x-ray diffractometer xrd-6000
DESCRIPTION
riccat_sihotangTRANSCRIPT
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X-ray Diffractometer
XRD-6000
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Application Field of X-ray Diffractometer
Achievement of shimadzu XRD
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NaCl Diamond
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Unit Cell of NaCl
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PDF2 Data of NaCl
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Data list of Carbon in PDF2
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DiamondC60Graphite
Crystal Structures of different Carbons
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Diamond
C60
Graphite
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History of Shimadzu X-ray DifractometerProducts Outline
1945 World first XRD
1996 XRD-6000 Windows95 operated XRD
1962 GX-31958 GX-21955 GX-1
Stand-alone XRD
Shimadzu first XRD}1970 VD-21965 VD-1 }Automated recording XRD with
GRS matching start function
1978 XD-3A,5A1974 XD-3,5 }Fully automated XRD with
small & safety case
1986 XD-610 Computer controlled XRD
1992 XD-D1 Fully computerized XRD
XRD-6000
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Big Features of XRD-6000
1. Compact & Safety Case Design
2.High Precision & Very StableVertical Goniometer
XRD-6000
3.User Friendly Operation(Windows95/98)
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1.Compact & Safety Case Design
・ Size of Main BodyW900×D700×H1600
・ Door is Locked whenthe X-ray Power is ON
・ No Switch for Cancellation of Interlock system
900 700
1600
XRD-6000
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2.High Precision & Very StableVertical Goniometer
・ Angle Reproducibility±0.001 ゜ (2θ)
・ Scanning Angle Range-6 ~+ 163 ゜( 2θ )-180 ~+ 180 ゜( θ )
・ θ-Axis oscillationEquipped as Standard
XRD-6000
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3.User Friendly Operation (Windows95/98 or NT)
・ Multitasking
・ Mouse Operation
・ Easy to Upgrade(H/W,S/W)
・ Ready for Network
・ Easy to Transfer the Datato the General-purposeS/W such as MS-Wordor Excel
XRD-6000
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MeasurementSection
Basic Data Processing
SearchMatch
Quant.Calc Advanced Data Process
Standard Configuration Optional Software
XRD-6000 Main Window
XRD-6000
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XRD-6000 STATUS DISPLAY WINDOW
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X-RAY POWER CONTROL WINDOW
XRD-6000
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GONIOMETER OPTICAL ADJUSTMENT
XRD-6000
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MEASUREMENT CONDITION EDITING
XRD-6000
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MEASUREMENT WINDOW
XRD-6000
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XRD-6000
BASIC DATA PROCESSING
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BASIC DATA PROCESSING
XRD-6000
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BASIC DATA PROCESSING
XRD-6000
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SEARCH/MATCH
XRD-6000
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SEARCH/MATCH
XRD-6000
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Search/Match result of some Minerals
Anorthite
Albite
Augite
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Search/Match result of some Minerals
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QANTITATIVE ANALYSIS
XRD-6000
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CALIBRATION CURVE
XRD-6000
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CALIBRATION CURVE
XRD-6000
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QUANTITATIVE ANALYSIS
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Thin Film Attachment
Specification・ Sample StageRotation 360°Fixation Vacuum SackingSize(max) φ102x10mm・ Adjustment for Sample Surfaceby Micrometer Head・ Rotation Speed 72rpm・ β-axis MeasurementContinuous/step scan・ Monochrometer Graphite
XRD-6000
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Crystalinity Measurement
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Calculation of Crystallite Size and Lattice Strain
β = β s+ βoβs: FWHM for Crystallite Size(D)
βo :FWHM for Lattice Strain(η)
β = β s+ βo =
β s= λ D ・ Cosθ
βo = 2η ・ Sinθλ
Sinθλ
λ D ・ Cosθ
+
β ・ Cosθλ
+ 2η ・ Sinθλ
1D=
Hall’s equation
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Crystallite size & Lattice Strain
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Counter Monochromator for XRD-6000
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Rotational Sample Stage for XRD-6000
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Environmental Measurement Stage for XRD-6000
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Sample Heating Attachment for XRD-6000
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Sample Heating Attachment for XRD-6000Low Temperature Stage TTK-450
Main Specification
Temperature Range -193 through 450degSize of ApparatusOuter Diameter 105mmThickness 60mmWindow for X-ray 12mm/200degMaterial of X-ray Window25 micron KAPTON Thin FilmDetector for TemperaturePlatinum(PT100)Consumption Rate of Liquid Nitrogen1.5 litter/hour(at -193degree)
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TTK-450 Low Temperature Stage
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TTK-450 Low Temperature Stage
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Application Data by TTK-450
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Main Specification
Sample Heating Attachment for XRD-6000High Temperature Stage HTK-1200
Temperature Range RT through 1200degSize of ApparatusOuter Diameter 150mmThickness 60mmWindow for X-ray 10mm/200degMaterial of X-ray Window25 micron KAPTON Thin FilmDetector for TemperatureThermocouple(Pt-PtRh)AtmosphereAir,Inert Gas, Vacuum, Corrosive Gas
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HTK-1200 High Temperature Stage
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HTK-1200 High Temperature Stage
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Pole Figure Attachment for XRD-6000
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Advanced Crystal Structure Analysis
• Precise Lattice Constant Calculation • Crystal System Determination• Rietveld Analysis (with NARiet
process)Refine Crystal ParametersQuantitative Analysis of Multi ComponentCrystal Solid Model Display
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TiO2 Rutile structure
Ti
O
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Fulleren C60 structure
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Summary
1. Shimadzu XRD has long history
2. Shimadzu XRD-6000 is most compact & safety
3. Shimadzu XRD-6000 has most stable hardware
4. Shimadzu XRD-6000 has user friendly S/W
5. Shimadzu XRD-6000 has more capability