tive ographyhplc series 2000includes: …...high effective hplc preparative system containing u-vvis...

8
Check out brand new preparative system! • Gradient Box ECB2004 • Analytical Pump ECP2010 • Column Oven ECO2080 • UV–VIS Detector ECD2800 HPLC SERIES 2000 includes: EQUIPMENT FOR ANALYTICAL, PREPARATIVE AND FLASH LIQUID CHROMATOGRAPHY

Upload: others

Post on 22-Jul-2020

7 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

Check out

brand new

preparative

system!

•GradientBox

ECB2004

•AnalyticalPump

ECP2010

•ColumnOven

ECO2080

•UV–VISDetector

ECD2800

HPLC SERIES 2000

includes:EQUIPMENT FOR ANALYTICAL, PREPARATIVE

AND FLASH LIQUID CHROMATOGRAPHY

Page 2: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

2

preparative systems

For more information and technical specifications see pages 6 and 7. this system is controlled by eCOmaC or Clarity chromatography software.

ask us for different configuration.

Preparative pump with flow-rate up to 50, 100

or 300 ml/min

Box ECB2005 with gradient valve or ECB2006 container

for solvent bottles

Flash 14 DAD detector in versions up to 400, 600

and 840 nm

ECS10 ECS11

P/N ASP1000X ASP1100X

Gradient Preparative System Isocratic Preparative SystemDetector Flash 14 DaD 600 Flash 14 DaD 400

pump eCp2100 eCp2100

Box eCB2005 eCB2006

High effective HPLC preparative system containing Uv-vis photodiode array detector, preparative pump and gradient box.the system is variable and allows different configurations of components. Detector measuring absorbance on four wavelengths simultaneously in one cell just as whole spectrum (scan). Preparative quaternary isocratic pump with flow-rates up to 50, 100 or 300 ml/min works together with gradient box as a gradient pump, achieving a preciselow-pressure gradient. Communication of all units is through rs232.

NOTE:

System configurations

NEW

Injection

valves

and fraction

collectors

available

Choice of preparative

cells for different

flow-rates

Try ECOMAC software!

Page 3: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

3

analytiCal systems

For more information and technical specifications see pages 4 and 5. this system is controlled by Clarity Chromatography software.

ask us for different configuration.

Gradient box with degasser ECB2004 or just

a container for solvent bottles ECB2006

Analytical HPLC pump ECP2010 with flow-rate

up to 10 ml/min and pressure up to 40 MPa

Column oven ECO2080 with heating and cooling or ECO2099 with heating

only

ECD2800 / ECD2600 UV-VIS detector with continuously variable

wavelength

High effective HPLC system containing Uv-vis detector, column oven, analytical pump and gradient box. the system is va-riable and allows different configurations of components. Detector with continuously variable wavelength 190-800/600 nm and very low noise level offers high-speed sampling up to 100 Hz. Isocratic pump with flow-rate up to 10 ml/min and pressu-re limit 40 mpa works together with gradient box also as gradient pump and is equipped with four way gradient mixing valve and degasser. Column oven with peltier heating/cooling can accommodate up to 3 columns. Communication of all units is through rs232 or lan.

NOTE:

ECS01 ECS02 ECS03

ASA0100X ASA0200X ASA0300X

Gradient Analytical System Gradient Analytical System Isocratic Analytical SystemDetector eCD2800 eCD2600 eCD2600

pump eCp2010 eCp2010 eCp2100

Column Oven eCO2080 eCO2099 –

Box eCB2004 eCB2004 eCB2006

System configurations

Ask for manual or autosampler injecting options!

Units controlled by Clarity

Page 4: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

4

Clarity is advanced Chromatography Data station with optional software modules for data acquisition, data processing and instrument control. its wide range of data acquisition interfaces (a/D converters, lan, UsB, rs232) allows connection to any our unit. single instrument sW is possible extend by sW module for lC control, sW module for as control, sW module for system suitability test, sW module for pDa Data processing, single instrument add-on and Offline version for data processing.

All ECOM units drivers are included in Module LC Con-trol. Drivers contain full control of instruments as well as diagnostics tools and are made by eCOm with Dataapex supervision that guarantees the highest quality and full integration into the Clarity station.

analytiCal Units OvervieW

CLARITY Chromatography Station

ECD2800 / ECD2600 UV-VIS Detector APATITEUv-vis detector with continuously variable wavelength in the range of 190 – 800 nm (190 – 600 nm) and noise level 3x10-6 aU. Controlled by rs232, lan or using keypad. aC05 analytical cell is included.

Detector with interference filter allowing to adjust the unit at one fixed wavelength in range of 200-600nm. noise level at 254nm is 5x10-6 aU. the unit is controlled via rs232 and it is supported in software eCOmaC and Clarity.

