vol. 2 1, anisotropy of the kinetic friction on a single …€¦ · (j) ,/p.1.) x ( ,1 .1. )3. a...

8
J ournal oiGlaci%gy, V o l. 2 1, No. 85 ,19 78 ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE CRYSTAL OF ICE By KATUTOS1 T US1MA ( In stitut e of Low Temperature Science, Hokkaido University, Sapporo, Japan 060) ABSTRACT. Mea sur ements wcr e m ade of the kine tic friction which occ ur s when a t ungsten ca rbid e ball slid es in va riou s directions on th e s urf ace of a single cr ysta l of ice, the track width produ ced o n the surf ace was a lso mea ur ed. Aniso tr opies were detected in bo th the fri c ti on coe ffi ci en t and the track width. T he track wid th </> was at a max imum wh en the ba ll was s lid normal to the basal plane and a minimum when it was mo ving parallel to (0001 ) in th e te mpera tur e range - 5 to - 30°C . A l though the fri ctio n coe ffi cient was a t a minimum when slid normal to (000 1) and max imum in pa rallel to (000 I) at temperatur es of - IgOC and below. this rela tion was found to be r eve rsed at temp e ratur es of - 10°C a nd a bo ve. An iso tropy in track width ca n be explain ed in terms of th e amo unt by which a sli p system co ntribut es to deformat ion in a specimen. H owever, o ur und erstanding of fri ct ional a ni sotropy ca ll s for kn owledge of the ploughing strength p defin ed by the a dh esion theory of fric ti o n. It was found t hat p reached a m ax imum in parallel to (0001 ) and a minimum normal to (000 1) a nd th at the frictional an isotropy on (000 1) was influen ced by th e value (j) , /p.1.) X (</> , 1</>.1. )3. A remarkab le frictiona l a ni sot ropy was also observed on th e surf ace inclin ed to the basa l plane at 30°; th e maximum fri c tion coe ffi cient wa s twi ce the minimum, whereas the maximum track width was o nl y 1. 3 tim es the minimum. R ESUME. Anisotropie dujrottelllent dyualllique sur 1I1llllonocristal de glace. No us avons fait des mes ur es de frotte- ment dyna miqu e entr e la glace ct un e bille de ca rbur e de tungstene, de te ll e maniere qu'un e trace de frottemcnt aya nt un e cer ta in e la r ge ur soit faite sur la s urf ace d' un mon oc ristal de glace dans des dir ections de g li sse ment differ e nt es. L 'a ni so tropi e est detectee a u m oyen d'un coefficie nt de fr otteme nt et de la largeur de la trace . Cette large ur de tr ace </> est maximum dan s la direction de glissement norma le a u plan basa l (0001) et minimum dan s la dir ect ion para ll ele au pl an (0001 ), le plan de gli sseme nt etant un p la n pri smat ique et la temp era tur e compri se e ntr e - 5 et - 30°C. Alors qu e le coe ffi cie nt d e fr otteme nt es t minimum lorsque le gl issc m e nt es t normal a (000 1) et ma x imum lorsque celui-ci es t para ll ele a (0001) pour d es temperat ur es egales et inf erie ur es a - IgOC , cc resul tat est inverse pour d es temperatures s up erieur es a - 10°C. L 'a ni so- tropie dans la la rge ur de la trace pe ut- e tr e ex pliqu ee par l'inAuence du sys teme de g li sse ment prepond era nt dan s I'ech ant ill on, ta ndis que la co mpreh ension de l 'a ni so tro pi e du frott eme nt necessitc la conn a issance de la force d e pen e tration p defini e par la theo ri e du fr otte me nt impliqua nt les fo rces d 'a dh es ion. Tl es t montr e qu e /) est maximum para ll element a (0001) et minimum norma lement a (000 I) ct l'a ni so tropi c d e fr ottement cs t fo nction d u te rme: (j) " 11) .1. ) x ( </> " I</> .1.) 3. Une a ni so trop ic nota blc es t aussi observee sur un e s urf ace inclinee de 30° sur le pl a n basal; le coe ffi cien t d e fr ottement maximal es t deux fois plu s eleve qu e la va le ur minima le alors que la large ur de trace ma ximal e est se ul eme nt 1,3 fois la vale ur minim ale. ZUSAMMENFASSUNG. Anisotropie der kinetischen Reibung arif ein em Eis-Eillkristall. Es wurd e die kinetische Reibung zw ischen Eis und einer Wolframkarbidkugel gemessen, sowie di e Br eite der Re ibungss pur , di e dur ch das Gleiten in versc hiedenen Ri chtungen a uf d er Obe rAac he eincs Eis-Einkrista ll s h e rvorgeruf en wurde . Dadurch wurd en Aniso tropien sowo hl im R e ibun gskoeffizienten a ls a uch in der Sp urbr e it e ent deckt. Die Sp urbr e it e </> wa r am grossten , wenn d ie Ku gel se nkr echt zur Basi se bene (0001) g li tt, un d a m kl einsten beim Glciten para ll el zur (0001 ) -Fl ache a ufPri sme nAachen im Te mperaturb ere ich - 5 bis - 30 °C. Wa hr end der Re ibun gskoeffizient bei T e mp e ratur en von - IgOC und da run ter am nie drigstcn war in Gl eit richtung senkrec ht z ur (ooo I)-Flac he und am gross ten in Richtung para ll el zu dieser, so wurde die umgekehrte Bezie hun g ge fund en bei T empera tur en von - 10°C unci da ruber. Aniso tropi c in der Spurbrc it c kann mit dem Be itragsa nt e il ein es in del' Probe a uftretcnden G leitsystems erkl art we rd en; dagegen e rford ert das Verstandn is der R eibungsaniso lrop ie die Ke nntni s der PAl"lgf es tigkeit p, d ie d ur ch die Ad hasionst heo ri e de r Re ibung d c fini ert isl. Es w urd e gefunden, dass p a m gross ten pa ra ll el zu (000 1) und am kl einsten se nkr echt d az u wa r, und dass di e R e ibun gsa ni so tropi e dur ch den \ Ve rt (P n/P L) X (</> nl cf>.1. )3 beinAusst wurde. Eine bcme rkun gswerte Re ibun gsanisotropie wurd e auch a uf der um 30° z ur Basisebene gencigten F1 ache beobac ht et; der grosste Reibun gskoe ffi zicnt war do pp elt so gross wie der kleinste, wohin gegen d ie grosste Sp u rbreite nur das I,3-fache der kl einsten betrug. I NTRODUCT [ON Friction a ni sot ropy h as been observed in non-metallic solids such as diamond a nd sapphire a nd in metals (e.g . copper). In th ese materia ls, track widths ca used by a sliding ind ent er h ave been shown to be relat ed to friction coefficie nts; wide track widths a nd high friction coe ffi cient s were obse rved for the non-metallic solids (Bowden and Brooks, 1966 ), whereas n arrow tracks were observed for co pp er (Dyer, 196 1; Bar quins a nd others, [ 968). In their ex pl anation of frictiona l a ni sotropy Bowd en and Brooks related low fri ction with n ar row trac k width . Ba rquin s a nd others exa min ed the a ni so tropi es in work- hard ened 66 ,

