Waste Management Division PO Box 95 29 Hazen Drive

Concord NH 03302 Type of Submittal Check One-Most Applicable

0 Work Scope 0 Reimbursement Request

U

0 0

Remedial Action bull Remedial Action Plan

bull Bid Plans and Specifications bull Remedial Action Implementation

Report Treatment System and POE OampM Activitv and Use Restriction

0 UST Facility Report 0 AST Facility Report

b EmergencyInitial Response Action (3J Groundwater Quality Assessment 0 Temporary Surface Water Discharge Permit

~ Initial Site Characterization D Site Investigation

0 0

bull Site Investigation Report

bull Supplemental Site Investigation Report

bull GMZ Del ineation Source Area Investigation bull

bull Data Submittal

bull Annual Summary Report Unsolicited Environmental Sampling Notification Closure Documentation

0

0 0

Groundwater Management Permit

bull Permit Application

bull Renewal Application

bull Deed Recordation Documentation

bull Abutter Notification Documentation

bull Release of Recordation Data Submittal Annual Summary Report

June 2010 Addendum to Sampling and Analysis Plan Mottolo Superfund Site

Raymond New Hampshire NHDES No 198704094

Prepared For

New Hampshire Department of Environmental Services Waste Management Division

29 Hazen Drive PO Box 95

Concord New Hampshire 03301-0095 Digitally signed by Mr Drew Hoffm an PE GZA

(603) 271-2910 ON cn=GZA o=GZA

G Z A GeoEnvironmental IncPrepared By ou=AdministrationGZA GeoEnvironmental Inc email c=US380 Harvey Road Date 201 00716 Manchester NH 03301-3347 50328 -0400 (603) 623-3600

Amy T Doherty PG

July 16 2010

Recommended Risk Category (Check One U 1 Immediale Human Heallh Risk I U 4 Surface Water Impact U 7 Alternate Water AvailablelLow

(Impacted water supply well etc_) D 5 No Alternate Water AvailableNo

Level Groundwater Contamlnshyation laquo 1 000 x AGQS)

lSI 2 Potential Human Health Risk Existing Wells in Area (Water supply well within 1000 or Site within SWPA) D 6 Alternate Water AvailableHigh

0 8 No AGQS ViolationNo Source Remaining

0 3 Free Product or Source Hazard ~vel Groundwai~ r Contamination gt 1000 x AGQS 0 Closure Recommended

Report Cover Sheet Template ReVIsed July 29 2005

Enginen-s andGZA

I ScienlislS GcoEnvironmcntal Inc

June 23 20 I 0 File No 04002446641

380 Harvey Road Manchester New Hampshi re 03103middot3)47 603middot623middot3600 FAX 603middot624middot9463 wwwgzacom

Mr Drew Hoffman PE New Hampshire Department of Environmental Services Waste Management Division 29 Hazen Drive PO Box 95 Concord New Hampshire 0330 1-0095

Re June 2010 Addendum to Sampling and Analysis Plan Monolo Superfund Site N HDES 198704094 Raymond New Hampshire

Dear Drew

GZA GeoEnvironmental Inc (GZA) has prepared this Addendum to the May 20 2010 Sampling and Analysis Plan (SAP) for the planned sampling of select residential water suppl y wells at the Mottolo Superfund Site (Mottolo) located in Raymond New Hampshire for the New Hampshire Department of Environmental Service (N HDES) and the United States Environmental Protection Agency (EPA) Refer to the attached updated Organizational Chart for sampling personnel planned for the event GZA anticipates referencing the NHDES- and EPA-approved May 20 I0 SAP for all sampling activities discussed herein

The following applicable tables and fi gure refer to the sampling planned for the week of June 21 2010 and June 28 20 I 0

bull Figure 1 illustrates all of the residential sampling locations near the Site

bull Table 2B refers to the specific sampling location and treatment methods at each residence to be sampled during the June 20 I0 sampling event

bull Table 3 refers to specific analytical methods sample vo lume containers and hold time requirements for the June 2010 sampling event and

bull Table 5 refers to the specific Quality Control sampling requirements for the June 2010 sampling event

Refer to the attached updated Chain-of-Custody fonn to be used for thi s sampling event

Copyright copy 20 10 GZA GeoEnvironmental Inc

An Equal Oppltgt11wriy Emplo MlfN1I 1

Enginen-s andGZA

I ScienlislS GcoEnvironmcntal Inc

June 23 20 I 0 File No 04002446641

380 Harvey Road Manchester New Hampshi re 03103middot3)47 603middot623middot3600 FAX 603middot624middot9463 wwwgzacom

Mr Drew Hoffman PE New Hampshire Department of Environmental Services Waste Management Division 29 Hazen Drive PO Box 95 Concord New Hampshire 0330 1-0095