ECD2800 P/N ADA0000X

ECD2600 P/N ADB0000X Apatite P/N DE00000X

Name P/N R [nm] NotesSeries 2000 variable wavelength, high-speed sampling 100 Hz, power supply 90-264 VeCD2800 Uv-vis detector aDa0000X 190-800 deuterium and halogen lampeCD2600 Uv-vis detector aDB0000X 190-600 deuterium lamp onlyApatite series UV-VIS fixed wavelength detector, wavelength according to used interference filterapatite De00000X filter deuterium lamp, choice of interference filters

Most commonly supplied cells available for analytical detectors (ask for other options)

Detectors

Type C Type A ECD2600ECD2800APATITE

P/N l]

name aC02 aC05 aC10 tC01 HplC 04 HplC 11 peeKl [mm] 2 5 10 test cell 5 5v [µl] 1 8 16 – 10 10thread UnF10-32 UnF10-32 UnF10-32 – – –tubing 1/16“ 1/16“ 1/16“ – 1/16“ 1/16“ml/min 10 10 10 – 10 50

C C C C A A

Page 5: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

5

analytiCal Units OvervieW

Kappa 10 P/N PK00000X

Kappa 10PP P/N PL00000X

Pumps

Name P/N F[ml/min.]

Max. press.[Mpa / PSI] D Pumping

system Notes

Series 2000 Analytical HPLC pump, isocratic / quaternary gradient with Gradient Box ECB2004eCp2010 apa0000X 0.01 – 10.00 40 / 5800 1/8“ 2x serial power supply 100-240 v aC

Kappa series Isocratic, single piston, pulsating, 40 MPa up to 2 ml/min., column washingKappa 10 pK00000X 0.01 – 10.00 40(20) / 4351 1/8“ 1x pulsating power supply 100, 115, 230 v aCKappa 10pp pl00000X 0.01 – 10.00 40(20) / 4351 1/8“ 1x pulsating pressure sensor, power supply 100, 115, 230 v aC

ECP2010 Analytical HPLC PumpWorks as isocratic pump and together with Gradi-ent Box eCB2004 also as gradient pump. Flow-rate range is 0.01–10 ml/min and pressure up to 40 mpa. Unit software includes new learning algorithm for pulsation suppression and many testing and diagnostic features.

these graphs show linear and stepped gradient (10 % steps and at the beginning and end 1 %) performed on HplC pump eCp2010 and gradient box eCB2004. this is used for measuring and testing performance criteria such as accuracy and repro-ducibility of solvent delivery system in production.

ECP2010 P/N ACA0000X

KAPPA 10 Isocratic One Piston Pump

single piston pump suited for column washing or other HplC chromatography processes.

ECB2004 Gradient Box with DegasserECB2006 Solvent Box

ECO2080 / ECO2099 Column Oven with heating and/or cooling

Box is suited for handling liquids in eCOm gradient systems. it accommodates container for solvent bot-tles, built-in high-efficiency vacuum degasser and four way gradient valve. Up to four solvent lines may be degassed simultaneously by one unit.

Four way gradient valve is controlled from the pump eCp2010. Box can be also supplied as a simple container for solvent bottles – eCB2006.

ECB2004 P/N ABA0000X

ECB2006 P/N ABC0000X

the peltier heating/cooling column oven with a big compartment room can accommodate up to 3 columns with length up to 25 cm. Unit is controlled via the keypad, rs232 or lan interface. settable overheating temperature protection to prevent destruction of

temperature sensitive columns caused by handling errors. Column oven can be also supplied only with heating option with temperature range up to 99° C as eCO2099.

ECO2080 P/N AOA0000X

ECO2099 P/N AOB0000X

Absolutelevel[1]

0

100

200

300

400

500

600

700

800

Time[min]0 2 4 6 8

LinearGradientS

tart

LinearGradientE

nd

Voltage[m

V]

0

100

200

300

400

500

600

700

800

Time[min]30 40 50 60 70

Page 6: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

30MPa

B

E

B

E

B

E

B B B

6

preparative Units OvervieWDetectors

lamp working hours are counted using built-in counter. easy flow-cell exchange.

3D evaluation of FlasH 12/14 DaD detectors is supported by Clarity sW.

NOTE:

Adapter with SMA optical connectors

all DaD detectors can be equipped with adapters allowing external cells connecting using fiber optic cables. Cells with various flow-rates with sma connectors are available.

Name P/N R [nm] Scan NotesFlash 10 DAD series diode array detectors (PDA), with display and keypad, 4 variable wavelengthsFlash 10 DaD 400 2053a00X 200-400 info standalone, 4x analog output, power supply 90-264 v

Flash 10 DaD 600 2053B00X 200-600 info standalone, 4x analog output, power supply 90-264 vFlash 10 DaD 800 2053e00X 190-840 info standalone, 4x analog output, power supply 90-264 vFlash 14 DAD series diode array detectors (PDA), without display and keypad, Clarity 3D evaluation for 400 and 800 version,

4 variable wavelengthsFlash 14 DaD 400 ana0000X 200-400 Full standalone, power supply 90-264 vFlash 14 DaD 600 anB0000X 200-600 info standalone, power supply 90-264 vFlash 14 DaD 800 anC0000X 190-840 Full standalone, power supply 90-264 vFlash 06/12 DAD series diode array detectors (PDA), without display and keypad, Clarity 3D evaluation for 400 and 800 version,

