pressure!¼chi glas uster... · 0.5liter 6bar tablemodel 47.30007.0000 1.0liter 6bar tablemodel...
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Catalog 2010/2011Büchi pressure autoclaves from A to Z
Pressure!
Table of contents
Inert autoclaves (non-metallic)miniclave 4inertclave 7
Autoclaves (metal/glass)tinyclave steel 14miniclave steel 18miniclave drive 22picoclave 26ecoclave 31polyclave 38versoclave 45kiloclave 51midiclave 58limbo 63limbo li 64limbo ls 68
Drivescyclone 075 70cyclone 300 71cyclone «i» 72Ex-Drive 73
Magnetic couplingsbmd 075 75bmd 300 / 800 / 1200 79bmd 1800 / 3600 83
Mixing elementsStirrer shafts 84Stirrers 90Baffles 93
Vesselstinyclave steel 94miniclave, miniclave steel, miniclave drive, picoclave 95inertclave, ecoclave, polyclave, versoclave, kiloclave 101midiclave 123limbo, limbo li 127
Cover platesCover plates 128
7
6
5
4
3
2
1
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Table of contents
Bursting discs / Relief valvesBursting discs 130Relief valves 131
ValvesValves 132
Fittings and tubesFittings 134Connection tubes 136Dip tubes 137
SealsFlat seals 140Collar packings 140Diamond shape seals for bottom valves 141Seals and packings for bottom valves 141PTFE-Tape 141O-Rings 142Seal for Torion valve 142Shaft seals for stirrer shafts and magnetic coupling 142
Variable componentsBurettes 143Sampling system 145Feeding funnel 146Heat exchanger 147Reflux cooler 148Catalyst basket 149Distillation system made of glass 150
Instrumentationbds md 151bds.sc 152bds mc 153bds mc Ex-Box 154pH-Measurement 155Temperature controller «btc» 156Temperature measurement 157Pressure measurement 160Speed measurement 162büchi pressflow gas controller «bpc» 164Software «bls 2» 165
AccessoriesAccessories 166
14
13
12
11
10
9
8
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Inert autoclaves (non-metallic)«miniclave»
The same device can be used with the following vessels:
� Glass vessels Type 1 without jacket 100 / 200 / 250 / 300ml
The reactor has no stirrer and can be heated
using a bath thermostat. Max. temperature 150°C.
The standard scope of delivery includes the following parts:
� Vessel holder with protective mesh
� Vessel Type 1
� Union nut
� Cover plate with standard setup:
Swagelok-fittings with bursting disc, manometer, valve, thermometer sleeve
� Tools and spare parts
� Documentation with operation manual, CE-declaration
of conformity and certificates
� Manufactured and tested according to PED, AD2000
Autoclave for small scale experiments, without stirrerall product touched parts are made of: Glass, PTFE, PFA, FEP, Viton
«miniclave» Type 1Standard cover plate up to max. 10 bar at 100°C or 6 bar at 150°C, glass vessel without bottom opening, for max. 10 bar in the laboratory and in the auto-
clave room, max. temperature 150°C, vessel holder with protective mesh, complete with accessories, spare parts and tools, assembled and ready for ope-
ration.
«miniclave» Type 1 Standard100 ml 10 bar 47.30003.0000200 ml 10 bar 47.30004.0000250 ml 10 bar 47.30005.0000300 ml 10 bar 47.30006.0000
4
1
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inert autoclaves (non-metallic)«miniclave»
5
1
Weight ca. 1.2 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
270
160 110
Inert autoclaves (non-metallic)«miniclave»
6
1
Setup, PTFE
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inert autoclaves (non-metallic)«inertclave»
The same device can be used with the following vessels:
� Glass vessels Type 1 with round bottom
� Glass vessels Type 1B with round bottom and Torion bottom valve
� Glass vessels Type 1I, with round bottom and insulation jacket
� Glass vessels Type 1BI with round bottom, bottom valve and insulation jacket
The autoclave is equipped with a magnetic drive «cyclone i»
for speeds of 10 – 900 min-1.
The stand is available in blue.
The standard scope of delivery includes the following parts:
� Stand with polycarbonate protective screen
� Glass vessel with stirrer, bottom valve depending on vessel type
� Cover plate made of PEEK with standard setup:
PFA Swagelok fittings, bursting disc made of graphite, manometer
with PTFE seal, glass Pt-100 and 2 PFA straight way valves
� Stirrer drive «cyclone i» with integrated magnetic coupling, 10 - 900 min-1
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«inertclave» Type 1Magnetic drive cyclone i, adjustable 10 - 900 min-1, motor 110 / 230 V, 50 / 60 Hz, cover plate up to max. 6 bar, glass vessel without bottom valve for max.
6 bar, graduated, jacket heatable up to max. 180°C, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled
and ready for operation.
«inertclave» Type 1 Standard0.5 Liter 6 bar Table model 47.30007.00001.0 Liter 6 bar Table model 47.30008.0000
7
1
Autoclave with all product touched partsmade of PEEK, PFA, PTFE, glass
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Inert autoclaves (non-metallic)«inertclave»
8
1
«inertclave» Type 1BMagnetic drive cyclone i, adjustable 10 - 900 min-1, motor 110 / 230 V, 50 / 60 Hz, cover plate up to max. 6 bar, glass vessel with bottom valve for max. 6
bar, graduated, jacket heatable up to max. 180°C, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and
ready for operation.
«inertclave» Type 1B Standard0.5 Liter 6 bar Table model 47.30009.00001.0 Liter 6 bar Table model 47.30010.0000
«inertclave» Type 1IMagnetic drive cyclone i, adjustable 10 - 900 min-1, motor 110 / 230 V, 50 / 60 Hz, cover plate up to max. 6 bar, glass vessel without bottom valve with ad-
ditional evacuated insulation jacket, for max. 6 bar, graduated, jacket heatable up to max. 180°C, complete with stand, polycarbonate protective screen,
accessories, spare parts and tools, assembled and ready for operation.
«inertclave» Type 1I Standard0.5 Liter 6 bar Table model 47.30011.00001.0 Liter 6 bar Table model 47.30012.0000
«inertclave» Type 1BIMagnetic drive cyclone i, adjustable 10 - 900 min-1, motor 110 / 230 V, 50 / 60 Hz, cover plate up to max. 6 bar, glass vessel with bottom valve and addi-
tional evacuated insulation jacket, for max. 6 bar, graduated, jacket heatable up to max. 180°C, complete with stand, polycarbonate protective screen,
accessories, spare parts and tools, assembled and ready for operation.
«inertclave» Type 1BI Standard0.5 Liter 6 bar Table model 47.30013.00001.0 Liter 6 bar Table model 47.30014.0000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inert autoclaves (non-metallic)«inertclave»
9
1
Dimensions
Weight ca. 25 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
975
675
474
ø415
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Inert autoclaves (non-metallic)«inertclave»
10
1
Setup
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Plug
Plug
O-RingO-Ring
Manometer
Bursting disc
Flexible tube
Seal
Seal
O-Ring
Male connector
Male connector
O-Ring
O-Ring
O-Ring
Y-Piece
Needle valve
Connection tube
Male connector
O-Ring
O-Ring2xPt100
Male connectorBT
O-Ring
Stirrer vessel
Stirrer
Seal
Dichtung
Screw cap
Inert autoclaves (non-metallic)«miniclave», «inertclave»
11
1
Connector 1/4" NPT / 1/4" Swagelok PFA 52.10114.0000 • •Connector BT 1/4" NPT / 1/4" Swagelok PFA 52.10115.0000 • •
Spare parts for connectorNut 40.02519.0000 • •Ferrule rear 1/4" PFA 40.01461.0000 • •Ferrule front 1/4" PFA 40.01460.0000 • •
Plug 1/4" NPT, PTFE 52.10116.0000 • •Plug 1/2" NPT, PTFE 40.02416.0000 •Plug Pg 13,5, PTFE 40.02415.0000 •
Housing for bursting foil cpl., PTFE 52.10110.0000 • •
Bursting foil FEP 10 bar 52.10112.0000 •
Bursting disc 6 bar, graphite 46.40079.0000 •
O-Ring 7.65 x 1.78, Viton (for NPT 1/4") 46.90078.0000 •O-Ring 7.65 x 1.78, Kalrez (for NPT 1/4") 46.90080.0000 •O-Ring 14.0 x 1.78, Kalrez (for NPT 1/2") 46.80091.0000 •O-Ring 12.37 x 2.62, Kalrez (for PG 13.5) 46.90079.0000 •O-Ring 17.86 x 2.62, Kalrez (for cyclone i) 46.80092.0000 •O-Ring 56.74 x 3.53, Viton 52.10109.0000 •O-Ring 56.74 x 3.53, Kalrez 52.10103.0000 •
Needle valve 1/4" Swagelok PFA 52.10113.0000 • •
Holder for needle valve 52.10137.0000 • •
Part number miniclave
inertclave
miniclave
inertclave
Accessories
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Inert autoclaves (non-metallic)«miniclave», «inertclave»
12
1
Y-piece 1/4" NPT male / 2 x 1/4" female, PTFE 52.10132.0000 • •
Holder for Y-piece 52.10148.0000 •Holder for Y-piece 40.02431.0000 •
Cover plate with 4 x 1/4" NPT, PTFE 52.10157.0000 •
Cover plate 4 x 1/4" NPT, 1 x 1/2" NPT, 1 x PG 13.5, PEEK 46.00002.0205 •
GL32 screw cap 40.02413.0000 •
Seal for cyclone i 29/18, Silicone / PTFE 40.02414.0000 •
Pt-100 2x, glass (without plug) 46.60143.0000 • •
Thermometer sleeve 140 mm, glass for 100 ml 52.10122.0000 •Thermometer sleeve 170 mm, glass for 200 ml 52.10128.0000 •Thermometer sleeve 200 mm, glass for 250 / 300 ml 52.10153.0000 • •
Part number miniclave
inertclave
miniclave
inertclave
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Connection tube 1/4", PFA 52.10146.0000 • •
Inert autoclaves (non-metallic)«miniclave», «inertclave»
13
1
Manometer -1/+15 bar, 1/4" NPT, with PTFE seal 52.10101.0000 • •
Feeding funnel NS29/32/NPT 1/2"PEEK with Kalrez O-Ring 46.90157.0000 •
Part number miniclave
inertclave
For Vessels see chapter 6
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Thermometer 150 mm / 0-150°C, glass for 100 ml 52.10133.0000 •Thermometer 180 mm / 0-150°C, glass for 200 ml 52.10134.0000 •Thermometer 210 mm / 0-150°C, glass for 250/300 ml 52.10154.0000 • •
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«tinyclave steel»
14
2
The same device can be used with the following vessels:
� Glass vessels Type 1 without jacket 10 / 25ml
The reactor has no stirrer and can be heated
using a bath thermostat. Max. temperature 200°C.
The standard scope of delivery includes the following parts:
� Vessel holder with protective mesh
� Vessel Type 1
� Union nut
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and valve
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«tinyclave steel» Type 1Standard cover plate, glass vessel without bottom opening, for max. 10 bar in the laboratory and in the autoclave room, max. temperature 200°C, vessel
holder with protective mesh, complete with accessories, spare parts and tools, assembled and ready for operation.
«tinyclave steel» Type 1 Standard Hastelloy
10 ml 10 bar 51.10200.0000 51.10200.220025 ml 10 bar 51.10201.0000 51.10201.2200
Autoclave for small scale experiments without stirrer
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«tinyclave steel»
15
2
Dimensions
Weight ca. 0.7 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
300
130 110
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«tinyclave steel»
16
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«tinyclave steel»
17
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«miniclave steel»
18
2
The same device can be used with the following vessels:
� Glass vessels Type 1 without jacket 100 / 200 / 250 / 300ml
The reactor has no stirrer and can be heated
using a bath thermostat. Max. temperature 200°C.
The standard scope of delivery includes the following parts:
� Vessel holder with protective mesh
� Vessel Type 1
� Union nut
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer, valve, thermometer sleeve
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«miniclave steel» Type 1Standard cover plate up to max. 60 bar, glass vessel without bottom opening, for max. 10 bar in the laboratory and in the autoclave room, max. tempera-
ture 200°C, vessel holder with protective mesh, complete with accessories, spare parts and tools, assembled and ready for operation.
«miniclave steel» Type 1 Standard Hastelloy
100 ml 10 bar 47.30015.0000 47.30015.2200200 ml 10 bar 47.30016.0000 47.30016.2200250 ml 10 bar 47.30017.0000 47.30017.2200300 ml 10 bar 47.30018.0000 47.30018.2200
Autoclave for small scale experiments, without stirrer
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«miniclave steel»
19
2
Dimensions
Weight ca. 3.3 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
320
180 120
Autoclaves (metal/glass)«miniclave steel»
20
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«miniclave steel»
21
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«miniclave drive»
22
2
The same device can be used with the following vessels with fast action closure:
� Steel vessels Type 3 with jacket and bottom opening
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The standard scope of delivery includes the following parts:
� Pipe frame with fittings and holding bracket
for height adjustable installation of the reactor system
� Vessel (Type 3) with suitable stirrer shaft and stirrer, Pt100 without plug
� Screw closure or fast action closure
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling, incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«miniclave drive» Type 3 with fast action closureMagnetic drive cyclone 075, adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
opening and plug, welded heating jacket, heatable up to max. 250°C, for max. 60 bar, complete with frame, accessories, spare parts and tools, assembled
and ready for operation.
«miniclave drive» Type 3 with fast action closure Standard Hastelloy
100 ml 60 bar Table model 47.30030.0000 47.30030.2200200 ml 60 bar Table model 47.30031.0000 47.30031.2200300 ml 60 bar Table model 47.30032.0000 47.30032.2200
Autoclave for small scale experiments with steel vessels
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Standard Hastelloy
Magnetic coupling «bmd075» instead
of «cyclone 075», incl. flexible shaft coupling
for external drive. (drive not included)
47.40001.0000 47.40001.2200
Options (add to base price)
Autoclaves (metal/glass)«miniclave drive»
23
2
Dimensions
Controller cc075: 240 x 210 x 90 mm / 1.0 kg «miniclave drive» Weight ca. 13.0 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
700
370500
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«miniclave drive»
24
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«miniclave drive»
25
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«picoclave»
26
2
The same device can be used with the following vessels:
� Glass vessels Type 1 with heating jacket
� Glass vessels Type 1B with heating jacket and bottom valve
� Steel vessels Type 3 with heating jacket and bottom opening
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The standard scope of delivery includes the following parts:
� Stand (choice of colors) with polycarbonate protective screen
� Vessel (Type 1 / 3) with suitable stirrer shaft and stirrer, Pt100 without plug
� fast action closure
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling,
incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity
and certificates
� Manufactured and tested according to PED, AD2000
«picoclave» Type 1 with fast action closureMagnetic drive cyclone 075, adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel without bot-
tom valve, for max. 10 bar in the laboratory and in the autoclave room, jacket heatable up to max. 200°C, complete with stand, accessories, spare parts
and tools, assembled and ready for operation.
«picoclave» Type 1 with fast action closure Standard Hastelloy
100 ml 10 bar Table model 47.30033.0000 47.30033.2200200 ml 10 bar Table model 47.30034.0000 47.30034.2200250 ml 10 bar Table model 47.30035.0000 47.30035.2200300 ml 10 bar Table model 47.30036.0000 47.30036.2200
Specify stand color upon ordering: blue or chrome
Autoclave for small scale experiments with steel- or glass vessels,with fast action closure, stand with protective screen
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«picoclave»
27
2
«picoclave» Type 1B with fast action closureMagnetic drive cyclone 075, adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel with bottom
valve, for max. 6 bar in the laboratory and in the autoclave room, jacket heatable up to max. 200°C, complete with stand, accessories, spare parts and
tools, assembled and ready for operation.