Upload: others

Post on 26-May-2020

7 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

J ournal oiGlaci%gy, V o l. 2 1, No. 85,1978

ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE CRYSTAL OF ICE

By KATUTOS1 T US1MA

(Institute of Low Temperature Science, Hokkaido University, Sapporo, Japan 060)

ABSTRACT. Measurements wcre made of the kine tic friction which occurs when a tungsten carbide ball slides in va rious directions on the surface of a single c rystal of ice, the track width produced o n the surface was a lso mea ured. Anisotropi es were detected in bo th the fri ction coeffi c ien t and the track width. T he track wid th </> was at a maximum wh en the ba ll was slid normal to the basal p la ne and a minimum when it was moving parallel to (0001 ) in the tempera ture range - 5 to - 30°C . A lthough the fri ction coeffi cien t was a t a minimum when slid norma l to (000 1) a nd maximum in parall el to (000 I ) at temperatures o f - IgOC a nd below. this re la tion was found to be reversed at temperatures of - 10°C a nd a bove. Anisotropy in track width can be exp la ined in terms of the a mount by which a sli p system contributes to deformation in a specimen. H owever, our understanding of fri ctiona l a nisotropy call s for knowledge o f th e ploughing strength p defin ed by the adhes ion theory of fri c tio n. It was found that p reached a max imum in parallel to (0001 ) and a minimum normal to (000 1) a nd that the frictional an iso tropy on (000 1) was influenced by the value (j) , /p.1.) X (</> , 1</> .1. )3. A remarkable frictiona l anisotropy was a lso observed on the surface inclin ed to the basa l plane at 30° ; the maximum fri c tion coeffi cient was twice the minimum, whereas the maximum track width was onl y 1.3 times the minimum.

