW8015C 03/27/17 13:33 03/29/17 17:33
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 106 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 56 of 109Page 56 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 107 03/27/17 08:50 03/27/17 13:44Silver
SW6010C 2.10 mg/kg CWO1.00 107 03/27/17 08:50 03/27/17 13:44Arsenic
SW6010C CWO<0.200 mg/kg 0.200 107 03/27/17 08:50 03/27/17 13:44Beryllium
SW6010C 0.904 mg/kg CWO0.200 107 03/27/17 08:50 03/27/17 13:44Cadmium
SW6010C 10.7 mg/kg CWO0.500 107 03/27/17 08:50 03/27/17 13:44Chromium
SW6010C 43.3 mg/kg CWO2.50 107 03/27/17 08:50 03/27/17 13:44Copper
SW7471B 0.036 mg/kg RCV0.008 107 03/27/17 08:20 03/27/17 11:50Mercury
SW6010C 6.06 mg/kg CWO0.500 107 03/27/17 08:50 03/27/17 13:44Nickel
SW6010C 8.32 mg/kg CWO0.500 107 03/27/17 08:50 03/27/17 13:44Lead
SW6010C CWO<5.00 mg/kg 5.00 107 03/27/17 08:50 03/27/17 13:44Antimony
SW6010C CWO<2.50 mg/kg 2.50 107 03/27/17 08:50 03/27/17 13:44Selenium
SW6010C CWO<2.50 mg/kg 2.50 107 03/27/17 08:50 03/27/17 13:44Thallium
SW6010C 40.7 mg/kg CWO0.500 107 03/27/17 08:50 03/27/17 13:44Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 107 03/28/17 09:54 03/28/17 15:00TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 107 03/28/17 09:54 03/28/17 15:00TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 107 03/28/17 09:54 03/28/17 15:00TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 107 03/28/17 09:54 03/28/17 15:00TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 107 03/28/17 09:54 03/28/17 15:00TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 107 03/28/17 09:30 03/28/17 14:31TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 107 03/28/17 09:54 03/28/17 15:00TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 107 03/28/17 09:54 03/28/17 15:00TCLP Selenium
SW1311 1 # BG-- 107 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 57 of 109Page 57 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.41 mg/kg 0.41 107 03/28/17 15:35 03/28/17 15:35TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:301,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:302,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:302-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:302-Chlorotoluene
Page 58 of 109Page 58 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:302-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:304-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:304-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:304-Methyl-2-pentanone (MIBK)
SW8260B 15.4 ug/kg LAOC 10.0 107 03/28/17 18:30 03/28/17 18:30Acetone
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Benzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Bromoform
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Chloroform
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 107 03/28/17 18:30 03/28/17 18:30Ethanol
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 107 03/28/17 18:30 03/28/17 18:30Ethyl-t-butyl ether (ETBE)
Page 59 of 109Page 59 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Styrene
SW8260B LAO<10.0 ug/kg 10.0 107 03/28/17 18:30 03/28/17 18:30TAA
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30TAEE
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30TAME
SW8260B LAO<100 ug/kg 100 107 03/28/17 18:30 03/28/17 18:30TBA
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Toluene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 107 03/28/17 18:30 03/28/17 18:30Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 107 03/28/17 18:30 03/28/17 18:30Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 107 03/28/17 18:30 03/28/17 18:30Xylenes, Total
Page 60 of 109Page 60 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Volatile Organic Compounds by GCMS
80-120102 %Surr: 1,2-Dichloroethane-d4 LAO07 SW8260B 03/28/17 18:30 03/28/17 18:30
85-12097.4 %Surr: 4-Bromofluorobenzene LAO07 SW8260B 03/28/17 18:30 03/28/17 18:30
78-11998.7 %Surr: Dibromofluoromethane LAO07 SW8260B 03/28/17 18:30 03/28/17 18:30
85-11599.2 %Surr: Toluene-d8 LAO07 SW8260B 03/28/17 18:30 03/28/17 18:30
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:001-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Naphthylamine
Page 61 of 109Page 61 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:003,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:003-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:003-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:004-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:007,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Aniline
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Anthracene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzidine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Benzyl alcohol
Page 62 of 109Page 62 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:002,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Chrysene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Fluorene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 107 03/28/17 09:03 03/29/17 04:00Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Isophorone
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Naphthalene
Page 63 of 109Page 63 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Phenol
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Pronamide
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Pyrene
SW8270D SKS<83.3 ug/kg 83.3 107 03/28/17 09:03 03/29/17 04:00Pyridine
35-12556.1 %Surr: 2,4,6-Tribromophenol SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
45-10551.3 %Surr: 2-Fluorobiphenyl SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
35-10556.8 %Surr: 2-Fluorophenol SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
35-10054.2 %Surr: Nitrobenzene-d5 SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
40-10056.8 %Surr: Phenol-d5 SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
30-12577.1 %Surr: p-Terphenyl-d14 SKS07 SW8270D 03/28/17 09:03 03/29/17 04:00
Page 64 of 109Page 64 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 16:55Date/Time Sampled:
PSB-2 Laboratory Sample ID:Sample I.D. 17C0845-07
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 107 03/27/17 13:33 03/29/17 18:00TPH-Semi-Volatiles (DRO)
40-16052.4 %Surr: Pentacosane CVH07 SW8015C 03/27/17 13:33 03/29/17 18:00
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 107 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 65 of 109Page 65 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Metals (Total) by EPA 6000/7000 Series Methods
SW6010C CWO<0.500 mg/kg 0.500 108 03/27/17 08:50 03/27/17 13:46Silver
SW6010C 3.27 mg/kg CWO1.00 108 03/27/17 08:50 03/27/17 13:46Arsenic
SW6010C CWO<0.200 mg/kg 0.200 108 03/27/17 08:50 03/27/17 13:46Beryllium
SW6010C 1.22 mg/kg CWO0.200 108 03/27/17 08:50 03/27/17 13:46Cadmium
SW6010C 15.5 mg/kg CWO0.500 108 03/27/17 08:50 03/27/17 13:46Chromium
SW6010C 62.7 mg/kg CWO2.50 108 03/27/17 08:50 03/27/17 13:46Copper
SW7471B 0.086 mg/kg RCV0.008 108 03/27/17 08:20 03/27/17 11:52Mercury
SW6010C 8.69 mg/kg CWO0.500 108 03/27/17 08:50 03/27/17 13:46Nickel
SW6010C 11.1 mg/kg CWO0.500 108 03/27/17 08:50 03/27/17 13:46Lead
SW6010C CWO<5.00 mg/kg 5.00 108 03/27/17 08:50 03/27/17 13:46Antimony
SW6010C CWO<2.50 mg/kg 2.50 108 03/27/17 08:50 03/27/17 13:46Selenium
SW6010C CWO<2.50 mg/kg 2.50 108 03/27/17 08:50 03/27/17 13:46Thallium
SW6010C 56.2 mg/kg CWO0.500 108 03/27/17 08:50 03/27/17 13:46Zinc
TCLP Metals by 6000/7000 Series Methods
SW6010C CWO<0.100 mg/L 0.100 108 03/28/17 09:54 03/28/17 15:02TCLP Silver
SW6010C CWO<0.100 mg/L 0.100 108 03/28/17 09:54 03/28/17 15:02TCLP Arsenic
SW6010C CWO<5.00 mg/L 5.00 108 03/28/17 09:54 03/28/17 15:02TCLP Barium
SW6010C CWO<0.0400 mg/L 0.0400 108 03/28/17 09:54 03/28/17 15:02TCLP Cadmium
SW6010C CWO<0.100 mg/L 0.100 108 03/28/17 09:54 03/28/17 15:02TCLP Chromium
SW7470A MWL<0.008 mg/L 0.008 108 03/28/17 09:30 03/28/17 14:33TCLP Mercury
SW6010C CWO<0.100 mg/L 0.100 108 03/28/17 09:54 03/28/17 15:02TCLP Lead
SW6010C CWO<0.250 mg/L 0.250 108 03/28/17 09:54 03/28/17 15:02TCLP Selenium
SW1311 1 # BG-- 108 03/27/17 15:56 03/28/17 10:05TCLP Extraction Fluid,
Metals
Page 66 of 109Page 66 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Volatile Hydrocarbons by GC
SW8015C CL<0.50 mg/kg 0.50 108 03/28/17 15:58 03/28/17 15:58TPH-Volatiles (GRO)
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1,1,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1,1-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1,2,2-Tetrachloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1,2-Trichloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,1-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2,3-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2,3-Trichloropropane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2,4-Trichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2,4-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2-Dibromo-3-chloropropane
(DBCP)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2-Dibromoethane (EDB)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2-Dichloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,3,5-Trimethylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,3-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,3-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:531,4-Dichlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:532,2-Dichloropropane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:532-Butanone (MEK)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:532-Chlorotoluene
Page 67 of 109Page 67 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:532-Hexanone (MBK)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:534-Chlorotoluene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:534-Isopropyltoluene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:534-Methyl-2-pentanone (MIBK)
SW8260B 22.3 ug/kg LAOC 10.0 108 03/28/17 18:53 03/28/17 18:53Acetone
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Benzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Bromobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Bromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Bromodichloromethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Bromoform
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Bromomethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Carbon disulfide
