ww engineering & science, · collected during january 6.7,8.1992 at the cam-or site (wells bl....

.WW Engineering & Science,5OiO ?,or:e M..: Hoac • 3.ooin.r.i;:::r. N -,7,.

March 26, 1992

Mr. Robert J. Boklund. MSESAdministrator 0 <" n A n «iLaPorte County Health Dept. " > u J - o 14th Floor - County ComplexCourt House SquareLaPorte, IN 46350

Dear Mr. Boklund:

Re: Cam-Or site.ground water sampling results (Dames & Moore;

Enclosed are two tables of analytical results for the ground water samplescollected during January 6.7,8.1992 at the Cam-Or site (wells Bl. B2, B4), and fromHealth Dept. wells in the vicinity of the Cam-Or site (wells LP1, LP2. LP3). Table 1presents the results of analyses performed by National Environmental Testing, Inc.(NET) under contract to WW Engineering & Science (WWES). Table 2 presents theresults of analyses performed by EMS Heritage Laboratories (EMS).

A discussion of the results of the NET analyses was presented to the Health Dept.in a WWES technical memorandum dated March 17.1992. The WWES report statedthat several volatile organic compounds (VOCs) and mercery were detected in B-seriessamples at concentrations above die current or proposed Primary Maximum ContaminantLevels (PMCLs) established under the Safe Drinking Water Act, and that one VOC andnitrate were detected in a sample from well LP1, also at concentrations in excess ofcurrent or proposed PMCLs. Neither semfvolanle organic compounds (SVOCs). orpolychlorinated biphenyis (PCBs) were detected in samples from the B-series or LP-series wells.

The EMS results (Table 2) for VOCs, SVOCs, and PCBs corroborate the findingsof the WWES technical memorandum. Several VOQ were detected in samples from theB-series wells in concentrations exceeding current or proposed PMCLs. No VOCs were

detected in samples from the LP-series wells. Neither SVOCs or PCBs were detected insamples from the B-sehes or LP-sehes wells. From the available data, it appears that theEMS analyses did not include inorganic parameters other than sulfide. Further, theanalyses for dissolved metals appear to have been limited to arsenic, barium, and lead(Table 2). Accordingly, it is not possible to evaluate the above PMCL detections ofnitrate and mercury noted in die WWES memorandum widi respect to the split samples.The use of such a limited number or inorganic and dissolved metals parameters is notsatisfactory for characterizing the quality of ground water.

In summary, the EMS data confirm, in a large measure, die presence of VOCs inthe ground water beneath the Cara-Or site, but fail to provide much information withregard to the inorganic and dissolved metals parameters. We continue to recommend re- ,.sampling of the LP-series wells for VOCs. We further recommend that the Health Dept.notify the Indiana Dept. of Environmental Management and the U.S. EnvironmentalProtection Agency of the results of both the NET and EMS analytical results.

If you have any questions, or need further information, please feel free to call me.

.Flores,CPG

L.;Porfe County Hearth CeparmentG ounc Water Barreling - Can Cr snssampling catas: _anuary 6, 7, 3,1992

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TABLE

a County K-eaitn LJ

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Parameter 1

sutfttnSCSCSCSeWpi- leaT«rrc.

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81 32

,1 .1NO CAT. NO DAT.NO CAT NO DAT,NODAT MO DAT.SO CAT. NO CAT,

• d.COBO <0.0050

<O.OO50 -.13.0050

0.0283.003E 0.1 CO

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Porter-Lakes Engineering, Inc. map (5/6/87V No scale was given on the original.

vx»6LLLOCATION AND EL 6V. OFTo?\^\m,

PORTER-LAKES ENGINEERING. INC148 Johnson Drive • Valparaiso, IN 46383

Phone: (219) 464-9264

.OWO.NO..- S

DRAWN BY:

Dames & Moore from the desk of

Tom CovilH

Scrvict location

•MS HERITAGE LABORATORIES, INC.1219 MARQUETTE DRIVEROMEOVILLE, IL 60441(708)378-1600

^tctivta09-JAN-92

17-OAN-92Printtti

18-OAN-92

.30 ::C12=52iPO Nunctr

swpin i08 -JAN-92 11:20 !

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OAME3 i MOORETOM COVILLI11356310 LAMAROVERLAND PARK, KS 66202

Bill To

DAMES i MOOREJOHN GROSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 63146

Siitavs 3tscr;st:onDESCRIPTION: SITE WELL 3-2SAMPLE I.O.: CAM-MW-B2

WVOLATILE ORGANIC* SW846-8240Analyst: U. OIAZ Analyst* 0«t: 13-JAM-92 'nstranntr. SC/MS VGA Ttst: 0910.3. 0

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1,2-OIGHtOROETMAHE - 11,1-DICHLOROETHENE

ETHYLBEHZENE —=2-HEXANONE '"" ' .......,,,..,,,,, .,,.,,,,,

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EvirrE-.ITASt LASOR.i'CRIES, INC.

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, VINYLACETATE 3DL

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: VOLATILE ORGANICS SW846-8240' inatyit: U. OIAZ Analvsia Oaca: 13-JAH-?2 InstruMnt: GC/MS VQA T*st: OS 10.3.

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ACROLEINACRYLONITRILE

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; 3ROMOFORM3ROHOMETHANECARBON OISULFIDE

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1.1.2-TRICHLOROETHANEVINYL ACETATE "VINYL :HLORIDE:-;^ -vv:XYLENE (TOTAL)

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ua/Lpaae ',

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GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW845-35IO.Analyst: 0. 3AOCUS Analysis Qatt: 13-JAN-?! Ttst: P223.5. 0

PiraMittrINITIAL WEIGHT OR VOLUMEFINAL VOLUME "_____

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INITIAL WEIGHT OR VOLUMEC T U •% I"" if Af**r inMk vVb A..../ ^^^

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GFAA ACID! DIGESTTOM-(P1SSOLVED?METALSXAQUEOUS

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! LEAD•arsMtar

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Page 3

•V.S' HERITAGE LABORATORIES. INC. :..a: S i -c 'a :i: :::::':ARSENIC GFAA SW846-7060 ' '• ' '*Analyst: «. KCSZA, JR. AnaCysis Oact: *i-jAH-?2 Irsmasentr 3FAA Test: *1C3'.2. :

Prep: GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846-3020ParaMttr

ARSENIC BDLJ Get. Linit ! Cn;:s1 0.0050 1 ra/L :

BARIUM FAA SW846-7080^ . . • \ --. .- . :'*'.^. -;;,, .^:.^'c^ v-'^ • ' 'Analyst: A. STOOCBUUCa :-: Analysis Oact: 13-JAN-91 Instrument! FAA; . : :; Test: M104.1. 0

Prep: FAA OR TCP ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846 -3005ParaiMttr

3ARIUM! Result1 3DL

i Oct. Limit i UnitsC.20 ! TG/L

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst: A. LEMONCZU.O Analysis Oact: 10-JAM-92

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

! itesul:780

! 10

Test: P233.U 0Oet. Limit | Units

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080. nalyst: A. LSWMCELLO Analysis Oatt: • 5- JAN-92 !nstr.atnt: 3C/SCT^^Pre?:. GC SEPARATORY FUNNEL LI QUID -LIQUID EXTRACTION Sy846-3510

ParameterPCS AROCHLOR 1016PCS AROCHLOR 1221SPCS AROCHLOR 1232PCS AROCHLOR 1242PC3 AROCHLOR 1248

; PCS AROCHLOR 12541 PCS AROCHLOR 1260: PCS AROCHLOR 1262

BDL• ' 'SOL :" ' ' " " " "

SOL

BOL

BOL: BOL " " : :--"""

Test: 0331.2. 3

Set. -imit units0.003 I na/L0.015 ! mg/L0.003 i mo/L

i 0.003 mg/L0.003 ma/L

;. OiOOOS!; mg/L ;: 0.0006 ma/L :

i 0.. 0006 na/L

SULFIDE SW846-9030-I Analyst: T. NONA. ;':":;;

ParameterSULFIDE

• . Analysis. Date-. 10- JAM-92 -.-^.. . . v,: . .•'v-':--^''"" ' ::"Result

BDL

Test: 6110".4-. 0 iOet. Limit Units ,

1 ma/L 1„

Staple 'COSMIC*BDL Below Detection UnitcST Estimated Value- , •

5a«o7e chafn of custody number 1687. —————————————————— __ —————————————

Quality Assurance Officer: > / Last Page

Str/ics (.stationEMS HERITAGE LABORATORIES, INC.1219 MAROUETTE DRIVEROMEOVILLE, IL 60441(708)378-1600

• 09-JAN-92 ' Cli ,

\ 1

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5-JAN-92Printta

7-OAN-92

?o

= ::•lZZt.1Nunecr

06-OAN-92 12:40 S

Rtmrt To

DAMES i MOORETOM COVILLI51356310 LAMAROVERLAND PARK, KS 66202

Bill To

OAMES 1 MOOREJOHN GROSSMAflSUITE 24011701 30RMAN DRIVEST. LOUIS, MO 63146

DESCRIPTION: SITE WELL B-lSAMPLE I.D.: CAM-MW-81

oil

VOLATILE ORGANICS SW846-8240Analyst: S. SHARP Analysis Oact: :3-jAM-?2

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OICHLOROETHANE-D4 108-GLUENE-D8 ; 943ROMOFLUOROBENZENE ' 91

5 uc/L10 ua/L10 uc/L

5 ug/L

% Reci r. RSC

GC/MS SEPARATOR*; RJNNEL: LIQUID-LIQUID. (ACID EXTRACTION) SW846-3510in«lystr-:0...8ACXOS::V\*:— :-;-;;: " :>.Sx':-r;:::'-;- •••;.;-Anaiy»fsvOat«r- 13-JAII-92. •^••^- " - " ' " • • ' : ' . : . •' •': v Tast:. P233.S. 0 ;

PariMtar RasulINITIAL WEIGHT OR VOLUME 870-INAL /VOLUME .,-.y;^T---^^jo-^.-.---vw-v-..^-yv::^ :. :,;;,::1,, •••••••••••- -•::••

t Oat. Limit j UnitsmL ;

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•MI-VOLATILE ORGANICS (ACID FRACTION) SW846-8270^-inaivst: H. OIAN Analysis Data: U-JAM-52 trstrunant: GC/MS SVGA Ttst: C5!3.2. C

Prap: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-3510Paranatar \ Xasui

2-METHYLPHENOL BOLi-?lETHYLPHENOL ; SOLPHENOL • BOL

SURROGATE RECOVERY.. |

i e-FLUOROPHENOL 52PHENOL-05 --• 382.4,6-TRIBROMOPHENOL 52

: : Oat. Liait Unitsi 11 ua/L

11 5 ug/L11 i ug/L

' J

S Rec% Rec <% Rec ;

GFAA ACID DIGESTION (DISSOLVEO«HETAtS)-AqUEOUSvSAMPJ.ES^ I84e-3020 ?Analyst: H.:.MI«AUcu; --. - •••'-• • Ai»ly»ir Oatat «?JAIIs92 -^ • •••'•+<•.*•'-••. '•••••.••?--:: : .-....- 'TaBt:. P13J.«>.0 ••

ParaMtar RajiwOITIAL HEIGHT OR VOLUME ' 50 '

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It '* Oat. Liait UnitsmL

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lit Oat. Unit Units

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LEAD GFAA SW846-7421Anaiyst: K..MUO . Anslysis Oatt: H-JA»-»2 Instruaanci WAA Taatt H114.2. 0

Preo: GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW848-3020___ | •••M

LEAD *'""'* Bptult Oat. Limit Units

0.0050 ma/L

ARSENIC GFAA SH846^7060•.•.-.-.-:• •/-. " . • • . • MA • «•••, » __ _ _ kj«f|V 9 nAmilwtt ' '"KOBZA'*'' ' JH:'v'""-'y:'"' ';''''''::'"---:':' " •'••:- • ' * " Anftiwift 0*1(0* I** JAK*T4t • lltafTrUMftC X"CcJU» ' !•*•* • ™ iiu**« v

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Page 2

1^5- HERITAGE -.-.2C?.ATCRIiS. I N C .