R ESUME. Anisotropie dujrottelllent dyualllique sur 1I1llllonocristal de glace. Nous avons fait des mesures de frotte ­ment dynamique entre la g lace ct une bille de carbure de tungstene, d e telle maniere qu'une trace de frottemcnt ayan t une certaine la rgeur soit faite sur la surface d 'un monocris tal de glace da ns d es direc tions de glissement differentes. L 'aniso tropie est detectee a u m oyen d'un coefficient de frottement e t d e la largeur de la trace. Cette largeur de trace </> est maximum dans la direction de g lissement normale a u plan basa l (0001) et minimum dans la direction parallele au plan (0001 ) , le plan de glissem ent etant un p la n prismatique e t la tempera ture comprise entre - 5 et - 30°C. A lors que le coeffi cient d e frottement es t minimum lorsque le gl isscment es t normal a (000 1) e t maximum lorsque cel ui-ci es t paralle le a (000 1) pour d es temperatures ega les et inferieures a - IgOC, cc resul tat est inverse pour des temperatures superieures a - 10°C . L 'aniso­tropie da ns la la rgeur de la trace p eut-etre expliquee par l' inAuence du sys teme de glissement preponderant dans I'echant illon, tandis que la comprehension de l'aniso tropie du frottem e nt necess itc la conna issance de la force de penetration p defini e par la theo rie du frottem ent impliqua nt les fo rces d 'adhes ion. Tl es t montre que /) est maximum para llelemen t a (000 1) et minimum normalement a (000 I) ct l'a niso tropic d e frottement cs t fo nction d u terme: (j) " 11).1. ) x ( </> " I</> .1.) 3. Une a niso trop ic notablc es t a uss i o bservee sur une surface inclinee de 30° sur le pl a n basal ; le coeffi c ien t d e frottement maximal es t deux fo is plus eleve que la valeur minima le a lors que la la rgeur de trace m a ximale est seulement 1,3 fois la va leur minima le.

ZUSAMMENFASSUNG. Anisotropie der kinetischen Reibung arif einem Eis-Eillkristall. Es wurde die kinetische R eibung zwisch en Eis und ei ner W olframkarbidkugel gemessen, sowie di e Breite der R eibungsspur, die durch das Gl e iten in verschied ene n Rich tungen a uf d er OberAache e incs Eis-Einkrista lls h ervorgerufen wu rde . Dadurch wurden An iso tropien sowohl im R eibungskoeffizienten a ls a u ch in der Spurbre ite entdeckt. Die Spurbreite </> war am grossten, wenn d ie Kugel senkrecht zur Bas isebe ne (000 1) gli tt, und a m kleinsten beim Glciten pa ra ll el zur (0001 )-Fl ach e a ufPrismenAachen im Temperaturbereich - 5 bis - 30°C. Wahrend der R eibungskoeffizient bei T emperaturen von - IgOC und da run ter am niedrigstcn war in G leitri chtung senkrecht zur (ooo I )-F lache und a m gross ten in Richtung para llel zu d ieser, so wurde die umgekehrte Beziehung gefund en bei T empera turen von - 10°C unci d aruber. Aniso tropi c in der Spurbrc itc kann mit dem Beitragsa nte il eines in del' Probe a uftretcnden G leitsystems erkl art werden ; dagegen erfordert das Verstandn is d e r R eibungsan isolropie die Kenntnis der PAl"lgfestigkeit p, d ie d urch die Ad has ionstheori e der Reibung d cfini ert isl. Es w urde gefunden , dass p a m gross ten pa ra ll e l zu (000 1) und a m kleinsten senkrech t dazu war, und dass die R eibungsanisotropie durch den \Vert (Pn/PL) X (</> nl cf> .1. )3 be inAusst wurde. Eine bcmerkungswerte Reibungsanisotropie wurde a u ch a uf der um 30° zur Basisebene ge nc igten F1ache beobachtet; d er grosste R eibungs koeffi zicnt war d oppelt so gross wie der kle inste, wohingegen d ie grosste Spurbreite nur d as I,3-fache der kl e insten betrug.

