the in-plane distribution of density in handsheets c.t.j. dodson, y. oba and w.w. sampson on the...

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in-plane distribution of den in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper Appita J. 54, 4 (2001) 385-389.

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Page 1: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

The in-plane distribution of densityin handsheets

C.T.J. Dodson, Y. Oba and W.W. SampsonOn the distributions of mass, thickness and density of paper

Appita J. 54, 4 (2001) 385-389.

Page 2: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

• Introduction

• Measurements

• Theory

• Conclusions

Overview

Page 3: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Affects pore size distribution, ink transfer,strain distributions under tension, etc.

Formation - Distribution of Mass Density

Page 4: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Distribution of Density

• Many physical properties, e.g. tensile index, tear index, light scattering coefficient, permeability, etc. are strongly correlated with mean sheet density.

• Expect therefore that the local properties of small zones will be dependent on local density.

Page 5: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Experimental

• Sheets with a range of structures and known forming conditions.

• Measure thickness and grammage of small zones knowing the position of each measurement.

Page 6: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

3 furnishes TMPChemical S/W50:50 Blend

2 consistencies Standard5 standard

2 grammages 40 g m2

60 g m2

4 settlingtimes

10, 30, 60,120 s

48 conditions

Page 7: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Local thickness determination

• Non contacting double laser triangulation thickness tester

• Computer controlled x-y stage

• 0.5 mm pitch. Local average thickness of 1mm square zone taken as average of 4 measure- ments

• Samples marked

1 mm

Page 8: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

60

80

100

120

140

160

80 100 120 140 160 180 200Thickness from Micrometer (m m )

Thi

ckne

ss f

rom

lase

r ( m

m)

TMP

Blend

Chem SW

Page 9: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Local grammage determination

• Ambertec -formation tester.

• Same 1 mm zones measured as for thickness.

• Formation at scales between 100 mm and 7 mm measured.

Page 10: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

grammage thickness

density

Page 11: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

5

10

15

5 10 15 20

CV(z), %

CV

(),

%

TMP

Blend

Chem SW

Page 12: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

5

10

15

4 6 8 10 12 14 16

CV( ), %

CV

(r),

%

TMP

Blend

Chem SW

Linear(Chem SW)Linear(TMP)Linear(Blend)

Page 13: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

5

10

15

5 10 15 20

CV(z ), %

CV

(r),

%

TMP

Blend

Chem SW

Linear(Chem SW)Linear(TMP)Linear(Blend)

Page 14: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

0.3

0.4

0.5

0.6

4 6 8 10 12 14 16

CV( ), %

Mea

n de

nsity

, r (

g m

-2)

TMP

Blend

Chem SW

Page 15: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

30 35 40 45 50 55 60

60

80

100

120T

hick

ness

, mm

Grammage, g m-2

Page 16: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Theory

zCV

zzCov

CVz

~~,

~2~

~

~)~(Var 22

2

r

If thickness and grammage are bivariate normally distributed we have:

where zzzCov ~~~,~

and if rr ~

zCVCVz

~~~

~)~(Var 22

2

r

Page 17: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

0

10

20

30

40

0 10 20 30 40

Var(r) determined experimentally, (g 2 cm -6 x 104)

Var

(r)

from

ful

l Biv

. Nor

m.,

( g2 c

m-6

x 1

04 )

TMPBlendChem SW

Page 18: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

0

10

20

30

40

0 10 20 30 40

Var(r) determined experimentally, (g 2 cm -6 x 104)

Var

(r)

from

app

x. B

iv. N

orm

., ( g

2 cm

-6 x

104 )

TMPBlendChem SW

Page 19: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

5.0

7.5

10.0

12.5

15.0

5.0 7.5 10.0 12.5 15.0

Experimental CV(r), %

Biv

. Nor

m. C

V(r

), %

TMPBlendChem SW

Page 20: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

0

5

10

15

0 5 10 15

Experimental CV(r), %

App

x. B

iv. N

orm

. CV

(r),

%TMPBlendChem SW

Page 21: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Conclusions

• Coefficients of variation of thickness and grammage are linearly dependent and independent of furnish.

• Bulk structure dominated by presence of TMP in blended furnish.

• Mean thickness depends on formation.

Page 22: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

• Relationship between local grammage and thickness is well described by the Bivariate normal distribution.

• An approximate model slightly under- estimates density variation.

Page 23: The in-plane distribution of density in handsheets C.T.J. Dodson, Y. Oba and W.W. Sampson On the distributions of mass, thickness and density of paper

Acknowledgments

Funding: Oji Paper Company Ltd., Japan