BARIUM FAA SW846-7080Analyst: A. STCCXBWttH " Analysis Oatt: 13-JAM-92 ir.struBtnt: FAA :«:: «ici 'Qrep: FAA OR ICP ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW848-3005

ParaMttrSARIUM

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GC SEPARATORY FUNNEL .LIQUID-LIQUID EXTRACTION SW846-3510Analyst: A.: LEMONC5LLQ : Analysis Oatai 10-JAH-92 Ttst: P233.1. 0

PiramtttrINITIAL WEIGHT OR VOLUME:IHAL VOLUME- " -

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| POLYCHLORINATED;BIPHENYLS (PCBS) SW846-8080.| Analyst: A. LEMOHC6UO Analysis Oattr 1S-JAM-92 Instruntnr: CC/fO1 Prep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW845-3510

BDL Below Detection LimitEST Estimated VilueSample chain of custody number 1687.

SMplt Conamcs

Ott. Liait units

T«st: 030'..2. 0

ParaMttr?C3 AROCHLOR 1016=C3 AROCHLOR 1221PCS AROCHLOR 1232?C3 AROCHLOR ::1242J;;?C3 AROCHLOR 1248rtO MRHtnLUKv>:I.ZI)ft.v:v>.v; .-.::..-....-. . -PCS AROCHLOR 1260?C3 AROCHLOR:.1262

i %tsui:i BDL1 SOL

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i HOL. . . . ..--.• :.3DL:

1 3tt. limit'• 0.003

0.0150.003

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0:003 | ma/L {JC.003 rnc/L

0.0006 ma/L0.00060.0006

mg/Lma/L

SULFIDE SH846-9030; Analyst: T. NOHA

ParaMttrSULFIOE

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Ttst: 6110.1. 0, Ott. Limit ! Units '

1 ! ma/L

Quality Assurance Officer: ^- •*•" T -' - *> "Last Page 3

Strvict 1. oeat-.cn•".S HERITAGE LASORAfORIES, INC.-.319 MARQUETTE DRIVEROMEOVILLE, IL 60441(708)378-1600

C9-JAN-92

', 17-JAN-92 ! .| Printta 1! 18-OAN-92 '

.53 ::r- 2==?sn Mu-rs«r

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DAMES i MOCRETOM COVILLI?1356310 LAMAROVERLAND PARK, KS 66202

Sill To

Z.-.MES i MCCRE•JOHN GROSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 53146

DESCRIPTION: SITE WELLSAMPLE I.D.: CAM-MW-34

:tic.-i=:icn

VOLATILE ORGAN I CS SW846-8240Analyst: I. OtAZ Analysis Oatt: !C-:AN-?2

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STYRENE1 ,1 , 2 , 2-TETRACHLCROETHANETETRACHLOROETHENETETRAHYOROFURANTOLUENE1 , 2-OICHLOROETHENE" (TOTAL)

! TRANS-1.3-OICHLOROPROPENE1 1.1,1-TRICHLOROETHANE

!n»tnj»«nt: GC/MS '«A

rssm:3DL3DLBOL64 •BOLBDLBOLBOL:-v-"? ::,;;:M -:i;.:::BOLlini ^ ^ ^>^ —.,x-: ":: -.:::::.JJUb: " ;s "::: : . : • ' . v:-:::-:-:v.::;x--Xv •EST 130a 4.tJUt£»-™>Xv »»: :-* v->>x"-:vX™v>Xv :»«»BOL ^

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i ua/LPage .

-•- • • - • • • • 1 ... „_ . . - ... ...;;_;

?*ra.it*:er1,1,2-TRICHLOROETHANE--ICHLOROETHENE •: 'VINYL ACETATEVINYL CHLORIDE.XYLENE (TOTAL)

SURROGATE RECOVERY

0::HLGROETHANE-D4-CLUENE-D8SRCMOFLUOROBEHZENECompounds outside of the calwas rerun at a dilution for

iI

;

ECLSOL i3CL !

BDLEOL

1129235

5 uc/L10 uc/L

.:.:..,:.:.. 10. UC/L j5 uc/L

,;..,,;,-;,.. !

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", ™ 3 r

ibration range are reporrsa as estimated. Samolethose compounds.

VOLATILE. ORGANIC* SW846-8Z40Ar»iy«: '.. OlAZ Analysis Qatt: *5- JAM-52 Irstruatnt: GC/J«S VOA Ttit: C510.2. ''

ParancttrACETONEACROLEINACRYLONITRILESENZENE3ROMOOICHLOROMETHANE3ROMOFORM3ROMOMETHANECARBON OISULFIDECARBON TETRACHLORIDECHLCROBENZENECHLOROETHANECHLOROFORMCHLOROMETHANEOIBROMOCHLOROMETHANECIS-1, 3-OICHLOROPROPENE

1 , 1 -OpL< ETHA|IE^ ^

1 , 1 -DICHLpRQETHENE ____

ETHYLBENZENEFLUOROTRICHLOROM^THANE;2-HEXANONEMETHYLENE"CHLORIOF •METHYL ETHYL KETOKE4-METHYL-Z.-PENTANOIIE::STYRENE1,1,?, 2-TETRACHLOROETHANETETRACHLOROETHENE. .

TOLUENE1 , Z-OICHLOROETHENE - (TOTAL)TRANS- 1 , 3-OICHLOROPROPENE1,1,1-TRICHLOROETHANE1,1,2-TRICHLOROETHANETRICHLOROETHENEVINYL ACETATEVINYL CHLORIDEXYLENE (TOTAL)

^•sut: iBOL !3DL :3DL

. ' 73 i2DL

. 3DL2DL :

'. BDL. BOL i1 8DL.i 2000 :.BOL; ;-.-; ...

iBDL . . . ........................Rni' :,.,. . .^.,-.x-;v^v,v, .VV..V,.

•X!1-!vr-"->>>;X<v>X>/.vi!V''\\IX:"/Xv^>-v • •/••"• •"•-'X-!

~,rt.......... ....................... ... ,. . . .,......,

«-

BOL•QfjrvX~™X'SS!lv1' v...;.x.fe.v.-.y.v.v.v.v.v.v.v,v.-i.y

300* - -•

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,.__ ,

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BOLam ••BOLBOL . • ; • • • ' ;" --.:: e:

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Oct. '. irait . Jni:s200 : UO/L \^500 | ug/L700 ua/L

50 ua/L£0 . uc/L50 : ua/L

100 ; ug/L50 ua/L50 ua/L50 i ua/L

100 i ug/L: -50 UQ/L ;

100 ug/Li.,::>.::-: 50 Ug/L .. :

50 ug/L t

50 ug/LM^Ste^g/L ^

50 ug/L1^ §?^Sw50S Sji^L'x/.y'V .:^ ^ _ 50... ..ug/L. .

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^.;±:xv:vv'v/ioo '; -ug/L50 ug/L

> v; x 50: ; ug/L.50. .ug/L

Pv"':::: :lZ50fc -ug/L.50 ug/L

:: "50" Ug/L50 ug/L

50 ug/L> v y 50 Ug/L

100 ua/L• 100 ug/L

50 ua/LPage 2

N C .Parameter

:'l?.SCGATc RECOVERY *

OICHLOROETHANE.-D4.7GIUENE-D85ROMOFLUORC3ENZENERe- analysis at a 1:10 dilution

11

ill. - . .. '• .,,, '•;'•10692 ' • •> ' : • • : : •

•

•i- "• Rec 'V. Rec !"• Rec i

i

GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-3510.raiyst: 3. BACKUS Analysis Oati: -3-JAN-92 T«st

ParamttarINITIAL WEIGHT OR VOLUMEFINAL -.VOLUME^^^W"----""-

Hasul: Da?.810

.-.., •..-.— ..,.:... . • . - . •- • ,..;j ....,.,.. .::. ,..;.:.; ....,,,.v;.:: ..,A:..,;,..........y.,. .,...,..,..,

'233.5. Q'.iait -nits

'••- • ' • ' . : i ml

SEMI -VOLATILE. ORGAN ICS (ACID FRACTION) SW846-3270;*r.aiyst: H. QIAN Analysis Satt: ', i-JAN-92 tnstrunantr GC/MS SVOA Tast: CJ1&.3. 0orao: GC/MS SEPARATORY FUNNEL LIQUIO-LICUID (ACID EXTRACTION) SW846-3510

^-^ Parameter2-METHYLPHENOLA-METHYLPHENOLPHENOL

SURROGATE RECOVERY

2-FlUOROPHENOLPHENOL-052.-1.5-TRIBROMOPHENOL

i Rasut; . Oat.3DL50L 1 •3DL

5344- ,. ,. . . i75

'.iait? . ^n;T312 uc/L12 ua/L1.2 i. ug/L

< % Rec; r. Rec

GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES:,SW84e-3020> v •Analyst: H. RANOALL Analysis Oats: 11 -JAM-92 • . . ; : • • fast: P133.fr. 0 •

INITIAL WEIGHT OR yOLUMERasult Oat.

50............. ........ ... ....... ..„..,......•. .,...„., ••)? ^*"*-'"*""****"jsy*"""***.a--jp'"""'"""' ••••-*••** '••••jLvrjsii..••.V.V....V.'.7..V... •.•.*.•.•-"'••••.•••,•"••.•.•.-.••.•.•.•.•.•.',•.•."••" •ff^^t'ff^."'--ff!XffSffu^.'»"ffVXffSSff*ftff£ffff.Vff:£y: V."V.T.'Sr

. _~ - .

GFAMACIDIDIfiESirOJffDlSSOkVAnaty«ts:-l iuiNbMJ^^^^W^^

Rfj-amatsrINITIAL WEIGHT OR VOLUMEFINAL' VOLUME- l P^ P^ ^

Ramilt I Oatso . ..:„..!.......„.... .. L_.. ........... ........... .. . .... . . . ....... ...... **SJB> A •"*".'.'.*.*.. • vA v/MV."MV.v/ v«v.vAVl .T . ".v/. ^TwV. |?.v•v.v.v.

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™rS>Xv»X-»Xv.v4::inL-v.~.v v j

^ ^ PIS? '?Z "• • v •:::.-.• j5j«ivpji j |fj *S::--;.. .• • |

I Lisrtt Units 1. ^^ ..iV,,.,.. J

j FAA OR ICPrACm^OMESTIOir (DISSOLVED METALS) AOAJEWS SAMPi:E^^846|3^^^ :*tr! Analyst: 1. HmiLL • . Analysis Data: 13-JAK-9Z •:: '.T^ --- ; 1S^ ^ aa«^>'tSaiK .flT-*' '"I •aramatar1 INITIAL WEIGHT OR VOLUME! FINAL VOLUME

Rasult5C

Oat. Limit UnitsmL

LEAD 6FAA-.SW84C-7421-. - . - . . . . -Sr " '••^v:^*^^^; • , • -Analyst: ».,MUW-«; : Analysis Data: 13-JAM-W Instnaants VUn.'" ;'\ .r Ta«t: M1U.2.