I NTRODUCT[ON

Friction a nisotropy has been observed in non-metallic solids such as diamond a nd sapphire a nd in metals (e.g. copper). In these materials, track widths caused by a sliding indenter have been shown to be related to friction coefficients; wide track widths and hig h friction coefficients were observed for the non-metallic solids (Bowden and Brooks, 1966), whereas narrow tracks were observed for copper (Dyer, 196 1; Barquins a nd others, [968).

In their expla na tion of frictional a nisotropy Bowden and Brooks related low friction with narrow track width . Barquins a nd others examined the a niso tropies in work- hardened

66 ,

Page 2: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

JOURN AL OF GLA C IO LOGY

ma teria ls and the development of a bulge in front of the friction slider. Since these studies of an isotropy were restricted to qualitative analysis only, they failed to give a clear interpretation of the anisotropy mechanisms.

Two problems are found in the anisotropy literature. First, the track width caused by the friction was not measured accurately; secondly, the ploughing term of the adhesion theory (Bowden and Tabor, 1950) was not seen as a cause of the anisotropy, although the radii of the sliders used were always very small.

If frictional heating is ignored, the resistance friction is considered to be composed of two parts: the interfacial shear resistance between the frictional surface and slider, and the resistance due to ploughing of the slider. Therefore, mechanical properties such as hardness, yield , and shearing strength must be very important in any interpretation of the mechanism of friction between solids. In particular, anisotropies in these properties should be taken into account in dealing with the friction made on the crystalline solid surfaces. The present author has attempted to examine the anisotropy of the friction coefficient as a function of orientation and temperature on a single crystal of ice. He used tungsten carbide balls as sliders and also measured the width of tracks through a microscope.

ApPARATUS AND EXPERIMENTAL METHOD

The apparatus used here has been reported in previous work (Tusima, 1977) . An ice sample was cut from a large single crystal of glacier ice; its surface lay parallel to a desired crystallographic plane. The specimen surface was carefully machined to a smooth finish, and then the samples were annealed for two hours in a cold room kept at -3°C. After this time, the ice was moved to the cold room and mounted on the experimental apparatus. Frictional experiments were never begun less than five hours after completion of this sample preparation.

In order to measure the friction coefficient as a function of sliding direction on a fresh surface for each test, the slider was moved radially 5 or 100 between tests. The sliders used were tungsten carbide spheres made by Ultra-Spheric Co., U .S.A., which had diameters of 2.34 or 6.4 mm (although some tests were carried out with different diameter sliders) . The surface roughness of the spheres was less than 10 fLm.

EXPERIMENTAL RESULTS

( I) Anisotropies in friction and track width on prism planes (0 I I 0) and ( I I 20) Friction was measured every ro O on a prism plane (0110). No abrasive fragmentation

occurred along the track, thus, friction tracks formed only by plastic deformation of ice. Figure I shows the variations in the coefficient of kinetic friction fJ-k and the track width 1>

as a function of the angle 8 from the [1120 J direction. Other parameters of the test were: temperature, - 2 I °C; sliding velocity, 6.0 X ro- 5 m /s; applied load, 6.9 N; diameter of the slider, 2.34 mm. The friction coefficient fJ-k reached its maximum in the [I I20J direction and a minimum along [000 I 1. The value of fJ-k ranged from o. I [5 to o. 155, the ratio maximum/ minimum being 1.35. In contrast to the friction coefficient, the maximum track width was observed in the direction [0001] and the minimum width along [I 120]. These widths ""ere, respectively, 0-46 and 0.31 mm, their ratio being 1.48.