Re June 2010 Addendum to Sampling and Analysis Plan Monolo Superfund Site N HDES 198704094 Raymond New Hampshire

Dear Drew

GZA GeoEnvironmental Inc (GZA) has prepared this Addendum to the May 20 2010 Sampling and Analysis Plan (SAP) for the planned sampling of select residential water suppl y wells at the Mottolo Superfund Site (Mottolo) located in Raymond New Hampshire for the New Hampshire Department of Environmental Service (N HDES) and the United States Environmental Protection Agency (EPA) Refer to the attached updated Organizational Chart for sampling personnel planned for the event GZA anticipates referencing the NHDES- and EPA-approved May 20 I0 SAP for all sampling activities discussed herein

The following applicable tables and fi gure refer to the sampling planned for the week of June 21 2010 and June 28 20 I 0

bull Figure 1 illustrates all of the residential sampling locations near the Site

bull Table 2B refers to the specific sampling location and treatment methods at each residence to be sampled during the June 20 I0 sampling event

bull Table 3 refers to specific analytical methods sample vo lume containers and hold time requirements for the June 2010 sampling event and

bull Table 5 refers to the specific Quality Control sampling requirements for the June 2010 sampling event

Refer to the attached updated Chain-of-Custody fonn to be used for thi s sampling event

Copyright copy 20 10 GZA GeoEnvironmental Inc

An Equal Oppltgt11wriy Emplo MlfN1I 1

New Hampshire Department of Environmental Services June 22 2010 File No 04002446641 Page 2

If you have any questions regarding this Addendum please do not hesitate to contact Stefanie Lamb at (603) 232-87 11

Very truly yours

GZA GEOENVlRONMENTA L INC

Stefani e Lamb PG Assistant Project Manager

)I-lJ t ~ t Lamb PG cGW P Michael B Asselin

Consul tant Reviewer

SGUSRLIM BArklltmd p()4jobltOO440Qs1Q4 0024466 00()4002446641 bull uolo 2010WOTklj un~ 2010 $lIpljunc 2010 sap ddcndumdolt

Attachments Figure - I Site Plan Updated Organizational Chart Table 2B - June 20 10 Res identia l Drinking Water Sampling Program Table 3 - June 20 I 0 Media Analysis Test Methods ContainersSample

Volume Preservation and Hold Time Table 5 - June 2010 Sununary of Quality Assurance Samples To Be

Collected Updated NHDES Chain of Custody Fonn

cc Michael Jasinski and Charles Porfert EPA Sharon Perkins NHDES

New Hampshire Department or Environmental Services June 22 2010 Fie No 04002446641 Page)

Jur-iE 2010 ADDEiiDUM TO THE SAMPLING AND ANALYSIS PLA~ MOlTOLO SUPERFUND SITE CERCUS 10 NO NHD980S03J611 NHDES 198704094 RAYMOND NEW HAMPSHIRE

)Qcument Title

Stefanie Lamb PG Prepared by (Preparer s Nam and Organiationo Affiliation)

380 Harvey Road Manchester New Hampshire (603) 232-8711 Address tma Telephone Number

June 23 2010 DayIMonthIYear

US Environmental ProtKtion AgellCY

Remed ial Project Manager -~~~~~~~~=l~-4~L Signature

Michael Jasinski Printed NomeDare

Nw Hmphi runnl of Eovronm~tal Sek Q JJl _ Project Manager ~~~~~________

$igntllure

Drew Hoffman PE Printed NomeDale

GZA Principalin-Charge --Signatllre

Steven R Lamb PG CGWP 612310

GZA Senior Project Manager

Signature

Michael B Asselin 6123110 Printed NamelDtlte

GZA Project Quality Assurance Officer

Amv T DohertY PG 612310 Printed NameDote

Signafllre

FIGURE I - SITE PLAN

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- $-

I shy-T

o o ~-

shy--

bull-shy

-shy

-shy

bull-shy

-shy

on-shy

M-shy

- r----r shy

--=~~~ ~-

1

raquo-shy13__ 5

-Jl~ ou~

T

0

shy

shy--

--1

~- T-

bull_ _ OlAV

ltCl2010 - CZA CoEVron nlol 1m GZAshy P04Jobs0024400s04002446600040024466J6 - ~olto lo Site InvesfgolionAccess AgfeementsJune 2010 Resceniol Sampling RoundFgure 1 June 2010 Rescentcl SomplOng Rouncdwg (Figure 1) June 22 2010 - J53pm JosepllNclgto ls

