university of bradford university of bradford micromoulding 2003 ukmig – update and future work dr...
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![Page 1: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/1.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
UkMIG – Update and Future WorkUkMIG – Update and Future Work
Dr Ben WhitesideDr Ben Whiteside
IRC in Polymer EngineeringIRC in Polymer Engineering
Bradford Bradford
February 2003February 2003
Dr Ben WhitesideDr Ben Whiteside
IRC in Polymer EngineeringIRC in Polymer Engineering
Bradford Bradford
February 2003February 2003
![Page 2: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/2.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Current WorkCurrent Work
• 1 Microsystem50 process monitoring• 2 Moulding Trials• 3 Morphology Measurements• 4 Publications• 5 Going smaller• 6 Future Work
• 1 Microsystem50 process monitoring• 2 Moulding Trials• 3 Morphology Measurements• 4 Publications• 5 Going smaller• 6 Future Work
![Page 3: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/3.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Dynisco PCI 4011 Piezo load transducer ( 10kN)
Dynisco PCI 4011 Piezo load transducer ( 10kN)
Dynisco PCI 4006 piezo load transducer (2.5kN)
Dynisco PCI 4006 piezo load transducer (2.5kN)
1 Process Measurement - Sensor Installation
1 Process Measurement - Sensor Installation
Temposonics R series displacement transducer
Temposonics R series displacement transducer
J-type thermocouplesJ-type thermocouples
![Page 4: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/4.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
1 Process Measurement – Data Capture
1 Process Measurement – Data Capture
Injection Pressure
Cavity Pressure
Ram Displacement
Ram Velocity
3 Temperature Channels
Injection Pressure
Cavity Pressure
Ram Displacement
Ram Velocity
3 Temperature Channels
Max sampling rate ~ 30 000HzMax sampling rate ~ 30 000Hz
![Page 5: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/5.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Nylon6 NC in stepped plaque mould
0.00
10.00
20.00
30.00
40.00
50.00
60.00
70.00
80.00
90.00
100.00
0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00
Time (s)
Inje
cti
on
/Ca
vit
y P
res
su
re
(Mp
a)/
Dis
pla
ce
me
nt
(mm
)
0.00
100.00
200.00
300.00
400.00
500.00
600.00
700.00
Inje
cti
on
Ve
loc
ity
(m
m/s
)Injection Pressure
Displacement
Cavity Pressure
Injection Velocity
![Page 6: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/6.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Process data for Nylon6 NC in 0.25mm plaque
0
20
40
60
80
100
120
140
160
180
200
0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00
Time (s)
Inje
ctio
n P
ress
ure
(M
Pa)
/Dis
pla
cem
ent
(mm
)
0
100
200
300
400
500
600
700
800
900
1000
Inje
ctio
n V
elo
city
(m
m/s
)Injection Pressure
Displacement
Injection Velocity
![Page 7: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/7.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Process data for Nylon6 NC in 0.25mm plaque
0
20
40
60
80
100
120
140
160
180
200
0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75 0.80 0.85 0.90
Time (s)
Inje
ctio
n P
ress
ure
(M
Pa)
/Dis
pla
cem
ent
(mm
)
0
100
200
300
400
500
600
700
800
900
1000
Inje
ctio
n V
elo
city
(m
m/s
)
Injection Pressure
Displacement
Injection Velocity
![Page 8: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/8.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
1 Process Measurement -Issues/Discussion
1 Process Measurement -Issues/Discussion
Isolate source of oscillation
• Servo drive?
• Mechanical linkage?
Intelligent monitoring
• Reject bad parts
• Process control
Isolate source of oscillation
• Servo drive?
• Mechanical linkage?
Intelligent monitoring
• Reject bad parts
• Process control
![Page 9: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/9.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
2 Moulding Trials 2 Moulding Trials
Materials moulded Dec 2002/Jan 2003: -
• BP Rigidex 5050 HDPE
• BIP POMC 109 Polyacetal co-polymer
• PA6 w/ 2% Carbon Nano-composite
Materials moulded Dec 2002/Jan 2003: -
• BP Rigidex 5050 HDPE
• BIP POMC 109 Polyacetal co-polymer
• PA6 w/ 2% Carbon Nano-composite
![Page 10: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/10.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
2 Moulding Trials2 Moulding Trials
Materials due for moulding Feb 2003: -
• PP based Nano-composite (Brunel)
• Hapex bone analogue material
• PEEK?
• High temperature oil heaters arrived Jan 2003
Materials due for moulding Feb 2003: -
• PP based Nano-composite (Brunel)
• Hapex bone analogue material
• PEEK?