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Carbon tetrachloride
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Chlorobenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Chloroethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Chloroform
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Chloromethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53cis-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53cis-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Dibromochloromethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Dibromomethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Dichlorodifluoromethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Di-isopropyl ether (DIPE)
SW8260B LAO<80.0 ug/kg 80.0 108 03/28/17 18:53 03/28/17 18:53Ethanol
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Ethylbenzene
SW8260B LAO<25.0 ug/kg 25.0 108 03/28/17 18:53 03/28/17 18:53Ethyl-t-butyl ether (ETBE)
Page 68 of 109Page 68 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Volatile Organic Compounds by GCMS
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Hexachlorobutadiene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Iodomethane
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Isopropylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53m+p-Xylenes
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Methylene chloride
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Methyl-t-butyl ether (MTBE)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Naphthalene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53n-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53n-Propylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53o-Xylene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53sec-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Styrene
SW8260B LAO<10.0 ug/kg 10.0 108 03/28/17 18:53 03/28/17 18:53TAA
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53TAEE
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53TAME
SW8260B LAO<100 ug/kg 100 108 03/28/17 18:53 03/28/17 18:53TBA
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53tert-Butylbenzene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Tetrachloroethylene (PCE)
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Toluene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53trans-1,2-Dichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53trans-1,3-Dichloropropene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Trichloroethylene
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Trichlorofluoromethane
SW8260B LAO<10.0 ug/kg 10.0 108 03/28/17 18:53 03/28/17 18:53Vinyl acetate
SW8260B LAO<5.00 ug/kg 5.00 108 03/28/17 18:53 03/28/17 18:53Vinyl chloride
SW8260B LAO<10.0 ug/kg 10.0 108 03/28/17 18:53 03/28/17 18:53Xylenes, Total
Page 69 of 109Page 69 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Volatile Organic Compounds by GCMS
80-12095.7 %Surr: 1,2-Dichloroethane-d4 LAO08 SW8260B 03/28/17 18:53 03/28/17 18:53
85-12099.1 %Surr: 4-Bromofluorobenzene LAO08 SW8260B 03/28/17 18:53 03/28/17 18:53
78-11995.7 %Surr: Dibromofluoromethane LAO08 SW8260B 03/28/17 18:53 03/28/17 18:53
85-11599.9 %Surr: Toluene-d8 LAO08 SW8260B 03/28/17 18:53 03/28/17 18:53
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,2,4,5-Tetrachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,2,4-Trichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,2-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,2-Diphenylhydrazine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,3-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341,4-Dichlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:341-Naphthylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,3,4,6-Tetrachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4,5-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4,6-Trichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4-Dimethylphenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4-Dinitrophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,4-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,6-Dichlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,6-Dinitrotoluene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Chloronaphthalene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Chlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Methylnaphthalene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Naphthylamine
Page 70 of 109Page 70 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:343,3'-Dichlorobenzidine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:343-Methylcholanthrene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:343-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344,6-Dinitro-2-methylphenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Aminobiphenyl
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Bromophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Chloroaniline
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Chlorophenyl phenyl ether
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Nitroaniline
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:344-Nitrophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:347,12-Dimethylbenz (a)
anthracene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Acenaphthene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Acenaphthylene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Acetophenone
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Aniline
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Anthracene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzidine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzo (a) anthracene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzo (a) pyrene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzo (b) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzo (g,h,i) perylene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzo (k) fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzoic acid
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Benzyl alcohol
Page 71 of 109Page 71 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34bis (2-Chloroethoxy) methane
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34bis (2-Chloroethyl) ether
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:342,2'-Oxybis
(1-chloropropane)
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34bis (2-Ethylhexyl) phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Butyl benzyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Chrysene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Dibenz (a,h) anthracene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Dibenz (a,j) acridine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Dibenzofuran
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Diethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Dimethyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Di-n-butyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Di-n-octyl phthalate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Diphenylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Ethyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Fluoranthene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Fluorene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Hexachlorobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Hexachlorobutadiene
SW8270D SKS<83.3 ug/kg C 83.3 108 03/28/17 09:03 03/29/17 04:34Hexachlorocyclopentadiene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Hexachloroethane
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Indeno (1,2,3-cd) pyrene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Isophorone
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Methyl methanesulfonate
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Naphthalene
Page 72 of 109Page 72 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Semivolatile Organic Compounds by GCMS
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Nitrobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34n-Nitrosodimethylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34n-Nitrosodi-n-butylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34n-Nitrosodi-n-propylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34n-Nitrosodiphenylamine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34n-Nitrosopiperidine
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34o+m+p-Cresols
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34o-Cresol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34p-(Dimethylamino)
azobenzene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34p-Chloro-m-cresol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Pentachloronitrobenzene
(quintozene)
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Pentachlorophenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Phenacetin
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Phenanthrene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Phenol
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Pronamide
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Pyrene
SW8270D SKS<83.3 ug/kg 83.3 108 03/28/17 09:03 03/29/17 04:34Pyridine
35-12559.4 %Surr: 2,4,6-Tribromophenol SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
45-10560.4 %Surr: 2-Fluorobiphenyl SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
35-10567.8 %Surr: 2-Fluorophenol SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
35-10063.7 %Surr: Nitrobenzene-d5 SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
40-10066.8 %Surr: Phenol-d5 SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
30-12585.3 %Surr: p-Terphenyl-d14 SKS08 SW8270D 03/28/17 09:03 03/29/17 04:34
Page 73 of 109Page 73 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Laboratory Order ID: 17C0845
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/23/2017 17:35Date/Time Sampled:
PSB-3 Laboratory Sample ID:Sample I.D. 17C0845-08
Analytical Results
Semivolatile Hydrocarbons by GC
SW8015C CVH<10.0 mg/kg 10.0 108 03/27/17 13:33 03/29/17 18:26TPH-Semi-Volatiles (DRO)
40-16054.4 %Surr: Pentacosane CVH08 SW8015C 03/27/17 13:33 03/29/17 18:26
Wet Chemistry Analysis
SW7196A MEC<0.005 mg/kg 0.005 108 03/27/17 09:30 03/28/17 15:00Chromium, Hexavalent
Page 74 of 109Page 74 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Analytical Summary
