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Institut für Integrierte Produktion Hannover | Produktion erforschen und entwickeln | „Hydroforming of Titanium Tubes“ Development of a multi stage hydroforming process for titanium tubes Hannover Messe | Hanover | April, 12th, 2013

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Page 1: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Institut für

Integrierte Produktion Hannover

| Produktion erforschen und entwickeln |

„Hydroforming of Titanium Tubes“

Development of a multi stage hydroforming process for titanium tubes

Hannover Messe | Hanover | April, 12th, 2013

Page 2: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Initial Situation

Context

- Hydroforming is a cost effective way of shaping metals into lightweight and strong pieces

- Titanium has a high potential for lightweight constructions

- Due to its low proportional elongation titanium was not processed by hydroforming yet

Intention

- Developing a hydroforming process for shaping titanium tubes

Result

- cost-efficient and complex lightweight parts with unprecedented properties

© IPH | Johannes Knust | Lehrstuhl für Umformtechnik Siegen | 2

Page 3: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Project Objectives

Overall Objective

Developing a cost effective process chain for hydroforming titanium tubes

Subtasks

– Subtask 1: Analyzing material properties of several titanium alloys and their hydroforming

process limits

– Subtask 2: Investigating adequate heat treatments to reestablish the formability

for several alloys and forming processes

– Subtask 3: Ascertain a suitable lubricant

© IPH | Johannes Knust | Lehrstuhl für Umformtechnik Siegen | 3

Page 4: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Experimental Studies

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 4

Expected Results

Selection of a suitable heat treatment

Analyze the influence of the tube

production on the workability of

titanium alloys

Ascertain suitable lubricants

Final outcome: Guidelines for

hydroforming titanium tubes

Scheduled Workflow

Pre-distension, heat treatment and

tensile test as well as microstructure

analysis of metal strips (UTS, PA)

Boundless expansion, heat treatment

and burst testing tube (UTS, PA)

Tribological examinations

(IPH, PA)

Process verification on a demonstration

part (IPH, if necessary PA)

Page 5: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Boundary conditions

Assimilation of tensile strength test

Pyramid of Inhomogeneity

Isothermal tensile test

© UTS Johannes Buhl | Lehrstuhl für Umformtechnik Siegen | 5

Page 6: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Isothermal Tensile Test

© UTS Johannes Buhl | Lehrstuhl für Umformtechnik Siegen | 6

Cooling Influence

Common tensile test

Isothermal tensile test

Isothermal tensile test

Based elongation φ [-]

Ba

se

d y

ield

str

ess

σ [

N/m

m²]

Based elongation φ [-]

Ba

se

d y

ield

str

ess

σ [

N/m

m²]

Water

(without current)

Page 7: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Isotherme Zugversuche

Mathematical description

― Nadai‘s approach:

© UTS Johannes Buhl | Lehrstuhl für Umformtechnik Siegen | 7

𝑘𝑓 𝑇, 𝑣 = 𝑣 = 0,001 − 10 𝑚𝑚/𝑠

𝑇 = 20 − 80 ° 𝐶

𝑘𝑓(𝑇, 𝑣) = 𝐴(𝑇, 𝑣) ∗ 𝜑𝑣𝑛(𝑇)

𝐴(𝑇, 𝑣) = 𝐴𝑆𝑡𝑎𝑟𝑡 + ln𝑉

𝑉𝑟𝑒𝑓 0,0077

𝑇

𝑇𝑟𝑒𝑓+ 20,804 − 1,7581

𝑇

𝑇𝑟𝑒𝑓

𝑛(𝑇) = 𝑛𝑆𝑡𝑎𝑟𝑡 − 0,00007𝑇

𝑇𝑟𝑒𝑓

True elongation φ [-]

Tru

e y

ield

str

ess σ

[N

/mm

²]

Velocity

v [mm/s]

Page 8: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Multi-Stage Process Chain

Illustration of a multi-stage process chain with sheet specimens

― tensile test with optimized heat treatment parameters:

– Pre-distension: εpre = 15 %, (εmin = 5 %)

– Annealing temperature: Theat = 750° C

– Annealing time: theat = 20 min

– Cooling: k = 750° C / 5 h

© UTS Johannes Buhl | Lehrstuhl für Umformtechnik Siegen | 8

Bas

ed

yie

ld s

tres

s σ

[N

/mm

²]

Based elongation φ [-]

Page 9: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Multi-Stage Process chain

Illustration of a multi-stage process chain with tubes

― Burst test with free ends

– Pre-distension: εpre = 12 %, (εmin = 5 %)