2t 11[10--

T

bull-~ T

$-

I I SITE 7 FORMER DRUM ~

DISPOSAL AREA

3

T

-----c~TREAM STAFF GAGE

e shy- cJ

0 0 1J~_

$5_ bullbull

bull_shy

T

bull_shy

D

_shy

T las_-

b

shybull

-shy

00

n __ 00

T

21 IIlMt

0[J

~-

1J __ 00

6 lID

D

shy-D0

~ -l

~ - ~

o

~ 2

NOTES

1) BASE MAP DEVELOPED USING

A) BAlSAM ENVIRONMENTAl CONSULTANTS INC SITE PlAN TITLED SITE AREA GROUND WATER amp SURFACE WATERSEDIMENT $AMPUNG LOCATIONS DATED 71990 DRAWING No 2-12

B) NHDES GIS FlGURE TTTLED MOTTOLO PIC FARM SUPERFUND SITE RAYMOND NEW HAMPSHIRE

C) LOCATION INFORMATION fROM AN AUGUST 24 2008 NOBIS DETAIL SHEET 4 GROUN DWATER MONITORING WEU SURVEY

D) RAYMOND TAX MAP 5 PLOT DATA 4 2308

2) THE LOCATION OF THE SITE FEATURES TEST BORINGS MONITORING WEUS SAMPLING LOCATIONS EXPLORATIONS WERE APPROXIMATELY DETERMINED BY SURVEY TAPE MEASUREMENTS THIS DATA SHOULD BE CONSIDERED ACCURATE ONLY TO THE DEGREE IMPLIED BY THE METHOD USED

LEGENDshy

OW- 4 SR EXISTING SHAUOW BEDROCK WEUS TO HAVE WATER lEVEL MEASURED

RESIDENTIAL WEU APPROXIMATE LOCATION

RESIDENCES INCLUDED IN THE JUNE 2010 SAMPLING ROUND

T TRANSDUCER

N

II DRAFT II - shy -

PREPARED BY

-- shySCALE IN FEET

(SCAlE IS AN ESTIMATE BASED ON TAX MAPS)

I BLUEBERRY HILL ROAD

RAYMOND NH

JUNE 2010 RESIDENTIAL SAMPLING ROUND

GZA GeoEnvironmental Inc Engineers and Scientists 380 HARVEY ROAD MANCHESTER NEW HAMPSHIRE 03103 (amp03) 623-3600

PREPARED FOR

NEW HAMPSHIRE DEPT OF ENVIRONMENTAL

SERVICES BUREAU OF WASTE MANAGEMENT

PROJ MGR MBA REVIEWED BY SRL CHECKED BY MBA FIGURE

DRAWN BY MJD SCALE EST 1200

1PROJECT NO REVISION NO

DESIGNED BY ANP

DATE

JUNE 2010 04002446641 0 SHEET NO

UPDATED ORGANIZATIONAL CHART

JUNE 2010 ADDENDUM TO THE SAMPLING AND ANALYSIS PLAN MOTTOIO SUPERFUND SITE

CERCUS ill NO NIID980S03361 NIIDES 198704094 RAYMON D NEW HAMPSHIRE

Project Organizational Chart

NUDES Irojecl Manager Andrew 1 Hoffman_Po E

603-271- 6778 EPA Regio I Remedial Irojecl Malager

Michael Jasinski 617-9 18-1352

N IIDES m VRB QA Coordillotor Sharon Perkins 603-271 -6805

GZA PrillcipalillChurge Steven R Lamb 603-232-8741

GZA Sellior Project MOlltlger Michaclll Asselin

603-232-8739 GZA Project QA Officer

Amy T Doherty 603-232-8763

GZA Ileal Olll Safety MOlager Mark P Ma1chik 781-278-5747

Luhorutory Sence~

NHDES in-house Laboratory GZA Teclmical Field Stuff(General Analytical Services)

Lou Barinclli Assistant Laboratory Stefanic lmnb PoGo Senior Sampler

Dincor 603-271middot2994 Amy Pisco(XJ Field Sampler Jessica Meeks Field Sampler

Katahdin Analytical ServicLS TallYJ Justham Field Sampler

(Supporting Analytical Services) Daniel Hartigan Field Support Alternate Sampler

Al Jacobsen Field Technician Microsccps hlcorpornted Mirsad Alihodzic Ahemate Field Technician for GW levels

(Supporting Analytical Services)