The inverse relationship between the friction coefficient and the track width reversed when the experiment was repeated at temperatures of - rooC and above. Figure 2 sh ows the friction coefficient and the track width plotted against 8 measured from [1120]. For this experiment, the temperature was - 10°C, the sliding velocity was 6.0 X 10- 5 m/s, the load was 14.4 N, and the slider diameter was 6-4 mm. The maxima of the friction coefficient and the track width were observed to b e in the same direction , which contrasts with the results obtained at temperatures of - 21 °C and below.

Page 3: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

F RI CT I ON AN I SO TR O PIE S ON I CE

:1 c QI U

::: QI 0 u c 0

u

LL

o E E u.

0.15

• • ••••

0.13

0.11 .

0.: .. 0 •

• 0.3

-looe •

• • •• •

•••

Deqrees from 90 . 180'

• •• •• •••

• • •

• • • •

• • • •• •

•• • . • [11"20J

270· 360"

• • • ••••• • • • • • ·0

Fig. I. Allisotropies in the killeticfrictioll coifficient I-' k alld the track width Oil (0[ / 0 ) . T emperalure : - 2IoG; load: 6·9 N;

velocity: 6.0 X 10- 5 m/s ; slider: 2.34 mm diameter.

A series of experiments were carried out on a prism plane ( I 120) . Similar r esults were obta ined to those observed on the prism plane ( 0 I 10). Inversion of the frictional anisotropy at a particula r temperature was also observed wh en the sliders were the same size for all tests, though the fric tion curves showed different maximum/minimum ra tios.

(2) Friction on basal plane (OOO I )

A series of fric tion experiments were carried ou t on the basal pla ne (000 I). A fa irly strong variation in the friction force w as observed a long whichever sliding direction was chosen . T his was in strong contras t to r esults observed for the prism pla n es where la rge fluctuations were never observed during sliding. The mean fri ctional force for each run was calculated , bu t no marked friction aniso tropy was observed on this plane.

(3) Anisotropy in f riction on inclined surfaces to (000 I ) As shown in F igures I and 2, a significant a mount of anisotropy in the /Lk value was found

on the prisma tic surface where the orientation of the basal planes in ice are norma l to the test surface, bu t on the basal surface itself no such a niso tropy was observed . This may suggest tha t

~

0.05 • _.0. . . ,rO.03 -QI

o ~O .2 u

~

,

0.7

• • 0

0 E E 'S.

kJ.S

.. .

= o o o = · 0

90 · •

'5' ,N

~ -- 21'C

• o • •• . . ..... • . . • 0···· 180 · 270 .

-.0. • • • • .. 0 ... 0 ..

• •

Fig. 2 . Allisotropies infrictioll I-'k and track w idth", 011 (o [ 10 ) . Teml)eratllre: - IOoG; load: [,J.4 N; velocity: 6.0 X 10- 5

m!-, ; slider : 6.4 IIlm ill dianifier.

Page 4: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

JO U RNAL OF GLAC I 0LOGY

the iLk value measured on a given surface of ice dep ends on the relationship between the sliding direction and the orientation of the basal planes in ice. Figure 3 shows anisotropies in the iLk value and the track width measured on a surface of ice cut diagonally against the basal plane. In this sample the (0001 ) p la ne was inclined at approximately 30° to the test surface. The abscissa is the a ngle of revolu tion of the test surface against the slid er. When the angle of the test surface was fixed at 0°, the slider moved parallel to the basal plane on the surface. As shown in Figure 3, two maxima in iLk appeared at 0° and 180° (where the slid er moved in paralle l with the basal plane), but two minima appeared at about 120° and 260° (where the slid er moved nearly perpendicular to the basal plane). Although values of iLk ch a nged significantl y with sliding direction, a slight variation in track width was observed .

c o

0.12 . . ..

0.10

0.08

0.06

.

. . I . , · 1 I

I . . T.. • . .

. • . . . . . . . . . .

" . . . . . (0001 )

e . .

Fig. 3. IIllisotropies in}i"iction and track width all pyramidal plane. T emperature: - [9cC; load : 6.9 N; velocity: 7.4 X [ 0-5

1II /s; slider : 2.34 mm ill diameter.

