the use of headspace with sample concentration to meet alberta tier 1 voc guidelines

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The Use of Headspace With Sample Concentration to Meet Alberta Tier 1 VOC Guidelines Pat Steffes K’(Prime) Technologies Inc. April 25, 2013

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The Use of Headspace With Sample Concentration to Meet Alberta Tier 1 VOC Guidelines. Pat Steffes K’(Prime) Technologies Inc. April 25, 2013. Purge and Trap. Current Techniques. Traditional Headspace. CTC Headspace. ITEX (In-Tube Extraction). ITEX Technique. Chromatography. - PowerPoint PPT Presentation

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Page 1: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

The Use of Headspace With Sample Concentration to MeetAlberta Tier 1 VOC Guidelines

Pat Steffes

K’(Prime) Technologies Inc.

April 25, 2013

Page 3: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

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ITEX (In-Tube Extraction)

Page 4: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

ITEX

Tech

niq

ue

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Page 5: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

Chromatography

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Page 6: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

Calibration Curve

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Page 7: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

0.1 ppb Vinyl Chloride Standard

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Page 8: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

Integration of Carbon Tetrachloride at 0.4 ppb

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Page 9: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

Further Work

• Determine life cycle of traps and heaters

• Experiment with other trap materials

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Page 10: The Use of Headspace  With Sample Concentration  to Meet Alberta Tier 1 VOC Guidelines

Thanks Preston Kulmatycki for

application work and application note

Joe Crumbaugh and Brenda Chomin of WEALA