Prgp; GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846-302C0 .«

1 LEADtcr

BOLOat. Limit

0.0050Units

ma/L

Paae

E^S HERITAGE _. -5GnA. I3.Ii-ARSENIC GFAA- 5W846-7060Analyst: R. KC82A, JR.. ' Analysis Catt: ' i -JAH-yZ Iratr-Jiunt: GrAA°res: GrAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846

Ttst: H133.2. C3020

ParaiMttrARSENIC

ResultBOL

Ott. '-imi:0.0050

Unitsma/L i

BARIUM FAA SW846-7080Aralyst: A. S7Cae8U«G8il Analysis Data: 13- JAM-92.- Instrunant: FAA : >;. • " - .?rao: FAA OR ICP ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES

-., : Tast: M104.V. 0SU846-3005

Piraiwcir I3GL

0«t. '.isiit i '.'nits" 0 : ~X i

GC SEPARATORY FUNNEL.LIQUID-LIQUID EXTRACTION SW846-3510Analyst: A. IE.10NCSU.O Analysis Date: 10-JAM-92 Tast: "233.1. C

ParaiMtarINITIAL WEIGHT OR VOLUMEFINAL VOLUME_________

! 900I ' i o0«t. Uni :s

ml

POLYCHLORINATED BIPHENYLS (PC8S) SW846-308Qanalyst: A. Ls.HOMCSLL3 Analysis 3at«: !i-JAN-92 '.nstrjat-:: 3C/SC5Prso: GC SEPARATORY FUNNEL LIQUID-LICUID EXTRACTION SWSio-3510

Tsst: 0301.2. 0

PCS?C3PCSPCS

! PCSi PCSi PCS

?C3

AROCHLORAROCHLORAROCHLORAROCHLORAROCHLORAROCHLORAROCHLORAROCHLOR

Paranatar1016122112321242124812S4-> 'I,:-. :•'••"•" . - • • - ••• ' . .12601262

Stsut:i BDL'...SOL.1 BDL{ BOL •-•-;

... ... J.BOL . .

! BOLi- BDL ••--.: c :

3«:. . i.-ni:i 0.0006' 0.003

0.0006••-. 0.0006i 0.0006

: :: !: o;ooo51 0.0006

• : ; • ! • . 0.0006

•Jp.its! mg/L! iw/L, ag/'.rng/L.I..-I/Li mg/Li mg/Li rr.a/L

SULFIDE SW845-9030Analyst: T. NONA Analysis Data: 10-JAH-92. Tasti. 8110.C. 0

1 SULFIOEPara«atar Hasult Oat. Uric

1! UnitsIraa/L

i

BDL Below Detection LimitEST Estimated

Saopla Ceanants

Samole chain of custody number 1687.

Quality Assurance Officer: Las. Page

o T 3 A N A '_ v 3 : t

Service LocationEMS HERITAGE LABORATORIES, INC.1319 MARQUETTE DRIVEROMEOVILLE, IL 60441(708)378-1600

• Seceivea

09-JAN-92CSOQlttl

15-JAN-92

17-JAN-92

.as ;:C125525?0 Nucocr :

Saoottd ;

06-OAN-92 17:00 i

Report To

DAMES 4 MOORETOM COVILLI11356310 LAMAROVERLAND PARK, KS 66202

Silt To

DAMES 1 MOOREJOHN GRQSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 63146

Saral* Ctts.-i::icnDESCRIPTION: COUNTY WELL LP-2SAMPLE I.D.: CAM-MW-LP2

VOLATILE ORGANICSSW846-8240Analyst: L. BtA2: : : ; Analyvfs Oatv: 11- JAN-52 InstruMnrr OC/MJ. VOA T«*t: C510.3. 0

?aranwtarACETONEACROLEINACRYLONITRILEBENZENE3ROMOOICHLOROMETHANE :3ROMOFORMBROMOMETHANE

CARBON TETRACHLORIDECHLOROBENZENE • "•'•>>xv"-x-»:v:v '^'- -•;• ••^•;:\."^:t*^-^x~---.".^ ••/^••:\~~xCHLOROETHANE

^HLOROMETHANE

CIS-1 ,3-OICHLpRi:)IPTOP.!ENE._

1,1-D I CHLOROETHANE• i >>"/nTrui-'fti»ncnii'Me25K5s-Hvx~1 r4rUl|UrtLVKUtii:UMllKl H i1,1-DICHLOROETHENEi^m^msmmmiL-.^ETHYLBENZENE

•.-.-..•.-• -V . VV.Y. -W.V.V.- ••.-.•.- .-.•..-..•.•..•.•.•.•.-.-.•.•-.•.•••.•.•.•.

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'^^^^^^^^"-^^M^:^.^^^-

2-HEXANONE " " " ^"^ ***"""METHYLENE^CHLORtOE-METHYL ETHYL KETONE4-METHYL-2-PENTANOWESTYRENE1,1,2, IrTETRACHLOROETHANETETRACHLOROETHENE

TOLUENE1 , 2-OICHLdROETHENeCTOTAL)TRANS-1, 3-OICHLOROPROPENE1.1.1-TRICHLORO^THANE

3DL3DLBOL3DL ;SOLSOL 'BOLBOL; !BOL

BOL .. ,.

BOL * 'BDL"' '"•'••'•••••'z*-'—'"" •'•• • •••••••"•— •—•••••'•• ••••••'

J^**————**.- . v .

"BDL '"™" ~BOL

- roL —"*-"*••---"••••-•-^ ..,_,_„.„.,... ;.. ...............

BOL" •-..-••:BOLBOL :BOLBOLBOLBOL ::^;--:-:/ • : , • ; . ..

.BOL

BOLBDL

20 ua/L50 ua/L70 ug/L

5" ua/L ;= ua/L !5 ug/L ;

10 j ua/L !5 ug/L |5 ug/L !5 ug/L !

10 ug/L ;:e : v :J : ug/L' ...... .. . . ..** -W9r ••

10 ug/L

^^,.^jg/L_:/

izizi'i cr,................. ...5 .ug/L...

5 ug/L:-™. 7-:rS..^g/L

10 ug/L5 ug/L.

10 ug/L10 ug/L

S ug/L5 ug/L5 ug/L

25 ug/L5 ug/L5 ug/L5 ug/L5 ua/L

Pace :

— t* e ,,^^ » — «/- *- * « -»n"* i ^ " * t ' ~ t1. .5 .;!.-%* . n^c LncCr.M, r».li ,

1,1,2-TRICHLOROETHANE,TRICHLOROETHENEVINYL ACETATEVINYL CHLORIDEXYLENE (TOTAL)

SURROGATE RECOVERYv ' - v - • • - . • • . . - . • • .:::• - - • • • - - - • • -

DICHLOROETHANE-D47CLUENE-D8- ; ;; .3ROMOFLUOROBENZENE

<esui: 0«t. i-.ni:50L • ;SOL ; =BDL ; IQ80L . JoBOL 5

••"cv : : :xK"J . • • -":- V . !108; io591 :

..-: :suc/Lua/L iuc/Luo/L iug/L |

ii- • . . . ii

ft Rec% R=c". Rsc

| 6C/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-3510: Analyst: D. BACXUS Analysis Oat*: 13- JAM-92 Tascr P2J3.5.. 0

PirMWttrINITIAL WEIGHT OR VOLUMEr:NAL VOLUME

ftnut: ! o«t. Limit! 965 !n : . .... • • . . . • - . - • -

UnitsmL

= nL

SENI-VOLATILE ORGANIC* (ACID FRACTION) SW846-8270Analyst: H. 01 AN Analysis Catat K-JAN-92 tnstnjwnti CC/NS: SVGA. Ttsi: CS'S.3.

Prep: GC/MS SEPARATORY:FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-2S10

I-METHYLPHENOL•i-METHYLPHENOL

! PHENOL

! SURROGATE RECOVERY

t«r3DL3DL3DL

Stsui: 3tt. Linri? ' Units10 ' ug/L10 UQ/L10 : ug/L

; 2-FLUOROPHENOLi PHENOL-OS-:.:...;/;: ,;,,,..,... • ;.. .. .! 2.4.6-TRIBROMOPHENOL

233456

i % Rec1 ~. Rec :! % Rec •:

SFAA,ACIDDI6E5TIOHl(DISSOLVEa^METALS)Taat: . 0

ttrINITIAL WEIGHT QR VOLUMEFINAMVQiaME!—————

50KMUlt • Ott. Liiait Units

mLIt:

INITIAL WEIGHT_OR 50RMUlt Oct. Uric Units

—— .„.,., TOB;;.......PreprGFAA^AEIOiDIGE

tr ^5^*11. v?;hwirtsi lwiU:-''::'' ' •:-'faitt"Hlif:a;-."0-' ''".."METALS) AQUEOus^AHPtES^sn846-302o •.•: ?;•BOL

RMUlt 0«t.o.ooso

Units

ARSENIIAnalyst:Prtp:

ARSENIC

C GFAA SW84••' KOKA JK»GFAA ACID

16-7060

DIGESTIONftfl ••tar

Analysis Date: K-JAM-(DISSOLVEO METALS)

92 tnatruaantt. WAA . Twti N103.2. 0AQUEOUS SAMPLES SW846 -3020

nni ••suit Ott. Kail0.0050

Unitsnw/L

Paae 2

E^S HERITAGE LAECRATCRI-S, INC,

BARIUM FAA SVJ846-70aO * •'in«lv«t- A STOCK«l«CZjl Analysis 0*te: 13-JAN-5c Instrjiwntr FAA T«»t: M1C4.1. 2Prep: FAA OR ICP ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES'SW846-3005

ParaMttrBARIUM

RtsultBOL

Ott. Limit0.20

Units :ma/L !

GC. SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst-. A..IWONCSUa : Analysis Data: 10-JAN-92

POLYCHLORINATED^BIPHENYLS?(pCBS>^SW846-8080:Analyst:.: A.::LSMOilttUO^ ;: Analyii* D«c«r T4- JAM-92 rnstrtaantr:6C/6COPrep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510

T«st; P233.1. tt

INITIAL WEIGHTFINAL* 'VOLUMES

ORParanwttr

VOLUMEResult

800..-.•T **............-.... ..•..•..-....-.•...-..-..• ;i.u '""-'•' • • • • . ' . • • • . . • - • . • • • • • • • • • •

D*c. Linit 1 Units! mL! TIL

7«»t: 0301.2.. 0

PC3 AROCHLOR 1016Pn AROCHLOR 1221R , AROCHLOR 1232PC3 AROCHLOR 1242PC3 AROCHLOR 1248PC3 AROCHCORS1Z54'PC3 AROCHLOR 1260PC3 AROCHLOR 1262

Parnwttr Xtsult; BOLi EOL• £DL' SOLi 3DLI BOL! 3DL

j SULFIDE SW846-9030i Analyst: T. MONA Analysis Date: 10-JAM-92

Otc. limit . jm:$0.0006 j *g/L

0.003 mg/LQ.0006 I mg/LO.C006 | mg/LC.OC05 i mg/L0.0006 [mg/L0.0005 ; mg/L0.0005 i mo/L

T«s:: C',10.4. Q

SULFIDEittSUl*

iBDL'• S«t. '-'•'-

mg/L

0c7<w Detection Unit

c/>a/n of custody number 1687.

