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Catalogue ViscometryViscoSystem® | AVS® | ViscoClock | Viscometers

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Content viscometry

Xylem Analytics Germany GmbH / SI Analytics GmbH / 독일

Application for AVS measurement systems

Page 3

자동 점도계 : ViscoClock Plus, AVS470, AVS370, AVSPro

Page 5

점도 측정용 Viscosity Bath : CT72 Transparent Thermostats (Bath & Cooler)

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모세관 점도계 Viscometers

Page 31

피스톤 뷰렛 Titronic (piston burette)

Page 45

Cannon Instrument Company / 미국

자동 점도계 : PolyVISC, MiniPV, MiniPV-HX

Page 49

점도 측정용 Temperature Bath

Page 57

모세관 점도계 Glass Capillary Viscometers

Page 64

점도표준액 Viscosity Standards

Page 77

Digital Vacuum Regulators

Page 83

Pro-Pak

Page 84

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Ufit.de / 독일

자동점도계 : UVS Basic

Page 85

Bah & chiiler

Page 91

Tamson Instruments / 네델란드

점도측정용 Viscosity Bath

Page 95

2mag AG / 영국

다점용해조 Stirring Heating Blocks

Page 105

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AVS®AVS® measurement systems within

quality assurance systems

Business sector Product Example

Automotive engineering motor oil (fresh and used)

high polymer plastics

bumpers

Brewery original wort

hop-wort

beer

beer

Electrical engineering and electronics high polymer plastics of all types chips, casings

Power supply turbine oil

transformer oil

generators

Plastics manufacturers high polymer plastics of all types

Plastics processors high polymer plastics of all types injection molding

Food industry starch

gelatin

packaging materials

milk products

fruit and fruit juice concentrates

gelatinizing agents

instant flour thickeners

jelly bears

yogurt containers

yogurt drink

pectin

Aviation high polymer plastics of all types

fuels

hydraulic fluids

kerosene

horizontal stabilizers and undercarriages

Mechanical engineering mold oil

hardening emulsions

hydraulic fluids

mill trains

stamp shops

Medicine body fluids

injection solutions

tinctures and drops

blood substitute materials

blood, bile

insulin

nose, eyes

blood plasma

Mineral oil light motor oil

turbine oil

liquid fuels of all types

gasoline, diesel fuel, kerosene (jet fuel)

Textile high polymer plastics of all types

cotton

for mixed fibers

Entertainment high polymer plastics CDs, DVDs

The table on the right illustrates the extensive area of high polymer plastics and the large variety of testing methods.

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AVS®Operating temperature

Suitability of the AVS® measurement systems

Type Abbr. Solvent Capillary Standards VC* 370 470 Pro

Cellulose C I

EWNCuen (CED)Cuen (CED)Cuen (CED)Cuen (CED) Cuen (CED)Cuen (CED)

20 °C20 °C20 °C25 °C25 °C25 °C25 °C

SNV 195598DIN EN 60450ASTM D 4243ISO 5351AST; D 1795 SCAN CM 15:99TAPPI T230-0M99

Cellulose acetate

CA Dimethyl- chloride/ methanol

0c I I Micro

25 °C ASTM D817

Polyamide PA Sulphuric acid (96 %)

II IIc

25 °C ISO 307

Polyamide PA Formic acid (90 %)

I Ic

25 °C ISO 307

Polyamide PA m-cresol II IIc

25 °C ISO 307

Polybutylene terephthalate

PBT Phenol/dichloro benzene (50 : 50)

Ic II

25 °C ISO 1628-5

Polycarbonate PC Dichloromethane 0c I

25 °C ISO 1628-4

Polyethylene PE Decahydro -naphthalene

I Ic

135 °C ISO 1628-3 ASTM D 1601

Polyethylene terephthalate

PET m-cresol II IIc IIc Micro

25 °C ISO 1628-5 ASTM D 4603


PET Phenol/dichloro benzene (50 : 50)

Ic II

25 °C ISO 1628-5 ASTM D 4603


PET Dichloroacetic acid

II IIc Micro

25 °C

Polymethyl methacrylate

PMMA Chloroform 0c I

25 °C ISO 1628-6

Polypropylene PP Decahydro- naphtalene

I Ic

135 °C ISO 1628-3

Polystyrene PS Toluene I Ic

25 °C

Polysulphone PSU Chloroform 0c 25 °C

Polyvinyl chloride PVC Cyclohexanone Ic 25 °C ISO 1628-2 ASTM D 1243

Styrene-acrylo- nitrile copolymer

SAN Ethyl methyl ketone

0c I

25 °C

Styrene-butadiene copolymer

SB Toluene 0c I

25 °C

Polymer applications for the AVS® measurement systems

Polymers, their applications and utilization of our automatic systems

VC* = ViscoClock

excellent suitability; can be used; limited suitability for application related reasons.

This table makes no claim to completeness.

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ViscoClock plus

ViscoCIock plus - Measurement plus data storage

The ViscoCIock plus is an electronic timing unit for glass capillary viscometers used to determine kinematic and relative viscosity. Succeeding the well-proven ViscoCIock, the new instrument features data storage and simpler handling. The ViscoClock plus is especially designed for Ubbelohde type viscometers which are well-known for highest precision.

The ViscoCIock plus

The ViscoClock plus automatically measures the fl ow time of temperature-stabilized liquids in capillary viscometers by means of infrared light barriers: the manual measurement with a stopwatch becomes obsolete. The viscometer including a sample is inserted into the ViscoClock plus and immersed into a thermostatic bath for temperature stabilization. After thermostating, the sample is pumped into the measuring bulb, and the fl ow time is detected automatically. The large display enables easy read-off of fl ow times and additional information: date, time, sample ID and viscometer ID.

ViscoClock plus

bath for temperature stabilization. After thermostating, the sample is pumped into the measuring bulb, and the fl ow time is detected automatically. The large display enables easy read-off of fl ow times and additional information: date, time, sample ID and viscometer ID.

ViscoClock plus ViscoClock plus - head

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ViscoClock plusViscoClock plus

Benefi tsViscoClock plus

Automatic and precise fl ow time measurement for a low price

Suitable for SI Analytics® Ubbelohde, Micro Ubbelohde and Micro Ostwald viscometers

Data storage incl. time, date, viscome-ter and sample ID

Stand is made of high performance engineering plastic PPA and enables measuring temperatures up to 150°C

Electromagnetic venting valve for convenient handling of Ubbelohde viscometer

Compatible with all SI Analytics® thermostatic bath types

ViscoClock plusViscoClock plus

Automatic measurement of fl ow times

The ViscoCIock plus is designed for SI Analytics® Ubbelohde, Micro Ubbelohde and Micro Ostwald viscometers. The fl ow time is measured automatically by two infrared light barriers which detect the passing liquid meniscus. The repeatability of the automatic time measurement is considerably higher in comparison to the measurement using a stop watch. Therefore some viscometry standards allow a fl ow time reduction in case of automatic fl ow time measurement.

Properties and materials

The ViscoCIock plus can be used for measuring temperatures ranging from -40 °C to 150 °C. The stand of the ViscoClock plus ist made of high quality polymer PPA. For temperature stabilization in a thermostatic bath, the following liquids are suitable: Water, alcohol, glycol, paraffi n oil, and silicon oil.The electronic measuring unit is built-in to a PP casing.

Easy handling

The ventilation of Ubbelohde viscometers is managed by an electromechanic valve which makes handling easier in comparison to the mechanical mechanism of the previous ViscoClock.

Data storage

The measuring results of the ViscoClock plus can be stored on a USB fl ash drive including date, time and sample/viscometer ID. The data are stored as pdf (non-editable) and csv (editable). Alternatively, for data transfer the ViscoClock plus can be connected to a printer (TZ 3863) or a PC.

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ViscoClock plusSample and viscometer identifi cation

To allocate the stored measuring results, the user can enter 2-digit numbers to the ViscoClock plus before measurement. These IDs – together with date and time – ensure an unambiguous assignment of the fl ow times.

Absolute viscosity

To determine absolute kinematic viscosities, calibrated viscometers have to be used. To guarantee best accuracy, viscometers which were calibrated by automatic measurement should be used. The constant of automatic calibration can be slightly different in comparison to manual calibration, as the level of the light barriers may not be identical to the position of timing marks.

Relative viscosity

For determination of relative viscosities, calibrated as well as non-calibrated viscometers can be used. For evaluation, the calibration constant is not required in this case.

ViscoCIock plus - The plus for your measurements

The viscometer stand:high-performance plastic PPA

Well arranged: The new display

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Technical Data - ViscoCIock plus

Measuring range - Time up to 999.99 s; resolution 0.01 s

Accuracy of time measurement

± 0.01 s / ± 1 digit; however no more precise than 0.1 %;

indicated as measuring uncertainty with a confidence level of 95 %

Measuring range - viscosity

0.35 to10,000 mm²/s (cSt)

the absolute, kinematic viscosity is additionally dependent on the uncertainty of the numerical value of the viscometer constant and on the measuring conditions, in particular the measuring temperature.

Display LCD grafic display (FSTN) 128x64 pixel, 51x31mm (w x h)

seconds indication with 2 decimal digits after the decimal point, resolution 0.01 s

Voltage supply DC + 9 V

Power supply socket for low voltage connection: coaxial power connector, inner diameter 2.1 mm, plus pole at inner contact

for connection of Universal power supply TZ 1858

Power supply in accordance to class of protection III

degree of protection for dust and humidity IP 50 in accordance with DIN 40 050

Universal power supply TZ 1858: 100 – 240 V, 50 – 60 Hz (9 V, 550 mA)

not suitable for use in areas subject to explosion hazards

Plug Connections USB Host to connect USB flash drive or printer (TZ 3863)

USB OTG to connect (PC), printer (TZ 3863) or USB flash drive

Type A USB connector

Type B mini USB connector

Ambient Conditions Ambient temperature + 10 to + 40 °C for storage and transport

Operating temperature stand: – 40 to + 150 °C

electronic measuring unit: +10 to +40 °C

Humidity in accordance with EN 61 010, Part 1;

max. relative humidity 80 % for temperatures up to 31 °C,

decreasing linearly to 50 % of relative humidity at a temperature of 40 °C

Housing Materials stand: polyphthalamide (PPA)

casing*: polypropylene (PP)

gaskets: silicone

Dimensions ~515 x 90 x 30 mm (H x W x D)

Weight ~450 g (without viscometer)

power supply unit: ~220 g

Country of origin Federal Republic of Germany

CE symbol In accordance with low voltage guideline 2014/35/EU

Test regulation EN 61 010-1:2011-07 for laboratory instruments in accordance with EMC regulation 2014/30/EU

Test regulation EN 61 326 Part1:2012

In accordance with RoHS regulation 2011/65/EU;

Test regulation EN 50 581:2013-02

FCC Symbol

Viscometer types Ubbelohde (DIN; ISO; ASTM; Micro), Micro-Ostwald, manufactured by SI Analytics®

Transparent thermostatic baths

The ViscoClock plus can be used in all SI Aanyltics bath types

* Use in heat carrier liquids can result in discoloration of the synthetic material. The discoloration does not, however, have any effect on the function and quality of the ViscoClock. Subject to technical changes.

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AVS® 470

Precise Capillary Viscometry –

Easy, Flexible and Independent: AVS® 470

No PC needed: “Suction” and “Pressure” measurements

with just one instrument

The AVS® 470 is the first viscosity measurement device that

allows “suction” and “pressure” measurements completely

independent of a PC. This allows for maximum indepen-

dence and flexibility; set up a measuring station that meets

the highest requirements even under difficult conditions,

e.g. to monitor production or quality control in the polymers

and mineral oil industry.

Perfectly equipped for fully

automatic viscosity measurements

The AVS® 470 is a measuring system that includes almost

everything you need to take precise and reproducible mea-

surements. All common types of viscosity calculation are

integrated into the device, a small PS2 keyboard allows you

to enter additional data. A serial printer can be used to con-

veniently document your results.

So, in a minimum of space, you can set up a measuring sta-

tion equal in every way to complex measuring installations in

terms of precision and reproducibility.

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AVS® 470 Automatic and highly precize measurements

– independent of a PC

"Suction" and "pressure" measurements

with the same system

Simple data input and parameterization via

included PS2-mini-keyboard

GLP documentation compliant when

connected to an optional printer

AdvantagesAVS® 470

“Pressure” “Suction”

highly viscous samples e.g. oils, polymers

Solvents: (examples)

highly volatile –

Dichloromethane –

Chloroform –

Sulfuric acid –

Dichloroacetic acid –

Toluene

Hexafluoro-isopropanol

m-cresol –

Formic acid –

Phenol-dichlorobenzene –

Phenol-Tetrachloroethane –

“Suction” or “Pressure”?

Preferred applications in comparison

Simple and updateable Modular Concept

The AVS® 470 is of a modular design and an optional optical

or TC version ViscoPump II module.

You can use your existing accessories such as thermostats,

stands, flow-through coolers or automatic cleaners e. g.

AVS® 26. Also, virtually all customary capillary viscometers

can be used.

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AVS® 470

Bild fehlt

AVS® 470 – Precise and Reliable

Working with the AVS® 470 is easy

The desired measurement method can be preselected and

started on the device. The entire measurement is automatic

to eliminate subjective measurement errors. Once the set

pre-heating time is reached, the desired number of mea-

surements are taken and the viscometer automatically

cleaned if required.The status of the measurements is con-

tinuously displayed.

If required, individual parameters may be input via an

included PS 2 keyboard. A serial printer can be used to print

measurement logs.

The connections are on the front panel of the device for easy

control. Over-pumping and oversuction are prevented by

the use of a an optional capacitive sensor.

Individually determined readings

Indication of method set

Designation of specimen

Readings usedfor evaluation

Set equalization time

Corrected average running time

Calculated Viscosity

Charge Number

User

Set maximum permissible deviation from average

Average of running times

Viscosimeter constant

Operating temperature, date and time at time of test

The print-out shows every-thing you need for reliable documentation of your test.

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AVS® 470

Clear user guidance, clear

status – even without PC!

Technical data

After switching on the AVS® 470 a self test is run and then an entry prompt appears.

The parameters can be set in the test mode. The t0 value is determined automatically.

All setup parameters can be preset conveniently, e.g. pressure/suction, velocity, waiting time between two tests, etc.

The readings can be read off conveniently on the display regardless of whether or not a printer is connected.

Measuring range (time) up to 9,999.99 s; resolution 0.01 s

Measuring range (viscosity)pressure: 0.35 to 1,800 mm²/s (cSt)

suction: 0.35 to ~5,000 mm²/s (cSt)

Measured parameter flow-through time [s]

Time measuring accuracy ± 0.01 %

Measured value display LC-Display

Display accuracy ± 0.01 s, ± 1 Digit, but not exceeding 0.1%

Pumping pressure fully automatically controlled

suction up to ~-160 mbar, pressure up to ~+160 mbar

Preselectable tempering period

0 to 20 min

Preselectable no. of measurements

1 to 99 for each sample

Connections Pneumatic connections threaded connections for viscometers

Electrical connections circular connector with bayonet lock for viscometer4-pin DIN socket for TC viscometer

4-pin circular connector for capacitive sensor

7-pin circular connector for AVS® 26, with bayonet lock

RS232-C interface 9-pin for serial printer

Mains connection connector in acc. with EN 60320

Pump connection socket outlet in accordance with EN 60320

Ambient Conditions Ambient temperature +10 to +40 °C for operation and storage

Air humidity max. 80 % in acc. with EN 61010, Part 1

Housing Material steel aluminium housing;

with chemically resistant 2-component coating

Dimensions (W x H x D) ~255 x 205 x 320 mm

Weight (incl. pump module) ~5.4 kg

Power supply 90 to 240 V ~, 50 to 60 Hz

Equipment safety EMC in acc. with Council Directive 89/336/EWG;

low-voltage directive

The AVS® 470 allows the use of the following viscometers: Ubbelohde viscometer to DIN, Ubbelohde viscometer to ASTM, micro Ubbelohde viscometer to DIN, micro Ostwald viscometer, Cannon-Fenske routine viscometer, TC Ubbelohde viscometer, TC micro Ubbelohde viscometer.

We reserve the right to make technical changes.AVS® is a registered trademark of SI Analytics and stands for: "Automatic Viscosity System".

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AVS® 370

AVS® 370 makes maximum precision …

Well equipped for all viscosity determination

The AVS® 370 is a measuring device, which not only mea-

sures as precisely and consistently as you expect, but also

offers maximum flexibility and future extensions. Further-

more, it saves laboratory space.

Now possible for the first time ever: “suction“ and

“pressure“ measure-ment – with one device

The AVS® 370 is the first viscosity measuring device, which

can be used for both “suction” and “pressure” measurement.

This enables simple adjustment of the measurement method

for sample. Significantly reducing investment costs for addi-

tional measuring stations at which pressure and suction

methods are to be used. In most cases, using the AVS® 370

also saves set-up time.

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AVS® 370

… easier and more flexible, with provision for future

expansion!

Easy modular concept ideal for future expansion

The AVS® 370 has a modu-lar design. The basic version is

available with one ViscoPump II module in optical or in TC

version. Up to 3 other ViscoPump II modules can be installed

in the compact 19“ housing. The measuring station can be

adapted to increasing requirements at any time.

Can be expanded from an affordable single

measuring station up to an 8-sample station

The basic version of the AVS® 370 is able to measure high or

low viscosity liquids. The TC version viscometers, for example,

it is ideal for measuring opaque and black fluids. If neces-

sary, each single measuring station can be expanded to a

multiple measuring station with PC-controlled multitasking.

The WinVisco 370 software included with the standard equip-

ment enables parallel operation of two fully equipped

AVS® 370, with a total of eight ViscoPump II modules. Each

module can measure a different sample using its own

method. All the results can be quickly and easily evaluated

and documented independently. It could hardly be more

flexible!

Compatible with existing accessories

Existing accessories (thermostats, stands, flow through cooler,

etc.) can continue to be used with the AVS® 370. Also, virtu-

ally all customary capillary viscometers can be used.

Automatic and highly precise measurements

"Suction" and "pressure" measurements

with the same module

Modular concept for up to four ViscoPump II

modules in one AVS® 370

Each ViscoPump II module in a AVS® 370 can

measure a different sample using a different

method.

Real multitasking for up to eight parallel

measurements with the software WinVisco 370

TC version for measurement of

nontransparent and black liquids

AdvantagesAVS® 370

“pressure” “suction”

Highly viscous samples e.g. oils, polymers

Solvent: (examples)

highly volatile –

Dichlormethane –

Chloroform –

Sulfuric acid –

Dichloroethanoic acid –

Toluene

Hexafluorisopropanol

m-Cresol –

Formic acid –

Phenol-dichlorobenzene –

Phenol-tetrachloroethane –

“Suction” or “pressure”?

A comparison of preferred applications

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AVS® 370AVS® 370 – the right solution for all situations

Anyone working with the AVS® 370 is

perfectly equipped for all tasks

involved in determining viscosity

using capillary viscometers.

How to automatically achieve

the right results

PC-controlled, the AVS® 370 deter-

mines the time which the liquid to be

examined requires to flow through the

measuring distance in the capillary vis-

cometer with quartz precision. The

time is displayed with a resolution of

0.01 s (1 digit).

Measurement of the flow time of the

liquid’s meniscus can be scanned

optoelectronically or with TC sen-

sors. During optoelectronic scanning

the meniscus is detected by glass

light fibers, with TC sensors the sen-

sor detects the different thermal con-

ductivity of the sample and air. The

AVS® 370 offers an extraordinarily

broad range of uses, from viscosity

measurement of clear fluids to black

or fully opaque liquids.

New: Two working principles

with the same device.

With the AVS® 370 you can use one

device to work with either “pressure”

or “suction” offering more flexibility

with the liquids to be examined.

In the “pressure” method an overpres-

sure is applied to the liquid in the cap-

illary, this is particularly advantageous

for fluids with a low boiling point. For

the “suction” principle the sample is

sucked up into the capillary by a

vacuum. Greater reproducibility is

achieved using the “suction” method

for higher viscosity samples.

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AVS® 370

Technical data

Measuring range (time) up to 9,999.99 s; resolution 0.01 s

Measuring range (viscosity)

pressure: 0.35 to 1,800 mm²/s (cSt)

suction: 0.35 to ~5,000 mm²/s (cSt)

Measured parameter flow through time [s]

Accuracy of the time measurement

± 0.01 %

Measured value display via PC

Display accuracy ± 1 digit (0.1 %)

Pump pressure automatically controlled

Preselectable tempering period

0 to 20 min

Preselectable number of measurements

up to 10

Connections Pneumatic connections threaded connections for viscometers

Electrical connections circular connector with bayonet lock for measuring stands and TC viscometers

RS232-C interface 9-pin

Mains connections plug in accordance with EN 60320

Pump connection socket outlet in accordance with EN 60320

Data Input/Output serial to EIA RS232-C

Ambient conditions Ambient temperature + 10 to + 40 °C

Air humidity max. 85 % rel.

Housing Material coated aluminum plate

Dimensions (for 1 to 4 modules) (W x H x D) ~255 x 205 x 320 mm

Weight (incl. 1 module) ~5.4 kg

Power supply 90 to 240 V ~, 50 to 60 Hz

Equipment safety EMC-Compatibility according to the Directive 89 / 336 / EEC of the Council;

low-voltage directive according to the Directive 73 / 23 / EEC of the Council,

as amended by the Directive 93 / 68 / EEC of the Council

Multi-tasking for 1 to 8 ViscoPump II modules, with WinVisco 370 software

The following viscometers can be used with the AVS® 370: Ubbelohde viscometer to DIN, Ubbelohde viscometer to ASTM, micro Ubbelohde viscometer to DIN, micro Ostwald viscometer, Cannon-Fenske routine viscometer, TC-Ubbelohde viscometer, TC-micro Ubbelohde viscometer.

We reserve the right to make technical changes.AVS® is a registered trademark of SI Analytics and stands for: "Automatic Viscosity System".

Working with AVS® 370 is easy

The entire measurement procedure is

place automatic, subjective measuring

errors are reliably eliminated. The PC

starts the measurement. After the set

preconditioning period the selected

number of measurements processed

and the measured values saved.

The system protects against acciden-

tal overpumping or oversuction by

means of a capacitive sensor. This pre-

vents the sample to be measured from

getting into the vessel containing the

liquid or inside the device.

Unique flexibility

In the PC-controlled multiple mea-

surement station, the AVS® 370 offers

unique flexibility while working in a

very small space: Up to eight modules,

which equates to two fully equipped

AVS® 370, can be run in parallel with

the WinVisco 370 software. Each

module can measure the same or dif-

ferent samples using “pressure” or

“suction”, independent of each other.

In this way, a series of measurements

can be prepared quickly and immedi-

ately evaluated and documented with

the computer. This significantly redu-

ces the time required to carry out vis-

cosity measurements, especially for in

process controls and quality assu-

rance.

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AVS® 370

Real multitasking for up to 8 measurements in parallel mode …

Easy to understand and proven: The

WinVisco 370 software

WinVisco 370 is the ideal software for

the AVS® 370*). It is supplied as part of

the standard equipment. Up to eight

viscosity measurement modules can

be controlled with only a few opera-

tional steps. The device parameters

are easy to enter: Constants, t0 flow

time, number of measurements, pre-

conditioning period, type of viscome-

ter, date and sample labeling for each

measurement station.

WinVisco 370 works in a real multitask-

ing mode making it possible for each

measurement to be processed inde-

pendently from the others. It also

means that time-consuming measure-

ments can be carried out from the

same PC, without hindering the course

of other, faster measurements. During

the measurements you can change

the monitor displays, start or stop

other measurements, print or save

measured values. All data provided by

the software can be passed on to LIMS

system.

WinVisco 370 supports three groups

of users. For simple use, access is lim-

ited to: select viscometer, measure,

load and save methods as well as

enter parameters. In the highest level,

users with administrator status can

access all the software’s facilities. Each

user is given a user ID, an access level

and a password.

*) The language (English or German) can be chosen after installation over the program menu.

All the important parameters required for the measurement are displayed on the “Methods/Results” page. If necessary, the parameter editor can be called up using “Add Parameter”, in order to enter non-standard or customer specific formulae.

All the measurements currently running can be monitored in parallel in the overview.

The viscometer data required for the evaluation can be stored in a table. This guarantees perfect allocation of e.g. the t0 runtime, viscometer constants, the series number, etc. for each individual viscometer being used.

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AVS® 370

… with the proven WinVisco 370 software

With AVS® 370 and WinVisco 370 the right connection for rinsing can

be quickly determined

With the daisy chain link of the AVS® 370, additional devices can be inte-

grated with the system and controlled using the WinVisco 370 software. For

example, when working in suction mode the viscometers can be rinsed using

the TITRONIC®300 or the TITRONIC® 500 burettes. The TITRONIC®300 is

preferable used for light solvents, the TITRONIC® 500 for solvents with a vis-

cosity >3 mm²/s. For highly aggressive solvents special changeable modules

are available (TA50V and WA50V).

A vacuum pump (accessory) integrated with the system can be used to con-

veniently remove samples and solvents.

The password protection prevents unwanted changes to the important measurement param-eters.

The parameters can be individually adjusted to the measurement for each measuring position.

Each rinse/dry step can be individually prese-lected. Even the application dependent quantity of solvent and the drying time can be separately determined.

Two basic concepts are available for the rinsing:

• An AVS® 370 with up to four ViscoPump II modules (max. four measurement

positions) and up to eight burettes, which enables each viscometer to be

rinsed with two solvents. Time consuming removal of the transparent ther-

mostat for external rinsing of the viscometer is no longer necessary.

• Two AVS® 370 complete with up to four ViscoPump II modules each (max.

eight measuring positions), which enables semi-automatic rinsing of the vis-

cometer with the next sample or solvent.

Vacuum pump

PC AVS® 370

Printer

Transparent thermostat with four measuring stands

TITRONIC® 500 TITRONIC® 300

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AVS® 370

AVS® 470Ordering information AVS® 370

Ordering information AVS® 470

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입력 텍스트

AVS® 370

AVS® 470

Accessories AVS® 470 and AVS® 370

Type no. Order no. Description

CT 72/P, 230V 285418526 Immersion thermostat 230 V and thermostatic bath (acrylic glass container with two manual gauge slides), basic configura tion for the attachment of one flow-through cooler.


CT 72/2, 230V 285418547 Immersion thermostat 230 V and thermostatic bath (stainless steel container with one manual gauge slide), basic configura tion for the attachment of one flow-through cooler.


CT 72/4, 230V 285418568 Immersion thermostat 230 V and thermostatic bath (stainless steel container with two manual gauge slides), basic configuration for the attachment of one flow-through cooler.


