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    A project report

    On

    To study the effect of heat treatment processes on the

    properties of Aluminum 6063 alloy

    Submitted for partial fulfillment of award of

    BACHELOR OF TECHNOLOGY

    Degree

    In

    Mechanical Engineering

    By

    Navneet Verma 0713340063

    Bhuvneshwar Prasad Panchal 0713340029

    Nikhil Kumar Singh 0713340064

    Ajay Kumar 0713340003

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    Name of guide

    Mr. Sandeep Chauhan

    MECHANICAL ENGINEERING DEPARTMENT

    NOIDA INSTITUTE OF ENGINEERING & TECHNOLOGY

    Greater Noida

    DECLARATION

    We hereby declare that this submission is our own work and that, to the best of

    our knowledge and belief, it contains no material previously published or written

    by another person nor material which to a substantial extent has been accepted

    for the award of any other degree or diploma of the university or other institute

    of higher learning, except where due acknowledgment has been made in the text.

    Bhuvneshwar Prasad Panchal

    Navneet Verma

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    Nikhil Kumar Singh

    Ajay Kumar

    CERTIFICATE

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    Certified that Navneet Verma, Bhuvneshwar Prasad

    Panchal, Ajay Kumar, Nikhil Kumar Singh have carried

    out the research work presented in this project entitled To

    study the effects of heat treatment processes on the

    properties of Aluminum 6063 alloy for the award of

    Bachelor Of Technology Degree from Uttar Pradesh

    Technical University, Lucknow under my supervision. The

    project embodies result of original work and studies carried

    out by Student himself and the contents of the project do not

    form the basis for the award of any other degree to the

    candidate or to anybody else.

    Mr. Sandeep Chauhan

    Sr. Lecturer

    NIET, Gr.Noida

    Date: June 2011

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    ACKNOWLEDGEMENT

    I believe that hard work is the only way to success to achieve something

    worthy.

    With feeling of immense gratitude and respect, I extend my deep sense of

    gratitude to thank my guide Mr. SANDEEP CHAUHAN for their continuous

    support throughout this work. Their incredulous guiding spirit and helping handat every step of my project has led to its successful completion.

    This project was a learning experience for me. Workings in different labs

    provide a real time experience of engineering. & technology being used,

    currently, in manufacturing industry.

    Finally I would like to thank Mr.Mahipal without their help this project would

    not have been possible and their support during this period has been inspired me

    to accomplish it.

    Bhuvneshwar Prasad Panchal (0713340029)

    Ajay Kumar (0713340003)

    Navneet Verma (0713340063)

    Nikhil Kumar Singh (0713340064)

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    TABLE OF CONTENTS

    Declaration iCertificate iiAcknowledgement iiiTable of Contents ivList of Figure vList of Table viAbstract

    Chapter 1- Introduction 01-19

    1.1 Introduction of Heat Treatment 01

    1.1.1.Stages Of Heat Treatment And Its Purposes 03

    1.2 The Objects Of Heat Treating Aluminium And Its Alloys 05

    1.3. Classification Of Heat Treatment 06

    1.4. Tempering 07

    1.5. Annealing 071.5.1. Objectives Of Annealing 081.5.2. Stages Of Annealing 08

    1.6. Normalizing 08

    1.6.1. Objectives Of Normalizing 09

    1.7. Hardening 091.7.1. Objectives Of Hardening 10

    1.8. Heat Treatment: Capabilities And Limitations 10

    1.9. Introduction Of Aluminium 11

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    1.9.1. Characteristics 121.9.2. Applications 131.9.3. Aluminium Alloys 14

    1.9.3.1. Aluminium Alloys In Structural Applications 151.9.3.2. Aluminium6063 Alloy 161.9.3.3. Chemical Composition Of Aluminium6063 Alloy 171.9.3.4. Physical Properties 171.9.3.5. Mechanical Properties 17

    1.10. Important Mechanical Properties 18

    Chapter 2- Literature Review 20-23

    2.1. Literature Review 21

    Chapter 3- Methodology Of Test Performed 24-29

    3.1. Methodology Of Project 25

    3.2. Test Performed On Aluminium 6063 Alloy 263.2.1. Tensile Test 26

    3.2.1.1. Tensile Test Specimen 26

    3.2.2. Izod Impact Test 27

    3.2.3. Charpy Impact Test 28

    3.2.4. Rockwell Hardness Test 28

    Chapter 4- Results And Analysis 30-44

    4.1. Test Performed 314.1.1. Tensile Test 31

    4.1.2. Impact Test By Izod Method 374.1.3. Impact Test By Charpy Method 39

    4.1.4. Rockwell Hardness Test 42

    4.2. Microstructures Of Aluminium 6063 Alloy 44

    Chapter 5- Conclusion 45

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    5.1. Conclusion 46

    5.2. Future Scope Of Aluminium 6063 Alloy 46

    References 47Appendix 1 48

    Appendix 2 50

    LIST OF FIGURES

    S.No. Title Page No.

    Fig 4.1 Tensile Test Specimen 32

    Fig 4.2 Izod Test Specimen 38

    Fig 4.3 Charpy Test Specimen 40

    Fig 5.1 Microstructure After Quenching 44

    Fig 5.2 Microstructure After Normalizing 44

    Fig 5.3 Microstructure After Annealing 44

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    LIST OF TABELS

    S.No. Title Page No.

    4.1 Tensile Test Table Before Heat Treatment 31

    4.2 Tensile Test Table After Normalizing 32

    4.3 Tensile Test Table After Quenching 34

    4.4 Tensile Test Table After Annealing 35

    4.5 Izod Impact Test Table Before Heat Treatment 37

    4.6 Izod Impact Test Table After Quenching 38

    4.7 Izod Impact Test Table After Normalizing 39

    4.8 Izod Impact Test Table After Annealing 39

    4.9 Charpy Impact Test Table Before Heat Treatment 40

    4.10 Charpy Impact Test Table After Quenching 41

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    4.11 Charpy Test Table After Normalizing 41

    4.12 Charpy Test Table After Annealing 42

    4.13 Rockwell Hardness Test Table Before Heat Treatment 42

    4.14 Rockwell Hardness Test Table After Quenching 43

    4.15 Rockwell Hardness Test Table After Normalizing 43

    4.16 Rockwell Hardness Test Table After Annealing 43

    ABSTRACT

    Heat treatment processes for aluminium are precision processes. Based on the objectives of

    this research, precipitate free zones in the aluminium alloy 6063 actually give bad effect to the

    mechanical properties of that alloy. The mechanical properties of the aluminium alloy should

    be altering properly to improve their behavior using precipitation hardening which one of the

    heat treatment types. Precipitation hardening is the most suitable heat treatment that should

    use to minimize the precipitate free zones in the microstructure of the aluminium alloy 6063.

    In the precipitation hardening process, the thermal and temperature condition is under control

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    with high precision to ensure the transformation of the aluminium alloy structure is in good

    condition and supervision limit. The samples of the material are placed in the furnace to make

    a heat treating process and then quench it in the water for quenching medium. The material

    testing that had been applied is based on hardness, impact and microstructure analysis. The

    purpose of the hardness testing are to find out the hardness reading for all the samples that

    used to look the wear resistance effect that occur after make a heat treating process to the

    aluminium alloy 6063. From the impact test, the purposes are to know impact energy that

    absorbed to fracture the samples of the material and then make a comparison data between

    after and before heat treatment. Lastly, for microstructure analysis it is important to determine

    because to look the narrow evaluation of precipitate free zones in the microstructure of

    aluminium alloy after make a precipitation hardening processes. From the data and result thatalready determined, it shown the positive result based on objectives and scope of this project.

    CHAPTER -1

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    INTRODUCTION

    1.1 INTRODUCTION OF HEAT TREATMENT

    Heat treatment is a group of industrialandmetal working processesused to alter thephysical, and sometimeschemical, properties of a material. The most common application is

    metallurgical. Heat treatments are also used in the manufacture of many other materials, such

    as glass. Heat treatment involves the use of heating or chilling, normally to extreme

    temperatures, to achieve a desired result such as hardening or softening of a material. Heat

    treatment techniques include annealing, case hardening, precipitation strengthening,

    tempering and quenching. It is noteworthy that while the term heat treatment applies only to

    processes where the heating and cooling are done for the specific purpose of altering

    properties intentionally, heating and cooling often occur incidentally during other

    manufacturing processes such as hot forming or welding.

    Metallic materials consist of a microstructure of small crystals called "grains" or

    crystallites. The nature of the grains (i.e. grain size and composition) is one of the most

    http://en.wikipedia.org/wiki/Industrial_processhttp://en.wikipedia.org/wiki/Industrial_processhttp://en.wikipedia.org/wiki/Metalworkinghttp://en.wikipedia.org/wiki/Metalworkinghttp://en.wikipedia.org/wiki/Metalworkinghttp://en.wikipedia.org/wiki/Physical_propertyhttp://en.wikipedia.org/wiki/Chemical_propertyhttp://en.wikipedia.org/wiki/Chemical_propertyhttp://en.wikipedia.org/wiki/Metallurgyhttp://en.wikipedia.org/wiki/Glasshttp://en.wikipedia.org/wiki/Annealing_(metallurgy)http://en.wikipedia.org/wiki/Case_hardeninghttp://en.wikipedia.org/wiki/Precipitation_strengtheninghttp://en.wikipedia.org/wiki/Temperinghttp://en.wikipedia.org/wiki/Quenchhttp://en.wikipedia.org/wiki/Microstructurehttp://en.wikipedia.org/wiki/Crystalhttp://en.wikipedia.org/wiki/Crystallitehttp://en.wikipedia.org/wiki/Industrial_processhttp://en.wikipedia.org/wiki/Metalworkinghttp://en.wikipedia.org/wiki/Physical_propertyhttp://en.wikipedia.org/wiki/Chemical_propertyhttp://en.wikipedia.org/wiki/Metallurgyhttp://en.wikipedia.org/wiki/Glasshttp://en.wikipedia.org/wiki/Annealing_(metallurgy)http://en.wikipedia.org/wiki/Case_hardeninghttp://en.wikipedia.org/wiki/Precipitation_strengtheninghttp://en.wikipedia.org/wiki/Temperinghttp://en.wikipedia.org/wiki/Quenchhttp://en.wikipedia.org/wiki/Microstructurehttp://en.wikipedia.org/wiki/Crystalhttp://en.wikipedia.org/wiki/Crystallite
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    effective factors that can determine the overall mechanical behavior of the metal. Heat

    treatment provides an efficient way to manipulate the properties of the metal by controlling

    rate ofdiffusion, and the rate of cooling within the microstructure.