J)utu Vulitlutioll

Nl-IDES Laboratory

TABLE 2B - JUNE 2010 RESIDENTIAL DRINKING WATER SAMPLING PROGRAM

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

shy

10 klUUllOt -shy-T

- $-

I shy-T

o o ~-

shy--

bull-shy

-shy

-shy

bull-shy

-shy

on-shy

M-shy

- r----r shy

--=~~~ ~-

1

raquo-shy13__ 5

-Jl~ ou~

T

0

shy

shy--

--1

~- T-

bull_ _ OlAV

ltCl2010 - CZA CoEVron nlol 1m GZAshy P04Jobs0024400s04002446600040024466J6 - ~olto lo Site InvesfgolionAccess AgfeementsJune 2010 Resceniol Sampling RoundFgure 1 June 2010 Rescentcl SomplOng Rouncdwg (Figure 1) June 22 2010 - J53pm JosepllNclgto ls

2t 11[10--

T

bull-~ T

$-

I I SITE 7 FORMER DRUM ~

DISPOSAL AREA

3

T

-----c~TREAM STAFF GAGE

e shy- cJ

0 0 1J~_

$5_ bullbull

bull_shy

T

bull_shy

D

_shy

T las_-

b

shybull

-shy

00

n __ 00

T

21 IIlMt

0[J

~-

1J __ 00

6 lID

D

shy-D0

~ -l

~ - ~

o

~ 2

NOTES

1) BASE MAP DEVELOPED USING

A) BAlSAM ENVIRONMENTAl CONSULTANTS INC SITE PlAN TITLED SITE AREA GROUND WATER amp SURFACE WATERSEDIMENT $AMPUNG LOCATIONS DATED 71990 DRAWING No 2-12

B) NHDES GIS FlGURE TTTLED MOTTOLO PIC FARM SUPERFUND SITE RAYMOND NEW HAMPSHIRE

C) LOCATION INFORMATION fROM AN AUGUST 24 2008 NOBIS DETAIL SHEET 4 GROUN DWATER MONITORING WEU SURVEY

D) RAYMOND TAX MAP 5 PLOT DATA 4 2308

2) THE LOCATION OF THE SITE FEATURES TEST BORINGS MONITORING WEUS SAMPLING LOCATIONS EXPLORATIONS WERE APPROXIMATELY DETERMINED BY SURVEY TAPE MEASUREMENTS THIS DATA SHOULD BE CONSIDERED ACCURATE ONLY TO THE DEGREE IMPLIED BY THE METHOD USED

LEGENDshy

OW- 4 SR EXISTING SHAUOW BEDROCK WEUS TO HAVE WATER lEVEL MEASURED

RESIDENTIAL WEU APPROXIMATE LOCATION

RESIDENCES INCLUDED IN THE JUNE 2010 SAMPLING ROUND

T TRANSDUCER

N

II DRAFT II - shy -

PREPARED BY

-- shySCALE IN FEET

(SCAlE IS AN ESTIMATE BASED ON TAX MAPS)

I BLUEBERRY HILL ROAD

RAYMOND NH

JUNE 2010 RESIDENTIAL SAMPLING ROUND

GZA GeoEnvironmental Inc Engineers and Scientists 380 HARVEY ROAD MANCHESTER NEW HAMPSHIRE 03103 (amp03) 623-3600

PREPARED FOR

NEW HAMPSHIRE DEPT OF ENVIRONMENTAL

SERVICES BUREAU OF WASTE MANAGEMENT

PROJ MGR MBA REVIEWED BY SRL CHECKED BY MBA FIGURE

DRAWN BY MJD SCALE EST 1200

1PROJECT NO REVISION NO

DESIGNED BY ANP

DATE

JUNE 2010 04002446641 0 SHEET NO

UPDATED ORGANIZATIONAL CHART

JUNE 2010 ADDENDUM TO THE SAMPLING AND ANALYSIS PLAN MOTTOIO SUPERFUND SITE

CERCUS ill NO NIID980S03361 NIIDES 198704094 RAYMON D NEW HAMPSHIRE

Project Organizational Chart

NUDES Irojecl Manager Andrew 1 Hoffman_Po E

603-271- 6778 EPA Regio I Remedial Irojecl Malager

Michael Jasinski 617-9 18-1352

N IIDES m VRB QA Coordillotor Sharon Perkins 603-271 -6805

GZA PrillcipalillChurge Steven R Lamb 603-232-8741

GZA Sellior Project MOlltlger Michaclll Asselin

603-232-8739 GZA Project QA Officer

Amy T Doherty 603-232-8763

GZA Ileal Olll Safety MOlager Mark P Ma1chik 781-278-5747

Luhorutory Sence~

NHDES in-house Laboratory GZA Teclmical Field Stuff(General Analytical Services)