4 variable wavelengthsFlash 12 DaD 400 2046000X 200-400 Full built-in, power supply 24-36 v DCFlash 06 DaD 600 2050000X 200-600 info built-in, power supply 24-36 v DCFlash 12 DaD 800 2052000X 190-840 Full built-in, power supply 24-36 v DC

FlasH detectors are designed for preparative and flash applications, with four continuously variable wavelength in the range listed for each instrument. noise level of FlasH detectors is at 254 nm 5x10-6 aU with an empty cell.All DAD detectors are available in version with optical connectors for external flow cells.

Most commonly supplied cells available for preparative detectors (ask for other options)

Type B

All Flash DAD detectorsname plCC 07 plCC 15 plCC 3l plCC 19 peeK plCC Hp HplC 09 peeKl [mm] 0.3 0.3 0.3 2.4 0.5 - 1.0 10v [µl] 40 40 80 70 20 20thread UnF10-32 1/4 “ - 28 5/16“ - 24 1/4 “ - 28 5/16“ - 24 UnF 10-32tubing 1/16“ 1/8“ 3/16“ 1/8“ 1/8“ 1/16“ml/min 200 500 3 000 500 500 50

Type EExternal cells with SMA optical connectors

l]

name plCC 19 eX peeK HplC 10 eX plCC 20 plusl [mm] 2.4 5 0.3v [µl] 70 10 220thread 1/4 “ - 28 UnF 10-32 npt 1/4 “ - 18tubing 1/8“ 1/16“ 1/2“ml/min 500 50 15 000

Flash 10 DAD Flash 06/12 DADFlash 14 DAD

Page 7: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

7

eCOmaC software is designed with maximal effort to do easy operation of ECOM chromatographic units. it is user friendly, but sophisticated for fraction collectingand preparative applications. it is suited for unitscontrolling and data collecting.

Program most important features:- easy installation- Connection using UsB, rs232 or ethernet (lan)- no need of a/D converter- Units controlling and data collecting from one place- smart marks, fractions collecting- Data export in various formats (tXt,mat,netCDF ...)- secured access througt users accounts- low hardware requirements for application itself

ECOMAC CHROMATOGRAPHIC SOFTWARE - PREPARATIVE

preparative Units OvervieW

ECP2050, 2100, 2300 Iota 50, 100, 300Theta 50, 100, 300

Pumps

all DaD detectors have numerous self-test functions, such as error messages, which allow easy problem identification and testing. test sW used in production releases valid production report only for units which met all requirements. Test report contains stored setting parameters, lamp working hours, lamp starting voltage and current, wavelength adjusting accuracy, lamp intensity and many other information. For service purpose is available service SW which allows comfortable units testing and diagnostics, ena-bling sending diagnostic report to service center easily, helping to simplify and speed up communication with them.

TESTING AND SERVICE TOOLS

Name P/N F[ml/min.]

Max. press.[MPa / PSI] D Pumping

system Notes

Series 2000 preparative HPLC pump, isocratic / gradient with Gradient Box ECB2005eCp2050 aCC0000X 0.1 – 50 30 / 4351 3/8“ 2x parallel standalone, power supply 90-264 v aC

eCp2100 aCD0000X 1 – 100 15 / 2176 3/8“ 2x parallel standalone, power supply 90-264 v aC

eCp2300 aCe0000X 1 – 300 7.5 / 1015 3/8“ 2x parallel standalone, power supply 90-264 v aC

Theta series isocratic, built-in, without pressure sensor

theta 50 pt00000X 0.1 – 50 30 / 4351 3/8“ 2x parallel built-in, power supply 24-36 v DC

theta 100 ptC0000X 1 – 100 15 / 2176 3/8“ 2x parallel built-in, power supply 24-36 v DC

theta 300 ptD0000X 1 – 300 7.5 / 1015 3/8“ 2x parallel built-in, power supply 24-36 v DC

Iota series isocratic, built-in, with pressure sensor

iota 50 pyF0000X 0.1 – 50 30 / 4351 3/8“ 2x parallel built-in, power supply 24-36 v DC

iota 100 pye00000 1 – 100 15 / 2176 3/8“ 2x parallel built-in, power supply 24-36 v DC

iota 300 py00000X 1 – 300 7.5 / 1015 3/8“ 2x parallel built-in, power supply 24-36 v DC

Page 8: TIVE OGRAPHYHPLC SERIES 2000includes: …...High effective HPLC preparative system containing U-vvis photodiode array detector, preparative pump and gradient box. the system is variable

VisitECOM

in Prague!

www.Instrument-Solutions.comTel: +31(0)88 4678 786 / Fax: +31(0)88 4678799De Liesbosch 50 - 3439 LC Nieuwegein (NLD)Instrument Solutions Benelux BV

[email protected]