    There are two mechanisms that may change an alloy's properties during heat

    treatment. The martensite transformation causes the crystals to deform intrinsically. The

    diffusion mechanism causes changes in the homogeneity of the alloy.

    The crystal structure consists of atoms that are grouped in a very specific arrangement,

    called a lattice. In most elements, this order will rearrange itself, depending on conditions like

    temperature and pressure. This rearrangement, called allotropy or polymorphism, may occur

    several times, at many different temperatures for a particular metal. In alloys, thisrearrangement may cause an element that will not normally dissolve into the base metal to

    suddenly become soluble, while a reversal of the allotropy will make the elements either

    partially, or completely insolubles

    1.1.1. STAGES OF HEAT TREATMENT AND ITS PURPOSES

    The term heat treatment for aluminium alloys is frequently restricted to the specific

    operations employed to increase strength & hardness of the precipitation-hardenable wrought

    and cast alloys. Heat Treatment- the term heat treatment may be defined as an operation or a

    combination of operations, involving the heating and cooling of a metal or an alloy in the

    solid state for the purpose of obtaining certain desirable conditions or properties without

    change in chemical composition. These usually are referred to as the heat treatable alloys to

    distinguish them from those alloys in which no significant strengthening can be achieved by

    heating and cooling. Heat treating in its broadest sense refers to any of the heating and cooling

    operations are performed for the purpose of changing the mechanical properties, metallurgical

    structure, or the residual stress state of the metal product .

    Heat treatment applied to aluminium and its alloys are preheating or homogenizing to

    reduce chemical segregation of cast structures and to improve material workability. Annealing

    http://en.wikipedia.org/wiki/Diffusionhttp://en.wikipedia.org/wiki/Martensitehttp://en.wikipedia.org/wiki/Deformation_(engineering)http://en.wikipedia.org/wiki/Deformation_(engineering)http://en.wikipedia.org/wiki/Allotropyhttp://en.wikipedia.org/wiki/Solvationhttp://en.wikipedia.org/wiki/Solubilityhttp://en.wikipedia.org/wiki/Diffusionhttp://en.wikipedia.org/wiki/Martensitehttp://en.wikipedia.org/wiki/Deformation_(engineering)http://en.wikipedia.org/wiki/Allotropyhttp://en.wikipedia.org/wiki/Solvationhttp://en.wikipedia.org/wiki/Solubility
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    to soften strain hardened and heat treated alloy components to relieve stresses and to

    stabilize properties and dimensions. Precipitation (age-hardening) heat treatment to provide

    hardening by precipitation of constituents from solid solution. Solution heat treatment to

    improve mechanical properties by putting alloying elements into solution.

    Heat treatment is a collection through may processes such as Annealing, Stress relief,

    Quenching, Tempering, normalizing and ageing. All the different heat treatment process

    consists the following three stages-.

    1- Heating of the material.

    2- Hold the temperature for a time (soaking time).

    3- Cooling usually to room temperature (Normalizing).

    However the temperature and time for the various processes is dependent on the material

    mechanism controlling the wanted effect. The purpose of heat treatment is to achieve one or

    more of the following object-

    To increase the hardness of metals.

    To relieve the stresses set up in the material after hot or cold working.

    To improve Machinability.

    To soften the metal.

    To modify the structure of the material to improve its electrical and magnetic

    properties.

    To change the grain size.

    To increase the qualities of the metal to provide better resistance to heat, corrosion and

    wear.

    Improve ductility and toughness.

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    Pure aluminum is too soft for most structural applications and therefore is usually

    alloyed with several elements to improve its corrosion resistance, inhibit grain growth and of

    course to increase the strength. The optimum strengthening of aluminum is achieved by

    alloying and heat treatments that promote the formation of small, hard precipitates which

    interfere with the motion of dislocations. Aluminum alloys that can be heat treated to form

    these precipitates are considered heat treatable alloys. Pure aluminum is not heat treatable

    because no such particles can form while many heat treatable aluminum alloys are not

    wieldable because welding would destroy the microstructure produced by careful heat

    treatment.

    Virtually all heat treatable aluminum alloys are strengthened by precipitation

    hardening. Precipitation hardening involves raising the temperature of the alloy into the single

    phase region so that all of the precipitates dissolve. The alloy is then rapidly quenched to form

    a supersaturated solid solution and to trap excess vacancies and dislocation loops which can

    later act as nucleation sites for precipitation. The precipitates can form slowly at room

    temperature (natural aging) and more quickly at slightly elevated temperatures, typically

    100C to 200C (artificial aging). The degree of hardening obtained depends on the size,

    number and relative strength of the precipitates. These factors are determined by the

    composition of the alloy and by the tempering temperature and tempering time.

    Proper heat treating requires precise control over temperature, the amount of time that

    an alloy remains at a certain temperature, and in the cooling rates of the particular technique.

    With the exception of stress-relieving, tempering, and aging, most heat treatments

    begin by heating an alloy beyond the upper transformation (A3) temperature. The alloy will

    usually be held at this temperature long enough for the heat to completely penetrate the alloy,

    thereby bringing it into a complete solid solution. Since a smaller grain size usually enhances

    mechanical properties, such as toughness, shear strength and tensile strength, these metals are

    often heated to a temperature that is just above the upper critical temperature, in order to

    prevent the grains of solution from growing too large. For instance, when steel is heated

    above the upper critical temperature, small grains of austenite form. These grow larger as

    temperature is increased. When cooled very quickly, during a martensite transformation, the

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    austenite grain size directly affects the martensitic grain size. Larger grains have large grain-

    boundaries, which serve as weak spots in the structure. The grain size is usually controlled to

    reduce the probability of breakage.

    The diffusion transformation is very time dependent. Cooling a metal will usually

    suppress the precipitation to a much lower temperature. Austenite, for example, usually only

    exists above the upper critical temperature. However, if the austenite is cooled quickly

    enough, the transformation may be surpressed for hundreds of degrees below the lower

    critical temperature. Such austenite is highly unstable and, if given enough time, will

    precipitate into various microstructures of ferrite and cementite. The cooling rate can be used

    to control rate of grain growth or can even be used to produce partially martensitic

    microstructures. However, the martensite transformation is time-independent. If the alloy is

    cooled to the martensite transformation temperature before other microstructures can fully

    form, the transformation will usually occur at just under the speed of sound.

    1.2. THE OBJECTS OF HEAT TREATING ALUMINIUM ALLOYS

    Speaking very generally, there are two principal purposes in view when aluminium

    and its alloys are industrially heat treated. These are broadly:-

    (i) Strengthening or hardening and

    (ii) Annealing or softening

    There are other objects in subjecting aluminium and its alloys to heat treatments and

    these include the alteration of electrical or corrosion properties, the release of casting stresses

    and the admission of permanent growth in , for example, pistons; these latter objects are

    however of minor importance as compared with the two main objectives indicated above.

    1.3. CLASSIFICATION OF HEAT TREATMENT

    Various types of heat treatment processes may be classified as follows:-

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    1. Tempering

    a) Austempering

    b) Mar tempering

    c) Temperature based

    i) Low temperature tempering

    ii) Medium temperature tempering

    iii) High temperature tempering

    2. Annealing

    a) Process annealing b) Full annealing

    c) Spheroids annealing d) Diffusion annealing

    3. Normalizing

    4. Hardening

    a) Case hardening (or carburizing) b) Flame hardening

    c) Induction hardening d) Age hardening

    e) Cyaniding e) Nitriding

    1.4 TEMPERING

    Tempering is a heat treatment technique for metals, alloys and glass. In steels,

    tempering is done to "toughen" the metal by transforming brittle martensite orBainite into a

    combination of ferrite and cementite or sometimes tempered martensite. Precipitation

    hardening alloys, like many grades of aluminum and super alloys are tempered to precipitate

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    intermetallic particles which strengthen the metal. Tempering is accomplished by a controlled

    reheating of the work piece to a temperature below its lower critical temperature.

    The brittle martensite becomes tough and ductile after it is tempered. Carbon atomswere trapped in the austenite when it was rapidly cooled, typically by oil or water quenching,

    forming the martensite. The martensite becomes strong after being tempered because when

    reheated, the microstructure can rearrange and the carbon atoms can diffuse out of the

    distorted body-centered-tetragonal (BCT) structure. After the carbon diffuses, the result is

    nearly pure ferrite with body-centered structure.

    In metallurgy, there is always a trade-off between strengthand ductility. This delicate

    balance highlights many of the subtleties inherent to the tempering process. Precise control of

    time and temperature during the tempering process are critical to achieve a metal with well

    balanced mechanical properties.