Preparation Method:
Preparation Method:
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
17C0845-01 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-02 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-03 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-04 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-05 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-06 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-07 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
17C0845-08 BAC0671 SAC0714SW7196A AC70142100 g / 100 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW1311 MetalsPreparation Method:TCLP Metals by 6000/7000 Series Methods
17C0845-01 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-02 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-03 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-04 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-05 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-06 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-07 BAC0682 SAC0690SW1311 100 g / 2000 mL
17C0845-08 BAC0682 SAC0690SW1311 100 g / 2000 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3010APreparation Method:TCLP Metals by 6000/7000 Series Methods
17C0845-01 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-02 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-03 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-04 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-05 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
Page 75 of 109Page 75 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
17C0845-06 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-07 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
17C0845-08 BAC0685 SAC0705SW6010C AC7013910.0 mL / 50.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3050BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
17C0845-01 BAC0651 SAC0668SW6010C AC701311.05 g / 50.0 mL
17C0845-02 BAC0651 SAC0668SW6010C AC701311.02 g / 50.0 mL
17C0845-02RE1 BAC0651 SAC0668SW6010C AC701311.02 g / 50.0 mL
17C0845-03 BAC0651 SAC0668SW6010C AC701311.06 g / 50.0 mL
17C0845-04 BAC0651 SAC0668SW6010C AC701311.06 g / 50.0 mL
17C0845-05 BAC0651 SAC0668SW6010C AC701311.08 g / 50.0 mL
17C0845-06 BAC0651 SAC0668SW6010C AC701311.04 g / 50.0 mL
17C0845-07 BAC0651 SAC0668SW6010C AC701311.03 g / 50.0 mL
17C0845-08 BAC0651 SAC0668SW6010C AC701311.00 g / 50.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW3550CPreparation Method:Semivolatile Organic Compounds by GCMS
17C0845-01 BAC0686 SAC0695SW8270D AC7007330.3 g / 1.00 mL
17C0845-02 BAC0686 SAC0695SW8270D AC7007330.1 g / 1.00 mL
17C0845-03 BAC0686 SAC0695SW8270D AC7007330.2 g / 1.00 mL
17C0845-04 BAC0686 SAC0695SW8270D AC7007330.1 g / 1.00 mL
17C0845-05 BAC0686 SAC0695SW8270D AC7007331.4 g / 1.00 mL
17C0845-06 BAC0686 SAC0695SW8270D AC7007331.8 g / 1.00 mL
17C0845-07 BAC0686 SAC0695SW8270D AC7007330.2 g / 1.00 mL
17C0845-08 BAC0686 SAC0695SW8270D AC7007332.2 g / 1.00 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW5030BPreparation Method:Volatile Hydrocarbons by GC
17C0845-01 BAC0672 SAC0681SW8015C AC701181.07 g / 5.00 mL
17C0845-02 BAC0672 SAC0681SW8015C AC701181.14 g / 5.00 mL
17C0845-03 BAC0672 SAC0681SW8015C AC701181.25 g / 5.00 mL
Page 76 of 109Page 76 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW5030BPreparation Method:Volatile Hydrocarbons by GC
17C0845-04 BAC0694 SAC0707SW8015C AC701181.00 g / 5.00 mL
17C0845-05 BAC0694 SAC0707SW8015C AC701181.02 g / 5.00 mL
17C0845-06 BAC0694 SAC0707SW8015C AC701181.03 g / 5.00 mL
17C0845-07 BAC0694 SAC0707SW8015C AC701181.23 g / 5.00 mL
17C0845-08 BAC0694 SAC0707SW8015C AC701181.00 g / 5.00 mL
SW5030BPreparation Method:Volatile Organic Compounds by GCMS
17C0845-01 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-02 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-03 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-04 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-05 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-06 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-07 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
17C0845-08 BAC0726 SAC0739SW8260B AC701385.00 g / 5.00 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW7470APreparation Method:TCLP Metals by 6000/7000 Series Methods
17C0845-01 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-02 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-03 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-04 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-05 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-06 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-07 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
17C0845-08 BAC0692 SAC0704SW7470A AC701361.00 mL / 20.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW7471APreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
17C0845-01 BAC0658 SAC0661SW7471B AC701300.553 g / 20.0 mL
17C0845-02 BAC0658 SAC0661SW7471B AC701300.549 g / 20.0 mL
17C0845-03 BAC0658 SAC0661SW7471B AC701300.569 g / 20.0 mL
17C0845-04 BAC0658 SAC0661SW7471B AC701300.543 g / 20.0 mL
Page 77 of 109Page 77 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
17C0845-05 BAC0658 SAC0661SW7471B AC701300.513 g / 20.0 mL
17C0845-06 BAC0658 SAC0661SW7471B AC701300.515 g / 20.0 mL
17C0845-07 BAC0658 SAC0661SW7471B AC701300.530 g / 20.0 mL
17C0845-08 BAC0658 SAC0661SW7471B AC701300.514 g / 20.0 mL
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
SW8100Preparation Method:Semivolatile Hydrocarbons by GC
17C0845-01 BAC0670 SAC0750SW8015C AC7010450.2 g / 1.00 mL
17C0845-02 BAC0670 SAC0750SW8015C AC7010450.4 g / 1.00 mL
17C0845-03 BAC0670 SAC0750SW8015C AC7010454.6 g / 1.00 mL
17C0845-04 BAC0670 SAC0750SW8015C AC7010450.3 g / 1.00 mL
17C0845-05 BAC0670 SAC0750SW8015C AC7010450.0 g / 1.00 mL
17C0845-06 BAC0670 SAC0750SW8015C AC7010451.3 g / 1.00 mL
17C0845-07 BAC0670 SAC0750SW8015C AC7010452.3 g / 1.00 mL
17C0845-08 BAC0670 SAC0750SW8015C AC7010451.0 g / 1.00 mL
Page 78 of 109Page 78 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0651 - SW3050B
Blank (BAC0651-BLK1) Prepared & Analyzed: 03/27/2017
0.500 mg/kg<0.500 mg/kgNickel
0.500 mg/kg<0.500 mg/kgChromium
2.50 mg/kg<2.50 mg/kgThallium
2.50 mg/kg<2.50 mg/kgCopper
5.00 mg/kg<5.00 mg/kgAntimony
0.200 mg/kg<0.200 mg/kgCadmium
2.50 mg/kg<2.50 mg/kgSelenium
0.500 mg/kg<0.500 mg/kgSilver
1.00 mg/kg<1.00 mg/kgArsenic
0.200 mg/kg<0.200 mg/kgBeryllium
0.500 mg/kg<0.500 mg/kgZinc
0.500 mg/kg<0.500 mg/kgLead
LCS (BAC0651-BS1) Prepared & Analyzed: 03/27/2017
1.00 98.2 80-12089.5mg/kg87.9 mg/kg mg/kgArsenic
5.00 98.2 80-12085.0mg/kg83.5 mg/kg mg/kgAntimony
0.500 98.2 80-12093.6mg/kg92.0 mg/kg mg/kgNickel
0.200 98.2 80-12093.4mg/kg91.8 mg/kg mg/kgCadmium
0.200 98.2 80-12091.8mg/kg90.2 mg/kg mg/kgBeryllium
0.500 98.2 80-12094.4mg/kg92.7 mg/kg mg/kgChromium
0.500 4.91 80-12091.0mg/kg4.47 mg/kg mg/kgSilver
0.500 98.2 80-12092.7mg/kg91.1 mg/kg mg/kgZinc
2.50 98.2 80-12090.4mg/kg88.8 mg/kg mg/kgThallium
2.50 98.2 80-12095.6mg/kg93.9 mg/kg mg/kgCopper
0.500 98.2 80-12091.2mg/kg89.6 mg/kg mg/kgLead
2.50 98.2 80-12085.4mg/kg83.9 mg/kg mg/kgSelenium
LCS Dup (BAC0651-BSD1) Prepared & Analyzed: 03/27/2017
2.50 96.4 2080-12096.2 4.27mg/kg92.7 mg/kg mg/kgThallium
2.50 96.4 2080-12098.9 1.48mg/kg95.3 mg/kg mg/kgCopper
0.500 96.4 2080-12096.9 1.59mg/kg93.5 mg/kg mg/kgNickel
0.500 96.4 2080-12096.4 3.66mg/kg93.0 mg/kg mg/kgLead
Page 79 of 109Page 79 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0651 - SW3050B
LCS Dup (BAC0651-BSD1) Prepared & Analyzed: 03/27/2017
2.50 96.4 2080-12091.0 4.49mg/kg87.7 mg/kg mg/kgSelenium
0.500 96.4 2080-12097.6 1.46mg/kg94.1 mg/kg mg/kgChromium
0.500 96.4 2080-12095.8 1.39mg/kg92.3 mg/kg mg/kgZinc
5.00 96.4 2080-12089.3 3.04mg/kg86.1 mg/kg mg/kgAntimony
0.500 4.82 2080-12094.0 1.37mg/kg4.53 mg/kg mg/kgSilver
0.200 96.4 2080-12096.6 1.51mg/kg93.1 mg/kg mg/kgCadmium
0.200 96.4 2080-12094.6 1.13mg/kg91.2 mg/kg mg/kgBeryllium
1.00 96.4 2080-12093.6 2.67mg/kg90.3 mg/kg mg/kgArsenic
Matrix Spike (BAC0651-MS1) Prepared & Analyzed: 03/27/2017Source: 17C0845-01
2.50 97.7 75-125100mg/kg128 mg/kg 29.6 mg/kgCopper
0.500 97.7 75-12595.2mg/kg95.5 mg/kg 2.61 mg/kgNickel
5.00 97.7 75-12550.5mg/kg49.3 mg/kg <5.00 mg/kgAntimony M
0.200 97.7 75-12593.7mg/kg91.5 mg/kg <0.200 mg/kgBeryllium
0.500 97.7 75-12595.5mg/kg95.7 mg/kg 2.42 mg/kgLead
1.00 97.7 75-12594.4mg/kg93.6 mg/kg 1.35 mg/kgArsenic
0.500 97.7 75-125120mg/kg146 mg/kg 28.5 mg/kgZinc
0.200 97.7 75-12594.4mg/kg92.5 mg/kg 0.299 mg/kgCadmium
0.500 97.7 75-12596.6mg/kg102 mg/kg 7.55 mg/kgChromium
2.50 97.7 75-12592.5mg/kg90.3 mg/kg <2.50 mg/kgThallium
2.50 97.7 75-12587.8mg/kg85.7 mg/kg <2.50 mg/kgSelenium
0.500 4.88 75-12592.9mg/kg4.54 mg/kg <0.500 mg/kgSilver
Matrix Spike Dup (BAC0651-MSD1) Prepared & Analyzed: 03/27/2017Source: 17C0845-01
2.50 95.5 2075-12584.0 6.62mg/kg80.2 mg/kg <2.50 mg/kgSelenium
0.500 95.5 2075-12593.2 21.3mg/kg117 mg/kg 28.5 mg/kgZinc P
0.200 95.5 2075-12592.7 4.01mg/kg88.9 mg/kg 0.299 mg/kgCadmium
2.50 95.5 2075-12598.8 2.85mg/kg124 mg/kg 29.6 mg/kgCopper
0.500 95.5 2075-12591.5 6.39mg/kg89.8 mg/kg 2.42 mg/kgLead
2.50 95.5 2075-12588.0 7.13mg/kg84.1 mg/kg <2.50 mg/kgThallium
5.00 95.5 2075-12547.3 8.81mg/kg45.2 mg/kg <5.00 mg/kgAntimony M
0.500 4.78 2075-12591.3 3.97mg/kg4.36 mg/kg <0.500 mg/kgSilver
Page 80 of 109Page 80 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0651 - SW3050B
Matrix Spike Dup (BAC0651-MSD1) Prepared & Analyzed: 03/27/2017Source: 17C0845-01
1.00 95.5 2075-12590.7 6.19mg/kg88.0 mg/kg 1.35 mg/kgArsenic
0.500 95.5 2075-12593.4 4.02mg/kg91.8 mg/kg 2.61 mg/kgNickel
0.200 95.5 2075-12591.7 4.39mg/kg87.6 mg/kg <0.200 mg/kgBeryllium
0.500 95.5 2075-12594.1 4.41mg/kg97.4 mg/kg 7.55 mg/kgChromium
Batch BAC0658 - SW7471A
Blank (BAC0658-BLK1) Prepared & Analyzed: 03/27/2017
0.008 mg/kg<0.008 mg/kgMercury
LCS (BAC0658-BS1) Prepared & Analyzed: 03/27/2017
0.008 0.0919 80-12095.3mg/kg0.088 mg/kg mg/kgMercury
LCS Dup (BAC0658-BSD1) Prepared & Analyzed: 03/27/2017
0.008 0.0977 2080-12093.3 3.88mg/kg0.091 mg/kg mg/kgMercury
Matrix Spike (BAC0658-MS1) Prepared & Analyzed: 03/27/2017Source: 17C0789-01
0.008 0.0994 80-12090.3mg/kg0.120 mg/kg 0.030 mg/kgMercury
Matrix Spike Dup (BAC0658-MSD1) Prepared & Analyzed: 03/27/2017Source: 17C0789-01
0.008 0.0960 2080-12087.7 4.79mg/kg0.114 mg/kg 0.030 mg/kgMercury