– After the third forming stage there was a maximum strain of φ = 0,35

© UTS Johannes Buhl | Produktion erforschen und entwickeln | 9

Expansion steps

Radia

l tr

ue s

train

φ [

-]

Page 10: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Tribological Examinations

Lubricants

Provided lubricants

– Berucoat AF 438 (air-hardening inorganic MoS2/Graphite – sliding lacquer) [B]

– Beruforge 150 DL (water-soluble drawing paste) [B]

– Beruforge 150 D (water-soluble drawing paste) [B]

– Kubibrac 4096-1 (fully synthetic high performance drawing oil) [B]

– Raziol IHU 350 Mg [R]

– Raziol IHU 1000 Mg [R]

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 10

Page 11: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Tribological Examinations

Results of the strip drawing test

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 11

Page 12: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Dies of the First Forming Stage

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 12

Page 13: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Dies of the Second Forming Stage

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 13

Page 14: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Results of the Hydroforming Experiments

Sample 44 Stage 1 Stage 2

(Strut-) Height 62,52 (~23 %) 70,56 (~38,9 % [~12,9 %])

Length 341,5 319

Circumference 199 214

Diameter ~ 51 51,09

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 14

Page 15: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Process Parameters

Sample 44

― Stage 1

― Stage 2

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 15

Time [s] 0,2 2 4 10,6 11,6 12,6

Pressure [bar] 180 250 330 380 390 585 (620)

Punch 1&2 [mm] 0,3 1,7 8 15 17 26 (27)

Strut [mm] 0 0 0 5 7 1

Time [s] 0,2 2 4 10,6 11,6 12,6

Pressure [bar] 180 250 330 380 390 620

Punch 1 [mm] 0,3 1,7 8 15 17 22

Punch 2 (T) [mm] 0,3 1,7 6 8 9 10

Strut [mm] 0 0 0 4 5 6

Page 16: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Simulations

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 16

Sample 44 Simulation Reality

(Strut-)Height 64,74 70,56 (~38,9 %)

Length 307,26 319

Failure No No

wall thickness

[mm]

Page 17: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Simulation

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 17

Component failure when considering anisotropy

Boundary conditions

Element type 16

Material Model 037 Transversely

Anisotropy

Anitsotropy 1

Boundary conditions

Element type 16

Material Model 037 Transversely

Anisotropy

Anitsotropy 4

Page 18: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Simulation

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 18

0

0,2

0,4

0,6

0,8

1

1,2

1,4

1,6

1,8

0 50 100 150 200 250 300 350

Wall T

hic

kn

ess

[m

m]

Position of the measurement points along the workpiece axis [mm]

R39

Sim-Rohr39-R1

Sim-Rohr39-R4

Wall thickness distribution in its dependencies of the anisotropy

Page 19: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Abstract and Forecast

Abstract

- Basic studies on hydroforming of titanium alloys have been successfully completed

- Multi-stage process chain has been successfully designed for shaping titanium tubes

- Demonstration parts have been successfully created

Forecast

- Improving the simulation results

- Defining an universal range of parameters

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 19

Page 20: „Hydroforming of Titanium Tubes“ - Deutsche …files.messe.de/abstracts/52747_121300_Knust_IPH_Hannover.pdfhydroforming titanium tubes Scheduled Workflow Pre-distension, heat treatment

Your Contacts

© IPH | Johannes Knust | Produktion erforschen und entwickeln | 20

FST1: Dipl. Ing. Johannes Knust

IPH - Institut für Integrierte Produktion Hannover gGmbH

Hollerithallee 6

30419 Hannover

+49 (0)511 27976-331

7 +49 (0)511 27976-888

@ [email protected]

www.iph-hannover.de

FST2: Dipl.-Ing. Johannes Buhl

Universität Siegen | Lehrstuhl für Umformtechnik

Paul – Bonatz – Straße 9-11

57076 Siegen

+49 (0)271 740-3059

7 +49 (0)271 740-2772

@ [email protected]

www.uni-siegen.de/fb11/fw/

www.ihu-titan.de Das IGF-Vorhaben 16452N der Forschungsvereinigung

Europäische Forschungsgesellschaft für Blechverarbeitung

e. V. wurde über die AiF im Rahmen des Programms zur

Förderung der industriellen Gemeinschaftsforschung und -

entwicklung (IGF) vom Bundesministerium für Wirtschaft und

Technologie aufgrund eines Beschlusses des Deutschen

Bundestages gefördert.