    1.5. ANNEALING

    Annealing, in metallurgy and materials science, is a heat treatment wherein a material

    is altered, causing changes in its properties such as strength and hardness. It is a process that

    produces conditions by heating to above the recrystallization temperature, maintaining a

    suitable temperature, and then cooling. Annealing is used for inducing ductility, soften

    material, relieve internal stresses, refine the structure by making it homogeneous, and

    improve cold working properties.

    In the cases ofcopper,steel,silver, andbrass, this process is performed by

    substantially heating the material (generally until glowing) for a while and allowing it to cool.

    Unlikeferrous metalswhich must be cooled slowly to annealcopper, silver and brass can

    be cooled slowly in air or quickly by quenching in water. In this fashion the metal is softened

    and prepared for further work such as shaping, stamping, or forming.

    1.5.1. OBJECTIVES OF ANNEALING

    To soften the aluminium so that it may be easily machined or cold worked.

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    To refine the grain size & structure to improve mechanical properties like strength &

    ductility.

    To relieve internal stresses which may have been caused by hot & cold working or byunequal contraction in casting.

    To alter electrical magnetic or other physical properties.

    To remove gases trapped in the metal during initial casting.

    1.5.2. STAGES OF ANNEALING

    There are three stages in the annealing process, with the first being the recovery phase,

    which results in softening of the metal through removal of crystaldefects (the primary type of

    which is the linear defect called a dislocation) and the internal stresses which they cause.

    Recovery phase covers all annealing phenomena that occur before the appearance of new

    strain-free grains. The second phase is recrystallization, where new strain-free grains nucleate

    and grow to replace those deformed by internal stresses. If annealing is allowed to continue

    once recrystallization has been completed, grain growth will occur, in which the

    microstructure starts to coarsen and may cause the metal to have less than satisfactory

    mechanical properties.

    1.6. NORMALIZING

    Normalizing is a type of heat treatment applicable to ferrous metals only. It differs

    from annealing in that the metal is heated to a higher temperature and then removed from the

    furnace for air cooling. The purpose of normalizing is to remove the internal stresses induced

    by heat treating, welding, casting, forg-ing, forming, or machining. Stress, if not controlled,

    leads to metal failure; therefore, before hardening steel, you should normalize it first to ensure

    the maximum desired results. Usually, low-carbon steels do not require normalizing;

    however, if these steels are normalized, no harmful effects result. Castings are usually

    annealed, rather than normalized; however, some castings require the normalizing treatment.

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    Table 2-2 shows the approximate soaking periods for normalizing steel. Note that the soaking

    time varies with the thickness of the metal. Normalized steels are harder and stronger than

    annealed steels. In the normalized condition, steel is much tougher than in any other

    structural condition. Parts subjected to impact and those that require maximum toughness

    with resistance to external stress are usually normalized. In normalizing, the mass of metal

    has an influence on the cooling rate and on the resulting structure. Thin pieces cool faster and

    are harder after normalizing than thick ones. In annealing (furnace cooling), the hardness of

    the two are about the same.

    1.6.1. OBJECTIVES OF NORMALIZING

    To refine the grain structure of the aluminum to improve the machaniabilty tensile

    strength & structure of weld.

    To remove strains caused by cold working processes like hammering rolling, bending

    etc which makes the metal brittle & unreliable.

    To remove dislocations caused in the internal structure of the aluminum due to hot

    working.

    To improve certain mechanical & electrical properties.

    1.7. HARDENING

    The hardening treatment for most steels consists of heating the steel to a set

    temperature and then cooling it rapidly by plunging it into oil, water, or brine. Most steels

    require rapid cooling (quenching) for hardening but a few can be air-cooled with thesame results. Hardening increases the hardness and strength of the steel, but makes it less

    ductile. Generally, the harder the steel, the more brittle it becomes. To remove some of the

    brittleness, you should temper the steel after hardening. Many nonferrous metals can be

    hardened and their strength increased by controlled heating and rapid cooling. In this case, the

    process is called heat treatment, rather than hardening. To harden steel, you cool the metal

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    rapidly after thoroughly soaking it at a temperature slightly above its upper critical point. The

    approximate soaking periods for hardening steel are listed in table 2-2. The addition of alloys

    to steel decreases the cooling rate required to produce hardness. A decrease in the cooling rate

    is an advantage, since it lessens the danger of cracking and warping. Pure iron, wrought iron,

    and extremely low-carbon steels have very little hardening properties and are difficult to

    harden by heat treatment. Cast iron has limited capabilities for hardening. When you cool cast

    iron rapidly, it forms white iron, which is hard and brittle. And when you cool it slowly, it

    forms gray iron, which is soft but brittle under impact. In plain carbon steel, the maximum

    hardness obtained by heat treatment depends almost entirely on the carbon content of the

    steel.

    To perform hardening process, Al-alloy is heated to a temperature above its critical

    range. It is held at this temperature for a considerable time and then allowed to cool by

    quenching in water, oil, brine solution.

    1.7.1. OBJECTIVES OF HARDENING

    To increase the hardness of the metal so that it can resist wear.

    To enable it to cut other metals i.e. to make it suitable for cutting tools.

    Various factors responsible for hardness in aluminium alloy are the following:

    Quenching rate

    Work size

    1.8. HEAT TREATMENT: CAPABILITIES AND LIMITATIONS

    Heat treatments are an established, if obscure, method of disinfesting certain empty

    structures and equipment. Since the anticipated phase-out of methyl bromide fumigants,

    interest in this non-chemical pest management technique has been growing. Many of the

    advantages, disadvantages, considerations, observations, costs and results of using heat to

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    disinfest empty food processing and storage structures are situational in reality. Like

    fumigation with methyl bromide, successful heat treatments depend upon trained personnel,

    careful preparation, employee cooperation, good weather, etc.

    Some possible advantages of a heat treatment include the following-

    Perceived to be less dangerous than fumigation

    Fewer regulations than associated with fumigation

    Can monitor and adjust treatment easier than fumigation

    More effective than fumigation of a leaky structure

    More effective against pathogenic microorganisms

    Some possible disadvantages of a heat treatment include the following-

    Generally ineffective at penetrating commodities and debris

    Significantly more expensive than a methyl bromide fumigation

    Exposure period may be longer than for a methyl bromide fumigation

    Strong potential for damage to equipment and structure

    Less known about actual heat treatments than fumigations

    1.9. INTRODUCTION OFALUMINIUM

    Aluminium is a silvery white member of theboron group ofchemical elements. It has

    the symbol Al and its atomic number is 13. It is not soluble in water under normal

    circumstances. Aluminium is the most abundant metal in the Earth's crust, and the third most

    abundant element, afteroxygenandsilicon. It makes up about 8% by weight of the Earth's

    solid surface. Aluminium is too reactive chemically to occur in nature as a free metal.

    Instead, it is found combined in over 270 different minerals. The chief source of aluminium

    isbauxiteore.

    http://en.wikipedia.org/wiki/Boron_grouphttp://en.wikipedia.org/wiki/Chemical_elementhttp://en.wikipedia.org/wiki/Atomic_numberhttp://en.wikipedia.org/wiki/Element_abundancehttp://en.wikipedia.org/wiki/Earthhttp://en.wikipedia.org/wiki/Earthhttp://en.wikipedia.org/wiki/Crust_(geology)http://en.wikipedia.org/wiki/Oxygenhttp://en.wikipedia.org/wiki/Oxygenhttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Mineralhttp://en.wikipedia.org/wiki/Mineralhttp://en.wikipedia.org/wiki/Bauxitehttp://en.wikipedia.org/wiki/Orehttp://en.wikipedia.org/wiki/Boron_grouphttp://en.wikipedia.org/wiki/Chemical_elementhttp://en.wikipedia.org/wiki/Atomic_numberhttp://en.wikipedia.org/wiki/Element_abundancehttp://en.wikipedia.org/wiki/Earthhttp://en.wikipedia.org/wiki/Crust_(geology)http://en.wikipedia.org/wiki/Oxygenhttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Mineralhttp://en.wikipedia.org/wiki/Bauxitehttp://en.wikipedia.org/wiki/Ore
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    Aluminium is remarkable for the metal's low density and for its ability to resist

    corrosion due to the phenomenon of passivation. Structural components made from

    aluminium and its alloys are vital to the aerospace industry and are very important in other

    areas of transportation and building. Its reactive nature makes it useful as a catalyst or

    additive in chemical mixtures, including ammonium nitrate explosives, to enhance blast

    power.

    Despite its prevalence in the environment, aluminium salts are not known to be used

    by any form of life. Also in keeping with the element's abundance, it is well toleratedby

    plants in soils (in which it is a major component), and to a lesser extent, by animals as a

    component of plant materials in the diet (which often contain traces of dust and soil). Soluble

    aluminium salts have some demonstrated toxicity to animals if delivered in quantity by

    unnatural routes, such as injection. Controversy still exists about aluminums possible long-

    term toxicity to humans from larger ingested amounts.

    1.9.1. CHARACTERISTICS

    Aluminium is a soft, durable, lightweight, ductile and malleable metal with

    appearance ranging from silvery to dull gray, depending on the surface roughness.

    Aluminium is nonmagnetic and no sparking. It is also insoluble in alcohol, though it can be

    soluble in water in certain forms. The yield strength of pure aluminium is 711 MPa, while

    aluminium alloys have yield strengths ranging from 200 MPa to 600 MPa. Aluminium has

    about one-third the density and stiffness of steel. It is easily machined, cast, drawn and

    extruded. Corrosion resistance can be excellent due to a thin surface layer of aluminium

    oxide that forms when the metal is exposed to air, effectively preventing further oxidation.