Z 900 285225620 RS232-C Data printer (230 V)

Measuring stand AVS®/SMeasuring stand AVS®/SK Measuring stand AVS®/SK-CF Measuring stand AVS®/SK-V

285410502

285410876

285410892

285410905

Metal measuring stand AVS®/S, preferably for nonaqueous bath fluids

PVDF measuring stand AVS®/SK, corrosion-free, suitable for aqueous and nonaqueous bath fluids

PVDF measuring stand AVS®/SK-CF, particularly for the use of Cannon-Fenske routine viscometers

PVDF measuring stand AVS®/SK-V, particularly for the use of dilution viscometers

CK 300, 115V 285414331 CFC-free flow-through cooler for enhancing the temperature constancy of the bath fluid (according to configuration and environmental conditions are ± 0.02 K possible) or for measurement at room temperature or below (min. + 5 °C).

CK 300, 230V 285414348 CFC-free flow-through cooler for enhancing the temperature constancy of the bath fluid (according to configuration and environmental conditions are ± 0.02 K possible) or for measurement at room temperature or below (min. + 5 °C).

05392 285405043 Fixing frame for Ubbelohde viscometers (not TC)

The AVS® 470 viscosity test station is composed of individual components.

Please request a detailed quote.


AVS® 470 basic unit for opto-electronic sensing

285415709 AVS® 470 basic unit, housing incl. one ViscoPump II module for opto-electronic sensing, Keyboard Version: 95 V to 230 V/50-60 Hz

AVS® 470 basic unit for TC sensing

285415708 AVS® 470 basic unit, housing incl. one ViscoPump II module for TC sensing, Keyboard Version: 95 V to 230 V/50-60 Hz

VZ 8511 1054306 ViscoPump II module for optical sensing

VZ 8512 1054304 ViscoPump II module for TC sensing

The AVS® 370 viscosity test station is composed of individual components.

Please request a detailed quote.


AVS® 370 basic unit for opto-electronic sensing

1056509 AVS® 370 basic unit, housing incl. one ViscoPump II module and WinVisco 370 software, for opto-electronic sensing

AVS® 370 basic unit for TC sensing

1056515 AVS® 370 basic unit, housing incl. one ViscoPump II module and WinVisco 370 software, for TC sensing

VZ 8511 1054306 ViscoPump II module for optical sending

VZ 8512 1054304 ViscoPump II module for TC sending

20

20

AVS® Pro III

Automatic viscosity measurement has been improved …

The AVS® Pro III automatic sampler is a fully automated

instrument for determining the viscosity of Newtonian fluids

with capillary viscometers. In spite of the high sample

throughput, the AVS® Pro III provides maximum accuracy

and reproducibility. Furthermore, working with the auto-

matic sampler is easy and allows unattended 24-hour opera-

tion.

Particularly with time consuming measurement runs, the

AVS® Pro III helps to substantially reduce the burden on

qualified users. The fully automatic mode offers an increased

level of safety when handling aggressive media, e.g. sulph-

uric acid.

The ProClean system and the microdosing make routine

operation safer. The filtration of solutions, which occasionally

may be harmful, may be ommitted. The capacitive sensors in

the suction pipe effectively prevent any damage of the

measurment system.

The AVS® Pro III automatic sampler works with the capillary

method, which is the most precise method for determining the

viscosity of Newtonian liquids in terms of physical chemistry.

The great versatility offered by vis-cometers with optical and

TC sensing systems opens up an extremely wide range of

applications. This includes measurements of clear liquids as

well as opaque petroleum products.

21

AVS® Pro III

… with the AVS® Pro III Automatic Sampler:

The viscosity measurement requirements of the polymer

and petroleum industries in particular have been incorpo-

rated into the design of the AVS® Pro III. The main feature of

the automatic unit is the three-axis positioning mechanism

of the sample dosing system. The X-Y-Z positioning mecha-

nism allows operation of up to four Micro TC viscometers in

two thermostatic baths, which can be set at two different

measurement temperatures. This method is used in oil indus-

try in order to determine the viscosity index.

The AVS® Pro III allows the operator to select the sample

sequence and which sample is to be filled into which viscom-

eter. The dosing system is available in either normal or micro

construction and operates without a valve. It is thus suitable

for nearly any type of sample.

The AVS® Pro III is equipped with opto-electronic and TC

scanning (TC = thermal conductivity method) functions for

the meniscus passage in the capillary viscometer. The sam-

ples are positioned in the easy-to-load sample rack, using

the motorized lifting mechanism. If needed, the rack can be

temperature-regulated.

AdvantagesAVS® Pro III

Fully automatic and highly precise measuring

station. Time measurement with a precision of

+/- 0.01s (but less precise than 0.1%)

Ideal for highly aggressive media

Although in combination of optical and thermical

sampling of the meniscus channel or different

capillary sizes and types, up to four viscometers

selectable

The ProClean system and micro-dosing

elminate dangerous manual filtration

of the sample

Two different sample racks are supplied: a) one rack with 56 positions for 20 ml sample bottles for micro-viscometer applica-tions

b) one rack with 16 positions to accommodate 100 ml sample bottles for normal volume applications

The electric sample lift ensures positioning of the samples in the rack at a convenient and easily monitored working height.

22

22

AVS® Pro III

Working with the AVS® Pro III is …

The AVS® Pro III is controlled by a PC, connected via RS232-

C interface. The intuitive user interface guides the user

clearly through the program. All data inputs are made using

the computer keyboard and mouse.

A faulty operating status is indicated by acoustic or optical

signals such as arrows, icons and other status messages or

request messages. During the entire work sequence, the

respective status of the AVS® Pro III is documented on the

computer screen. Furthermore, status indicators can be

selected for each individual measuring position, which pro-

vide additional information on operation.

For the respective type of measurement, pre-parameterized

sets of para meters depending on the viscometers, tempera-

ture and other measurement criteria are already provided. In

addition, all parameters can be individually adjusted to spe-

cial requirements at a special menu level. All of the standard

calculation methods are available.

The proved and tested AVS® Pro III software also makes it

possible to prepare additional individually selected calcula-

tions, such as:

• mean value,

• standard deviation,

• outlier test (A %),

• Hagenbach correction,

• absolute viscosity, dynamic viscosity (density value

required),

• viscosity index (measurement at two temperatures required),

• SUS and SFS,

• relative viscosity,

• specific viscosity,

• reduced viscosity (viscosity number),

• inherent viscosity

• intrinsic viscosity and

• K-value after Fikentscher

During the entire process, all of the parameters (depending

on the menu level) and the respective status of the individual

measuring positions, the temperature regulation system and

the sample transfer system are either visible or can be

selected.

The operator interface of the AVS® Pro III is available in Ger-

man and English. Commercially available printers for which

Windows drivers are available are suitable for documenta-

tion purposes.

Precision, reproducibility and comparability comply with

DIN 51 562-1(1999-01), ASTM D 445 and ISO 3105 standards.

The AVS® Pro III is built in accordance with international equip-

ment safety standards: CE symbol (equipment safety, low volt-

age safety, emitted interference and interference immunity).

If requested, the AVS® Pro III automatic sampler can be sup-

plied with a manufacturer’s inspection certificate based on

direct comparison with normal viscometers of the first order

in accordance with DIN 51 562 - 4: 1999-01.

›16 sample rack‹

The AVS® Pro III allows individual allocation between the

characteristics of the sample and the viscometers that are

currently in operation.

23

AVS® Pro III

… easy, reliable and safe

This means that it is not only possible to simultaneously test

the characteristics of samples with greatly differing viscosi-

ties, but also to perform measurements in various capillary

sizes and different types of viscometers. This even applies to

a combination of optical and thermal scanning. Therefore,

preliminary sorting of the samples with regard to viscosity

and the size of capillary required for the testing process is

not necessary.

It is possible to “individually” allocate each sample to a capil-

lary viscometer that is currently being used by means of the

conventional MS-Windows® “drag and drop” method.

The allocation between the sample and the viscometer is

shown on the status display.

›selection of method‹

This mode is used to specify what monitoring pa-rameters

are to be activated, e.g. if the temperature control of the

thermostats is supposed to be handled via the PC.

›options‹

This mode is used to specify the number of mea sure ments,

the preliminary temperature regulation period, the allow-

able standard deviation, the maximum allowable tempera-

ture tolerance, the rinsing type and method of the viscome-

ter.

›dosing parameters‹

This mode is used to specify the filling quantity of the vis-

cometer, the dosing speed depending on the viscosity and

the type of rinsing.

24

AVS® Pro IIITechnical data AVS® Pro III

Sampling system Sample bottles 100 ml screw-type and bottles with standard ground joint (16 pcs per rack)

20 ml round bottom glass pieces (56 pcs. per rack)

Sample rack for 100 ml screw-type and bottles with standard ground joint

for 100 ml screw-type and bottles with standard ground joint (temperature controlled up to 135°C)

for 20 ml round bottom glass pieces

Measured value recording Method meniscus scanning by means of opto-electronic system or thermal conductivity (TC)

Measuring parameter throughput time in seconds [s]

temperature in degrees Celsius [°C]

Calculated parameters mean value, standard deviation, outlier test (A %), Hagenbach correction, absolute viscosity, dynamic viscosity (knowledge of density required), viscosity index (measurement at two temperatures required) SUS and SFS, relative viscosity, specific viscosity, reduced viscosity (viscosity number), inherent viscosity, K-value

Selection parameters by means of PC keyboard, mean value, standard deviation, outlier test (A %), Hagenbach correction, absolute viscosity, dynamic viscosity (knowledge of density required), viscosity index (measurement at two temperatures required) SUS and SFS, relative viscosity, specific viscosity, reduced viscosity (viscosity number), inherent viscosity, K-value, rack position, date/time, temperature regulation period, number of measurements, number of rinsing operations, start, stop/reset

Number of measurements 1 to 99

Temperature regulation period 0 to 99 min., selectable in increments of 1 min.

Number of Viscometer tests 0 to 9 with next sample (observe sample quantity) or with preselected rack position

Data memory by means of PC

Viscosity measurement range 0.35 to 1,200 mm²/s (at room temperature of samples)

Time up to 9999.99 s, resolution = 0.01 s

Vacuum pressure automatically controlled

Viscometers available for use Ubbelohde viscometer in accordance with DIN standards

Ubbelohde viscometer in accordance with ASTM standards

Micro-Ubbelohde viscometer in accordance with DIN standards

Micro-Ostwald viscometerCannon-Fenske-Routine visco

Cannon-Fenske-Routine viscometer

TC Ubbelohde viscometer

TC Micro-Ubbelohde viscometer

25

AVS® Pro IIIMeasuring accuracy ± 0.01 s ± 1 digit, but not more precise than 0.01 %

The measuring uncertainty for measurements of absolute kinematic viscosity is also dependent on the uncertainty of the numeric value for the viscometer constant and on the measuring conditions, especially the measuring temperature.

Evaluations / results Correction Hagenbach correction (HC) for Ubbelohde, Cannon-Fenske-Routine, Micro-Ubbelohde and Micro-Ostwald viscometers

Statistical evaluation standard deviation, outlier search

Ambient conditions Ambient temperature 10 to + 40 °C

Air humidity max. 85 % relative humidity

Equipment safety CE-symbol in accordance with Guideline 89 / 336 / EEC of the Council (EMC compatibility)

in accordance with Standard EN 50 081, Part 1;

interference immunity in accordance with Standard EN 50 082, Part 2;

in accordance with Guideline 73 / 23 / EEC of the Council (low-voltage guideline)

Housing plastic/stainless steel / aluminium casing with chemically resistant two-component coating of the plastic pieces

Dimensions w = 1,300 mm, h = 1,000 mm, d = 620 mm (~51“ x 43“ x 24“)

Weight dependent on the number of measuring positions

~70 kg

Connections Pneumatic connections screw-type connections for viscometer

Electric connections circular connectors with bayonet lock for measuring stand and TC viscometer

Viscometers up to 8 viscometers connected by individual control units

Temperature via serial interface RS232-C of suspended thermostat,

type: 1 pc. CT 72/4 or up to 2 pcs. CT 72/2

Interfaces control system using PC with 2 x RS232-C interfaces

Safety overfilling safety device of waste bottle and suction hose

Mains connection European built-in plug DIN 49 457 6 with fuse

Data transmission Interface internal bidirectional serial interface in accordance with EIA RS232-C (daisy chain concept)

Interface external via PC, bidirectional serial interface in accordance with EIA RS232-C

Power supply Mains voltage 230 V (AC) or 115 V (AC), 50 to 60 Hz (AC)

26

26

CT 72

CT 72 Thermostat Series –

Transparent Thermostats conforming to Standards

As their predecessor CT 52 the new transparent thermostats

CT 72/P, CT 72/2, CT 72/2-TT and CT 72/4 meet DIN 51 562

(part 1), ASTM D 445 and ISO 3105 standards.

The SI Analytics transparent thermostats are particularly

designed for the determination of the viscosity of newtonian

liquids in glass capillary viscometers. They may be adapted

for manual as well as for automatic measurements. The new

models offer the core features of the CT 52 series incorporat-

ing the new improved immersion thermostats.

CT 72/4

27

CT 72

Bright display shows ongoing process,

at any time.

Programmable set temperatures through inte-

grated clock with controller.

Display of the momentary and the set

temperature.

Increased safety from separate operation and

temperature safety sensors.

Over-temperature safety system

on front panel.

Automatic fuses on the back panel.

Output of data formats

via RS232 connection.

CT 72/2 and CT 72/4 can be used up to 150 °C.

High temperature version is standard.

Draining valve comes with

CT 72/2, CT 72/2-TT and

CT 72/4. Newimmersion

thermostatsAdvantages

baths

CT 72/2

28

28

CT 72

Transparent Thermostats conforming to Standards:

The CT 72 series

Technical data

Suitable temperature control liquids

Liquid Alcohol Water Paraffine oil Silicon oil

Temperature range – 40 °C to + 10 °C + 5 °C to +80 °C + 40 °C to +150 °C + 80 °C to +150 °C

CT 72/P CT 72/2-TT CT 72/2 CT 72/4

Working temperature + 10 °C to +60 °C – 40 °C to + 150 °C + 5 °C to +150 °C + 5 °C to + 150 °C

Measuring positions for AVS 2 2 2 4

Measuring positions TC 2 2 2 4

Measuring positions micro TC 2 2 2 4

Temperature stability according DIN 58 966 at 25 °C

± 0.01 K ± 0.01 K ± 0.01 K ± 0.01 K

Size (W x H x D in mm) 355 x 370 x 250 355 x 370 x 250 355 x 370 x 250 605 x 370 x 250

Filling volume 18 l 15 l 15 l 27 l

Material PMMA St. steel & glass St. steel & glass St. steel & glass

Weight (empty) ~5 kg ~14 kg ~13.5 kg ~28 kg

At applications within normal temperature range (+ 5 °C up to approx. + 40 °C) cooling will be necessary for maintaining temperature stability.

CT 72/PCT 72/4

CT 72/2CK 310

29

CT 72

Ordering information






CT 72/2 - M, 230V 285418584 Immersion thermostat 230 V and thermostatic bath (stainless steel container with one manual gauge slide), equipped with two magnetic stirrer positions. Basic configuration for the attachment of one flow-through cooler.

CT 72/2 - M, 115V 285418593 Immersion thermostat 115 V and thermostatic bath (stainless steel container with one manual gauge slide), equipped with two magnetic stirrer positions. Basic configuration for the attachment of one flow-through cooler.

CT 72/2 - TT, 230V 285418615 Immersion thermostat 230 V and thermostatic bath (stainless steel container with one manual gauge slide), basic configuration for the attachment of one flow-through cooler.

CT 72/2 - TT, 115V 285418607 Immersion thermostat 115 V and thermostatic bath (stainless steel container with one manual gauge slide), basic configuration for the attachment of one flow-through cooler.



CT 72/E, 230V 285418501 Immersion thermostat 230 V/50 Hz

CT 72/E, 115V 285418495 Immersion thermostat 115 V/60 Hz

More Accessories and spare parts

CK 300, 230V 285414348 Flow through cooler, 230 V

CK 300, 115V 285414331 Flow through cooler, 115 V

CK 310, 230V 285414320 Flow through cooler, 230 V, stainless steel version

CK 310, 115V 285414310 Flow through cooler, 115 V, stainless steel version

VZ 5210 1007628 CT 72 retrofit set for CT 62-thermostatic bath, contains: Immersion thermostat CT72/E-230 V, adapter plate and cooling devices

VZ 5213 285420397 CT 72 retrofit set for CT 62-thermostatic bath, contains: Immersion thermostat CT72/E-115 V, adapter plate and cooling devices

VZ 5402 285415171 Manual gauge slide for transparent thermostats

VZ 5403 285420684 3-fold manual gauge slide for transparent thermostats

VZ 5404 285418573 Dust protection cover for transparent thermostat

VZ 5405 285418620 Transparent thermostatic bath backlight

VZ 7100 285421051 Control thermometer measuring range + 19 to + 21 °C

VZ 7101 285421068 Control thermometer measuring range + 24 to + 26 °C

VZ 7102 285421076 Control thermometers measuring range + 29 to + 31 °C




30

Ubbelohde

Viscometers and their range of use

Viscometer type

Measurement substance property

Transparent liquids manual measurement

++ ++ - + + + o

Transparent liquids automatic measurement

++ ++ + - + + -

Opaque liquids manual measurement

- - - - - - +

Opaque liquids automatic measurement

- - ++1) - - - -

Foaming liquids o o o + + + o

Liquid mixture with highly volatile components

o o o + + + o

Minimum measurement substance and/or rinsing agent quantities

- ++ - - + - -

High-temperature or low- temperature measurements

+ + + o o o o

Selection of glass capillary viscometers ++ use preferably 1) up to 30,000 mm²/s + highly suitable 2) above 30,000 mm²/s o less suitable - unsuitable

Ubbelohde

Micr

o Ubbelo

hde

TC Ubbelo

hde

Ostw

ald

Micr

o Ostw

ald

Cannon-Fensk

e-Routin

e

Cannon-Fe

nske re

verse

flow

31

Ubbelohde

Ubbelohde viscometers, normal form (DIN)

Viscometers with suspended level for

determination of absolute and relative

kinematic viscosity of liquids with Newto-

nian flow behavior. The calibrated viscom-

eters are delivered with manufacturer’s

certificate in accordance with DIN 55 350,

Part 18. All viscometers are provided

with ring marks. This ensures that vis-

cometers for automatic measurements

can also be checked by means of man-

ual measurements. The recommended

minimum flowthrough time is 200s for

absolute measurements of kinematic

viscosity. For relative measurements

(polymer analytics), the minimum flow

time of 50s is allowed by ISO 1628-1

(depending on the capillary size).

calibrated, with constant, for manual measurements

calibrated with constant, for manual measurements; automatic measurement with stand AVS®/SK-HV

ν = K · tK = ν

t

t = ν K

Type No.

Order No.

Type No.

Order No.

Capillary No. acc. DIN

Capillary Ø i ± 0,01 [mm]

Constant K (approx.)

Measuring range [mm²/s] (approx.)

501 00 285400004 – – 0 0.36 0.001 0.3 to 1501 03 285400012 – – 0c 0.47 0.003 0.5 to 3501 01 285400029 – – 0a 0.53 0.005 0.8 to 5501 10 285400037 – – I 0.63 0.01 1.2 to 10501 13 285400045 – – Ic 0.84 0.03 3 to 30501 11 285400053 – – la 0.95 0.05 5 to 50501 20 285400061 – – II 1.13 0.1 10 to 100501 23 285400078 – – IIc 1.50 0.3 30 to 300501 21 285400086 – – lla 1.69 0.5 50 to 500501 30 285400094 – – III 2.01 1 100 to 1,000501 33 285400107 – – IIIc 2.65 3 300 to 3,000501 31 285400115 – – IIla 3.00 5 500 to 5,000501 40 285400123 – – IV 3.60 10 1,000 to 10,000– – 502 43 285400131 IVc 4.70 30 3,000 to 30,000– – 502 41 285400148 IVa 5.34 50 6,000 to 30,000– – 502 50 285400156 - 6.30 100 > 10,000

not calibrated, without constant; for determination of relative viscosity

calibrated, with constant for automatic measurements

ν = K · tK = ν

t

t = ν K

ν = kinematic viscosity in mm²/sK = constant [mm²/s]t = flow-through time in s

Type No.

Order No.

Type No.

Order No.

Capillary No. acc. DIN

Capillary Ø i ± 0,01 [mm]



– – 532 00 285400164 0 0.36 0.001 0.3 to 1530 03 285400304 532 03 285400201 0c 0.47 0.003 0.5 to 3530 01 285400312 532 01 285400218 0a 0.53 0.005 0.8 to 5530 10 285400329 532 10 285400226 I 0.63 0.01 1.2 to 10530 13 285400337 532 13 285400234 Ic 0.84 0.03 3 to 30– – 532 11 285400172 la 0.95 0.05 5 to 50530 20 285400345 532 20 285400242 II 1.13 0.1 10 to 100530 23 285400353 532 23 285400259 IIc 1.50 0.3 30 to 300– – 532 21 285400189 lla 1.69 0.5 50 to 500530 30 285400361 532 30 285400267 III 2.01 1 100 to 1,000530 33 285400378 532 33 285400275 IIIc 2.65 3 300 to 3,000– – 532 31 285400197 IIla 3.00 5 500 to 5,000530 40 285400386 532 40 285400283 IV 3.60 10 1,000 to 10,000

Ubbelohde-Viskosimeter (DIN)

- in accordance with DIN 51 562 Part 1, ISO/DIS 3105 (BS-IP-SL)- filling quantity: 15 to 20 ml- overall length: approx. 290 mm

32

Ubbelohde

Ubbelohde viscometers, normal form (ASTM)

calibrated, with constant for manual measurements

not calibrated, without constant for determination of relative Viscosity


Type No. Order No. Type No. Order No. Type No. Order No. Capillary No.Capillary Ø i ± 0,01 [mm]



525 00 285400501 526 00 285400707 527 00 285401255 0 0.24 0.001 0.35 to 1

525 03 285400518 526 03 285400715 527 03 285401271 0c 0.36 0.003 0.6 to 3

525 01 285400526 526 01 285400723 527 01 285401263 0b 0.46 0.005 1 to 5

525 10 285400534 526 10 285400731 527 10 285401152 I 0.58 0.01 2 to 10

525 13 285400542 526 13 285400748 527 13 285401169 Ic 0.78 0.03 6 to 30

525 20 285400559 526 20 285400756 527 20 285401177 II 1.03 0.1 20 to 100

525 23 285400567 526 23 285400764 527 23 285401185 IIc 1.36 0.3 60 to 300

525 30 285400575 526 30 285400772 527 30 285401193 III 1.83 1 200 to 1,000

525 33 285400583 526 33 285400789 527 33 285401288 IIIc 2.43 3 600 to 3,000

525 40 285400591 526 40 285400797 527 40 285401296 IV 3.27 10 2,000 to 10,000

525 43 285400604 526 43 285400801 527 43 285401309 IVc 4.32 30 6,000 to 30,000

Ubbelohde Viscometer (ASTM)

• in accordance with ISO 3105, ASTM D 2515, ASTM D 446• filling quantity: 15 to 20 ml• overall length: approx. 285 mm

33

Ubbelohde

Ubbelohde viscometers,

with additional tube and threads


determination of absolute or relative

kinematic viscosity. These viscometers

are preferably used for automatic

measurements. The additional filling

and cleaning tube and the glass

thread ensure safe operational use.

The calibrated viscometers are deliv-

ered with manufacturer’s certificate in

accordance with DIN 55 350, Part 18.

The ring marks present serve as auxil-

iary marks in case the viscometers

must be checked by manual measure-

ments.


Type No. Order No. Capillary No.Capillary Ø i [mm]



541 03 285401925 0c 0.47 0.003 0.5 to 3541 01 285401917 0a 0.53 0.005 0.8 to 5541 10 285401933 I 0.63 0.01 1.2 to 10541 13 285401941 Ic 0.84 0.03 3 to 30541 11 285401950 Ia 0.95 0.05 5 ... 50541 20 285401958 II 1.13 0.1 10 to 100541 23 285401966 IIc 1.50 0.3 30 to 300541 21 285408719 IIa 1,69 0,5 50 ... 500541 30 285401974 III 2.01 1 100 to 1,000541 33 285401982 IIIc 2.65 3 300 to 3,000541 40 285401999 IV 3.60 10 1,000 to 6,000


Type No. Order No.Capillary No. acc. DIN

Capillary Ø i [mm]



545 00 285402005 0 0.24 0.001 0.35 to 1545 03 285402021 0c 0.36 0.003 0.6 to 3545 01 285402013 0b 0.46 0.005 1 to 5545 10 285402038 I 0.58 0.01 2 to 10545 13 285402046 Ic 0.78 0.03 6 to 30545 20 285402054 II 1.03 0.1 20 to 100545 23 285402062 IIc 1.36 0.3 60 to 300545 30 285402079 III 1.83 1 200 to 1,000545 33 285402087 IIIc 2.43 3 600 to 3,000545 40 285402095 IV 3.27 10 2,000 to 10,000545 43 285402108 IVc 4.32 30 6,000 to 30,000

Ubbelohde viscometer (DIN)

• in accordance with ISO 3105, DIN 51 562, Part 1, BS 133, NFT 60-100• filling quantity: 18 to 22 ml• overall length: approx. 290 mm

Ubbelohde viscometer (ASTM)

• the technical measurement characteristics are in accordance with ISO 3105, ASTM D 2515, ASTM D 446

• filling quantity: 15 to 22 ml• overall length: approx. 290 mm

34

Micro- Ubbelohde

Micro-Ubbelohde viscometers

Viscometers for dilution viscometry


determination of absolute and relative

kinematic viscosity of liquids with

Newtonian flow behavior. Due to their

design, these viscometers are espe-

cially suitable for measurement of

small liquid quantities and for particu-

larly short running times. All viscome-

ters are provided with ring marks. This

ensures that viscometers for automatic

measurements can also be checked

by means of manual measurements.

Micro-Ubbelohde viscometers (DIN)

The calibrated viscometers are deliv-

ered with manufacturer’s certificate in

accordance with DIN 55 350, Part 18.

For measurements with automatic vis-

cosity measuring instruments, another

constant is valid. This constant is deter-

mined by multiplication of the con-

stant K with the correction factor F.

• in accordance with DIN 51562, Part 2

• filling quantity: 3 to 4 ml

• overall length: approx. 290 mm

Viscometers for dilution viscometry

Viscometers with suspended level

designed according to the principle of

the Ubbelohde viscometers for

determination of the limit viscosity

number of polymers. The limit viscos-

ity number can be determined auto-

matically in combination with one of

our piston burettes TITRONIC® 300 or

TITRONIC® 500.

• filling quantity: 15 to 75 ml


calibrated, with constant for manual measurement

calibrated, with constant for automatic measurement


Type No. Order No. Type No. Order No. Type No. Order No. Capillary No.Capillary Ø i [mm]



536 10 285401009 537 10 285401103 538 10 285401206 M I 0.40 0.01 0.4 to 6536 13 285401017 537 13 285401111 538 13 285401214 M Ic 0.53 0.03 1.2 to 18536 20 285401025 537 20 285401128 538 20 285401222 M II 0.70 0.1 4 to 60536 23 285401033 537 23 285401136 538 23 285401239 M llc 0.95 0.3 12 to 180536 30 285401041 537 30 285401144 538 30 285401247 M lll 1.26 1 40 to 800

calibrated, for automatic measurements, Model with glass filter on request

Type No.