«picoclave» Type 1B with fast action closure Standard Hastelloy
100 ml 6 bar Table model 47.30037.0000 47.30037.2200200 ml 6 bar Table model 47.30038.0000 47.30038.2200250 ml 6 bar Table model 47.30039.0000 47.30039.2200300 ml 6 bar Table model 47.30040.0000 47.30040.2200
Specify stand color upon ordering: blue or chrome
«picoclave» Type 3 with fast action closureMagnetic drive cyclone 075, adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
opening and plug, welded heating jacket, heatable up to max. 250°C, for max. 60 bar, complete with stand, accessories, spare parts and tools, assembled
and ready for operation.
«picoclave» Type 3 with fast action closure Standard Hastelloy
100 ml 60 bar Table model 47.30041.0000 47.30041.2200200 ml 60 bar Table model 47.30042.0000 47.30042.2200300 ml 60 bar Table model 47.30043.0000 47.30043.2200
Specify stand color upon ordering: blue or chrome
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«picoclave»
28
2
Dimensions
Controller cc075: 240 x 210 x 90 mm / 1.0 kg «picoclave» Weight ca. 15.0 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
768
513
334
353
Autoclaves (metal/glass)«picoclave»
29
2
Bursting disc
Manometer
Glass reactor
Stirrer
Stirrer shaft
Fast acting closure
Protecting ring
Internalmagnet
Adapter for manometer
Tube bent
Adapter for manometer
O-Ring
SealSeal
Plate
Pt 100
Control valve
Plug
Dip tube
Connection tube 90mm
Control valve
cycl
one
075
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«picoclave»
30
2
Bursting disc
Manometer
Glass reactor
Stirrer
Stirrer shaft
Fast acting closure
Protecting ring
Internalmagnet
Adapter for manometer
Tube bent
Adapter for manometer
O-Ring
SealSeal
PlatePlug
Dip tube
Connection tube 105mm
Straight way valve
Connection tube 50mm
Pt 100
cycl
one
075
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«ecoclave»
The same device can be used with the following vessels:
� Glass vessels Type 1 with round bottom
� Glass vessels Type 1B with round bottom and bottom valve
� Glass vessels Type 1I, with round bottom and insulation jacket
� Glass vessels Type 1BI with round bottom, bottom valve and insulation jacket
� Glass vessels Type 2, cylindrical with bottom valve
� Steel vessels Type 3 with bottom valve
� Steel vessels Type 4 with sight glasses and bottom valve
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The stand is available in blue or chrome.
The standard scope of delivery includes the following parts:
� Stand (choice of colors) with polycarbonate protective screen
� Vessel (Type 1 / 2 / 3 / 4) with suitable stirrer shaft, stirrer, baffle, Pt-100 without plug,
bottom valve depending on vessel Type
� Cover plate with standard setup: Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling, incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
Autoclave for reactions with steel- or glass vessels,stand with protective screen
«ecoclave 075» Type 1Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel without bot-
tom valve, for max. 6 bar in the laboratory, max. 12 bar in the autoclave room, graduated, jacket heatable up to max. 200°C, complete with stand, polycar-
bonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«ecoclave 075» Type 1 Standard Hastelloy
0.25 Liter 6 bar Table model 47.30044.0000 47.30044.22000.5 Liter 6 bar Table model 47.30045.0000 47.30045.22001.0 Liter 6 bar Table model 47.30046.0000 47.30046.22001.6 Liter 6 bar Table model 47.30047.0000 47.30047.2200
Specify stand color upon ordering: blue or chrome
31
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«ecoclave»
32
2
«ecoclave 075» Type 1BMagnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel with Torion
bottom valve, for max. 6 bar in the laboratory and in the autoclave room, graduated, jacket heatable up to max. 200°C, complete with stand, polycarbona-
te protective screen, accessories, spare parts and tools, assembled and ready for operation.
«ecoclave 075» Type 1B Standard Hastelloy
0.25 Liter 6 bar Table model 47.30048.0000 47.30048.22000.5 Liter 6 bar Table model 47.30049.0000 47.30049.22001.0 Liter 6 bar Table model 47.30050.0000 47.30050.22001.6 Liter 6 bar Table model 47.30051.0000 47.30051.2200
Specify stand color upon ordering: blue or chrome
«ecoclave 075» Type 1IMagnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel without bot-
tom valve, for max. 6 bar in the laboratory, max. 12 bar in the autoclave room, graduated, jacket heatable up to max. 200°C, addl. evacuated insulation ja-
cket, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«ecoclave 075» Type 1I Standard Hastelloy
0.5 Liter 6 bar Table model 47.30052.0000 47.30052.22001.0 Liter 6 bar Table model 47.30053.0000 47.30053.22001.6 Liter 6 bar Table model 47.30054.0000 47.30054.2200
Specify stand color upon ordering: blue or chrome
«ecoclave 075» Type 1BIMagnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel with Torion
bottom valve, for max. 6 bar in the laboratory and in the autoclave room, graduated, jacket heatable up to max. 200°C, addl. evacuated insulation jacket,
complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«ecoclave 075» Type 1BI Standard Hastelloy
0.5 Liter 6 bar Table model 47.30055.0000 47.30055.22001.0 Liter 6 bar Table model 47.30056.0000 47.30056.22001.6 Liter 6 bar Table model 47.30057.0000 47.30057.2200
Specify stand color upon ordering: blue or chrome
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«ecoclave»
33
2
«ecoclave 075» Type 2Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, cylindrical glass vessel
with bottom opening and bottom valve, for max. 3/6 bar in the laboratory, max. 5/12 bar in the autoclave room, graduated, with bottom- and intermediate
flange, jacket heatable up to max. 200°C, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready
for operation.
«ecoclave 075» Type 2 Standard Hastelloy
0.5 Liter 6 bar Table model 47.30058.0000 47.30058.22001.0 Liter 6 bar Table model 47.30059.0000 47.30059.22001.5 Liter 6 bar Table model 47.30060.0000 47.30060.22002.0 Liter 3 bar Table model 47.30061.0000 47.30061.2200
Specify stand color upon ordering: blue or chrome
«ecoclave 075» Type 3Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, polycarbonate protective screen, accessories, spare parts
and tools, assembled and ready for operation.
«ecoclave 075» Type 3 Standard Hastelloy
0.5 Liter 60 bar Table model 47.30062.0000 47.30062.22001.0 Liter 60 bar Table model 47.30063.0000 47.30063.22001.5 Liter 60 bar Table model 47.30064.0000 47.30064.22002.0 Liter 60 bar Table model 47.30065.0000 47.30065.22003.0 Liter 60 bar Table model 47.30066.0000 47.30066.22005.0 Liter 40 bar Table model 47.30067.0000 47.30067.2200
Specify stand color upon ordering: blue or chrome
«ecoclave 075» Type 4Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve and 2 sight glasses, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, polycarbonate protective screen, acces-
sories, spare parts and tools, assembled and ready for operation.
«ecoclave 075» Type 4 Standard Hastelloy
1.0 Liter 60 bar Table model 47.30068.0000 47.30068.22001.5 Liter 60 bar Table model 47.30069.0000 47.30069.22002.0 Liter 60 bar Table model 47.30070.0000 47.30070.22003.0 Liter 60 bar Table model 47.30071.0000 47.30071.22005.0 Liter 40 bar Table model 47.30072.0000 47.30072.2200
Specify stand color upon ordering: blue or chrome
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«ecoclave»
34
2
Electric heatingFor Type 3 and Type 4 vessels, complete with PID controller,
water cooling with solenoid valve, 230V/110V, 50/60Hz
Not ATEX! The surcharge is identical for standard and Hastelloy systems
Type 3E 0.50 L, complete 47.40052.0000Type 3E 1.00 L, complete 47.40053.0000Type 3E 1.50 L, complete 47.40054.0000Type 3E 2.00 L, complete 47.40055.0000
Type 4E 1.00 L, complete 47.40056.0000Type 4E 1.50 L, complete 47.40057.0000Type 4E 2.00 L, complete 47.40058.0000
Standard Hastelloy
«cyclone 300»Drive with integrated magnetic coupling
and controller
47.40002.0000 47.40002.2200
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
987
675
ø415
476
843
755
603
Autoclaves (metal/glass)«ecoclave»
35
2
Dimensions
Weight ca. 33 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«ecoclave»
36
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«ecoclave»
37
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«polyclave»
The same device can be used with the following vessels:
� Glass vessels Type 1 with round bottom
� Glass vessels Type 1B with round bottom and bottom valve
� Glass vessels Type 1I, with round bottom and insulation jacket
� Glass vessels Type 1BI with round bottom, bottom valve and insulation jacket
� Glass vessels Type 2, cylindrical with bottom valve
� Steel vessels Type 3 with bottom valve
� Steel vessels Type 4 with sight glasses and bottom valve
The autoclave is equipped with a magnetic drive «cyclone 300»
for stirrer speeds of 0 – 2000 min-1.
The stand is available in blue or chrome.
The standard scope of delivery includes the following parts:
� Stand (choice of colors) with polycarbonate protective screen
� Vessel (Type 1 / 2 / 3 / 4) with suitable stirrer shaft, stirrer, baffle, Pt-100 without plug,
bottom valve depending on vessel Type
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 300» with integrated magnetic coupling, incl. controller «cc300»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«polyclave» Type 1Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel without bot-
tom valve, for max. 6 bar in the laboratory, max. 12 bar in the autoclave room, graduated, jacket heatable up to max. 200°C, complete with stand, polycar-
bonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«polyclave» Type 1 Standard Hastelloy
0.25 Liter 6 bar Table model 47.30073.0000 47.30073.22000.5 Liter 6 bar Table model 47.30074.0000 47.30074.22001.0 Liter 6 bar Table model 47.30075.0000 47.30075.22001.6 Liter 6 bar mobile floor model 47.30076.0000 47.30076.22002.0 Liter 6 bar mobile floor model 47.30077.0000 47.30077.2200
Specify stand color upon ordering: blue or chrome
38
Autoclave for reactions with steel- or glass vessels,stand with protective screen, modular setup
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«polyclave»
«polyclave» Type 1BMagnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel with Torion
bottom valve, for max. 6 bar in the laboratory and in the autoclave room, graduated, jacket heatable up to max. 200°C, complete with stand, polycarbona-
te protective screen, accessories, spare parts and tools, assembled and ready for operation.
«polyclave» Type 1B Standard Hastelloy
0.25 Liter 6 bar Table model 47.30078.0000 47.30078.22000.5 Liter 6 bar Table model 47.30079.0000 47.30079.22001.0 Liter 6 bar Table model 47.30080.0000 47.30080.22001.6 Liter 6 bar mobile floor model 47.30081.0000 47.30081.22002.0 Liter 6 bar mobile floor model 47.30082.0000 47.30082.2200
Specify stand color upon ordering: blue or chrome
«polyclave» Type 1IMagnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel without bot-
tom valve, for max. 6 bar in the laboratory, max. 12 bar in the autoclave room, graduated, jacket heatable up to max. 200°C, addl. evacuated insulation ja-
cket, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«polyclave» Type 1l Standard Hastelloy
0.5 Liter 6 bar Table model 47.30083.0000 47.30083.22001.0 Liter 6 bar Table model 47.30084.0000 47.30084.22001.6 Liter 6 bar mobile floor model 47.30085.0000 47.30085.22002.0 Liter 6 bar mobile floor model 47.30086.0000 47.30086.2200
Specify stand color upon ordering: blue or chrome
«polyclave» Type 1BIMagnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, glass vessel with Torion
bottom valve, for max. 6 bar in the laboratory and in the autoclave room, graduated, jacket heatable up to max. 200°C, addl. evacuated insulation jacket,
complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready for operation.
«polyclave» Type 1Bl Standard Hastelloy
0.5 Liter 6 bar Table model 47.30087.0000 47.30087.22001.0 Liter 6 bar Table model 47.30088.0000 47.30088.22001.6 Liter 6 bar mobile floor model 47.30089.0000 47.30089.22002.0 Liter 6 bar mobile floor model 47.30090.0000 47.30090.2200
Specify stand color upon ordering: blue or chrome
39
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«polyclave»
40
2
«polyclave» Type 2Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, cylindrical glass vessel with
bottom opening and bottom valve, for max. 3/6 bar in the laboratory, max. 5/12 bar in the autoclave room, graduated, with bottom- and intermediate flan-
ge, jacket heatable up to max. 200°C, complete with stand, polycarbonate protective screen, accessories, spare parts and tools, assembled and ready for
operation.
«polyclave» Type 2 Standard Hastelloy
0.5 Liter 6 bar Table model 47.30091.0000 47.30091.22001.0 Liter 6 bar Table model 47.30092.0000 47.30092.22001.5 Liter 6 bar Table model 47.30093.0000 47.30093.22002.0 Liter 6 bar mobile floor model 47.30094.0000 47.30094.22002.0 Liter 3 bar Table model 47.30095.0000 47.30095.22003.0 Liter 3 bar mobile floor model 47.30096.0000 47.30096.22005.0 Liter 3 bar mobile floor model 47.30097.0000 47.30097.2200
Specify stand color upon ordering: blue or chrome
«polyclave» Type 3Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, polycarbonate protective screen, accessories, spare parts
and tools, assembled and ready for operation.
«polyclave» Type 3 Standard Hastelloy
0.5 Liter 60 bar Table model 47.30098.0000 47.30098.22001.0 Liter 60 bar Table model 47.30099.0000 47.30099.22001.5 Liter 60 bar Table model 47.30100.0000 47.30100.22002.0 Liter 60 bar Table model 47.30101.0000 47.30101.22003.0 Liter 60 bar Table model 47.30102.0000 47.30102.22005.0 Liter 40 bar Table model 47.30103.0000 47.30103.2200
Specify stand color upon ordering: blue or chrome
«polyclave» Type 4Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve and 2 sight glasses, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, polycarbonate protective screen, acces-
sories, spare parts and tools, assembled and ready for operation.
«polyclave» Type 4 Standard Hastelloy
1.0 Liter 60 bar Table model 47.30104.0000 47.30104.22001.5 Liter 60 bar Table model 47.30105.0000 47.30105.22002.0 Liter 60 bar Table model 47.30106.0000 47.30106.22003.0 Liter 60 bar Table model 47.30107.0000 47.30107.22005.0 Liter 40 bar Table model 47.30108.0000 47.30108.2200
Specify stand color upon ordering: blue or chrome
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«polyclave»
41
2
Electric heatingFor Type 3 and Type 4 vessels, complete with PID controller,
water cooling with solenoid valve, 230V/110V, 50/60Hz
Not ATEX! The surcharge is identical for standard and Hastelloy systems
Type 3E 0.50 L, complete 47.40052.0000Type 3E 1.00 L, complete 47.40053.0000Type 3E 1.50 L, complete 47.40054.0000Type 3E 2.00 L, complete 47.40055.0000Type 3E 3.00 L, complete 47.40059.0000Type 3E 5.00 L, complete 47.40060.0000
Type 4E 1.00 L, complete 47.40056.0000Type 4E 1.50 L, complete 47.40057.0000Type 4E 2.00 L, complete 47.40058.0000Type 4E 3.00 L, complete 47.40061.0000Type 4E 5.00 L, complete 47.40062.0000
TrolleyH=500mm
Vessel lift and fast action closurefor vessels Type 1-4, max. 60 bar
Vessel lift (without fast action closure)
for vessels Typ 1-4 with bolt-on closure
Ex drive «Ex e II T4»Motor 230/400V, 50 Hz,
with adjustable transmission and bmd 300
(price for ATEX version of bmd is not included)
47.40004.0000
47.40005.0000
47.40006.0000 47.40006.2200
42.40118.0000
Standard Hastelloy
«cyclone 075»Drive with integrated magnetic coupling
and controller
47.40003.0000 47.40003.2200
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«polyclave»
42
2
Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Weight ca. 100 kg
Dimensions
1640
1605
1100
505
530
530
692
Autoclaves (metal/glass)«polyclave»
43
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«polyclave»
44
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«versoclave»
45
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
The same device can be used with the following vessels:
� Steel vessels Type 3 with bottom valve
� Steel vessels Type 4 with sight glasses and bottom valve
The autoclave is equipped with a magnetic drive «cyclone 300»
for stirrer speeds of 0 – 2000 min-1.
The standard scope of delivery includes the following parts:
� Stand
� Vessel (Type 3 / 4) with suitable stirrer shaft, stirrer, baffle, Pt-100 without plug,
bottom valve
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 300» with integrated magnetic coupling, incl. controller «cc300»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«versoclave» Type 3Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, accessories, spare parts and tools, assembled and ready for
operation.