    The strongest aluminium alloys are less corrosion resistant due to galvanic reactions with

    alloyed copper. This corrosion resistance is also often greatly reduced when many aqueous

    salts are present, particularly in the presence of dissimilar metals.

    Aluminium atoms are arranged in a face-centered cubic (fcc) structure. Aluminium is

    one of the few metals that retain full silvery reflectance in finely powdered form, making it an

    important component of silver paints. Aluminium mirror finish has the highest reflectance of

    http://en.wikipedia.org/wiki/Densityhttp://en.wikipedia.org/wiki/Corrosionhttp://en.wikipedia.org/wiki/Passivationhttp://en.wikipedia.org/wiki/Passivationhttp://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Aerospacehttp://en.wikipedia.org/wiki/Transporthttp://en.wikipedia.org/wiki/Catalysthttp://en.wikipedia.org/wiki/Ammonium_nitratehttp://en.wikipedia.org/wiki/Explosiveshttp://en.wikipedia.org/wiki/Toxicityhttp://en.wikipedia.org/wiki/Ductilityhttp://en.wikipedia.org/wiki/Malleablehttp://en.wikipedia.org/wiki/Malleablehttp://en.wikipedia.org/wiki/Malleablehttp://en.wikipedia.org/wiki/Metalhttp://en.wikipedia.org/wiki/Yield_(engineering)http://en.wikipedia.org/wiki/Pascal_(unit)http://en.wikipedia.org/wiki/Pascal_(unit)http://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Densityhttp://en.wikipedia.org/wiki/Elastic_modulushttp://en.wikipedia.org/wiki/Steelhttp://en.wikipedia.org/wiki/Machininghttp://en.wikipedia.org/wiki/Casting_(metalworking)http://en.wikipedia.org/wiki/Drawing_(metalworking)http://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Oxidationhttp://en.wikipedia.org/wiki/Galvanic_cellhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Cubic_crystal_systemhttp://en.wikipedia.org/wiki/Reflectancehttp://en.wikipedia.org/wiki/Densityhttp://en.wikipedia.org/wiki/Corrosionhttp://en.wikipedia.org/wiki/Passivationhttp://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Aerospacehttp://en.wikipedia.org/wiki/Transporthttp://en.wikipedia.org/wiki/Catalysthttp://en.wikipedia.org/wiki/Ammonium_nitratehttp://en.wikipedia.org/wiki/Explosiveshttp://en.wikipedia.org/wiki/Toxicityhttp://en.wikipedia.org/wiki/Ductilityhttp://en.wikipedia.org/wiki/Malleablehttp://en.wikipedia.org/wiki/Metalhttp://en.wikipedia.org/wiki/Yield_(engineering)http://en.wikipedia.org/wiki/Pascal_(unit)http://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Densityhttp://en.wikipedia.org/wiki/Elastic_modulushttp://en.wikipedia.org/wiki/Steelhttp://en.wikipedia.org/wiki/Machininghttp://en.wikipedia.org/wiki/Casting_(metalworking)http://en.wikipedia.org/wiki/Drawing_(metalworking)http://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Oxidationhttp://en.wikipedia.org/wiki/Galvanic_cellhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Cubic_crystal_systemhttp://en.wikipedia.org/wiki/Reflectance
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    any metal in the 200400 nm (UV) and the 3,00010,000 nm (farIR) regions; in the 400

    700 nm visible range it is slightly outperformed by tin and silverand in the 7003000 (near

    IR) by silver,gold, and copper.

    Aluminium is a good thermal and electrical conductor, having 62% the conductivity of

    copper. Aluminium is capable of being a superconductor, with a superconducting critical

    temperature of 1.2 Kelvins and a critical magnetic field of about 100 gauss (10 milliteslas).

    1.9.2.APPLICATIONS

    Aluminium is the most widely used non-ferrous metal. Global production of

    aluminium in 2005 was 31.9 million tonnes. It exceeded that of any other metal except iron(837.5 million tonnes). Forecast for 2012 is 4245 million tons, driven by rising Chinese

    output. Relatively pure aluminium is encountered only when corrosion resistance and/or

    workability is more important than strength or hardness. A thin layer of aluminium can be

    deposited onto a flat surface by physical vapour depositionor (very infrequently) chemical

    vapour deposition or other chemical means to form optical coatings and mirrors. When so

    deposited, a fresh, pure aluminium film serves as a good reflector (approximately 92%) of

    visible light and an excellent reflector (as much as 98%) of medium and far infrared radiation.

    Pure aluminium has a low tensile strength, but when combined with thermo-mechanical

    processing, aluminium alloys display a marked improvement in mechanical properties,

    especially when tempered. Aluminium alloys form vital components ofaircraft androcketsas

    a result of their high strength-to-weight ratio. Aluminium readily forms alloys with many

    elements such as copper, zinc,magnesium, manganeseand silicon (e.g., duralumin). Today,

    almost all bulk metal materials that are referred to loosely as "aluminium", are actually alloys.

    For example, the common aluminium foils and beverage cans are alloys of 92% to 99%aluminium.

    Some of the many uses for aluminium metal are in:

    Transportation (automobiles, aircraft, trucks, railway cars, marine vessels, bicycles

    etc.) as sheet, tube, castings etc.

    http://en.wikipedia.org/wiki/Ultraviolethttp://en.wikipedia.org/wiki/Infraredhttp://en.wikipedia.org/wiki/Infraredhttp://en.wikipedia.org/wiki/Tinhttp://en.wikipedia.org/wiki/Silverhttp://en.wikipedia.org/wiki/Goldhttp://en.wikipedia.org/wiki/Goldhttp://en.wikipedia.org/wiki/Heat_conductionhttp://en.wikipedia.org/wiki/Electrical_conductorhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Superconductorhttp://en.wikipedia.org/wiki/Kelvinhttp://en.wikipedia.org/wiki/Gauss_(unit)http://en.wikipedia.org/wiki/Milliteslahttp://en.wikipedia.org/wiki/Ironhttp://en.wikipedia.org/wiki/Physical_vapour_depositionhttp://en.wikipedia.org/wiki/Physical_vapour_depositionhttp://en.wikipedia.org/wiki/Chemical_vapour_depositionhttp://en.wikipedia.org/wiki/Chemical_vapour_depositionhttp://en.wikipedia.org/wiki/Optical_coatinghttp://en.wikipedia.org/wiki/Mirrorhttp://en.wikipedia.org/wiki/Visible_lighthttp://en.wikipedia.org/wiki/Tensile_strengthhttp://en.wikipedia.org/wiki/Temperinghttp://en.wikipedia.org/wiki/Aircrafthttp://en.wikipedia.org/wiki/Rockethttp://en.wikipedia.org/wiki/Rockethttp://en.wikipedia.org/wiki/Rockethttp://en.wikipedia.org/wiki/Zinchttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Manganesehttp://en.wikipedia.org/wiki/Manganesehttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Duraluminhttp://en.wikipedia.org/wiki/Aluminium_foilhttp://en.wikipedia.org/wiki/Automobilehttp://en.wikipedia.org/wiki/Truckhttp://en.wikipedia.org/wiki/Railway_carhttp://en.wikipedia.org/wiki/Bicyclehttp://en.wikipedia.org/wiki/Ultraviolethttp://en.wikipedia.org/wiki/Infraredhttp://en.wikipedia.org/wiki/Tinhttp://en.wikipedia.org/wiki/Silverhttp://en.wikipedia.org/wiki/Goldhttp://en.wikipedia.org/wiki/Heat_conductionhttp://en.wikipedia.org/wiki/Electrical_conductorhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Superconductorhttp://en.wikipedia.org/wiki/Kelvinhttp://en.wikipedia.org/wiki/Gauss_(unit)http://en.wikipedia.org/wiki/Milliteslahttp://en.wikipedia.org/wiki/Ironhttp://en.wikipedia.org/wiki/Physical_vapour_depositionhttp://en.wikipedia.org/wiki/Chemical_vapour_depositionhttp://en.wikipedia.org/wiki/Chemical_vapour_depositionhttp://en.wikipedia.org/wiki/Optical_coatinghttp://en.wikipedia.org/wiki/Mirrorhttp://en.wikipedia.org/wiki/Visible_lighthttp://en.wikipedia.org/wiki/Tensile_strengthhttp://en.wikipedia.org/wiki/Temperinghttp://en.wikipedia.org/wiki/Aircrafthttp://en.wikipedia.org/wiki/Rockethttp://en.wikipedia.org/wiki/Zinchttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Manganesehttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Duraluminhttp://en.wikipedia.org/wiki/Aluminium_foilhttp://en.wikipedia.org/wiki/Automobilehttp://en.wikipedia.org/wiki/Truckhttp://en.wikipedia.org/wiki/Railway_carhttp://en.wikipedia.org/wiki/Bicycle
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    Packaging (cans, foil, etc.)

    Construction (windows, doors, siding, building wire, etc.)

    A wide range of household items, from cooking utensils tobaseball bats, watches.

    Street lighting poles, sailing ship masts, walking poles etc. Outer shells of consumer

    electronics, also cases for equipment e.g. photographic equipment.

    Electrical transmission lines for power distribution

    MKM steel and Alnico magnets

    Super purity aluminium (SPA, 99.980% to 99.999% Al), used in electronics and CDs.

    Heat sinks for electronic appliances such as transistors and CPUs.

    Substrate material ofmetal-core copper clad laminates used in high brightness LED

    lighting.

