vw(qj&rpp 7klv · w4d3 260 w4p3 428 energy loss peak 448 w4p1 495 na1s 1072.7 o1s 531 okl1* 970...
TRANSCRIPT
![Page 1: VW(QJ&RPP 7KLV · W4d3 260 W4p3 428 Energy Loss Peak 448 W4p1 495 Na1s 1072.7 O1s 531 OKL1* 970 * Auger Peak (a) 10 (b) 10 (e) 10 20 20 20 30 40 50 60 2Theta (deg) 30 40 50 60 2Theta](https://reader035.vdocuments.net/reader035/viewer/2022081222/5f787c0d65f8090e1a5c5be3/html5/thumbnails/1.jpg)
Fig. S1 as-prepared (a)WO3-x films and (b) WO3 films deposited on glass (red line) and quartz (blue line) before annealing. (c)WO3-x films sputtered on quartz after annealing, the profile of WO3-x (JCPDS file: 53-0434) is listed at the bottom. WO3 films sputtered on glass (d) and quartz (e) after annealing, the profile of Na2W2O7 (JCPDS file: 32-1185) and WO3 (JCPDS file: 05-0388) are listed at the bottom correspondingly.
Electronic Supplementary Material (ESI) for CrystEngComm.This journal is © The Royal Society of Chemistry 2017
![Page 2: VW(QJ&RPP 7KLV · W4d3 260 W4p3 428 Energy Loss Peak 448 W4p1 495 Na1s 1072.7 O1s 531 OKL1* 970 * Auger Peak (a) 10 (b) 10 (e) 10 20 20 20 30 40 50 60 2Theta (deg) 30 40 50 60 2Theta](https://reader035.vdocuments.net/reader035/viewer/2022081222/5f787c0d65f8090e1a5c5be3/html5/thumbnails/2.jpg)
Fig. S2 FTIR spectra of (a) as-prepared samples and NaxWO3 film (b) annealed at 500oC.
Fig. S3 Top morphology of different samples before annealing (a) WO3-x/BK7, (b) WO3-
x/SiO2, (c)WO3/BK7, (d)WO3/SiO2
![Page 3: VW(QJ&RPP 7KLV · W4d3 260 W4p3 428 Energy Loss Peak 448 W4p1 495 Na1s 1072.7 O1s 531 OKL1* 970 * Auger Peak (a) 10 (b) 10 (e) 10 20 20 20 30 40 50 60 2Theta (deg) 30 40 50 60 2Theta](https://reader035.vdocuments.net/reader035/viewer/2022081222/5f787c0d65f8090e1a5c5be3/html5/thumbnails/3.jpg)
Fig. S4 Top morphology of different samples after 500oC annealing (a) NaxWO3/BK7, (b) WO3-x/SiO2, (c)Na2W2O7/BK7, (d)WO3/SiO2
Fig. S5 Cross morphology of different samples after 500oC annealing (a) NaxWO3/BK7, (b) WO3-x/SiO2, (c)Na2W2O7/BK7, (d)WO3/SiO2
![Page 4: VW(QJ&RPP 7KLV · W4d3 260 W4p3 428 Energy Loss Peak 448 W4p1 495 Na1s 1072.7 O1s 531 OKL1* 970 * Auger Peak (a) 10 (b) 10 (e) 10 20 20 20 30 40 50 60 2Theta (deg) 30 40 50 60 2Theta](https://reader035.vdocuments.net/reader035/viewer/2022081222/5f787c0d65f8090e1a5c5be3/html5/thumbnails/4.jpg)
Table S1. XPS Peaks
Peak Energy
C1s 285
N1s 400
W4f 36.5
W4d5 248
W4d3 260
W4p3 428
Energy Loss Peak 448
W4p1 495
Na1s 1072.7
O1s 531
OKL1* 970
* Auger Peak