(4 ) NIicroscope observation offrictional track

As seen above, iLk values on the prismatic plane in diagonally cut surfaces depended on sliding direction . In order to interpret the observed anisotropy, the fric tion tracks produced on the specimen surfaces were observed using optical microscopy. According to our observa­tion, recrystalliza tion, cleavage fissures, microcracks, slip lines, and small-angle boundaries were found to have formed along a friction track.

Figure 4 shows photographs of the terminal areas of friction tracks produced by a slid er on the prismatic surface at -2 1°C . The deformed regions (broken lines) are extended beyond the sides of the track revealing mainly horizontal slip lines a nd microscopic cracks oriented normally to the slip lines . The symbol 0 indicates the width of frictional track produced by the slider (2.34 mm in diameter). Figure 4(b) shows a deformed bulge that moved in front of the slider parallel to the basal plane. Note that many cracks which are oriented normal to the basal planes propagate ahead of the slider , but that no significant deformation areas were found at the sides of track. The deformed area which formed near the terminus when the slider was moved diagonally to the basal plane (Fig. 4(c)) showed a n intermediate pattern between those of Figure 4 (a) and (b). Note that many cracks were created normal to slip lines oriented in the [1120] direction.

From inspection of these photographs, we may conclude that when the slider is moved para llel to the basal plane (Fig. 4 (b )) , comparatively higher values of iLk may be obtained because of bulge formation in front of the slider.

Page 5: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

FRICTION ANISOTROPIES ON I CE 665

ib)

(a) (c) .. ,. _ .;~~ .... sliding direction"", ;'>.- ~'--:- ":'<- ''-" t~CM.x i s , , r f //Oo~~~/~~ :r.~4 "ft.ill//" ,.~ '.~'~~.>,,'

JP, II/. .' I ". r/) , 1/,· ,.<."(::.{,;,, ..... ' ...

~/.;I:;lJ:~~.' :,':;~'1ij" ~,t ; /J.j.f-;,'~ ,._ • .'-~;":~ ,,' , ..

I 1:' 'r<7-16~ ... o----Fig, 4. Traces ill track ends of f riction Oil (OlIO). Sliding directions : (a) [0001 ]; (b) [[[20]; (c) 30° from [000 1].

Note that the basal slit) lines extend parallel to [I 120] and there is a dark line normal to the slil) lilies.

DISCUSSION

Since the velocity of the slider was roughly 10- 5 m /s in our experiments, frictional heat created at the interface between the slider a nd ice can b e ignored. The coefficient of kinetic fric tion f-Lk may be explained solely in terms of the plastic deformation of ice. According to the adhesion theory, f-Lk is given by

f-Lk = (kcfh/4+ k'cp3p/6R)/ W, ( I ) where s is the interfacial shear strength be tween ice and slider, p the ploughing strength of ice, R the diameter of slider, W the applied load on the slider , <p the width of track produced by friction , k and k' the shape factors (for the sake of convenience, we shall assume that k = 0.8 and that k' = I (Tusima, 1977)) .

As seen in Equation ( I ), f-Lk is composed of two terms, the first term of the right-hand side of this equation represents the fr iction d ue to interfacial shear and the second term represents friction associated with the p loughing effect of the slider.

Figure 5 shows f-L k, m easured on the prism surface, as a function of temperature and reciprocal slider diameter. The velocity of the slider and value of applied load are indicated on the figure. f-Lk is inversely proportiona l to the diameter of the slider , suggesting that Equa tion ( I) can be used in the interpreta tion of our results. According to Equation ( I), the effect of slider ploughing disa ppears if the slider can be considered to have an infinite diameter. The la rges t slider diame ter used in our experiments was 12.5 mm. If we assume that the ploughing term is neglig ible in values of f-Lk measured with this slider, then we can plot the shear strength of ice calculated by the shear term in Equa tion ( I) as a function of temperature (Fig. 6) .

From Equation ( I), the ploughing strength p of ice is expressed as

p = 6R(f-LkW- kcp2S/4)/k'<p3. (2) Since the s is known from Figure 6, if we substitute numerical values for f-Lk a nd cp measured in the various sliding directions into Equation (2), we can es tima te p as a function of direction. Figure 7 shows the p a nisotropy measured on the prism surface (0 I (0), P is one of the indices used to express ice surface hardness .