Page 81 of 109Page 81 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0682 - SW1311 Metals
Blank (BAC0682-BLK1) Prepared: 03/27/2017 Analyzed: 03/28/2017
0 #1 #Extraction Fluid, Metals
Batch BAC0685 - SW3010A
Blank (BAC0685-BLK1) Prepared & Analyzed: 03/28/2017
0.100 mg/L<0.100 mg/LArsenic
5.00 mg/L<5.00 mg/LBarium
0.0400 mg/L<0.0400 mg/LCadmium
0.100 mg/L<0.100 mg/LChromium
0.100 mg/L<0.100 mg/LLead
0.250 mg/L<0.250 mg/LSelenium
0.100 mg/L<0.100 mg/LSilver
LCS (BAC0685-BS1) Prepared & Analyzed: 03/28/2017
0.100 2.50 80-12096.1mg/L2.40 mg/L mg/LArsenic
5.00 2.50 80-120101mg/L<5.00 mg/L mg/LBarium
0.0400 2.50 80-12094.1mg/L2.35 mg/L mg/LCadmium
0.100 2.50 80-12095.5mg/L2.39 mg/L mg/LChromium
0.100 2.50 80-12095.5mg/L2.39 mg/L mg/LLead
0.250 2.50 80-12092.0mg/L2.30 mg/L mg/LSelenium
0.100 0.500 80-12095.4mg/L0.477 mg/L mg/LSilver
LCS Dup (BAC0685-BSD1) Prepared & Analyzed: 03/28/2017
0.100 2.50 2080-12098.5 2.48mg/L2.46 mg/L mg/LArsenic
5.00 2.50 2080-120103 1.82mg/L<5.00 mg/L mg/LBarium
0.0400 2.50 2080-12096.1 2.15mg/L2.40 mg/L mg/LCadmium
0.100 2.50 2080-12097.7 2.29mg/L2.44 mg/L mg/LChromium
0.100 2.50 2080-12098.1 2.74mg/L2.45 mg/L mg/LLead
0.250 2.50 2080-12095.2 3.43mg/L2.38 mg/L mg/LSelenium
0.100 0.500 2080-12096.5 1.16mg/L0.483 mg/L mg/LSilver
Page 82 of 109Page 82 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0685 - SW3010A
Matrix Spike (BAC0685-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0854-01
0.100 2.50 75-125100mg/L2.51 mg/L <0.100 mg/LArsenic
5.00 2.50 75-125114mg/L<5.00 mg/L <5.00 mg/LBarium
0.0400 2.50 75-12597.9mg/L2.45 mg/L <0.0400 mg/LCadmium
0.100 2.50 75-12599.9mg/L2.50 mg/L <0.100 mg/LChromium
0.100 2.50 75-125100mg/L2.50 mg/L <0.100 mg/LLead
0.250 2.50 75-12596.9mg/L2.42 mg/L <0.250 mg/LSelenium
0.100 0.500 75-12599.6mg/L0.498 mg/L <0.100 mg/LSilver
Matrix Spike Dup (BAC0685-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0854-01
0.100 2.50 2075-12598.6 1.71mg/L2.47 mg/L <0.100 mg/LArsenic
5.00 2.50 2075-125113 1.09mg/L<5.00 mg/L <5.00 mg/LBarium
0.0400 2.50 2075-12597.1 0.761mg/L2.43 mg/L <0.0400 mg/LCadmium
0.100 2.50 2075-12599.2 0.718mg/L2.48 mg/L <0.100 mg/LChromium
0.100 2.50 2075-12598.6 1.54mg/L2.46 mg/L <0.100 mg/LLead
0.250 2.50 2075-12598.0 1.05mg/L2.45 mg/L <0.250 mg/LSelenium
0.100 0.500 2075-12598.0 1.61mg/L0.490 mg/L <0.100 mg/LSilver
Batch BAC0692 - SW7470A
Blank (BAC0692-BLK1) Prepared & Analyzed: 03/28/2017
0.008 mg/L<0.008 mg/LMercury
LCS (BAC0692-BS1) Prepared & Analyzed: 03/28/2017
0.008 0.0500 80-12082.5mg/L0.041 mg/L mg/LMercury
LCS Dup (BAC0692-BSD1) Prepared & Analyzed: 03/28/2017
0.008 0.0500 2080-12082.1 0.426mg/L0.041 mg/L mg/LMercury
Page 83 of 109Page 83 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0692 - SW7470A
Matrix Spike (BAC0692-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0827-01
0.008 0.0500 80-12083.4mg/L0.042 mg/L <0.008 mg/LMercury
Matrix Spike (BAC0692-MS2) Prepared & Analyzed: 03/28/2017Source: 17C0845-08
0.008 0.0500 80-12084.1mg/L0.042 mg/L <0.008 mg/LMercury
Matrix Spike Dup (BAC0692-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0827-01
0.008 0.0500 2080-12082.1 1.65mg/L0.041 mg/L <0.008 mg/LMercury
Matrix Spike Dup (BAC0692-MSD2) Prepared & Analyzed: 03/28/2017Source: 17C0845-08
0.008 0.0500 2080-12083.8 0.367mg/L0.042 mg/L <0.008 mg/LMercury
Page 84 of 109Page 84 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0672 - SW5030B
Blank (BAC0672-BLK1) Prepared & Analyzed: 03/27/2017
0.10 mg/kg<0.10 mg/kgTPH-Volatiles (GRO)
LCS (BAC0672-BS1) Prepared & Analyzed: 03/27/2017
0.10 1.00 70-13088.4mg/kg0.88 mg/kg mg/kgTPH-Volatiles (GRO)
Matrix Spike (BAC0672-MS1) Prepared & Analyzed: 03/27/2017Source: 17C0845-01
0.50 5.00 70-13076.7mg/kg3.83 mg/kg <0.50 mg/kgTPH-Volatiles (GRO)
Matrix Spike Dup (BAC0672-MSD1) Prepared & Analyzed: 03/27/2017Source: 17C0845-01
0.49 4.85 2070-13066.9 16.5mg/kg3.25 mg/kg <0.49 mg/kgTPH-Volatiles (GRO) M
Batch BAC0694 - SW5030B
Blank (BAC0694-BLK1) Prepared & Analyzed: 03/28/2017
0.10 mg/kg<0.10 mg/kgTPH-Volatiles (GRO)
LCS (BAC0694-BS1) Prepared & Analyzed: 03/28/2017
0.10 1.00 70-13089.0mg/kg0.89 mg/kg mg/kgTPH-Volatiles (GRO)
Matrix Spike (BAC0694-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0845-04
0.48 4.81 70-13086.2mg/kg4.14 mg/kg <0.48 mg/kgTPH-Volatiles (GRO)
Matrix Spike Dup (BAC0694-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0845-04
0.47 4.67 2070-13087.4 1.45mg/kg4.09 mg/kg <0.47 mg/kgTPH-Volatiles (GRO)
Page 85 of 109Page 85 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Blank (BAC0726-BLK1) Prepared & Analyzed: 03/28/2017
5.00 ug/kg<5.00 ug/kg1,1,1,2-Tetrachloroethane
5.00 ug/kg<5.00 ug/kg1,1,1-Trichloroethane
5.00 ug/kg<5.00 ug/kg1,1,2,2-Tetrachloroethane
5.00 ug/kg<5.00 ug/kg1,1,2-Trichloroethane
5.00 ug/kg<5.00 ug/kg1,1-Dichloroethane
5.00 ug/kg<5.00 ug/kg1,1-Dichloroethylene
5.00 ug/kg<5.00 ug/kg1,1-Dichloropropene
5.00 ug/kg<5.00 ug/kg1,2,3-Trichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2,3-Trichloropropane
5.00 ug/kg<5.00 ug/kg1,2,4-Trichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2,4-Trimethylbenzene
5.00 ug/kg<5.00 ug/kg1,2-Dibromo-3-chloropropane (DBCP)
5.00 ug/kg<5.00 ug/kg1,2-Dibromoethane (EDB)
5.00 ug/kg<5.00 ug/kg1,2-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg1,2-Dichloroethane
5.00 ug/kg<5.00 ug/kg1,2-Dichloropropane
5.00 ug/kg<5.00 ug/kg1,3,5-Trimethylbenzene
5.00 ug/kg<5.00 ug/kg1,3-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg1,3-Dichloropropane
5.00 ug/kg<5.00 ug/kg1,4-Dichlorobenzene
5.00 ug/kg<5.00 ug/kg2,2-Dichloropropane
5.00 ug/kg<5.00 ug/kg2-Butanone (MEK)
5.00 ug/kg<5.00 ug/kg2-Chlorotoluene
5.00 ug/kg<5.00 ug/kg2-Hexanone (MBK)
5.00 ug/kg<5.00 ug/kg4-Chlorotoluene
5.00 ug/kg<5.00 ug/kg4-Isopropyltoluene
5.00 ug/kg<5.00 ug/kg4-Methyl-2-pentanone (MIBK)
10.0 ug/kg<10.0 ug/kgAcetone
5.00 ug/kg<5.00 ug/kgBenzene
5.00 ug/kg<5.00 ug/kgBromobenzene
5.00 ug/kg<5.00 ug/kgBromochloromethane
Page 86 of 109Page 86 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Blank (BAC0726-BLK1) Prepared & Analyzed: 03/28/2017
5.00 ug/kg<5.00 ug/kgBromodichloromethane
5.00 ug/kg<5.00 ug/kgBromoform
5.00 ug/kg<5.00 ug/kgBromomethane
5.00 ug/kg<5.00 ug/kgCarbon disulfide
5.00 ug/kg<5.00 ug/kgCarbon tetrachloride
5.00 ug/kg<5.00 ug/kgChlorobenzene
5.00 ug/kg<5.00 ug/kgChloroethane
5.00 ug/kg<5.00 ug/kgChloroform
5.00 ug/kg<5.00 ug/kgChloromethane
5.00 ug/kg<5.00 ug/kgcis-1,2-Dichloroethylene
5.00 ug/kg<5.00 ug/kgcis-1,3-Dichloropropene
5.00 ug/kg<5.00 ug/kgDibromochloromethane
5.00 ug/kg<5.00 ug/kgDibromomethane
5.00 ug/kg<5.00 ug/kgDichlorodifluoromethane
5.00 ug/kg<5.00 ug/kgDi-isopropyl ether (DIPE)
80.0 ug/kg<80.0 ug/kgEthanol
5.00 ug/kg<5.00 ug/kgEthylbenzene
25.0 ug/kg<25.0 ug/kgEthyl-t-butyl ether (ETBE)
5.00 ug/kg<5.00 ug/kgHexachlorobutadiene
5.00 ug/kg<5.00 ug/kgIodomethane
5.00 ug/kg<5.00 ug/kgIsopropylbenzene
5.00 ug/kg<5.00 ug/kgm+p-Xylenes
5.00 ug/kg<5.00 ug/kgMethylene chloride
5.00 ug/kg<5.00 ug/kgMethyl-t-butyl ether (MTBE)
5.00 ug/kg<5.00 ug/kgNaphthalene
5.00 ug/kg<5.00 ug/kgn-Butylbenzene
5.00 ug/kg<5.00 ug/kgn-Propylbenzene
5.00 ug/kg<5.00 ug/kgo-Xylene
5.00 ug/kg<5.00 ug/kgsec-Butylbenzene
5.00 ug/kg<5.00 ug/kgStyrene
10.0 ug/kg<10.0 ug/kgTAA
Page 87 of 109Page 87 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Blank (BAC0726-BLK1) Prepared & Analyzed: 03/28/2017
5.00 ug/kg<5.00 ug/kgTAEE
5.00 ug/kg<5.00 ug/kgTAME
100 ug/kg<100 ug/kgTBA
5.00 ug/kg<5.00 ug/kgtert-Butylbenzene
5.00 ug/kg<5.00 ug/kgTetrachloroethylene (PCE)
5.00 ug/kg<5.00 ug/kgToluene
5.00 ug/kg<5.00 ug/kgtrans-1,2-Dichloroethylene
5.00 ug/kg<5.00 ug/kgtrans-1,3-Dichloropropene
5.00 ug/kg<5.00 ug/kgTrichloroethylene
5.00 ug/kg<5.00 ug/kgTrichlorofluoromethane
10.0 ug/kg<10.0 ug/kgVinyl acetate
5.00 ug/kg<5.00 ug/kgVinyl chloride
10.0 ug/kg<10.0 ug/kgXylenes, Total
50.0 80-120Surr: 1,2-Dichloroethane-d4 94.347.2 ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 97.949.0 ug/kg
50.0 78-119Surr: Dibromofluoromethane 96.348.2 ug/kg
50.0 85-115Surr: Toluene-d8 10150.7 ug/kg
LCS (BAC0726-BS1) Prepared & Analyzed: 03/28/2017
5 50.0 75-12590.1ug/L45.0 ug/L ug/L1,1,1,2-Tetrachloroethane
5 50.0 70-13585.0ug/L42.5 ug/L ug/L1,1,1-Trichloroethane
5 50.0 55-13076.3ug/L38.2 ug/L ug/L1,1,2,2-Tetrachloroethane
5 50.0 60-12593.7ug/L46.9 ug/L ug/L1,1,2-Trichloroethane
5 50.0 75-12590.5ug/L45.3 ug/L ug/L1,1-Dichloroethane
5 50.0 65-13584.0ug/L42.0 ug/L ug/L1,1-Dichloroethylene
5 50.0 70-13583.4ug/L41.7 ug/L ug/L1,1-Dichloropropene
5 50.0 60-13587.3ug/L43.7 ug/L ug/L1,2,3-Trichlorobenzene
5 50.0 65-13085.1ug/L42.5 ug/L ug/L1,2,3-Trichloropropane
5 50.0 65-13088.1ug/L44.1 ug/L ug/L1,2,4-Trichlorobenzene
5 50.0 65-13589.8ug/L44.9 ug/L ug/L1,2,4-Trimethylbenzene
5 50.0 40-13579.7ug/L39.9 ug/L ug/L1,2-Dibromo-3-chloropropane (DBCP)
Page 88 of 109Page 88 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
LCS (BAC0726-BS1) Prepared & Analyzed: 03/28/2017
5 50.0 70-12591.0ug/L45.5 ug/L ug/L1,2-Dibromoethane (EDB)
5 50.0 75-12085.8ug/L42.9 ug/L ug/L1,2-Dichlorobenzene
5 50.0 70-13590.9ug/L45.4 ug/L ug/L1,2-Dichloroethane
5 50.0 70-12091.9ug/L45.9 ug/L ug/L1,2-Dichloropropane
5 50.0 65-13587.9ug/L43.9 ug/L ug/L1,3,5-Trimethylbenzene
5 50.0 70-12585.5ug/L42.7 ug/L ug/L1,3-Dichlorobenzene
5 50.0 75-12590.2ug/L45.1 ug/L ug/L1,3-Dichloropropane
5 50.0 70-12583.8ug/L41.9 ug/L ug/L1,4-Dichlorobenzene
5 50.0 65-13588.0ug/L44.0 ug/L ug/L2,2-Dichloropropane
5 50.0 30-16087.1ug/L43.6 ug/L ug/L2-Butanone (MEK)
5 50.0 70-13086.0ug/L43.0 ug/L ug/L2-Chlorotoluene
5 50.0 45-14595.9ug/L48.0 ug/L ug/L2-Hexanone (MBK)
5 50.0 75-12588.3ug/L44.2 ug/L ug/L4-Chlorotoluene
5 50.0 75-13588.5ug/L44.3 ug/L ug/L4-Isopropyltoluene
5 50.0 45-14591.7ug/L45.8 ug/L ug/L4-Methyl-2-pentanone (MIBK)
10 50.0 20-160103ug/L51.4 ug/L ug/LAcetone
5 50.0 75-12590.3ug/L45.1 ug/L ug/LBenzene
5 50.0 65-12086.7ug/L43.4 ug/L ug/LBromobenzene
5 50.0 70-12586.8ug/L43.4 ug/L ug/LBromochloromethane
5 50.0 70-13090.0ug/L45.0 ug/L ug/LBromodichloromethane
5 50.0 55-13584.2ug/L42.1 ug/L ug/LBromoform
5 50.0 30-16073.6ug/L36.8 ug/L ug/LBromomethane
5 50.0 45-160119ug/L59.5 ug/L ug/LCarbon disulfide
5 50.0 65-13592.6ug/L46.3 ug/L ug/LCarbon tetrachloride
5 50.0 75-12584.3ug/L42.1 ug/L ug/LChlorobenzene
5 50.0 40-15577.8ug/L38.9 ug/L ug/LChloroethane
5 50.0 70-12584.8ug/L42.4 ug/L ug/LChloroform
5 50.0 50-13065.3ug/L32.6 ug/L ug/LChloromethane
5 50.0 65-12581.6ug/L40.8 ug/L ug/Lcis-1,2-Dichloroethylene