Quality Assurance Officer: Last Pace 3

Service Lccaticn ,EMS HERITAGE LABORATORIES, INC.1319 MARQUETTE DRIVERCMEOVILLE, IL 60441(708)378*1600

r 3ec«iv«o! 09-OAN-92| Csanttte

1 17-JAN-92| Printed1 1S-JAN-92

-33 '.2

C135527?Q Hurctr

SamDlta

06-JAN-92 13 :50

R«eort To

DAMES 1 MOORETOM COVILLI#1356310 LAMAROVERLAND PARK, KS 65202

3 i l l To

CAMES i MOOREJOHN GROSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 63146

DESCRIPTION: COUNTY WELL LP-3SAMPLE I.D.: CAM-MW-LP3

sit Ottertotion

VOLATILE ORGANIC S SW846-S240Analyst: 1. OIAZ Analysts Oat«: :j-;AH-92 Irwtrvawnrr SC/SS VGA Tut: 0510.3. 0

ParamttrACETONEACROLEIN iACRYLONITRILE !BENZENE3ROMOOICHLOROMETHANE8ROMOFORM8ROHOMETHANECARBON BISULFIDECARBON TETRACHLORIDECHLOROBENZENE - :-^^.^Z..;..^.;..siQ&&CHLOROETHANE

CHLOROMETHANE .

CIS-1, 3-DICHLbROPROpffir"U ILHLUKUUiMUUKOnttHANt-.v::: ^.zz^^t:^-^^.:~^:^~xtzx1,1-DICHLORO ETHANE1,2-OICHLOROETHAHE^M> ." r x1,1-DICHLOROETHENE1,2-OICHLOROPROPANEETHYLBENZENEFLUOROTRICHLOROHETHANE2-HEXANONEMETHYLiNEECHU3Rl1bEm:t x: llMETHYL ETHYL KETONE

STYRENEi , 1 , 2 , 2 -TETRACHLdROETHANETETRACHLOROETHENETETRAHYOROFURANTOLUENEI , 2-OICHLOROETHENE (TOTAL)TRANS-1.3-OICHLOROPROPENE1.1,1-TRICHLOROETHANE

BOL3DL :BOL iBOL8DL • :BOL ...-..; •BOLnni ........... ....::..ouu. . . . .BOLrtn |.4v!**; !3£5:vI-Iv! -IIvIvM* 'DU b>££X«>£v>£X -Xv >.v

BDL • •

BDL.m___

BOL "" "

BOLiBOLlii ^BOL

•i»nr i xffix-x:^• OUU. • .: :viv.v.v.— •BOL,goL

iBOLi y«BOL

?BOL^ i ..:'-^xBOLiBOL: ;::->•

BOL

»

.-xv»: :-™KV~ v™-

.- • .*. .:::• v.y.v.v.v.v. •.•.-.•:

QQI . • • . . ..•••••.•.....•.•.-.•.•.•.•.•.•.•

BOL

BOLBDL

205070

5

10:.• .. :. . : . ; . : . 5,

........................ 5

_ 10

izrrii.............. ....5

rrmio"""7 'io

,.,,.,:,,v,,, 5

.'.'•'.:.:'.':• '..'. •" -• C

5•.•••.•..-... • "2S

5•...^•••-•: '5

55

un; :suc/ Luo/Lua/Lua/Lua/Lug/L

ug/L !

ug/L ;ug/Lug/L-%/L;..—ug/Lv..

Ig/Lt:ug/L

?Sg/Lug/L

ug/Liug/L:

ug/Lug/Lug/Lug/Lifig/Lug/L

ug/Lug/Lua/LPaae

>3 «L L.~.i.w."sn i

Parameter1,1,2-TRICHLOROETHANE.TRICHLOROETHENE 8r ;

, VINYL ACETATE• V T M V I PKI fiPTHP --'•"»;•: - : : . . . : • . : : • • . : . . • • ;-...

! XYLENE (TOTAL): SURROGATE RECOVERY

3ICHLOROETHANE-04. "TOLUENE-OS! 5ROMOFLUOROBENZENE

SOLSOLBOLnniSOL

• - . • . ' • : • - . . . ' . . :. . .

'.'109gg

C

. . . . . . ..10::•:,,;_,;. 10

5

ua/Luc/Lug/L !ua/L 1

i. . . (

% ""Rec !

i % Rec% Rec

GC/MS •'. SEPARATOR^ FUNNEL LrQUID-LIQUID (ACID EXTRACTION )AnalystrO. MOOJS; AnmLysfs Qatar 1S-JA»-91.: :T«sc: P233.5. 0

ParsMttrINITIAL WEIGHT OR VOLUMEVOLUME •••;•:: ": 940

itMUtt j 0«t. Limit i Units! mL

-VOLATILE OR6ANICS (ACID FRACTION) SW846-8270*n«iv»;: H. OIAN Analysts 3at«: li-JAM-92 Instrjwnti 1ZSXS SVOA Test: C3T3.3. 0?rsn: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-3510

:-METHYLPHENOL^-METHYLPHENOLPHENOL

SURROGATE RECOVERY

?ar»mattr=DL3DL

atsul:

2-FLUOROPHENOLPHENOL-052,4.6-TRIBROMOPHENOL 43

{ Oct. Limit { units10 ' ug/L

: 10 ; uc/L10 I ug/L

i • I

% Reci % Rec! r. Rec

GFAA ACID DieESTION (DISSOLVED.METALS) AQUEOaS: AMPLESiSW84e. ;:'• I :x-y;y. : : An>ty«fa """"' '' - "'

INITIAL WEIGHT OR VOLUME

GFAA ACIDlOISESTl...v . ..-.>;. *v^• •.-Av.:<-:-it5SftM&»!Analyst: K.:,RAHDAtl

INITIAL WEIGHT OR VOLUMEFINAL VOLUME ;^x "

RaMiit,&..........................._____

Oat. Units

FAA OR ICP ACID DIGESTION (DISSOLVED METALS)Analyst; I. NCRRtll Analysis Qatar 13-JA»-92

•sraMtarINITIAL WEIGHT OR VOLUMEFINAL- VOLUME mmmmmtm

taault50

Oat. li«itmLint

Units

LEAD GFAA SW84*-74Z1 • " -- ••••••:.•Analyst: N. MUIW • • • ' . Analysis Oaist

Prep; GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846?3020

fe/:.;;;^

.EADParajiatar

BOLRasult Oat. Limit

! 0.0050units

mo/L

Paca 2

rv«c urr^icr LAEOSATC-RIE3. INC.

ARSENIC GrAA SW846-7060Ar.alyst: ». KCtZA, M. * Analysis Date: 'i-JAN-92 Instrument: GfAA Test: "103.2. CPrep: GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846-3020

ParaiMterARSENIC

ResultSOL

Oet. Limit0.0050

1 '.'nits |1 ma/L 1

BARIUM FAA SW846-7080Analyst: A .. STOCXBUHG8* Analysis Oat«t 13-JAN-9t Insmjasntt:Prep: FAA OR ICP ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW84&-300S

Parameter3ARIUM 3DL

tisult I Set. Limit j• 0.20 :

'.'ntti

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-35IOAnalyst: A. LSHOMCStLO Analysts Oatt: 10-JAM-92 :

POLYCHLORINATED BIPHENYLS (PC8S) SW846-S080Analyst: A. LBtONCS'.LQ Analysis Oats: '--JAH-?; trstrxjeenti 1C/J3Prep: GC. SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510

T«st: PZ33.1. 0Parvwter

INITIAL WEIGHT OR VOLUME":*IAL VOLUME

I .Result880; 10

Oct. Limit j Uni:s1 mL

r- - :-L

Test: 0301.2. 0

PCS AROCHLORPCS AROCHLORPCS AROCHLORPCB AROCHLORPCS AROCHLORPCS AROCHLOR

' PCS AROCHLORPCS AROCHLOR

SULFIDE SW8Analyst: n now

SULFIOE

Parameter < Rtsui: . Set. L:1016 i SOL 0.1221 i BDL: 01232 i BOL 0.1242 i BDL j 0.1248 BOL ; 0.1254 BDL ."• 0.1260 ! BOL ! 0.1262'- " ' '" ^'- •<(' BDD'- '''' -'--^"''""''' ••'"•'•'••'••••• /;"' • • • ' ! • • • ' • ••'••Q-'

4&$S$!Mi&»^

mi : | Jni :s0006 ' ma/L.003 ; saa/L000600060006000600060006

mc/Lrag/Lmg/Lmg/Lma/Lmo/L i

-lf; -;.k;v:. ,':;: ..^ * ^<:?4 *lt;; il: iijHI 0;

ParsMtcr Remitt 0«t. Li>itBOL " •' 1

Unitsma/L

• ' _^"'

BDL Below Detection -Limit . . i

Saaiole chain of custody nuotar 1687.

Quality Assurance Officer: Last Page

A N-Z5"

Strvict I scan on

E.MS HERITAGE LABORATORIES, INC.1319 MARQUETTE DRIVEROMEOVILLE, IL 60441(708)378-1600

1 09-JAN-92 C12S52QCcfflplct t ?o Hmc r

17-JAN-92 .............. iTintad SamoiH .

18-JAN-92 08-JAN-92 14-Q8 I

atcort To 3ill To !

DAMES 1 MOORE DAMES i MOORETOM COVILLI JOHN GROSSMAM#135 SUITE 3406310 LAMAR 11701 BORMAN DRIVEOVERLAND PARK, KS 65202 ST. LOUIS, MO 63146

Samolt Otter ipt ionDESCRIPTION: DUPLICATE OF COUNTY NELL LP-1SAMPLE I.D.: CAM-MW-LP1-OP

VOLATILE ORGAN I CS SW846-8240Analvst: S. SH*«P Analysis 3att: 10-JAH-52 tnstruwnt: 3C/KS VGA Ttst: 0510.3. .8

ACETONE """* *ACROLEIN •ACRYLONITRILEBENZENE] ' •

1 BROMOOICHLOROMETHANE !BROMOFORMBROMOMETHANECARBON 01 SULFIOE-;- -••.••CARBON TETRACHLORIOE1 rui nonocuTCMC "'• ••• ••• • • •••••'••'•InLUKUDcN&blit •.-...•.

1 CHLOROETHANE, UOROFORM - -fTTHLOROMETHANE

C I S - 1 , 3:#][CHJL.p' ROTR^^

1 , 1 -OICHLOROETHAME """""

1 , 1-OICHLpROETHEHE ^ __ ..,.._.,..................ETHYLBEN2ENE ' ' ^"^"^ ————' "FLUOROTRICHLOROMETHANE2-HEXANONEMETHYLENE CHLORIDEMETHYL ETHYL KETONE4-METHYL-2-PENTANONESTYRENE1,1,2, 2-TnRACHtOROETHANE]TETRACHLOROETHENE

TOLUENE1,2-OICHLOROETHENE; (TOTAL)TRANS-i,3-OICHLOROPROPENE1.1.1-TR I CHLOROETHANE

3DLBDLHOLBOL !BOL IBDL :BOLBOL ' ;'::':;: .::BOL

BOL .- ...

.BOL.........._...._;._.._ ...„_........_.

'BOL •- "•™"'--"-- ••*•--..BOL _ .v_.. ._ ____.. . ............ ......... .... -•••••--••-

BOLBOL " ; '••:BOL

.wLr.'i\^r^7r2i™^'BOL'"""BOL

"BOL- - "•'^•••: ' . •":•" •"•BOLBDL

3«t. .:mit20 :50 !70

3

510•5"5

10

JO

"" """'5'

rmiir5"........ T".5 ."™""lo

. - • - - , ..5-10

"' r™. s,.,....... ...... 5,...,- 5

. ' ' • • • : :55'5

•Jni:*

ua/Lug/L

ug/Lua/Lua/Lua/L ;ug/Lug/L

ug/Lug/Li:

,U9/V

jI/VWL'ug/Lug/L.ug/L

'ug/Lug/Lug/L

,ug/Lug/Lug/Lug/Lua/L

—————————————————————————————————————————— - Haae :

.'.43 HERITAGE LA EC?