Order No.

Capillary No.

Capillary Ø i [mm]



531 00 285401403 0 0.36 0.001 0.35 to 0.6531 03 285401428 0c 0.47 0.003 0.5 to 2531 01 285401411 0a 0.53 0.005 0.8 to 3531 10 285401436 I 0.64 0.01 1.2 to 6531 13 285401444 Ic 0.84 0.03 3 to 20531 20 285401452 II 1.15 0.1 10 to 60

35

Cannon- Fenske

Cannon-Fenske viscometers

Cannon-Fenske routine viscometers

comply with standards ISO 3105,

ASTM D 2515, BS 188 with respect to

technical measuring specifications.

• are suitable for all Newtonian

liquids with a viscosity of 0.35 to

20,000 mm²/s

• the present design has a deepen-

ing in the lower bend. Accord-

ingly, these viscometers can also

be used for automatic measure-

ments.

• filling quantity: approx. 7 to 10 ml


Cannon-Fenske reverse flow

viscometers

• Comply with standards ISO 3105,

ASTMD 2515, ASTM D 446, NF T

60 - 100 with respect to technical

measuring specifications.

• filling quantity: approx. 12 ml


calibrated, with ring mark, for manual measurements

with constant for automatic measurements

Type No. Order No. Type No. Order No. Capillary No.Capillary Ø i [mm]



513 00 285403507 520 00 285403704 25 0.30 0.002 0.4 to 1.6513 03 285403515 520 03 285403712 50 0.44 0.004 0.8 to 3.2513 01 285403523 520 01 285403729 75 0.54 0.008 1.6 to 6.4513 10 285403531 520 10 285403737 100 0.63 0.015 3 to 15513 13 285403548 520 13 285403745 150 0.78 0.035 7 to 35513 20 285403556 520 20 285403753 200 1.01 0.1 20 to 100513 23 285403564 520 23 285403761 300 1.27 0.25 50 to 200513 21 285403572 520 21 285403778 350 1.52 0.5 100 to 500513 30 285403589 520 30 285403786 400 1.92 1.2 240 to 1,200513 33 285403597 520 33 285403794 450 2.35 2.5 500 to 2,500513 40 285403601 520 40 285403807 500 3.20 8 1,600 to 8,000513 43 285403618 520 43 285403815 600 4.20 20 4,000 to 20,000

calibrated, with 3 ring marks, with 2 constants, only for manual measurement

Type No.

Order No.

Capillary No.

Capillary Ø i [mm]



511 00 285403001 25 0,31 0.002 0.4 to 1.6511 03 285403018 50 0,42 0.004 0.8 to 3.2511 01 285403026 75 0,54 0.008 1.6 to 6.4511 10 285403034 100 0,63 0.015 3 to 15511 13 285403042 150 0,78 0.035 7 to 35511 20 285403059 200 1,02 0.1 20 to 100511 23 285403067 300 1,26 0.25 50 to 200511 21 285403075 350 1,48 0.5 100 to 500511 30 285403083 400 1,88 1.2 240 to 1,200511 33 285403091 450 2,20 2.5 500 to 2,500511 40 285403104 500 3,10 8 1,600 to 8,000511 43 285403112 600 4,00 20 4,000 to 20,000

36

Cannon- Fenske

Cannon-Fenske routine viscometers

with additional tube and threads

comply with standards ISO 3105, ASTM

D 2515, BS 188 with respect to technical

measuring specifications. These viscom-

eters are preferably used for automatic

measurements. The additional filling

and cleaning tube and the glass thread

ensure safe operational use. The cali-

brated viscometers are delivered with

manufacturer’s certificate in accor-

dance with DIN 55 350, Part 18.

• are suitable for all Newtonian

liquids with a viscosity

of 0.35 to 20,000 mm²/s.

• filling quantity: approx. 7 to 12 ml


calibrated, with ring marks, with constant for automatic measurements

Type No.

Order No.

Capillary No.

Capillary Ø i [mm]



546 00 285402116 25 0.30 0.002 0.4 to 1.6

546 03 285402132 50 0.44 0.004 0.8 to 3.2

546 01 285402124 75 0.54 0.008 1.6 to 6.4

546 10 285402149 100 0.63 0.015 3 to 15

546 13 285402157 150 0.78 0.035 7 to 35

546 20 285402165 200 1.01 0.1 20 to 100

546 23 285402181 300 1.27 0.25 50 to 200

546 21 285402173 350 1.52 0.5 100 to 500

546 30 285402198 400 1.92 1.2 240 to 1,200

546 33 285402202 450 2.35 2.5 500 to 2,500

546 40 285402219 500 3.20 8 1,600 to 8,000

546 43 285402227 600 4.20 20 4,000 to 20,000

37

Ostwald

Ostwald viscometers

Ostwald viscometers

• filling quantity: 3 ml


with ring marks, without constant, for manual measurements

Type No. Order No.Capillary Ø i [mm]

Transit time for water ~ [s]


for use from [mm²/s] (approx.)

509 03 285404006 0.3 250 0.004 0.3

509 04 285404014 0.4 75 0.01 1

509 05 285404022 0.5 30 0.03 2.5

509 06 285404039 0.6 15 0.07 5.5

509 07 285404047 0.7 10 0.1 10

Micro-Ostwald viscometers

• are suitable for measurements of

small liquid quantities even with

excessive foam formation.

• filling quantity: 2 ml


calibrated, with ring marks, with constant, for manual measurements

calibrated, with ring marks, with constant, for automatic measurements


Type No. Order No. Type No. Order No. Typ-Nr. Bestell-Nr. Capillary No.Capillary Ø i [mm]



516 10 285404203 517 10 285404306 518 10 285404409 I 0.43 0.01 0.4 to 6

516 13 285404211 517 13 285404314 518 13 285404417 Ic 0.60 0.03 1.2 to 18

516 20 285404228 517 20 285404322 518 20 285404425 II 0.77 0.1 4 to 60

516 23 285404236 517 23 285404339 518 23 285404433 IIc 1.00 0.3 12 to 180

516 30 285404244 517 30 285404347 518 30 285404441 III 1.36 1 40 to 800

38

Ostwald

Accessories

Brackets and stands

All brackets and stands are designed

to ensure that the viscometers are

held vertically. They also protect the

viscometers from breakage. The maxi-

mum deviation is < 1°. In conjunction

with SI Analytics and other commer-

cially available seethrough thermo-

stats the viscometers can only be used

with the appropriate stand or bracket.

For DIN Ubbelohde viscometers that

are used as reference measuring stan-

dard, specifically modified bracket (VZ

5840) must be used.

Type No. Order No.

053 92 285405043

VZ 5840 (accessory for reference measuring standard) 285417201

Brackets made of stainless steel

suitable for use with all Ubbelohde viscometers

for manual and automatic measurements

Type No. Order No.

053 93 285405035

suitable for use with Ubbelohde viscometers with TC sensors

Type No. Order No.

053 96 285405019

suitable for use with all reverse flow viscometers

(Cannon-Fenske and BS/IP U-tube viscometers) for manual and

automatic measurements (not illustrated)

Type No. Order No.

053 97 285405027

suitable for use with Micro-Ostwald viscometers

for manual and automatic measurements

39

Accessories

Accessories

Brackets for reference measuring

standard

DIN Ubbelohde viscometers which

are used as testing standard should be

stored in a specially modified viscom-

eter bracket according to official

inspection / calibration authorities.

The extension set for the test standard

(VZ 5840) as supplement to the

bracket guarantees vertical slope with

a maximum deviation of < 1° and the

centered positioning of the capillaries.

Type No. Order No.

VZ 5840 285417201

Type No. Order No. Measuring range °C Graduation °C

VZ 2801 285415763 – 5 to + 38 1/10

VZ 2802 285415771 + 33 to + 67 1/10

VZ 2803 285415788 + 66 to + 102 1/10

VZ 2804 285415796 + 95 to + 152 1/10

VZ 2901 285415809 + 20 to + 25 1/100

VZ 2907 285417078 + 22 to + 27 1/100

VZ 2908 285415825 + 37 to + 42 1/100

VZ 2905 285415841 + 45 to + 50 1/100

VZ 2906 285415858 + 97 to + 101 1/100

VZ 2909 285417094 + 132 to + 137 1/100

Control thermometers

Type No. Order No. Measuring range °C Graduation °C

VZ 7100 285421051 + 19 to + 21 1/100

VZ 7101 285421068 + 24 to + 26 1/100

VZ 7102 285421076 + 29 to + 31 1/100

VZ 7103 285421084 + 39 to + 41 1/100

VZ 7104 285421092 + 99 to + 101 1/100

VZ 7105 285421105 + 134 to + 136 1/100

Control thermometers for CT 72 thermostat series

40

Accessories

Accessories

LabPump

The LabPump VZ 5655 (not illustrated)

used with manual and semi-automatic

measurements to extract and pump

solutions:

• filling of viscometers

• rinsing with the next sample

• extract between manual

measurements

• emptying of viscometers without

removing them from the

thermostatic bath

Since the LabPump VZ 5655 and the

connections are made of PTFE or

stainless steel, the pump is suitable for

use with aggressive mediums.

The range of use for semi-automatic

processing of samples, e.g. with a vis-

cosity measuring instrument AVS®

360, AVS® 370 or AVS® 470, is possi-

ble up to a viscosity of 30,000 mm²/s.

For semi-automatic processing work,

the PTFE tube combination with stand

(see illus-tration) and the waste bottle,

type no. VZ 5624, are used.

Type No. Order No.

VZ 5655 1040755

Type No. Order No.

064 99 285405105

Polyamide bracket

for use with Cannon-Fenske routine viscometers,

Cannon-Fenske reverse flow viscometers and all Ostwald viscometers

for manual measurements only

Type No. Order No.

065 99 285405113

PTFE bracket

for use with Cannon-Fenske routine viscometers,

for automatic measurements only (not illustrated)

41

Accessories

Accessories

Temperature stabilization jackets

In the absence of a see-through ther-

mostat the temperature of capillary

viscometers can be stabilized in this

type of jacket using circulation ther-

mostats in the temperature range 0 to

180 °C. The shape of the jacket and

the number of holes in the support

plate depend upon the type of vis-

cometer being used. The support

plate has been designed to facilitate

changing the viscometer when

required. An additional hole is pro-

vided in the support plate so that a

control thermometer can be fitted. A

quick-action seal simplifies changing

viscometers.

Type No. Order No. Item No. Comment

577 00 285405508 complete, without viscometer

Component parts

577 01 285405516 1 temperature stabilization jacket, straight

238 00 285405524 2 support plate with 4 silicone rings (d = 4, 6, 8 and 10 mm)

225 34 285405532 3 silicone O-ring, ND 60

072 34 285405549 4 quick-action seal, NW 60

Temperature stabilization jacket with support plate

for Ubbelohde viscometers

Type No. Order No. d mm D mm h mm

228 11 285405808 4 10 5

228 14 285405816 6 16 5

228 16 285405824 8 16 5

228 17 285405832 10 16 5

Silicone rings

42

measuring stands

AVS® measuring stands

AVS® measuring stands

Measuring stands of the series AVS®/S

can be used to measure the flow-

through time in viscometers automati-

cally.

The measuring stands can be con-

nected to all measuring instruments

made by SI Analytics for automatic mea-

surement of viscosity and operate with

all standard viscometers for repetitive

measurements.

Automatic measurements have the fol-

lowing advantages:

• the repetitive standard deviation is

less than for manual measurements

• the measurement is free from

subjec-tive factors of influence

• the results can be printed and/or be

automatically documented with a

data memory system

• automatic processing of sample

series is available.

The use of different materials ensures

adaptation to existing measurement

temperatures and applications.

The measuring stands or brackets can

be exchanged.

The distance between the levels of the

automatic optoelectronic unloading

system is 40.00 mm ± 0.03 mm. This

results in a standard deviation of

VK = 0.05 % for Ubbelohde viscometers

if the measuring stand is replaced or

changed within the process.

For repetitive measurements with vis-

cosity measuring instruments and

Ubbelohde viscometers with measur-

ing stands, the standard deviation

VK = 0.03 %.

Manually calibrated Ubbelohde visco-

meters can also be used in AVS® mea-

suring stands. If the automatic sensing

levels do not correspond to the ring

marks, the superimposed meniscus

detection system will provide a higher

constant. The difference amounts to

0.1 % per millimeter of height offset.

43

measuring stands

Measuring stands

AVS®/S AVS®/S-HT AVS®/SK AVS®/S-CF AVS®/SK-V

Available viscometers

Ubbelohde viscometers in accordance with DIN, ASTM, ISO 3105, Micro-Ubbelohde viscometers,

Micro-Ostwald viscometers

Cannon-Fenske- routine

viscometer

Ubbelohde- dilution

viscometer

Temperature range

– 80 to + 100 °C – 80 to + 200 °C 0 to + 60 °C – 80 to + 100 °C 0 to + 60 °Cother

temperature ranges available

on request

Suitable brackets (type no.)

05392 05397

no bracket required

Material Aluminium, TiO2-anodized PVDF, stainless steel

Aluminium, TiO2-anodized

PVDF, stainless steel

Dimensions (W x H x D) mm

90 x 447 x 90 90 x 496 x 90 90 x 447 x 90 90 x 447 x 90 90 x 447 x 90

Weight (kg) appr.

1.0 1.25 0.8 1.0 0.8

Accessories included in scope of delivery

Bracket Type No. 05392 for Ubbelohde viscometers, tube/cable combination VZ 5505

tube/cable combination

VZ 5505

tube/cable combination

VZ 5857, magnetic stirring

rods, fastening springs

for viscometer

Note: When TC viscometers are being used, a bracket type no. 05393, with the necessary tube set is required only. A measuring stand is not required.

Suitable for use with the measuring units: AVS® 350, AVS® 360, AVS® 370,

AVS® 450, AVS® 470, AVS®Pro

Suitable for use with the thermostatic baths: CT 72/P, CT 72/2-TT, CT 72/2, CT 72/4

Electrical connection: Cable VZ 6225 for all measuring stands to all instruments (is

included in hose sets VZ 5505, VZ 5622 and VZ 5857), con-

trol lamp as function display

Distance between measuring levels: 40.00 mm ± 0.03 mm at 25 °C

Signal transmission: Optically using optical fibres from the measuring level in the

stand head, converted into analogue signal from stand to

measuring instrument

44

Manual Titration

It is true that the automatic titration is gaining ground, but manual titration remains one of the standard cost effective applications in the lab, whereever high precision and flexibility are required.

Titration with hand controller (mouse).

Titration rate can be adjusted in five different steps to optimize the titration speed and accuracy.

Automatic calculation of results in different units and exportation to a printer or USB memory device.

Automatic weight recording when a balance is connected.

TITRONIC® 300 - the new piston burette from SI Analytics Titrating manually, perfectly dosing

Dosing

Beside the titration there are various routine dosing tasks that must be performed in the lab. A piston burette is the ideal device for precise dosing tasks:

Adjustable dosing and filling rate for each method.

Adjustable filling between each dose step.

The intelligent filling function checks if a dosing step is feasible without filling in advance. This reduces faulty operations during a serial dosing process.

The TITRONIC® 300 is a perfect motor-driven burette for manual titration and and precise dosing instrument for dispensable liquids, solvents and titrating agents. However, the TITRONIC® 300 is not only first-rate as a stand-alone instrument, it also thrives as the heart of a computer-controlled dosing or titrating system.

76

45

Manual Titration

It is true that the automatic titration is gaining ground, but manual titration remains one of the standard cost effective applications in the lab, whereever high precision and flexibility are required.

Titration with hand controller (mouse).

Titration rate can be adjusted in five different steps to optimize the titration speed and accuracy.

Automatic calculation of results in different units and exportation to a printer or USB memory device.

Automatic weight recording when a balance is connected.

TITRONIC® 300 - the new piston burette from SI Analytics Titrating manually, perfectly dosing

Dosing

Beside the titration there are various routine dosing tasks that must be performed in the lab. A piston burette is the ideal device for precise dosing tasks:

Adjustable dosing and filling rate for each method.

Adjustable filling between each dose step.

The intelligent filling function checks if a dosing step is feasible without filling in advance. This reduces faulty operations during a serial dosing process.

The TITRONIC® 300 is a perfect motor-driven burette for manual titration and and precise dosing instrument for dispensable liquids, solvents and titrating agents. However, the TITRONIC® 300 is not only first-rate as a stand-alone instrument, it also thrives as the heart of a computer-controlled dosing or titrating system.

76

46

10

Simple and accurate dosing with the new TITRONIC® 500

piston burette

The TITRONIC® 500 is the ideal piston burette for manual

titrations, accurate dosing applications as well as the prepa-

ration of solutions. When used with TitriSoft 3.0, it acts as a

titration burette or with the TitroLine®7000 and TitriSoft 3.0,

it is an automatic dosing unit perfect to pre-dose a titrant.

Important features:

Intelligent interchangeable modules with 5, 10, 20

and 50 ml volume capacity.

Connect to a printer and/or an analytical balance.

Remote control access via RS232 or USB interface.

Connect up to 16 devices using the two RS232 ports.

The first burette is connected to one PC RS232 or

USB port.

47

11

Dosing, preparing solutions and performing manual titrations

Manual Titration

It is true that the automatic titration is gaining ground, but

manual titration remains one of the standard cost effective

applications in the lab. Everywhere high precision and flexi-

bility are required; a piston burette with an interchangeable

dosing module is the best choice.

Important features:

• Titration using the manual controller dosing buttons.

• Titration rate can be adjusted to optimize titration

speed and accuracy.

• Programmable automatic calculations, printer ready.

• Automatic weight recording when balance is con-

nected.

Dosing

Besides titration, there are various routine dosing tasks that

must be performed in the lab.

Important features:

• Control dosing using the manual controller and the

dedicated keypad.

• Adjustable dosing and filling rates optimize speed and

accuracy.

• Store dosing methods with different parameters.

Solutions preparation

A special sample preparation mode is available on the

TITRONIC® 500 where a reagent is dosed into a sample until

the required concentration is reached. The sample is

weighed, the dosing volume is determined. The volume can

then be automatically added to the sample.

Important features:

• Adjustable dosing and filling speed.

• Dosing volume is automatically calculated without

additional PC software.

• Automatic weight recording when balance is con-

nected.

48

CANNONINSTRUMENT COMPANY

®

PolyVISC® Automatic Viscometer

Instruments forAutomatedViscosityDetermination

49

Instruments for Automated Viscosity

CANNON® PolyVISC® Automatic Viscometer

� Automatic glass capillary polymer viscosityanalysis between 0.3 to 20,000 cSt*

� Compatible with most solvents usedfor polymer work

� Unique AIRBATH® technology – ultrastablethermostatic air chamber

� Temperatures from 20 to 100°C(135°C with High Temperature Option)

� VISCPRO® Windows® software calculates relativeviscosity, inherent viscosity, reduced viscosity, andintrinsic viscosity

� May also be used for other viscosity applications* Special viscosity ranges available upon request

Features:The CANNON® PolyVISC® Automatic Glass CapillaryViscometer combines automatic sampling, viscositymeasurement, viscometer washing, and polymer solventcompatibility to provide a convenient benchtop unit ideal fordilute solution polymer viscosity analysis. Both transparent andopaque samples can be measured with the accuracy requiredby ASTM D 2857. Infrared optical sensors are used for alltransparent samples and some opaque samples. Thermalsensors are available upon request for heavily opaquesamples.

The PolyVISC Viscometer utilizes a unique “air bath”technology to maintain excellent temperature control. Analysesare made in an ultra-stable thermostatic air chamber (theAIRBATH® Chamber). The AIRBATH Chamber consists of anouter insulated chamber enclosing a second, inner chamber,where the viscometer and sample are continuously bathed in athermally stabilized stream of air. Temperature is controlledwithin 0.01°C with advanced measuring electronics,thermoelectric cooling, and controlling software. Because boththe sample carousel and the viscometer are completelycontained in the AIRBATH Chamber, only the first samplerequires a delay for thermal equilibrium. The AIRBATHChamber also allows rapid temperature and viscometerchanges. Built-in thermoelectric cooling enables testing below40°C without the need for an external chiller.

Overview of Automatic SampleLoading and AnalysisSamples are placed in disposable vials which are then loadedinto a carousel and inserted into the AIRBATH for analysis. Thecarousel accepts eleven vials, each containing 10 to 15 mL ofsample. The extended-range viscometer used in the PolyVISCdevice is similar to that in the CANNON Automatic Viscometer(CAV). The viscometer contains a lower and an upper timingbulb. First the sample is pulled into the lower chamber of theviscometer. The time required to fill the lower bulb is measured.If the time is short, the sample is pulled into the upper bulb. Ifthe time is long, the lower bulb is used. A PolyVISC viscometercovers a range of approximately 100-fold viscosity range. Thismeans that a single size 1-100 PolyVISC viscometer cananalyze a range of samples that would require five manualviscometers. Viscometers can be easily changed in less than 60seconds without the inconvenience of messy bath liquids.

After each analysis is completed, the sample flows back intothe sample vial. Residual sample is cleaned from the inside,outside, and tip of the viscometer by automatic rinsing with awash solvent, followed by a drying solvent. The viscometer isthen dried. A typical wash requires only 10 to 20 mL ofwashing solvent and 10 mL of drying solvent. Wash parametersare adjustable by the user.

Software FeaturesThe operating system is designed to be user friendly. PowerfulVISCPRO® software for Windows automatically calculatesrelative, inherent, reduced, and two types of intrinsic viscosity(limiting viscosity number), Solomon-Ciuta and Billmeyerrelationships, and the K-value relationship after Fickentscher. Inaddition, it provides flexible and sophisticated control anddatabase management features. Data can be printed,displayed on the computer screen, or automatically routed toan existing LIMS data-processing network. Data storage is in aMicrosoft® Access database.

Solvent Compatibility*The PolyVISC Viscometer is compatible with most solventscommonly used for the dilute solution viscosity determinationof polymers. Polymer solutions routinely analyzed in thestandard PolyVISC Viscometer include polyacrylonitrile in DMF,nylon in formic acid, nylon in sulfuric acid, polyester in HFIP,polyester in phenol-TCE, epoxy resins in methanol, vinyl resinsin MIBK, cellulose acetate in acetone and methylene chloride,and polycarbonate in methylene chloride, and others. We willbe happy to answer any questions concerning the compatibilityof the PolyVISC Viscometer with other solvents.

CANNON INSTRUMENT COMPANY • 2139 HIGH TECH ROAD • STATE COLLEGE • PA • 16803-1733 • USA

800-676-6232 • 814-353-8000 • Fax 814-353-8007 • [email protected] • www.cannoninstrument.com2

CANNON PolyVISC® Automatic Viscometer

ASTM D 2857/D 1628/D 4603 (PET), ASTM D 789, ISO 307 (Nylon), ASTM D 1243/D 3591,D 4603 (PVC), ASTM D 871/D 1795 (Cellulose), ASTM D 1601 (Ethylene Polymers)

50

PVDF/PTFE component upgradesA PVDF coating upgrade is available for the PolyVISCinstrument. The AIRBATH Chamber interior is coatedwith this durable polyvinylidene fluoride (PVDF)compound. The upgrade permits testing with highlyaggressive solvents, including concentrated sulfuricacid. The PVDF coating upgrade also includes aPTFE wash platform and solid PTFE sample carrierand wash station.

PolyVISC Volatile Sample TestingOptionProvides protection from solvent evaporation. Thetopless plastic screw cap for standard PolyVISCsample vials can be modified by the addition of ascored film and rubber seat.

In conjuction with an aluminum foil seal, the rubberinserts enhance test precision for

highly volatile samples by preventing evaporation that canaffect the concentration of the polymer solution. The designalso helps to reduce toxic and/or corrosive vapors in theAIRBATH® by resealing the cap aperture following the test,and the rubber inserts wipe the exterior of the viscometertube as it is withdrawn from the vial, further reducing the riskof cross-contamination when performing multiple sampletests.

The solvent-resistant rubber inserts are sold in packages ofone dozen each, and can be re-used multiple times withappropriate cleaning and drying procedures.

PolyVISC viscometer tubesTwo tube types are available for the PolyVISC instrument.The modified Atlantic compound viscometer tube is suitablefor most samples. The modified Ubbelohde tube isparticularly suited for more volatile samples, and maysignificantly enhance determinability and repeatability.Contact CANNON Technical Services for orderinformation.

Atlantic

Extended-Range ViscometersSize/Range (cSt)

0.14 – 14 16 – 1600

0.3 – 30 25 – 2500

0.5 – 50 75 – 7500

1 – 100 300 – 30000

3 – 300 600 – 60000

8 – 800

PVDF interiorwith PTFE carousel

CANNON INSTRUMENT COMPANY • 2139 HIGH TECH ROAD • STATE COLLEGE • PA • 16803-1733 • USA

800-676-6232 • 814-353-8000 • Fax 814-353-8007 • [email protected] • www.cannoninstrument.com

* Some solvents and solvent vapors may be corrosive to AIRBATHcomponents. The user is responsible for determining chemicalcompatibility with PolyVISC components. Contact CANNON forconsultation and special maintenance guidelines when using potentiallyincompatible chemicals.

Ubbelohde

PolyVISC Specifications

Dimensions: 515 mm wide x 756 mm high x 520 mm deep(20.3 x 29.8 x 20.5")

Viscosity Range: 0.3 to 20,000 cSt (special ranges available on request)

Solvent Volume: 10 mL for each wash and rinse (application dependent)

Temperature Range: 20 to 100°C(135°C High-Temperature Option available)

Temperature Stability: ± 0.01°C at calibrated temperature

Drop Time Resolution ± 0.01 second

Electrical: 115/230V, 50/60 Hz, 1750/1850 watts(please specify voltage when ordering)

Compliance: CE Mark; EMC directive (89/336/EEC); Low voltagedirective (73/2/EEC); HI-POT (1900 VDC, 60 sec.)

Computer Requirements

Please contact CANNON for Computer Specifications.

Order Information

Catalog # Item Description

9724-Z18 PolyVISC Automatic Viscosity MeasuringSystem 115V, 50/60 Hz, 1750 watts

9724-Z20 PolyVISC Automatic Viscosity MeasuringSystem 230V, 50/60 Hz, 1850 watts

P65.7500 PVDF/PTFE Component Upgrades

P65.3283 PolyVISC Volatile Sample Testing Option

PolyVISC Viscometer Tubes


CANNON® PolyVISC® Accessories & Options

ASTM D 2857

51

� Prepares polymer solutions for relative viscositymeasurements using weight-to-weight methodology

� Eliminates errors due to variations in solvent densityand cumbersome manual weight and volumemeasurements

� Provides concentration accuracy often better than±0.02%

The PolyVISC® SPS Solution Preparation System from CANNONInstrument Company is a semi-automated solution preparation systemthat uses gravimetric rather than volumetric methodology. The SPS canbe used with the CANNON PolyVISC® Automatic Viscometer toprovide a complete polymer analysis system.