«versoclave» Type 3 Standard Hastelloy
0.5 Liter 60 bar Table model 47.30160.0000 47.30160.22001.0 Liter 60 bar Table model 47.30161.0000 47.30161.22001.5 Liter 60 bar Table model 47.30162.0000 47.30162.22002.0 Liter 60 bar Table model 47.30163.0000 47.30163.22003.0 Liter 60 bar Table model 47.30164.0000 47.30164.22005.0 Liter 40 bar Table model 47.30165.0000 47.30165.2200
«versoclave» Type 4Magnetic drive «cyclone 300», adjustable 0-2000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve and 2 sight glasses, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, accessories, spare parts and tools, as-
sembled and ready for operation.
«versoclave» Type 4 Standard Hastelloy
1.0 Liter 60 bar Table model 47.30166.0000 47.30166.22001.5 Liter 60 bar Table model 47.30167.0000 47.30167.22002.0 Liter 60 bar Table model 47.30168.0000 47.30168.22003.0 Liter 60 bar Table model 47.30169.0000 47.30169.22005.0 Liter 40 bar Table model 47.30170.0000 47.30170.2200
Autoclave for reactions with steel vessels,modular setup
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«versoclave»
46
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
200 bar versionNot available with fast action closure!
Type 3 0.50 L, 200 bar, complete 47.40090.0000 47.40090.2200Type 3 1.00 L, 200 bar, complete 47.40091.0000 47.40091.2200Type 3 1.50 L, 200 bar, complete 47.40092.0000 47.40092.2200Type 3 2.00 L, 200 bar, complete 47.40093.0000 47.40093.2200Type 3 3.00 L, 200 bar, complete 47.40094.0000 47.40094.2200Type 3 5.00 L, 200 bar, complete 47.40095.0000 47.40095.2200
TrolleyH=500mm
Vessel lift and fast action closurefor vessels Type 3-4, max. 60 bar
Vessel lift (without fast action closure)
for vessels Typ 3-4 with bolt-on closure
Ex drive «Ex e II T4»Motor 230/400V, 50 Hz,
with adjustable transmission and bmd 300
(price for ATEX version of bmd is not included)
47.40004.0000
47.40005.0000
47.40006.0000 47.40006.2200
42.40118.0000
Standard Hastelloy
«cyclone 075»Drive with integrated magnetic coupling
and controller
47.40003.0000 47.40003.2200
Options (add to base price)
200 bar
Autoclaves (metal/glass)«versoclave»
47
2
Electric heatingFor Type 3 and Type 4 vessels, complete with PID controller,
water cooling with solenoid valve, 230V/110V, 50/60Hz
Not ATEX! The surcharge is identical for standard and Hastelloy systems
Type 3E 0.50 L, complete 47.40052.0000Type 3E 1.00 L, complete 47.40053.0000Type 3E 1.50 L, complete 47.40054.0000Type 3E 2.00 L, complete 47.40055.0000Type 3E 3.00 L, complete 47.40059.0000Type 3E 5.00 L, complete 47.40060.0000
Type 4E 1.00 L, complete 47.40056.0000Type 4E 1.50 L, complete 47.40057.0000Type 4E 2.00 L, complete 47.40058.0000Type 4E 3.00 L, complete 47.40061.0000Type 4E 5.00 L, complete 47.40062.0000
Standard Hastelloy
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«versoclave»
48
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Weight ca. 80 kg
Dimensions
1147
505
454
500
685
Autoclaves (metal/glass)«versoclave»
49
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Setup, stainless steel
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«versoclave»
50
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Setup, Hastelloy
Autoclaves (metal/glass)«kiloclave»
The same device can be used with the following vessels:
� Steel vessels Type 3 with bottom valve
� Steel vessels Type 4 with sight glasses and bottom valve
The stand is equipped with a hydraulic vessel lift and a tilt mechanism.
An Ex-motor with adjustable transmission for speeds of 0-2400 min-1
is used as agitator drive in combination with a bmd 300 magnetic coupling.
The standard scope of delivery includes the following parts:
� Stand with hydraulic vessel lift and tilt mechanism
� Vessel (Type 3 / 4) with suitable stirrer shaft, stirrer, baffle, Pt-100 without plug, bottom valve
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive: Ex-drive with transmission. manually adjustable, 0-2400 min-1,
magnetic coupling «bmd 300»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«kiloclave» Type 3Ex-drive with transmission, adjustable 0-2400 min-1, motor 3x400V/3x220V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, accessories, spare parts and tools, assembled and ready for
operation.
«kiloclave» Type 3 Standard Hastelloy
0.5 Liter 60 bar Floor model 47.30109.0000 47.30109.22001.0 Liter 60 bar Floor model 47.30110.0000 47.30110.22001.5 Liter 60 bar Floor model 47.30111.0000 47.30111.22002.0 Liter 60 bar Floor model 47.30112.0000 47.30112.22003.0 Liter 60 bar Floor model 47.30113.0000 47.30113.22005.0 Liter 40 bar Floor model 47.30114.0000 47.30114.220010.0 Liter 20 bar Floor model 47.30115.0000 47.30115.220020.0 Liter 10 bar Floor model 47.30116.0000 47.30116.2200
51
Autoclave for reactions with steel vessels,stand with vessel lift
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«kiloclave»
52
2
«kiloclave» Type 4Ex-drive with transmission, adjustable 0-2400 min-1, motor 3x400V/3x220V, 50 / 60 Hz, standard cover plate up to max. 60 bar, steel vessel with bottom
valve and 2 sight glasses, welded heating jacket, heatable up to max. 250°C for max. 60 bar, complete with stand, accessories, spare parts and tools,
assembled and ready for operation.
«kiloclave» Type 4 Standard Hastelloy
1.0 Liter 60 bar Floor model 47.30117.0000 47.30117.22001.5 Liter 60 bar Floor model 47.30118.0000 47.30118.22002.0 Liter 60 bar Floor model 47.30119.0000 47.30119.22003.0 Liter 60 bar Floor model 47.30120.0000 47.30120.22005.0 Liter 40 bar Floor model 47.30121.0000 47.30121.220010.0 Liter 20 bar Floor model 47.30122.0000 47.30122.220020.0 Liter 10 bar Floor model 47.30123.0000 47.30123.2200
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«kiloclave»
53
2
100 / 200 bar versionNot available with fast action closure!
Type 3 0.50 L, 200 bar, complete 47.40090.0000 47.40090.2200Type 3 1.00 L, 200 bar, complete 47.40091.0000 47.40091.2200Type 3 1.50 L, 200 bar, complete 47.40092.0000 47.40092.2200Type 3 2.00 L, 200 bar, complete 47.40093.0000 47.40093.2200Type 3 3.00 L, 200 bar, complete 47.40094.0000 47.40094.2200Type 3 5.00 L, 200 bar, complete 47.40095.0000 47.40095.2200Type 3 10.0 L, 100 bar, complete 47.40096.0000 47.40096.2200Type 3 20.0 L, 100 bar, complete 47.40097.0000 47.40097.2200
fast action closurefor vessels Type 3-4, max. 60 bar
Wheels2 swivel casters with brakes
and 2 fixed casters
«cyclone 300»Drive with integrated magnetic coupling
and controller
47.40008.0000 47.40008.2200
47.40009.0000 47.40009.2200
47.40010.0000
Standard Hastelloy
«cyclone 075»Drive with integrated magnetic coupling
and controller
47.40007.0000 47.40007.2200
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
100/200 bar
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoklaven (Metall/Glas)54
2
Electric heatingFor Type 3 and Type 4 vessels, complete with PID controller,
water cooling with solenoid valve, 230V/110V, 50/60Hz
Not ATEX! The surcharge is identical for standard and Hastelloy systems
Type 3E 0.50 L, complete 47.40052.0000Type 3E 1.00 L, complete 47.40053.0000Type 3E 1.50 L, complete 47.40054.0000Type 3E 2.00 L complete 47.40055.0000Type 3E 3.00 L, complete 47.40059.0000Type 3E 5.00 L, complete 47.40060.0000Type 3E 10.0 L, complete 47.40063.0000Type 3E 20.0 L, complete 47.40064.0000
Type 4E 1.00 L, complete 47.40056.0000Type 4E 1.50 L, complete 47.40057.0000Type 4E 2.00 L, complete 47.40058.0000Type 4E 3.00 L, complete 47.40061.0000Type 4E 5.00 L, complete 47.40062.0000Type 4E 10.0 L, complete 47.40065.0000Type 4E 20.0 L, complete 47.40066.0000
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«kiloclave»
55
2
Dimensions
Weight ca. 160 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
1646
1377
738
700
705
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«kiloclave»
56
2
Setup, stainless steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«kiloclave»
57
2
Setup, Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«midiclave»
58
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
The same device can be used with the following vessels:
� Steel vessels Type 3 with bottom valve
� Steel vessels Type 4 with sight glasses and bottom valve
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The standard scope of delivery includes the following parts:
� Stand
� Lift and fast action closure
� Vessel (Type 3 / 4) with suitable stirrer shaft, stirrer, baffle, Pt-100 without plug, bottom valve
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling, incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
«midiclave» Type 3Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 200 bar, steel vessel with bot-
tom valve, welded heating jacket, heatable up to max. 300°C for max. 200 bar, complete with stand, lift, fast action closure, accessories, spare parts and
tools, assembled and ready for operation.
«midiclave» Type 3 Standard Hastelloy0.1 Liter 200 bar Table model 47.30139.0000 47.30143.00000.25 Liter 200 bar Table model 47.30140.0000 47.30144.00000.5 Liter 200 bar Table model 47.30141.0000 47.30145.00001.0 Liter 200 bar Table model 47.30142.0000 47.30146.0000
«midiclave» Type 4Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 200 bar, steel vessel with bot-
tom valve and 2 sight glasses, welded heating jacket, heatable up to max. 300°C for max. 200 bar, complete with stand, lift, fast action closure, accesso-
ries, spare parts and tools, assembled and ready for operation.
«midiclave» Type 4 Standard Hastelloy0.5 Liter 200 bar Table model 47.30147.0000 47.30149.00001.0 Liter 200 bar Table model 47.30148.0000 47.30150.0000
High pressure autoclave with fast action closure
Autoclaves (metal/glass)«midiclave»
59
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Electric heatingFor Type 3 and Type 4 vessels, complete with PID controller,
water cooling with solenoid valve, 230V/110V, 50/60Hz
Not ATEX! The surcharge is identical for standard and Hastelloy systems
Type 3E 0.10 L, complete 47.40087.0000Type 3E 0.25 L, complete 47.40088.0000Type 3E 0.50 L, complete 47.40052.0000Type 3E 1.00 L, complete 47.40053.0000
Type 4E 0.50 L, complete 47.40089.0000Type 4E 1.00 L, complete 47.40056.0000
Ex drive «Ex e II T4»Motor 230/400V, 50 Hz,
with adjustable transmission and bmd 075
(price for ATEX version of bmd is not included)
«cyclone 300»Drive with integrated magnetic coupling
and controller
47.40002.0000 47.40002.2200
47.40086.0000
Standard
TrolleyH=500mm
42.40118.0000
Options (add to base price)
Hastelloy
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«midiclave»
60
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Dimensions
Weight ca. 60 kg
873
454
500
Autoclaves (metal/glass)«midiclave»
61
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Setup, stainless steel
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«midiclave»
62
2
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Setup, Hastelloy
Autoclaves (metal/glass)«limbo»
63
2
The vessel is heated by an electric heating with integrated cooling coil.
The temperature is controlled using a programmable
PID controller (heating / cooling).
The same device can be used with the following vessels:
� Type 3 without bottom valve 100 / 200 / 285 / 450 ml
The cover plate with 5 openings is sealed with a metallic O-ring.
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The standard scope of delivery includes the following parts:
� Electric heating with base
� Programmable PID-controller «btc»
� Vessel Type 3 with suitable stirrer shaft, stirrer and Pt-100 with plug
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling, incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
High pressure autoclave up to max. 350 bar / 350°C,vessels max. 450 ml
«limbo» Type 3Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 350 bar, steel vessel without
bottom valve, heatable up to max. 350°C for max. 350 bar, complete with electric heating and controller «btc», accessories, spare parts and tools, assem-
bled and ready for operation.
«limbo» Type 3 Standard Hastelloy
100 ml 350 bar Table model 47.30124.0000 47.30124.2200200 ml 350 bar Table model 47.30125.0000 47.30125.2200285 ml 350 bar Table model 47.30126.0000 47.30126.2200450 ml 350 bar Table model 47.30127.0000450 ml 150 bar Table model 47.30128.0000450 ml 200 bar Table model 47.30129.0000
Standard Hastelloy
Vessel liftStand with manual vessel lift
47.40011.0000
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«limbo li»
64
2
The vessel is heated by an electric heating with integrated cooling coil.
The temperature is controlled using a programmable
PID controller (heating / cooling).
The same device can be used with the following vessels:
� Type 3 without bottom valve 100 / 200 / 285 / 450 ml
The cover plate with 5 openings is sealed with a metallic O-ring.
The autoclave is equipped with a magnetic drive «cyclone 075»
for stirrer speeds of 100 – 3000 min-1.
The vessel lift facilitates the vessel handling.
The standard scope of delivery includes the following parts:
� Stand with vessel lift and electric heating
� Programmable PID-controller «btc»
� Vessel Type 3 with suitable stirrer shaft, stirrer and Pt-100 with plug
� Cover plate with standard setup:
Swagelok fittings with bursting disc, manometer and 2 valves
� Stirrer drive «cyclone 075» with integrated magnetic coupling, incl. controller «cc075»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
High pressure autoclave up to max. 350 bar / 350°C,vessels max. 450 ml, stand with vessel lift
«limbo li» Type 3Magnetic drive «cyclone 075», adjustable 100-3000 min-1, motor 110 / 230 V, 50 / 60 Hz, standard cover plate up to max. 350 bar, steel vessel without
bottom valve, heatable up to max. 350°C for max. 350 bar, complete with lift, electric heating and controller «btc», accessories, spare parts and tools,
assembled and ready for operation.
«limbo li» Type 3 Standard Hastelloy
100 ml 350 bar Table model 47.30130.0000 47.30130.2200200 ml 350 bar Table model 47.30131.0000 47.30131.2200285 ml 350 bar Table model 47.30132.0000 47.30132.2200450 ml 350 bar Table model 47.30133.0000450 ml 150 bar Table model 47.30134.0000450 ml 200 bar Table model 47.30135.0000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«limbo»
65
2
Dimensions
Weight ca. 23 kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
250
566
551
256
280
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«limbo li»
66
2
Dimensions
Weight ca. 83kg
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
1186
1061
786
601
463
657
400
Autoclaves (metal/glass)«limbo», «limbo li»
67
2
Setup, stainless steel and Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Autoclaves (metal/glass)«limbo ls»
68
2
The vessel is heated by an electric heating with integrated cooling coil.
The temperature is controlled using a programmable
PID controller (heating / cooling).
The same device can be used with the following vessels:
� Type 3 with bottom valve 1.0 / 2.0l
The cover plate with 8 openings is sealed with a metallic O-ring.
An Ex-motor with adjustable transmission for speeds of 0-2400 min-1
is used as agitator drive in combination with a bmd 300 magnetic coupling.
The stand is equipped with a hydraulic vessel lift and a tilt mechanism.
The standard scope of delivery includes the following parts:
� Stand with vessel lift and electric heating
� Programmable PID-controller «btc»
� Vessel Type 3 with suitable stirrer shaft and stirrer
� Cover plate with standard setup:
Sitec-HP fittings with bursting disc, manometer, 2 valves and Pt-100 with plug
� Stirrer drive: Ex-drive with transmission. manually adjustable, 0-2400 min-1,
magnetic coupling «bmd 300»
� Tools and spare parts
� Documentation with operation manual, CE-declaration of conformity and certificates
� Manufactured and tested according to PED, AD2000
High pressure autoclave up to max. 350 bar / 350°C,vessels 1.0 l or 2.0 l, stand with vessel lift
«limbo ls»Ex-drive with transmission, adjustable 0-2400 min-1, motor 3x400V/3x127V, 50 / 60 Hz, standard cover plate up to max. 350 bar, steel vessel with bottom
valve, heatable up to max. 350°C for max. 350 bar, complete with lift, electric heating and controller «btc», accessories, spare parts and tools, assembled
and ready for operation.
