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Page 1: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

World Wide Web home pageon the Internet at:

http://www.aspentech.com/

@ Heri Rustamaji

Page 2: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

INTRODUCTION

Page 3: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

STARTING ASPEN PLUS

Page 4: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

STARTUP

• Blank Simulation : rancangan proses general

• Blank Simulation : British Unit

Page 5: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

TEMPLATES

Dengan template, user bisa memilih kondisiproses, misalnya :1.Unit measurement2.Property method3.Stream composition and information4.Stream report format3.Stream composition and information4.Stream report format5.dll

Sistem Proses tahu,pilih template yang tepat1. Property method sudah pas2.Hemat waktu untuk penyesuaian satuan

Page 6: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Untuk mengetahui fungsi masing-masing toolbar,letakkan kursor Anda di atas toolbar, fungsi daritoolbar tersebut akan muncul dalam bentuk pop up

ToolbarToolbar

FLOWSHEET AREA

MODEL LIBRARY

Page 7: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

FLOWSHEET WINDOWS

Untuk menampilkan Flow SheetWindow, Klik menu window danpilih salah satu :1. Normal

FLOWSHEETING :1. Klik media library dan pilih

NextData Browser

1. Normal2. Flow sheet as wallpaper3. Workbook mode

1. Klik media library dan pilihalat yang digunakan

2. Geser kursor pada Flowsheet window dan klik

Page 8: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

+ data komponen di dalam process flowsheet

+ property method, property sets

+ Model input+ Input stream

+ Input data reaksi

+ Input data alat di flowsheet+ input data kebutuhan utilitas

+ Pemilihan metode konvergensi untuk perhitungan

+ Pengaturan Design-Spec, Sensitivity, dsb

+ Optimasi proses

Page 9: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

STATUS INDICATOR

Page 10: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

PROPERTY METHOD

Blank simulation, pilihproperty method sendiri

Property method adalah model danmetode yang digunakan oleh Aspen untukmenghitung sifat termodinamika dantransportThermodynamics = fugacity coefficient,

enthalpy, entropy, gibbs free energy, danvolumeTransport = viskositas, konduktifitas

termal, koefisien difusi, tegangan muka.

Page 11: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

PROPERTY METHODS

• Tools >Property Method Selection Assistant• Ideal Property Method

( Ideal )• Equation of State Property Methods

( PENG-ROB, RK-SOAVE, SR-POLAR )( PENG-ROB, RK-SOAVE, SR-POLAR )• Activity Coefficient Property Methods

(NRTL, UNIFAQ, UNIQUAC )• Property Methods for Special Systems

(AMINES, SOLIDS)

Page 12: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Tutorial 2

EQUILIBRIUMEQUILIBRIUMEQUILIBRIUMEQUILIBRIUM

Page 13: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Contoh kasus

FLASH

2 Suatu umpan dengan suhu 50o

C terdiri atas 50 kg etanol dan40 kg air dipisahkan hinggakemurnian etanol mencapaiFLASH

1

3

kemurnian etanol mencapai98%

Tentukan konfigurasi dariseparator untuk memperolehkemurnian tersebut!

Page 14: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Property Method

IDEAL EOS ACTIVITY SPECIAL

IdealSolidNRTLPeng-Rob

Ideal

SYSOP0

Solid

Amines

Chao-sea

NRTL

UNIFAC

UNIQUAC

Peng-Rob

PSRK

SR-Polar

Page 15: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 16: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Hints for choosing method

Page 17: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 18: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Phase Equilibrium Diagram

1

• Buat simulasi baru

• New simulation

2

• Go To DATA BROWSER

• F8

3• Property Method UNIFAC

Page 19: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

WaterEthanol

Page 20: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

2. Property specification

ALL

UNIFAC

Page 21: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

3. Tools

Analysis > Property > Binary

Page 22: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

4.Binary analysis

Txy/Pxy

Page 23: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

azeotrop

Page 24: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

6. Plot grafik yang lain

Choose binary analysis tab

Plot wizard

nextnext

Page 25: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

FINISHFINISH

Page 26: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Residue Curve Map (RCM)*