Lou Barinclli Assistant Laboratory Stefanic lmnb PoGo Senior Sampler

Dincor 603-271middot2994 Amy Pisco(XJ Field Sampler Jessica Meeks Field Sampler

Katahdin Analytical ServicLS TallYJ Justham Field Sampler

(Supporting Analytical Services) Daniel Hartigan Field Support Alternate Sampler

Al Jacobsen Field Technician Microsccps hlcorpornted Mirsad Alihodzic Ahemate Field Technician for GW levels

(Supporting Analytical Services)

J)utu Vulitlutioll

Nl-IDES Laboratory

TABLE 2B - JUNE 2010 RESIDENTIAL DRINKING WATER SAMPLING PROGRAM

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

UPDATED ORGANIZATIONAL CHART

JUNE 2010 ADDENDUM TO THE SAMPLING AND ANALYSIS PLAN MOTTOIO SUPERFUND SITE

CERCUS ill NO NIID980S03361 NIIDES 198704094 RAYMON D NEW HAMPSHIRE

Project Organizational Chart

NUDES Irojecl Manager Andrew 1 Hoffman_Po E

603-271- 6778 EPA Regio I Remedial Irojecl Malager

Michael Jasinski 617-9 18-1352

N IIDES m VRB QA Coordillotor Sharon Perkins 603-271 -6805

GZA PrillcipalillChurge Steven R Lamb 603-232-8741

GZA Sellior Project MOlltlger Michaclll Asselin

603-232-8739 GZA Project QA Officer

Amy T Doherty 603-232-8763

GZA Ileal Olll Safety MOlager Mark P Ma1chik 781-278-5747

Luhorutory Sence~

NHDES in-house Laboratory GZA Teclmical Field Stuff(General Analytical Services)

Lou Barinclli Assistant Laboratory Stefanic lmnb PoGo Senior Sampler

Dincor 603-271middot2994 Amy Pisco(XJ Field Sampler Jessica Meeks Field Sampler

Katahdin Analytical ServicLS TallYJ Justham Field Sampler

(Supporting Analytical Services) Daniel Hartigan Field Support Alternate Sampler

Al Jacobsen Field Technician Microsccps hlcorpornted Mirsad Alihodzic Ahemate Field Technician for GW levels

(Supporting Analytical Services)

J)utu Vulitlutioll

Nl-IDES Laboratory

TABLE 2B - JUNE 2010 RESIDENTIAL DRINKING WATER SAMPLING PROGRAM

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

JUNE 2010 ADDENDUM TO THE SAMPLING AND ANALYSIS PLAN MOTTOIO SUPERFUND SITE

CERCUS ill NO NIID980S03361 NIIDES 198704094 RAYMON D NEW HAMPSHIRE

Project Organizational Chart

NUDES Irojecl Manager Andrew 1 Hoffman_Po E

603-271- 6778 EPA Regio I Remedial Irojecl Malager

Michael Jasinski 617-9 18-1352

N IIDES m VRB QA Coordillotor Sharon Perkins 603-271 -6805

GZA PrillcipalillChurge Steven R Lamb 603-232-8741

GZA Sellior Project MOlltlger Michaclll Asselin

603-232-8739 GZA Project QA Officer

Amy T Doherty 603-232-8763

GZA Ileal Olll Safety MOlager Mark P Ma1chik 781-278-5747

Luhorutory Sence~

NHDES in-house Laboratory GZA Teclmical Field Stuff(General Analytical Services)

Lou Barinclli Assistant Laboratory Stefanic lmnb PoGo Senior Sampler

Dincor 603-271middot2994 Amy Pisco(XJ Field Sampler Jessica Meeks Field Sampler

Katahdin Analytical ServicLS TallYJ Justham Field Sampler

(Supporting Analytical Services) Daniel Hartigan Field Support Alternate Sampler

Al Jacobsen Field Technician Microsccps hlcorpornted Mirsad Alihodzic Ahemate Field Technician for GW levels

(Supporting Analytical Services)

J)utu Vulitlutioll

Nl-IDES Laboratory

TABLE 2B - JUNE 2010 RESIDENTIAL DRINKING WATER SAMPLING PROGRAM

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

TABLE 2B - JUNE 2010 RESIDENTIAL DRINKING WATER SAMPLING PROGRAM

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

TABLE 2B - J UNE 2010 RESlDENTIAL DRINKING WATER SAMPLE PROGRAM Mottolo Superfund Sitc