«limbo ls» Standard Hastelloy
1.0 l 350 bar Floor model 47.30136.0000 47.30136.22002.0 l 350 bar Floor model 47.30137.0000 47.30137.2200
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Autoclaves (metal/glass)«limbo ls»
69
2
«cyclone 300»Drive with integrated magnetic coupling
and controller
Standard Hastelloy
«cyclone 075»Drive with integrated magnetic coupling
and controller
47.40007.0000 47.40007.2200
47.40008.0000 47.40008.2200
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Drives«cyclone 075»
70
3
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Cyclone 075 with M36 x1.5 thread, for flat seal, controller, cable 55.10002.0000 55.10003.0000 • • • •Cyclone 075 with M36 x1.5 thread, for O-ring, controller, cable 55.10007.0000 55.10008.0000 •Cyclone 075 with NS 29 / 32, controller, cable 55.10004.0000 55.10005.0000Cyclone 075 – upper part with external manget incl. controller 55.10001.0000 • • •Controller cc075 22.08020.0000Analog cable for setpoint, open ends 40.20552.0000Analog cable for setpoint, for bds mc 40.20661.0000Connection cable cc075-cyclone075, 1m 55.10020.0000Connection cable cc075-cyclone075, 3m 55.10018.0000
For spare parts see magnetic coupling bmd 075
Standard Hastelloy
The «cyclone075» consists of an electric motor with integrated magnetic
coupling «bmd075» and «cc075» controller. The drive is connected
to the cover plate ith a M36 x 1,5 thread. The controller is connected
to the drive with a cable.
Electrial connection: 110 / 230 VAC
50 / 60Hz
The standard scope of delivery includes the following parts:
� Drive with magnetic coupling
� Controller
� Connection cable
� Power cable
� Spare parts and tools
� Operation manual
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Drives«cyclone 300»
71
3
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Cyclone 300 with M36 x 1,5 thread, for flat seal, controller, cable 55.30000.0000 55.30001.0000 • • • •Cyclone 300 with M36 x 1,5 thread, for O-ring, controller, cable 55.30002.0000 55.30003.0000 •Cyclone 300 upper part with external magnet 55.30016.0000 •Controller cc300-2 22.08041.0000Analog cable for setpoint, open ends 40.20552.0000
Options (add to base price)
cc300-2 with analog speed in/out (4…20 mA) 47.40012.0000cc300-2 with analog speed in/TQ out (4…20 mA) 47.40013.0000
Standard Hastelloy
The «cyclone 300» consists of an electric motor with integrated magnetic
coupling «bmd 300» and controller «cc300-2». The drive is connected to
the cover plate with a M36 x 1,5 thread and is secured against twisting by
a bolt. The controller is connected to the drive with two cables.
Electrial connection: 110 / 230 VAC
50 / 60Hz
The standard scope of delivery includes the following parts:
� Drive with magnetic coupling
� Controller
� Connection cable
� Power cable
� Spare parts and tools
� Operation manual
� Serial interface cable RS-232
For spare parts see magnetic coupling bmd 300
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Drives«cyclone i»
72
3
inertclave
The unique design of the cyclone «i» is based on a magnetic coupling.
The main difference from a traditional magnetic coupling is that the driving
magnet is rotating inside the stationary glass tube and the paddle stirrer
has the magnets on the outside. All wetted parts are made of glass,
PTFE or PFA.
The cyclone «i» is for applications where highest corrosion resistance,
leak-tightness and effective mixing are required.
Electrial connection: 110 / 230 VAC
50 / 60Hz
The standard scope of delivery includes the following parts:
� Drive with magnet inside glass tube
� Adapter NS29/32
� 1 stirrer
� AC adapter with cable
� Operation manual
cyclone «i» complete with PFA stirrer 78 mm,glass adapter and AC adapter 55.30022.0000 •cyclone «i» complete with PFA stirrer 68 mm,glass adapter and AC adapter 55.30019.0000 •
Stirrer, PFA 78 mm 46.10129.0000 •Stirrer, PFA 68 mm 46.10131.0000 •
Glass adapter NS29/32 46.10130.0000 •
GL32 screw cap 40.02413.0000 •
Sheath gasket, silicone / PTFE 40.02414.0000 •
Standard Hastelloy
The cyclone i can also be used for non-pressurized reactions with laboratory glass vessels with NS 29/32 nozzles.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
DrivesEx-Drive
73
3
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Ex-drive with motor 3x400V / 50 Hz 42.10197.0000 • • •42.10009.0000 • •
Ex-drive with motor 3x220V / 60 Hz 42.10198.0000 • • •42.10062.0000 • •
Standard Hastelloy
Motor pressure encapsulated EEx d IIC T4 47.40015.0000
Standard Hastelloy
Stirrer drive for applications in Ex-areas.
The standard scope of delivery includes the following parts:
� Motor 3-phase, 3x 400V / 0,22 kW / EEx e ll T4
� adjustable transmission 0 to 2400 Rpm
� Ex-switch
� Motor support with support bolt, drive support arm, toothed belt wheels,
toothed belt and belt cover
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Motor 3x400V 50Hz EEx e II T4, 0,22kW, 2820 Rpm 42.10031.0000 • • • • •Motor 3x220V 60Hz EEx e II T4, 0,22kW, 3380 Rpm 42.10015.0000 • • • • •Motor 3x400V 50Hz EEx e II T4, 0,35kW, 2810 Rpm 42.10082.0000 • • • • •Motor 3x400V 50Hz EEx d IIC T4, 0,25kW, 2730 Rpm 42.10036.0000 • • • • •Motor 3x400V 50Hz EEx d IIC T4, 0,37kW, 2800 Rpm 42.10037.0000 • • • • •
Speed transmission 0-1200 Rpm, MR3 (BG63) 42.10079.0000 • • • • •Speed transmission 0-1200 Rpm, MR3 (BG71) 42.10083.0000 • • • • •
Switch EEx de IIC T6, 3-pole, 400V, 10A 42.10078.0000 • • • • •
Toothed belt wheel HDT 24-5M-12 42.10021.0000 • • • • •Toothed belt wheel HDT 49-5M-12 42.10022.0000 • • • • •
Toothed belt HTD 665-5M-12 conductive 42.10020.0000 • •Toothed belt HTD 800-5M-12 conductive 42.10088.0000 • • •
0.5 liter transmission oil Santotrac 42.10103.0000 • • • • •
DrivesEx-Drive
74
Standard Hastelloy miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
3
Spare parts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Bmd 075 with M36 x 1,5 42.55001.0000 42.55001.2200 • • • • •
Bmd 075 with NS 29 / 32 42.55002.0000 42.55002.2200
Magnetic couplings«bmd 075»
75
StandardMagnetic couplings Hastelloy miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
4
The magnetic coupling is available withM 36x1,5 thread or NS29/32 ground joint.
Operating conditions: max. speed 3000 rpm
max. temperature 250 °C
max. pressure 100 bar
Torque 75 Ncm
The standard scope of delivery includes the following parts:
� Magnetic coupling
� flexible shaft coupling
� Spare parts and tools
� Operation manual
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Magnetic couplings«bmd 075»
76
4
Internal magnet encased 42.55016.0000 42.55015.2200 • • • • • • •Internal magnet encased 60.10139.0000 60.10145.0000 •Setscrew M6 46.10084.0000 46.10086.2200 • • • • • • • •
Closing cap for flat seal M 36x1.5 42.55019.0000 42.55021.2200 • • • •Closing cap for O-ring M 36x1.5 42.55090.0000 42.55091.0000 •
Closing cap NS 29 / 32 42.55022.0000 42.55024.2200
Magnetic coupling upper part with external magnet 42.55035.0000 • • • • • • • •
Slide bearing upper 14x16 mm PTFE/Graphite 42.55003.0000 • • • • • • • •Slide bearing upper 14x16 mm PTFE 42.55004.0000 • • • • • • • •Slide bearing upper 14x16 mm PEEK 42.55005.0000 • • • • • • • •
Slide bearing lower 20.4x16x17mm PTFE/Graphite 42.55006.0000 • • • • • • •Slide bearing lower 20.4x16x17mm PTFE 42.55007.0000 • • • • • • •Slide bearing lower 20.4x16x17mm PEEK 42.55008.0000 • • • • • • •
Slide bearing lower Metal/Graphite 60.10136.0000 60.10156.0000 •
Ball bearing upper 6/15x5 mm 1.3505 40.02286.0000 • • • • • • •Ball bearing lower 15/24x7 mm 1.3505 40.02285.0000 • • • • • • •
Annular spring 42.55013.0000 42.55014.2200 • • • • • • •
Standard Hastelloy miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
Spare parts / Tools
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Magnetic couplings«bmd 075»
77
4
Assembling pin 11x120 mm 42.55027.0000 • • • • •
Fork for slide bearing dismantling 42.55028.0000 • • • • • • • •
Glycerin 25ml 42.20099.0000 • • • • • • • •
Standard Hastelloy miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
Miniflex coupling LM 8x9 mm 42.10052.0000 • • • • • • • •
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Magnetic couplings«bmd 075»
78
4
Shaft M36x1,5, for hall switch Ex-i 47.40016.0000 47.40016.2200 • • • • • • • •
Magnetic couplingwith ball bearings steel 1.3505 47.40017.0000 • • • • • • •
Magnetic coupling with ATEX-certificate 47.40018.0000 47.40018.2200 • • • • • • • •
Standard Hastelloy miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Magnetic couplings«bmd 300 / 800 / 1200»
79
4
bmd 300 43.20000.0000 43.20004.0000 • • • •bmd 800 43.30000.0000 43.30002.0000 • • • •bmd 1200 43.31000.0000 43.31001.0000 • • • •
StandardMagnetic couplings Hastelloy ecoclave
polyclave
versoclave
kiloclave
midiclave
The magnetic coupling is installed with a M 36x1,5 threadon the cover plate and is sealed with a Flex-O-Formflat gasket.
Operating conditions: max. speed 2000 rpm
max. temperature 250 °C
max. pressure 150 bar
Torque 300 – 1200 Ncm
The standard scope of delivery includes the following parts:
� Magnetic coupling
� Spare parts and tools
� Operation manual
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Magnetic couplings«bmd 300 / 800 / 1200»
80
4
Internal magnet encased bmd 300 43.20102.0000 43.20110.0000 • • • • • •Internal magnet encased bmd 800 43.30102.0000 43.30107.0000 • • • •Internal magnet encased bmd 1200 43.31101.0000 43.31102.0000 • • • •
Coupling upper part bmd 300 with external magnet 43.20105.0000 • • • • •Coupling upper part bmd 800 with external magnet 43.30105.0000 • • • •Coupling upper part bmd 1200 with external magnet 43.31002.0000 • • • •
Closing cap bmd 300 40.01287.0000 40.01585.0000 • • • • •Closing cap bmd 800 40.01439.0000 • • • • •Closing cap bmd 1200 43.31009.0000 • • • • •
Slide bearing upper with collarbmd 300-1200 PTFE/Graphite 42.20014.0000 • • • • • •Slide bearing upper with collar bmd 300 - 1200 PTFE 42.20021.0000 • • • • • •Slide bearing upper with collar bmd 300 - 1200 PEEK 42.20086.0000 • • • • • •Slide bearing upper with collarbmd 300 - 1200 electro graphite 42.20116.0000 • • • • • •
Slide bearing middle with collarbmd 300 - 1200 PTFE/Graphite 42.80002.0000 • • • • • •Slide bearing middle with collar bmd 300 - 1200 PTFE 42.80025.0000 • • • • • •Slide bearing middle with collar bmd 300 - 1200 PEEK 42.80030.0000 • • • • • •Slide bearing middle with collarbmd 300 - 1200 electro graphite 42.20118.0000 • • • • • •
Slide bearing lower without collar bmd 300 - 1200PTFE/Graphite 42.80001.0000 • • • • •Slide bearing lower without collar bmd 300 - 1200 PTFE 42.80024.0000 • • • • •Slide bearing lower without collar bmd 300 - 1200 PEEK 42.80029.0000 • • • • •Slide bearing lower without collarbmd 300 - 1200 electro graphite 42.20119.0000 • • • • •
Slide bearing lower Metal / Graphite 60.10027.0000 60.10028.0000 •
Ball bearing 28/12x8 mm Ceramic Si 3N4 40.02230.0000 • • • • •
Shaft for bmd 300–1200 M36 x 1.5 43.20101.0000 43.20111.0000 • • • •
Standard Hastelloy ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
ls
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
ls
Spare parts / Tools
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Magnetic couplings«bmd 300 / 800 / 1200»
81
4
Assembling pin for upper bearing13 x 240 mm anti magnetic 42.20102.0000 • • • • • •
Assembling pin for middle and lower bearing20 x 120 mm anti magnetic 42.20101.0000 • • • • • •
Fork wrench SW 36 42.20123.0000 • • • • •
Pin wrench 42.20124.0000 • • • • • •
Glycerin 25ml 42.20099.0000 • • • • • •
Standard Hastelloy ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
ls
Locking ring Ø 16 mm 42.80026.0000 42.80028.2200 • • • •
Distance bushing 19.5 x 12.2 x 16 mm 40.01282.0000 40.01335.0000 • • • • • •
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Magnetic couplings«bmd 300 / 800 / 1200»
82
4
Shaft for bmd 300 - 1200 M36x1,5, with O-Ring 47.40019.0000 47.40019.2200 • • • • •Shaft for bmd 300 - 1200 M36x1,5, for hall switch Ex-i 47.40020.0000 47.40020.2200 • • • • • •Shaft for bmd 300 - 1200 M36x1,5, gassing nipple 47.40021.0000 47.40021.2200 • • • • • •Shaft Shaft for bmd 300 - 1200 M36x1,5,with cooling jacket 47.40022.0000 47.40022.2200 • • • • • •
Magnetic couplingWith ceramic ball bearings 47.40023.0000 47.40023.2200 • • • • •
Magnetic coupling with ATEX-certificate(only bmd 300 / 800) 47.40024.0000 47.40024.2200 • • • • • •
Standard Hastelloy ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
ls
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Magnetic couplings«bmd 1800 / 3600»
83
4
bmd 1800 44.70030.0000 44.71032.0000bmd 3600 44.80030.0000 44.81032.0000
StandardMagnetic coupling Hastelloy
The magnetic coupling is installed with a Ø 140 mm flangeon the cover plate and is sealed with a flat gasket.Including pulse generator for speed measuring.