    Powdered aluminium is used in paint, and inpyrotechnics such as solid rocket fuels

    and thermite.

    Aluminium can be reacted with hydrochloric acid to form hydrogen gas.

    A variety of countries, including France, Italy, Poland,Finland, Romania, Israel, and

    the formerYugoslavia, have issued coins struck in aluminium or aluminium-copper

    alloys.[39]

    Some guitar models sports aluminium diamond plates on the surface of the

    instruments, usually either chrome or black. Kramer Guitars and Travis Bean are both

    known for having produced guitars with necks made of aluminium, which gives the

    instrument a very distinct sound.

    http://en.wikipedia.org/wiki/Aluminium_canhttp://en.wikipedia.org/wiki/Windowhttp://en.wikipedia.org/wiki/Doorhttp://en.wikipedia.org/wiki/Sidinghttp://en.wikipedia.org/wiki/Cooking_utensilhttp://en.wikipedia.org/wiki/Baseball_bathttp://en.wikipedia.org/wiki/Mast_(sailing)http://en.wikipedia.org/wiki/Walking_polehttp://en.wikipedia.org/wiki/Walking_polehttp://en.wikipedia.org/wiki/Electrical_transmission_linehttp://en.wikipedia.org/wiki/MKM_steelhttp://en.wikipedia.org/wiki/Alnicohttp://en.wikipedia.org/wiki/Compact_dischttp://en.wikipedia.org/wiki/Heat_sinkhttp://en.wikipedia.org/wiki/Transistorhttp://en.wikipedia.org/wiki/Central_processing_unithttp://en.wikipedia.org/w/index.php?title=Metal-core_copper_clad_laminates&action=edit&redlink=1http://en.wikipedia.org/wiki/LED_lightinghttp://en.wikipedia.org/wiki/LED_lightinghttp://en.wikipedia.org/wiki/Painthttp://en.wikipedia.org/wiki/Pyrotechnicshttp://en.wikipedia.org/wiki/Solid_rockethttp://en.wikipedia.org/wiki/Thermitehttp://en.wikipedia.org/wiki/Francehttp://en.wikipedia.org/wiki/Italyhttp://en.wikipedia.org/wiki/Polandhttp://en.wikipedia.org/wiki/Finlandhttp://en.wikipedia.org/wiki/Finlandhttp://en.wikipedia.org/wiki/Romaniahttp://en.wikipedia.org/wiki/Israelhttp://en.wikipedia.org/wiki/Yugoslaviahttp://en.wikipedia.org/wiki/Coinhttp://en.wikipedia.org/wiki/Aluminium#cite_note-38http://en.wikipedia.org/wiki/Kramer_Guitarshttp://en.wikipedia.org/wiki/Travis_Beanhttp://en.wikipedia.org/wiki/Aluminium_canhttp://en.wikipedia.org/wiki/Windowhttp://en.wikipedia.org/wiki/Doorhttp://en.wikipedia.org/wiki/Sidinghttp://en.wikipedia.org/wiki/Cooking_utensilhttp://en.wikipedia.org/wiki/Baseball_bathttp://en.wikipedia.org/wiki/Mast_(sailing)http://en.wikipedia.org/wiki/Walking_polehttp://en.wikipedia.org/wiki/Electrical_transmission_linehttp://en.wikipedia.org/wiki/MKM_steelhttp://en.wikipedia.org/wiki/Alnicohttp://en.wikipedia.org/wiki/Compact_dischttp://en.wikipedia.org/wiki/Heat_sinkhttp://en.wikipedia.org/wiki/Transistorhttp://en.wikipedia.org/wiki/Central_processing_unithttp://en.wikipedia.org/w/index.php?title=Metal-core_copper_clad_laminates&action=edit&redlink=1http://en.wikipedia.org/wiki/LED_lightinghttp://en.wikipedia.org/wiki/LED_lightinghttp://en.wikipedia.org/wiki/Painthttp://en.wikipedia.org/wiki/Pyrotechnicshttp://en.wikipedia.org/wiki/Solid_rockethttp://en.wikipedia.org/wiki/Thermitehttp://en.wikipedia.org/wiki/Francehttp://en.wikipedia.org/wiki/Italyhttp://en.wikipedia.org/wiki/Polandhttp://en.wikipedia.org/wiki/Finlandhttp://en.wikipedia.org/wiki/Romaniahttp://en.wikipedia.org/wiki/Israelhttp://en.wikipedia.org/wiki/Yugoslaviahttp://en.wikipedia.org/wiki/Coinhttp://en.wikipedia.org/wiki/Aluminium#cite_note-38http://en.wikipedia.org/wiki/Kramer_Guitarshttp://en.wikipedia.org/wiki/Travis_Bean
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    1.9.3. ALUMINIUM ALLOYS

    Aluminium alloys are alloys in which aluminium (Al) is the predominant metal. The

    typical alloying elements are copper, magnesium, manganese, silicon, and zinc. There are twoprincipal classifications, namely casting alloys and wrought alloys, both of which are further

    subdivided into the categories heat-treatable and non-heat-treatable. About 85% of aluminium

    is used for wrought products, for example rolled plate, foils and extrusions. Cast aluminium

    alloys yield cost effective products due to the low melting point, although they generally have

    lowertensile strengths than wrought alloys. The most important cast aluminium alloy system

    is Al-Si, where the high levels of silicon (4.0% to 13%) contribute to give good casting

    characteristics. Aluminium alloys are widely used in engineering structures and components

    where light weight or corrosion resistance is required.

    Alloys composed mostly of the two lightweight metals aluminium and magnesium

    have been very important in aerospace manufacturing since somewhat before 1940.

    Aluminium-magnesium alloys are both lighter than other aluminium alloys and much less

    flammable than alloys that contain a very high percentage of magnesium.

    Aluminium alloy surfaces will keep their apparent shine in a dry environment due to

    the formation of a clear, protective layer ofaluminium oxide. In a wet environment, galvanic

    corrosion can occur when an aluminium alloy is placed in electrical contact with other metals

    with more negative corrosion potentials than aluminium.

    Aluminium alloy compositions are registered with The Aluminum Association. Many

    organizations publish more specific standards for the manufacture of aluminium alloy,

    including the Society of Automotive Engineers standards organization, specifically its

    aerospace standards subgroups, and ASTM International.

    http://en.wikipedia.org/wiki/Alloyshttp://en.wikipedia.org/wiki/Aluminiumhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Manganesehttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Zinchttp://en.wikipedia.org/wiki/Castinghttp://en.wikipedia.org/wiki/Heat_treatmenthttp://en.wikipedia.org/wiki/Extrudinghttp://en.wikipedia.org/wiki/Tensile_strengthhttp://en.wikipedia.org/wiki/Aerospace_manufacturinghttp://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Galvanic_corrosionhttp://en.wikipedia.org/wiki/Galvanic_corrosionhttp://en.wikipedia.org/wiki/The_Aluminum_Associationhttp://en.wikipedia.org/wiki/Society_of_Automotive_Engineershttp://en.wikipedia.org/wiki/ASTM_Internationalhttp://en.wikipedia.org/wiki/Alloyshttp://en.wikipedia.org/wiki/Aluminiumhttp://en.wikipedia.org/wiki/Copperhttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Manganesehttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/Zinchttp://en.wikipedia.org/wiki/Castinghttp://en.wikipedia.org/wiki/Heat_treatmenthttp://en.wikipedia.org/wiki/Extrudinghttp://en.wikipedia.org/wiki/Tensile_strengthhttp://en.wikipedia.org/wiki/Aerospace_manufacturinghttp://en.wikipedia.org/wiki/Aluminium_oxidehttp://en.wikipedia.org/wiki/Galvanic_corrosionhttp://en.wikipedia.org/wiki/Galvanic_corrosionhttp://en.wikipedia.org/wiki/The_Aluminum_Associationhttp://en.wikipedia.org/wiki/Society_of_Automotive_Engineershttp://en.wikipedia.org/wiki/ASTM_International
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    1.9.3.1. ALUMINIUM ALLOYS IN STRUCTURAL APPLICATIONS

    Aluminium alloys with a wide range of properties are used in engineering structures.

    Alloy systems are classified by a number system (ANSI) or by names indicating their mainalloying constituents (DIN and ISO).

    The strength and durability of aluminium alloys vary widely, not only as a result of the

    components of the specific alloy, but also as a result of heat treatments and manufacturing

    processes. A lack of the knowledge of these aspects has from time to time led to improperly

    designed structures and gained aluminium a bad reputation. One important structural

    limitation of aluminium alloys is their fatigue strength. Unlike steels, aluminium alloys have

    no well-defined fatigue limit, meaning that fatigue failure eventually occurs, under even very

    small cyclic loadings. This implies that engineers must assess these loads and design for a

    fixed life rather than an infinite life.

    Another important property of aluminium alloys is their sensitivity to heat. Workshop

    procedures involving heating are complicated by the fact that aluminium, unlike steel, melts

    without first glowing red. Forming operations where a blow torch is used therefore require

    some expertise, since no visual signs reveal how close the material is to melting. Aluminium

    alloys, like all structural alloys, also are subject to internal stresses following heating

    operations such as welding and casting. The problem with aluminium alloys in this regard is

    their low melting point, which make them more susceptible to distortions from thermally

    induced stress relief. Controlled stress relief can be done during manufacturing by heat-

    treating the parts in an oven, followed by gradual coolingin effect annealing the stresses.