5 50.0 70-12585.5ug/L42.8 ug/L ug/Lcis-1,3-Dichloropropene
5 50.0 65-13094.5ug/L47.2 ug/L ug/LDibromochloromethane
Page 89 of 109Page 89 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
LCS (BAC0726-BS1) Prepared & Analyzed: 03/28/2017
5 50.0 75-13086.6ug/L43.3 ug/L ug/LDibromomethane
5 50.0 35-13557.1ug/L28.5 ug/L ug/LDichlorodifluoromethane
5 50.0 75-12590.6ug/L45.3 ug/L ug/LEthylbenzene
5 50.0 55-14085.4ug/L42.7 ug/L ug/LHexachlorobutadiene
5 50.0 75-13093.0ug/L46.5 ug/L ug/LIsopropylbenzene
5 100 80-12587.0ug/L87.0 ug/L ug/Lm+p-Xylenes
5 50.0 55-14087.0ug/L43.5 ug/L ug/LMethylene chloride
5 50.0 65-12584.8ug/L42.4 ug/L ug/LMethyl-t-butyl ether (MTBE)
5 50.0 40-12587.1ug/L43.5 ug/L ug/LNaphthalene
5 50.0 65-14090.7ug/L45.3 ug/L ug/Ln-Butylbenzene
5 50.0 65-13591.2ug/L45.6 ug/L ug/Ln-Propylbenzene
5 50.0 75-12588.0ug/L44.0 ug/L ug/Lo-Xylene
5 50.0 65-13086.1ug/L43.1 ug/L ug/Lsec-Butylbenzene
5 50.0 75-12592.1ug/L46.0 ug/L ug/LStyrene
5 50.0 65-13089.7ug/L44.9 ug/L ug/Ltert-Butylbenzene
5 50.0 65-140140ug/L70.1 ug/L ug/LTetrachloroethylene (PCE) L
5 50.0 70-12589.5ug/L44.8 ug/L ug/LToluene
5 50.0 65-13583.2ug/L41.6 ug/L ug/Ltrans-1,2-Dichloroethylene
5 50.0 65-12592.5ug/L46.2 ug/L ug/Ltrans-1,3-Dichloropropene
5 50.0 75-12596.7ug/L48.3 ug/L ug/LTrichloroethylene
5 50.0 25-18570.4ug/L35.2 ug/L ug/LTrichlorofluoromethane
5 50.0 60-13072.4ug/L36.2 ug/L ug/LVinyl chloride
50.0 80-120Surr: 1,2-Dichloroethane-d4 94.847.4 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10050.1 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 93.546.8 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 96.948.4 ug/kg ug/kg
Matrix Spike (BAC0726-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 75-12586.0ug/L43.0 ug/L <5 ug/L1,1,1,2-Tetrachloroethane
5 50.0 70-13580.8ug/L40.4 ug/L <5 ug/L1,1,1-Trichloroethane
5 50.0 55-13083.0ug/L41.5 ug/L <5 ug/L1,1,2,2-Tetrachloroethane
Page 90 of 109Page 90 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Matrix Spike (BAC0726-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 60-12591.0ug/L45.5 ug/L <5 ug/L1,1,2-Trichloroethane
5 50.0 75-12585.2ug/L42.6 ug/L <5 ug/L1,1-Dichloroethane
5 50.0 65-13579.4ug/L39.7 ug/L <5 ug/L1,1-Dichloroethylene
5 50.0 70-13578.6ug/L39.3 ug/L <5 ug/L1,1-Dichloropropene
5 50.0 60-13581.5ug/L40.7 ug/L <5 ug/L1,2,3-Trichlorobenzene
5 50.0 65-13084.2ug/L42.1 ug/L <5 ug/L1,2,3-Trichloropropane
5 50.0 65-13080.8ug/L40.4 ug/L <5 ug/L1,2,4-Trichlorobenzene
5 50.0 65-13588.1ug/L44.2 ug/L <5 ug/L1,2,4-Trimethylbenzene
5 50.0 40-13583.7ug/L41.9 ug/L <5 ug/L1,2-Dibromo-3-chloropropane (DBCP)
5 50.0 70-12588.1ug/L44.0 ug/L <5 ug/L1,2-Dibromoethane (EDB)
5 50.0 75-12080.6ug/L40.3 ug/L <5 ug/L1,2-Dichlorobenzene
5 50.0 70-13584.3ug/L42.1 ug/L <5 ug/L1,2-Dichloroethane
5 50.0 70-12091.4ug/L45.7 ug/L <5 ug/L1,2-Dichloropropane
5 50.0 65-13585.1ug/L42.5 ug/L <5 ug/L1,3,5-Trimethylbenzene
5 50.0 70-12582.2ug/L41.1 ug/L <5 ug/L1,3-Dichlorobenzene
5 50.0 75-12583.6ug/L43.4 ug/L <5 ug/L1,3-Dichloropropane
5 50.0 70-12577.1ug/L38.5 ug/L <5 ug/L1,4-Dichlorobenzene
5 50.0 65-13579.1ug/L39.5 ug/L <5 ug/L2,2-Dichloropropane
5 50.0 30-16072.9ug/L36.4 ug/L <5 ug/L2-Butanone (MEK)
5 50.0 70-13083.3ug/L41.6 ug/L <5 ug/L2-Chlorotoluene
5 50.0 45-14576.6ug/L38.3 ug/L <5 ug/L2-Hexanone (MBK)
5 50.0 75-12585.0ug/L42.5 ug/L <5 ug/L4-Chlorotoluene
5 50.0 75-13584.4ug/L42.2 ug/L <5 ug/L4-Isopropyltoluene
5 50.0 45-14575.5ug/L37.7 ug/L <5 ug/L4-Methyl-2-pentanone (MIBK)
10 50.0 20-16083.0ug/L44.4 ug/L <10 ug/LAcetone
5 50.0 75-12588.5ug/L44.2 ug/L <5 ug/LBenzene
5 50.0 65-12084.2ug/L42.1 ug/L <5 ug/LBromobenzene
5 50.0 70-12581.1ug/L40.6 ug/L <5 ug/LBromochloromethane
5 50.0 70-13088.7ug/L44.3 ug/L <5 ug/LBromodichloromethane
5 50.0 55-13586.5ug/L43.2 ug/L <5 ug/LBromoform
5 50.0 30-16079.9ug/L40.0 ug/L <5 ug/LBromomethane
Page 91 of 109Page 91 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Matrix Spike (BAC0726-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 45-16085.3ug/L42.7 ug/L <5 ug/LCarbon disulfide
5 50.0 65-13592.8ug/L46.4 ug/L <5 ug/LCarbon tetrachloride
5 50.0 75-12581.4ug/L40.7 ug/L <5 ug/LChlorobenzene
5 50.0 40-15574.2ug/L37.1 ug/L <5 ug/LChloroethane
5 50.0 70-12577.2ug/L38.6 ug/L <5 ug/LChloroform
5 50.0 50-13061.0ug/L30.5 ug/L <5 ug/LChloromethane
5 50.0 65-12576.4ug/L38.2 ug/L <5 ug/Lcis-1,2-Dichloroethylene
5 50.0 70-12581.0ug/L40.5 ug/L <5 ug/Lcis-1,3-Dichloropropene
5 50.0 65-13092.4ug/L46.2 ug/L <5 ug/LDibromochloromethane
5 50.0 75-13085.2ug/L42.6 ug/L <5 ug/LDibromomethane
5 50.0 35-13557.0ug/L28.5 ug/L <5 ug/LDichlorodifluoromethane
5 50.0 75-12588.3ug/L44.3 ug/L <5 ug/LEthylbenzene
5 50.0 55-14079.8ug/L39.9 ug/L <5 ug/LHexachlorobutadiene
5 50.0 75-13092.1ug/L46.1 ug/L <5 ug/LIsopropylbenzene
5 100 80-12587.5ug/L87.9 ug/L <5 ug/Lm+p-Xylenes
5 50.0 55-14078.9ug/L41.1 ug/L <5 ug/LMethylene chloride
5 50.0 65-12582.1ug/L41.0 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 40-12585.9ug/L43.0 ug/L <5 ug/LNaphthalene
5 50.0 65-14086.0ug/L43.0 ug/L <5 ug/Ln-Butylbenzene
5 50.0 65-13586.8ug/L43.4 ug/L <5 ug/Ln-Propylbenzene
5 50.0 75-12587.2ug/L43.8 ug/L <5 ug/Lo-Xylene
5 50.0 65-13082.5ug/L41.3 ug/L <5 ug/Lsec-Butylbenzene
5 50.0 75-12589.5ug/L44.7 ug/L <5 ug/LStyrene
5 50.0 65-13085.4ug/L42.7 ug/L <5 ug/Ltert-Butylbenzene
5 50.0 65-140118ug/L59.1 ug/L <5 ug/LTetrachloroethylene (PCE)
5 50.0 70-12584.6ug/L42.8 ug/L <5 ug/LToluene
5 50.0 65-13577.7ug/L38.9 ug/L <5 ug/Ltrans-1,2-Dichloroethylene
5 50.0 65-12587.9ug/L43.9 ug/L <5 ug/Ltrans-1,3-Dichloropropene
5 50.0 75-12586.0ug/L43.0 ug/L <5 ug/LTrichloroethylene
5 50.0 25-18565.0ug/L32.5 ug/L <5 ug/LTrichlorofluoromethane
5 50.0 60-13069.6ug/L34.8 ug/L <5 ug/LVinyl chloride
Page 92 of 109Page 92 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Matrix Spike (BAC0726-MS1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
50.0 80-120Surr: 1,2-Dichloroethane-d4 92.246.1 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10150.7 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 89.744.8 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 97.848.9 ug/kg ug/kg
Matrix Spike Dup (BAC0726-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 3075-12574.0 15.0ug/L37.0 ug/L <5 ug/L1,1,1,2-Tetrachloroethane M
5 50.0 3070-13573.3 9.68ug/L36.7 ug/L <5 ug/L1,1,1-Trichloroethane
5 50.0 3055-13072.9 13.0ug/L36.4 ug/L <5 ug/L1,1,2,2-Tetrachloroethane
5 50.0 3060-12578.3 14.9ug/L39.2 ug/L <5 ug/L1,1,2-Trichloroethane
5 50.0 3075-12575.4 12.3ug/L37.7 ug/L <5 ug/L1,1-Dichloroethane
5 50.0 3065-13572.4 9.19ug/L36.2 ug/L <5 ug/L1,1-Dichloroethylene
5 50.0 3070-13571.2 9.87ug/L35.6 ug/L <5 ug/L1,1-Dichloropropene
5 50.0 3060-13566.8 19.8ug/L33.4 ug/L <5 ug/L1,2,3-Trichlorobenzene
5 50.0 3065-13074.7 11.9ug/L37.4 ug/L <5 ug/L1,2,3-Trichloropropane
5 50.0 3065-13067.3 18.2ug/L33.7 ug/L <5 ug/L1,2,4-Trichlorobenzene
5 50.0 3065-13573.4 18.1ug/L36.8 ug/L <5 ug/L1,2,4-Trimethylbenzene
5 50.0 3040-13575.4 10.5ug/L37.7 ug/L <5 ug/L1,2-Dibromo-3-chloropropane (DBCP)
5 50.0 3070-12575.3 15.6ug/L37.7 ug/L <5 ug/L1,2-Dibromoethane (EDB)
5 50.0 3075-12069.5 14.9ug/L34.7 ug/L <5 ug/L1,2-Dichlorobenzene M
5 50.0 3070-13576.2 10.0ug/L38.1 ug/L <5 ug/L1,2-Dichloroethane
5 50.0 3070-12081.1 11.9ug/L40.6 ug/L <5 ug/L1,2-Dichloropropane
5 50.0 3065-13572.4 16.1ug/L36.2 ug/L <5 ug/L1,3,5-Trimethylbenzene
5 50.0 3070-12570.0 16.0ug/L35.0 ug/L <5 ug/L1,3-Dichlorobenzene M
5 50.0 3075-12574.2 11.5ug/L38.7 ug/L <5 ug/L1,3-Dichloropropane M
5 50.0 3070-12567.5 13.2ug/L33.8 ug/L <5 ug/L1,4-Dichlorobenzene M
5 50.0 3065-13569.8 12.6ug/L34.9 ug/L <5 ug/L2,2-Dichloropropane
5 50.0 3030-16067.3 8.05ug/L33.6 ug/L <5 ug/L2-Butanone (MEK)
5 50.0 3070-13073.2 12.8ug/L36.6 ug/L <5 ug/L2-Chlorotoluene
5 50.0 3045-14569.3 9.98ug/L34.7 ug/L <5 ug/L2-Hexanone (MBK)
5 50.0 3075-12573.9 13.9ug/L36.9 ug/L <5 ug/L4-Chlorotoluene M
Page 93 of 109Page 93 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Matrix Spike Dup (BAC0726-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 3075-13571.7 16.3ug/L35.8 ug/L <5 ug/L4-Isopropyltoluene M
5 50.0 3045-14568.8 9.29ug/L34.4 ug/L <5 ug/L4-Methyl-2-pentanone (MIBK)
10 50.0 3020-16082.2 0.931ug/L43.9 ug/L <10 ug/LAcetone
5 50.0 3075-12577.5 13.3ug/L38.7 ug/L <5 ug/LBenzene
5 50.0 3065-12072.5 15.0ug/L36.3 ug/L <5 ug/LBromobenzene
5 50.0 3070-12573.2 10.2ug/L36.6 ug/L <5 ug/LBromochloromethane
5 50.0 3070-13078.6 12.1ug/L39.3 ug/L <5 ug/LBromodichloromethane
5 50.0 3055-13574.4 15.1ug/L37.2 ug/L <5 ug/LBromoform
5 50.0 3030-16065.2 20.3ug/L32.6 ug/L <5 ug/LBromomethane
5 50.0 3045-16080.2 6.20ug/L40.1 ug/L <5 ug/LCarbon disulfide
5 50.0 3065-13580.0 14.9ug/L40.0 ug/L <5 ug/LCarbon tetrachloride
5 50.0 3075-12569.6 15.7ug/L34.8 ug/L <5 ug/LChlorobenzene M
5 50.0 3040-15569.5 6.60ug/L34.7 ug/L <5 ug/LChloroethane
5 50.0 3070-12570.1 9.69ug/L35.1 ug/L <5 ug/LChloroform
5 50.0 3050-13054.3 11.7ug/L27.1 ug/L <5 ug/LChloromethane
5 50.0 3065-12569.8 8.98ug/L34.9 ug/L <5 ug/Lcis-1,2-Dichloroethylene
5 50.0 3070-12571.6 12.3ug/L35.8 ug/L <5 ug/Lcis-1,3-Dichloropropene
5 50.0 3065-13082.1 11.8ug/L41.1 ug/L <5 ug/LDibromochloromethane
5 50.0 3075-13076.3 11.0ug/L38.1 ug/L <5 ug/LDibromomethane
5 50.0 3035-13549.2 14.7ug/L24.6 ug/L <5 ug/LDichlorodifluoromethane
5 50.0 3075-12574.0 17.6ug/L37.1 ug/L <5 ug/LEthylbenzene M
5 50.0 3055-14063.4 22.9ug/L31.7 ug/L <5 ug/LHexachlorobutadiene
5 50.0 3075-13076.6 18.4ug/L38.3 ug/L <5 ug/LIsopropylbenzene
5 100 3080-12573.8 16.8ug/L74.3 ug/L <5 ug/Lm+p-Xylenes M
5 50.0 3055-14071.8 8.96ug/L37.6 ug/L <5 ug/LMethylene chloride
5 50.0 3065-12574.3 9.87ug/L37.2 ug/L <5 ug/LMethyl-t-butyl ether (MTBE)
5 50.0 3040-12574.2 14.7ug/L37.1 ug/L <5 ug/LNaphthalene
5 50.0 3065-14070.6 19.7ug/L35.3 ug/L <5 ug/Ln-Butylbenzene
5 50.0 3065-13574.1 15.8ug/L37.1 ug/L <5 ug/Ln-Propylbenzene
5 50.0 3075-12572.9 17.8ug/L36.7 ug/L <5 ug/Lo-Xylene M
5 50.0 3065-13068.0 19.2ug/L34.0 ug/L <5 ug/Lsec-Butylbenzene
Page 94 of 109Page 94 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0726 - SW5030B
Matrix Spike Dup (BAC0726-MSD1) Prepared & Analyzed: 03/28/2017Source: 17C0850-09
5 50.0 3075-12576.0 16.3ug/L38.0 ug/L <5 ug/LStyrene
5 50.0 3065-13073.0 15.7ug/L36.5 ug/L <5 ug/Ltert-Butylbenzene
5 50.0 3065-14097.2 19.4ug/L48.6 ug/L <5 ug/LTetrachloroethylene (PCE)
5 50.0 3070-12575.4 11.4ug/L38.2 ug/L <5 ug/LToluene
5 50.0 3065-13572.5 6.93ug/L36.3 ug/L <5 ug/Ltrans-1,2-Dichloroethylene