Operating conditions: max. speed 1200 Rpm
max. temperature -20 bis + 250°C
max. pressure 50 bar
max. torque 1800 – 3600 Ncm
The standard scope of delivery includes the following parts:
� Magnetic coupling
� Operation manual
� ATEX certificate
Cylinder roller bearing CeramicØ 55 x 30 x 13 mm (lower) 44.00000.0003Grooved ball bearing CeramicØ 55 x 30 x 13 mm (upper) 44.00000.0004
StandardSpare parts Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
110 mm • • 52.50107.0000 52.50109.0000110 mm for gassing • • 52.50113.0000 52.50111.0000170 mm • • 52.50106.0000 52.50108.0000170 mm for gassing • • 52.50112.0000 52.50110.0000190 mm • 52.50161.0000 52.50164.0000190 mm for gassing • 52.50167.0000 52.50166.0000220 mm • • 52.50173.0000 52.50177.0000220 mm for gassing • • 52.50176.0000 52.50178.0000
Mixing elementsStirrer shafts for «miniclave drive», «picoclave»
84
StandardLength HastelloyType
1100ml
200ml
250ml
300ml
Type
3100ml
200ml
300ml
5
bmd 075 / cyclone 075Ø 8mm with and without fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Mixing elementsStirrer shafts for «ecoclave», «polyclave», «versoclave», «kiloclave»
85
5
124 mm • 42.55040.0000 42.55041.0000146 mm • 42.55053.0000 42.55054.0000146 mm for gassing • 42.55055.0000 42.55056.0000194 mm • • • • • • • • • 42.55025.0000 42.55036.0000194 mm for gassing • • • • • • • • • 42.55057.0000 42.55058.0000264 mm • 42.55042.0000 42.55043.0000264 mm for gassing • 42.55051.0000 42.55063.0000294 mm • • • 42.55026.0000 42.55037.0000294 mm for gassing • • • 42.55050.0000 42.55064.0000339 mm • 42.55044.0000 42.55045.0000339 mm for gassing • 42.55059.0000 42.55060.0000359 mm • • 42.55038.0000 42.55039.0000359 mm for gassing • • 52.55061.0000 42.55062.0000
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
180 mm • 43.40227.0000 43.40228.0000200 mm • 43.40229.0000 43.40230.0000200 mm for gassing • 43.40231.0000 43.40232.0000250 mm • • • • • • • • • 43.40111.0000 43.40211.0000250 mm for gassing • • • • • • • • • 43.40233.0000 43.40234.0000320 mm • 43.40114.0000 43.40214.0000320 mm for gassing • 43.40235.0000 43.40236.0000350 mm • • • 43.40237.0000 43.40238.0000350 mm for gassing • • • 43.40239.0000 43.40240.0000390 mm • 43.40116.0000 43.40216.0000390 mm for gassing • 43.40241.0000 43.40242.0000415 mm • • 43.40243.0000 43.40244.0000415 mm for gassing • • 43.40245.0000 43.40246.0000
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
bmd 075 / cyclone 075Ø 10mm without fast action closure
bmd 075 / cyclone 075Ø 10mm with fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Mixing elementsStirrer shafts for «ecoclave», «polyclave», «versoclave», «kiloclave»
86
5
185 mm • 42.90134.0000 42.90135.0000185 mm for gassing • 42.90136.0000 42.90137.0000207 mm • 42.90106.0000 42.90107.0000207 mm for gassing • 42.90114.0000 42.90115.0000255 mm • • • • • • • • • 42.90108.0000 42.90109.0000255 mm for gassing • • • • • • • • • 42.90116.0000 42.90117.0000325 mm • 42.90110.0000 42.90111.0000325 mm for gassing • 42.90118.0000 42.90119.0000355 mm • • • 42.90112.0000 42.90113.0000355 mm for gassing • • • 42.90120.0000 42.90121.0000400 mm • 42.90092.0000 42.90093.2200400 mm for gassing • 42.90088.0000 42.90089.2200
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
5.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
bmd 300 / 800 / 1200 / cyclone 300Ø 16/10mm without fast action closure
240 mm • 42.90150.0000 42.90163.0000240 mm for gassing • 42.90178.0000 42.90179.0000262 mm • 42.90154.0000 42.90167.0000262 mm for gassing • 42.90180.0000 42.90181.0000310 mm • • • • • • • • • 42.90157.0000 42.90161.0000310 mm for gassing • • • • • • • • • 42.90182.0000 42.90183.0000380 mm • 42.90151.0000 42.90164.0000380 mm for gassing • 42.90170.0000 42.90184.0000410 mm • • • 42.90149.0000 42.90162.0000410 mm for gassing • • • 42.90185.0000 42.90186.0000455 mm • 42.90152.0000 42.90165.0000455 mm for gassing • 42.90187.0000 42.90188.0000
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
bmd 300 / 800 / 1200 / cyclone 300Ø 16/10mm with fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Mixing elementsStirrer shafts for «ecoclave», «polyclave», «versoclave», «kiloclave»
87
5
207 mm • 42.90102.0000 42.90103.0000207 mm for gassing • 42.90104.0000 42.90105.0000255 mm • • • • • • • • • 42.90002.0000 42.90030.2200255 mm for gassing • • • • • • • • • 42.90001.0000 42.90034.2200325 mm • 42.90098.0000 42.90099.2200325 mm for gassing • 42.90100.0000 42.90101.2200355 mm • • • 42.90004.0000 42.90038.2200355 mm for gassing • • • 42.90003.0000 42.90042.2200400 mm • 42.90006.0000 42.90065.2200400 mm for gassing • 42.90005.0000 42.90067.2200422 mm • • 42.90094.0000 42.90095.2200422 mm for gassing • • 42.90096.0000 42.90097.2200442 mm • 42.90174.0000 42.90177.0000442 mm for gassing • 42.90175.0000 42.90176.0000570 mm • 42.90086.0000 42.90087.2200570 mm for gassing • 42.90090.0000 42.90091.2200
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
5.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
bmd 300 / 800 / 1200 / cyclone 300Ø 16mm without fast action closure
262 mm • 42.90189.0000 42.90190.0000262 mm for gassing • 42.90191.0000 42.90192.0000310 mm • • • • • • • • • 42.90193.0000 42.90194.0000310 mm for gassing • • • • • • • • • 42.90195.0000 42.90196.0000380 mm • 42.90197.0000 42.90198.0000380 mm for gassing • 42.90199.0000 42.90200.0000410 mm • • • 42.90201.0000 42.90202.0000410 mm for gassing • • • 42.90203.0000 42.90204.0000455 mm • 42.90205.0000 42.90206.0000455 mm for gassing • 42.90207.0000 42.90208.0000475 mm • • 42.90209.0000 42.90210.0000475 mm for gassing • • 42.90211.0000 42.90212.0000500 mm • 42.90218.0000 42.90219.0000500 mm for gassing • 42.90220.0000 42.90221.0000625 mm • 42.90213.0000 42.90214.0000625 mm for gassing • 42.90215.0000 42.90216.0000
StandardLength HastelloyType
10.25
0.50
1.00
1.60
2.00
Type
20.50
1.00
1.50
2.00
3.00
5.00
Type
3/4
0.50
1.00
1.50
2.00
3.00
5.00
10.00
20.00
bmd 300 / 800 / 1200 / cyclone 300Ø 16mm with fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Mixing elementsStirrer shafts for «midiclave»
88
5
105 mm • 52.50240.0000 52.50241.0000105 mm for gassing • 52.50242.0000 52.50243.0000145 mm • 52.50246.0000 52.50247.0000145 mm for gassing • 52.50244.0000 52.50245.0000170 mm • 52.50106.0000 52.50108.0000170 mm for gassing • 52.50112.0000 52.50110.0000220 mm • 52.50173.0000 52.50177.0000220 mm for gassing • 52.50176.0000 52.50178.0000
Lenght
Type
3/4
0.10
0.25
0.50
1.00
bmd 075 / cyclone 075Ø 8mm with fast action closure
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Mixing elementsStirrer shafts for «limbo», «limbo li»
89
5
135 mm • 52.50162.0000 52.50165.0000135 mm for gassing • 52.50169.0000 52.50168.0000157 mm • 52.50160.0000 52.50163.0000157 mm for gassing • 52.50170.0000 52.50171.0000190 mm • • 52.50161.0000 52.50164.0000190 mm for gassing • • 52.50167.0000 52.50166.0000
StandardLength HastelloyType
3100ml
200ml
285ml
450ml
bmd 075 / cyclone 075Ø 8mm without fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Mixing elementsStirrers
90
5
Impeller Ø 32 mm 46.10099.0000 46.10098.0000 • • • •
Propeller Ø 32 mm 46.10100.0000 46.10101.0000 • • • •
Anchor Ø 42 x 40 mm 46.10111.0000 46.10112.0000 • • • •
Turbine Ø 35 mm 46.10102.0000 46.10103.0000 • • • •
Set screw M3 46.10109.0000 46.10055.2200 • • • •
StandardType Dimension Hastelloy
8 mm stirrer shafts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Mixing elementsStirrers
91
5
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Blade stirrer Ø 50 x 14 mm 46.10004.0000 46.10041.2200 • • • • •Blade stirrer Ø 50 x 37 mm 46.10005.0000 46.10042.2200 • • • • •Blade stirrer Ø 80 x 17 mm 46.10006.0000 46.10043.2200 • • • • •Blade stirrer Ø 76 x 57 mm 46.10007.0000 46.10044.2200 • • • • •
Impeller Ø 40 mm 46.10001.0000 46.10045.2200 • • • • •Impeller Ø 60 mm 46.10002.0000 46.10046.2200 • • • • •Impeller Ø 94 mm 46.10003.0000 46.10047.2200 • • • • •
Propeller Ø 35 mm 46.10008.0000 46.10048.2200 • • • • •Propeller Ø 50 mm 46.10009.0000 46.10049.2200 • • • • •
Anchor Ø 75 x 80 mm 46.10010.0000 46.10050.2200 • • • • •Anchor Ø 91 x 90 mm 46.10011.0000 46.10051.2200 • • • • •
Turbine Ø 45 x 10 mm 46.10012.0000 46.10052.2200 • • • • •Turbine Ø 60 x 10 mm 46.10104.0000 46.10105.0000 • • • • •
Helicoil Ø 76 x 72 mm 46.10020.0000 46.10053.2200 • • • • •
Set screw M3 46.10109.0000 46.10055.2200 • • • • •
StandardType Dimension Hastelloy
10 mm stirrer shafts
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Mixing elementsStirrers
92
5
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Blade stirrer Ø 50 x 57 46.10093.0000 46.10095.2200 • • • •Blade stirrer Ø 80 x 57 mm 46.10065.0000 46.10081.2200 • • • •Blade stirrer Ø 80 x 17 mm 46.10066.0000 • • • •
Impeller Ø 60 mm 46.10062.0000 46.10078.2200 • • • •Impeller Ø 94 mm 46.10063.0000 46.10079.2200 • • • •
Propeller Ø 60 mm 46.10064.0000 46.10080.2200 • • • •Propeller Ø 80 mm 46.10088.0000 46.10097.0000 • • • •
Anchor Ø 75 x 75 46.10060.0000 46.10076.2200 • • • •Anchor Ø 91 x 90 46.10061.0000 46.10077.2200 • • • •
Turbine Ø 60 mm 46.10067.0000 46.10083.2200 • • • •
Helicoil Ø 76 x 72 mm 46.10132.0000 46.10132.2200 • • • •
Set screw M6 46.10084.0000 46.10086.2200 • • • •
StandardType Dimension Hastelloy
16 mm stirrer shafts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Mixing elementsBaffles
93
5
Blade 35 x 27 46.10013.0000 46.10058.2200 • • • • • •Blade 55 x 40 46.10014.0000 46.10059.2200 • • • • •
Blade for helicoil stirrer 80 x 28(only for helicoil with 10mm stirrer shaft) 46.10021.0000 46.10054.2200 • • • • •
Baffle rod with check nut 110 mm 46.10018.0000 46.10090.2200 • • • • • •Baffle rod with check nut 150 mm 46.10123.0000 46.10127.0000 • • • • • •Baffle rod with check nut 165 mm 46.10015.0000 46.10056.2200 • • • • • •Baffle rod with check nut 205 mm 46.10113.0000 46.10125.0000 • • • • •Baffle rod with check nut 265 mm 46.10016.0000 46.10057.2200 • • • • •Baffle rod with check nut 305 mm 46.10122.0000 46.10126.0000 • • • •Baffle rod with check nut 410 mm 46.10124.0000 46.10128.0000 • • •
Set screw M3 46.10109.0000 46.10055.2200 • • • • •
StandardType Dimension Hastelloy ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
ls
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Glass vessel 10 ml 10 bar / 150°C 51.10101.0000 •Glass vessel 25 ml 10 bar / 150°C 51.10102.0000 •
Holder for glass vessel 10 / 25ml, 1.4301 51.10105.0000
PTFE insert ring for glass vessel 51.10104.0000
Vessels«tinyclave steel»
94
Standard Hastelloy
tinyclave
steel
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
6
Type 1Glass stirrer vessel for max. 10 bar / 150°C
Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Glass vessel 100 ml 10 bar / 200°C 52.10104.0000 • •Glass vessel 200 ml 10 bar / 200°C 52.10130.0000 • •Glass vessel 250 ml 10 bar / 200°C 52.10149.0000 • •Glass vessel 300 ml 10 bar / 200°C 52.10150.0000 • •
Holder for glass vessel 100ml, 1.4301 52.10105.0000Holder for glass vessel 200ml, 1.4301 52.10123.0000Holder for glass vessel 250ml, 1.4301 52.10151.0000Holder for glass vessel 300ml, 1.4301 52.10152.0000
PTFE insert ring for glass vessels 52.10108.0000
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
95
Standard Hastelloy
miniclave
miniclave
steel
miniclave
drive
picoclave
6
Type 1Vessel for screw closure, without jacket, without bottom opening� max. 10 (6) bar / 200°C
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
96
6
Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Glass vessel 100 ml 10 bar / 200°C 52.50210.0000 •Glass vessel 200 ml 10 bar / 200°C 52.50211.0000 •Glass vessel 250 ml 10 bar / 200°C 52.50212.0000 •Glass vessel 300 ml 10 bar / 200°C 52.50213.0000 •
Glass vessel 100 ml 6 bar / 200°C 52.50224.0000 •Glass vessel 200 ml 6 bar / 200°C 52.50225.0000 •Glass vessel 250 ml 6 bar / 200°C 52.50226.0000 •Glass vessel 300 ml 6 bar / 200°C 52.50227.0000 •
PTFE insert ring 2-piece, for glass vessels 52.50219.0000
For heating jacket connections see chapter 10.
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
97
Standard Hastelloy
Standard Hastelloy
miniclave
miniclave
steel
miniclave
drive
picoclave
6
miniclave
miniclave
steel
miniclave
drive
picoclave
Type 1BVessel for fast action closure, with jacket and adapteron M16x1, with Torion bottom valve� max. 6 bar / 200°C
Type 1Vessel for fast action closure, with jacket and adapteron M16x1, without bottom opening� max. 10 bar / 200°C
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
98
6
Type 1Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
99
6
Type 1BDimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Steel stirrer vessel 100 ml 60 bar / 250°C 52.50190.0000 52.50192.0000 • •Steel stirrer vessel 200 ml 60 bar / 250°C 52.50191.0000 52.50193.0000 • •Steel stirrer vessel 300 ml 60 bar / 250°C 52.50234.0000 52.50235.0000 • •
Vessels«miniclave», «miniclave steel», «miniclave drive», «picoclave»
100
6
Standard Hastelloy miniclave
miniclave
steel
miniclave
drive
picoclave
Type 3Steel stirrer vessel for fast action closure, with welded jacket,for max. 60 bar / 250°C, with bottom opening 3/8" Gi, incl. plug.Heating connections M16 x 1
Typ 3 for fast action closureDimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Glass stirrer vessel Type 1 0.25 L, 6 bar 45.10017.0000 • •Glass stirrer vessel Type 1 0.50 L, 6 bar 45.10018.0000 • • •Glass stirrer vessel Type 1 1.00 L, 6 bar 45.10019.0000. • • •Glass stirrer vessel Type 1 1.60 L, 6 bar 45.10020.0000 • •Glass stirrer vessel Type 1 2.00 L, 6 bar 45.10021.0000 •
Adapter flange for fast action closure,complete with screws and seal 40.02771.0000 40.02771.2200 •
Adapter for vessel lift, complete with screws 40.02305.0000 •
Spare partsPressure vessel Type 1 0.25 L, 6 bar 45.10002.0000Pressure vessel Type 1 0.50 L, 6 bar 45.10004.0000Pressure vessel Type 1 1.00 L, 6 bar 45.10005.0000Pressure vessel Type 1 1.60 L, 6 bar 45.10007.0000Pressure vessel Type 1 2.00 L, 6 bar 45.10008.0000
Heating jacket Type 1 for 0.25 / 0.50 / 1.0 L 45.10001.0000Heating jacket Type 1 for 1.60 L 45.10009.0000Heating jacket Type 1 for 2.00 L 45.10010.0000
Ring flange for Type 1 45.10003.0000Stud bolt M10 x 60 45.20001.0000Nut M10 / A4 45.20032.0000Washer M 10 / A4 45.20033.0000Clamp clip for heating jacket Type 1 45.10011.0000Screw M6 x 25 / A4 09.02274.0000Clamping ring Viton 46.80003.0000Silicone insert 40.00222.0000
For heating jacket connections see chapter 10.