1,1,2-TRICHLOROETHANETRICHLOROETHENEVINYL ACETATEVIHYL CHLORIDE. -;;;;; :,-.,.XYLENE. (TOTAL)

SURROGATE RECOVERY

OICHLOROETHANE-D4TOLUENE-083ROMOFLUOR08ENZENE

3CLEOLSOLSOL :, .••:.."BOL

1 ..-..vx-:. .: ' . ........ .- : •. . ;.:.Ill

• 92• 102

10.- -.-.. 10

5

uc/Lug/Lua/L iug/L i

i% Rec

! " Rsc

GC/MS SEPARATORY FUNNEL.LIQUID-LIQUID (ACID EXTRACTION) SW846-35IOAnalyst:. 0. BACKUS Analysis Oatt: 11-JAM-92 Tasti P23I.5. 0

'• INITIAL WEIGHT OR?• NAL • VOLUME --.T^

ParameterVOLUME

Result830

Oet. Limit Unitsml

•.V.YV-....V;. •;.;.— ;• •.•••-.• j .

SEMI-VOLATILE ORGANICS (ACID FRACTION) SW846-8270Analyst: H. QIAM Analysis Oatt: 15-JAM->2 InstruMnt: CC/HS SVOA Test: C518.3. C?rap: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW846-3510

I-METHYLPHENOL4-METHYLPHENOLPHENOL

SURROGATE RECOVERY

ParaMterBOL

: 3DL1 BCL

2-FLUOROPHENOLPHENOL-OS'" ' -JMM£2.4.6-TRIBROMOPHENOL

! c4

91

! Oat. Limit | Jni;s12 , ug/L12 ! ug/L

; 12 j ug/L

% Reci % Rec! * Rec

SFAAM. UWALCl •••

S),rAW^ «.0«f«-Al^T«:^.^.»r^;^

INITIAL WEIGHT OR VOLUME"*"CTftlAI ûnt^lMf•^:•fî^SsS!isiSs!iK^^fnA'y.•\'^x'•'••'::^x^';:xKr 1NAL «"••""•* •••—.-.»•_.._._•«•....••... . . . . . . . . .

50Rttult Oct. Limit

.Y.V.V.-V.Y.V.V.YT.*

unit?fflL

FAA OR ICrAMDltteESHON ISSOLYED METALSÂ^': 1. HtMJIL ttwlyiU Oat*: 13*J*M-« Twtt M32.4.-0

i1 INITIAL HEIGHT OR1 FINAL VOLUME

•arwtarVOLUME

Xasult50.50"- -• ' • ' : ' . " • • • • '.•••- "-"'M'-Af^'y-:'

Oat. Liait

..... •«.f«< j. " • •••.•*.• * " * " .".*•"

UnitsmLIRL

I LEAD GFAA SW846-7421! Analytt: Hw MUBt:::::.- : ;:': ;v:"-::" Analysis Oata: 15-JAM-91 ..._.._.._._. __.. ... ,..„..,......,,-,.-1 Prep: GFAA ACID-DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SH846-a02fr

i LEADParaawtar iMUlt Oct. Llarft Units

0.0050 ma/L

Paae 2

ARSENIC GFAA SW846-7060Aralyst: R. KCBZA, JR. * Analysis Date: :4-jAN-52 lnstrun«ncr GFAA Tast: M103.2. 0

Prep: GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS. SAMPLES SW846-3020 .. ;

Paramtar Rasult 0ARSENIC BDL

it. Limit units0.0050 mo/L

BARIUM FAA SW846 -7080 ,Analyst: A» STCOCSURG2* Analysis Oatat 13-JAN-91 Irwtrumant:. FAA ' , Tastt.MKK.t^O

Prep: FAA OR 1C? ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846-3005?aram«ter ; 3«sui: ! Q«t. Linit Units

3ARIUM : 30L 0.20 mc/L

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SM84&-3510Analyst: A.. LeHCMCeiLO . Analysis Data: 10-JAM-92 . . last:. ?233.U. 0

I Parimatar Rasult 0INITIAL WEIGHT OR VOLUME i 810=:NAL VOLUME : ' 10

at. Limit { Unitsmi

' *L

i 'OLYCHLORINATED BIPHENYLS (PCBS) SW846-8080^^nalyst: A. LSHONCSLLO Analvsis Satt: :&-jAM-?2 !nstrunant: GC/SO

Prep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-351.0' Paraiaatar i Kasult ; :

?C3 AROCKLOR 1015 ! BDL?C3 AROCHLOR. 1221 i -BDL: : ...,..:. iPCS AROCHLOR 1232 BDL tPCS AROCHLW;;1242:;:. -::,.•. ,.: --.. .. ,-.,,.,,;;, :JDL;,,.,,i:-.:,,:;i::-:: ^x.:-,, C .PCB AROCHLOR 1248 30L

1 DPQ ADnrMI nP"19iJ;4 v •: '" ••:••-. • • • • . • -.y.-.v. ••..•.-.-. .-.v-.^.y. - v - v - • . . . • . . . . . ..v.-;y;yv|v,,ipi|;H-:.:.-.:.vy»::: .;; - yy-^.y.;..-...- v.v.vf

: PCS AROCHLOR 1260 BDL• rV,O AKUvMUUK.'- IZOt • • • • • • • • • - • - • . . - - . ••—:?•:—— •— .:.-.::~:.^:.:;-:.\xlj\J[z'"''""~"""""--:""-'--"-:-''--' •'•'•' •'•'• \

•est: C301.2. C

)at. Limit units0.0006 nw/L

Q'ijQ03 ma/L0.0006 ma/L

:.^.Oi0006^^mg/L0.0006 mg/L

•: 0.0006-: ynw/L0.0006 ma/L

.:-. 0, 0006- -i ma/L

SULFIOE SH846-9030 .,: v ,: •Analyst: T. DOHA Analysis Data: 10-JAN-92 . • y : : . : : :'

I Paraawttr Rasalt"ULFIDE BOL •' •'

I«»t:. GVI0.4. 0

Oct. LiBil Units1 ma/L

•^^

Saapia ConaantsBDL Below Dttectioa^Limit .

Sinols chsin of custody nunbtr 1687

Quality Assurance Officer: Last Pace

Strvict Location

-IMS HERITAGE LABORAfORIES, INC,1319 MARQUETTE DRIVERCMEOVILLE, IL 60441(708)378-1600

09 -JAN- 92CCflSJUtt

17-JAN-92Prtnitd

18-JAN-92

?0

08-JAN-92 14;aa

Seeort To

DAMES 1 MOORETOM C O V I L L I11356310 LAMAROVERLAND PARK, KS 66202

am TO

DAMES 1 MOOREJOHN GROSSHANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 63146

DESCRIPTION: COUNTY WELL LP-1SAMPLE I.O.: CAM-MW-LP1

Sarnie aweription

VOLATILE ORGAN I CS SW846-3240An«iy«t: '.. OIAZ Analysis Oac*: '3-JAM-92

?ara*wcirACETONEACROLEIM :ACRYLONITRILE3ENZENE3ROMOOICHLOROMETHANE3ROMOFORM: -I.....................;,....... ...;.--...-""-..:..-^ - ^:BROHOMETHAHE. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

CARBON TETRACHLORIDECHLOROBEHZEHE'v'v:-.vXX:-.-XvX .-:""••••::•"::' . •• • •••••••->. •• :.>>:>V -''-"i>"v-. '>-''-''X''\:'K-X'"Cv:-xCHLOROETHANECHLOROFORM - ??

CHLOROMETHANEOIBROMOCHLOROMETHANECIS-1, 3-OICHLOROPROPENEOICHLOROOIFLUOROMETHlflE1,1-OICHLOROETHANE

\\ l-OICHLOTOETHJaiE " ZZII I . 7ETHYLBENZENE ».————.•.•.,-,...,•-•.,

2-HEXANONEMETriYLENE CHLORIDE

' METHYL ETHYL KETONE4-'4ETHYL-2-PENTANONESTYRENE1 , 1 , 2, 2-TETRACHLOROETHANE:TETRACHLOROETHENEV tTRAHYOROFURAH'-v-v.v •'•••••• ..':..-x-.'.'-»:'.' • .... •.TOLUENE

i 1 , 2-OICHLOROETHENE; (TOTAL) -TRANS-1 ,3-DICHLOROPROPENE1,1.1-TR I CHLOROETHANE

Instnjncnt: GC/MS VOA

StS»l-BDLBOLBOL :

•pr»i ..••;•

BDLgQ ... .......... 1

BOL j

BOL^Q(Si-si?fe->XvX</TX-y :->>:.--x->x-'->/:-x-:-x-"::v

BOL - .-BDfc > -•••••,;•:•:•: - ;:::-: :;;:-;;;BOLBOL " .;. ..•••• ::5%<ip-vvBOLBOL ..:•'".:.:: •"• '^••''•/:' •:BOL

IBOI/ZZIIT ' zrziBOL

BOL

. B°L ... 1 .77L1IL....Z''BOL ' ' ' -"v" "w"•Dm -"-'•- ' •.•.••••: .. .:.:.:;::• ::::\..':' '"DUL •"••• ••- .-.-.. ..-.v.v.... ..-...•-.-..•.•. •.•.-....•..•.-.•.•. ••

BOL• -•BOL'".''."' v>.-.v>X-.''\'v''>:.vXvXvIvX'.vX •'.-•.".'.

BOL:.BOL.VT -"ix-^ v • : : • ' • • 'BOLBOL

T««t: C51Q.3.

2050.70

c;

?

10'•. • . :•". •"•• ' 5::

r^ •:•,;:•;•. i .10

10• - • . . . . ..."•• R ;

....'.... ...5;5

17 ''^''s5

10

...1..1..I ...10.^::™~- 5•:C ..-./.. •" •..•.v.v.-.S'

•5;V.v.;."V, '.v.-.v .-,.25.

555

'5

^-^

• rt"ug/Lua/Lug/Lua/Lug/Lua/L 'ug/Lua/L !

ug/Lug/L ^ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

:ua/Lug/iiig/L :...ug/L;ug/Lug/LHjg/Lug/Lua/Lua/L

1 ua/LPace

!JS HERITAGE L.-sCRA.T3?

1,1,2-TRICHLOROETHTRICHLOROETHENEVINYL ACETATEVINYL CHLORIDE.XYLENE (TOTAL)

SURROGATE RECOVERY

DICHLOROETHANE-D4TOLUENE-08 ' • .'SP.OMOFLUOROBENZENE

GC/MS SEPARATORYAnalyst: 0. 3ACXUS

INITIAL WEIGHT ORr!NAL VOLUME

&NE ; EOL! BCL

EDL... ,-BOL-. :,-,.,:,,-., ;x':-:.v;Jv.:::.,.:: -..i .:,::,:•:.:,•::/.:

.B.Pk.. ..................................... ..................

, ...,,,... .,..,,.,, ,,,, ...... ... . .,,, ,,.,„ ,=,,,.. .,,,,,.,, ,,,,,,,,,,,.,v,, ,,,:,,,-

. . - irioe-- • -•:•••••••:"• \ ••'• 93 i

FUNNEL LIQUID-LIQUID (ACID EXTRACTION) 5W846-3510Analysis Oats: 13- JAM-92 Test:.