Why Gravimetric Measurement?When manual volumetric methods of preparing solutions areemployed, variations of solvent density with temperature can lead toerrors larger than the error inherent in the subsequent analyticalprocedure. In the PolyVISC SPS Solution Preparation System, thesolvent is weighed rather than measured volumetrically, eliminatingerrors due to variations in solvent density. For samples over 100 mL,concentration accuracy is often better than ± 0.02 percent.

When solutions are prepared using the gravimetric method, thesolution concentration can be expressed in units of volume when thedensity of the solvent is known. Thus, it is possible for the PolyVISC SPSSolution Preparation System to prepare solutions for procedureswritten for the volumetric method.

PolyVISC® SPS componentsA computer-controlled burette pump and proprietary PolyVISC SPS software are at the heart of the Solvent Preparation System.The software permits convenient user configuration of multiple sample/solvent recipes. Other required system components(ordered separately) include a Windows-compatible computer and an electronic balance. A number of digital electronicbalances having an RS-232 (COM) output are compatible with the SPS software package.

Solution PreparationSPS software for Windows® makes solution preparation rapid and simple. No volumetric glassware is used. After the sample IDinformation is entered, and the user-configured recipe is selected, the operator places an empty container on the balance pan.The container is weighed and the operator adds the amount of solute specified by the computer to the sample container. Theprecise solute weight is obtained; then the computer calculates the appropriate amount of solvent and adds the solvent to thesample container on the balance. Solution concentration is calculated by the software, and all sample information is stored onthe computer hard disk drive. A sample label can be printed.

CANNON® PolyVISC® SPS Solution Preparation System

Specifications for the PolyVISC® SPS Solution Preparation SystemPump Module

Number of Pumps: One

Type of Pumps: Syringe

Flow Rate: 0 to 400 mL/min

Solution Types: Weight-to-Weight, Weight-to-Volume, Dilution-to-Volume

Solution PreparationAccuracy:

± 0.02% or better for samples over 100 mL

Solution Preparation Time: 2 minutes (50 mL of solvent)

Compatible Balances: Contact CANNON for updated list

Computer Operating System: Windows® 95/98/XP®/NT®

Order Information


9724-Z61 PolyVISC® SPS SolutionPreparation System, 115V,50/60HZ

9724-Z62 PolyVISC® SPS SolutionPreparation System, 230V,50/60HZ

CANNONINSTRUMENT COMPANY

®

2139 High Tech Road • State College • PA • 16803 • USA800 676 6232 • 814 353 8000 • Fax 814 353 8007e-mail: [email protected] • www.cannoninstrument.com

© 2009 CANNON Instrument Company


CANNON® PolyVISC® SPS Solution Preparation System

52

Accurate and Fast Analysis •

Supports Standard and • Proprietary Methods

Intuitive and Versatile Software•

Simple Operation•

Robust Performance•

Now Availablewith 10-place Auto-Sampler

53

Essential Automation for Polymer Solution ViscosityThe miniPV® from CANNON Instrument Company is an essential tool for the measurement of polymer solution viscosities. Its accuracy and convenience are based on the masterful design of temperature control, fluid handling, sensor technology, and automation. Complete control of the instrument is provided through VISCPRO II software (for Windows® 98/NT®/XP®) which also facilitates procedural tasks such as calibration, data entry, method specification, calculation selection, report formatting, and data exporting. All data is securely maintained by VISCPRO II in a Microsoft Access database.

The miniPV® occupies roughly the same footprint as an analytical balance, yet is able to provide a high level of automation which includes sample loading, temperature equilibration, flow time measurement, and cleaning of the entire system between measurements. Support for a sequence of samples is available with the optional autosampler.

VISCPRO II is unique in its ability to perform the Huggins-Kraemer determination of intrinsic viscosity in addition to single-point methods based on Billmeyer and on Solomon-Ciuta. Multiple viscosity calculations are also available, leading to relative, inherent, and reduced viscosity determinations. In addition, the software provides flexible and sophisticated control of data export options and database management.

OperationOperation of the miniPV® is simple. First, the sample vial is charged with about 15 mL of solution. Second, the sample vial is positioned in the vial holder beneath the viscometer. Third, the sample platform is raised to the viscometer. This action initiates the sample loading procedure and the subsequent series of automatic processes that were specified by the user in the VISCPRO II method parameters. In general, the sample is drawn into the viscometer tube, held until the temperature has equilibrated, and then released to drain during automatic timing of the flow rate. Data is transferred via the RS-232 serial connection to a host computer that stores and maintains the data in a MS Access® database. The sample is then ejected as waste and the sample vial becomes a wash station as solvent is automatically injected into the viscometer tube to initiate the cleaning cycle which can include a second solvent for a subsequent rinse and a final purge of compressed air. Following tube drying, the vial holder is returned to its original position, ready to receive the next sample.

Auto-SamplerThe user fills the sample vials and then places them into a numbered carousel beneath the viscometer. Carousel locations are numbered 1 to 10. Sample ID information is entered via the computer. The user initiates the test with a single mouse click.

CANNON® miniPV® and miniPV-X POLYMER SOLUTION Automatic Viscometers

INNOVATIONS IN VISCOSITY MEASUREMENT

Designed to Meet the Unique • Needs of Users in the Polymer Industry

Calculation of Relative, • Inherent, Reduced and Intrinsic Viscosity

0.3 to 5,000 centistokes range •

(special ranges available on • request)

Superb Temperature Control • from

20 to 100°C •

Accurate Flow Times ( to 0.01 • seconds)

miniPV® Automatic Viscometer Specifications

miniPV® Dimensions: 254 mm wide x 437 mm deep x 598 mm high (10 x 17.2 x 23.5”)

Power Supply Dimensions: 330 mm wide x 396 mm deep x 172 mm high (13 x 15.6 x 6.8”)

Weight: Bath Unit: 27 kg (45 lbs); Power Supply: 12 kg (26 lbs); Waste Receiver: 6 kg (13 lbs)

Shipping Weight: 72 kg (159 lbs) with all units/accessories

Fuse Rating: 115V & 100V Units: M 250V 8A, 1.25 x 0.25”; 230VUnit M 250V 4A, 1.25 x 0.25”

Compliance: CE Mark

Computer Requirements Computer not included, please contact Cannon for specifications.

2139 High Tech Road • State College • PA • 16803 800-676-6232 • 814-353-8000 • Fax 814-353-8007email: [email protected] • www.cannoninstrument.com

©2011 CANNON Instrument Company • Printed in USA

miniPV® Order Information


9725-A91 miniPV® 115V 50/60 hz

9725-A92 miniPV® 100V 50/60 hz

9725-A93 miniPV® 230V 50/60 hz

9725-C11 miniPV-X 115V 50/60 Hz

9725-C12 miniPV-X 230V 50/60 Hz

P61.5600 Dostmann Thermometer, Calibrated, Digital Dual Channel Kit

P61.5601 Standard Size Smart Probe

Thermistor Sensors•

Peltier Technology Cooling for • efficient operation near ambient temperatures

Powerful VISCPRO II® Software for • Control, Calculation and Database Management

Compatible with Most Solvents used • for Polymer Characterization

Applications: Solutions of • Elastomers, Plastics, TPEs, Copolymers, Bio-polymers, Blends, Oligomers, Pre-Polymers, Resins, Viscosity Modifiers, Pulp and Cellulose

For applications using potentially incompatible chemicals, pleae consult CANNON for special maintentance

miniPV® and miniPV-X Features

54

• Chemically Resistant to Solvent and Acid

• Accurate and Fast Unattended Analysis

• Minimize Operator Exposure

• Robust Performance

• Small Foot Print

• On-Board Diagnostics

55

Essential Automation for Polymer Solution ViscosityThe miniPV®-HX™from CANNON Instrument Company is an essential tool for the measurement of polymer solution viscosities. Its accuracy and convenience are based on the masterful design of temperature control, fluid handling, sensor technology, and automation. Complete control of the instrument is provided through VISCPRO II software (for Windows® 98/XP®/Vista®/Windows 7®) which also facilitates procedural tasks such as calibration, data entry, method specification, calculation selection, report formatting, and data exporting.

The miniPV®-HX™occupies roughly the same footprint as an analytical balance, yet is able to provide a high level of automation which includes sample loading, temperature equilibration, flow time measurement, and cleaning of the entire system between measurements. VISCPRO II® is unique in its ability to perform an automatic Huggins-Kraemer determination of intrinsic viscosity in addition to single-point methods based on Billmeyer and on Solomon-Ciuta. Multiple viscosity calculations are also available, leading to relative, inherent, and reduced viscosity determinations. In addition, the software provides flexible and sophisticated control of data export options and database management.

OperationSamples are prepared using optional Cannon Instrument SPS Sample Preparation System in reusable or disposable sample vial. The samples are inserted into the multiple position auto carousel. The user then selects start. This action initiates the sample loading procedure and the subsequent series of automatic processes that were specified by the user in the VISCPRO II® method parameters. In general, the sample is drawn into the viscometer tube, held until the temperature has equilibrated, and then released to drain during automatic timing of the flow rate. Data is transferred via the RS-232 serial connection to a host computer that stores and maintains the data in a database. The sample is then ejected as waste and the sample vial becomes a wash station as solvent is automatically injected into the viscometer tube to initiate the cleaning cycle. The user may select to run a second solvent for a subsequent rinse and a final purge of compressed air during the wash cycle. Following tube drying, the sample carousel advances to the next position and repeats the automation process.

miniPV®-HX Automatic Viscometer Specifications

miniPV®-HX Dimensions: 254 mm wide x 396 mm deep x 787.4 mm high (10 x 15.6 x 30.5”)

Power Supply Dimensions: 330 mm wide x 396 mm deep x 172 mm high (13 x 15.6 x 6.8”)

Weight: Bath Unit: 24 kg (53 lbs); Power Supply: 12 kg (26 lbs); Waste Receiver: 6 kg (13 lbs)

Shipping Weight: 72 kg (159 lbs) with all units/accessories Unit M 250V 4A, 1.25 x 0.25”

Compliance:

Computer Requirements: Computer not included, please contact Cannon for specifications.

Order Information


9725-C17 miniPV®-HX 115V 50/60 hz

9725-C16 miniPV®-HX 100V 50/60 hz

9725-C18 miniPV®-HX 230V 50/60 hz

P61.5600 Dostmann Thermometer, Calibrated, Digital Dual Channel Kit

P61.5601 Standard Size Smart Probe

CANNON® miniPV®-HX Fully Automated Polymer Solution Viscometer

INNOVATIONS IN VISCOSITY MEASUREMENT

Automates standard & Proprietary solution viscosity methods • ASTM D2857, D4603, D789, D1243, D1795, USP 911, D4243, SCAN-CM 15:99 • ISO 1628, ISO 307, ISO 5351, Tappi T230, PAPTAC G.24P, Etc.

2139 High Tech Road • State College • PA • 16803 800-676-6232 • 814-353-8000 • Fax 814-353-8007email: [email protected] • www.cannoninstrument.com

©2012 CANNON Instrument Company • Printed in USA

• Designed to Meet the Unique Needs of Users in the Polymer Industry

• Calculation of Relative, Inherent, Reduced and Intrinsic Viscosity

• 0.3 to 5,000 centistokes range

• (special ranges available on request)

• Superb Temperature Control from

• 20 to 100°C (±0.01°C)

• Accurate Flow Times ( to 0.01 seconds)

• Thermistor Sensors

• Peltier Technology Cooling for efficient operation near ambient temperatures

• Powerful VISCPRO II® Software for Control, Calculation and Database Management

• Compatible with Acids and Solvents used for Polymer Characterization

CANNON® PolyVISC SPSSolution Preparation System

• Prepares polymer solutions for relative viscosity measurements using weight-to-weight methodology

• Eliminates errors due to variations in solvent density and cumbersome manual weight and volume measurements

• Provides concentration accuracy often better than ±0.02%

The PolyVISC® SPS Solution Preparation System from CANNON Instrument Company is a semi-automated solution preparation system that uses gravimetric rather than volumetric methodology. The SPS can be used with the CANNON miniPV®-HX Automatic Viscometer to provide a complete polymer analysis system.

CANNON® miniPV-HX® Fully Automated Polymer

Solution Viscometer

56

TE-1500 – page 22The thermoelectrically-cooled TE-1500 providesrock-steady cooling to –30°C using Peltier celltechnology. Cooling fans and front panel controls arethe only moving parts in this advanced design. Afour-pane frost-free viewing window and twin fluorescentlamps provide excellent visibility and illumination withinthe bath.

TE-3000 – page 23Our premiere digital bath model for low-temperatureapplications, the TE-3000 combines reliablethermoelectric cooling with convenient keypadoperation. Temperature settings remain stored inmemory even if bath power is cut off. The liquid-crystaldisplay indicates temperature in Celsius or Fahrenheit. Aself-diagnostic routine and upgradable firmware are justtwo of many improvements in our internationally-respected bath technology.

Analog Digital Analog

-30°C -30°C

+10°C

+100°C

+10°C+30°C

-40°C

-30°C

-20°C

-10°C

0°C

50°C

75°C

100°C

150°C

200°C

+10°C*

+150°C +150°C

+200°C

+100°C

+20°C +20°C +25°C

Digital Analog Analog AnalogTE-1500 TE-3000 CT-600 CT-2000 CT-500/518 CT-1000 CT-1000HT

* Requires optional chiller/cooler and/or use of built-in cooling coil for operation near and below ambient.

CANNON® Commitment to Quality & to You!

CANNON®

Commitment to Quality & to You!

ASTM D 445/ISO 3104

TE-3000TE-1500

*Need a CTbath manifold?See page 70.

57

� Accurate TemperatureControl from 20°C to100°C

� Safe/Reliable Operation

The CANNON CT-500/518baths maintain accuratetemperature control of ± 0.01°Cwithin the range of 20°C to100°C, providing the temperaturesensitivity required by ASTM D445 for kinematic viscositymeasurements with glass capillaryviscometers. Two electric heatingelements inside the bath rapidlyheat the medium to any desiredtemperature within the range. Acooling coil, when connected totap water or a cooling system,permits operation below or slightlyabove ambient temperature.

Temperature SelectionA special selector switch on thefront panel facilitates rapid settingof ten popular temperatures forkinematic viscosity determinations.

Temperatures which may beselected with this switch are 20,25, 30, 40, 50, 60, 70, 80, 90,and 100°C. After the switch hasbeen set, the bath will equilibrateto within a fraction of one degreeof the desired temperature. A finetuning control then allows temperature adjustment to within ±0.01°C of the target temperature. By switching to the“variable” setting on the front panel, any temperature withinthe operating range can be obtained.

Description of BathA solid-state control circuit provides proportional control oftemperature. The sensing element for the control circuit is astainless steel-encased thermistor.

A motor-driven stirrer ensures a uniform temperaturethroughout the bath. The entire electrical control system islocated in a convenient drawer, mounted on glides for easyaccess if adjustment or repair is necessary.

The CT-500 bath chamber is acylindrical clear glass vessel 305mm (12 inches) in diameter and305 mm (12 inches) high. TheCT-518 bath chamber is a full457 mm (18 inches) high. ATeflon®-coated stainless steelbaffle located in the center ofthe bath provides a plainreflective background to aid inviewing instruments. The topcover contains seven roundholes 51 mm (2 inches) indiameter for insertion ofviscometer holders, allowing upto seven viscosity measurementsto be made simultaneously.Covers are supplied for cappingunused holes. Two additionalholes 10 mm (p-inch) indiameter, are provided forthermometers. Other holeconfigurations are available onspecial order. All wetted parts ofthe CT-500/518 ConstantTemperature Baths are made ofstainless steel, glass, or Teflon.The frame is fabricated fromheavy aluminum and coatedwith a corrosion-resistant epoxyfinish. Viscometers, holders, bathoil, and thermometers must bepurchased separately.

Safety FeaturesA thermistor in the bath senses

any over-temperature fault condition. If such a conditionoccurs, all power is removed from the bath until an operatorresets the over-temperature limit circuit. A second safetyfeature cuts power to the bath heaters if the control thermistoris disconnected. Finally, operation of the bath is not possibleunless it is filled with liquid to a safe operating level. Aliquid-level sensor prevents the control circuit from heating thebath until a safe operating level is attained. The bath heatersare automatically turned off when the bath liquid drops belowminimum safe level.

CANNON CT-500 Constant Temperature Bath

18 CANNON INSTRUMENT COMPANY • 2139 HIGH TECH ROAD • STATE COLLEGE • PENNSYLVANIA • 16803 • USA800-676-6232 • 814-353-8000 • Fax: 814-353-8007 • [email protected] • www.cannoninstrument.com

CT-500 Constant Temperature Bath Specifications

Size (CT-500): 407 mm wide x 362 mm deep x610 mm high (16 x 14.25 x 24inches)

Capacity CT-500: 17 L (4.5 gal)

Capacity CT-518: 23.8 L (6.3 gal)

Weight (CT-500): 22 kg (48 lbs)

Shipping Weight (CT-500): 34 kg (75 lbs)

Order Information


9726-A10 Model CT-500, 120 volts AC, 50/60 Hz, 1000 watts

9726-A15 Model CT-500F, 240 volts AC, 50/60 Hz, 1000 watts

9726-A17 Model CT-518, 120 volts AC, 50/60 Hz, 1300 watts

9726-A19 Model CT-518F, 240 volts AC, 50/60 Hz, 1300 watts

Constant Temperature Bath

CANNON®

CT-500 Constant Temperature Bath

ASTM D 445/ISO 3104

58

� Select Temperature from20 to 150°C; 200°C forHT Model

� Multiple Safety Features

The CANNON CT-1000 ConstantTemperature Bath maintains theaccurate control required by ASTMD 445 for kinematic viscositymeasurements with glass capillaryviscometers. Within the range of 20to 100°C temperature is controlledto 0.01°C; above 100°Ctemperature is controlled to 0.03°C.

Setting TemperatureTen of the most populartemperatures for kinematic viscositymeasurement can be quickly set byrotating a special switch on thebath’s front panel. This switch allows20, 25, 30, 40, 50, 60, 80, 100,135, and 150°C to be selected.After selection of the temperature,the bath will equilibrate within afraction of one degree of thedesired temperature. A fine tuningcontrol then allows temperatureadjustment to within 0.01°C of thetarget temperature. By switching tothe “variable” setting on the frontpanel, any temperature within theoperating range can be obtained.

Bath FeaturesThe bath chamber is a cylindrical clear Pyrex® vessel 300 mm(12 inches) in diameter x 300 mm (12 inches) high. Astainless steel baffle coated with white Teflon is located in thecenter of the bath to provide a good background for viewingviscometers. Two fluorescent lamps illuminate the interior ofthe bath brightly and uniformly, without glare.

Two heating elements inside the bath rapidly heat the bathmedium to any temperature within the bath range.A stainless steel cooling coil is also incorporated. Whenconnected to tap water or a recirculating water chiller, thecooling coil allows operation at temperatures slightly aboveor below ambient.

The top cover contains sevenround holes 51 mm (2 inches) indiameter. Up to seven glasscapillary viscometers (in holders)can be placed in the bath. Otherhole configurations can besupplied on special order.

A solid-state control circuitequipped with a stainlesssteel-encased thermistor providesproportional control oftemperature. A motor-drivenstirrer ensures a uniformtemperature throughout the bath.

All wetted parts of the bath aremade of stainless steel, glass, orTeflon®. The bath housing isfabricated from heavy aluminumand coated with acorrosion-resistant epoxy finish.Viscometers, holders, bath oil,and thermometers must bepurchased separately.

Safety FeaturesThere are multiple safetyfeatures. A thermistor in the bathsenses any over-temperaturefault condition. If such acondition occurs, all power isremoved from the bath until anoperator resets theover-temperature limit control

circuit. A second safety feature cuts power to the heaters if thecontrol thermistor is disconnected. A liquid-level sensorprevents the control circuit from heating the bath until a safeoperating level is attained.


Dimensions: 438 mm wide x 464 mm deep x 584 mm high(17.25 x 18.25 x 23 inches)

Capacity: 17 L (4.5 gal)

Weight: 43 kg (95 lb)

Shipping Weight: 55.8 kg (123 lb)

Order Information


9726-A20 CT-1000, 120 volts AC, 50/60 Hz, 1400 watts

9726-A25 CT-1000F, 240 volts AC, 50/60 Hz, 1400 watts

9726-A27 CT-1000HT, 120 volts AC, 50/60 Hz, 1400 watts

9726-A29 CT-1000HTF, 240 volts AC, 50/60 Hz, 1400 watts


19CANNON INSTRUMENT COMPANY • 2139 HIGH TECH ROAD • STATE COLLEGE • PENNSYLVANIA • 16803 • USA800-676-6232 • 814-353-8000 • Fax: 814-353-8007 • [email protected] • www.cannoninstrument.com


CANNON®

CT-1000/1000HT Constant Temperature Baths

ASTM D 445/ISO 3104

CT-1000HT Constant Temperature Bath� Precision temperature control to 200°CThe CT-1000HT Constant Temperature Bath is identical tothe CT-1000, except that the CT-1000HT can achieve atemperature range from 25°C to 200°C. The temperatureselection dial includes quick-set options for 25, 40, 60,80, 100, 135, 150, 165, 185, and 200°C Temperaturesfrom 150 to 200°C can be controlled to 0.03°C (moreprecise than required by ASTM D 445 for hightemperature viscometry).

59

� Microprocessor-ControlledTemperature Regulationto 150°C

� Built-in Platinum ResistanceThermometer

� On-Screen TemperatureMonitoring

The CANNON CT-2000 ConstantTemperature Bath maintains theaccurate control required by ASTM D445 for kinematic viscositymeasurements. Within the range of20 to 100°C temperature iscontrolled to 0.01°C; above 100°Ctemperature is controlled to 0.03°C.

Setting TemperatureA keypad permits microprocessor-controlled temperature selection tothree decimal places at any settingwithin the operational range of theinstrument. Twin electric heatingelements inside the bath rapidly heatthe medium to any desiredtemperature within the range. Acooling coil, when connected to tapwater or a cooling system, permitsoperation below or slightly aboveambient temperature. The built-in platinum resistancethermometer continuously monitors bath temperature anddisplays it digitally on a four line by twenty character back-litliquid-crystal screen. Either Celsius or Fahrenheit display oftemperature may be selected. On power-up the CT-2000performs an automatic self-test of its circuits.

The CT-2000 also features RS-232 and RS-485communication ports which permit data acquisition andnetworking via an external computer. Several baths may benetworked to a single computer.

Bath FeaturesThe bath chamber is a cylindrical clear Pyrex® vessel 300 mm(12 inches) in diameter x 300 mm (12 inches) high. Astainless steel baffle coated with white Teflon is located in thecenter of the bath to provide a good background for viewing

viscometers. Two fluorescent lamps illuminate the interior ofthe bath brightly and uniformly, without glare.

The top cover contains sevenround holes 51 mm (2 inches)in diameter. Up to seven glasscapillary viscometers (inholders) can be placed in thebath. Two additional holes 10mm (p-inch) in diameter areprovided for thermometers.

A solid-state control circuitequipped with a stainlesssteel-encased thermistorprovides proportional controlof temperature. A motordriven stirrer ensures auniform temperaturethroughout the bath. Theentire electrical control systemis located in a convenientdrawer for easy access ifadjustment or repair isnecessary.

All wetted parts of the bath aremade of stainless steel, glass,or Teflon®. The bath housing isfabricated from heavyaluminum and coated with acorrosion-resistant epoxyfinish. The top cover consistsof three parts: a stainless steeltop surface, an insulating

layer, and a bottom stainless steel heat reflector. The bath isdesigned to use water or oil (not supplied). Viscometers,holders, bath oil and thermometers must be purchasedseparately.

Safety FeaturesThere are multiple safety features. A thermistor in the bathsenses any over-temperature fault condition. If such acondition occurs, all power is removed from the bath until anoperator resets the over-temperature limit control circuit. Asecond safety feature cuts power to the heaters if the controlthermistor is disconnected. A liquid-level sensor prevents thecontrol circuit from heating the bath until the safe operatinglevel is attained. The bath heaters are automatically turnedoff when the bath liquid drops below the minimum safe level.




Size: 438 mm wide x 464 mm deep x 584 mmhigh (17.3 x 18.3 x 23 inches)

Bath Volume: 17 liters (4.5 gallons)

Weight: 51.4 kg (113 lbs) without bath fluid

Shipping Weight: 60 kg (131 lbs) (total/two boxes)

Electrical: Specify exact line voltage when ordering

Display Resolution: 3 decimal places

Order Information


9726-A30 CT-2000, 100-130 VAC, 50/60 Hz, 1400 watts

9726-A35 CT-2000F, 200-250 VAC, 50/60 Hz, 1400 watts


CANNON®

CT-2000 Constant Temperature Bath

ASTM D 445/ISO 3104

60

CT-600 Constant Temperature Bath� Ideal for kinematic viscosity determinations

between 10 and 30°C� Built-in thermoelectric cooling provides

“rock-solid” temperature control at ambientand below

� Meets ASTM D 445 precision specificationsfrom 10° to 100°C

The new Cannon CT-600 has many of the engineeringand control features of the CT-500 bath (see page 18),but the CT-600 also includes a built-in thermoelectriccooling unit. The CT-600 controls temperature perASTM D 445 precision specifications between 10°Cand 100°C, and is ideal for controlled temperatureapplications between 10°C and 30°C. When tests atlow temperatures are to be made, the cooling unit isengaged via a switch on the front panel. When workingat higher temperatures (30°C and above), the switch isturned off. Nothing could be simpler.

A special selector switch on the front panel facilitatesrapid setting of ten popular temperatures for kinematic viscositydeterminations: 10, 15, 20, 25, 30, 40, 50, 60, 80, and 100°C. After theswitch has been set the bath will equilibrate to within a fraction of a degreeof the desired temperature. A fine-tuning control then allows temperatureadjustment to within ± 0.01°C of the target temperature as measured bythe user’s reference thermometer. By switching to the “variable” setting onthe front panel, any temperature within the operating range can beobtained.

For a description of bath safety features, see the CT-500 entry on page 18.

CBC-100 Bath Cooler� Thermoelectrically Cools

Baths as much as 15°C BelowAmbient

� Compact – 1/10th the Size ofStandard Refrigeration Units

� Improves TemperatureStability at Ambient andBelow

The CANNON Bath Cooler(CBC-100) is a powerful addition tothe quality line of CANNONthermoelectric products.

About one-tenth the size of manyconventional chillers, theenvironmentally-friendly CBC-100 isan efficient and reliable laboratoryworkhorse. Solid-state electronics andproven thermoelectric technologiesprovide enough cooling power to

control accurately at15°C below ambient,even in open shallowbaths.

Power Supply (same for both versions)

Size: 121 mm wide x 241 mm deep x 102 mm high(4.75 x 9.5 x 4 inches)

Cooling Column (excluding immersion probe)

Size: 108 mm wide x 190 mm deep x 222 mm high(4.25 x 7.5 x 8.75 inches)

CBC-100R: Total height including immersion probe is572 mm (22.5-inches)

*Need a CT bath manifold? See page 70.