For collar packing see chapter 11.
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
101
Standard
Options (add to base price)
Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
inertclave
ecoclave
polyclave
versoclave
kiloclave
Type 1Glass stirrer vessel without bottom opening, for max. 6 bar in the laboratory,and max. 12 bar in the autoclave room, heatable up to max. 200°C,consisting of:Pressure vessel, wall 9 mm, graduated
� Heating jacket with plane joint NW 15, incl. adapters PS15 on M16x1
� Flange with stud bolts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
102
6
Pressure vessel
Clamping ring
Nut
Washer
Stud bolt
Flange
Clamp clip
Silicone insert
Screw
Collar packing
Heating jacket
Heating jacket connection
Type 1Assembly
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
103
6
Type 1Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Glass stirrer vessel Type 1B 0.25 L / 6 bar 45.10025.0000 • •Glass stirrer vessel Type 1B 0.50 L / 6 bar 45.10026.0000 • • •Glass stirrer vessel Type 1B 1.00 L / 6 bar 45.10027.0000 • • •Glass stirrer vessel Type 1B 1.60 L / 6 bar 45.10028.0000 • •Glass stirrer vessel Type 1B 2.00 L / 6 bar 45.10029.0000 •
Spare partsGlass vessel Type 1B 0.25 L / 6 bar 45.10030.0000Glass vessel Type 1B 0.50 L / 6 bar 45.10031.0000Glass vessel Type 1B 1.00 L / 6 bar 45.10032.0000Glass vessel Type 1B 1.60 L / 6 bar 45.10033.0000Glass vessel Type 1B 2.00 L / 6 bar 45.10034.0000
Ring flange parted with stud bolts and nuts 45.10023.0000Stud bolt M10 x 60 45.20001.0000Nut M10 / A4 45.20032.0000Washer M 10 / A4 45.20033.0000Clamping ring 140/100x2mm, Viton 46.80003.0000Clamping ring, silicone 46.80001.0000
For heating jacket connections see chapter 10.
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
104
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
inertclave
ecoclave
polyclave
versoclave
kiloclave
Adapter flange for fast action closure,complete with screws and seal 40.02771.0000 40.02771.2200 •
Adapter for vessel lift, complete with screws 40.02306.0000 •
Options (add to base price)
Type 1BGlass stirrer vessel with bottom opening, for max. 6 bar in the laboratoryand in the autoclave room, heatable up to max. 200°C, consisting of:� Pressure vessel, wall 9 mm, with melted-on heating jacket, graduated, jacket connections
with plane joint NW 15, incl. adapters PS15 on M16x1
� Ring flange parted with stud bolts
� Torion bottom valve complete, PTFE / 15% glass
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Nut
Seal
Torion valvecomplete
Nut
Spindle
Washer
Stud bolt
Glass vessel
Flange
Heating jacket connection
Clamping ring Viton
Clamping ring Silicone
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
105
6
Type 1BAssembly
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
106
6
Type 1BDimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Glass stirrer vessel Type 1BI 0.50 L / 6 bar 45.10065.0000 • • •Glass stirrer vessel Type 1BI 1.00 L / 6 bar 45.10066.0000 • • •Glass stirrer vessel Type 1BI 1.60 L / 6 bar 45.10067.0000 • •Glass stirrer vessel Type 1BI 2.00 L / 6 bar 45.10089.0000 •
Spare partsGlass vessel Type 1BI 0.50 L / 6 bar 45.10071.0000Glass vessel Type 1BI 1.00 L / 6 bar 45.10072.0000Glass vessel Type 1BI 1.60 L / 6 bar 45.10082.0000Glass vessel Type 1BI 2.00 L / 6 bar 45.10090.0000
Ring flange parted with stud bolts and nuts 45.10023.0000Stud bolt M10 x 60 45.20001.0000Nut M10 / A4 45.20032.0000Washer M 10 / A4 45.20033.0000Clamping ring 140/100x2mm, Viton 46.80003.0000Clamping ring, silicone 46.80001.0000
For heating jacket connections see chapter 10.
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
107
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
inertclave
ecoclave
polyclave
versoclave
kiloclave
Adapter flange for fast action closure,complete with screws and seal 40.02771.0000 40.02771.2200 •
Adapter for vessel lift, complete with screws 40.02306.0000 •
Options (add to base price)
Type 1BIGlass stirrer vessel with evacuated jacket and with bottom valve,for max. 6 bar in the laboratory and in the autoclave room,heatable up to max. 200°C, consisting of:
� Pressure vessel, wall 9 mm, with melted-on heating jacket and evacuated insulation jacket, graduated.
� Jacket connections with plane joint NW 15, incl. adapters PS15 on M16x1
� Ring flange parted with stud bolts
� Torion bottom valve complete, PTFE / 15% glass
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
108
6
Nut
Seal
Torion valvecomplete
Nut
Spindle
Washer
Stud bolt
Glass vessel
Flange
Heating jacket connection
Clamping ring Viton
Clamping ring Silicone
Type 1BIAssembly
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
109
6
Type 1BIDimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
6
Glass stirrer vessel Type 1I 0.50 L / 6 bar 45.10061.0000 • • •Glass stirrer vessel Type 1I 1.00 L / 6 bar 45.10062.0000 • • •Glass stirrer vessel Type 1I 1.60 L / 6 bar 45.10063.0000 • •Glass stirrer vessel Type 1I 2.00 L / 6 bar 45.10088.0000 •
Spare partsGlass vessel Type 1I 0.50 L / 6 bar 45.10084.0000Glass vessel Type 1I 1.00 L / 6 bar 45.10069.0000Glass vessel Type 1I 1.60 L / 6 bar 45.10083.0000Glass vessel Type 1I 2.00 L / 6 bar 45.10087.0000
Ring flange parted with stud bolts and nuts 45.10023.0000Stud bolt M10 x 60 45.20001.0000Nut M10 / A4 45.20032.0000Washer M 10 / A4 45.20033.0000Clamping ring 140/100x2mm, Viton 46.80003.0000Clamping ring, silicone 46.80001.0000
For heating jacket connections see chapter 10.
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
110
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
inertclave
ecoclave
polyclave
versoclave
kiloclave
Adapter flange for fast action closure,complete with screws and seal 40.02771.0000 40.02771.2200 •
Adapter for vessel lift, complete with screws 40.02306.0000 •
Options (add to base price)
Type 1IGlass stirrer vessel with evacuated jacket, without bottom valve, for max. 6 barin the laboratory, max. 12 bar in the autoclave room, heatable up to max. 200°C, consisting of:� Pressure vessel, wall 9 mm, with melted-on heating jacket and evacuated insulation jacket, graduated.
� Jacket connections with plane joint NW 15, incl. adapters PS15 on M16x1
� Ring flange parted with stud bolts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
6
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
111
6
Nut
Heating jacket connection
Washer
Stud bolt
Glass vessel
Flange
Clamping ring Viton
Clamping ring silicone
Type 1IAssembly
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
112
6
Type 1IDimensions
0.5 lt.
195
229c
a.
ø175
ø72
1.0 lt.
279c
a.
195ø82
ø175
1.6 lt.
311
395c
a.
ø175
ø82
2.0 lt.47
5ca.
391
ø82
ø175
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Glass stirrer vessel Type 2 0.50 L / 6 bar / Ø 82 45.20088.0000 45.20100.2200 • •Glass stirrer vessel Type 2 1.00 L / 6 bar / Ø 82 45.20089.0000 45.20101.2200 • •Glass stirrer vessel Type 2 1.50 L / 6 bar / Ø 82 45.20090.0000 45.20102.2200 • •Glass stirrer vessel Type 2 2.00 L / 6 bar / Ø 82 45.20091.0000 45.20103.2200 •Glass stirrer vessel Type 2 2.00 L / 3 bar / Ø 112 45.20109.0000 45.20109.2200 • •Glass stirrer vessel Type 2 3.00 L / 3 bar / Ø 112 45.20092.0000 45.20104.2200 •Glass stirrer vessel Type 2 5.00 L / 3 bar / Ø 112 45.20093.0000 45.20105.2200 •
Pressure tubesPressure tube for Type 2 0.50 L / 6 bar / Ø 82 45.20036.0000Pressure tube for Type 2 1.00 L / 6 bar / Ø 82 45.20002.0000Pressure tube for Type 2 1.50 L / 6 bar / Ø 82 45.20003.0000Pressure tube for Type 2 2.00 L / 6 bar / Ø 82 45.20004.0000Pressure tube for Type 2 2.00 L / 3 bar / Ø112 45.20106.0000Pressure tube for Type 2 3.00 L / 3 bar / Ø112 45.20023.0000Pressure tube for Type 2 5.00 L / 3 bar / Ø112 45.20022.0000
Heating jacketsHeating jacket for Type 2 0.50 L / Ø 82 / PS15 45.20037.0000Heating jacket for Type 2 1.00 L / Ø 82 / PS15 45.20006.0000Heating jacket for Type 2 1.50 L / Ø 82 / PS15 45.20007.0000Heating jacket for Type 2 2.00 L / Ø 82 / PS15 45.20008.0000Heating jacket for Type 2 2.00 L / Ø 112 / PS15 45.20107.0000Heating jacket for Type 2 3.00 L / Ø 112 / PS15 45.20026.0000Heating jacket for Type 2 5.00 L / Ø 112 / PS15 45.20027.0000
ComponentsIntermediate flange for Type 2 / Ø 82 45.20010.0000 45.20042.2200Intermediate flange for Type 2 / Ø 112 45.20021.0000 45.20044.2200Stud bolt M10 x 50 45.20019.0000Nut M10 45.20032.0000Washer M10 45.20033.0000Washer M10, Novapress 46.80065.0000Screw rod 145 mm for 0.50 L / Ø 82 45.20046.0000Screw rod 225 mm for 1.00 L / Ø 82 45.20012.0000Screw rod 300 mm for 1.50 L / Ø 82 45.20013.0000Screw rod 375 mm for 2.00 L / Ø 82 45.20014.0000
Screw rod 245 mm for 2.00 L / Ø 112 45.20108.0000Screw rod 345 mm for 3.00 L / Ø 112 45.20024.0000Screw rod 545 mm for 5.00 L / Ø 112 45.20025.0000Protective sleeve, silicone 40.00853.0000
Bottom flangewith 3/8" Gi opening for vessels 0.50 – 2.00 L /Ø 82 45.20011.0000 45.20043.2200Bottom flangewith 3/8" Gi opening for vessels 2.0 – 5.0 L /Ø 112 45.20020.0000 45.20045.2200
Options (add to base price)
Opening 1/8"NPT for Pt100 47.40025.0000 47.40025.2200Opening Gi 1/2" incl. plug 47.40026.0000 47.40026.2200Opening Gi 3/4" incl. plug 47.40027.0000 47.40027.2200Opening 13 mm for ball valve 47.40028.0000 47.40028.2200Opening 22 mm for ball valve 47.40029.0000 47.40029.2200Heating- cooling ducts 47.40030.0000 47.40030.2200Round bottom 47.40031.0000 47.40031.2200
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
113
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
Type 2Glass stirrer vessel with bottom opening, max. 3 / 6 bar in the laboratory,max. 5 / 12 bar in the autoclave room, heatable up to max. 200°C, consisting of:� Pressure tube graduated, wall 9 mm
� Jacket connections with plane joint NW 15, incl. adapters PS15 on M16x1
� Flange with stud bolts
� Bottom flange with 3/8" Gi opening and plug
� 4 screw rods with nuts and washers
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
For bottom valves see chapter 9
For closing plugs see chapter 10
For heating jacket connections see chapter 10
For bottom opening seals and collar packing see chapter 11
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
114
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
Adapter flange for fast action closure,complete with screws and seal 40.02772.0000 40.02772.2200 •
Adapter for vessel lift, complete with screws,for vessels Ø 82 40.02305.0000 •Adapter for vessel lift, complete with screws,for vessels Ø 112 40.02308.0000 •
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Type 2Assembly
Nut
Stud Bolt
Intermediate flange
Seal
Packing
Pressure tube
Protective sleeve
Screw rod
Washer NovapressWasherNut
Plug
Washer
Bottom flange
Bottom opening seal
Heating jacket
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
115
6
Heating jacket connection
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
116
6
Type 2Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Stirrer vessel Type 3 0.50 L / 60 bar / M16x1 45.30001.0000 45.30025.2200 • • • •Stirrer vessel Type 3 1.00 L / 60 bar / M16x1 45.30002.0000 45.30026.2200 • • • •Stirrer vessel Type 3 1.50 L / 60 bar / M16x1 45.30059.0000 45.30027.2200 • • • •Stirrer vessel Type 3 2.00 L / 60 bar / M16x1 45.30003.0000 45.30028.2200 • • • •Stirrer vessel Type 3 3.00 L / 60 bar / M16x1 45.30004.0000 45.30029.2200 • • • •Stirrer vessel Type 3 5.00 L / 40 bar / M16x1 45.30005.0000 45.30030.2200 • • • •Stirrer vessel Type 3 10.0 L / 20 bar / M30x1.5 45.30144.0000 45.30145.2200 •Stirrer vessel Type 3 20.0 L / 10 bar / M30x1.5 45.30146.0000 45.30147.2200 •
Components of Type 3Stud bolt M12 x 53 mm 45.30015.0000Nut M12 45.30016.0000
ModificationsBottom opening 1/2" Gi incl. plug 47.40032.0000 47.40032.2200Bottom opening 3/4" Gi incl. plug 47.40033.0000 47.40033.2200Bottom opening for 13 mm ball valve 47.40034.0000 47.40034.2200Bottom opening for 22 mm ball valve 47.40035.0000 47.40035.2200Bottom opening 1/8" NPT for Pt-100 47.40036.0000 47.40036.2200
For bottom valves see chapter 9
For bottom opening seals see chapter 11
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
117
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
inertclave
ecoclave
polyclave
versoclave
kiloclave
Adapter flange for fast action closure,complete with screws and seal 40.02773.0000 40.02773.2200 • • •
Adapter for vessel lift, complete with screws 40.02307.0000 • •
Vessel Type 3E with electric heating,integrated cooling coil and insulation.Ready for connection to btc temperature controller.The surcharge is identical for standard and Hastelloy vessels
Stirrer vessel Type 3E 0.50 L 47.40067.0000 • • • •Stirrer vessel Type 3E 1.00 L 47.40068.0000 • • • •Stirrer vessel Type 3E 1.50 L 47.40069.0000 • • • •Stirrer vessel Type 3E 2.00 L 47.40070.0000 • • • •Stirrer vessel Type 3E 3.00 L 47.40071.0000 • • •Stirrer vessel Type 3E 5.00 L 47.40072.0000 • • •Stirrer vessel Type 3E 10.0 L 47.40073.0000 •Stirrer vessel Type 3E 20.0 L 47.40074.0000 •
Options (add to base price)
Type 3Steel stirrer vessel complete, for max. 60 bar / 250°C, consisting of:� Pressure vessel with welded heating jacket, jacket connections M16 x 1
male (0.5–5.0 L), resp. M30x1.5 male (10.0–20.0 L)
� Bottom opening 3/8" Gi, incl. plug
� Stud bolts M 12 x 53 with nuts
� Works- and test certificates
� Manufactured and tested according to PED, AD2000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Nut
Vessel
Seal
Plug
Stud bolt
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
118
6
Type 3Assembly
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
119
6
Type 3Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
120
Standard Hastelloy
inertclave
ecoclave
polyclave
versoclave
kiloclave
6
inertclave
ecoclave
polyclave
versoclave
kiloclave
Stirrer vessel Type 4 1.00 L / 60 bar / M16x1 45.40001.0000 45.40017.2200 • • • •Stirrer vessel Type 4 1.50 L / 60 bar / M16x1 45.40025.0000 45.40018.2200 • • • •Stirrer vessel Type 4 2.00 L / 60 bar / M16x1 45.40002.0000 45.40023.2200 • • • •Stirrer vessel Type 4 3.00 L / 60 bar / M16x1 45.40003.0000 45.40019.2200 • • • •Stirrer vessel Type 4 5.00 L / 40 bar / M16x1 45.40004.0000 45.40020.2200 • • • •Stirrer vessel Type 4 10.0 L / 20 bar / M30x1.5 45.40075.0000 45.40076.0000 •Stirrer vessel Type 4 20.0 L / 10 bar / M30x1.5 45.40077.0000 45.40078.0000 •
Components of Type 4Stud bolt M12 x 53 mm 45.30015.0000Nut M12 45.30016.0000
Sight glass Metaglas Ø53 x 15 mm 45.40007.0000Sight glass solid Ø53 x 15 mm 45.40008.0000Sight glass solid Ø53 x 15 mm 3.1B 45.40035.0000
ModificationsBottom opening 1/2" Gi incl. plug 47.40032.0000 47.40032.2200Bottom opening 3/4" Gi incl. plug 47.40033.0000 47.40033.2200Bottom opening for 13 mm ball valve 47.40034.0000 47.40034.2200Bottom opening for 22 mm ball valve 47.40035.0000 47.40035.2200Bottom opening 1/8" NPT for Pt-100 47.40036.0000 47.40036.2200
For bottom valves see chapter 9For bottom opening seals see chapter 11
Adapter flange for fast action closure,complete with screws and seal 40.02773.0000 40.02773.2200 • • •