Raymond Ncw Hampshire

IMae l Lot I I 19

I 18

I 5

5 4

5 88

5 3- 1

I 2

5 3-2

5 3-5

5 3-3

5 3-6

5 3-7

1J 34-7

1J 34shy 10

1J 34-6

1J 34-36

1J 34-35

1J 34-34

1J 34- 12

1J 34-32

1J 34shy 13

Locatio n I WelllD ISamelc Location ISa mele 1(e IC urrent Treatment

II Stmwbeny Ln MOT OW-9 Outsidc front ta Raw

No trcatment confimloo MOT OW-9A Outsidc rear ta Raw

Outside tap rear after Raw after Cartridge filter amp radon MOT_OW-IO

trcatmcnt b~lss treatment bypass treatmcnt (Radon trcatmcnt

15 Stmwbeny Ln not working lots of

Outsidc front tap lifter Raw after sediment in water Notified MOT_OWshy lOA

treatment b)plt1ss treatment bypass of scdimc nt filtcr in May 7010

16 Stmwbeny Ln MOT OW-5 Outsidc front tap Raw MtllE POE

MOT OWshy 13 Basement tank Raw POE for VOCs (TCE)

31-33 Blueberry Hill Rd Outsidc tllP on le ftMOT_OWshy 13C

WindmcTC sidc) Raw installed in 2009 Softcner

40 Blueberry Hill Rd MOT_OW-34 Outside rear tap Raw Softener

MOT OW-28 Basement tank Raw

Outsidc rear tap on left Raw after MOT_OW-28A aller disconnecting disconnect ing

41 lllucberry Hill Rd softener sollener Softcncr amp iron filtcr

Outside right tap aller Raw after

MOT_OW-28B disconnecting softcncr

disconnecting sollcncr

48 Blueberry Hill Rd MOT_OW-73 Outside rear tap on lell Raw No trcatmcnt

POE for VOCs c rCE) POU I Windmcrc Dr MOT OW-29 Bascmcnt tlUlk Raw lor As installed 2009

Softener

2 Wind mere Dr MOT_OW-33 Basement tank Raw Softener brine sediment

3 Wind mere Dr MOT OW-30A Bascmcnt tank Raw

No treatment MOT OW-30 Outside front lap Raw

4 Wind mere Dr MOT_OW-32 Basement tank Raw Sollener amp Mg

14 Windmcrc Dr MOT DW-35 Bascmcnt tank Raw Softcncr

Outsidc front tap on Raw after

35 Holman Way MOT_OW-94 left after bypassing treatmcnt bypass

Radon filtcr amp softcncr treatment

40 Holman Way MOT_DW-9 1 Outsidc rear tap on Icft Raw Carbon treatment amp water softcner

54 Parkcr Rd MOT DW-92 Bascmcnt tlUlk w Softcncr

59 Parker Rd MOT_OW-96 Basement tank Raw Radon filter

75 Parkcr Road MOT DW-97 Outsidc front tap Raw No treatmcnt

83 Parker Rd MOT_OW-93 Outside front tap on rilht

Raw Filtration system

86 Parker Rd MOT_OW-99 Basement tank Raw Charcoal filter Bypass is broken

127 Parker Rd MOT_OW-IOO Basement tank Raw Radon treatmcnt

24 Rand Drivc MOT_DW-98 Outsidc rear tap on

Raw No trcatmcnt ri ht

I

GZA GtoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

TABLE 3 -JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSSAMPLE VOLUME PRESERVATION AND HOLD TIME

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

TABLE 3 - JUNE 2010 MEDIA ANALYSIS TEST METHODS CONTAINERSI SAMPLE YOLUME PRESERVATION AN D HOLD TIME

Mottolo Superfund Site Raymond New Hampshire

PARAMETE R MATRIX NUM BER OF SAMPLES (including lield QCI ODdl)

ANALYTICAL METHOD

SA P SOpJ

CONT AINERS (size lind tyl)C)

PRESERVATION REQUIREMENTS4

MAXIMUM HOLDING TIME

RESIDEil1AL DRlNKING WATER

VOCs

Drinking Water

21 fi eld samples 2 duplicates 524 A-6 3- 40mL VOAI1 Hel 4degC +_2degC 14 days

T olal Arsenic

21 field samp les 2 duplicates

2008

A-6 1- SoomL plastic HN03 4degC +_2degC 6 months

Calcium

2007

Iron

Magnesium

Manganese

Sodium

Uranium 2008

Alkalinity

21 fi eld samples 2 duplicates

SM 23200

A-6 1- SoomL

plastic 4degC +_2 degC

14 days

Chloride Laehat 10-117-1-8 28 days

NitratcIN itritc Lueha 10-107-04shyI-e

48 hours 1t

Sul fate Laehat 10-511 -00shyI-A

28 days

Total Organic Carbon

21 field samples 2 duplicates 4153 A-6 3 - 40mL amber

VOA H3P04 4degC +_2degC 28 days

Notes

Nitrate samples must be delivered to the laboratory by 2pm on Fridays

1 Trip blanks will be included wit h each cooler containing VOC samp les and 14-dioxalle samples Trip blanks will include HCL-preserved blanks for aqueous VOC samples and unpreserved blanks for aqueous I A-dioxane samples (2 VOA Vials each) There will be one lemperarnre blank per cooler