    The low melting point of aluminium alloys has not precluded their use in rocketry;

    even for use in constructing combustion chambers where gases can reach 3500 K. The Agenaupper stage engine used a regeneratively cooled aluminium design for some parts of the

    nozzle, including the thermally critical throat region.

    http://en.wikipedia.org/wiki/American_National_Standards_Institutehttp://en.wikipedia.org/wiki/DINhttp://en.wikipedia.org/wiki/International_Organization_of_Standardizationhttp://en.wikipedia.org/wiki/Fatigue_(material)http://en.wikipedia.org/wiki/Fatigue_limithttp://en.wikipedia.org/wiki/Fatigue_(material)#Design_against_fatiguehttp://en.wikipedia.org/wiki/Blow_torchhttp://en.wikipedia.org/wiki/Melting_pointhttp://en.wikipedia.org/wiki/Annealing_(metallurgy)http://en.wikipedia.org/wiki/RM-81_Agenahttp://en.wikipedia.org/wiki/American_National_Standards_Institutehttp://en.wikipedia.org/wiki/DINhttp://en.wikipedia.org/wiki/International_Organization_of_Standardizationhttp://en.wikipedia.org/wiki/Fatigue_(material)http://en.wikipedia.org/wiki/Fatigue_limithttp://en.wikipedia.org/wiki/Fatigue_(material)#Design_against_fatiguehttp://en.wikipedia.org/wiki/Blow_torchhttp://en.wikipedia.org/wiki/Melting_pointhttp://en.wikipedia.org/wiki/Annealing_(metallurgy)http://en.wikipedia.org/wiki/RM-81_Agena
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    1.9.3.2. ALUMINIUM 6063 ALLOY

    Al 6063 is an aluminium alloy, with magnesium and silicon as the alloying elements.

    The standard controlling its composition is maintained by The Aluminum Association. It hasgenerally good mechanical properties and is heat treatable and weld able. It is similar to the

    British aluminium alloy HE9.

    6063 Aluminium alloy is mostly used in extrudedshapes for architecture, particularly

    window frames, door frames, and roofs. It is typically produced with very smooth surfaces fit

    foranodizing.

    1.9.3.3. CHEMICAL COMPOSITION OF ALUMINIUM 6063 ALLOY

    Table1.1-Chemical Composition Of Aluminium 6063 AlloyCu Si Fe Mn Mg Zn Cr Ti Al

    0.10 0.20 /

    0.60

    0.35 0.10 0.45 /

    0.90

    0.10 0.10 0.10 Balance

    1.9.3.4. PHYSICAL PROPERTIES OF ALUMINIUM 6063 ALLOY

    Table1.2-Physical Properties Of Aluminum 6063 Alloy

    Property Value

    Density 2.70g/cm3

    Melting point 750o

    CModulus of elasticity 69.5GPa

    Electrical resistivity 0.35 x 10-6 ohm

    Thermal conductivity 200 W/mK

    Thermal expansion 23.5 x 10-6 /K

    1.9.3.5. MECHANICAL PROPERTIES

    http://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/The_Aluminum_Associationhttp://en.wikipedia.org/wiki/Extrusionhttp://en.wikipedia.org/wiki/Extrusionhttp://en.wikipedia.org/wiki/Anodizinghttp://en.wikipedia.org/wiki/Aluminium_alloyhttp://en.wikipedia.org/wiki/Magnesiumhttp://en.wikipedia.org/wiki/Siliconhttp://en.wikipedia.org/wiki/The_Aluminum_Associationhttp://en.wikipedia.org/wiki/Extrusionhttp://en.wikipedia.org/wiki/Anodizing
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    Table1.3- Mechanical Properties

    Temper O T4 T6Minimum proof stress 0.2% (MPa) 50 60 160

    Minimum tensile strength (MPa) 100 130 195Shear strength(MPa) 70 110 150

    Elongation (%) 22 21 14

    Hardness Vickers 25 50 80

    1.10. IMPORTANT MECHANICAL PROPERTIES

    a) TENSILE STRENGTH:-

    It is the ability of the material to resist the externally applied forces without breaking or

    yielding. Tensile strength measures the force required to pull something such as rope, wire, or

    a structural beam to the point where it breaks. The tensile strength of a material is the

    maximum amount oftensile stress that it can take before failure, for example breaking.

    b) HARDNESS:-

    Hardness is the measure of how resistant solidmatteris to various kinds of permanent

    shape change when a force is applied. Macroscopic hardness is generally characterized bystrong intermolecular bonds, however the behavior of solid materials under force is complex,

    therefore there are different measurements of hardness: scratch hardness, indentation

    hardness, and rebound hardness. Hardness is dependent on ductility, elasticity, plasticity,

    strain,strength, toughness, visco-elasticity, and viscosity. Common examples of hard matter

    are ceramics, concrete, certainmetals, and super hard materials, which can be contrasted with

    soft matter

    c) BRITTLENESS:-

    A material is brittle if, when subjected to stress, it breaks without significant

    deformation (strain). Brittle materials absorb relatively little energy prior to fracture, even

    those of highstrength. Breaking is often accompanied by a snapping sound. Brittle materials

    include mostceramicsand glasses (which do not deform plastically) and somepolymers, such

    http://simple.wikipedia.org/wiki/Forcehttp://simple.wikipedia.org/wiki/Ropehttp://simple.wikipedia.org/wiki/Wirehttp://simple.wikipedia.org/wiki/Materialhttp://simple.wikipedia.org/wiki/Materialhttp://simple.wikipedia.org/wiki/Tensile_stresshttp://simple.wikipedia.org/wiki/Tensile_stresshttp://en.wikipedia.org/wiki/Solidhttp://en.wikipedia.org/wiki/Solidhttp://en.wikipedia.org/wiki/Matterhttp://en.wikipedia.org/wiki/Matterhttp://en.wikipedia.org/wiki/Forcehttp://en.wikipedia.org/wiki/Forcehttp://en.wikipedia.org/wiki/Intermolecular_bondhttp://en.wikipedia.org/wiki/Ductilityhttp://en.wikipedia.org/wiki/Elasticity_(physics)http://en.wikipedia.org/wiki/Plasticity_(physics)http://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Toughnesshttp://en.wikipedia.org/wiki/Toughnesshttp://en.wikipedia.org/wiki/Viscoelasticityhttp://en.wikipedia.org/wiki/Ceramichttp://en.wikipedia.org/wiki/Concretehttp://en.wikipedia.org/wiki/Metalshttp://en.wikipedia.org/wiki/Metalshttp://en.wikipedia.org/wiki/Superhard_materialshttp://en.wikipedia.org/wiki/Soft_matterhttp://en.wikipedia.org/wiki/Materialhttp://en.wikipedia.org/wiki/Stress_(physics)http://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Energyhttp://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Ceramicshttp://en.wikipedia.org/wiki/Ceramicshttp://en.wikipedia.org/wiki/Ceramicshttp://en.wikipedia.org/wiki/Glasshttp://en.wikipedia.org/wiki/Polymerhttp://en.wikipedia.org/wiki/Polymerhttp://simple.wikipedia.org/wiki/Forcehttp://simple.wikipedia.org/wiki/Ropehttp://simple.wikipedia.org/wiki/Wirehttp://simple.wikipedia.org/wiki/Materialhttp://simple.wikipedia.org/wiki/Tensile_stresshttp://en.wikipedia.org/wiki/Solidhttp://en.wikipedia.org/wiki/Matterhttp://en.wikipedia.org/wiki/Forcehttp://en.wikipedia.org/wiki/Intermolecular_bondhttp://en.wikipedia.org/wiki/Ductilityhttp://en.wikipedia.org/wiki/Elasticity_(physics)http://en.wikipedia.org/wiki/Plasticity_(physics)http://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Toughnesshttp://en.wikipedia.org/wiki/Viscoelasticityhttp://en.wikipedia.org/wiki/Ceramichttp://en.wikipedia.org/wiki/Concretehttp://en.wikipedia.org/wiki/Metalshttp://en.wikipedia.org/wiki/Superhard_materialshttp://en.wikipedia.org/wiki/Soft_matterhttp://en.wikipedia.org/wiki/Materialhttp://en.wikipedia.org/wiki/Stress_(physics)http://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Energyhttp://en.wikipedia.org/wiki/Strength_of_materialshttp://en.wikipedia.org/wiki/Ceramicshttp://en.wikipedia.org/wiki/Glasshttp://en.wikipedia.org/wiki/Polymer
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    2.1. LITERATURE REVIEW

    Heat treatment processes for aluminium are precision processes. Based on the

    objectives of this research, precipitate free zones in the aluminium alloy 6063 actually give

    bad effect to the mechanical properties of that alloy. The mechanical properties of the

    aluminium alloy should be altering properly to improve their behavior using precipitation

    hardening which one of the heat treatment types. Precipitation hardening is the most suitable

    heat treatment that should use to minimize the precipitate free zones in the microstructure of

    the aluminium alloy 6063. In the precipitation hardening process, the thermal and temperature

    condition is under control with high precision to ensure the transformation of the aluminium

    alloy structure is in good condition and supervision limit. The samples of the material areplaced in the furnace to make a heat treating process and then quench it in the water for

    quenching medium. The material testing that had been applied is based on hardness, impact

    and microstructure analysis. The purpose of the hardness testing are to find out the hardness

    reading for all the samples that used to look the wear resistance effect that occur after make a

    heat treating process to the aluminium alloy 6063. From the impact test, the purposes are to

    know impact energy that absorbed to fracture the samples of the material and then make a

    comparison data between after and before heat treatment. Lastly, for microstructure analysis it

    is important to determine because to look the narrow evaluation of precipitate free zones in

    the microstructure of aluminium alloy after make a precipitation hardening processes. From

    the data and result that already determined, it shown the positive result based on objectives

    and scope of this project.