Butkovich (1954) a nd Offenbacher and R oselman ( 197 I) measured the hardness a niso­tropy of ice single crystals. Offenbacher a nd Roselman fo und that, on the prism plane, Knoop hardness measured in the direction normal to the b asal plane was smaller than the value obtained parallel to the basal pla ne. The p anisotropy obtained by the present a uthor seems to agree rough ly with the Knoop-hardness valu es obtained by Offenbacher and Roselman.

Page 6: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

666 JO UR NAL OF GLAC I OLOGY

Temperature

-, V= 7. 4Xl0 m /s W = 4. 7 N

u ....

-o

c .~ u

Fig. 5. The size effect of a slider on the friction. Friction coefficients on (OIIO) are jJlotted against the inverse diameters of sliders and the temperature. Velocity: 7.4 X 1 0 - 5 mJs,. load: 4·7 N .

50r-------.-------~----~

"-

~30

If)

-20 °c

-30

Fig. 6. Interfacial shear strength plotted against temperature,for planes (Ol / O) and (OOOI ).

Page 7: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

20 ( a ) - 10·e Cl.

10

. 201---. -....

F RI CT I ON AN I SOT R OP I ES O N I CE

. ..

. . .. 360·

• • I •• . . ... . t . . .. .

i· e o 90· lBO· 270· 360·

cS {J>

~ 40

Vi {J>

c £2 0 {J>

:::J o

<1-

(C) -. . . - .

l-

l-

f-

o

-30·e I . .

I - I--. . .. ... .. . . I . . . . ...

T . . degrees from [1 1 20J e

90 . 18 0 . 270 . Fig . 7. Ploughing strength on (OJ 10) calculated from friction coefficients and track width. (a) T emperature : - /OoG; load :

14.4 N ; velocity: 6_o X lO- 5 m /s ; slider_' 6.4 mm in diameter. (b) T emperature : - 2[oG; load: 6 .9 N ; velocity : 6.o x [ 0- 5 m/s ; slider: 2.34 mm. (c) T emperature : - 30oG; Load _' 6-9 N; velocity 7-4 X /0 - 5 m/s; sLider: 2.34 mm.

The a ppeara nce of a m aximum in the value of p along [I 120 J may be understood by the bulge formed a head of the slideI' (Fig. 4 (b)) . The anisotropy in the coefficien t of kinetic friction on the prism surface of ice can be explained in terms of the anisotropy in p and if> . Therefore, the anisotropy in ILk depends on pif>3. T he values of p and if> showed maxima or minima in the sliding directions [I 120] a nd [000 I] . T hus, the frictional anisotropy ILk [II20J!ILk [0001 ] may b e proportional to (p [1120] !p [0001 ]) x (if> [II20 ]jif> [0 001 ]) 3.

These values are summa rized for various temperatures in T a ble I. When the ra tio of pif> 3 [I [20 1!pif>3 [000 I J becom es smaller tha n I , frictional a niso tropy is dominated by the track-wid th a nisotropy. \,yhen the ra tio is la rger than I , fric tiona l anisotropy is dominated by ploughing-strength anisotropy. Both results agree with the experimental observa tions. The a nisotropy in friction can b e well explained by the aniso tropies in ploughing strength and track width .

TA BLE I. T HE R ATIO OF T R ACK W IDT H , PLOUG HING ST RENGTH , AN D F R ICTION COEFFIC IENT BETWEEN

[DIRECT IONS OF [ 11 20] A ND [ 000 1] FOR DIF F E R ENT TEMPE R AT U RES ON PRISM P LANE ( 0 I io)

T elllperature I-' [ 11 20] / 1-' [000 1]

°C [</> [11 20] 1</> [ 000 1] ] 3 Jl [II 20] /p [ 000 1] calculated observed - 1 0 0 .4 0 L 8 0.72 0 .67 - 2 1 0 · 39 3 -4 L 3 0 L 3 0