2 Refer specifically to Table 5 for equipment blank details as well as other QC sampling requirements 1 f dedicated sampling equipment is used (ie tubing) an initial equipment blank is required No additional equipment blanks arc required for dedicated equipment If non-dedicated sampli ng equipment is used one equipment blank per sampling event will be requi red

3 The sampling SOP appendix is referenced for the appropriate media 4 Note that the pH requirements for samples preserved via an acid are less than 2 units

04002446641 GZA GeoEnvironmental Inc

TABLE 5 - JUNE 2010 SUMMARY OF QUALITY ASSURANCE SAMPLES TO BE COLLECTED

TABLE 5 - JUNE 2010 SUMMARY OF QUAL ITY ASSURANCE SAM PLES TO BE COLLECTED Monolo Superfund Sile

Raymond New Hampshire

SAMPLING MEDIA SAMPLING

FREQUENCY

ASSOCIATED SAMPLING

EQUIPMENT SAMPLE ID

DESIGNATED NOTE TO BE USED ON

CHAJN-Of-CUSTODY ANALYSES

EQUIPMENT BLANK SAMPLES

No equipment blanks for the June 201 0 resident ial sampling event

DUPLICATE SAMPLES

Drinking Water June 2010 NIA

MOT OWmiddotI3C OUP 3-33 Blueberry Hill Rd YOCs Total Arseni c Ca Fe Mg Mn Na U Alkalini ty Chlori de NitralcNitrilc Sulfate amp TOe

MOT_DW-29 DUP J Willdmere Drive

TRIP BLANKJTEMPERATURE BLANK SAMPLES

Aqueous VOCs (1 per cooler with aqueous

VOCs sampl es) June 20[ 0 NIA TRI P BLANK

ldellfiJY all Sample IDs associafed willi Trip Bialik illlotes section oreGe

voe

Temperature Blank (I per coolcr)

June 201 0 NIA TEMP BLANK

Inelude illloies sectioll of CDC Ihal a temperalire blank has been ineluded in fhe cooler

Temperature

Note

I Analyses include Volati le Organic Compounds (VOCs the New Hampshire Department o f Environmenta l Services [NHDESj full list) analyzed by EPA Method 524 and 14 Dioxane analyzed by EPA Method 82608Arsenic by EPA Method 2008 and Calcium Iron Magnesium Manganese and Sodium by EPA Method 2007 Alkalinity Chloride NitratclNitrite Sulfate and Sulfide by SM 23208 Lachat 10-117-07-1-8 Lachat 10- 1 07-07-04- I-C Lachat 10-51I-00- I-A and EPA Method 3761 respectively and Tota l Organi c Carbon (TOe) by 4 153

04002446641 GlA GeoEnvironmental Lnc

TABLE 5 - JUNE 2010 SUMMARY OF QUAL ITY ASSURANCE SAM PLES TO BE COLLECTED Monolo Superfund Sile

Raymond New Hampshire

SAMPLING MEDIA SAMPLING

FREQUENCY

ASSOCIATED SAMPLING

EQUIPMENT SAMPLE ID

DESIGNATED NOTE TO BE USED ON

CHAJN-Of-CUSTODY ANALYSES

EQUIPMENT BLANK SAMPLES

No equipment blanks for the June 201 0 resident ial sampling event

DUPLICATE SAMPLES

Drinking Water June 2010 NIA

MOT OWmiddotI3C OUP 3-33 Blueberry Hill Rd YOCs Total Arseni c Ca Fe Mg Mn Na U Alkalini ty Chlori de NitralcNitrilc Sulfate amp TOe

MOT_DW-29 DUP J Willdmere Drive

TRIP BLANKJTEMPERATURE BLANK SAMPLES

Aqueous VOCs (1 per cooler with aqueous

VOCs sampl es) June 20[ 0 NIA TRI P BLANK

ldellfiJY all Sample IDs associafed willi Trip Bialik illlotes section oreGe

voe

Temperature Blank (I per coolcr)

June 201 0 NIA TEMP BLANK

Inelude illloies sectioll of CDC Ihal a temperalire blank has been ineluded in fhe cooler