5 50.0 3065-12578.0 11.9ug/L39.0 ug/L <5 ug/Ltrans-1,3-Dichloropropene
5 50.0 3075-12576.7 11.4ug/L38.3 ug/L <5 ug/LTrichloroethylene
5 50.0 3025-18559.0 9.58ug/L29.5 ug/L <5 ug/LTrichlorofluoromethane
5 50.0 3060-13064.3 8.03ug/L32.1 ug/L <5 ug/LVinyl chloride
50.0 80-120Surr: 1,2-Dichloroethane-d4 93.846.9 ug/kg ug/kg
50.0 85-120Surr: 4-Bromofluorobenzene 10050.2 ug/kg ug/kg
50.0 78-119Surr: Dibromofluoromethane 90.845.4 ug/kg ug/kg
50.0 85-115Surr: Toluene-d8 98.349.1 ug/kg ug/kg
Page 95 of 109Page 95 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0686 - SW3550C
Blank (BAC0686-BLK1) Prepared & Analyzed: 03/28/2017
83.3 ug/kg<83.3 ug/kg1,2,4,5-Tetrachlorobenzene
83.3 ug/kg<83.3 ug/kg1,2,4-Trichlorobenzene
83.3 ug/kg<83.3 ug/kg1,2-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1,2-Diphenylhydrazine
83.3 ug/kg<83.3 ug/kg1,3-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1,4-Dichlorobenzene
83.3 ug/kg<83.3 ug/kg1-Chloronaphthalene
83.3 ug/kg<83.3 ug/kg1-Naphthylamine
83.3 ug/kg<83.3 ug/kg2,3,4,6-Tetrachlorophenol
83.3 ug/kg<83.3 ug/kg2,4,5-Trichlorophenol
83.3 ug/kg<83.3 ug/kg2,4,6-Trichlorophenol
83.3 ug/kg<83.3 ug/kg2,4-Dichlorophenol
83.3 ug/kg<83.3 ug/kg2,4-Dimethylphenol
83.3 ug/kg<83.3 ug/kg2,4-Dinitrophenol
83.3 ug/kg<83.3 ug/kg2,4-Dinitrotoluene
83.3 ug/kg<83.3 ug/kg2,6-Dichlorophenol
83.3 ug/kg<83.3 ug/kg2,6-Dinitrotoluene
83.3 ug/kg<83.3 ug/kg2-Chloronaphthalene
83.3 ug/kg<83.3 ug/kg2-Chlorophenol
83.3 ug/kg<83.3 ug/kg2-Methylnaphthalene
83.3 ug/kg<83.3 ug/kg2-Naphthylamine
83.3 ug/kg<83.3 ug/kg2-Nitroaniline
83.3 ug/kg<83.3 ug/kg2-Nitrophenol
83.3 ug/kg<83.3 ug/kg3,3'-Dichlorobenzidine
83.3 ug/kg<83.3 ug/kg3-Methylcholanthrene
83.3 ug/kg<83.3 ug/kg3-Nitroaniline
83.3 ug/kg<83.3 ug/kg4,6-Dinitro-2-methylphenol
83.3 ug/kg<83.3 ug/kg4-Aminobiphenyl
83.3 ug/kg<83.3 ug/kg4-Bromophenyl phenyl ether
83.3 ug/kg<83.3 ug/kg4-Chloroaniline
83.3 ug/kg<83.3 ug/kg4-Chlorophenyl phenyl ether
Page 96 of 109Page 96 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0686 - SW3550C
Blank (BAC0686-BLK1) Prepared & Analyzed: 03/28/2017
83.3 ug/kg<83.3 ug/kg4-Nitroaniline
83.3 ug/kg<83.3 ug/kg4-Nitrophenol
83.3 ug/kg<83.3 ug/kg7,12-Dimethylbenz (a) anthracene
83.3 ug/kg<83.3 ug/kgAcenaphthene
83.3 ug/kg<83.3 ug/kgAcenaphthylene
83.3 ug/kg<83.3 ug/kgAcetophenone
83.3 ug/kg<83.3 ug/kgAniline
83.3 ug/kg<83.3 ug/kgAnthracene
83.3 ug/kg<83.3 ug/kgBenzidine
83.3 ug/kg<83.3 ug/kgBenzo (a) anthracene
83.3 ug/kg<83.3 ug/kgBenzo (a) pyrene
83.3 ug/kg<83.3 ug/kgBenzo (b) fluoranthene
83.3 ug/kg<83.3 ug/kgBenzo (g,h,i) perylene
83.3 ug/kg<83.3 ug/kgBenzo (k) fluoranthene
83.3 ug/kg<83.3 ug/kgBenzoic acid
83.3 ug/kg<83.3 ug/kgBenzyl alcohol
83.3 ug/kg<83.3 ug/kgbis (2-Chloroethoxy) methane
83.3 ug/kg<83.3 ug/kgbis (2-Chloroethyl) ether
83.3 ug/kg<83.3 ug/kg2,2'-Oxybis (1-chloropropane)
83.3 ug/kg<83.3 ug/kgbis (2-Ethylhexyl) phthalate
83.3 ug/kg<83.3 ug/kgButyl benzyl phthalate
83.3 ug/kg<83.3 ug/kgChrysene
83.3 ug/kg<83.3 ug/kgDibenz (a,h) anthracene
83.3 ug/kg<83.3 ug/kgDibenz (a,j) acridine
83.3 ug/kg<83.3 ug/kgDibenzofuran
83.3 ug/kg<83.3 ug/kgDiethyl phthalate
83.3 ug/kg<83.3 ug/kgDimethyl phthalate
83.3 ug/kg<83.3 ug/kgDi-n-butyl phthalate
83.3 ug/kg<83.3 ug/kgDi-n-octyl phthalate
83.3 ug/kg<83.3 ug/kgDiphenylamine
83.3 ug/kg<83.3 ug/kgEthyl methanesulfonate
Page 97 of 109Page 97 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0686 - SW3550C
Blank (BAC0686-BLK1) Prepared & Analyzed: 03/28/2017
83.3 ug/kg<83.3 ug/kgFluoranthene
83.3 ug/kg<83.3 ug/kgFluorene
83.3 ug/kg<83.3 ug/kgHexachlorobenzene
83.3 ug/kg<83.3 ug/kgHexachlorobutadiene
83.3 ug/kg<83.3 ug/kgHexachlorocyclopentadiene
83.3 ug/kg<83.3 ug/kgHexachloroethane
83.3 ug/kg<83.3 ug/kgIndeno (1,2,3-cd) pyrene
83.3 ug/kg<83.3 ug/kgIsophorone
83.3 ug/kg<83.3 ug/kgm+p-Cresols
83.3 ug/kg<83.3 ug/kgMethyl methanesulfonate
83.3 ug/kg<83.3 ug/kgNaphthalene
83.3 ug/kg<83.3 ug/kgNitrobenzene
83.3 ug/kg<83.3 ug/kgn-Nitrosodimethylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodi-n-butylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodi-n-propylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosodiphenylamine
83.3 ug/kg<83.3 ug/kgn-Nitrosopiperidine
83.3 ug/kg<83.3 ug/kgo+m+p-Cresols
83.3 ug/kg<83.3 ug/kgo-Cresol
83.3 ug/kg<83.3 ug/kgp-(Dimethylamino) azobenzene
83.3 ug/kg<83.3 ug/kgp-Chloro-m-cresol
83.3 ug/kg<83.3 ug/kgPentachloronitrobenzene (quintozene)
83.3 ug/kg<83.3 ug/kgPentachlorophenol
83.3 ug/kg<83.3 ug/kgPhenacetin
83.3 ug/kg<83.3 ug/kgPhenanthrene
83.3 ug/kg<83.3 ug/kgPhenol
83.3 ug/kg<83.3 ug/kgPronamide
83.3 ug/kg<83.3 ug/kgPyrene
83.3 ug/kg<83.3 ug/kgPyridine
3320 35-125Surr: 2,4,6-Tribromophenol 57.51910 ug/kg
1660 45-105Surr: 2-Fluorobiphenyl 63.91060 ug/kg
Page 98 of 109Page 98 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0686 - SW3550C
Blank (BAC0686-BLK1) Prepared & Analyzed: 03/28/2017
3320 35-105Surr: 2-Fluorophenol 63.62110 ug/kg
1660 35-100Surr: Nitrobenzene-d5 66.91110 ug/kg
3320 40-100Surr: Phenol-d5 69.62310 ug/kg
1660 30-125Surr: p-Terphenyl-d14 85.11410 ug/kg
LCS (BAC0686-BS1) Prepared: 03/28/2017 Analyzed: 03/29/2017
83.3 3310 44-14260.2ug/kg1990 ug/kg ug/kg1,2,4-Trichlorobenzene
83.3 3310 20-12463.4ug/kg2100 ug/kg ug/kg1,4-Dichlorobenzene
83.3 3310 15-14069.9ug/kg2310 ug/kg ug/kg4-Nitrophenol
83.3 3310 45-11066.0ug/kg2190 ug/kg ug/kgAcenaphthene
83.3 3310 40-11570.4ug/kg2330 ug/kg ug/kgn-Nitrosodi-n-propylamine
83.3 3310 25-12071.6ug/kg2370 ug/kg ug/kgPentachlorophenol
83.3 3340 40-10060.3ug/kg2020 ug/kg ug/kgPhenol
83.3 3310 45-12570.7ug/kg2340 ug/kg ug/kgPyrene
3310 35-125Surr: 2,4,6-Tribromophenol 68.02250 ug/kg ug/kg
1660 45-105Surr: 2-Fluorobiphenyl 65.01080 ug/kg ug/kg
3310 35-105Surr: 2-Fluorophenol 74.32460 ug/kg ug/kg
1660 35-100Surr: Nitrobenzene-d5 69.21150 ug/kg ug/kg
3310 40-100Surr: Phenol-d5 70.02320 ug/kg ug/kg
1660 30-125Surr: p-Terphenyl-d14 73.51220 ug/kg ug/kg
Matrix Spike (BAC0686-MS1) Prepared: 03/28/2017 Analyzed: 03/29/2017Source: 17C0845-08
83.3 3190 44-14250.0ug/kg1600 ug/kg <83.3 ug/kg1,2,4-Trichlorobenzene
83.3 3190 20-12450.9ug/kg1630 ug/kg <83.3 ug/kg1,4-Dichlorobenzene
83.3 3190 15-14052.9ug/kg1690 ug/kg <83.3 ug/kg4-Nitrophenol
83.3 3190 45-11056.7ug/kg1810 ug/kg <83.3 ug/kgAcenaphthene
83.3 3190 40-11565.8ug/kg2100 ug/kg <83.3 ug/kgn-Nitrosodi-n-propylamine
83.3 3190 25-12061.0ug/kg1950 ug/kg <83.3 ug/kgPentachlorophenol
83.3 3230 40-10050.7ug/kg1630 ug/kg <83.3 ug/kgPhenol
83.3 3190 45-12568.9ug/kg2200 ug/kg <83.3 ug/kgPyrene
3190 35-125Surr: 2,4,6-Tribromophenol 60.21920 ug/kg ug/kg
Page 99 of 109Page 99 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by GCMS - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0686 - SW3550C
Matrix Spike (BAC0686-MS1) Prepared: 03/28/2017 Analyzed: 03/29/2017Source: 17C0845-08
1600 45-105Surr: 2-Fluorobiphenyl 56.1896 ug/kg ug/kg
3190 35-105Surr: 2-Fluorophenol 60.71940 ug/kg ug/kg
1600 35-100Surr: Nitrobenzene-d5 58.3932 ug/kg ug/kg
3190 40-100Surr: Phenol-d5 58.41860 ug/kg ug/kg
1600 30-125Surr: p-Terphenyl-d14 70.11120 ug/kg ug/kg
Matrix Spike Dup (BAC0686-MSD1) Prepared: 03/28/2017 Analyzed: 03/29/2017Source: 17C0845-08
83.3 3330 2044-14254.8 13.4ug/kg1830 ug/kg <83.3 ug/kg1,2,4-Trichlorobenzene
83.3 3330 2020-12456.3 14.3ug/kg1880 ug/kg <83.3 ug/kg1,4-Dichlorobenzene
83.3 3330 2015-14065.2 25.1ug/kg2170 ug/kg <83.3 ug/kg4-Nitrophenol P
83.3 3330 2045-11061.6 12.6ug/kg2050 ug/kg <83.3 ug/kgAcenaphthene
83.3 3330 2040-11563.7 1.03ug/kg2120 ug/kg <83.3 ug/kgn-Nitrosodi-n-propylamine
83.3 3330 2025-12070.5 18.7ug/kg2350 ug/kg <83.3 ug/kgPentachlorophenol
83.3 3370 2040-10054.3 11.2ug/kg1830 ug/kg <83.3 ug/kgPhenol
83.3 3330 2045-12570.8 6.86ug/kg2360 ug/kg <83.3 ug/kgPyrene
3330 35-125Surr: 2,4,6-Tribromophenol 64.22140 ug/kg ug/kg
1670 45-105Surr: 2-Fluorobiphenyl 59.2987 ug/kg ug/kg
3330 35-105Surr: 2-Fluorophenol 67.42250 ug/kg ug/kg
1670 35-100Surr: Nitrobenzene-d5 62.31040 ug/kg ug/kg
3330 40-100Surr: Phenol-d5 63.32110 ug/kg ug/kg
1670 30-125Surr: p-Terphenyl-d14 69.21150 ug/kg ug/kg
Page 100 of 109Page 100 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Hydrocarbons by GC - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0670 - SW8100
Blank (BAC0670-BLK1) Prepared: 03/27/2017 Analyzed: 03/29/2017
10.0 mg/kg<10.0 mg/kgTPH-Semi-Volatiles (DRO)
5.00 40-160Surr: Pentacosane 73.13.65 mg/kg
LCS (BAC0670-BS1) Prepared: 03/27/2017 Analyzed: 03/29/2017
10.0 98.4 40-16056.8mg/kg55.9 mg/kg mg/kgTPH-Semi-Volatiles (DRO)
5.00 40-160Surr: Pentacosane 64.13.20 mg/kg mg/kg
Matrix Spike (BAC0670-MS1) Prepared: 03/27/2017 Analyzed: 03/29/2017Source: 17C0824-01
10.0 97.7 40-16055.5mg/kg54.2 mg/kg <10.0 mg/kgTPH-Semi-Volatiles (DRO)
4.96 40-160Surr: Pentacosane 70.53.50 mg/kg mg/kg
Matrix Spike Dup (BAC0670-MSD1) Prepared: 03/27/2017 Analyzed: 03/29/2017Source: 17C0824-01
10.0 99.0 2040-16090.1 48.8mg/kg89.2 mg/kg <10.0 mg/kgTPH-Semi-Volatiles (DRO) P
5.03 40-160Surr: Pentacosane 75.83.81 mg/kg mg/kg
Page 101 of 109Page 101 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Wet Chemistry Analysis - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAC0671 - No Prep Wet Chem
Blank (BAC0671-BLK1) Prepared: 03/27/2017 Analyzed: 03/28/2017
0.005 mg/kg<0.005 mg/kgChromium, Hexavalent
LCS (BAC0671-BS1) Prepared: 03/27/2017 Analyzed: 03/28/2017
0.005 0.100 80-12099.0mg/kg0.10 mg/kg mg/kgChromium, Hexavalent
Matrix Spike (BAC0671-MS1) Prepared: 03/27/2017 Analyzed: 03/28/2017Source: 17C0845-08
0.005 0.100 80-120mg/kg<0.005 mg/kg <0.005 mg/kgChromium, Hexavalent M
Matrix Spike Dup (BAC0671-MSD1) Prepared: 03/27/2017 Analyzed: 03/28/2017Source: 17C0845-08
0.005 0.100 2080-120mg/kg<0.005 mg/kg <0.005 mg/kgChromium, Hexavalent M
Page 102 of 109Page 102 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
SW1311 in Solids
Extraction Fluid, Metals VELAP
SW6010C in Non-Potable Water
Arsenic VELAP,WVDEP
Barium VELAP,WVDEP
Cadmium VELAP,WVDEP
Chromium VELAP,WVDEP
Lead VELAP,WVDEP
Selenium VELAP,WVDEP
Silver VELAP,WVDEP
SW6010C in Solids
Antimony VELAP
Arsenic VELAP
Beryllium VELAP
Cadmium VELAP,WVDEP
Chromium VELAP
Copper VELAP
Lead VELAP,WVDEP
Nickel VELAP
Selenium VELAP,WVDEP
Silver VELAP,WVDEP
Thallium VELAP
Zinc VELAP
SW7196A in Solids
Chromium, Hexavalent VELAP
SW7470A in Non-Potable Water
Mercury VELAP,WVDEP
SW7471B in Solids
Mercury VELAP,WVDEP
SW8015C in Solids
TPH-Semi-Volatiles (DRO) VELAP,NC,WVDEP
TPH-Volatiles (GRO) VELAP,NC,WVDEP
SW8260B in Solids