Power Supply and Cooling Column for both versions

Weight: 5.7 kg (12.5 lbs)

PowerRequirements:

100 to 240 volts, 50/60 Hz, 250 watts

Maximum BathTemperature

The Cannon Bath Cooler should not beexposed to temperatures above 80°C.

Order Information


9726-A36 CT-600 Constant Temperature Bath, 115V, 50/60 Hz

9726-A37 CT-600F Constant Temperature Bath, 230V, 50/60 Hz

9726-D05 CBC-100R (regular version with US plug)

9726-D10 CBC-100R-F (regular version with special plug)

CT Series Storage Unit Specifications

Size: 457 mm wide x 457 mmdeep x 165 mm high(18 x 18 x 6.5 inches)

Weight: 10.9 kg (24 lbs)

Shipping Weight: 13.6 kg (30 lbs)

Order Information


9726-A50 CT Series Storage UnitCT Series Storage Unit


CANNON®

CT-600 & Bath Accessories

ASTM D 445/ISO 3104

CT Series Storage Unit� Convenient Viscometer Storage

can be used as Bath SupportThis sturdy two-drawer unit fits beneathall CANNON constant temperaturebaths. It provides elevated viewing of thebath, and ample room for storage ofviscometers and other accessories.

CBC-100 Bath Cooler

61

� Temperature Range from+10°C to –30°C

� Precision and StabilitySatisfying ASTM D 445Specifications

� Environmentally-FriendlyThermoelectric CoolingSystem

� Compact Footprint;No AccessoryHeating/CoolingUnits Required

The CANNON TE-1500Thermoelectric Low TemperatureBath incorporates many newadvances in science andtechnology, includingcustom-developed Peltier Cellsand fan-cooled high-density heatsinks. The TE-1500 provides theprecision required by ASTM D 445for measurement of kinematicviscosity at low temperatures.

Compact FeaturesThe TE-1500 is a compact,tabletop instrument which uses anair-cooled thermoelectric coolingsystem requiring no accessoryheating or cooling units.

A selector switch on the frontpanel allows direct setting of eighttemperatures commonly used forlow-temperature measurement:10, 0, –5, –10, –15, –20, –25,and –30°C. After this switch hasbeen set, the bath will equilibrateto within a fraction of a degree of the desired temperature. Afine-tuning control then allows exact temperature adjustment.By switching to the “variable” setting on the front panel, anytemperature within the operating range can be obtained.

Safety/ReliabilityBath safety and reliability areensured by a number ofbuilt-in features including aninternal thermostat whichsenses any over-temperaturefault condition. If such acondition occurs, all power isremoved from the bath untilthe internal temperaturedecreases sufficiently to resetthe thermostat. If the controlthermistor is disconnected, allpower is removed from thebath until the thermistorconnection is restored.

Description of BathThe bath holds 2.5 liters ofbath medium (not supplied).The bath housing is fabricatedfrom heavy aluminum coatedwith a corrosion-resistantepoxy finish. The top cover ofthe bath contains two roundholes 51 mm (2 inches) indiameter for insertion of glasscapillary viscometers or otherinstruments.

An additional hole is providedfor a reference thermometeror probe. The aluminum bathvessel measures 305 mmhigh x 121 mm wide x 83mm (12" x 4.75" x 3.25")deep. A baffle within the bathvessel facilitates circulation ofliquid and provides abackground for easy viewingof instruments. A four-pane

“frost-free” viewing window and internal illumination by twinfluorescent lamps provide excellent visibility within the bath.Viscometers, holders, appropriate bath medium, andthermometers must be purchased separately.

CANNON TE-1500Thermoelectric Low Temperature Bath


TE-1500 Specifications

Bath Size: 375 mm wide x 420 mm deep x 620 mm high(14.8 x 16.5 x 24.4 inches)

Bath Capacity: 2.5 liters (0.66 gal)

Bath Dimensions(Internal):

121 mm wide x 83 mm deep x 305 mm high(4.75 x 3.25 x 12 inches)

Viewing Area: 265 mm high x 95 mm wide (10.45 x 3.75 inches)

Bath Weight: 43.1 kg (95 lbs)

Bath Shipping Weight: 59 kg (130 lbs)

Electrical: Available in 120V, 220V, and 240V models. All models 50/60 HzPlease specify exact line voltage when ordering.

Order Information


9726-A62 TE-1500, 120 volts,50/60 Hz, 1000 watts

9726-A66 TE-1500F, 230 volts,50/60 Hz, 1000 watts

9726-A68 TE-1500, 100 volts,50/60 Hz, 1000 watts

Constant Temperature Baths

CANNON®

TE-1500 Constant Temperature Bath

ASTM D 445/ISO 3104

62

� Temperature Range from –30°C to +30°C� Self-Contained Thermoelectric Cooling —

No Accessory Units Required� Convenient Keypad Data Entry� Selectable Temperature Scale

(Celsius or Fahrenheit)� Meets ASTM D 445 Requirements

for Temperature Stability

The CANNON TE-3000 Thermoelectric Constant Temperature Bathprovides accurate temperature control between –30°C and +30°C,meeting the requirements of ASTM D 445 for measurement ofkinematic viscosity at low temperatures.

The low temperatures are obtained by built-in air-cooled Peltier cellswhich provide thermoelectric cooling. No external refrigeration unitor air/water heat exchanger is used.

Keypad OperationThe desired bath temperature and calibration temperatures areentered digitally by means of a keypad located on the front panel.Temperatures remain in memory even if power to the bath isaccidentally cut off. Both the target temperature and the actualtemperature of the bath are displayed continuously on a liquidcrystal display. An on-screen menu permits selection of Celsius orFahrenheit operation, along with several diagnostic features.

Durable ConstructionThe top cover of the bath contains two round holes 51 mm(2 inches) in diameter for insertion of glass capillary viscometers orother instruments. An additional hole is provided for a referencethermometer or probe. A four-pane “frost-free” viewing window andinternal illumination by fluorescent lamps provide excellent visibilitywithin the bath.

The bath holds 2.5 liters (0.66 gal) of bath medium (not supplied).The bath housing is fabricated from heavy aluminum coated with acorrosion-resistant epoxy finish. Contained in the housing is analuminum bath vessel that measures 305 mm high x 121 mm widex 83 mm deep. A baffle within the bath vessel facilitates circulationof the liquid and provides a smooth background for viewinginstruments.

Viscometers, holders, appropriate bath medium, and thermometersmust be purchased separately.

CANNON TE-3000 ThermoelectricConstant Temperature Bath

TE-3000 Specifications

Bath Size: 375 mm wide x 420 mm deep x 620 mm deep(14.8 x 16.5 x 24.4 inches)

Bath Capacity: 2.5 liters (0.66 gal)

Bath Dimensions(Internal):

121 mm wide x 83 mm deep x 305 mm high(4.75 x 3.25 x 12 inches)

Viewing Area: 265 mm high x 95 mm wide (10.45 x 3.75 inches)

Bath Weight: 43.1 kg (95 lbs)

Bath Shipping Weight: 59 kg (130 lbs)

Electrical: Available in 120V, 220V, and 240V models.All models 50/60 HzPlease specify exact line voltage when ordering.

Order Information


9726-A70 TE-3000, 120 volts, 50/60 Hz, 1000watts

9726-A75 TE-3000F, 240 volts, 50/60 Hz, 1000watts

9726-A77 TE-3000, 100 volts, 50/60 Hz, 1000watts

Constant Temperature Baths

CANNON®

TE-3000 Constant Temperature Bath

ASTM D 445/ISO 3104

63

Glass Capillary ViscometersThe tables on this page provide size and range information for viscometers onpages 26-30. Additional sizing information is available on the individual productpages for other viscometer types.

Why does CANNON offer so many different types of glass capillary viscometers?Primarily because no single capillary viscometer is ideally suited for all kinematicviscosity determinations. Individual analysts also have their own preferences. Thebrief descriptions on the following page may assist you in determining whichviscometer is most appropriate for your particular application. Feel free to contactCANNON with your questions. Our experienced staff will be happy to assist you.

Expanded UncertaintyCANNON Instrument Company provides expanded uncertainty data with allof our calibrated viscometers. This is the universally accepted statistic when dealingwith calibration data. In order to maintain A2LA accreditation, we are required todetermine and specify the expanded uncertainty for all our calibration data.

ISO publications define expanded uncertainty as "quantity defining the interval aboutthe result of a measurement within which the values that could reasonably beattributed to the measurement may be expected to lie with a high level ofconfidence."

Expanded uncertainty is a more comprehensive and meaningful term than"precision" because it incorporates all variables in the measurement process. Whencomparing the accuracy of viscometers it is essential that the expanded uncertaintybe specified. Detailed information regarding CANNON measurements andexpanded uncertainty is available for download from the CANNON website,www.cannoninstrument.com.

CANNON Instrument Company also provides uncertainty data with every bottle ofour certified viscosity standards (see pages 42-49).

CANNON Glass Capillary Viscometers

24

Specifications forCANNON

®

Viscometers

Table 1

Cannon-Fenske,Cannon-Ubbelohde, andCannon-Ubbelohde DilutionViscometers

Size

Approx.constant,

cSt/sRangecentistokes*

25 0.002 0.5 to 2

50 0.004 0.8 to 4

75 0.008 1.6 to 8

100 0.015 3 to 15

150 0.035 7 to 35

200 0.1 20 to 100

300 0.25 50 to 250

350 0.5 100 to 500

400 1.2 240 to 1200

450 2.5 500 to 2500

500 8 1600 to 8000

600 20 4000 to 20 000

650 45 9000 to 45 000

700 100 20 000 to 100 000

* Ranges in centistokes represent flow timesof 250 to 1000 seconds for Size 25, and200 to 1000 for all other sizes.

Table 2

Ubbelohde Viscometers

Size

Approx.constant,

cSt/sRangecentistokes*

0 0.001 0.3 to 1

0C 0.003 0.6 to 3

0B 0.005 1 to 5

1 0.01 2 to 10

1C 0.03 6 to 30

1B 0.05 10 to 50

2 0.1 20 to 100

2C 0.3 60 to 300

2B 0.5 100 to 500

3 1.0 200 to 1000

3C 3.0 600 to 3000

3B 5.0 1000 to 5000

4 10 2000 to 10 000

4C 30 6000 to 30 000

4B 50 10 000 to 50 000

5 100 20 000 to 100 000

* Ranges in centistokes represent flow timesof 300 to 1000 seconds for Size 0, and 200to 1000 seconds for all other sizes.

CANNON INSTRUMENT COMPANY • 2139 HIGH TECH ROAD • STATE COLLEGE • PENNSYLVANIA • 16803 • USA800-676-6232 • 814-353-8000 • Fax: 814-353-8007 • [email protected] • www.cannoninstrument.com

Glass Capillary Viscometers

CANNON®

Glass Capillary ViscometersSize, Range, & Expanded Uncertainty

ASTM D445ASTM D 446, ASTM D 2171, ISO 3104, ISO 3105

64

Cannon-Fenske Routine Viscometers

Calibrated CFRC SeriesFor measuring kinematic viscosity of transparent Newtonianliquids, particularly petroleum products or lubricants, accordingto ASTM D 445 and ISO 3104. Specifications conform toASTM D 446 and ISO 3105.

Provided with certificate of calibration and instruction sheet. Seepage 24 for significance of expanded uncertainty.

� Minimum sample volume 7 mL. Require liquid bath depth of203 mm (8 inches).

� Constants and ranges are as specified in Table 1 onpage 24.

� Holder is not supplied. For holders, see 9726-M50 and-M53 on page 37.

� Viscometers with special constants are available by specialorder at additional cost.

Uncalibrated CFRU SeriesSimilar to 9721-B50 series, but uncalibrated.

� Holder is not supplied. For holders, see 9726-M50, -M53, and -M79 on page 37.

Cannon-Fenske Opaque Viscometers

Reverse-flow type for dark liquids

Calibrated CFOC SeriesReverse-flow type, for measurement of kinematic viscosity ofdark Newtonian liquids according to ASTM D 445 and ISO3104. Permit measurements of liquids whose meniscus cannotbe seen at the timing marks when using Cannon-FenskeRoutine-type viscometer. Used to measure kinematic viscosity ofliquid (cutback) asphalts and road oils at 60°C (140°F) inrange of 30 to 6000 centistokes according to ASTM D 2170.Also used to study lubricating oils at low temperatures wheninvestigating the effect of various additives on lubricating andhydraulic oils. External pressure can be applied to vary shearstress and shear rate. Specifications conform to ASTM D 446and ISO 3105 for single determinations of viscosity for opaqueliquids. Upper bulb may be used for determining the degree ofnon-Newtonian behavior of the sample.


� Minimum sample volume 12 mL. Require liquid bath depthof 229 mm (9 inches).

� Size 25 has approximate constant 0.002 cSt/s and range of 0.4 to 2 cSt. Constants and ranges forother sizes are as given in Table 1 on page 24.

� Holder is not supplied. For holders, see 9726-M50 and -M53 on page 37.

� For replacement micro stoppers, see 9726-N98 on page 37.

� Viscometers with special constants are available by special order at additional cost.

Uncalibrated CFOU SeriesSimilar to 9721-F50 series, but uncalibrated.


9721-A50 Series9721-B50 Series

26

SizeUncalibratedCFRU Series

CalibratedCFRCSeries

25 9721-A50 9721-B50

50 9721-A53 9721-B53

75 9721-A56 9721-B56

100 9721-A59 9721-B59

150 9721-A62 9721-B62

200 9721-A65 9721-B65

300 9721-A68 9721-B68

350 9721-A71 9721-B71

400 9721-A74 9721-B74

450 9721-A77 9721-B77

500 9721-A80 9721-B80

600 9721-A83 9721-B83

650 9721-A86 9721-B86

700 9721-A89 9721-B89

SizeUncalibratedCFOU Series

CalibratedCFOCSeries

25 9721-E50 9721-F50

50 9721-E53 9721-F53

75 9721-E56 9721-F56

100 9721-E59 9721-F59

150 9721-E62 9721-F62

200 9721-E65 9721-F65

300 9721-E68 9721-F68

350 9721-E71 9721-F71

400 9721-E74 9721-F74

450 9721-E77 9721-F77

500 9721-E80 9721-F80

600 9721-E83 9721-F83

650 9721-E86 9721-F86

700 9721-E89 9721-F89

9721-E50 Series9721-F50 Series



Routine & Qpaque Cannon-Fenske Viscometers

ASTM D 445, ASTN D 446, ISO 3104, ISO 3105

65

Ubbelohde Viscometers

Calibrated UBC SeriesFor measurement of kinematic viscosity oftransparent Newtonian liquids by suspended levelprinciple as described in ASTM D 445 and D 446,and ISO 3104 and 3105. Similar toCannon-Ubbelohde but less rugged in design.

Provided with certificate of calibration and instructionsheet. See page 24 for significance of expandeduncertainty.

� Minimum sample volume 11 mL. Require liquidbath depth of 241 mm (9.5 inches).

� Constants and ranges are as specified in Table 2on page 24.

� Holder is not supplied. For holder, see9726-M82 on page 37.

Uncalibrated UBU SeriesSimilar to 9721-R50 series, but uncalibrated.

� Holder is not supplied. For holder, see9726-M82 on page 37.

Ubbelohde Unity Factor Calibrated UBXC SeriesSimilar to 9721-R50 series, but with constant within ± 0.2% of values listed in Table 2 on page 24.Provided with certificate of calibration and instruction sheet.

� Holder is not supplied. For holder, see 9726-M82 on page 37.

Cannon-Ubbelohde Viscometers

Calibrated CUC SeriesSuspended level viscometer for measurement of kinematicviscosity of transparent Newtonian liquids according to ASTM D445 and ISO 3104. Also used for evaluating jet and hydrauliclubricants. Especially suited for use at temperatures above 93°C(200°F) or below –18°C (0°F). Require no kinetic energycorrections over 0.5 to 100 000 centistokes range. Viscometerconstant is same at all temperatures. Specifications conform toASTM D 446 and ISO 3105.


� Minimum sample volume 11 mL. Require liquid bath depthof 254 mm (10-inches); must be submerged toapproximately 220 mm (8.5-inches).


� Holder is not supplied. For holders, see 9726-M70, -M73,and -M76 on page 37.

Uncalibrated CUU SeriesSimilar to 9721-K50 series, but uncalibrated.

Holder is not supplied. For holders, see 9726-M70, -M73, and -M76 on page 37.

9721-N50 Series9721-R50 Series9721-U50 Series

SizeUncalibratedUBU Series

CalibratedUBC Series

CalibratedUBXC Series

0 9721-N50 9721-R50 9721-U50

0C 9721-N53 9721-R53 9721-U53

0B 9721-N56 9721-R56 9721-U56

1 9721-N59 9721-R59 9721-U59

1C 9721-N62 9721-R62 9721-U62

1B 9721-N65 9721-R65 9721-U65

2 9721-N68 9721-R68 9721-U68

2C 9721-N71 9721-R71 9721-U71

2B 9721-N74 9721-R74 9721-U74

3 9721-N77 9721-R77 9721-U77

3C 9721-N80 9721-R80 9721-U80

3B 9721-N83 9721-R83 9721-U83

4 9721-N86 9721-R86 9721-U86

4C 9721-N89 9721-R89 9721-U89

4B 9721-N92 9721-R92 9721-U92

5 9721-N95 9721-R95 9721-U95

SizeUncalibratedCUU Series

CalibratedCUC Series

25 9721-J50 9721-K50

50 9721-J53 9721-K53

75 9721-J56 9721-K56

100 9721-J59 9721-K59

150 9721-J62 9721-K62

200 9721-J65 9721-K65

300 9721-J68 9721-K68

350 9721-J71 9721-K71

400 9721-J74 9721-K74

450 9721-J77 9721-K77

500 9721-J80 9721-K80

600 9721-J83 9721-K83

650 9721-J86 9721-K86

700 9721-J89 9721-K89

9721-J50 Series9721-K50 Series


Suspended Level Ubbelohde Viscometers

ASTM D 445, ASTM D 446, ISO 3104, ISO 3105

66

Cannon-UbbelohdeSemi-Micro Viscometers

Semi-Micro Calibrated CUSMC SeriesFor measuring kinematic viscosity of small samples oftransparent Newtonian liquids according to ASTM D 445and ISO 3104. Specifications conform to ASTM D 446and ISO 3105. Viscometer constant is same at alltemperatures.


� Minimum sample volume approximately 1.0 mL. Sizes400 through 600 may require larger sample volume.Initial sample can be diluted to as much as 20 mL forintrinsic viscosity determinations. Require liquid bathdepth of 240 mm (9.5 inches).

� Size 25 has approximate constant 0.002 cSt/s and a range of 0.4 to 2 cSt. Constants and rangesfor all other sizes are as given in Table 1 on page 37.


Semi-Micro Uncalibrated CUSMU SeriesSimilar to 9722-H50 series, but uncalibrated.


Cannon-UbbelohdeDilution Viscometers

Dilution Type Calibrated CUDC SeriesFor measurement of intrinsic viscosity of transparentNewtonian liquids according to ASTM D 445 and ISO3104. Specifications conform to ASTM D 446 and ISO3105. Viscometer constant is same at all temperatures.


� Minimum sample volume of 8 mL can be diluted to 40mL. Require liquid bath depth of 305 mm (12 inches).The CANNON CT-518 bath is recommended.


� Holder is not supplied. For holders, see 9726-M70,-M73, and -M76 on page 37.

Dilution Type Uncalibrated CUDU SeriesSimilar to 9722-M50 series, but uncalibrated.



Semi-Micro & Dilution Cannon-Ubbelohde Viscometers


9722-G50 Series9722-H50 Series

9722-L50 Series9722-M50 Series

SizeUncalibratedCUSMU Series

CalibratedCUSMC Series

25 9722-G50 9722-H50

50 9722-G53 9722-H53

75 9722-G56 9722-H56

100 9722-G59 9722-H59

150 9722-G62 9722-H62

200 9722-G65 9722-H65

300 9722-G68 9722-H68

350 9722-G71 9722-H71

400 9722-G74 9722-H74

450 9722-G77 9722-H77

500 9722-G80 9722-H80

600 9722-G83 9722-H83

Size

UncalibratedCUDUSeries

CalibratedCUDCSeries

25 9722-L50 9722-M50

50 9722-L53 9722-M53

75 9722-L56 9722-M56

100 9722-L59 9722-M59

150 9722-L62 9722-M62

200 9722-L65 9722-M65

300 9722-L68 9722-M68

350 9722-L71 9722-M71

400 9722-L74 9722-M74

450 9722-L77 9722-M77

500 9722-L80 9722-M80

600 9722-L83 9722-M83

67

Cannon-Ubbelohde Four-Bulb ShearDilution Viscometers

Five-fold dilution type

Calibrated CUSDC-11 SeriesFor measurement of intrinsic viscosities extrapolated tozero shear rate. Provide five-fold range of shear rates.Design gives extra mechanical strength. Negligiblekinetic energy correction.


� Minimum sample volume 20 mL. Require liquid bathdepth of 280 mm (11 inches).


Uncalibrated CUSDU-11 SeriesSimilar to 9723-M50 series, but uncalibrated.


Ten-fold dilution type

Calibrated CUSDC-17 SeriesSimilar to 9723-M50 series, but provide ten-fold rangeof shear rates.

Provided with certificate of calibration and instructionsheet. See page 24 for significanceof expanded uncertainty.

� Minimum sample volume 20 mL. Require liquid bathdepth of 430 mm (17 inches). The CT-518 bath isrecommended.


Uncalibrated CUSDU-17 SeriesSimilar to 9723-R50 series, but uncalibrated.


9723-L50 Series9723-M50 Series9723-N50 Series9723-R50 Series

Specificationsfor Five-fold Dilution Type

Size†

Approx.Constant,cSt/s

*RangecSt

Shear rateat wall,reciprocalseconds

25 0.002 0.4 to 2 82 to 1650

50 0.004 0.8 to 4 45 to 900

75 0.008 1.6 to 8 24 to 480

100 0.015 3 to 15 15 to 300

150 0.035 7 to 35 8 to 160

* Ranges in centistokes represent flow times of200 to 1000 seconds.

Size†

UncalibratedCUSDU-11Series

CalibratedCUSDC-11Series

25 9723-L50 9723-M50

50 9723-L53 9723-M53

75 9723-L56 9723-M56

100 9723-L59 9723-M59

150 9723-L62 9723-M62

Specifications forTen-fold Dilution Type

Size†

Approx.constant, cSt/s

*RangecSt

Shear rate atwall, reciprocalseconds

25 0.002 0.4 to 2 82 to 3300

50 0.004 0.8 to 4 45 to 1800

75 0.008 1.6 to 8 24 to 960

100 0.015 3 to 15 15 to 600

150 0.035 7 to 35 8 to 320

* Ranges in centistokes represent flow times of200 to 1000 seconds.

Size†

UncalibratedCUSDU-17Series

CalibratedCUSDC-17Series

25 9723-N50 9723-R50

50 9723-N53 9723-R53

75 9723-N56 9723-R56

100 9723-N59 9723-R59

150 9723-N62 9723-R62


Cannon-Ubbelohde Four-Bulb Shear Dilution Viscometers


†Additional tube sizes with larger constantsavailable by request.

68

pargiro

Cross-Out

pargiro

Replacement Text

Five fold

pargiro

Cross-Out

pargiro

Replacement Text

Ten-fold

Cannon-ManningSemi-Micro Viscometers

Calibrated CMSMC SeriesFor measurement of kinematic viscosity of small samples oftransparent Newtonian liquids, including petroleum productsor lubricants, according to ASTM D 445 and ISO 3104.Specifications conform to ASTM D 446 and ISO 3105.

Provided with certificate of calibration and instruction sheet.See page 24 for significance of expanded uncertainty.

� Sample volume approximately 1.0 mL. Sizes 400 through600 may require more sample. Require liquid bath depthof 200 mm (8 inches).

� Size 25 has approximate constant 0.002 cSt/s and arange of 0.4 to 2 cSt. Constants and ranges for all othersizes are as given in Table 1 on page 24.

� Holder is not supplied. For holders, see 9726-M50 and-M53 on page 37.

Uncalibrated CMSMU SeriesSimilar to 9721-Y50 series, but uncalibrated.

� Holder is not supplied. For holders, see 9726-M50 and -M53 on page 37.

Cannon-Manning Semi-MicroExtra Low Charge Viscometers

Extra Low Charge Calibrated CMSMEC SeriesSimilar to 9721-Y50 series, but require smaller samplevolume of approximately 0.5 mL. Sizes 200 through 600may require larger volume of sample.


� Without holder.

Extra Low Charge Uncalibrated CMSMEU SeriesSimilar to 9722-D50 series, but uncalibrated.

� Without holder.

9721-X50 Series9721-Y50 Series

30

SizeUncalibratedCMSMU Series

CalibratedCMSMC Series

25 9721-X50 9721-Y50

50 9721-X53 9721-Y53

75 9721-X56 9721-Y56

100 9721-X59 9721-Y59

150 9721-X62 9721-Y62

200 9721-X65 9721-Y65

300 9721-X68 9721-Y68

350 9721-X71 9721-Y71

400 9721-X74 9721-Y74

450 9721-X77 9721-Y77

500 9721-X80 9721-Y80

600 9721-X83 9721-Y83

Size

UncalibratedCMSMEUSeries

CalibratedCMSMECSeries

25 9722-C50 9722-D50

50 9722-C53 9722-D53

75 9722-C56 9722-D56

100 9722-C59 9722-D59

150 9722-C62 9722-D62

200 9722-C65 9722-D65

300 9722-C68 9722-D68

350 9722-C71 9722-D71

400 9722-C74 9722-D74

450 9722-C77 9722-D77

500 9722-C80 9722-D80

600 9722-C83 9722-D83

9722-C50 Series9722-D50 Series



Cannon-Manning Semi-Micro Low Charge Viscometers


Companion Product!Constant Temperature Baths(ASTM D 445 compliant) -see pages 16-23.

69

Zeitfuchs®

Transparent Viscometers

With permanently attachedround metal holder

Calibrated ZTC-RO SeriesFor measurement of kinematic viscosity of transparentNewtonian liquids according to ASTM D 445 and ISO3104. Specifications conform to ASTM D 446 andISO 3105. Filling, measurement, and cleaning can bedone without removal from constant temperature bath.

Certificate of calibration and instruction sheetprovided. See page 24 for significance of expandeduncertainty.


� For constants and ranges, see table at right.

� Manufactured with permanently attached roundmetal holder, for hole 51 mm (2 inches) indiameter.

Uncalibrated ZTU-RO SeriesSimilar to 9723-B50 series, but uncalibrated.

With permanently attachedrectangular metal holder

Calibrated ZTC-RE SeriesFor measurement of kinematic viscosity of transparentNewtonian liquids according to ASTM D 445 and ISO3104. Specifications conform to ASTM D 446 andISO 3105. Filling, measurement, and cleaning can bedone without removal from constant temperature bath.



� For constants and ranges, see table (above right).