Temperature

Note

I Analyses include Volati le Organic Compounds (VOCs the New Hampshire Department o f Environmenta l Services [NHDESj full list) analyzed by EPA Method 524 and 14 Dioxane analyzed by EPA Method 82608Arsenic by EPA Method 2008 and Calcium Iron Magnesium Manganese and Sodium by EPA Method 2007 Alkalinity Chloride NitratclNitrite Sulfate and Sulfide by SM 23208 Lachat 10-117-07-1-8 Lachat 10- 1 07-07-04- I-C Lachat 10-51I-00- I-A and EPA Method 3761 respectively and Tota l Organi c Carbon (TOe) by 4 153

04002446641 GlA GeoEnvironmental Lnc

UPOATEO NHOES CHAI N OF CUSTOOY FORM

NH DES LABORATORY SERVICES LOGIN AND CUSTODY SHEET (Laboratory Policy Samp les IlOI meeting method requi remell ts will be analYLcd ullhc discretion of the NH DES Laboratory)

Samples must be delivered in a cooler with ice or ice packs LAB ACCOUNT (Bi ll ing) 04-0002104 One SlOP (PROJECT) 10 SUPERFND DES Site Number 198704094 Temp 0c __ Description MottoJo Superfund Site Town Ravmond NH NHDES Contact Drew Hoffman (603) 271 - 6778 Sharon Pt-kins (603) 271- 6805 Comments GZA Contact Michael Asselin (603) 232-8739 Amy Doherty (603) 361-4222

Collected By amp Phone Amy Piscopo (603) 232-8756 Tanya Justham (603) 493_1 548 Jessica Meeks (207) 233 0693 -

Qthe

ibull~ ~B

~ I~- ~Date Time ~sample Location lID Ii~ f~i u Lab ID Sampled bull N CommentsU

~ ic e ( For Lab Use Only)~tB~ _ lI _ I0 cis - Jo~ shy

~ 62

PItStITil lion AQucous VOCs HC[J4degC +middot2degC Me1alsHardness HNOJ4degC +2degC Toe H3P04i4degC +1C All other containers 4degC +2degC o Tcmperature Blank Included in Cooler Relinquished By_____________Datc and Time _______RlCc ivl([ By NUDES Laboratory Ilia cumer Matrix A~ Air S= Soil SED~ Slxl i mltnts A AqueousOthCf_

Relinquished By_____________Datc and Time_______Rcccivcd By________

Rclinquishti By_____________Datc and Time _______ Recd H lIlor LHbotory Br _____

PHge __ __ Data Rcvicwed By ___________ Datc_____

Section No_ 22_0 Revision No_ 6 (HWRIJ) Date 4middot8middot10 Pagc I of I

1. barcode 468354
2. barcodetext SDMS DocID 468354

NH DES LABORATORY SERVICES LOGIN AND CUSTODY SHEET (Laboratory Policy Samp les IlOI meeting method requi remell ts will be analYLcd ullhc discretion of the NH DES Laboratory)

Samples must be delivered in a cooler with ice or ice packs LAB ACCOUNT (Bi ll ing) 04-0002104 One SlOP (PROJECT) 10 SUPERFND DES Site Number 198704094 Temp 0c __ Description MottoJo Superfund Site Town Ravmond NH NHDES Contact Drew Hoffman (603) 271 - 6778 Sharon Pt-kins (603) 271- 6805 Comments GZA Contact Michael Asselin (603) 232-8739 Amy Doherty (603) 361-4222

Collected By amp Phone Amy Piscopo (603) 232-8756 Tanya Justham (603) 493_1 548 Jessica Meeks (207) 233 0693 -

Qthe

ibull~ ~B

~ I~- ~Date Time ~sample Location lID Ii~ f~i u Lab ID Sampled bull N CommentsU

~ ic e ( For Lab Use Only)~tB~ _ lI _ I0 cis - Jo~ shy

~ 62

PItStITil lion AQucous VOCs HC[J4degC +middot2degC Me1alsHardness HNOJ4degC +2degC Toe H3P04i4degC +1C All other containers 4degC +2degC o Tcmperature Blank Included in Cooler Relinquished By_____________Datc and Time _______RlCc ivl([ By NUDES Laboratory Ilia cumer Matrix A~ Air S= Soil SED~ Slxl i mltnts A AqueousOthCf_

Relinquished By_____________Datc and Time_______Rcccivcd By________

Rclinquishti By_____________Datc and Time _______ Recd H lIlor LHbotory Br _____

PHge __ __ Data Rcvicwed By ___________ Datc_____

Section No_ 22_0 Revision No_ 6 (HWRIJ) Date 4middot8middot10 Pagc I of I

1. barcode 468354
2. barcodetext SDMS DocID 468354