Adapter for vessel lift, complete with screws 40.02307.0000 • •
Options (add to base price)
Vessel Type 4E with electric heating,integrated cooling coil and insulation.Ready for connection to btc temperature controller.The surcharge is identical for standard and Hastelloy vessels
Stirrer vessel Type 4E 1.00 L 47.40075.0000 • • • •Stirrer vessel Type 4E 1.50 L 47.40076.0000 • • • •Stirrer vessel Type 4E 2.00 L 47.40077.0000 • • • •Stirrer vessel Type 4E 3.00 L 47.40078.0000 • • •Stirrer vessel Type 4E 5.00 L 47.40079.0000 • • •Stirrer vessel Type 4E 10.0 L 47.40080.0000 •Stirrer vessel Type 4E 20.0 L 47.40081.0000 •
Type 4Steel stirrer vessel complete, for max. 60 bar / 250°C, consisting of:� Pressure vessel with welded heating jacket, jacket connections M16 x 1
male (0.5–5.0 L), resp. M30x 1.5 male (10.0–20.0 L)
� 2 Sight glasses
� Bottom opening 3/8" Gi, incl. plug
� Stud bolts M12 x 53 with nuts
� Works- and test certificates
� Manufactured and tested according to PED, AD2000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
121
6
Nut
Stud bolt
Seal
Sight glass
Seal
Type 4Assembly
Seal
Plug
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«inertclave», «ecoclave», «polyclave», «versoclave», «kiloclave»
122
6
Type 4Dimensions
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Vessels«midiclave»
123
6
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Stirrer vessel Type 3 0.10 L / 200 bar / M16x1 45.30155.0000 45.30155.2200 •Stirrer vessel Type 3 0.25 L / 200 bar / M16x1 45.30156.0000 45.30156.2200 •Stirrer vessel Type 3 0.50 L / 200 bar / M16x1 45.30157.0000 45.30157.2200 •Stirrer vessel Type 3 1.00 L / 200 bar / M16x1 45.30158.0000 45.30158.2200 •
ModificationsBottom opening 1/2" Gi incl. Plug 47.40032.0000 47.40032.2200Bottom opening 3/4" Gi incl. Plug 47.40033.0000 47.40033.2200Bottom opening 1/8" NPT for Pt-100 47.40036.0000 47.40036.2200
For bottom valves see chapter 9
For bottom opening seals see chapter 11
Vessel Type 3E with electric heating,integrated cooling coil and insulation.Ready for connection to btc temperature controller.The surcharge is identical for standard and Hastelloy vessels
Stirrer vessel Type 3E 0.10 L 47.40098.0000 •Stirrer vessel Type 3E 0.25 L 47.40099.0000 •Stirrer vessel Type 3E 0.50 L 47.40067.0000 •Stirrer vessel Type 3E 1.00 L 47.40068.0000 •
Standard Hastelloy
midiclave
Type 3Steel stirrer vessel complete, for max. 200 bar / 300°C, consisting of:� Pressure vessel with welded heating jacket, jacket connections M16 x 1 male
� Bottom opening 3/8" Gi, incl. plug
� Manufactured and tested according to PED, AD2000
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«midiclave»
124
6
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Type 3Dimensions
Vessels«midiclave»
125
6
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Stirrer vessel Type 4 0.50 L / 200 bar / M16x1 45.30159.0000 45.30159.2200 •Stirrer vessel Type 4 1.00 L / 200 bar / M16x1 45.30160.0000 45.30160.2200 •
Components of Type 4Sight glass Ø53 x 15 mm 40.10138.0000
ModificationsBottom opening 1/2" Gi incl. Plug 47.40032.0000 47.40032.2200Bottom opening 3/4" Gi incl. Plug 47.40033.0000 47.40033.2200Bottom opening 1/8" NPT for Pt-100 47.40036.0000 47.40036.2200
For bottom valves see chapter 9
For bottom opening seals see chapter 11
Vessel Type 4E with electric heating,integrated cooling coil and insulation.Ready for connection to btc temperature controller.The surcharge is identical for standard and Hastelloy vessels
Stirrer vessel Type 4E 0.50 L 47.40100.0000 •Stirrer vessel Type 4E 1.00 L 47.40075.0000 •
Standard Hastelloy
midiclave
Type 4Steel stirrer vessel complete, for max. 200 bar / 300°C, consisting of:� Pressure vessel with welded heating jacket, jacket connections M16 x 1 male
� 2 Sight glasses
� Bottom opening 3/8" Gi, incl. plug
� Manufactured and tested according to PED, AD2000
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Vessels«midiclave»
126
6
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Type 4Dimensions
Vessels«limbo», «limbo li»
127
limbo
/lim
boli
6
Vessel 100 ml / Ø i 40 mm / 350°C / 350 bar 60.10078.0000 60.10079.0000 •Vessel 200 ml / Ø i 52 mm / 350°C / 350 bar 60.10012.0000 60.10081.0000 •Vessel 285 ml / Ø i 52 mm / 350°C / 350 bar 60.10011.0000 60.10080.0000 •Vessel 450 ml / Ø i 66 mm / 350°C / 150 bar 60.10089.0000 •Vessel 450 ml / Ø i 66 mm / 350°C / 200 bar 60.10087.0000 •Vessel 450 ml / Ø i 66 mm/ 350°C / 350 barMaterial 1.4980 60.10088.0000 •
Standard Hastelloy
Type 3Steel stirrer vessel, without jacket and bottom opening,for use with electric heating, for max. 350 bar / 350°C
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Type 3Dimensions
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Cover plate max. 10 bar, 2 x 1/8" NPT 51.10111.0000 51.10111.2200 •
Cover plate max. 10 bar, 4 x 1/4" NPT 52.10145.0000 52.10145.2200 •
Cover plate with welded closing cap for systemswith fast action closure, max. 60 bar, 6 x Swagelok 1/4" 52.50181.0000 52.50203.0000 • •
Cover plate, for systems with fast action closure,max. 60 bar, center M36 x 1.55 x 1/4" NPT, 1 x 3/8" NPT, 1 x 1/2" NPT 46.00107.0000 46.00108.0000 • • •
Cover plate, max. 60 bar, center M36 x 1.55 x 1/4" NPT, 1 x 3/8" NPT, 1 x 1/2" NPT 46.00100.0000 46.00101.0000 • • • •
Cover plate with welded closing capmax. 350 bar, 5 x 1/4" Gi 60.10094.0000 60.10095.0000 •
Cover plate, for systems with fast action closure,max. 200 bar, center M36 x 1.57 x 1/4" NPT 46.00227.0000 46.00228.0000 •
Cover plates128
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
7
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
The cover plate is the connecting link betweenthe vessel and the cover plate setup.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Cover plate with integrated closing capmax. 350 bar4 x Sitec HP M16 x 1.5, 4 x Sitec HP M20 x 1.5 60.10013.0000 60.10237.0000 •
Cover plates129
7
Heating- / cooling ducts with hose nozzles 10mm 47.40037.0000 47.40037.2200 • • • •Heating- / cooling ducts with M16x1 47.40038.0000 47.40038.2200 • • • •Heating- / cooling ductswith hose nozzles 10mm for fast action closure 47.40039.0000 47.40039.2200 • • •Heating- / cooling ductswith M16x1 for fast action closure 47.40040.0000 47.40040.2200 • • •
Modification heating- / cooling ducts for operationwith heat exchanger 47.40041.0000 47.40041.2200 • • • •
Welded flange for 13 / 22mm ball valve 47.40042.0000 47.40042.2200 • • • •
Additional openings 1/4", 3/8" or 1/2"NPT * 47.40043.0000 47.40043.2200 • • • • • •
Other openings * 47.40044.0000 47.40044.2200 • • • • • •
* it must be determined if there is enough space on the cover plate.
PTFE splash protection (not for fast action closure) 46.00044.0000 • • • •
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
3 bar DN 6 1/4"Ga 46.40048.0000 46.40059.0000 • • • • • • • •6 bar DN 6 1/4"Ga 46.40045.0000 46.40049.0000 • • • • • • • •8 bar DN 6 1/4"Ga 46.40051.0000 • • • • • • • •
10 bar DN 6 Ga 1/4" 46.40071.0000 46.40056.0000 • • • • • • • •12 bar DN 6 Ga 1/4" 46.40040.0000 46.40072.0000 • • • • • •20 bar DN 6 Ga 1/4" 46.40041.0000 46.40074.0000 • • • • • •40 bar DN 6 Ga 1/4" 46.40058.0000 46.40057.0000 • • • • • •60 ba DN 6 Ga 1/4" 46.40042.0000 46.40044.0000 • • • • • •100 bar DN 6 Ga 1/4" 46.40053.0000 46.40070.0000 • • • •
10 bar DN 15 NPT 1/2" 46.40082.0000 46.40083.0000 • • • •20 bar DN 15 NPT 1/2" 46.40084.0000 46.40085.0000 • • • •40 bar DN 15 NPT 1/2" 46.40086.0000 46.40087.0000 • • • •60 bar DN 15 NPT 1/2" 46.40088.0000 46.40089.0000 • • • •100 bar DN 15 NPT 1/2" 46.40090.0000 46.40091.0000 • • • •
150 bar DN 4.5 1/4" tube 46.40075.0000 • •200 bar DN 4.5 1/4" tube 46.40080.0000 46.40081.0000 •200 bar DN 4.5 1/4" tube 46.40076.0000 • •350 bar DN 4.5 1/4" tube 46.40060.0000 46.40061.0000 • •
Bursting discs / Relief valves130
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
8
Bursting disc unit with membrane,UKB (reversible)
10 bar DN 6 46.50028.0000 46.50024.0000 • • • • • • • •12 bar DN 6 46.50014.0000 46.50029.0000 • • • • • •20 bar DN 6 46.50015.0000 46.50030.0000 • • • • • •40 bar DN 6 46.50026.0000 46.50025.0000 • • • • • •60 bar DN 6 46.50016.0000 46.50019.0000 • • • • • •100 bar DN 6 46.50022.0000 46.50027.0000 • • • •
10 bar DN 15 46.50032.0000 46.50033.0000 • • • •20 bar DN 15 46.50034.0000 46.50035.0000 • • • •40 bar DN 15 46.50036.0000 46.50037.0000 • • • •60 bar DN 15 46.50038.0000 46.50039.0000 • • • •100 bar DN 15 46.50040.0000 46.50041.0000 • • • •
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Bursting membranes UKB (reversible)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Bursting discs / Relief valves131
8
Relief valve 6 mm / 1/4"Ga / 4 bar 46.20002.0000 46.20039.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 6 bar 46.20003.0000 46.20040.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 8 bar 46.20004.0000 46.20041.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 10 bar 46.20005.0000 46.20042.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 12 bar 46.20006.0000 46.20043.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 15 bar 46.20007.0000 46.20044.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 20 bar 46.20008.0000 46.20045.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 30 bar 46.20009.0000 46.20046.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 40 bar 46.20010.0000 46.20047.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 50 bar 46.20011.0000 46.20048.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 60 bar 46.20012.0000 46.20049.2200 • • • • • • • •Relief valve 6 mm / 1/4"Ga / 70 bar 46.20013.0000 46.20050.2200 • • • • • • • •
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Relief valves
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Bottom valve Ga 3/8" / DN 8 mm 46.20020.1000 46.20038.2222 • • • • • • •Bottom valve Ga 1/2" / DN 12 mm* 46.20062.1000 46.20063.2200 • • • • •Bottom valve Ga 3/4" / DN 16 mm* 46.20071.1000 46.20072.2200 • • • • •
* requires modification of bottom opening (see chapter vessels Type 2 to 4)
Valves132
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
9
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Heatable bottom valves with M16x1 mm connectionsBottom valve Ga 3/8" / DN 8 mm 46.20061.1000 46.20085.1000 • • • • • • •Bottom valve Ga 1/2" / DN 12 mm* 46.20083.1000 46.20086.1000 • • • • •Bottom valve Ga 3/4" / DN 16 mm* 46.20084.1000 46.20087.1000 • • • • •
* requires modification of bottom opening (see chapter vessels Type 2 to 4)
Ball valve DN 13,1 mm * 46.20016.0000 46.20052.0000 • • • •Ball valve DN22 mm * 46.20053.0000 46.20054.0000 • • • •
* Can be used as bottom valve. Requires modification of bottom opening (see chapter vessels Type 2 to 4)
Straight way valve1/4"HP / DN 3 mm / 350 bar / 350°C 46.20074.0000 46.20075.0000 • • • • • • • • • • •
Control valve 1/4" Swagelok / DN 4.4 mm / PN 200 46.20102.0000 • • • • • • • • •
Plug valve 6 mm Swagelok / DN 3.2 mm / PN 170 46.20128.0000Ball valve 1/4" Swagelok / DN 3.2 mm / PN 170 46.20127.0000 • • • • • • • •
Torion valve complete L=71mm, PTFE / 15% glass 40.01935.0000 • • •Torion valve complete L=84mm, PTFE / 15% glass 40.01936.0000 • •Torion valve complete L=110mm, PTFE / 15% glass 40.02721.0000 •
Nut for Torion valve 09.00177.0000 • • •
Bottom valves, straight way valves, ball valves
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
9Valves
133
Stem for Torion valve 71mm, PTFE / 15% glass 40.01956.0000 • • •Stem for Torion valve 84mm, PTFE / 15% glass 40.01957.0000 • •Stem for Torion valve 110mm, PTFE / 15% glass 40.02722.0000 •
Standard Hastelloy
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
9
Fittings and tubesFittings
134
10
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Plug M36x1.5 for cover plate 46.00018.0000 46.00016.2200 • • • •Plug 3/8"Ga for vessel bottom 45.30033.0000 45.30037.2200 • • • • • • •Plug 1/2"Ga for vessel bottom 46.00064.0000 46.00064.2200 • • • • •Plug 3/4"Ga for vessel bottom 46.00056.0000 46.00058.0000 • • • • •
Plug 1/4"NPT 40.01002.0000 46.00050.0000 • • • • •Plug 3/8"NPT 40.01003.0000 46.00033.2200 • • • •Plug 1/2"NPT 40.01049.0000 46.00027.2200 • • •
Plug 1/4" Swagelok 40.01046.0000 40.01340.0000 • • • • • • • • • • •
Male connector 1/4"NPT-1/4" Swagelok 40.01722.0000 40.01778.0000 • • • • •Male connector 1/4"NPT-1/4" Swagelok BT (bored through) 40.01045.0000 40.01779.0000 • • • • •Male connector 1/4"Ga-1/4" Swagelok BT (bored through) 40.02459.0000 40.02467.0000 •Male connector 1/4"NPT-8mm Swagelok BT (bored through) 40.02462.0000 40.02496.0000 • • • • •Male connector 3/8"NPT-1/4" Swagelok 40.02727.0000 40.02813.0000 • • • •Male connector 3/8"NPT-1/4" Swagelok BT (bored through) 40.02613.0000 40.02814.0000 • • • •Male connector 1/2"NPT-1/4" Swagelok 40.02728.0000 40.02815.0000 • • • •Male connector 1/2"NPT-1/4" Swagelok BT (bored through) 40.02729.0000 40.02816.0000 • • • •
Spare parts for connectorNut 40.01265.0000 40.02212.0000Ferrule rear 1/4" 40.01446.0000 40.01360.0000Ferrule front 1/4" 40.01445.0000 40.01359.0000
Adapter for manometer 1/4"Gi-1/4" tube 52.10118.0000 40.01845.0000 • • • • • • •
Adapter for manometer 1/4"Gi-1/4" Swagelok 40.00386.0000 60.10163.0000 • • • •
Y-piece 1/4" tube-2x1/4"Gi 51.10113.0000 51.10114.0000 • • • • • • • • •
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Fittings and tubesFittings
135
10
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Standard Hastelloy
Adapter 90° PS15 on M16x1 male,complete with screw cap, O-ring, insert ring 46.90055.0000 • • • • •
Adapter 90° PS15 on hose nozzle 13mm,complete with screw cap, O-ring, insert ring 46.90056.0000 • • • • •
Insert ring for adapter, PTFE 46.80050.0000
Adapter M16x1female on hose nozzle 13mm, 90° 46.90054.0000 • • • • • • •
Adapter M16x1female on hose nozzle 13mm 46.90126.0000 • • • • • • •
Adapter straight PS15 on M16x1 male,complete with screw cap, O-ring, insert ring 46.90116.0000 • • • • •
Adapter straight PS15 on hose nozzle 13mm,complete with screw cap, O-ring, insert ring 46.90115.0000 46.90140.0000 • • • • •
Y-piece 1/4" tube-2x1/4" tube 46.90121.0000 46.90160.0000 • • • • • • • •
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Fittings and tubesConnection tubes
136
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
10
Connection tube 1/4" x 90mm 52.50154.0000 • • • • • • • •
Connection tube bent 1/4" 52.50149.0000 52.50172.0000 • •
Connection tube 1/4" x 50mm for HP valve 60.10075.0000 60.10169.0000 • • • • • • • • • •Connection tube 1/4" x 105mm for HP valve 60.10207.0000 • • • • • •Connection tube 1/4" x 135mm for HP valve 60.10069.0000 60.10072.0000 • • • •
Spiral 1/4" for manometer / transducer 60.10068.0000 60.10162.0000 • •
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Fittings and tubesDip tubes
137
10
Dip tubes are used to introduce gases or liquidsinto reaction vessels. They are always attachedwith Swagelok fittings to the cover plate.