1,1,1,2-Tetrachloroethane NC,VELAP,WVDEP
1,1,1-Trichloroethane NC,VELAP,WVDEP
1,1,2,2-Tetrachloroethane NC,VELAP,WVDEP
Page 103 of 109Page 103 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
1,1,2-Trichloroethane NC,VELAP,WVDEP
1,1-Dichloroethane NC,VELAP,WVDEP
1,1-Dichloroethylene NC,VELAP,WVDEP
1,1-Dichloropropene NC,VELAP,WVDEP
1,2,3-Trichlorobenzene NC,VELAP,WVDEP
1,2,3-Trichloropropane NC,VELAP,WVDEP
1,2,4-Trichlorobenzene NC,VELAP,WVDEP
1,2,4-Trimethylbenzene NC,VELAP,WVDEP
1,2-Dibromo-3-chloropropane (DBCP) NC,VELAP,WVDEP
1,2-Dibromoethane (EDB) NC,VELAP,WVDEP
1,2-Dichlorobenzene NC,VELAP,WVDEP
1,2-Dichloroethane NC,VELAP,WVDEP
1,2-Dichloropropane NC,VELAP,WVDEP
1,3,5-Trimethylbenzene NC,VELAP,WVDEP
1,3-Dichlorobenzene NC,VELAP,WVDEP
1,3-Dichloropropane NC,VELAP,WVDEP
1,4-Dichlorobenzene NC,VELAP,WVDEP
2,2-Dichloropropane NC,VELAP,WVDEP
2-Butanone (MEK) NC,VELAP,WVDEP
2-Chlorotoluene NC,VELAP,WVDEP
2-Hexanone (MBK) NC,VELAP,WVDEP
4-Chlorotoluene NC,VELAP,WVDEP
4-Isopropyltoluene NC,VELAP,WVDEP
4-Methyl-2-pentanone (MIBK) NC,VELAP,WVDEP
Acetone NC,VELAP,WVDEP
Benzene NC,VELAP,WVDEP
Bromobenzene NC,VELAP,WVDEP
Bromochloromethane NC,VELAP,WVDEP
Bromodichloromethane NC,VELAP,WVDEP
Bromoform NC,VELAP,WVDEP
Bromomethane NC,VELAP,WVDEP
Carbon disulfide NC,VELAP,WVDEP
Carbon tetrachloride NC,VELAP,WVDEP
Chlorobenzene NC,VELAP,WVDEP
Chloroethane NC,VELAP,WVDEP
Chloroform NC,VELAP,WVDEP
Chloromethane NC,VELAP,WVDEP
cis-1,2-Dichloroethylene NC,VELAP,WVDEP
Page 104 of 109Page 104 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
cis-1,3-Dichloropropene NC,VELAP,WVDEP
Dibromochloromethane NC,WVDEP
Dibromomethane NC,VELAP,WVDEP
Dichlorodifluoromethane NC,VELAP,WVDEP
Di-isopropyl ether (DIPE) NC,VELAP,WVDEP
Ethanol NC,VELAP,WVDEP
Ethylbenzene NC,VELAP,WVDEP
Ethyl-t-butyl ether (ETBE) NC,VELAP,WVDEP
Hexachlorobutadiene NC,VELAP,WVDEP
Iodomethane NC,VELAP,WVDEP
Isopropylbenzene NC,VELAP,WVDEP
m+p-Xylenes NC,VELAP,WVDEP
Methylene chloride NC,VELAP,WVDEP
Methyl-t-butyl ether (MTBE) NC,VELAP,WVDEP
Naphthalene NC,VELAP,WVDEP
n-Butylbenzene NC,VELAP,WVDEP
n-Propylbenzene NC,VELAP,WVDEP
o-Xylene NC,VELAP,WVDEP
sec-Butylbenzene NC,VELAP,WVDEP
Styrene NC,VELAP,WVDEP
TAA NC,VELAP,WVDEP
TAEE NC,VELAP,WVDEP
TAME NC,VELAP,WVDEP
TBA NC,VELAP,WVDEP
tert-Butylbenzene NC,VELAP,WVDEP
Tetrachloroethylene (PCE) NC,VELAP,WVDEP
Toluene NC,VELAP,WVDEP
trans-1,2-Dichloroethylene NC,VELAP,WVDEP
trans-1,3-Dichloropropene NC,VELAP,WVDEP
Trichloroethylene NC,VELAP,WVDEP
Trichlorofluoromethane NC,VELAP,WVDEP
Vinyl acetate NC,VELAP,WVDEP
Vinyl chloride NC,VELAP,WVDEP
Xylenes, Total NC,VELAP,WVDEP
Dibromofluoromethane VELAP
SW8270D in Solids
1,2,4,5-Tetrachlorobenzene NC,VELAP,WVDEP
Page 105 of 109Page 105 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
1,2,4-Trichlorobenzene NC,VELAP,WVDEP
1,2-Dichlorobenzene NC,VELAP,WVDEP
1,2-Diphenylhydrazine NC,VELAP,WVDEP
1,3-Dichlorobenzene NC,VELAP,WVDEP
1,4-Dichlorobenzene NC,VELAP,WVDEP
1-Chloronaphthalene NC,VELAP,WVDEP
1-Naphthylamine NC,VELAP,WVDEP
2,3,4,6-Tetrachlorophenol NC,VELAP,WVDEP
2,4,5-Trichlorophenol NC,VELAP,WVDEP
2,4,6-Trichlorophenol NC,VELAP,WVDEP
2,4-Dichlorophenol NC,VELAP,WVDEP
2,4-Dimethylphenol NC,VELAP,WVDEP
2,4-Dinitrophenol NC,VELAP,WVDEP
2,4-Dinitrotoluene NC,VELAP,WVDEP
2,6-Dichlorophenol NC,VELAP,WVDEP
2,6-Dinitrotoluene NC,VELAP,WVDEP
2-Chloronaphthalene NC,VELAP,WVDEP
2-Chlorophenol NC,VELAP,WVDEP
2-Methylnaphthalene NC,VELAP,WVDEP
2-Naphthylamine NC,VELAP,WVDEP
2-Nitroaniline NC,VELAP,WVDEP
2-Nitrophenol NC,VELAP,WVDEP
3-Methylcholanthrene NC,VELAP,WVDEP
3-Nitroaniline NC,VELAP,WVDEP
4,6-Dinitro-2-methylphenol NC,VELAP,WVDEP
4-Aminobiphenyl NC,VELAP,WVDEP
4-Bromophenyl phenyl ether NC,VELAP,WVDEP
4-Chloroaniline NC,VELAP,WVDEP
4-Chlorophenyl phenyl ether NC,VELAP,WVDEP
4-Nitroaniline NC,VELAP,WVDEP
4-Nitrophenol NC,VELAP,WVDEP
7,12-Dimethylbenz (a) anthracene NC,VELAP,WVDEP
Acenaphthene NC,VELAP,WVDEP
Acenaphthylene NC,VELAP,WVDEP
Acetophenone NC,VELAP,WVDEP
Aniline NC,VELAP,WVDEP
Anthracene NC,VELAP,WVDEP
Benzidine NC,VELAP,WVDEP
Page 106 of 109Page 106 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Benzo (a) anthracene NC,VELAP,WVDEP
Benzo (a) pyrene NC,VELAP,WVDEP
Benzo (b) fluoranthene NC,VELAP,WVDEP
Benzo (g,h,i) perylene NC,VELAP,WVDEP
Benzo (k) fluoranthene NC,VELAP,WVDEP
Benzoic acid NC,VELAP,WVDEP
Benzyl alcohol NC,VELAP,WVDEP
bis (2-Chloroethoxy) methane NC,VELAP,WVDEP
bis (2-Chloroethyl) ether NC,VELAP,WVDEP
2,2'-Oxybis (1-chloropropane) NC,VELAP,WVDEP
bis (2-Ethylhexyl) phthalate NC,VELAP,WVDEP
Butyl benzyl phthalate NC,VELAP,WVDEP
Chrysene NC,VELAP,WVDEP
Dibenz (a,h) anthracene NC,VELAP,WVDEP
Dibenz (a,j) acridine NC,VELAP,WVDEP
Dibenzofuran NC,VELAP,WVDEP
Diethyl phthalate NC,VELAP,WVDEP
Dimethyl phthalate NC,VELAP,WVDEP
Di-n-butyl phthalate NC,VELAP,WVDEP
Di-n-octyl phthalate NC,VELAP,WVDEP
Diphenylamine NC,VELAP,WVDEP
Ethyl methanesulfonate NC,VELAP,WVDEP
Fluoranthene NC,VELAP,WVDEP
Fluorene NC,VELAP,WVDEP
Hexachlorobenzene NC,VELAP,WVDEP
Hexachlorobutadiene NC,VELAP,WVDEP
Hexachlorocyclopentadiene NC,VELAP,WVDEP
Hexachloroethane NC,VELAP,WVDEP
Indeno (1,2,3-cd) pyrene NC,VELAP,WVDEP
Isophorone NC,VELAP,WVDEP
m+p-Cresols NC,VELAP,WVDEP
Methyl methanesulfonate NC,VELAP,WVDEP
Naphthalene NC,VELAP,WVDEP
Nitrobenzene NC,VELAP,WVDEP
n-Nitrosodimethylamine NC,VELAP,WVDEP
n-Nitrosodi-n-butylamine NC,VELAP,WVDEP
n-Nitrosodi-n-propylamine NC,VELAP,WVDEP
n-Nitrosodiphenylamine NC,VELAP,WVDEP
Page 107 of 109Page 107 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
n-Nitrosopiperidine NC,VELAP,WVDEP
o+m+p-Cresols NC,VELAP,WVDEP
o-Cresol NC,VELAP,WVDEP
p-(Dimethylamino) azobenzene NC,VELAP,WVDEP
p-Chloro-m-cresol NC,VELAP,WVDEP
Pentachloronitrobenzene (quintozene) NC,WVDEP
Pentachlorophenol NC,VELAP,WVDEP
Phenacetin NC,VELAP,WVDEP
Phenanthrene NC,VELAP,WVDEP
Phenol NC,VELAP,WVDEP
Pronamide NC,VELAP,WVDEP
Pyrene NC,VELAP,WVDEP
Pyridine NC,VELAP,WVDEP
Code Description Lab Number Expires
341 12/31/2017Maryland DE Drinking WaterMdDOE
495 12/31/2017North Carolina DENRNC
001 10/31/2017NELAC-PennsylvaniaPADEP
460021 06/15/2017NELAC-Virginia Certificate #8886VELAP
350 11/30/2017West Virginia DEPWVDEP
Page 108 of 109Page 108 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Summary of Data Qualifiers
C Continuing calibarion verification response for this analyte is outside specifications.
L LCS recovery is outside of established acceptance limits
M Matrix spike recovery is outside established acceptance limits
P Duplicate analysis does not meet the acceptance criteria for precision
S Surrogate recovery was outside acceptance criteria
Relative Percent DifferenceRPD
QualifersQual
Denotes sample was re-analyzed-RE
Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F.
TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library .
A TIC spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations are estimated
and are calculated using an internal standard response factor of 1.
PCBs, Total Total PCBs are defined as the sum of detected Aroclors 1016, 1221, 1232, 1248, 1254, 1260, 1262, and 1268.
Page 109 of 109Page 109 of 111
Page 110 of 111
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
3/31/2017 15:28
COR Water Purification Plant Feeder Channel
Final Report
Samples Received at: 2.20°C
How were samples received?
NA
Sample Conditions Checklist
NA
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Walk In
Work Order Comments
Were Custody Seals used? If so, were they received intact?
Are the custody papers filled out completely and correctly?
Do all bottle labels agree with custody papers?
Is the temperature blank or representative sample within acceptable limits? (above freezing to 6°C) or received on ice and
recently taken?
Are all samples within holding time for requested laboratory tests?
Is a sufficient amount of sample provided to perform the tests included?
Are all samples in appropriate containers for the analyses requested?
Were volatile organic containers received?
Are all volatile organic and TOX containers free of headspace?
Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011, EPA504, EPA8260, EPA624,
EPA8015 GRO, EPA8021, EPA524, and RSK-175.
Are all samples received appropriately preserved? Note that metals containers do not require field preservation but lab
preservation may delay analysis.
As per Joe Felton the samples received with illegible labels are "RL-S-51A+51B".
BAR 03/24/17 1453
Page 111 of 111
1941 Reymet Road l Richmond, Virginia 23237 l Tel: (804)-358-8295 Fax: (804)-358-8297
Laboratory Order ID 17D0241
Certificate of Analysis
Client Name:
Enclosed are the results of analyses for samples received by the laboratory on 04/07/2017 14:20. If you
have any questions concerning this report, please feel free to contact the laboratory.
Sincerely,
Ted Soyars
Laboratory Manager
Richmond, VA 23235
9030 Stony Point Parkway, Suite 220
Purchase Order:
46510-003Project Number:
Date Issued:
Date Received:
Submitted To:
Client Site I.D.:
April 14, 2017 12:02
April 7, 2017 14:20Whitman, Requardt & Associates, LLP - Richmond
Joe Felton
End Notes:
The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.
Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen,
temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely
short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler
included in the Certificate of Analysis are done so at the client�s request and are not included in the laboratory�s fields of certification
nor have they been audited for adherence to a reference method or procedure.
The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified.
For a complete list of the Laboratory�s NELAC certified parameters please contact customer service.
This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air
Water & Soil Laboratories, Inc.
COR WPP Feeder Channel Sediment Testing
Final Report
Page 1 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
ANALYTICAL REPORT FOR SAMPLES
Laboratory Order ID 17D0241
MatrixSample ID Laboratory ID Date Sampled Date Received
RL-S-1 to RL-S-4 17D0241-05 04/07/2017 14:20Soil 03/21/2017 13:00 to 03/21/2017 14:00
RL-S-53A + 53B 17D0241-06 04/07/2017 14:20Soil 04/06/2017 15:15
Results have been calculated based on dry weight.
The Certificate of Analysis is being re-issued on 4-13-17 to reflect final VS results.
The Certificate of Analysis is being reissued on 4-14-17 to report VS results in percentages.