- 3 0 0.5 1 2.8 L 4 0 1. 20

C O NC LUSIO N

Friction a nisotropy on the basal (000 I ), prism (0 [ 10) and ( I 120), and pyra midal planes of ice was m easured as a function of track width , the amount of plastic deforma tion caused by frictional sliding, and so on . I t was found that, for the prism pla nes, friction r eaches a maxi­mum in the [[ 120] sliding direction on the (0 I 10) planes a nd in the [1010] direction on the

Page 8: Vol. 2 1, ANISOTROPY OF THE KINETIC FRICTION ON A SINGLE …€¦ · (j) ,/p.1.) X ( ,1 .1. )3. A remarkable frictional anisotropy was also observed on the surface

668 JO URN AL OF GLACIOLOGY

(1120) planes: Friction is a t a minimum in the 10001] direction for both planes at tempera­tures below - IgoC. At temperatures of - IQoC and above, the maximum friction was observed in the [0001] direction and the minimum in the [I 120] direction for (01 IQ) planes, and in the [ IO I 0] direction for ( II 20). A remarkable friction anisotropy was observed on pyramidal planes, although track-width anisotropy was very small. No marked anisotropy in friction was observed on the basal plane.

The width of the frictional track a lso varied with the sliding direction on the prism pla n e; that is, it was at a maximum along [0001 ] and reached minima along [I 120] for the (0 1 10) plane a nd a long [IOIO] for the (1120) plane, independent of temperature. The anisotropy was closely correlated with the volume of distortion caused by plastic deformation of ice in and a round the fri ction track.

ACKNOWLEDGEMENTS

The author wishes to express his d eepest appreciation to Professor G. Wakahama and Professor D. Kuroiwa for their kind discussion and comm ents while he was conducting this study.

REFEREN CES

Barquins, M., and others. 1968. Comportement de monocrystaux de cuivre sous l'action d e contact d 'un frotteur hemispherique, par M. Ba rquins, M. Kennel e t R. COUl"te!. Wear, Vo!. 11 , No. 2, p. 87- 11 0.

Bowden, F. P. , and Brooks , C. A. 1966. Frictional an isotropy in nonmetallic crystals. Proceedings of the R oyal Society of London, Ser. A, Vo!. 295, No. 1442 , p. 244- 58.

Bowden, F. P ., and Tabor, D . 1950. Thefrictioll and lubrication of solids. [Part l.] Oxford, Clarendon Press. (The International Series of Monographs on Physics. )

Butkovich , T. R . 1954. Hardness of single ice crys ta ls. U.S. Snow, Ice and Permafrost Research E stablishment. R esearch Paper 9.

Dyer, L. D . 196\. R olling friction on single crystals of copper in the plastic range. Acta Metallurgica, Vo!. 9, No. 10, p. 926- 36.

Offenbacher, E. L. , and R oselman, I. C. 197 I . Hardness anisotropy of single crystals of ice Ih. Nature, Physical Science, Vo!. 234, No. 49, p. 11 2- 13.

Tusima [i. e. T sushimaJ, K . 1977. Friction of a steel ball on a single crys tal of ice. Journal of Glaciology, Vo!. 19, No. 8 I , p. 225- 35.

DISCUSSION

VV. B. K AMB : Can you explain why a maximum in friction corresponds to a mll11mUm 111

track width at one temperature and to a maximum at a nother ?

K. TUSIMA: In this experiment, friction is mainly composed of ploughing resistance. The values of track width 1> a nd ploughing strength p were inverse as regards the position of maxima and minima. These tendencies do not change with temperature. Anisotropy of 1> increased with increasing temperature and anisotropy of p increased with d ecreasing tempera­ture. So the tendency of friction is mainly dependent on the behaviour of 1> at higher temperatures and p at lower temperatures . Taking a ll this into account, friction changes from m aximum to minimum at a particular temperature .

D. TABOR: The results are very pretty. However the sliding of a hard sphere over the ice measures the sum of the a dhesion and ploughing term. I wonder if the a uthor would consider measuring each of these terms separately: first, by sliding an ice slider on a hard substra te (adhesion without ploughing); secondly, by rolling a hard sphere over ice (ploughing with negligible adhesion) ?

TusIMA: I think so. I am now carrying out friction experiments with a h emispherical single crystal of ice on a metal plate to obtain the shearing term . I want to do experiments on rolling friction to find the ploughing term according to your suggestion.