Paranwor | Result Oet. LVOLUME ' 850; i • !

5 Uff/L10 ua/L

MO- ::yg/L. . .His m- . •.,,,,,, .£,

"' Rec' ". Rsc

P233.5. 0imi; , units

iMI -VOLATILE ORGANICS (ACID FRACTION) SW846-3270Analyst: H. OIAH Analysis Oate: 16-JAN-9Z tnstraiant: GC/MS SVGA Test:

Prap: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID (ACID EXTRACTION) SW845-3510

Z-METHYLPHENOL•i-METHYLPHENOLPHENOL

SURROGATE RECOVERS

2-FLUOROPHENOL

Paranacer I Result : Qet. L' 3DL ;

3DLSDL

... i •r

.

2.4, 6-TRIBRbMbPHENOL i 74

0513.2. 3

init . Units12 : ua/L12 i ua/L12 ; ug/L

% Rec

"'"""T's Rec

GFAA ACID DIGEST: - " . . ' • •;• _ " • x-VijSjft

INITIAL WEIGHT ORFINAL VOLUME

W^SJSESSIParameter " R«sjult 0«t.

VOLUME 50m ^.::^. -x;;-: - . :.^m^/^ --::; -

^^•- :Li«it Units

mL

GFAA ACID DIGESTIONAnalyst: K. (UU0M.L

"(DISSOLVED METALS) AQUEOUS SAMPLESAnalysis Date: 1S-JAH-9Z

INITIAL WEIGHT JiyST1* . . . SOS50ll>

SW46;-302a•"/.•T '"-.':-"1. •"•2-""-'..," -,.>^Ta«r PtJJ.0". 1 : ••-RMUlt Oat. Llaiit units

.™L

FAA OR ^Analyst: I.

METALS^AQUEOUS^'

' INITIAL WEIGHT OR VOLUME**1*'i FINAL VOLUME

I ResultI S O

Oat. Ltatt UnitsmL ..

•v.^vX-^-vyX^^ JBtvv .

LEAD GFAA SW846-7421.Analyst: N> MUCH Analysis Data:

Prep: GFAA ACID DIGESTION (DISSOLVED METALS) AQUEOUS

i LEADParaimar

RillXMUlt Oat. Li«it

0.0050Units

ma/L

Pace 2

r i jc i - i rz r** ' *~ ' * 2 ' * n * ^ ' " ' * ' w * ~ " • ^^*

ARSENIC GFAA SW846-7060inalyst: ft. KC8ZA, JR. " Analysis 3at«: r i - jAH-92 I.istr^err: GFAA T,,t.Prep: GFAA ACID. DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES SW846-3020 '

Paraawtar1 4RSENIC

StsultBDL

Ott. Limit0.0050

Unitsma/L '•

BARIUM FAA SH846-7080An»lystr A. STCCXBWCfR:- • v : : : Analysis. Data: .- 13-JAK-9?" Instruasnt:. FAAPreo: FAA OR.1C? ACID DIGESTION (DISSOLVED METALS) AQUEOUS SAMPLES

T«st: M104.1. 0SW846-3005

?»r«m«terSARIUM 3DL

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510inalyst: A. LEMMCELLO Analysis 5»tt: 10-JAM-92

i 3 ST. Li.lHJ

0 .20

T«»t: '223.1. CPiramctr

HITIAL WEIGHT OR VOLUMEINAL VOLUME

! 8201 10

fttsul:

POLYCHLORINATED BIPHENYLS (PCBS) 5W846-S08Ciralyst: A. LS.VOMCSLLO Analysis :«tt: :i-JAN-?2 :.-.s;r-j»ar!t: 5C/IC3?rsp: GC SEPARATORY FUNNEL LIOUIO-LIC'JID EXTRACT I C?l SW846-25IO

3«t. Linit 'Jni:»

raL

Test:

3C3 AROCHLCR 10IS?C3 AROCHLOR 1221PC3 AROCHLOR 1232PCS AROCHLOR 1242PCS AROCHLOR 1243PCS AROCHLOR:1254^=C3 AROCHLOR 1260?C8 AROCHLOR-

3DL:.BDLSOL

:!>BDL; BDL

! BDL•/ f n

SULFIDE SW846-9030Analyst: T. MOM Analysis Oatt: 10-JAN-92

BDL Below DttectionJ.imit


its

3tt. .isiit ' .n::s0.0005 .7C/L

O.C03 ! sw/LC.0006 i sng/L

:..O.OOOff.i..nig/L0.0005 ma/L

' 0.0006 rng/L0.0006 ! ^a/L0.0006 I rna/L

T«st: C110.4. Q

i Paraa»tar! SULFIDE BOL

ftasult Oat. Limit1

Unitsmo/L - '

v j

Quality Assuranca Officer: ' l_

S«rvict locationEMS HERITAGE LABORATORIES, INC.1319 MARQUETTE DRIVE3QMEOVILLE, IL 60441(708)378-1600

Rectivea09-JAN-92

Ccnoiatt13-JAN-92

Printaa14-JAN-92

.« ::C135520?0 Nunocr

Samite ii

Rtport To

OAMES i MOORETOM COVILLI?1355310 LAMAROVERLAND PARK, KS 66202

S i l l To

OAMES 4 MOOREJOHN GROSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 62146

DESCRIPTION: TRIP BLANKSAMPLE I.O.: CAM-TRIPFIELD BLANK FOR C135523-CL2S=2i

alt Otscriotion

VOLATILE ORGANICS SW846-8240Analyst: S. SHARP Analysis Oats: 10-jAM-?c

ParsswtarACETONE iACROLEINACRYLONITRILEBENZENE3ROMOOICHLOROMETHANEBROMOFORMBROMOMETHANE

CARBON TETRACHLORIDE• ^ u y'jnbnri itf fci y f fci ""^"^-•^'••"'-'--"'-"'^-•'-''••" '*.'^-'''f'*'.'^*.*''f.'"*-'.*''.''.'*'.*^'*'""ls^ffffj^f.\t^^sfsxKix?x

LORQET>IAJM|J

CHLOROMETHANEri TQ|lfki^^|TtJf <\JTi/UJ]f**inyfli|M| ' ** ;'"-;'~A~.rj«ArvAVAV'rA«1v/: ^

CIS-1 ,3-DICHLOROPROPEHEOICHLORODIFUW»g|!&HANE^> - - - /v / : , -x ,1,1-DICHLOROETHANE1,2-OICHLOROETHANE*1 , 1 -OICHLOROETHEN|_. . . . . . .

ETHYLBEN2ENE '""""'" ~--'air"~""-"— ••"•••"•"

2-HEXANONE

METHYL ETHYL JJ|TO^^-'^^^";S^^^^"-A--- ~4 -METHYL- Z-PENTANONE-:^: . . ,-STYRENE1 , 1 , 2 , 2-TETRACHLOROETHANE.TETRACHLOROETHENETETRAHYOROFURANTOLUENE1,2-OICHLOROETHENE:(TQTAL)

. TRANS-1.3-DICHLOROPROPENE ________________

instrjatnt: 3S/MS VGA

ResultBDLBOLBOLBOL •BDL :BOL: ..: . .,:.'•• i30kv... , ,.,,.,:.... I

BDLSf\ tSrlSKXff. ".V.VtJJ.'. V.V.'.ViV,* .V.V.V.V.V.'.V.V.V.*.'

BOL^ ___ .__ ,,.,..,.,,.,,..,,

BOLAMfeag.rj.'.vjsa'.vr.vj *.* v.v.*v. AV.T." •.•.*.••••*••.•••

BOL

^BOL."'.'."V'.r. .... ' ''"' 7

BOL

jroCTrri."'"'rBOL

BOL

BOL•;BOL:,v-;- -;•;., . . '

BOL•BOL--':;;--.: -".-•:••.. • • •BOL

BOL

-«st: CS'0.2. ::•:. . -..nit

20 :5070 :

• c10

C. 1

5

."Z".""""Iio..'::::::::K

5

5 .

...5

105

1010

5.. •• .5

525

55

.ni:sua/Lug/Lua/Lug/Lua/Lug/L !ua/L >ua/L iug/L jBg/tv--. !ug/Lua/L.>*3/.>-

ua/Lui/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lua/Lug/L.ug/Lug/Lug/Lua/L

' ua/L?aae .

?aram«ter-,1,1-TRICHLOROETHANE

7RICHLOROETHENEVINYL ACETATE:::VINYL CHLORIDEXYLENE (TOTAL)

SURROGATE:. RECOVERY

=CLl:eoL30LBOLBOL

I BOL

DICHLOROETHANE-04TCLUENE-083RQMOFLUORQBENZENE ••i 103

..-.! :s

310105

: : 'jg/L' ug/L

ug/Lug/.Lug/Lug/L

1 ;i Rec• % Rsc: % Rec

3DL Selow Detection Limit

Ssnols chain of custody number 1537

Swot* C

Quality Assurance Officer: Last Page 2

C £ R U.Y s : s 33Strviet Location

' EMS HERITAGE LABORATORIES, INC.i 1319 MARQUETTE DRIVE! ROMEOVILLE, IL 60441j (708)378-1600

Rteiivcd

09-JAN-92Conolatt

13-OAN-92

14-JAN-92

w*o ::C135531PO IKMMr

—Report To

DAMES 4 MOORETOM COVILLI

6310 LAMAROVERLAND PARK, KS 65202

Sill To

OAME3 & MOOREJOHN GROSSMANSUITE 34011701 BORMAN DRIVEST. LOUIS, MO 63146

DESCRIPTION: TRIP BLANKSAMPLE I.D.: CAM-TRIPTRIP BLANK FOR C13S523-C135529

Samolt 3«scription

VOLATILE- ORGANICS SW846-8240vAnalyst: 1. SUMP ' Analysis Oatt: 'Q- JAN-92

Paranattr 'ACETONE :ACROLEIN jACRYLONITRILE3ENZENE iBROMOOICHLGROMETHANE i

BROMOMETHANE

CARBON TETRACHLORIDE

HLOROETHANE"(""HI HRDPnOH • xxx-XvXvX-x-r./- : . .%:--v./.:x:v.-: • -.: ' . :" • " • . ::::.-.. •:::..•..•. •-.•:•>•uriLUKurunn •... ••...•.-••...........••...... . . - . • • • • •• .. • .. ••• . • • • ..-.•.-CHLOROMETHANE

CIS-1,3-PICHLPRPPROPWIE _.,„.....

1 • l-DICHLOROETHENE^^^1 f aw ~ iJ .1 HlfcUKU mZ. fctij CTCTM fesS J ' '''''''''''''''*'*'''''-*'*' '" ••'• • • • • • • • • - • • ' • ••• •-••• •- ' ' •-••.••"•.••".:.•

ETHYLBENZENEFLUOROTRICHLORWiETl''(ANJf' ' "''""'-- • • *~ : :

2-HEXANONEMETHYLENE: CHLORIDE-METHYL ETHYL KETONE4-METHYL-2-PENTANONESTYRENE1 , 1 ,.2 , 2-TETRACHLOROETHANETETRACHLOROETHENETETRAHYOROFURAN: :TOLUENE1 , 2 -0 1 CHLOROETHENE:x (TOTAL )TRANS-1.3-OICHLOROPROPENE

!ratr-jB«-!t: GC/MS VGA

SOLBOL iBDLBDL.BOLBDI-- iBOLbni :BDL

BDL

BDL

BOk....... ..;;;.. ..:.,__,. ,.,.,.,.,...^ , _,,,,.

iBOPS^ M^xVxWMP^,80 . . ..,.,. ,...,....,,...,,v.0U t".v. v.v • • • . . . • . . . .'.' •*••.• .• • •• • . • • • • •

BOL"BOL:...BOL

BOLBOLBOLBOLBOLBOLBOLBDL

! 3DL

T«tt: CS'0.3. (3«t. Limit

205070.