� Manufactured with permanently attached rectangularmetal holder which requires a bath opening of 25 x48 mm (1 x 1.9 inches).

Calibrated ZTU-RE SeriesSimilar to 9723-D50 series, but uncalibrated.


9723-A50 Series9723-B50 Series

Specifications for Zeitfuchs®

Transparent* & Zeitfuchs® Cross-ArmViscometers

SizeApproximateconstant, cSt/s Viscosity, cSt†

1 0.003 0.6 to 3

2 0.01 2 to 10

3 0.03 6 to 30

4 0.1 20 to 100

5 0.3 60 to 300

6 1.0 200 to 1000

7 3.0 600 to 3000

8 10 2000 to 10 000

9 30 6000 to 30 000

10 100 20 000 to 100 000

* Zeitfuchs Transparent viscometers are*availableonly in sizes 1 through 7.

† Ranges in centistokes represent flow times of 200to 1000 seconds.

SizeUncalibratedZTU-RO Series

CalibratedZTC-RO Series

1 9723-A50 9723-B50

2 9723-A55 9723-B55

3 9723-A60 9723-B60

4 9723-A65 9723-B65

5 9723-A70 9723-B70

6 9723-A75 9723-B75

7 9723-A80 9723-B80

SizeUncalibratedZTU-RE Series

CalibratedZTC-RE Series

1 9723-C50 9723-D50

2 9723-C55 9723-D55

3 9723-C60 9723-D60

4 9723-C65 9723-D65

5 9723-C70 9723-D70

6 9723-C75 9723-D75

7 9723-C80 9723-D80

9723-C50 Series9723-D50 Series


CANNON®

Zeitfuchs Transparent Viscometers


70

Calibrated Zeitfuchs®

Cross-Arm ViscometersFor measurement of kinematic viscosity of transparent andopaque Newtonian liquids according to ASTM D 445 andISO 3104. Specifications conform to ASTM D 446 and ISO3105. Also used to measure kinematic viscosity of liquid(cutback) asphalts and road oils at 60°C (140°F) andasphalt cements at 135°C (275°F) in the range of 30 to6000 centistokes according to ASTM D 2170. Can be filledand cleaned while in constant temperature bath.

� Minimum sample volume 1 to 3 mL. Require liquid bathdepth of 230 mm (9 inches).

� Constants and ranges are as described in table on page33.

� All instruments calibrated. Certificate of calibration andinstruction sheet provided. See page 24 for expandeduncertainty. Offered with and without holder as describedbelow.

ZCAC SeriesAs described above. Without holder.

� For holder, see 9726-M95 and -M98 on page 37.

Unity Factor ZCAXC SeriesSimilar to 9723-S50 series, but have constant within ±0.2% of values listed in table on page33.

� For holder, see 9726-M95 and -M98 on page 37.

With permanently attachedround metal holder

ZCAC-RO SeriesAs described above. Supplied with permanentlyattached round metal holder, for hole 51 mm(2 inches) in diameter.

Unity Factor ZCAXC-RO SeriesSimilar to 9723-W50 series, but have constantwhich is within ± 0.2% of values listed in tableon page 33.

With permanently attachedrectangular metal holder

ZCAC-RE SeriesAs described above. Supplied with permanentlyattached rectangular metal holder whichrequires bath opening25 x 48 mm (1 x 1.9 inches).

Unity Factor ZCAXC-RE SeriesSimilar to 9724-B50 series, but have constantwithin ± 0.2% of value listed in table on page 33.

9723-S50 Series9723-U50 Series

32

SizeZCACSeries

ZCAXC SeriesUnity Factor

1 9723-S50 9723-U50

2 9723-S53 9723-U53

3 9723-S56 9723-U56

4 9723-S59 9723-U59

5 9723-S62 9723-U62

6 9723-S65 9723-U65

7 9723-S68 9723-U68

8 9723-S71 9723-U71

9 9723-S74 9723-U74

10 9723-S77 9723-U77

SizeZCAC-ROSeries

Unity FactorZCAXC-ROSeries

1 9723-W50 9723-Y50

2 9723-W53 9723-Y53

3 9723-W56 9723-Y56

4 9723-W59 9723-Y59

5 9723-W62 9723-Y62

6 9723-W65 9723-Y65

7 9723-W68 9723-Y68

8 9723-W71 9723-Y71

9 9723-W74 9723-Y74

10 9723-W77 9723-Y77

SizeZCAC-RESeries

Unity FactorZCAXC-RESeries

1 9724-B50 9724-D50

2 9724-B53 9724-D53

3 9724-B56 9724-D56

4 9724-B59 9724-D59

5 9724-B62 9724-D62

6 9724-B65 9724-D65

7 9724-B68 9724-D68

8 9724-B71 9724-D71

9 9724-B74 9724-D74

10 9724-B77 9724-D77

9723-W50 Series9723-Y50 Series

9724-B50 Series9724-D50 Series



CANNON®

Zeitfuchs Cross-Arm Viscometers

ASTM D 445, ASTM D 446, ASTM D 2170, ISO 3104, ISO 3105

71

BS/U-Tube ViscometersFor Transparent LiquidsFor measurement of kinematic viscosity of transparentNewtonian liquids according to ASTM D 445 and ISO3104. Specifications conform to ASTM D 446 and ISO3105.


� Minimum sample volume 7 mL in sizes A to C, 12 mL insizes D to F, and 23 mL in sizes G and H. Require liquidbath depth of 280 mm (11 inches).

� Without holder.

BS/U/M MiniatureU-Tube ViscometersFor measurement of kinematic viscosity of transparentNewtonian liquids according to ASTM D 445and ISO 3104. Specifications conform to ASTM D 446 andISO 3105.


� Minimum sample volume 2 mL. Require liquid bath depthof 230 mm (9 inches).

� Without holder.


9724-E50 Series

Specifications for BS/U-TubeViscometers

Size

Approx.Constant,mm2/s2 (cSt/s)

Viscosity Rangemm2/ sec (cSt)*

A 0.003 0.9 to 3

B 0.01 2.0 to 10

C 0.03 6 to 30

D 0.1 20 to 100

E 0.3 60 to 300

F 1.0 200 to 1000

G 3.0 600 to 3000

H 10.0 2000 to 10 000

* Ranges in centistokes represent flow timesof 300 to 1000 seconds for Size A and 200to 1000 seconds for all other sizes.

SizeCalibratedBS/U-Tube Series

A 9724-E50

B 9724-E53

C 9724-E56

D 9724-E59

E 9724-E62

F 9724-E65

G 9724-E68

H 9724-E71

Specifications for BS/U/M MiniatureU-Tube Viscometers

Size


Viscosity Range,mm2/ sec (cSt)*

M1 0.001 0.2 to 1

M2 0.005 1 to 5

M3 0.015 3 to 15

M4 0.04 8 to 40

M5 0.1 20 to 100

* Ranges in centistokes represent flow timesof 200 to 1000 seconds.

SizeCalibratedBS/U/M Series

M1 9724-E80

M2 9724-E83

M3 9724-E86

M4 9724-E89

M5 9724-E92

9724-E80 Series


CANNON®

BS/U-Tube Viscometers


72

BS/IP/SL SuspendedLevel ViscometersFor measurement of kinematic viscosityof transparent Newtonian liquidsaccording to ASTM D 445 and ISO3104. Specifications conform toASTM D 446 and ISO 3105.

Provided with certificate of calibrationand instruction sheet.See page 24 for significanceof expanded uncertainty.

� Minimum sample volume 11 mL.Require liquid bath depth of 250mm (10 inches).

� Holder is not supplied. For holder,see 9726-M99 on page 37.

BS/IP/SL(S) ViscometersFor measurement of kinematic viscosityof transparent Newtonian liquidsaccording to ASTM D 445 and ISO3104. Specifications conform toASTM D 446 and ISO 3105.

Provided with certificate of calibrationand instruction sheet. See page 24 forsignificance of expanded uncertainty.



9724-F10 Series


Specifications for BS/IP/SLSuspended Level Viscometers

Size

Approx.Constantmm2/s2 (cSt/s)

Viscosity Range,mm2/sec (cSt)*

CalibratedBS/IP/SL Series

1 0.01 3.5 to 10 9724-F10

1A 0.03 6 to 30 9724-F13

2 0.1 20 to 100 9724-F16

2A 0.3 60 to 300 9724-F19

3 1.0 200 to 1000 9724-F22

3A 3.0 600 to 3000 9724-F25

4 10 2000 to 10 000 9724-F28

4A 30 6000 to 30 000 9724-F31

5 100 20 000 to 100 000 9724-F34

* Ranges in centistokes represent flow times of 350 to 1000 secondsfor Size 1 and 200 to 1000 seconds for all other sizes.

Specifications for Shortened Form BS/IP/SL(S)Suspended Level Viscometers

Size


Viscosity Range,mm2/sec (cSt)

CalibratedBS/IP/SL(S) Series

1 0.0008 1.05 minimum* 9724-F50

2 0.003 2.1† to 3 9724-F53

3 0.01 3.8‡ to 10 9724-F56

4 0.03 6¤ to 30 9724-F59

5 0.1 20 to 100 9724-F62

6 0.3 60 to 300 9724-F65

7 1.0 200 to 1000 9724-F68

8 3.0 600 to 3000 9724-F71

9 10 2000 to 10 000 9724-F74

* 1 320 seconds minimum flow time.

† 600 seconds minimum flow time to 1000 seconds.

‡ 380 seconds minimum flow time to 1000 seconds.

¤ Ranges in centistokes represent flow times of 200 to 1000 secondsfor all other sizes.

9724-F50 Series


CANNON®

Suspended Level Viscometers


73

BS/IP/MSL MiniatureSuspended LevelViscometersFor measurement of kinematic viscosityof transparent Newtonian liquidsaccording to ASTM D 445 and ISO3104. Specifications conform toASTM D 446 and ISO 3105.

Provided with certificate of calibrationand instruction sheet.See page 24 for significanceof expanded uncertainty.

� Minimum sample volume 4 mL.Require liquid bath depth of305 mm (12 inches).


BS/IP/RF U-Tube ReverseFlow ViscometersFor measurement of kinematic viscosityof opaque Newtonian liquids accordingto ASTM D 445 and ISO 3104.Specifications conformto ASTM D 446 and ISO 3105.

Provided with certificate of calibrationand instruction sheet. See page 24 forsignificance of expanded uncertainty.


� Holder is not supplied. For holder,see 9726-N45 on page 37.


9724-G10 Series

Specifications for BS/IP/MSLMiniature Suspended Level Viscometers

Size


Viscosity Range,mm2/sec (cSt)*

CalibratedSeriesBS/IP/MSL

1 0.003 0.6 to 3 9724-G10

2 0.01 2 to 10 9724-G13

3 0.03 6 to 30 9724-G16

4 0.1 20 to 100 9724-G19

5 0.3 60 to 300 9724-G22

6 1.0 200 to 1000 9724-G25

7 3.0 600 to 3000 9724-G28

* Ranges in centistokes represent flow times of 200 to 1000 seconds.

Specifications for BS/IP/RFU-Tube Reverse Flow Viscometers

Size

Approx.Constantmm2/s2 (cSt/s)

Viscosity Rangemm2/sec (cSt)*

CalibratedBS/IP/RFU-Tube Series

1 0.003 0.6 to 3 9724-G50

2 0.01 2 to 10 9724-G53

3 0.03 6 to 30 9724-G56

4 0.1 20 to 100 9724-G59

5 0.3 60 to 300 9724-G62

6 1.0 200 to 1000 9724-G65

7 3.0 600 to 3000 9724-G68

8 10 2000 to 10 000 9724-G71

9 30 6000 to 30 000 9724-G74

10 100 20 000 to 100 000 9724-G77

11 300 60 000 to 300 000 9724-G80

* Ranges in centistokes represent flow times of 200 to 1000 seconds.

9724-G50 Series


Suspended Level & Reverse Flow BS/IP Viscometers


74

9724-H50 Series


SizeCalibratedCMVC Series

CalibratedCMVC-RO Series

4 9724-H50 9724-L50

5 9724-H53 9724-L53

6 9724-H56 9724-L56

7 9724-H59 9724-L59

8 9724-H62 9724-L62

9 9724-H65 9724-L65

10 9724-H68 9724-L68

11 9724-H71 9724-L71

12 9724-H74 9724-L74

13 9724-H77 9724-L77

14 9724-H80 9724-L80

Specifications forAsphalt Institute Vacuum Viscometers

SizeViscosityrange, poise

Approx. constantpoise/second at 300

mm Hg vacuum

at B at C at D

25 42 to 800 2 1 0.7

50 180 to 3200 8 4 3

100 600 to 12 800 32 16 10

200 2400 to 52 000 128 64 40

400R 9600 to 1 400 000 500 250 160

800R 38 000 to 5 800 000 2000 1000 640

SizeCalibratedAIVC Series

CalibratedAIVC-RO Series

25 9724-R50 9724-T50

50 9724-R55 9724-T55

100 9724-R60 9724-T60

200 9724-R65 9724-T65

400R 9724-R70 9724-T70

800R 9724-R75 9724-T75

Specifications for Cannon-ManningVacuum Viscometers

SizeViscosityrange, poise

Approx. constant poise/secondat 300 mm Hg vacuum

Bulb B Bulb C

4 0.036 to 0.8 0.002 0.0006

5 0.12 to 2.4 0.006 0.002

6 0.36 to 8 0.02 0.006

7 1.2 to 24 0.06 0.02

8 3.6 to 80 0.2 0.06

9 12 to 240 0.6 0.2

10 36 to 800 2 0.6

11 120 to 2400 6 2

12 360 to 8000 20 6

13 1200 to 24 000 60 20

14 3600 to 80 000 200 60

9724-R50 Series

Cannon-ManningVacuum Viscometers

Cannon-Manning VacuumCalibrated CMVC SeriesFor measurement of viscosity of highlyviscous materials such as asphalt cement at60°C (140°F) according to ASTM D 2171.Applicable to materials with viscosity range of0.036 to 80 000 poise. Vacuum of 300 mmHg is applied to small arm with timing bulbs;two bulbs are incorporated to extend viscosityrange of viscometer.

� Minimum sample volume 6 mL. Requireliquid bath depth of 180 mm (7.1 inches).

� Provided with certificate of calibration andinstruction sheet. See page 24 forsignificance of expanded uncertainty.

� Holder is not supplied. For holder, see9726-N15 on page 37.

Cannon-Manning VacuumCalibrated CMVC-RO SeriesSame as 9724-H50 series, but withpermanently attached round metal holder, forhole 51 mm (2 inches) in diameter.

Asphalt InstituteVacuum Viscometers

Asphalt Institute VacuumCalibrated AIVC SeriesSimilar to 9724-H50 series, but withgraduated capillary instead of two timingbulbs.

� Minimum sample size 3 mL. Require bathdepth of 180 mm (7.1 inches).

� Note: For sizes 400R and 800R, the“roofing” design is normally used forsegment B, which extends the viscosityrangeto 1 400 000 and 5 800 000 poise,respectively. See ASTM D 2171, Table X2.

� Provided with certificate of calibration andinstruction sheet. See page 24 forsignificance of expanded uncertainty.

� Holder is not supplied. For holder, see9726-N15 on page 37.

Asphalt Institute VacuumCalibrated AIVC-RO SeriesSame as 9724-R50 series, but withpermanently attached round metal holder, forhole 51 mm (2 inches) in diameter.


CANNON®

Vacuum Viscometers

ASTM D 2171

75

Cannon Modified KoppersVacuum Viscometers

Calibrated MKVC SeriesFor measurement of viscosity of asphalts at 60°C(140°F) in accordance with ASTM Standard D 2171.Applicable to materials with viscosity range of 42 to200 000 poise. Two-piece design, with samplereservoir and calibrated capillary. Vacuum of 300 mmHg must be applied to top of capillary tube.

� Minimum sample volume 2 mL. Require liquid bathdepth of 178 mm (7 inches).

� Provided with certificate of calibration andinstruction sheet. See page 24 for significance ofexpanded uncertainty.

� Holder is not supplied. For holder, see 9726-N30.

Removable Holders for Cannon ViscometersAll CANNON viscometer holders fit holes 51 mm (2 inches) in diameter. Rubber holders are made ofneoprene rubber. Plastic holders are self-aligning and hold the viscometer firmly by means of a springclip. Metal holders are also self aligning, and are constructed of chrome-plated machined brass. Allmetal holders are provided with a handle.


9724-W50 Series

Specifications for Cannon ModifiedKoppers Vacuum Viscometers

Size Viscosityrange, poise

Approx. constantpoise/second at300 mm Hg vacuum

at B at C at D

25 42 to 800 2 1 0.7

50 180 to 3200 8 4 3

100 600 to 12 800 32 16 10

200 2400 to 52 000 128 64 40

400 9600 to 200 000 500 250 160

Size Calibrated MKVC Series

25 9724-W50

50 9724-W55

100 9724-W60

200 9724-W65

400 9724-W70

Catalog Numbers ForViscometer Holders

Holder Catalog #

H100 9726-M50

H101 9726-M70

H110 9726-M53

H113 9726-M79

H115 9726-M95

H120 9726-M73

H130 9726-M82

H131 9726-M76

H132 9726-M98

H133 9726-M99

H140 9726-N15

H141 9726-N30

H142 9726-N45

Viscometer Holder Selection Chart

ViscometerType of Holder

Plastic Rubber Metal

Cannon-Fenske Routine H100 H110 H113

Cannon-Fenske Opaque H100 H110 H113

Cannon-Ubbelohde H101 H120 H131

Ubbelohde — — H130

Cannon-Manning Semi-Micro H100 H110 —

Cannon-Ubbelohde Semi-Micro H101 H120 H131

Cannon-Ubbelohde Dilution H101 H120 H131

Cannon-Ubbelohde Four-BulbShear Dilution

H101 H120 H131

Zeitfuchs® Cross-Arm — H115 H132

BS/IP/SL Suspended Level — — H133

BS/IP/SL(S) Suspended Level — — H133

BS/IP/MSL Miniature Suspended Level — — H133

BS/IP/RF U-Tube Reverse Flow — H142 —

Cannon-Manning Vacuum — H140 —

Asphalt Institute Vacuum — H140 —

Modified Koppers Vacuum — H141 —

Cannon-Ubbelohde Filter Stick — H142 —

Viscometer Holders


CANNON®

Vacuum Viscometers & Viscometer Holders

ASTM D 2171

76

The Table below provides kinematic viscosity values for the General Purpose Viscosity Standards from CANNON InstrumentCompany. CANNON certified standards are useful for calibration and verification procedures for all types of viscometers,including glass capillary viscometers, rotational viscometers, falling ball viscometers, cup viscometers, and others. Calibrationor verification with a certified viscosity standard helps to ensure the reliability of measurements made with any viscometer.

For information on CANNON's available in-house testing services please see the inside back cover of this catalog.

Table 1 • Kinematic Viscosity in mm2/s (Centistokes)

CatalogNumber

ViscosityStandard

20°C68°F

25°C77°F

37.78°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

98.89°C210°F

100°C212°F

SUS100°F

SUS210°F

9727-C10 N.4† 0.47 0.45 0.41 0.40 — — — — — — —

9727-C15 N.8† 0.74 0.70 0.61 0.60 — — — — — — —

9727-C20 N1.0† 1.3 1.2 1.0 0.97 0.91 — — — — — —

9727-C22 N2 2.9 2.6 2.1 2.0 1.7 — 1.1 0.95 0.93 — —

9727-C25 S3* 4.6 4.0 3.0 2.9 2.4 — 1.5 1.2 1.2 — —

9727-C27 N4 6.7 5.8 4.2 4.0 3.2 — 1.9 1.5 1.5 — —

9727-C30 S6 11 8.9 6.0 5.7 4.4 — 2.4 1.8 1.8 — —

9727-C31 N7.5 14 12 8.0 7.5 5.8 — 3.1 2.3 2.3 — —

9727-C32 N10 21 17 11 10 7.3 — 3.5 2.5 2.4 — —

9727-C34 N14 30 25 15 14 10 — 5.0 3.5 3.4 — —

9727-C35 S20 44 34 20 18 13 — 5.6 3.9 3.8 100 —

9727-C36 N26 57 46 27 25 18 — 7.9 5.3 5.2 130 —

9727-C37 N35 87 66 35 32 21 — 8.5 5.4 5.3 170 —

9727-C38 N44 110 86 48 44 30 — 12 7.7 7.5 220 —

9727-C40 S60 160 120 60 54 35 — 12 7.7 7.5 280 —

9727-C41 N75 200 150 82 75 50 — 19 12 12 380 —

9727-C42 N100 330 230 110 97 60 — 19 11 11 500 —

9727-C43 N140 400 300 160 140 90 — 31 19 18 720 —

9727-C45 S200 550 400 200 180 110 — 35 22 20 925 105

9727-C46 N250 770 570 280 250 160 — 51 30 29 1300 140

9727-C47 N350 1000 720 340 310 190 — 55 34 32 1570 160

9727-C48 N415 1400 990 470 420 250 — 77 43 41 2180 200

9727-C50 S600‡ 1700 1300 590 520 310 — 93 51 50 — 240

9727-C51 N750 2600 1900 850 750 440 — 130 68 66 — —

9727-C52 N1000 3400 2400 — 940 550 350 150 — 80 — —

9727-C53 N1400 5100 3600 — 1400 820 510 220 — 120 — —

9727-C55 S2000 8300 5300 1900 1600 800 — 160 75 72 — 360

9727-C56 N2500 8400 6000 — 2500 1500 950 430 — 230 — —

9727-C57 N4000 20000 12000 — 3400 1600 850 290 — 120 — —

9727-C58 N5100 28000 18000 — 5100 2500 1300 420 — 170 — —

9727-C60 S8000 41000 25000 8000 6700 3200 — 530 — 215 — —

9727-C61 N10200 58000 36000 — 10200 4900 2500 775 — 300 — —

9727-C62 N15000 77000 47000 — 13000 6100 3000 980 — 360 — —

9727-C63 N18000 103000 64000 — 18000 8500 4300 1320 — 500 — —

9727-C65 S30000 — 79000 27000 22000 11000 — 1700 — 630 — —

* cSt value at –40°C/–40°F (70) also provided

† Incurs additional shipping charges due to low flash point

‡ SFS value at 122°C (150) also provided


Viscosity Standards

CANNON®

General Purpose Viscosity Standards

77

Quality/TraceabilityThe Table below provides dynamic viscosity values for the General Purpose Viscosity Standards from CANNON InstrumentCompany. Viscosities for all standards sold by CANNON are based on the National Institute of Standards and Technology(NIST) value of 1.0016 mPa·s (centipoise) for water at 20°C (68°F).

All CANNON viscosity standards meet the precision specifications of ASTM D 445/446 and ISO 3104/3105, and aretraceable to the NIST (National Institute of Standards and Technology). CANNON viscosity standards are manufactured and/orcertified in CANNON's ISO 9001:2000 registered and A2LA-accredited laboratory. A2LA has accredited CANNON fortechnical competence in the field of calibration (certificate number 1262.01). The accreditation includes the determination ofkinematic and dynamic viscosity (including that of viscosity standards and customer samples) in accordance with ISO/IEC17025-1999. All calibrations are based on the master viscometer procedures detailed in ASTM D 2162.

CANNON has been delegated by NIST to provide U.S. national measurement standards and to issue calibrationand measurement certificates for certified liquid viscosity reference standards.

Table 2 • Dynamic Viscosity in mPa·s (Centipoise)

CatalogNumber

ViscosityStandard

20°C68°F

25°C77°F

37.78°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

98.89°C210°F

100°C212°F

SUS100°F

SUS210°F

9727-C10 N.4† 0.32 0.30 0.28 0.27 — — — — — — —

9727-C15 N.8† 0.64 0.60 0.52 0.51 — — — — — — —

9727-C20 N1.0† 0.93 0.86 0.72 0.70 0.62 — — — — — —

9727-C22 N2 2.2 2.0 1.6 1.5 1.3 — 0.85 0.66 0.65 — —

9727-C25 S3 3.9 3.3 2.5 2.4 1.9 — 1.2 0.90 0.90 — —

9727-C27 N4 5.2 4.5 3.3 3.1 2.5 — 1.4 1.1 1.1 — —

9727-C30 S6 10 8.0 5.3 5.0 3.8 — 2.0 1.5 1.5 — —

9727-C31 N7.5 11 9.5 6.3 5.9 4.5 — 2.4 1.7 1.7 — —

9727-C32 N10 21 16 9.5 8.8 6.3 — 2.9 2.1 2.0 — —

9727-C34 N14 24 20 12 11 8.2 — 3.8 2.7 2.6 — —

9727-C35 S20 37 29 17 15 11 — 4.6 3.0 3.0 100 —

9727-C36 N26 47 37 22 20 14 — 6.2 4.1 4.0 130 —

9727-C37 N35 75 56 30 27 18 — 7.1 4.5 4.4 170 —

9727-C38 N44 92 71 39 36 24 — 9.5 6.0 5.9 220 —

9727-C40 S60 141 104 52 47 30 — 10 6.4 6.2 280 —

9727-C41 N75 160 125 68 61 41 — 16 9.5 9.2 380 —

9727-C42 N100 283 202 95 84 52 — 16 9.5 9.2 500 —

9727-C43 N140 340 250 130 120 74 — 25 15 14 720 —

9727-C45 S200 460 330 160 145 90 — 25 16 14 925 105

9727-C46 N250 650 480 230 210 130 — 41 23 23 1300 140

9727-C47 N350 830 600 280 250 150 — 40 26 24 1570 160

9727-C48 N415 1200 830 390 350 210 — 62 34 33 2180 200

9727-C50 S600‡ 1500 1100 490 440 260 — 75 41 40 — 240

9727-C51 N750 2200 1600 710 620 370 — 100 55 53 — —

9727-C52 N1000 2900 2000 — 800 460 280 120 — 65 — —

9727-C53 N1400 4300 3000 — 1200 680 420 180 — 92 — —

9727-C55 S2000 7300 4700 1700 1400 700 — 140 62 59 — 360

9727-C56 N2500 7100 5100 — 2100 1200 780 350 — 180 — —

9727-C57 N4000 17000 11000 — 2900 1400 730 250 — 100 — —

9727-C58 N5100 25000 16000 — 4500 2100 1100 360 — 140 — —

9727-C60 S8000 33000 20000 7000 5900 2800 — 450 — 200 — —

9727-C61 N10200 52000 32000 — 9000 4200 2100 660 — 250 — —

9727-C62 N15000 68000 41000 — 11000 5400 2600 840 — 320 — —

9727-C63 N18000 92000 57000 — 16000 7500 3800 1140 — 420 — —

9727-C65 S30000 — 71000 23000 20000 9300 — 1400 — 540 — —

† Incurs additional shipping charges due to low flash point.

‡ SFS value at 122°C (150) also provided


Viscosity Standards

CANNON®

General Purpose Viscosity StandardsDynamic Viscosity Values

78

High-Viscosity StandardsThese standards are furnished in a range of viscosities and temperatures which are of particular interest in asphalt viscositydeterminations and the determination of the viscosities of polymers. See ASTM D 2170 and D 2171.