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    The literature review of existing heat treatments indicates that heat straightening with

    maximum temperature limited to 1200F is relatively similar to the process annealing heat

    treatment. Heat straightening with maximum temperature limited to 1400oF is similar to the

    normalizing annealing heat treatment. Both these heat treatments repair plastically deformed

    microstructure by the phenomenon known as recovery and recrystallization. Normalizing

    annealing is more efficient and faster than process annealing in repairing the plastically

    deformed microstructure by recrystallization. Heat treatment and repair of the material

    microstructure is incidental to the heat straightening repair process. The heat straightened

    beam can be further heat treated to complete the repair of the material microstructure

    (recrystallization etc.). The practical and economic feasibility of additional heat treatment

    using electrically powered and controlled radiant heaters was evaluated and found to bereasonable.

    The effects of heat treatment on the dynamic compressive properties and energy

    absorption characteristics of open cell aluminium 6063 alloy produced by

    infiltrating process were studied. various kinds of heat treatment were exploited such as

    quenching normalising and annealing. Tensile compressive and hardness test has been

    performed to define the properties of aluminium 6063 alloy. The results show that tha

    hardness of the alloy increases also it softens on quenching the grain structure also define bythe tests .

    The effects of solution-ageing treatment on the mechanical properties of aluminium

    6063 products were studied by the method of orthogonal experiment. The mechanical

    properties at different treatment conditions were analyzed. The results show that the effects of

    heat treatment were obviously influenced by the original microstructure of the aluminium

    60603. Higher temperature is favorable for the sufficient solution of alloy elements, but the

    grains will grow up when treated at a higher temperature or soaked for a longer time. There is

    a contradiction between the maximum tensile strength and elongation percentage. The surplus

    phases not melted in the substrate and the solution precipitated supersaturated elements are

    the main factors influencing the properties of the alloys.

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    To examine the effectiveness of the treatment, simulating experiments are conducted

    using a heat-treatable 6063 aluminum alloy, and the grain size, hardness property, and tensile

    properties are measured and compared with those of the conventionally heat-treated sheets.

    The results are summarized as follows: (1) resistance heating at a current density of about

    100 A mm2 realizes heating the aluminum alloy sheet into the solution temperature range in

    2 s, (2) complete achievement of rapid solution treatment by the resistance heating requires

    the condition that the precipitates exist finely in the matrix, (3) the new treatment decreases

    the grain size by approximately one-half but the mechanical properties are not remarkably

    improved.

    A systematic experimental investigation of the effect of heat-treatment technique on

    the mechanical properties of 6063 aluminum alloy was carried out. Particularly, an artificial

    neural network and a genetic algorithm were used to search for the optimum technique,

    adapted for 6063 aluminum alloy. The results indicated strongly that an artificial neural

    network combined with a genetic algorithm indeed offer a new effective means for the

    optimization of materials processing technique.

    A series of heat treatments were made on samples cut from bars of a 6063

    heat treatable aluminum alloy that were solubilized for 4 h at 520 C, and were cooled down

    to room temperature by placing one of their ends into a shallow tank of water to produce a

    continuous thermal gradient along their length. Heating and cooling are carried

    simultaneously for carrying out different tests. Various test are being conducted on different

    equipments such as UTM machine is being used for testing compressive and tensile tests of

    aluminium 6063 alloy . for hardness test Rockwell hardness test is being conducted IZOD

    and Charpy tests are being conducted to find the impact strength of aluminium 6063 alloy.

    These tests are performed on different temperatures for carrying out Quenching, Normalising

    and Annealing processes and results are being calculated.

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    CHAPTER - 3

    METHODOLOGY AND TESTS

    PERFORMED

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    c) HARDENING: - Hardening is performed at 525oC for 3 hrs and then immediately

    quenched in water.

    This is applicable to the heat treatable alloys and involves a heat treatment process

    whereby the alloying constituents are taken into solution and retained by rapid quenching.

    Subsequent heat treatment at tower temperatures i.e. ageing or natural ageing at room

    temperature allows for a controlled precipitation of the constituents thereby achieving

    increased hardness and strength. Time at temperature for solution treatment depends on

    the type of alloy and the furnace load. Sufficient time must be allowed to take the alloys

    into solution if optimum properties are to be obtained.

    5) Now we will again measure all the mechanical properties which we had checked

    earlier.

    6) Now compare the properties of aluminium 6063 alloy before & after heat treatment

    3.2. TESTS PERFORMED ON ALUMINUM 6063 ALLOY

    3.2.1. TENSILE TEST

    Tensile testing, also known as tension testing, is a fundamental materials science test

    in which a sample is subjected to uniaxial tension until failure. The results from the test are

    commonly used to select a material for an application, forquality control, and to predict how

    a material will react under other types of forces. Properties that are directly measured via a

    tensile test are ultimate tensile strength, maximum elongation and reduction in area. From

    these measurements the following properties can also be determined: Young's modulus,

    Poisson's ratio, yield strength, and strain-hardening characteristics.

    3.2.1.1. Tensile Test Specimen

    http://en.wikipedia.org/wiki/Materials_sciencehttp://en.wikipedia.org/wiki/Tensionhttp://en.wikipedia.org/wiki/Quality_controlhttp://en.wikipedia.org/wiki/Forcehttp://en.wikipedia.org/wiki/Ultimate_tensile_strengthhttp://en.wikipedia.org/wiki/Elongation_(materials_science)http://en.wikipedia.org/wiki/Young's_modulushttp://en.wikipedia.org/wiki/Poisson's_ratiohttp://en.wikipedia.org/wiki/Yield_strengthhttp://en.wikipedia.org/wiki/Strain-hardeninghttp://en.wikipedia.org/wiki/Materials_sciencehttp://en.wikipedia.org/wiki/Tensionhttp://en.wikipedia.org/wiki/Quality_controlhttp://en.wikipedia.org/wiki/Forcehttp://en.wikipedia.org/wiki/Ultimate_tensile_strengthhttp://en.wikipedia.org/wiki/Elongation_(materials_science)http://en.wikipedia.org/wiki/Young's_modulushttp://en.wikipedia.org/wiki/Poisson's_ratiohttp://en.wikipedia.org/wiki/Yield_strengthhttp://en.wikipedia.org/wiki/Strain-hardening
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    A tensile test specimen is a standardized sample cross-section. It has two shoulders

    and a gage section in between. The shoulders are large so they can be readily gripped, where

    as the gage section has a smaller cross-section so that the deformation and failure can occur in

    this area.

    The shoulders of the test specimen can be manufactured in various ways to mate to various

    grips in the testing machine (see the image below). Each system has advantages and

    disadvantages; for example, shoulders designed for serrated grips are easy and cheap to

    manufacture, but the alignment of the specimen is dependent on the skill of the technician. On

    the other hand, a pinned grip assures good alignment. Threaded shoulders and grips also

    assure good alignment, but the technician must know to thread each shoulder into the grip at

    least one diameter's length, otherwise the threads can strip before the specimen fractures.

    In large castings and forgings it is common to add extra material, which is designed to be

    removed from the casting so that test specimens can be made from it. These specimen not be

    exact representation of the whole work piece because the grain structure may be different

    throughout. In smaller work pieces or when critical parts of the casting must be tested, a work

    piece may be sacrificed to make the test specimens. For work pieces that are machined from

    bar stock, the test specimen can be made from the same piece as the bar stock.

    3.2.2. IZOD IMPACT TEST:-

    Izod impact strength testing is an ASTM standard method of determining impact

    strength. A notched sample is generally used to determine impact strength.

    The test is named after the English engineer Edwin Gilbert Izod (18761946), who

    described it in his 1903 address to the British Association, subsequently published in

    Engineering.

    The specimen is clamped into the pendulum impact test fixture with the notched side

    facing the striking edge of the pendulum. The pendulum is released and allowed to strike

    through the specimen. If breakage does not occur, a heavier hammer is used until failure

    http://en.wikipedia.org/wiki/Casting_(metalworking)http://en.wikipedia.org/wiki/Forginghttp://en.wikipedia.org/wiki/Machininghttp://en.wikipedia.org/wiki/Bar_stockhttp://en.wikipedia.org/wiki/ASTMhttp://en.wikipedia.org/wiki/British_Associationhttp://en.wikipedia.org/wiki/Casting_(metalworking)http://en.wikipedia.org/wiki/Forginghttp://en.wikipedia.org/wiki/Machininghttp://en.wikipedia.org/wiki/Bar_stockhttp://en.wikipedia.org/wiki/ASTMhttp://en.wikipedia.org/wiki/British_Association
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    occurs. Since many materials (especially thermoplastics) exhibit lower impact strength at

    reduced temperatures, it is sometimes appropriate to test materials at temperatures that

    simulate the intended end use environment.

    Impact is a very important phenomenon in governing the life of a structure. In the case

    of aircraft, impact can take place by the bird hitting the plane while it is cruising, during take

    off and landing there is impact by the debris present on the runway

    An arm held at a specific height (constant potential energy) is released. The arm hits

    the sample and breaks it. From the energy absorbed by the sample, its impact strength is

    determined.

    The dimensions of a standard specimen for ASTM D256 are 4 x 12.7 x 3.2 mm (2.5" x

    0.5" x 1/8"). The most common specimen thickness is 3.2 mm (0.125"), but the width can

    vary between 3.0 and 12.7 mm (0.118" and 0.500").

    This test can also be used to determine the notch sensitivity.

    3.2.3CHARPY IMPACT TEST:-The Charpy impact test, also known as the Charpy v-notch test, is a standardized high

    strain-rate test which determines the amount ofenergy absorbed by a material during fracture.