• High temperature oil heaters arrived Jan 2003
![Page 11: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/11.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements - AFM3 Morphology Measurements - AFM
![Page 12: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/12.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements - Structure3 Morphology Measurements - Structure
Nano-indentNano-indent
Crystal StructureCrystal Structure
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MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements – Spherulite size
3 Morphology Measurements – Spherulite size
![Page 14: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/14.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements – Amorphous layer
3 Morphology Measurements – Amorphous layer
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MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements - Importance
3 Morphology Measurements - Importance
• Proportion and geometry/orientation of crystal structures have a very significant influence on the mechanical properties of the product
• Material data sheets specify mechanical property data based on tests on thick ~4mm sections
• Not applicable to these components
• Proportion and geometry/orientation of crystal structures have a very significant influence on the mechanical properties of the product
• Material data sheets specify mechanical property data based on tests on thick ~4mm sections
• Not applicable to these components
How will the micromoulded component perform?How will the micromoulded component perform?
![Page 16: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/16.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
3 Morphology Measurements - Application
3 Morphology Measurements - Application
• Influence of processing parameters upon morphology can be assessed
• Careful control of processing conditions may allow the moulder to ‘tune’ the mechanical performance of the final product
• Influence of processing parameters upon morphology can be assessed
• Careful control of processing conditions may allow the moulder to ‘tune’ the mechanical performance of the final product
• Proportion of amorphous material is inversely proportional to the size of product
• Smaller products offer more control
• Proportion of amorphous material is inversely proportional to the size of product
• Smaller products offer more control
![Page 17: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/17.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
4 Publications4 Publications
Conference Papers: -
• Antec2003 – Nashville, USA, 2003• PPS19 – Melbourne, Australia, 2003
Journal Papers: -
• Plastics Rubber Composites• Polymer Engineering and Science
Conference Papers: -
• Antec2003 – Nashville, USA, 2003• PPS19 – Melbourne, Australia, 2003
Journal Papers: -
• Plastics Rubber Composites• Polymer Engineering and Science
![Page 18: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/18.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
5 Going smaller…5 Going smaller…
Mini/Micromoulding cavities have proved useful for:
• Familiarisation with the micromoulding process
• Surface finish measurements
• Developing property measurement techniques
Mini/Micromoulding cavities have proved useful for:
• Familiarisation with the micromoulding process
• Surface finish measurements
• Developing property measurement techniques
But the work performed so far suggests we now need to move to smaller length scalesBut the work performed so far suggests we now need to move to smaller length scales
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MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
5 Going smaller…5 Going smaller…
![Page 20: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/20.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
5 Going smaller - ‘Top Hat’ Moulding5 Going smaller - ‘Top Hat’ Moulding
‘Disc’ diameter = 1mm‘Cylinder’ diameter = 0.5mm Volume = 0.34mm2
‘Disc’ diameter = 1mm‘Cylinder’ diameter = 0.5mm Volume = 0.34mm2
1 m
m
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MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
6 Future Work – coming months6 Future Work – coming months
February 2003
• Complete moulding trials with remaining materials
• Commissioning of ‘top hat’ micromoulds
March 2003
• Complete characterisation of moulded samples
• Morphology measurements
• Nano-composite dispersion
• Mould/product surface detail comparisons
February 2003
• Complete moulding trials with remaining materials
• Commissioning of ‘top hat’ micromoulds
March 2003
• Complete characterisation of moulded samples
• Morphology measurements
• Nano-composite dispersion
• Mould/product surface detail comparisons
![Page 22: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/22.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
6 Future Work - onwards6 Future Work - onwards
March
• Moulding of ‘top hat’ cavities
• Product assessment
• Bradford/Rondol Micro-Injection Compounder experiments
• Bringing it all together – EPSRC final report
March
• Moulding of ‘top hat’ cavities
• Product assessment
• Bradford/Rondol Micro-Injection Compounder experiments
• Bringing it all together – EPSRC final report
![Page 23: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/23.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
6 Future Work – New Bid6 Future Work – New Bid
Areas of interest:
• Mould manufacture – techniques, precision, detail, surface finish
• Modelling of the process – can accepted theories cope?
• Smaller length scales – build on existing infrastructure
• Controlling morphology
Areas of interest:
• Mould manufacture – techniques, precision, detail, surface finish
• Modelling of the process – can accepted theories cope?
• Smaller length scales – build on existing infrastructure
• Controlling morphology
![Page 24: UNIVERSITY OF BRADFORD UNIVERSITY OF BRADFORD MicroMoulding 2003 UkMIG – Update and Future Work Dr Ben Whiteside IRC in Polymer Engineering Bradford February](https://reader030.vdocuments.net/reader030/viewer/2022012922/55141b0a550346ec488b554c/html5/thumbnails/24.jpg)
MicroMoulding 2003MicroMoulding 2003
UNIVERSITY OFBRADFORD
UNIVERSITY OFBRADFORD
Thank YouThank You