Page 2 of 7Page 2 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17D0241
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
03/21/2017 14:00Date/Time Sampled:
RL-S-1 to RL-S-4 Laboratory Sample ID:Sample I.D. 17D0241-05
Analytical Results
Wet Chemistry Analysis
SM18 2540G 93.5 % JCM0.1 105 04/07/17 14:18 04/07/17 14:18Percent Moisture
SM18 2540G 6.46 % JCM0.10 105 04/07/17 14:18 04/07/17 14:18Percent Solids
SM22
2540G-2011
31.9 % DLF0.0200 105RE1 04/10/17 15:30 04/10/17 15:30Volatile Solids
Page 3 of 7Page 3 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Laboratory Order ID: 17D0241
ResultParameter
Reporting
LimitMethod Qual AnalystAnalysis
Date/TimeD.F. Samp IDSample Prep
Date/Time
04/06/2017 15:15Date/Time Sampled:
RL-S-53A + 53B Laboratory Sample ID:Sample I.D. 17D0241-06
Analytical Results
Wet Chemistry Analysis
SM18 2540G 89.5 % JCM0.1 106 04/07/17 14:18 04/07/17 14:18Percent Moisture
SM18 2540G 10.5 % JCM0.10 106 04/07/17 14:18 04/07/17 14:18Percent Solids
SM22
2540G-2011
27.7 % DLF0.0200 106RE1 04/10/17 15:30 04/10/17 15:30Volatile Solids
Analytical Summary
Sample IDPreparation Factors
Initial / FinalSequence ID Calibration IDBatch IDMethod
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
17D0241-05 BAD0167 SAD0184SM18 2540G 1.00 g / 1.00 mL
17D0241-06 BAD0167 SAD0184SM18 2540G 1.00 g / 1.00 mL
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
17D0241-05 BAD0206 SAD0288SM22 2540G-2011 11.4 g / 11.4 mL
17D0241-05RE1 BAD0206 SAD0288SM22 2540G-2011 11.4 g / 11.4 mL
17D0241-06 BAD0206 SAD0288SM22 2540G-2011 11.3 g / 11.3 mL
17D0241-06RE1 BAD0206 SAD0288SM22 2540G-2011 11.3 g / 11.3 mL
Page 4 of 7Page 4 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Wet Chemistry Analysis - Quality Control
Air Water and Soil Laboratories, Inc.
Batch BAD0167 - No Prep Wet Chem
Blank (BAD0167-BLK1) Prepared & Analyzed: 04/07/2017
0.10 %100 %Percent Solids
0.1 %<0.1 %Percent Moisture
Duplicate (BAD0167-DUP1) Prepared & Analyzed: 04/07/2017Source: 17D0241-06
0.10 201.62%10.6 % 10.5 %Percent Solids
0.1 200.192%89.4 % 89.5 %Percent Moisture
Batch BAD0206 - No Prep Wet Chem
Blank (BAD0206-BLK1) Prepared & Analyzed: 04/10/2017
0.0200 %0.0229 %Volatile Solids B
Duplicate (BAD0206-DUP1) Prepared & Analyzed: 04/10/2017Source: 17D0241-06
0.0200 203.33%26.7 % 27.6 %Volatile Solids
Duplicate (BAD0206-DUP2) Prepared & Analyzed: 04/10/2017Source: 17D0241-06RE1
0.0200 203.27%26.8 % 27.7 %Volatile Solids
Page 5 of 7Page 5 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Code Description Lab Number Expires
341 12/31/2017Maryland DE Drinking WaterMdDOE
495 12/31/2017North Carolina DENRNC
001 10/31/2017NELAC-PennsylvaniaPADEP
460021 06/15/2017NELAC-Virginia Certificate #9035VELAP
350 11/30/2017West Virginia DEPWVDEP
Page 6 of 7Page 6 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Summary of Data Qualifiers
B Blank contamination. The recorded result is associated with a contaminated blank.
Relative Percent DifferenceRPD
QualifersQual
Denotes sample was re-analyzed-RE
Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F.
TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral library .
A TIC spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations are estimated
and are calculated using an internal standard response factor of 1.
PCBs, Total Total PCBs are defined as the sum of detected Aroclors 1016, 1221, 1232, 1248, 1254, 1260, 1262, and 1268.
Page 7 of 7Page 7 of 10
Page 8 of 10
Page 9 of 10
Client Site I.D.:
Project Number:Submitted To:
Date Issued:Whitman, Requardt & Associates, LLP - Richmond
9030 Stony Point Parkway, Suite 220
46510-003Joe Felton
Richmond VA, 23235
1941 Reymet Road l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297
Certificate of Analysis
Client Name:
Purchase Order:
4/14/2017 12:02
COR WPP Feeder Channel Sediment Testing
Final Report
Samples Received at: 0.20°C
How were samples received?
NA
Sample Conditions Checklist
NA
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
Walk In
Work Order Comments
Were Custody Seals used? If so, were they received intact?
Are the custody papers filled out completely and correctly?
Do all bottle labels agree with custody papers?
Is the temperature blank or representative sample within acceptable limits? (above freezing to 6°C) or received on ice and
recently taken?
Are all samples within holding time for requested laboratory tests?
Is a sufficient amount of sample provided to perform the tests included?
Are all samples in appropriate containers for the analyses requested?
Were volatile organic containers received?
Are all volatile organic and TOX containers free of headspace?
Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011, EPA504, EPA8260, EPA624,
EPA8015 GRO, EPA8021, EPA524, and RSK-175.
Are all samples received appropriately preserved? Note that metals containers do not require field preservation but lab
preservation may delay analysis.
As per Joe Felton, Work Order 17C0754 to be relogged and samples RL-S-1 to
RL-S-4 to be composited and analyzed for percent moisture, percent solids on a next
day TAT.
Volatile Solids to be analyzed on a 2 day TAT.
Work Order 17C0845 to be relogged and RL-S- 53a+ 53 b analyzed for percent
moisture, percent solids on a next day TAT.
Volatile Solids to be analyzed on a 2 day TAT.
Analyze volatile solids outside of holding time. MMB 4/7/17 14:20
Page 10 of 10
Supplement C Summary Sheet of Lagoon Residuals Removal since 2004
City of Richmond Department of Public UtilitiesLagoon Residuals Removal, Phase 4Contract #1800011316Purchase Order #19000002938
Summary Sheetof
Lagoon Residuals Removal, Phase 4
MONTH
MONTHLY DRY TONS
REMOVED
TOTAL DRY TONS
REMOVEDTOTAL TONS REMAINING
AVERAGE %TS
AVERAGE TRUCK GROSS
WEIGHT (LBS)
AVERAGE RESIDUALS REMOVED
PER TRUCK (LBS)
PAYMENT TO MOBILE FOR
SOLIDS REMOVAL THIS MONTH
REMAINING CONTRACT
FUNDING FOR SOLIDS REMOVAL
CONTRACT #1800011316 4,000.00 Cost per Ton $ 299.00 $ 1,196,000.00
May-18 0.00 0.00 4,000.00 NA NA NA -$ 1,196,000.00$ June-18 585.87 585.87 3,414.13 19.21 73,870 43,884 175,175.13$ 1,020,824.87$ July-18 775.14 1,361.01 2,638.99 19.68 76,172 46,330 231,766.86$ 789,058.01$
August-18 1,108.97 2,469.98 1,530.02 23.30 78,345 47,942 331,582.03$ 457,475.98$ September-18 940.18 3,410.16 589.84 26.38 77,989 47,702 281,113.82$ 176,362.16$
October-18 600.38 4,010.54 -10.54 18.96 77,220 47,190 179,513.62$ (3,151.46)$
TOTAL THIS CONTRACT PERIOD 4,010.54 1,199,151.46$
TOTAL SINCE JUNE 2004 69,481.34 16,706,082.65$
3/29/2019
Supplement D Construction Site Safety Plan for Contractors Working on or near
Hazardous Conditions at the Water Purification Plant.
Contractor Safety Revision No.: 1 July 9, 2008
15a 1
City of Richmond, Virginia Department of Public Utilities
Construction Site Safety Plan for Contractors
Working on or near Hazardous Conditions at the Water Purification Plant
The Process Safety Management (PSM) and Risk Management Plan (RMP) programs under OSHA 1910.119 and 40 CFR 68, respectively, specify that all contractors involved in performing activities that have the potential for affecting process safety, including, but not limited to, maintenance or repair, turnaround, major renovation, or specialty work, on or adjacent to the ammonia, or other covered processes are subjected to this plan. However, contractors performing demolition, construction, equipment installation, performing incidental services such as ammonia delivery, and other work that might affect the safety of a covered process are also included in this section. 1. PUBLIC CONVENIENCE AND SAFETY The Contractor shall at all times conduct the work safely and assure a safe work site. The Contractor shall be responsible for the safety of the Contractor’s employees, agents and subcontractors, City of Richmond personnel, and all other personnel or persons at the work site. The Contractor shall be responsible for the adequacy and safety of all construction methods or procedures and safe prosecution of the work. The Contractor shall be responsible at all times to conduct the work and keep the work site in compliance with federal, state, and local safety laws and regulations, including, but not limited to OSHA requirements. The Contractor shall, prior to actual construction or providing services, submit the name(s) of an authorized person who is a competent person as defined by OSHA (29 CFR 1926) responsible for site safety activities. A resume of the qualifications of the competent person must be submitted to the City of Richmond Department of Public Utilities (DPU). The resume shall include such items as: experience, education, special safety and first aid courses completed, safety conferences attended, familiarity with standards and regulations and certifications or registrations. The Contractor shall have an authorized and competent safety representative as defined above on the work site at frequent and regular intervals, or more often as conditions require. Failure to have such person at the site as specified herein constitutes an unsafe practice. The Contractor shall be responsible to suspend work whenever a work method or procedure or a condition at a work site is unsafe. The Contractor shall submit a written notification to the City of Richmond DPU of any accident or injury. (A copy of the notification shall be sent to the City of Richmond Occupational Safety and Health Specialist by the Contractor.) Failure of the Contractor to comply with these provisions, or any federal, state, or local safety laws and regulations constitutes just cause for the City of Richmond DPU to order suspension of work. None of the provisions of this section are intended to nor shall be construed to create any duty of responsibility on the City of Richmond DPU to provide or enforce safety requirements for the
Contractor Safety Revision No.: 1 July 9, 2008
15a 2
Contractor. The duty, responsibility, and liability for safety shall remain with the Contractor. Any failure of the City of Richmond DPU to suspend work or detect violation of any local, state, or federal safety standard or regulation shall in no case relieve the Contractor of the Contractor’s safety responsibility. 2. SITE SAFETY PLAN The Contractor shall file with the City of Richmond Technical Services or Operations Support Division prior to the pre-construction meeting a Site Safety Plan, which at minimum shall: Provide current documentation and other information about the contractor’s safety performance
and programs (e.g., OSHA - 200 Log for the past 5 years, written training documentation). Provide documented certifications demonstrating that each employee has received, understood
and completed the safety training program in key areas related to the PSM. (e.g., a record that contains the identity of the contract employee, the date of training, and means used to verify that the employee understood the training.)
Provide documented evidence showing compliance with confined space entry, lockout/tagout,
emergency response, and safe work practices. Provide a document or procedure describing open communications between the City of
Richmond DPU and Contractor in case the Contractor introduces a hazard to the present hazardous work area.
Name key personnel and alternates responsible for site safety along with means of contacting
these personnel at all times. Describe the risks associated with each operation conducted.
Confirm that personnel are adequately trained to perform their job responsibilities in a safe
manner, to handle the specific hazardous situations they may encounter on the job, or conditions that apply to the Plant’s safety program and emergency response plan.
Describe the protective clothing and equipment to be worn by personnel during various site
operations. Describe the actions to be taken to mitigate existing hazards (e.g., containment of contaminated
materials) to render the work environment less hazardous. Define site control measures and include a site map.
Set forth the site’s Standard Operating Procedures (SOPs). SOPs are those activities that can be
standardized and where a checklist can be used. The SOPs will be: - Prepared in advance. - Based on the best available information, operational principles, and technical
guidance. - Field-tested by qualified health and safety professionals, and revised as appropriate. - Appropriate to the types of risk at the site.
Contractor Safety Revision No.: 1 July 9, 2008
15a 3
- Formulated to be easy to understand and practice. - Provided in writing to all site personnel who will be briefed on their use. - Included in training programs for site personnel.
Set forth a Contingency Plan for safe and effective response to emergencies.
A copy of any safety information or documentation shall be supplied to the City of Richmond Water Purification and Pumping, Technical Services, or Operations Support Division. In addition, the Contractor shall comply with all safety requirements outlined in the bidding procedures pertaining to the work being performed (e.g., Accident Prevention, Protection of Work and Property, etc.).
Supplement E Manufacturer’s Certificate of Proper Installation.
492599 MANUFACTURERS’ FIELD SERVICES MAY 28, 2015 01 43 33 SUPPLEMENT - 1 ©COPYRIGHT 2015 CH2M HILL
MANUFACTURER’S CERTIFICATE OF PROPER INSTALLATION
OWNER EQPT SERIAL NO: EQPT TAG NO: EQPT/SYSTEM:
PROJECT NO: SPEC. SECTION: I hereby certify that the above-referenced equipment/system has been:
(Check Applicable) Installed in accordance with Manufacturer’s recommendations.
Inspected, checked, and adjusted. Serviced with proper initial lubricants.
Electrical and mechanical connections meet quality and safety standards. All applicable safety equipment has been properly installed.
Functional tests. System has been performance tested, and meets or exceeds specified performance requirements. (When complete system of one manufacturer) Note: Attach any performance test documentation from manufacturer.
Comments:
I, the undersigned Manufacturer’s Representative, hereby certify that I am (i) a duly authorized representative of the manufacturer, (ii) empowered by the manufacturer to inspect, approve, and operate their equipment and (iii) authorized to make recommendations required to ensure equipment furnished by the manufacturer is complete and operational, except as may be otherwise indicated herein. I further certify that all information contained herein is true and accurate. Date: _________________________________, 20___
Manufacturer: By Manufacturer’s Authorized Representative: (Authorized Signature)