Azeotrope

SeparationFeasibility

Nonideal

system

Keterangan lebih lanjut: Baca Perry 7th ed halaman 13-56

Page 27: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Contoh:

Tambahkan ethyl acetate di komponen

Masuk ke : tools > analysis >property > residue

Page 28: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 29: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 30: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 31: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

AZEOTROPE SEARCH

Page 32: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 33: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 34: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

TERNARY MAP

Plot azeotrop :

tools>conceptual design>ternary maps

Page 35: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 36: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Penyelesaian kasus:

Page 37: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SEPARATOR

Tutorial 3Tutorial 3

SEPARATOR

Page 38: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SEPARATOR

Model Simulasi alat pemisah untuk memisahkan komponenkimia berdasar sifat fisisnya (Kesetimbangan, Densitas, dll.),dan berdasarkan neraca massa

Page 39: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

o FLASH 2

o FLASH 3

o DECANTER

SEP

SEP 2

Page 40: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

REVIEW FROM ASPEN HELPModel Description Purpose Use For

Flash2Flash2 Two-outlet flash Separates feed into two outletstreams, using rigorous vapor-liquid or vapor-liquid-liquidequilibrium

Flash drums, evaporators,knock-out drums, single stageseparators

Flash3Flash3 Three-outlet flash Separates feed into three outletstreams, using rigorous vapor-liquid-liquid equilibrium

Decanters, single-stageseparators with two liquidphasesliquid-liquid equilibrium phases

DecanterDecanter Liquid-liquiddecanter

Separates feed into two liquidoutlet streams, using liquid-liquid equilibrium

Decanters, single-stageseparators with two liquidphases and no vapor phase

SepSep Componentseparator

Separates inlet streamcomponents into multiple outletstreams, based on specifiedflows or split frractions

Component separationoperations, such as distillationand absorption, when thedetails of the separation areunknown or unimportant

Sep2Sep2 Two-outletcomponentseparator

Separates inlet streamcomponents into two outletstreams, based on specifiedflows, split fractions, or purities

Component separationoperations, such as distillationand absorption, when thedetails of the separation areunknown

Page 41: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

REFERENCE

• Smith, J.M., Van Ness, H.C., Abbott,M.M., 2001, “Introduction to ChemicalEngineering Thermodunamics”, 6ed,Engineering Thermodunamics”, 6ed,Chapter 14 Topics in Phase Equilibria,McGraw-Hill International Edition.

• VLE

• LLE

• VLLE

Page 42: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SIMULASI – equilibrium based

Umpan pada suhu 25 oC dan tekanan 1 atm, yang terdiri dari :

25 liter/menit air

50 liter/menit dietil eter

25 liter/menit benzen

Ingin dipisahkan dengan berbagai alat pemisah (Flash2, Flash3,Ingin dipisahkan dengan berbagai alat pemisah (Flash2, Flash3,Decanter)

Semua alat beroperasi pada tekanan 1 atm, dengan suhu :

Flash2 : 60 oC

Flash3 : 50 oC

Decanter : 30 oC

Gunakan Property Method : NRTL

Page 43: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Penamaan arus-arus, kenapa didahului dengan angka?

Page 44: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

hanyahanyapenamaan,

Jangan terkecoh

Page 45: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 46: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 47: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 48: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Spesifik komponen untuk arus-arus ekstrak dan rafinat,,

Tidak diisi tidak masalah.

Page 49: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Pilihan untuk menentukan spesifikasi dari flash2 :

Pressure, temperature, vapor fraction, heat duty

Page 50: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Di RUN ,

dan tampilkan hasilnya pada Microsoft Excel .. !

Coba pada suhu yang berbeda .. !

Page 51: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Tampilan dalam format GENERAL_METRIC

Page 52: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SIMULASI – split fraction

Page 53: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SEP

Page 54: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

SEP2

Yang diisi 3

Page 55: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid

Analisis apa arti dari arus-arus tersebut…

Page 56: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 57: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 58: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 59: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 60: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 61: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 62: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid
Page 63: VLE -LLE Calculation dg ASPEN · PDF fileliquid or vapor-liquid-liquid equilibrium Flash drums, evaporators, knock-out drums, single stage separators ... separators with two liquid