钍基熔盐核能系统

ASTM and TMSR irradiation program

Derek TsangSINAP

20.09.2013

Introduction SINAP has a irradiation program to get i-data for

material used in molten salt reactors. Metal and graphite ASTM standards will be used in all the material

properties measurement. Irradiation temperature is 650℃ Max dose for metal is 2.5×1019 n/cm2（ E >

0.1MeV） Max dose for graphite is 5×1020 n/cm2（ E >

0.1MeV）

Metal irradiation program

Total samples = 136 Samples for irradiation = 46

Properties ASTMHardness ASTM E18-12, E10-12Fatigue ASTM E606/E606M-12

Charpy impact test ASTM E23-12Modulus and Poisson's ratio ASTM E111-04, ASTM E132-04

Tensile test ASTM E8/E8M-09, ASTM E21-09

Alloy System

Corrosion Evaluation

Property Evaluation

Forming and Welding process

High cycle fatigue life

Low cycle fatigue life & Fracture toughness

Creep & Rupture & Impact

Oxidation evaluation

Thermal Stability & Thermal fatigue

Neutron irradiation properties

Corrosion specification

Corrosion verification

Corrosion performance of weldment

Corrosion calculation

Gas tungsten arc welding process

High energy beam welding process

Makeup and Repair & Stress evaluation

Pipe and Fittings process

Elbow and Drum process

Bending and Stamping process

Technical specification

Corrosion evaluation

Zhijun li

Guojun Yu

Jianping Liang

Li jiang

Bomou Zhou

Guangzhou Yuan

Yanling Lu

Fenfen Han

Li & Yan

Guojun Yu

Jingfeng Yang

Hua Sun

Juan Hou

Hua Ai

Shuangjian Chen

Kun Yu

Chaowen Li

Jianping Liang

Yongfeng Zhou

Xiaoke Li

Ye Zhang

Zhijun li

Tension and Impact Lab Creep and Rupture Lab

Fatigue Lab

Heat Treatment Lab

Metallographic Preparation Lab

Hardness Tester and Microscope

Mechanical Properties Platform

Lab Introduction-1

Other Analytical Instrument

Lab Introduction-2

Corrosion Lab

6

Thermal Properties Lab Microscope and Photometer

TEM石墨样品制备实验室

We

ldin

g L

ab

Graphite irradiation program

Total samples = 312 Samples for irradiation = 94 + 94

Properties ASTM no. of samplesThermal diffusivity ASTM C714 16+16

Specific heat capacity ASTM E1269 16+16Bulk Density ASTM C559 16+16

Young's modulus ASTMC769 16+16Flexural strength ASTM C651 16+16Tensile strength ASTM D3967 30+30

Compressive strength ASTM C695 16+16CTE ASTM E228 16+16

Tensile strength

Tensile strength sample size in ASTM is too big for our irradiation program

D3967 is for rock tensile strength Underestimate graphite tensile strength More experiment and

analytical/numerical studies. New ASTM standard for graphite tensile

strength?

DYM or SYM

Gas cooled reactor: gas has no mechanical effect on graphite.

May not be true for molten salt reactor. 3 ways to do graphite irradiation

experiment for molten salt reactorsA. Not consider molten salt at allB. Graphite samples in a container with molten

salt and irradiate together.C. Force molten salt into graphite samples

before irradiation experiment.

Standard requires no liquid inside the samples!

After irradiation experiment to measure DYM at what temperature? High DYM at room temperature Virgin DYM at high temperature

Virgin graphite with molten salt

Virgin graphite without molten salt

Some thoughts

ASTM Standards mainly for nuclear graphite in gas cooled reactor.

Nuclear graphite in molten salt reactor may need NEW ASTM standards???

Thank you!