• i

1055

..,, .XX..., -5.

10

10

........ .,5..

IIIIZA.5

... j

55

105

1010

5, .--; • "s

525-

55

• 5

)'Jni ts

UQ/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lig/L :, 9/L ::.

J /1!!ug/L

^g/L .ug/Lug/Lug/Lug/L

,«g/L.ug/Lug/L.ug/Lug/Lug/Lua/Lua/L?aae .

EMS HERITAGE LABORAIOKlLi, iNL.Paramtcr

1,1,1 -TRICHLOROETHANE

TRICHL^R.P.ETHENJ =_^

VINYL CHLORIDE

SURROGATE:::RECliVERY^^::^^^ : ••" '"'"':': ::':-"::::::.;

i nortcru'ftMC "nii """"" ...

TOLUENE-083ROMOFLUOR08ENZENE-vv-v""'" •->..:••••.•.•.•.•.•.•/.•.•.•.•.•.•.:..•.;.•.•.•• • .... ...- .•..•...•..•..•...•.;.;;

SMplt Com3DL Below Detection Limit


-

SQL

BOL" D n i • — '•'• •'•'•'• ••••••••'•••..-.•.... ••••-. -••••• ••....•.•.••.---.•.•. . . .•:•:

BDL'•'Oni - •"••'•v-X:-X--- ••••.•.;.;/.;/.; •.-..:;.:.-v:.v.-...v..^v.•/: B U L •: :-""v>: ::•:•:•:;: ::•:•:•>:•/. :•:•:•• -••• : :•:;: : : : : • ;..v:; ; . , -

^•^^^^'•/^•/•^•^:''': :'-:':'v '•'. ••• '•'•': : : : ';

•::rrn:- -..-• •: ••!• 1 iW

H5— •- •—••••.9 *••••"•••• ••• •••••••••-•.• ••.-.— .-•••.. .

•nts

=0 5a^3 9 .

3tc. .'..•ait

•:.'•:.:':'..: : ............5..

.5

10

- : - -;:;^ .

'-'9/L *

ug/L !ug/L iug/Lug/L

i r/Rec% Rsc% R9C

Quality Assurancg Officer:CQ v^. Las

NET NATIONALENVIRONMENTALTESTING, INC.

NEinoianaoons Division6964 Hiiisdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCEsolo Stone Mill RoadBloomington, IN 47408

ANALYTICAL REPORT01/28/1992

rr Chloride

CODConductivityFluorideNitrogen, AmmoniaNitrogen, NitratePhenolSolids, DissolvedSulfateArsenic, 6FAABarium, ICP WWBoron, ICP WWCadmium, ICP WWChromium, ICP WWCopper, ICP WWIron, ICP WWLead, GFAAManganese, ICP WWMercurySelenium, GFAASilver, ICP WWSodium, ICP WWZinc, ICP WW

Sample No.: 47802NET Job No.: 92.0061P.O. NO.: VerbalPage l

Sample Description: LP2 CAMORJob Description: CAM-OR LAPORTE, IN

Date Taken: 01/06/1992

Parameters

Date Received:

Results

29.

01/09/1992

Units

573.0.14<0.17.9<0.005360.51.<0.00500.020.50<0.0050<0.010<0.0100.08<0.00500.03<0.0005<0.0050<0.01030.<0.020

«g/L•g/Luahos/cmmg/Lmg/L•g/L•g/L•g/L«g/L»g/L•g/L•g/L•g/L•g/Lng/Lng/L•g/L•g/L•g/L•g/L•g/L•g/L

rohnsonProject Manager

NET NATIONALENVIRONMENTAL

,. TESTING, INC.

NET Midwest inc.Indianapolis Division6964 Hiilsaaie CourtIndianapolis. IN 46250T0I: (317) 842-4261Fax:(317)842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCE5010 Stone Hill RoadBloomington, IN 47408


Sample No.: 47802NET Job No.: 92.0061P.O. NO.: VerbalPage 2


Date Taken: 01/06/1992 Date Received: - X) 1/09/1992

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBronod ichloromethaneBromofornBromomethane2-Butanone (MEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloromethaneDibromomethaneDibronochloronethaneDichlorodifluoromethane1,2-Dibromoethane (EDB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoromethane1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenetrans-1,2-Dichloroethenecis-1,2-Dichloroethene1.2-Dichloropropane

Results

<20.<50.<50.

<5.0

<5.0

onits

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

Proj

IIIIiIIvIIIi


NET6964 Hiiisaaie CourIndianapolis. IN 46250Tel: (31 7) 842-4261Fax: (317) 842-4286

Mr. Richard FlorasWW. ENGINEERING & SCIENCE5010 Stone Mill RoadBloonington, IN 47408

Sample Description: LP2 CAMORJob Description: CAM-OR LAPORTE,


Parameters

VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcetateEthylbenzeneEthyl nethacrylate2-HexanonelodonethaneMethylene chlorideParaldehyde4-Methyl-2-pentanone (MIBK)Styrene1,1,2,2-TetrachlbroethaneTetrachloroetheneTetrahydrofuranToluene1,2,3-Trichloropropane1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideXylenesSURROGATE COMPOUNDS1,2-Dichloroethane-d4Toluene-d84-Bromofluorobenzene



IN

Date Received: 01/09/1992

Results

% RECOVERY100.102.97.

Unite

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/LLIMITS76-11488-11086-115

Projson

Manager

I

I

I

I

I

I


NET Midwest, inc.Indianapolis Division6964 Hillsdale CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FlorasWW ENGINEERING fr SCIENCE5010 Stone Mill RoadBloomington, IN 47408




Date Taken: 01/06/1992 Date Received: 01/09/1992

Parameters

PCB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCS-1260Dibutylchlorendate

Results

99.

Units

ug/Lug/Lug/Lug/Lug/Lug/Lug/L

Project Manager


I. TESTING, INC.

\ET Miawest. 'ncindianapons Division6964 Hiilsaaic CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FlorasWW ENGINEERING & SCIENCE5010 Stone Mill RoadBlooaington, IN 47408





Parameters

ChlorideCODConductivityFluorideNitrogen, AmmoniaNitrogen, NitratePhenolSolids, DissolvedSulfateArsenic, 6FAABarium, ICP WWBoron, ICP WWCadmium, ICP WWChromium, ICP WWCopper, ICP WWIron, ICP WWLead, GFAAManganese, ICP WWMercurySelenium, GFAASilver, ICP WWSodium, ICP WWZinc, ICP WW

8.5

614.0.06<0.10.96<0.005370.110.<0.00500.070.61<0.0050<0.010<0.010<0.020<0.00500.08<0.0005<0.0050<0.0107.7<0.020

mg/Lmg/Lumhos/cm«g/L•g/Lmg/L•g/L•g/Lmg/L•g/L•g/Lmg/Lmg/Lmg/L•g/Lmg/Lmg/L•g/Lmg/Lmg/Lmg/Lmg/Lmg/L

Projon

Manager


NET Midwest. ;ncIndianapolis Division6964 Hillsdale CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

Mr. Richard FlorasWW ENGINEERING & SCIENCE5010 Stone Mill RoadBloomington, IN 47408





Parameters

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBromodichloromethaneBromoformBromomethane2-Butanone (MEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloromethaneDibromomethaneDibromochloromethaneDichlorodifluoromethane1,2-Dibromoethane (EDB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoromethane1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenetrans-l,2-Dichloroethenecis-l,2-Dichloroethene1.2-Dichloropropane

Results

<20.<50.<50.

<5.0

Units

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

<5.0

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

Proj Manager


NET Midwest. :rcindianaoons6964 Hiiiscaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCE5010 Stone Mill RoadBloomington, IN 47408





Parameters

VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcetateEthylbenzeneEthyl methacrylate2-HexanonelodomethaneMethylene chlorideParaldehyde4-Methyl-2-pentanone (MIBK)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene1,2,3-Trichloropropane1.1.1-Trirchloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideXylenesSURROGATE COMPOUNDS1,2-Dichloroethane-d4Toluene-d84-Bromofluorobenzene

Results

% RECOVERY100.102.98.

Units


Projon

Manager1 -f-


NET VliOwest. inc.inCianaooiis Oivisic^6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

ANALYTICAL REPORT01/28/1992Mr. Richard Floras

WW, ENGINEERING & SCIENCE5010 Stone Mill &oadBloomington, IN 47408





Parameters

PCB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Dibutylchlorendate

Results

94.


Proj

IIfIIItIIIIIII


NET Miawest. ireinaianapoiis Division6964 Hillsdale CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

•Vj



Parameters

ChlorideCOOConductivityFluorideNitrogen, AmmoniaNitrogen, NitratePhenolSolids, DissolvedSulfateArsenic, GFAABarium, ICP WWBoron, ICP WWCadmium, ICP WWChromium, ICP WWCopper, ICP WWIron, ICP WWLead, GFAAManganese, ICP WWMercurySelenium, GFAASilver, ICP WWSodium, ICP WWZinc, ICP WW




Results

16.

702.0.13<0.118.<0.005480.40.<0.00500.050.52<0.0050<0.010<0.010<0.020<0.0050<0.010<0.0005<0.0050<0.0107.8<0.020

Onita

mg/L•g/tumhos/cmmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Projson

Manager


NETMicwest. -cinflianaooiis Divis.on6964 Hiiisdale CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

Mr. Richard FlorasWW ENGINEERING & SCIENCE5010 Stone Mill* RoadBloomington, IN 47408





Parameters

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBroaodichloronethaneBronofomBroaonethane2-Butanone (MEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloromethaneDibromomethaneDibronochloromethaneOichlorodifluoronethane1,2-Dibronoethane (EDB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoromethane1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenetrans-1,2-Dichloroethenecis-1,2-Dichloroethene1.2-Dichloropropane

Results

<20.<50.<50.

<5.0

<5.0

Pnita


Projon

Manager

I

I

I

1


\9 TESTING, INC.

Mr. Richard FloresWW ENGINEERING £ SCIENCE5010 Stona Mill RoadBloonington, IN 47408


NET vindianaoons Division6964 Hiilsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

Sample No.: 47804NET Job No.: 92.0061P.O. NO.: VarbalPage 11


Data Takan: 01/08/1992 Data Racaivad: 01/09/1992

I

I

I

I

I

I

I

I

Parameters

VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcatataEthylbenzeneEthyl methacrylate2-HexanonalodomathanaMathylana chloridaParaldahyda4-Mathyl-2-pentanone (MIBK)Styrena1,1,2,2-TatrachloroathanaTetrachloroetheneTetrahydrofuranToluena1,2,3-Trichloropropane1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroathanaTrichlorofluoromethaneVinyl acatatavinyl chloridaXylanasSURROGATE COMPOUNDS1,2-Dichloroathana-d4Toluene-d84-Bromofluorobenzene

Results

6.4

% RECOVERY102.102.98.