See Table 3 for approximate viscosities. Exact values are supplied with each standard. All data are traceable to the NIST.

Table 3 • High-Viscosity Standards

CatalogNumber

ViscosityStandard

Approximate Viscosity in mPa·s (cP) Kinematic Viscositymm2/s (cSt)

20°C/68°F

25°C/77°F

40°C/104°F

60°C/140°F

135°C/275°F

60°C/140°F

100°C/212°F

9727-E10 N600† — 1100 — 160 17 200 —

9727-C52 N1000* 2900 2000 800 280 — 350 80

9727-E15 N2000† — 4900 — 380 21 440 —

9727-C57 N4000* 17 000 11 000 2900 730 — 850 120

9727-E20 N8000 — 20 000 — 1400 — 1600 —

9727-C62 N15000* 68 000 41 000 11 000 2600 — 3000 360

9727-E25 N30000 130 000 80 000 — 4700 — 5400 —

9727-E27 N62000 — 200 000 — 13 000 — — 1600

9727-E29 N150000 — 420 000 — 24 000 — — 3000

9727-E30 N190000 900 000 520 000 140 000 33 000 — — 4000

9727-E35 N450000 — 1 600 000 — 100 000 2350 — —

9727-E40 N2700000 — 5 300 000 — 340 000 — — —

9727-E42 N2700000SP Dynamic Shear Rheometer (DSR) standard at 52, 58, 64, 70, & 76°C* Additional data provided with these standards are listed in Tables 1 and 2.

† Additional data provided at 135°C.

Low-Temperature StandardsFor Low Temperature Gear Oils (SAE 70W, 75W, 80W and 85W). Also for ATF fluids. See ASTM D 2983.

CatalogNumber

ViscosityStandard Table 4 • Low-Temperature Viscosity Standards

9727-G10 N27B Viscosities in centistokes/centipoise at –40°F (24,000/20,000), –30°F (12,000/10,000),–20°F (6100/5200), –15°F ( 4500/4000), –10°F (3500/3000), and 0°F (2000/1700)

9727-G12 N27C Viscosities in centistokes/centipoise at –40°F (45,000/40,000), –30°F (22,000/20,000),–20°F (12,000/10,000), –15°F (8000/7000), –10°F (6100/5000), and 0°F (3500/3000)

9727-G15 N115B Viscosities in centistokes/centipoise at –20°F (160,000/140,000), –15°F (110,000/95,000),–10°F (75,000/65,000), 0°F (37,000/30,000), +10°F (20,000/17,000), and +20°F (12,000/9500)

9727-G25 N60B 150,000 mPa·s (cP) at –55°C

9727-G30 N120B 150,000 mPa·s (cP) at –40°C

9727-G35 N480B 150,000 mPa·s (cP) at –26°C

9727-G40 N1400B 150,000 mPa·s (cP) at –12°C

9727-G45 N2B* Jet Fuel standard, 8 mm2/s (cSt) at –20°C

9727-G50 N74B 3400 mPa·s (cP) at 0°C

9727-G55 N38B 3100 mPa·s (cP) at –10°C

9727-G60 N25B 8000 mPa·s (cP) at –25°C

9727-G65 N14B 17,000 mPa·s (cP) at –40°C

* Incurs additional shipping charges due to low flash point

For CANNON Mini-Rotary Viscometer (CMRV) (see ASTM D 3829 and ASTM D 4684).

CatalogNumber

ViscosityStandard Table 5 • Approximate Viscosity in mPa·s (Centipoise)

9727-T10 N105B CMRV viscosity standard, 30,000 mPa·s (cP) at –20°C; 56,200 mPa·s (cP) at –25°C

9727-T20 YS-30 Exhibits yield stress of 70 Pa ±35 Pa at –30°C

9727-T25 YS-35 Exhibits yield stress of 70 Pa ±35 Pa at –35°C

Viscosity Standards

High-Viscosity & Low Temperature Viscosity Standards

ASTM D 2170/2171, ASTM D 2983, ASTM D 3829/4684

79

CANNON CL Standards provide certified dynamic viscosity data (in cP or mPa·s) at temperatures from –5°C to –35°C. Thesestandards are used to calibrate the CANNON Cold-Cranking Simulator (CCS) oil testing (see ASTM D 5293 and SAESpecification J300).

Table 6 • Dynamic Viscosity in mPa·s (Centipoise)

CatalogNumber

ViscosityStandard* –5°C –10°C –15°C –20°C –25°C –30°C –35°C

9727-N02 CL080 — — — — — — 800

9727-N04 CL090 — — — — — — 1200

9727-N06 CL100 (CL10) — — — — — 900 1700

9727-N07 CL110 — — — — — 1400 2500

9727-N08 CL120 (CL12) — — — — 800 1600 3200

9727-N09 CL130 — — — — 1500 2700 4800

9727-N10 CL140 (CL14) — — — 800 1600 3300 7000

9727-N11 CL150 — — — 1200 2500 4500 8000

9727-N12 CL160 (CL16) — — — 1200 2500 5500 11000

9727-N13 CL170 — — 1100 1800 3500 6200 11000

9727-N14 CL190 (CL19) — — 900 1800 3500 7400 17200

9727-N16 CL200 — — 1200 2400 4300 7400 13000

9727-N18 CL220 (CL22) — — 1300 2500 5000 11000 25000

9727-N20 CL240 — — 1700 3400 6000 10000 20000

9727-N22 CL250 (CL25) — 900 1800 3500 7300 15900 33000

9727-N24 CL260 — 1200 2500 4400 7200 14000 —

9727-N26 CL280 (CL28) — 1300 2500 5000 9300 21000 50000

9727-N28 CL300 — 1700 3500 6000 11000 18000 —

9727-N30 CL320 (CL32) — 1800 3500 7300 15900 32000 —

9727-N31 CL340 — 2500 4200 7000 12000 — —

9727-N32 CL380 (CL38) 1600 2900 5800 13000 26000 — —

9727-N33 CL420 — 5000 8500 15000 — — —

9727-N34 CL480 (CL48) 2300 4500 9500 21000 — — —

9727-N35 CL530 — 5900 10000 18000 — — —

9727-N36 CL600 (CL60) 3700 7300 15600 — — — —

9727-N37 CL680 — 9500 — — — — —

9727-N38 CL740 (CL74) 6000 12000 — — — — —

9727-N43 Set of 14 Set of CCS-2050/2100 Low Temp Standards (includes CL10, CL12, CL14, CL16, CL19, CL22, CL25(2),CL28, CL32, CL38, CL48, CL60, & CL74)

9727-N42 Set of 8 Set of CCS Low Temp Standards (includes CL14, CL19, CL22, CL25, CL28, CL32, CL48, & CL74)

* CL Standards nomenclature has changed. The previous standard names are indicated in parentheses.

Viscosity Standards

CANNON®

CCS Viscosity Standards

NIST will delegate responsibility for U.S. national standards for certified liquidviscosity reference standards to the CANNON Instrument Company.

James R. Whetstone, ChiefProcess Measurements Division/Chemical Science and Technology LaboratoryNational Institute of Standards and TechnologyJanuary 6, 2003

"

"

80

Table 7 • Certified Data at 25°C

CatalogNumber

ViscosityStandard

Kinematicviscositymm2/s(cSt)

Zahn Cup Shell Cup Ford Cup

Size Draintime,sec

Size Draintime,sec

Size Draintime,sec

9727-W10 C6 8.9 ——

——

12

5220

——

——

9727-W12 C10 17 1—

45—

22¼

3522

1—

70—

9727-W15 C20 34 12—

6024—

22½3

644024

2——

42——

9727-W20 C35 66 2——

33——

2½3

3½

744632

23—

6435—

9727-W25 C60 120 2—

48—

3½4

5736

34

5836

9727-W30 C100 230 34

2721

45

6836

4—

64—

9727-W35 C200 460 34

4736

56

7229

5—

40—

9727-W40 C350 850 45

6237

6—

53—

5—

72—

9727-W45 C600 1300 5 54 — — — —

Viscosity Standardsfor Zahn, Shell,& Ford Cups

Approximate valuesare shown in Table 7.Exact valuescalculated from theequations in Table VIIIare supplied witheach standard.

For more informationon cups, contactCannon InstrumentCompany.

Table 8 • Ranges of Viscosity Cups

CupNumber

Equations‡ wheret = Time of flow, seconds

� = kinematic viscosity, mm2/s

Drain timeseconds

Kinematic viscositycentistokes

min max min max

Zahn Cups (See ASTM D 4212)

1 � = 1.1 (t – 29) 35 80 5 60

2 � = 3.5 (t – 14) 20 80 20 250

3 � = 11.7 (t – 7.5) 20 80 100 800

4 � = 14.8 (t – 5) 20 80 200 1200

5 � = 23t 20 80 400 1800

Shell Cups (See ASTM D 4212)

1 � = 0.226 (t – 13) 20 80 2 20

2 � = 0.576 (t – 5) 20 80 10 50

2½ � = 0.925 (t – 3) 20 80 20 80

3 � = 1.51 (t – 2) 20 80 30 120

3½ � = 2.17 (t – 1.5) 20 80 40 170

4 � = 3.45 (t – 1) 20 80 70 270

5 � = 6.5 (t – 1) 20 80 125 520

6 � = 16.2 (t – 0.5) 20 80 320 1300

Ford Cups (See ASTM D 1200)

1 � = 0.49 (t – 35.0) 55 100 10 35

2 � = 1.44 (t – 18.0) 40 100 25 120

3 � = 2.31 (t – 6.58) 20 100 49 220

4 � = 3.85 (t – 4.49) 20 100 70 370

5 � = 12.1 (t – 2.00) 20 100 200 1200‡ While the equations in Table VIII are widely used, the equation � = at - b/t is often more applicable,

especially at low flow times and low kinematic viscosity.

See page 43!

Need SAEViscosity Check Oils?

Equationsfor Zahn, Shell,& Ford CupsEquations for conversion ofkinematic viscosity or viscosity intoother viscometric units are givenhere. All data must be at 25°C. Notethat the equations apply onlybetween the minimum andmaximum drain times shown.

Viscosity Standards

CANNON®

Cup Viscosity Standards

81

Table 10 • Certified Data at 25°CCatalogNumber

ViscosityStandard Viscosity (Centipoise) Krebs Unit (KU)

9727-Y10 S200(KU)9727-Y15 N350(KU)9727-Y20 K400(KU) 940 849727-Y25 S600(KU) 1060 889727-Y30 N1000(KU) 2000 106

Viscosity Standardsfor Thomas®-Stormer®

ViscometerThe KREBS UNIT (KU) is often used forTHOMAS-STORMER Viscometers.

CatalogNumber

ViscosityStandard Table 9 • High-Temperature Standards

9727-U50 HT39 2.0 mPa·s (cP) at 150°C, 4.7 mPa·s (cP) at 100°C9727-U55 HT75 2.7 mPa·s (cP) at 150°C, 7.0 mPa·s (cP) at 100°C9727-U60 HT150 3.7 mPa·s (cP) at 150°C, 10.5 mPa·s (cP) at 100°C9727-U65 HT240 5.0 mPa·s (cP) at 150°C, 15.4 mPa·s (cP) at 100°C9727-U70 HT390 7.0 mPa·s (cP) at 150°C, 23.5 mPa·s (cP) at 100°C9727-U92 HTNN-1 Non-Newtonian standard, 3.6 mPa·s (cP) at 150°C and 106s-1

9727-U94 HTNN-2 Non-Newtonian standard, 3.1 mPa·s (cP) at 150°C and 106s-1

High-Temperature StandardsFor High-Temperature High-ShearViscometer measurements at 150°C and106s-1 shear rate.See ASTM D 5481.

Table 11 • Silicone Viscosity Standards

CatalogNumber

ViscosityStandard

ApproximateViscosity mPa·s

(Centipoise)25°C (77°F)

9727-Z10 RT5 4.99727-Z14 RT10 9.49727-Z18 RT50 489727-Z22 RT100 969727-Z26 RT500 4809727-Z30 RT1000 9609727-Z34 RT5000 48009727-Z38 RT12500 120009727-Z42 RT30000 290009727-Z46 RT60000 580009727-Z50 RT100000 97000

Silicone Viscosity Standardsfor Rotational ViscometersCANNON silicone standards are intended for calibration of Brookfield typerotational viscometers, such as the 2020 Series Rotary Viscometers (page 51)offered by CANNON. Viscosity data at 20, 23, 24, 25, 26, 27, and 40°C isprovided. CANNON has been granted ISO 9001 registration for themanufacture and certification of viscosity standards, including the siliconestandards listed here.

Viscosities for all silicone standards sold by CANNON are based on theNational Institute of Standards and Technology (NIST) value of 1.0016 mPa•s(centipoise) for water at 20°C (68°F). All silicone standards are traceable to theNIST. Silicone standards are sold in 500 mL bottles.Note: The listed silicone standards are intended for use with rotational viscometers only.Silicone standards are not recommended for glass capillary viscometers (including vacuumviscometers), metal cup-type viscometers (such as ISO, Zahn, Ford, Shell, and Fisher cups),or any other viscometers providing kinematic viscosity – CANNON hydrocarbon-based oilstandards should be used for these types of viscometers.

Table 12 • Flash Point Reference Materials

CatalogNumber Product ID

ASTM D 56Nominal Flash

Point (°C)


Point (°C)


Point (°C)9727-A10 FPRM10* 50 – 559727-A15 FPRM11* 66 – 729727-A20 FPRM14 – 116 1139727-A25 FPRM16 – 137 1329727-A30 FPRM2D – 163 1559727-A35 FPRM4D – 224 218

*Incurs additional shipping charges due to low flash point

Flash Point Reference MaterialsCANNON Instrument Company can now provideFlash Point Reference Materials for calibrating FlashPoint Testers. A total of six different standards areavailable for the following ASTM methods: ASTM D56, ASTM D 92, and ASTM D 93. The dataprovided for each standard includes the averageflash point for the lot and the standard deviationobserved from 20 tests in 10 different laboratories.Nominal flash points for the various standards areshown in the accompanying table. The fourstandards with lower flash points are made from highpurity alkane materials, while the two standards withhigher flash points are made from narrowdistributions of decane oligomers. Flash PointStandards are sold in 200 mL bottles (155 g).

Viscosity Standards

CANNON® Viscosity Standards & Flash Point Reference Materials

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330 61.2 600 77

The CANNON DVR 1000 Series Digital Vacuum Regulators

� Solid-State Components—Contains No Mercury� Preset for Vacuum Viscometry per ASTM D 2171� Horizontal or Vertical Configuration� Convenient Keypad Controls

The CANNON DVR 1000 Series Digital Vacuum Regulators are designed for precise measurement and control of vacuum at300 mm Hg below atmospheric pressure. Unlike other vacuum regulators, the solid-state DVR-1000 and DVR-1500 modelsuse no mercury.

The DVR meter displays the amount of vacuum in mm/Hg or one of nine other units of measurement selected using a keypadon the meter.

In asphalt laboratories the Digital Vacuum Regulator (DVR) may be used in conjunctionwith Cannon-Manning, Asphalt Institute, and Modified Koppers vacuum viscometers formeasurement of highly viscous materials such as asphalt cement at 60°C (140°F) accordingto ASTM D 2171. The DVR is also useful in other laboratory systems where accuratemeasurement and control of vacuum is required.

Two basic versions of the DVR are available. The DVR-1500 is equipped with an internalvacuum pump and does not require an external vacuum source. The DVR-1000 uses thecustomer’s in-house vacuum system.

The internal set points for the instrument gauge are preset at CANNON to regulatevacuum at 300 ± 0.5 mm Hg below atmospheric pressure (the vacuum required byASTM D 2171). These set points may be altered to fit the user’s specific needs within theDVR’s operating range of 28 to 410 mmHg below atmospheric pressure.

Both the DVR-1000 and DVR-1500 areavailable in either horizontal or verticalconfigurations (the horizontal version willsupport the weight of a constanttemperature bath like the CANNONCT-1000 or CT-2000).

The instrument housing is made of durableenameled steel and is supported on non-sliprubber feet.

DVR 1000 Series Specifications

Dimensions: 470 mm wide x 458 mm deep x 172 mmhigh (18.5 x 18 x 6.75 inches) [in thehorizontal position]

Weight: 20 kg (45 lbs)

Range: Preset at 300 mm Hg below atmosphericpressure, but may be adjusted to accuratelycontrol from 28 mm to 410 mm Hg belowatmospheric pressure

Reading Accuracy: ± 0.05% of reading ± the least significantdigit (includes combined effects of linearity,repeatability, hysteresis, and temperature)[NIST certification is supplied]

Vacuum RegulationAccuracy:

± 0.5 mm Hg (as required by ASTM D2171)

Operating Temperature: 0 to 40°C (32 to 104°F)

Upper/Lower Safety Limit: 746 mm Hg below atmospheric pressure

Order Information


9726-T20 DVR-1000H (DVR without vacuum pump,horizontal orientation, 120V, 100 watts)

9726-T23 DVR-1000HF (DVR without vacuum pump,horizontal orientation, 240V, 100 watts)

9726-T25 DVR-1000V (DVR without vacuum pump,vertical orientation, 120V, 100 watts)

9726-T27 DVR-1000VF (DVR without vacuum pump,vertical orientation, 240V, 100 watts)

9726-T60 DVR-1500H (DVR with vacuum pump,horizontal orientation, 120V, 175 watts)

9726-T63 DVR-1500HF (DVR with vacuum pump,horizontal orientation, 240V, 175 watts)

9726-T65 DVR-1500V (DVR with vacuum pump,vertical orientation, 120V, 175 watts)

9726-T67 DVR-1500VF (DVR with vacuum pump,vertical orientation, 240V, 175 watts)

Asphalt Industry Test Equipment

CANNON®

DVR 1000 Series Digital Vacuum Regulators

ASTM D 2171

83

� Ideal for Laboratory and Pilot ScaleDistillation Columns

� High Efficiency Design� Unique Wetting Properties� Atmospheric and Reduced Pressure

Distillation Applications

Pro-Pak is a high efficiency distillation column packingwith unique wetting properties. Applications rangefrom laboratory and pilot plant distillation columns tothose used in small manufacturing plants. Pro-Pak isself wetting, so equilibrium time is reduced —

distillations can be stopped and started without lengthydelay. The entire surface of the packing is available formass transfer, contributing to its high efficiency. Theshape of the packing eliminates interlocking andmakes filling and emptying the column as easy aspouring water.

Pro-Pak is formed from metal ribbon through whichmore than 1000 tiny holes per square inch have beenpunched. As the points of the die push through themetal, jagged burrs are formed on the reverse side of

the ribbon. Pro-Pak’s self-wetting properties derive from a rectangular network of capillaries on the surface of the metal,produced by the combined effect of the holes in the ribbon and the roughness of the burrs. These properties ensure thatPro-Pak stays wet in service in the distillation column and retains its high efficiency. Because the surface area of the packingremains effective under low liquid loadings, high column efficiency is maintained at vapor velocities very much lower than theflooding velocity.

Pro-Pak can be used for both atmospheric and reduced pressure distillations down to 10 mm Hg condenser pressure. As theoperating pressure decreases, efficiency increases. The HETP (height equal to a theoretical plate) varies from 0.5 inch to 1.4inch in a 1-inch diameter column, depending on operating pressure and reflux rate.

The large surface area made effective by the wettability of Pro-Pak allows for efficient mass transfer between the liquid andvapor phases. The surface area is approximately 576 square feet per cubic foot for the 0.16-inch size and 372 square feet percubic foot for the 0.24-inch size. The packing factor is 693 for the 0.16-inch size and 420 for the 0.24-inch size.

High free space is especially important in vacuum distillation (for reduction of pressure drop) and in extractive distillation andabsorption (where high liquid or vapor loading is common). Pro-Pak has high free space: 94% for the 0.16-inch size and 96%for the 0.24-inch size. Because of its high free space, Pro-Pak has a high flood rate.

In addition to type 316 stainless steel packing, listed below, Pro-Pak is also available in Monel, nickel, and other metals onspecial order. Discounts are provided for bulk quantities.

CANNON manufactures special interdistributor screens and hold down screens that provide optimum efficiency for Pro-Pakcolumns. These screens are manufactured on a custom basis to fit any specified column diameter.

Our Pro-Pak technical bulletin contains additional information. A free sample of Pro-Pak can also be supplied. Please contactCANNON to receive a free copy of the Pro-Pak bulletin and a sample of the packing.

CANNON Pro-Pak Distillation Packing

Order Information


3947-A20 316 Stainless Steel Packing, 0.16-inch. 1 L

3947-A30 316 Stainless Steel Packing, 0.16-inch. cubic foot

3947-A60 316 Stainless Steel Packing, 0.24-inch. 1 L

3947-A70 316 Stainless Steel Packing, 0.24-inch. cubic foot Interdistributor& Hold-Down Screens

also Available!

Pro-Pak®

CANNON®

Pro-Pak Distillation Packing

84

UVS®

Viscosity Systems

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Viscosity Systems

Measuring Instruments

®UVS basic

®UVS BASIC is the new introduction viscosity measurement device which is capable of determining the intrinsic viscosity of polymers as well as the kinematic viscosity of mineral oil products in compliance with DIN51562-FF, ASTM D 445 and DIN ISO EN 3105 and all polymere standards (see table typical examples)The measuring instrument not only saves place of work, but also measures automatically precise and reproducible processing times.

®The UVS BASIC consists of the measuring ® unit UVS MD.

®The UVS BASIC is expandable.

It is always possible to use in the case either ® another unit of measurement UVS MD or the

®controlled vacuum pump UVS DRAIN for automatic sample exhauster. This exhauster can also be integrated in a sample changer SC8. Thus, the instrument becomes a fully automatic machine for polymer applications.

®All UVS measuring instruments work independently and are able to operate multiple devices with a PC.

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Configurations UVS basic

Measuring points

Sample filling

Cleaning solvents per MP

Waste bottles

Measuring samples at same time

Max. positions

UVS basic MD 1 Manual Manual

X 0 1 1

UVS basic MD / MD 2 Manual Manual

X 0 2 2

UVS basic MD + UVS basic MD / MD 3 Manual Manual

X 0 3 3

2 x UVS basic MD / MD 4 Manual Manual

X 0 4 4

1 x UVS basic MD / Drain 1 Manual Semiauto

X 1 1 1

1 x UVS basic MD / Drain + SC8 1 Automatic Automatic

2 1 1 24

1 x UVS basic MD / MD + SC8 + UVS waste

2 Automatic Automatic

1 1 ~1.5 24

1 x UVS basic MD / MD + 2 x SC8 + UVS waste


2 1 2 48



1 (2) 1/2 ~2.5 48



4 1 4 96



8 1 8 192

other combinations possible

Viscosity Systems


®UVS basic

UVS BASIC, Configuration

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Viscosity Systems


®UVS MD

UVS MD, the measuring device for flow time measuring of Newtonian fluids in common capillary viscometers with precision to the millisecond. The UVS MD is suitable for all measurements of polymer solutions and mineral oils products. Meniscus detection is effected optical through light barriers or with thermistors by determining the heat conductance. The optical measurement amplifier supports the scanning of a third safety light barrier (Triple Detection)

UVS MD, the measuring device for flow time measuring of Newtonian fluids in common capillary viscometers with precision to the millisecond. The UVS MD is suitable for all measurements of polymer solutions and mineral oils products. Meniscus detection is effected optical through light barriers or with thermistors by determining the heat conductance. The optical measurement amplifier supports the scanning of a third safety light barrier (Triple Detection)

UVS Drain, the device is responsible for automated cleaning. This device controls the discharging of the sample, rinsing with solvent, drying and discharging solvent to the waste bottle. Sensor detection for a full waste bottle complies safety requirements. The cleaning process can be optimzed by configuration to save time and get best results.

88

Viscosity Systems


®UVS MD

UVS MD, Technical Data

Measuring range (time) Time 0.100 to 9999.000 s Resolution 0.001 s Accuracy (flow time : 0 - 100s) ± 0.001 s Accuracy (flow time : > 100 s) <10 ppm Ambient temp. error of time base (15 - 35°C) < 4 ppm

Measuring range (viscosity) Pressure mode 0.35 to 1000 mm

2/s

Suction mode 0.35 to 10000 mm2/s

Pumping pressure power + 350 hPa Pumping suction power - 350 hPa

Configuration Parameters (with PC) Tempering period 0 to 20 min Additional quite tempering period 0 to 20 min No. of measurements 1 to 10 (250) pump power range 1 to 100 % Rising time (ramp) of pump power 0.02 to 2 % /s

Connections UVS LB triple light barrier 5 pin connector with screw lock SI Analytics light barriers with adapter cable TC-Viscometers 4 pin connector with screw lock Viscometer tubes M12x1,25 Communication backplane DIN 41612

Size

Dimensions (W x H x D) 70 x 128 x 170 mm Weight 2 kg

Materials Pumps PTFE, FFKM, PPS housing Valves ETFE, FFKM Cover anodized aluminium Internal tubes, seals PTFE, ETFE

89

Viscosity Systems

Sample Changer

Sc8

SC8 the sample changer with 8 and respectively 24 positions in dependance of sample bottle size. With integration of a SC8 the UVS Basic becomes a fully automatic machine. The sampler can serve one or two viscometers. In case of two viscometers the filling and rinsing procedure works in an alternating operation mode. The turntable is available for common laboratory 100 ml sample bottles, 50 ml centrifugal tubes, 30 ml disposable PP beakers and 20 ml micro tubes. An adaption of individual sample vessels are possible on request. With the stage of extension - 2x UVS Basic and 4x SC8 - the system have up to 96 sample positions and can measure 80 samples per hour. The rinsing of the sample transfer tube and piston pump is realized with build-in ports for a rinsing and a drying solvent. Additional the recommended rinsing with next sample is also configurable. The used valves are chemical resistant and have a lean dead volume. Sample filtration with filter backwashing is available as an option for low viscous samples.

! Sensor for recognition of empty sample flasks or unused positions

! Inputs for fluid level sensor! Configurable sample transfer speed

90

Viscosity Systems

Viscometer baths

Chiller Viscosity Systems

Viscometer baths

Chiller

JB 18 TB 2 -2V (4 V)

Our viscometer baths are in compliance with DIN 51 562 (Part 1) and ASTM D 445.

Each our viscometer bath models are for use with temperatures between +10 °C and

+100 °C.For working temperatures below 35°C the

chiller HMC is recommended to maintain the temperature constancy.

The models JB18 are able to work at high temperature conditions till 150°C. The resolution of 0.01°C is displayed. Other temperatures and bath sizes are on request deliverable.

JB 18 TB 2 -2V (4 V)

Our viscometer baths are in compliance with DIN 51 562 (Part 1) and ASTM D 445.

Each our viscometer bath models are for use with temperatures between +10 °C and

+100 °C.For working temperatures below 35°C the

chiller HMC is recommended to maintain the temperature constancy.

The models JB18 are able to work at high temperature conditions till 150°C. The resolution of 0.01°C is displayed. Other temperatures and bath sizes are on request deliverable.