    This absorbed energy is a measure of a given material's toughness and acts as a tool to study

    temperature-dependent brittle-ductile transition. It is widely applied in industry, since it is

    easy to prepare and conduct and results can be obtained quickly and cheaply. But a major

    disadvantage is that all results are only comparative.

    The test was developed in 1905 by the French scientist Georges Charpy. It was pivotal

    in understanding the fracture problems of ships during the Second World War. Today it is

    used in many industries for testing building and construction materials used in the

    construction of pressure vessels, bridges and to see how storms will affect materials used in

    building.

    http://en.wiktionary.org/wiki/standardizedhttp://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Energyhttp://en.wikipedia.org/wiki/Fracturehttp://en.wikipedia.org/wiki/Toughnesshttp://en.wikipedia.org/wiki/Georges_Charpyhttp://en.wiktionary.org/wiki/standardizedhttp://en.wikipedia.org/wiki/Strain_(materials_science)http://en.wikipedia.org/wiki/Energyhttp://en.wikipedia.org/wiki/Fracturehttp://en.wikipedia.org/wiki/Toughnesshttp://en.wikipedia.org/wiki/Georges_Charpy
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    The apparatus consists of a pendulumaxe swinging at a notched sample of material.

    The energy transferred to the material can be inferred by comparing the difference in the

    height of the hammer before and after a big fracture.

    The notch in the sample affects the results of the impact test, thus it is necessary for

    the notch to be of regular dimensions and geometry. The size of the sample can also affect

    results, since the dimensions determine whether or not the material is in plane strain. This

    difference can greatly affect conclusions made.

    The "Standard methods for Notched Bar Impact Testing of Metallic Materials" can be

    found in ASTM E23, ISO 148-1 or EN 10045-1, where all the aspects of the test and

    equipment used are described in detail.

    3.2.4. ROCKWELL HARDNESS TEST

    The Rockwell scale is a hardness scale based on the indentation hardness of a material.

    The Rockwell test determines the hardness by measuring the depth of penetration of an

    indenter under a large load compared to the penetration made by a preload. There are different

    scales, which are denoted by a single letter, that use different loads or indenters. The result,

    which is a dimensionless number, is noted by HRX where X is the scale letter.

    When testing metals, indentation hardness correlates linearly with tensile strength.

    This important relation permits economically important nondestructive testing of bulk metal

    deliveries with lightweight, even portable equipment, such as hand-held Rockwell hardness

    testers

    http://en.wikipedia.org/wiki/Pendulumhttp://en.wikipedia.org/wiki/Axehttp://en.wikipedia.org/wiki/Inferhttp://en.wikipedia.org/wiki/Hardnesshttp://en.wikipedia.org/wiki/Indentation_hardnesshttp://en.wikipedia.org/wiki/Tensile_strengthhttp://en.wikipedia.org/wiki/Pendulumhttp://en.wikipedia.org/wiki/Axehttp://en.wikipedia.org/wiki/Inferhttp://en.wikipedia.org/wiki/Hardnesshttp://en.wikipedia.org/wiki/Indentation_hardnesshttp://en.wikipedia.org/wiki/Tensile_strength
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    CHAPTER - 4

    RESULTS AND ANALYSIS

    4.1. TESTS PERFORMED

    4.1.1. TENSILE TEST

    BEFORE HEAT TREATMENT:-

    a- Original dimensions:

    Diameter of specimen (d1) = 10mm

    Cross sectional area of specimen (A1)= 1)2 mm2 = 78.53mm2

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    Gauge length of specimen (l1) = 5.65 1 = 50.0 mm

    b- Final dimensions:

    Diameter of specimen (d2) = mm

    Cross sectional area of specimen (A2)= 2)2 mm2

    Gauge length of specimen (l2) = 5.65 2

    Table No.4.1- Tensile Test Table Before Heat Treatment

    S.No Ultimate

    load

    (kN)

    Extension

    (l2-l1) mm

    Ultimate

    strength=

    (MPa)

    % elongation = % reduction in

    area =

    1 18.5 60-50=10 235.5 20 84.00

    2 16.25 58-50=8 206.9 16 80.66

    3 18.0 59-50=9 229.1 18 82.36

    Mean diameter at breaking point = 4.2mm

    1- Mean Ultimate strength = (235.5+206.6+229.1) / 3

    = 223.8 MPa

    2- Mean % elongation = (20+16+18) / 3

    = 18 %

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    3- Mean % reduction in area = (84+80.66+82.36) / 3

    = 82.34 %

    FFig 4.1 Tensile Test Specimen Before Heat Treatment

    AFTER HEAT TREATMENT:-

    i) TENSILE TEST AFTER NORMALIZING:-

    Table No.4.2- Tensile Test Table After Normalizing

    S.No Ultimate

    load

    (kN)

    Extension

    (l2-l1) mm

    Ultimate

    strength=

    (MPa)

    % elongation = % reduction in

    area =

    1 8.5 64-50=14 108.2 28 82.36

    2 9 63-50=13 114.6 26 81.5

    3 9.2 64-50=14 117.15 28 82.36

    Area =/4(D12)

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    = /4(10)2 = 78.53 mm2

    Ultimate strength = 1000

    (i) Ultimate strength= (8.5 x1000) / 78.53 = 108.2 MPa

    (i) Ultimate strength= (9 x1000) / 78.53 = 114.6 MPa

    (iii) Ultimate strength= (9.2 x1000) / 78.53 = 117.15 MPa

    Mean ultimate strength = (108.2+114.6+117.15) / 3 = 113.31 MPa

    Percentage elongation =

    (i) % age elongation = [(64-50) / 50] x100 = 28%

    (ii) % age elongation = 26%

    (iii)% age elongation = 28%Mean percentage elongation = (28+26+28) / 3 = 27.33 %

    Percentage reduction in area =

    A1=78.53 mm2

    (i) A2= /4 x (4.2)2 = 13.85 mm2

    %age reduction= 82.36%

    (ii) A2= /4 x (4.3)2 = 14.52 mm2

    %age reduction= 81.5%

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    (iii) A2= /4 x (4.2)2 = 13.85 mm2

    %age reduction= 82.36%

    Mean reduction in area = (82.36+81.5+82.36) / 3= 82.07%

    ii) TENSILE TEST AFTER QUENCHING:-

    Table No.4.3- Tensile Test Table After Quenching

    S.No Ultimate

    load(kN)

    Extension

    (l2-l1) mm

    Ultimate

    strength=

    (MPa)

    % elongation = % reduction in

    area =

    1 9.75 60-50=10 124.15 20 76.9

    2 10 63-50=13 127.15 26 84.00

    3 9.5 61-50=11 120.97 22 19.63

    Area =/4(D12)

    = /4(10)2 = 78.5mm2

    Ultimate strength = 1000

    (i) Ultimate strength= (9.75 x1000) / 78.53 = 124.15 MPa

    (ii) Ultimate strength= (10 x1000) / 78.53 = 127.33 MPa

    (iii) Ultimate strength= (9.5 x1000) / 78.53 = 120.97 MPa

    Mean ultimate strength = (12.15 + 127.33 + 120.97) / 3 = 124.15 MPa

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    Percentage elongation =

    (i) % age elongation = [(60-50) / 50]x100 = 20%

    (ii) % age elongation = [(63-50) / 50]x100 = 26%

    (iii) % age elongation = [(61-50) / 50]x100 = 22%

    Mean percentage elongation = (20+26+22) / 3 = 22.66 %

    Percentage reduction in area =

    A1=78.53 mm2

    (i) A2= /4 x (4.8)2 = 18.095 mm2

    %age reduction= [(78.53-18.0955) / 78.53] x100

    = 76.9%

    (ii) A2= /4 x (4)2 = 12.56 mm2

    %age reduction= 84.0%

    (iii) A2= /4 x (5)2 = 19.6325 mm2

    %age reduction= 75.0%

    Mean reduction in area = (76.9+ 84+ 75) / 3= 78.63%

    iii) TENSILE TEST AFTER ANNEALING:-

    Table No.4.4- Tensile Test Table After Annealing

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    S.No Ultimate

    load

    (kN)

    Extension

    (l2-l1) mm

    Ultimate

    strength=

    (MPa)

    % elongation = % reduction in

    area =

    1 6 68-50=18 76.403 36 87.7

    2 6 66-50=16 78.95 32 85.5

    3 6 68-50=18 77.25 36 87.7

    Area =/4(D12)

    = /4(10)2

    = x 25= 78.5 mm2

    Ultimate strength = 1000

    (i) Ultimate strength= (6 x1000) / 78.53 = 76.403 MPa

    (ii) Ultimate strength= (6 x1000) / 78.53 = 78.95 MPa

    (iii) Ultimate strength= (6 x1000) / 78.53 = 76.403 MPa

    Mean ultimate strength = (76.403+78.95+76.403) / 3 = 77.25 MPa

    Percentage elongation =

    (i) % age elongation = [(68-50) / 50]x100 = 36%

    (ii) % age elongation = 32%

    (iii) % age elongation = 36%

    Mean percentage elongation = (36+32+36) / 3 = 34.66 %

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    Percentage reduction in area =

    A1=78.53 mm2

    (i) A2= /4 x (3.5)2 = 9.6 mm2

    %age reduction= 87.7%

    (ii) A2= /4 x (3.8)2 = 11.34 mm2

    %age reduction= 85.5%

    (iii) A2= /4 x (3.5)2 = 9.6 mm2

    %age reduction= 87.7%

    Mean reduction in area = (87.7+85.5