Pnita

uq/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

-ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/LLIMITS76-11488-11086-115

I

I

1

IIi


I. TESTING, INC.

NET M.cwes:. ;rcindianaooiis Divis.cn6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FloresWW ENGINEERING 4 SCIENCE5010 Stone Mill RoadBloomington, IN 47408


Ift*-••.'

i



w Date Taken: 01/08/1992 Date Received: 01/09/1992

Parameters

PCB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Dibutylchlorendate

Results

91.

Onita


I1

nion

Project Manager


inaianapoiis Division6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

CHA.HM OF CUSTODY

Client

Send Report to

ProjectNamc

* jAddressTelephone

Collected by:

Collection Infonattai

S-PU10

S-pUnoLoot ton

OiM TIM

T»P»or

Cowtafrar

ISA

iPJ /-5 ~ r

Remarks: ^>4/njL -/Sv ^»^aRelinquished by: Date Time Received by:

^ . 4Date Time

if fyi

Shipping Notes/1

Samples Field Filtered:Seals Intact Upon Receipt.

Received for NET Midwest by

YesYes NO N/A

IIIIIIII


|e TESTING, INC.

NETInaianapons6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCE5010 Stone Mill RoadBloomington -IN 47408


Parameters

ChlorideCODConductivityFluorideNitrogen, AmmoniaNitrogen, NitratePhenolSolids, DissolvedSulfateArsenic, GFAABariua, ZCP wwBoron, ICP wwCadmium, GFAAChromium, ICP WWCopper, ICP WWiron, ICP wwLead, GFAAManganese, ICP-WWMercuryselenium, GFAASilver, ICP WWSodium, ICP WWZinc, ICP WW


Sample Description: B2 CAM ORJob Description: CAM-OR LAPORTE, IN


Results

67.140.966.0.220.52<0.100.009620.79.<0.00500.042.4<0.0010<0.0100.01<0.020<0.0050-276- ——<0.0050<0.0050<0.01049.<0.020

Units

mg/Lmg/Lumhos/cnmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Corrected Report

dfc** J*!"<~0n~Steve JohnsonProject Manager

I

I

I

I

I

I

LII


NET Micwes: reInoianaooiis Division6964 Hillsdaie CourtIndianapolis, IN 46250Tel: (317) 842-4261Fax:(317)842-4286


Sample Description: B2 CAM ORJob Description: CAM-OR LAPORTE


Parameters

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBromodichloroaethaneBroBoforB


Sample No.: 47730NET Job No.: 92.0037P.O. NO.: Verbal

Page 2

IN

2-Butanone (MEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloromethaneDibromomethaneDibromochloromethaneDichlorodifluoromethane1,2-Dibromoethane (EDB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoromethane1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenetrans-1,2-Dichloroethenecis-1,2-Dichloroethene1.2-Dichloropropane


Results

<200.<500.<500.

<50.<100.

<100.<50.

<100.<100.

<100.

<100.94.

11.640.

S^^GA/***' J4*fa»**}n*Steve JohnsonProject Manager

Units

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/LJig/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L


NE~inoianaoons6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286



Parameters

VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcetateEthylbenzeneEthyl nethacrylate2-HexanoneZodonethaneMethylene chlorideParaldehyde4-Methyl-2-pentanone (MIBK)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene1,2,3-Trichloropropane1.1.1-Trichloroethane1.1.2-Trichloroethane~TrichloroetheneTrichlorofluoroaethaneVinyl acetatevinyl chlorideXylenesSURROGATE COMPOUNDS1,2-Dichloroethane-d4Toluene-da4-Bronofluorobenzene




Results

<100.

<100.<100.<100.<100.<100.<100.

15.280.

<100.19.

40.

<100.<50.

% RECOVERY103.102.100.

U(»~>^Steve JohnsonProject Manager

Units


iIIIII




NET Vlicwest. PC.Indianaoous Division.6964 Hillsdaie CourtIndianapolis. 1N 46250Tel: (317) 842-4261Fax: (317) 842-4286


Saaple Description: B2 CAM ORJob Description: CAM-OR LAPORTE, IN


II1I

Pa.ra.p»eters

FOB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Dibutylchlorendate

Results

78.

Units


IIIi

>< fc !*«!»<•*>»-.Steve JohnsonProject Manager

IIIIIIIii

52


U TESTING, INC.

NET Vlicwest. inc.Indianapolis Division6964 Hillsaaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286




Page 5

Sample Description: Bl CAM ORJob Description: CAM-OR LAPORTE, IN


Ii*ii


Parameters Results

Chloride 140.COD 12.Conductivity 1170.Fluoride 0.09Nitrogen, Ammonia 0.15Nitrogen, Nitrate <0.10Phenol <0.005Solids, Dissolved 660.Sulfate 50.Arsenic, GFAA <0.0050Barium, ICP WW 0.04Boron, ICP ww 0.36Cadmium, GFAA <0.0010Chromium, ICP ww <0.010copper, ICP ww 0.02Iron, ICP ww 0.26Lead-, -GFAA - - <0.0050Manganese, ICP WW 0.49Mercury <0.0005Selenium, GFAA <0.0050Silver, ICP WW <0.010Sodium, ICP WW 68.Zinc, ICP ww <o.020

Units

mg/Lmg/Lumhos/cmmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L»g/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

X^feifc. J+****0n~Steve '-JohnsonProject Manager


NET Viiawest. TC.Inoianaooiis Division6964 Hiiisdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

I

I


Sample Description: Bl CAM ORJob Description: CAM-OR LAPORTE,


Parameters

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBroBodichloroBethaneBroBOformBroBoaethane2-Butanone (NEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloroaethaneDibroBomethaneOibroBochloroBethaneDichlorodifluoroBethane1,2-DibroBoethane (BOB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoroBethane1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenetrans-1,2-Dichloroetheneci»-l,2-Dichloroethene1.2-Dichloropropane


Saaple No.: 47731NET Job No.: 92.0037P.O. NO.: Verbal

Page 6

IN


Results

<20.<50.<50.

<5.0

<5.0


Steve ^JohnsonProject Manager


NETindianacos OivsiC"6964 Hiilsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCE5010 Stone Hill RoadBloomington, IN 47408

Sample Description: Bl CAM ORJob Description: CAM-OR LAPORTE,Date Taken: 01/06/1992



Page 7

IN


Results

VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcetateEthylbenzeneEthyl methaerylate2-HexanonelodoaethaneMethylene chlorideParaldehyde4-Methyl-2-pentanone (MIBK)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene1,2,3 -Trichloropropane1.1.1-Trichloroethane1.1.2-TrichlbroetnaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideXylenesSURROGATE COMPOUNDS1,2-Dichloroethane-d4Toluene-d84-Bromofluorobenzene

1.2

% RECOVERY96.99.108.

Units


X/fet, J**k+0n+Steve JohnsonProject Manager

0IIa


NET ViGwest. ire.indianaoons Oivisicr6964 Hillsaaie CourtIndianapolis. IN 46250Tel: (317} 842-4261Fax: (317) 842-4286




Page 8

Sample Description: Bl CAM ORJob Description: CAM-OR LAPORTE, IN


Parameters

PCB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCS-1248PCB-1254PCB-1260Dibutylchlorendate

Results

85.

Units


Steve JohnsonProject Manager

MU

jI NET NATIONAL

ENVIRONMENTALTESTING, INC.

NET Micwest '-cInaianaooiis Division6964 Hillsdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax:(317)842-4286

I Mr. Richard FlorasWW ENGINEERING 6 SCIENCE5010 Stone Mill RoadBloomington, IN 47408



Page 9

IIIIIIIIIIIIII



Parameters

ChlorideCODConductivityFluorideNitrogen, AmmoniaNitrogen, NitratePhenolSolids, DissolvedSulfateArsenic, GFAABarium, ICP WWBoron, ICP WWCadmiu GFAAChromium, ICP WWCopper, ICP WWIron, ICP wwLead, GFAAManganese, ICP WWMercurySelenium, GFAASilver, ICP WWSodium, ICP WWZinc, ICP WW


Results

50.150.974.0.2610.<0.250.099560.55.0.0160.052.0<0.0010<0.010<0.01014.<0.00500.970.015<0.0050<0.01049.<0.020

Units

mg/Lmg/Lumhos/cmmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

x£w *~ J*™*Steve '•$ohns<Steve JohnsonProject Manager


NiEr M'CweSt. ireinaiaraooiis Division6964 Hiiisdaie CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286




Page 10Sample Description: B4 CAM ORJob Description: CAM-OR LAPORTE, IN


Parameters

VOLATILE COMPOUNDS - 8260AcetoneAcroleinAcrylonitrileBenzeneBromodichloromethaneBroaofonnBroaoaethane2-Butanone (MEK)Carbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChloromethaneDibroadMthaneDibroBOChlorpaethaneDichlorodifluoroBethane1,2-DibroBoethane (EDB)1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-DichlorobenzeneDichlorodifluoroBethane1.1-Dichloroethane1.2-Dichloroethane"L, 1-Dichloroethenetrans-1,2-Dichloroethenecis-1,2-Dichloroethene1,2-Dichloropropane

Results

<400.<1000.<1000.54.<20.<20.<100.<200.<20.<20.<20.1500.<100.<20.<200.<200.<20.<200.<20.<20.<20.<20.<200.210.<20.<20.<20.<20.<20.

X^fcc- J*hSteve JohnsonProject Manager

Units


IIii1I1III


NE ire

6964 Hdlsaaie Courtmdtanapons. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

Mr. Richard FloresWW ENGINEERING & SCIENCE5010 Stone Mill RoadBloonington, IN 47408



Page 11Sample Description: B4 CAM ORJob Description: CAM-OR LAPORTE, IN


VOLATILE COMPOUNDS - 8260cis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthyl AcetateEthylbenzeneEthyl methacrylate2-HexanonelodoaethaneMethylene chlorideParaldehyde4-Methyl-2-pentanone (MIBK)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene1,2,3-Trichloropropane1,1 rl-?Tr ichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideXylenesSURROGATE,2-Dichloroethane-d4

Toluene-d84-BroBofluorobenzene


Units

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L-ug/Lug/Lug/Lug/Lug/LLIMITS76-11488-11086-115

<20.<20.<200.<20.<200.<200.<200.<200.<200.<200.<20.<20.<20.330.<20.<200.<20.<20.<20.<20.<200.<100.<20.% RECOVERY104.102.97.

Steve 'JohnsonProject Manager


I. TESTING, INC.

NET MiGwest. ;rcindianapons Qwrsicn6964 Hillsdale CourtIndianapolis. IN 46250Tel: (317) 842-4261Fax: (317) 842-4286

57

Mr. Richard FlorasHW ENGINEERING t SCIENCE5010 Stone Mill RoadBlooBington, IN 47408


Saaple No.: 47732NET Job No.: 92.0037P.O. NO.: VerbalPag* 12



I

I

I

Parameters

PCB'S - 608PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCS-1260Dibutylchlor«uidat*i

Results

76.

Units


iIIIIII

St«w« aohnsonProject Manager

III

NETNATIONALENVIRONMENTALTESTING, INC.

6964 riiiiscaie CourtIndianapolis. IN 46250T«l: (317) 842-4261Fax: (317) 842-4286

CHAIN OF CUSTODY

ClientSend Report to

ProjectName

Address

Telephone

Collected by:

fcs: .«_<»

Date Time /-Relinquished by: ceiyed by: Date Time

IX- r - j\ ——— ————————

ipping Notes Lab Comments Received for NET Midwest by:

Samples Field Filtered:Seals Intact Upon Receipt

I

ww engineering & science, · collected during january 6.7,8.1992 at the cam-or site (wells bl....

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