HMC91

Viscosity Systems Control and Evaluation Software

VisKey - The Key to Viscosity

PCalculation of kinematic, dynamic, relative and intrinsic viscosity

PDetermination of capillary constant by system calibration, blank value (t0), viscosity index, enzyme kinetic, dilution viscoity

PFormula editor for individual calculationsPNo limitation of method numbersPEach measuring station can work in a

different methodPViscometer databasePUser level access controlled software with

three levels: administrator, authorized user, worker

PAccess restrictions can be disabledPMultitasking operations – each measuring

point works independentPPossibility to enter sample ID using a

barcode scannerPLogbook features, CFR21 part 11

compliantPResult database with screening and sorting

functionsPSample changer functions like priority

sample, subsequent addition or removal of samples

PSupported operating system Windows XP, Vista, Win7, Win8

PSupported periphery: UVS Basic, UVS Tower, UVS Clean, SC8 92

Viscosity Systems

Light Barrier

®UVS LB Viscosity Systems

Light Barrier

®UVS LB

UVS LB, the Triple Detection light barrier made of PVDF.The stand with integrated viscometer fixation is suited for all common capillaries. Viscometers. with fixing bracket are also usable. The light barriers are working with infrared light and are able to detect certainly the meniscus pass. The third and topmost light barrier is used as "over suck" protection. For measurements with Micro-Ubbelohde viscometers this light barrier can increases the reproducibility of values through constant kept start conditions.Additional fixation holder for Canon-Fenske Routine, Canon-Fenske Ubbelohde, Witeg-, Paragon-, Tamson-Ubbelohde available.

93

Viscosity Systems

ViscometersViscometers

Viscometer type

Ubbelohde Micro Ubbelohde

TC Ubbelohde

TC Micro Ubbelohde

Micro Ostwald

Cannon-Fenske routine

Cannon-Fenske

reverse flow

Application characteristics

Polymer solutions

++

+

-

-

+

+

-

Polymer solutions Ultra short flowtimes

+

++

-

-

+

-

-

Mineraloil transparent

++

++

++

++

+

+

+

Mineraloil opaque

-

-

++

++

-

-

++*

Foaming liquids

o

o

o

o

+

+

o

Liquid mixture with highly volatile components

+

+

+

+

++

++

o

sample volume (ml)

15-20*

3-4

18-22

3-4

2

7-10

12

Exact volume necessary

no

no

no

no

yes

(yes)

yes

*4-leg re-

commended 18-22 ml

Short flowtime

Short flowtime

* only manual measurement

Ubbelohde with Thermistor Cannon-Fenske Routine Micro-Ubbelohde ASTM-Ubbelohde

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TV2000 TV4000 TV7000

A S T M E q u i p m e n t

1.6 ASTM D445 High Temperature Viscosity Baths - TV SeriesASTM D445 - ASTM D2162 - ASTM D2170 - ISO/EN 3104 - IP 71 - DIN 51366

This test method specifies a procedure for the determination of the kinematic viscosity of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer.

Main characteristicsBath can be operated from ambient +5°C up to +230°C (41..446°F). With the use of the built-in cooling coil and an external Tamson cooling circulator, span lies 5°C above the temperature of the cold flow of the external cooling circulator. The TV2000, TV4000(DC), and TV7000DC have a bath volume of 20, 40, and 70 litres respectively. The TV2000 has a cover with three openings and lids. The TV4000(DC) and TV7000DC have a cover with seven openings and lids. These openings accommodate glass capillary viscometers in viscometer holders. The TV4000DC has the same specifications as the TV4000, but with a unique stability of 0.002°C at 40°C. The TV7000DC is used to calibrate long thermometers, to calibrate master viscometers or for oxidation stability tests. A bath overflow outlet protects from expanding bath oil when the bath filling is expanding at higher temperatures. A bath drain is standard included. The bath is fitted with a double window of which the front pane is detachable for cleaning purposes.

Range …230°C/…446°F

Reading Standard °C, °F on request

Used materials inside bath Stainless steel 304, brass bearings

Setting 0.01°C

Offset ± 0.01°C (optional 0.005°C)

Stability ± 0.01°C 0.01°C0.002°C @40°C0.005°C @100°C0.010°C @150°C

0.01°C

Heating 2800 W

Heaters 2

Bath volume 20 L 40 L 40 L 70 L

Number of Ø 51 mm lids 3 (4 optional) 4 + 3 (4 + 4 optional)

Window 140 x 285 mm 270 x 285 mm 270 x 585 mm

Opening bath (without cover) 130 x 165 mm 260 x 240 mm 260 x 240 mm

Depth bath 300 mm 300 mm 630 mm

TV2000 P/N 00T0782 (230V/50-60Hz) • P/N 00T0784 (115V/60Hz) TV4000 P/N 00T0772 (230V/50-60Hz) • P/N 00T0774 (115V/60Hz) TV4000DC P/N 00T0802 (230V/50-60Hz) • P/N 00T0804 (115V/60Hz) TV7000DC P/N 00T0796 (230V/50-60Hz) • P/N 00T0798 (115V/60Hz)

TV4000

TV7000DCTV4000DCTV4000TV2000

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TV2500 TV3500

1.7 ASTM D445 High Temperature Viscosity Baths - TV2500 and TV3500

ASTM D445 - ASTM D2162 - ISO/EN 3104 - IP 71 - DIN 51366 - ASTM D1298

Main CharacteristicsThe TV2500 or TV3500 bath can be operated from ambient +5°C up to +120°C (41..248°F). With the use of the built-in cooling coil and an external Tamson cooling circulator, span lies 5°C above the temperature of the cold flow of the external cooling circulator. The TV2500 has a bath volume of 25 liters. The TV3500 has a bath volume of 35 liters. The TV2500 offers two rows of two openings with lids. The TV3500 can be equipped with a cover with nine openings and lids. These openings will accommodate glass capillary viscometers in viscometer holders. A bath overflow outlet protects from expanding bath fluid when the bath filling is too high. A bath drain is standard included.

TV2500 TV3500

Range …120°C/…248°F


Used materials inside bath Stainless steel 304

Setting 0.01°C

Stability ± 0.02°C

Heating 1400 W

Heaters 1

Bath volume 25 L 35 L

Number of lids 4 9

Opening lid Ø51 mm

Window 230 x 300 mmOpening bath (without cover) 185 x 155 mm 400 x 120 mm

Depth bath 300 mm 320 mm

TV2500 P/N 19T1003 (230V/50-60Hz) • P/N 19T1004 (115V/60Hz)

For ASTM D1298 (density by hydrometer) you can use the TV2500 in combination with a special cover with three holes (P/N 03T2119) and a TLC10-3 cooling circulator. Please also see section ‘ASTM D1298 – Density by Hydrometer’.

TV3500

TV2500 for ASTM D1298

TV3500 P/N 19T1005 (230V/50-60Hz) • P/N 19T1006 (115V/60Hz)

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TV12

1.8 ASTM D445 High Temperature Viscosity Baths - TV12ASTM D445 - ISO/EN 3104 - IP 71 - DIN 51366

Main CharacteristicsThe TV12 is a unique viscosity bath with a small footprint. The TV12 can be operated from ambient +5°C up to +120°C (41..248°F). With the use of the built-in cooling coil and an external Tamson cooling circulator, span lies 5°C above the temperature of the cold flow of external cooling circulator. The TV12 has a bath volume of only 12 liters and a unique stability of 0.005°C. The TV12 offers one row of four openings with lids. These openings will accommodate glass capillary viscometers in viscometer holders. A permanent LED light is located in the top plate to supply clear light and guarantees optimal visibility inside the bath. A bath overflow outlet protects from expanding bath fluid when the bath filling is too high. A bath drain is standard included. The bath is fitted with a double window of which the front pane is detachable for cleaning purposes.

Range …120°C/…248°F



Setting 0.01°C

Offset ± 0.01°C


Heating 1280 W

Heaters 2

Bath volume 12..15 L

Number of lids 4

Opening lid Ø 51 mm

Window 140 x 285 mm

Opening bath 248 x 73 mm

Depth bath 300 mm

TV12 P/N 00T0400 (230V/50-60Hz) • P/N 00T0405 (115V/60Hz)

For spare parts, options and accessories, please see our TV12LT.

PowerPoint with more details at

www.tamson.com

TV12

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C a l i b r a t i o n B a t h s & M e a s u r e m e n t

TV12LT

1.10 ASTM D445 Low Temperature Viscosity Bath: TV12LTASTM D445 - ISO/EN 3104 - IP 71 - DIN 51366 - IP EM PJ - IEC 61868

This test method specifies a procedure for the determination of the kinematic viscosity of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer.

Main CharacteristicsThe TV12LT with integrated cooling is a unique viscosity bath with a small footprint. It can be operated from -42°C up to +20°C (-40..68°F). Ranges from -42°C up to +80°C and -50°C up to +20°C are available. The TV12LT has a small bath volume of 15 liters and a unique temperature stability. The TV12LT offers one row of four openings with lids. These openings will accommodate glass capillary viscometers in viscometer holders. A permanent LED light is located in the top plate to supply clear light and guarantees optimal visibility inside the bath. A bath overflow outlet protects from expanding bath fluid when the bath filling is too high. A bath drain is standard included. The bath is fitted with two windows of which the front panel is detachable for cleaning purposes. TV12LT is specially designed for kinematic viscosity testing of aviation fuels at sub zero temperatures. The TV12LT also is suitable to calibrate thermometers or other sensors.

Range -42..+20°C*/-43.6..+68°F



Setting 0.01°C

Offset ± 0.01°C (optional 0.005°C)


Heating 1200 W

Heaters 2

Bath volume 15....18 L

Number of lids 4

Window 255 x 230 mm



TV12LT P/N 00T0410 (230V/50Hz) • P/N 00T0420 (230V/60Hz) • P/N 00T0415 (115V/60Hz)

* Range from -42°C up to +80°C TV12LT P/N 00T0425 (230V/50Hz) • P/N 00T0435 (230V/60Hz) • P/N 00T0430 (115V/60Hz)

* Range from -50°C up to +20°C TV12LT P/N 00T0470 (230V/50Hz) • P/N 00T0480 (230V/60Hz) • P/N 00T0475 (115V/60Hz)

TV12LT


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C a l i b r a t i o n B a t h s & M e a s u r e m e n t

TV4000LT TV70000LT


1.11 ASTM D445 Low Temperature Viscosity Baths 40&70 litresASTM D445 - ASTM D2162 - ISO/EN 3104 - IP 71 - DIN 51366

Main CharacteristicsThe TV4000LT and TV7000LT are unique visibility baths with wide dimensions. Working temperature ranges from -40°C up to +100°C. The integrated cooling system is able to lower the temperature of the bath content down to -40°C within approximately two hours. The cooling power can be controlled over several stages, so that the heat removal capacity is trimmed to the desired set point temperature, saving up to 50% of energy. Due to its wide temperature range, the bath can be used for multiple purposes varying from low temperature viscosity measurement to calibration of sensors and thermometers. The large windows show the bath contents clearly. The windows are heated preventing built up of condensate. The maximum temperature lies around +100°C. Overall accuracy is better than ± 0.02°C over the whole temperature range. Ambient temperature drifts <0.003°C/°C. The homogeneity is better than 0.02°C. Drift, accuracy and homogeneousness were measured with methanol as bath medium and are true min-max values found over eight hours. The TV7000LT can be used to calibrate long thermometers or to calibrate hydrometers.

TV4000LT

TV4000LT

Range -40..100°C/-40..212°F



Setting 0.01°C

Offset ± 0.01°C


Heating 2000 W

Heaters 2

Bath volume 40 L 70 L

Number of lids 4 + 3 (4 + 4 optional)

Window 270 * 285 mm 270 * 585 mm



Depth bath 300 mm 600 mm

TV4000LT P/N 00T0460 (230V/50Hz) TV7000LT P/N 00T0450 (230V/50Hz)

TV7000LT

99

TLV25


1.12 ASTM D445 Ultra Low Temperature Viscosity BathASTM D445 - ISO/EN 3104 - IP 71 - DIN 51366 - ASTM D2532

Main CharacteristicsThe TLV25 system contains a 25 litres Dewar flask. The fluid in this flask must permanently be cooled by a separate immersion cooler when using at temperatures below ambient. The temperature set point is maintained via a microprocessor controlled heating element. When using the TCC-IC, a minimum working temperatures of -80°C can be reached. All presented data is measured by using a TLV25 filled with methanol and a TCC-IC immersion cooler. At the minimum temperature, the provided heat removal is still enough to maintain stable tem pera-ture control, even when glass capillary viscometers are placed in the bath. The systems accuracy is better than the requirements of ASTM D445 and ISO 3104. The bath is illuminated by a fluor escent light built-in behind the Dewar flask. The top lid has a turn table construction with three openings and three lids. By turning the lid, the immersed viscometer can be positioned in front of the window. This window is heated to keep clear sight at sub zero temperatures. The set point can be set in steps of 0.1°C from -90°C up to +60°C (-130..140°F). Overall accuracy is better than ± 0.04K. Set-up of TLV25 and TCC-IC can also be used for ASTM D2532.

TLV25Range -80..60°C/-130…140°F



Setting 0.1°C

Offset ± 0.1°C


Heating 1500 W

Heaters 1

Bath volume 25 L

Number of lids 3


Opening bath Ø 161 mm

Depth bath 400 mm

TLV25 P/N 00T0650 (230V/50-60Hz) • P/N 00T0780 (115V/60Hz)

Please also see our ‘TCC-IC’ where you will find the necessary TCC-IC immersion cooler for the TLV25.

Necessary options TLV25P/N 00T0300 TCC-IC to reach -80°C (230V/50HZ) •

P/N 00T0301 TCC-IC to reach -80°C (230V/60HZ) •

Accessories TLV25P/N 10T6066 Viscohanger •

P/N 10T6090 8 Channel stop-watch •

P/N 00T0239 ASTM thermometer holder •

P/N 14T0303 Adapter to insert an E20 thermometer in the bath cover •

For Viscosity Accessories, see section ‘Viscosity Accessories’.

100

Density by Hydrometer


1.16 ASTM D1298 Density by HydrometerASTM D287 - ASTM D1298 - ASTM D6822 - IP 160 - ASTM E126 - API 2547 - ISO 3675

This specific method covers following laboratory determinations by hydrometer method: -Density, -Relative density (specific gravity), -American Petroleum Institute (gravity of crude petroleum and liquid petroleum products).

Main CharacteristicsA Tamson TLC15-5 refrigerator circulates a (cold) flow through the double walls of the cylinders. The TLC15-5 maintains the bath temperature within ± 0.25°C of the test temperature required by the method. The PTFE valves ensure fast drainage and cleaning of the cylinders. The easy detachable spill tray prevents that portions of the sample are spilled on the workbench. The rack offers full view on the hydrometer. Our special ASTM D1298 support eliminates the problem of mounting brackets or portions of a thermostatic bath blocking the view. The Tamson D1298 apparatus is a complete set-up existing of three Jacketed glass cylinders, rack and TLC15-5 circulator. Our system offers an interesting price advantage compared to other solutions based on a combination of a thermostatic bath with an external chiller. The ASTM D1298 set-up can also be used for ASTM D287 or ASTM D6822 test methods.

Range 5°C....120°C

Setting 0.01°C

Stability ± Better than 0.1°C

TLC15-5 Rack

Bath volume 5 L

Opening bath 85 x 150 mm (effective use)

Depth bath 150 mm

Length 420 mm (460 mm incl drain) 360 mm (front to back)

Width 265 320 (left to right)

Height 565 800 mm

Weight 30 kg 9 kg (glass parts included)

Power 1100 W (1 heater)Ambient temperature 15..28°C

CE Products conform to CE regulation

Set-up ASTM D1298 P/N 00T2000 (230V/50Hz) • P/N 00T2001 (230V/60Hz) • P/N 00T2002 (115V/60Hz) An additional rack is available to get an apparatus for six positions with one circulator • P/N 00T1260 Alternative for this setup is a TV2500 in combination with the TLC10-3. For further information, please see section 1.7.

Accessories ASTM D1298P/N 25T0928BW Thermometer with blue filling similar to ASTM 34C •

P/N 25T2153 Thermometer holder D1298 •

ASTM D1298 Apparatus

101

L o w T e m p e r a t u r e B a t h s

TLC10-3

TLC10-3

The TLC10-3 has been developed to be used as general purpose circulator and it can be used in various applications where cooling is needed. Experiments, refractometers, rotary-evaporators, distillation units, water baths, viscosity baths, flash point testers are applications for which the TLC10-3 can be used.

Main CharacteristicsThe apparatus holds a small bath containing 3.5 litres and the filling opening measures 40 x 120 mm. Due to its special design the system is extremely quiet, compact and saves costly laboratory space. Readout is in degrees °C or in °F. The bath comes standard with RS232 communication and when using the free software tool Tamcom, it provides temperature logging or a predefined temperature set point curve. A pump provides circulation in the bath or via an external circuit. The pump offers seven litres per minute with a maximum counter pressure of 300 mBar.

Range -10..60°C* / 14..140°F



Setting 0.01°C


Heating 1100 W

Bath volume 3.5 L


Depth bath 150 mm

Pump (mBar) Max pressure 300

Pump (L/min) Max flow 7

Dimension LxWxH 360 x 228 x 552 mm

Weight 18 kg

Heat removal See section 3.1

* On request the TLC10-3 can have a working range from -10..120°C

TLC10-3 P/N 00T0050 (230V/50Hz) • P/N 00T0051 (230V/60Hz) • P/N 00T0052 (115V/60Hz)

For options and spare parts, please see section `TC15-5 • TC30-5’

3.2 Tamson Cooling Circulators - TLC Line TLC10-3


Manuals see www.tamson.com

102

Tamson Instruments

Tel. +31 10 522 43 73Email [email protected] www.tamson.com


TLC15-5 TLC30-5

3.3 Tamson Cooling Circulators – TLC Line TLC15-5, TLC30-5The TLC15-5 and TLC30-5 have been developed to be used as general purpose circulator and they can be used in various applications where cooling is needed. Examples are experiments, refractometers, rotary-evaporators, distillation units, water baths, viscosity baths, flash point testers, foaming tests and ductility tests.

Main CharacteristicsThe apparatus holds a small bath containing five litres and the filling opening measures 85 x 150 mm. Due to its special design the system is extremely quiet, compact and saves costly laboratory space. Readout is in degrees °C or in °F. A pump provides circulation in the bath or to an external circuit. The pump offers seven litres per minute with a maximum counter pressure of 300 mBar.

TLC15-5

Range -15..60°C*/-5..140°F -30..60°C**/-5..140°F



Setting 0.01°C


Heating 1100 W

Bath volume 5 L


Depth bath 150 mm

Pump (mBar) Max pressure 300

Pump (L/min) Max flow 7

Dimension LxWxH 420 X 265 X 565 mm

Weight 30 kg

Heat removal See section 3.1* On request the TLC15-5 can have a working range from -15..120°C** On request the TLC30-5 can have a working range from -30..120°C

TLC15-5 P/N 00T0565 (230V/50Hz) • P/N 00T0567 (230V/60Hz) • P/N 00T0570 (115V/60Hz) TLC30-5 P/N 00T0555 (230V/50Hz) • P/N 00T0562 (230V/60Hz) • P/N 00T0560 (115V/60Hz)

TLC15-5 TLC30-5

103

Tamson Instruments

Tel. +31 10 522 43 73Email [email protected] www.tamson.com

74 TLC40 TLC80 TLC90


TLC40 TLC80 TLC90

TLC40-14

3.4 Tamson Cooling Circulators – TLC Line TLC40, TLC80, TLC90The TLC40-14 cooling circulator can be used for multiple heat removal purposes such as replacement of tap water, fast cool down, flash point, distillation, density or cloud and pour point testing. Also, this unit can be used to cool down water baths and viscosity baths which have a large bath volume. TLC80-14 and TLC90-14 cooling circulators can be used for general low temperature use and shows excellent heat removal performance in combination with cloud and pour point tests or cold filter plugging point tests.

Main CharacteristicsThe apparatus holds a bath containing 14 litres and the filling opening measures 240 x 170 mm. Due to its special design the system is extremely quiet, compact and saves costly laboratory space. The minimum temperature which can be reached with the TLC40-14 is -40°C. The minimum temperature which can be reached with the TLC80-14 is -80°C. At -80°C the heat removal capacity is still 300 Watts! The minimum temperature which can be reached with the TLC90-14 is -90°C. Readout is in degrees °C or in °F. A pump provides circulation in the bath or pumps the flow to an external circuit. The pump offers seven litres per minute with a maximum counter pressure of 300 mBar. Optional is a performance pump which offers 16 litres per minute.

Range -40..+20°C*/-40..+68 °F -80..+20°C/-112..+68°F -90..+20°C/-130..+68°F

Reading Standard °C, °F on requestUsed materials inside bath Stainless steel 304, brass bearings

Setting 0.1°C


Heating 1550 W

Bath volume 14 .. 15 L


Depth bath 150 mm

Pump (mBar) Max pressure 300 (optional 1 Bar)

Pump (L/min) Max flow 7 (optional 16) Max flow 10 (optional 16) Max flow 10 (optional 16)

Dimension LxWxH 810 x 460 x 770 mm

Weight 65 kg 80 kg 80 kg

Heat removal See section 3.1

TLC40-14 TLC80-14 TLC90-14

* On request the TLC40-14 can have an optional working range from -45..+20°C.

TLC40-14 P/N 00T0520 (230V/50Hz) • P/N 00T0522 (230V/60Hz) • P/N 00T0525 (115V/60Hz) TLC80-14 P/N 00T0530 (230V/50Hz) • P/N 00T0532 (230V/60Hz) • P/N on request (115V/60Hz) TLC90-14 P/N 00T0580 (230V/50Hz) • P/N 00T0585 (230V/60Hz) • P/N on request (115V/60Hz)

For options and spare parts, please see section TLC80-14DP

104

For viscosity measurements, R&D, combinatorial chemistry, biological applications, testing the solution behavior of synthetic materials, quality control in food, chemical and waste water technology, simple and easy system integration.

STIRRING DRYBATH 15-100 / STIRRING DRYBATH 15-250Stirring-heating block combination with 15 bore holes, suitable for 100 ml lab-flasks and for 150 ml beaker glasses tall form (ø 57.5 mm, depth 48 mm, distance 65 mm) or with 15 bore holes suitable for 250 ml lab-flasks and for 400 ml beaker glasses tall form (ø 71.5 mm, depth 78 mm, distance 84 mm).

STIRRING-HEATING BLOCKS WITH EXTERNAL CONTROL UNIT

Fast heating-up Energy-saving Insulated frame Durable quality Developed and made in Germany

Stirring - maintenance-free and wear-free by inductive 2mag-Magnetic-Drive concept, extremely wide speed range of 100 to 2,000 rpm, 100% synchronized speed, jerk-free stirring even at low speeds, 10-step power setting of the stirrer, high stirring power for viscous liquids and reduced stirring power for long-term operation without any heating effects caused by the stirrer, clear digital display for settings of stirrer speed, stirrer power and temperature of the integrated heater, SoftStart procedure for reliable catching/centering and safe acceleration of the stirring bar.

Heating - Heating plate made of resistant aluminium alloy, PTFE-coated for increased chemical resistance and easier cleaning, fast heating-up by powerful integrated electrical heater, homogenous temperature distribution, maximum heating temperature +200 °C, PowerDetect for automatic compensation of physically determined loss in stirring power which can come up to 40% at high temperatures, independent over-temperature protection inside the plate.

Inclusive separate control unit for operation of magnetic stirrer and integrated heater, for long-term protection of the electronics against aggressive liquids and gases as well as thermal influences, stainless steel housing.

Accessories

External probe sensor Pt100Stand for heatMIXcontrolReducing adapters - Inserts for reducing the bore hole diameter




Accessories





Accessories


Type DRYBATH 15-100 DRYBATH 15-250Stirring points 15Stirring point distance 65 mm 84 mmBore holes Ø/T Ø 57.5 / 48 mm Ø 71.5 / 78 mmStirring volume/stirring point 1 - 150 ml 1 - 400 mlStirring power (max.) 40 WPower setting 4 - 40 W (10-step)Temperature (max.) +200 °CSpeed range 100 - 2,000 rpmOperating voltage (max.) 230 V / 1,000 WDimensions (WxDxH) 280 x 430 x 120 mm 335 x 515 x 150 mmProtection category IP20Weight (gross) approx. 23 kg approx. 31 kgOrder no. 63100 63250

Individual units and dimensions on request.3 years warranty on material and manufacturing.

We reserve the right to make technical alterations. We do not assume liability for errors in printing or typeing.

105

STIRRING-HEATING BLOCKS WITH EXTERNAL CONTROL UNITSTIRRING-HEATING BLOCKS WITH EXTERNAL CONTROL UNIT For viscosity measurements, R&D, combinatorial chemistry, biological applications, testing the solution behavior

of synthetic materials, quality control in food, chemical and waste water technology, simple and easy system integration.

STIRRING DRYBATH 8-250 ERLStirring-heating block combination with 8 stirring positions (ø 87.2 mm, depth 78 mm, distance 100/140 mm), suitable for 250 ml Erlenmeyer flasks.

Stirring - Maintenance-free and wear-free by inductive 2mag-Magnetic Drive concept, extremely wide speed range of 100 to 2,000 rpm, 100% synchronized speed, jerk-free stirring even at low speeds, 10-step power setting of the stirrer, high stirring power for viscous liquids and reduced stirring power for long-term operation without any heating effects caused by the stirrer, clear digital display for settings of stirrer speed, stirrer power and temperature of the integrated heater, SoftStart procedure for reliable catching/centering and safe acceleration of the stirring bar.

Heating - Massive heating block made of resistant aluminium alloy, PTFE-coated for increased chemical resistance and easier cleaning, contact adapters for an optimal heat transfer, lowest possible temperature gradient inside the stirring vessels, integrated electrical heater, maximum heating temperature +200 °C.

PowerDetect for automatic compensation of physically determined loss in stirring power which can come up to 40% at high temperatures, specially made insulated stainless steel frame for energy- and time saving heating process, additionally for a homogenous temperature distribution and protection against accidental contact, independent over-temperature protection inside the plate.


Inclusive 8 contact adapters for an optimized heat transfer.

Accessories

External probe sensor Pt100Stand for heatMIXcontrol

Fast heating-up Energy-saving Insulated frame Durable quality Developed and made in Germany

Type DRYBATH 8-250 ERLStirring points 8Stirring point distance 100 / 140 mmBore holes Ø/T Ø 87.2 / 78 mmStirring volume/stirring point 1 - 250 mlStirring power (max.) 40 WPower setting 4 - 40 W (10-step)Temperature (max.) +200 °CSpeed range 100 - 2,000 rpmOperating voltage (max.) 230 V / 1,000 WDimensions (WxDxH) 335 x 515 x 150 mmProtection category IP20Weight (gross) approx. 38 kgOrder no. 63825

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CO2 NEUTRAL

by flyeralarm143432573

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