Dip tubes in Hastelloy:Dip tubes made of Hastelloy can only be used in combination
with valves equipped with HP-fittings.
Dip tubes which are not listed in the catalog:A new part number can be created for dip tubes which are not listed in the catalog.
The last four digits of the part number indicate the tube length.
Example: Dip tube, length 410mm 46.90180.0410 für 1/4" tube, stainless steel
46.90181.0410 für 1/4" HP tube, Hastelloy
The price is the same as for the next longer tube from the price list.
140 mm • • 52.50155.0000180 mm for HP valve • • 60.10082.0000190 mm • • 52.50156.0000235 mm for HP valve • • 60.10074.0000215 mm • 46.90150.0000250 mm for HP valve • 46.90147.0000240 mm • • 46.90145.0000270 mm for HP valve • • 46.90151.0000
StandardDip tube Ø 1/4" HastelloyType
1100ml
200ml
250ml
300ml
Type
3100ml
200ml
300ml
Dip tubes for «miniclave steel», «miniclave drive» and «picoclave»
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Fittings and tubesDip tubes
138
10
245 mm • 46.90180.0245255 mm for HP valve • 46.90181.0255265 mm • 46.90180.0265275 mm for HP valve • 46.90181.0275315 mm • • • • • • • • 46.90180.0315325 mm ffor HP valve • • • • • • • • 46.90181.0325385 mm • 46.90180.0385395 mm for HP valve • 46.90181.0395415 mm • • • 46.90180.0415425 mm for HP valve • • • 46.90181.0425460 mm • • 46.90180.0460470 mm for HP valve • • 46.90181.0470480 mm • • 46.90180.0480490 mm for HP valve • • 46.90181.0490630 mm • 46.90180.0630640 mm for HP valve • 46.90181.0640
StandardDip tube Ø 1/4" HastelloyType
10.25
l0.50
l1.00
l1.60
l2.00
lType
20.50
l1.00
l1.50
l2.00
l3.00
l5.00
lType
3/4
0.50
l1.00
l1.50
l2.00
l3.00
l5.00
l10.00l
20.00l
Dip tubes for «polyclave», «versoclave» and «kiloclave» with fast action closure
195 mm • 46.90180.0195205 mm for HP valve • 46.90181.0205215 mm • 46.90180.0215225 mm for HP valve • 46.90181.0225265 mm • • • • • • • • 46.90180.0265275 mm for HP valve • • • • • • • • 46.90181.0275335 mm • 46.90180.0335345 mm for HP valve • 46.90181.0345365 mm • • • 46.90180.0365375 mm for HP valve • • • 46.90181.0375410 mm • • 46.90180.0410420 mm for HP valve • • 46.90181.0420430 mm • • 46.90180.0430440 mm for HP valve • • 46.90181.0440580 mm • 46.90180.0580590 mm for HP valve • 46.90181.0590
StandardDip tube Ø 1/4" HastelloyType
10.25
l0.50
l1.00
l1.60
l2.00
lType
20.50
l1.00
l1.50
l2.00
l3.00
l5.00
lType
3/4
0.50
l1.00
l1.50
l2.00
l3.00
l5.00
l10.00l
20.00l
Dip tubes for «ecoclave», «polyclave», «versoclave» and «kiloclave» without fast action closure
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Fittings and tubesDip tubes
139
10
180 mm for HP valve • 60.10083.0000 60.10082.0000200 mm for HP valve • 60.10070.0000 60.10073.0000235 mm for HP valve • • 60.10071.0000 60.10074.0000
StandardDip tube Ø 1/4" HastelloyType
3100ml
200ml
285ml
450ml
Dip tubes for «limbo», «limbo li»
324 mm for HP valve • • 60.10033.0000 60.10033.2200
StandardDip tube Ø 1/4" HastelloyType
31.00
l2.00
l
Dip tubes for «limbo ls»
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
155 mm • 46.90180.0155180 mm for HP valve • 60.10082.0000170 mm • 46.90180.0170205 mm for HP valve • 46.90181.0205190 mm • 52.50156.0000225 mm for HP valve • 46.90181.0225240 mm • 46.90145.0000275 mm for HP valve • 46.90181.0275
StandardDip tube Ø 1/4" HastelloyType
3/4
0.10
l0.25
l0.50
l1.00
l
Dip tubes for «midiclave»
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Cover plate 118 / 100 x 2 46.80028.0000 46.80002.0000 46.80004.0000 46.80033.0000 • • • •Shaft 46 / 36 x 2 46.80031.0000 46.80078.0000 46.80035.0000 • • • •Cover connectionsmall 11.5 / 6 x 2 46.80027.0000 46.80017.0000 • • • • • • • • • • •Cover connectionsmall 11 / 7 x 1 60.10228.0000 •
Bottom opening3/8" 25 / 16.5 x 2 46.80115.0000 46.80020.0000 • • • • • • •Bottom opening1/2" 29 / 21 x 1.5 46.80067.0000 46.80055.0000 • • • •Bottom opening3/4" 35 / 27 x 2 46.80073.0000 • • • •
Type 2 Ø82mm 104 / 86 x 2 46.80034.0000 46.80019.0000 • •Type 2 Ø112mm 134 / 116 x 2 46.80057.0000 • •
Type 4 sight glass 55 / 40 x 5 45.40009.0000 • • • •
Burette 25ml 22 / 13 x 2 46.80022.0000 • • • • • • •Burette 100ml 36 / 27 x 2 46.80023.0000 • • • • • • •Burette 250ml 53 / 37 x 2 46.80036.0000 • • • •Burette 500ml 63 / 47 x 2 46.80037.0000 • • • •Burette 1000ml 84 / 65 x 2 46.80038.0000 • • • •
Seals140
PTFE with insertPTFEFlex-O-FormSeal for Size mm Viton Silver
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
11
Flat seals
Type 1 & Type 2 Øi 82mm 125 / 98 x 15 46.80042.0000 • •Type 1 & Type 2 Øi 82mm 125 / 98 x 15 46.80041.0000 • •Type 2 Øi 112mm 165 / 128 x 16 46.80066.0000 • •
SiliconeCollar packing for vessel Size mm Silicone / PTFE
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Collar packingfor Type 1 and Type 2 vessels
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Seals141
11
Diamond shapefor valve 8 mm 25 x 16.7 mm Ni 46.80010.0000 46.80011.0000 46.80012.0000 • • • • •Diamond shapefor valve 12 mm 29 x 21 mm Ni 46.80013.0000 46.80014.0000 46.80015.0000 • • • • •Diamond shapefor valve 16 mm 35.5 x 26 mm Ni 46.80079.0000 46.80080.0000 46.80081.0000 • • • • •
Thickness2.45/2.6 mm
Thickness2.0 mmSize / MaterialSeal
Thickness2.9/3.2 mm
Diamond shape sealsfor bottom valves
ecoclave
polyclave
versoclave
kiloclave
midiclave
Packing ring 17.9 x 8 x 5 46.20064.0000 • • •Packing ring 23 x 13 x 5 40.01241.0000 • •Seal for hose nozzle 14.5 x 8 x 2 46.80070.0000 • •Seal for hose nozzle 19.5 x 13 x 2 46.80107.0000 • •Seal for hose nozzle 25 x 16 x 2 46.80093.0000 • •
Part no.Seal Size
PTFE
Flex-O
-Form
Grafoil
8mm
12mm
16mm
PTFE-Tape max. 260°C 12.7 x 0.1 mm, L=13.7m 10022 • • • • • •PTFE/Ceramic-Tape max. 1300°C 12.7 x 0.2 mm, L=15.2m 10412 • • • • • • •
Part no.Size mm
PTFE-Tapefor sealing of NPT threads
Seals and packingsfor bottom valves
8 / 12 / 16 mm
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Seals142
11
bmd shaft M36 x 1.5 26.64 x 2.62 46.80069.0000 46.80007.0000 • • • • •bmd 075 shaft NS29/32 21.95 x 1.78 42.55009.0000 42.55010.0000
25.12 x 1.78 42.55011.0000 42.55012.0000bmd 300/800/1200 closing cap 34.6 x 2.62 43.20106.0000 46.80082.0000 • • • •bmd 1800 25.07 x 2.62 42.10089.0000 44.00000.0001bmd 1800 91.67 x 3.53 44.00000.0006 44.00000.0002Feeding funnel NS29/32 23.47 x 2.62 42.50045.0000 42.50062.0000 • • • •Sight Glass 21.95 x 1.78 42.55010.0000 • • • •Jacket connection PS15 18.72 x 2.62 46.90081.0000 46.90141.0000 • • •Cover plate 26.57 x 3.53 51.10119.0000 51.10103.0000 •
56.74 x 3.53 52.10109.0000 52.10103.0000 • • •59.7 x 3.2 60.10351.0000 •52.39 x 3.53 60.10235.0000 •88.5 x 3.53 44.00000.0007 •111 x 3.2 60.10352.0000 •113.90 x 3.53 46.80083.0000 46.80084.0000 • • •
KalrezVitonSize mmO-Ring for Silver (C-Ring)
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Torion valve 22 /14 09.00178.0000 • • •
Size mm PTFE / Silicone
Sealfor Torion valve
O-Rings
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Burette 25 ml / 15 bar 46.90000.1003 46.90000.1004 • • • • • • •Burette 100 ml / 15 bar 46.90000.2003 46.90000.2004 • • • • • • •
Burette 250 ml / 15 bar 46.90000.3003 46.90000.3004 • • • •Burette 500 ml / 15 bar 46.90000.4003 46.90000.4004 • • • •Burette 1000 ml / 12 bar 46.90000.5003 46.90000.5004 • • • •
Burette 250 ml / 15 bar with exhaust valve 46.90001.3003 • • • •Burette 500 ml / 15 bar with exhaust valve 46.90001.4003 • • • •Burette 1000 ml / 12 bar with exhaust valve 46.90001.5003 • • • •
Holder for burette for 250 / 500 / 1000 ml, for Ex-Drive 46.90058.0000 • • •
Holder for burette for 250 / 500 / 1000 ml 46.90149.0000 • • • •
Variable componentsBurettes
143
Standard Hastelloy tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
12
Burettes are used to feed liquidsto a running pressure reaction.
The standard scope of delivery includes the following parts:
� Glass cylinder, flanges, protection tube and
screw rods ( from 250 ml), connection tube 1/4" and seals.
� Operating manual and certificate according to PED
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Variable componentsBurettes
144
12
Pressure tube 15 bar for 25 ml / glass 46.90019.0000Pressure tube 15 bar for 100 ml / glass 46.90027.0000Pressure tube 15 bar for 250 ml / glass 46.90013.0000Pressure tube 15 bar for 500 ml / glass 46.90014.0000Pressure tube 12 bar for 1000 ml / glass 46.90015.0000
Protection tube for burette 25 ml / Plexiglas 46.90032.0000Protection tube for burette 100 ml / Plexiglas 46.90033.0000
Protection tube for burette 25 ml / steel 46.90025.0000Protection tube for burette 100 ml / steel 46.90026.0000Protection tube for burette 250 ml / steel 46.90039.0000Protection tube for burette 500 ml / steel 46.90001.0000Protection tube for burette 1000 ml /steel 46.90003.0000
Connection tube for burette 250 / 500 / 1000 ml 46.90158.0000 46.90159.0000
Standard Hastelloy
Spare parts
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Variable componentsSampling system
145
12
Sampling system 46.90182.0000 46.90182.2200 • • • •Sampling system 46.90183.0000 46.90183.2200 • • •
Standard Hastelloy tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Sampling system for samplingduring a pressure reaction.
The standard scope of delivery includes the following parts:
for eco-/poly-/verso-/kiloclave:
� Dip tube with filter
� 2 valves
� Sample cylinder 5 ml
� Cover connection and T-piece
for miniclave steel/miniclave drive/picoclave:
� Dip tube with filter
� 2 valves
� Sample tube 1 ml
Filter 7 micron 46.90113.0000 40.02191.0000 • • • •Filter 0.5 bis 2 micron 46.90114.0000 40.02778.0000 • • • •
Filter tube 0.5 micron 46.90185.0000 46.90185.2200 • • •
Standard Hastelloy tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Filter for sampling system
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Variable componentsFeeding funnel
146
12
Feeding funnel NS29/32 / NPT 1/2" 46.90068.0000 46.90070.2200 • • • •Feeding funnel NS29/32 / M24 x 1.5 46.90143.0000 46.90144.0000
Standard Hastelloy ecoclave
polyclave
versoclave
kiloclave
The opening of the feeding funnel has a NS 29/32 joint.
It may also be used to connect e.g. a condenser with NS29/32 connection.
The standard scope of delivery includes the following parts:
� Feeding funnel with screw cap and NS29/32 plug, O-ring sealed.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Variable componentsHeat exchanger
147
12
Heat exchanger with 8 mm tube 46.90071.0000 46.90073.2200 • • • •
Standard Hastelloy
Heat exchanger for heating or cooling inside the vessel.
For this application the cover plate must be equipped with welded Swagelok fittings
on the under side. (see chapter cover plates)
The standard scope of delivery includes the following parts:
� Heat exchanger with welded 8mm tubes
The tube length must be fitted depending on the vessel size and stirrers!
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Variable componentsReflux cooler
148
12
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Reflux cooler both ends NPT 1/2", max. 100 bar 46.90074.0000 46.90074.2200 • • • •
Standard Hastelloy
Reflux cooler for direct installation on the cover plate.
Thread connection both ends NPT 1/2" male
Thread for cooling connection 2 x NPT 1/8" female
Exchange surface 0.015 m2
max. 100 bar, max. 250°C
The standard scope of delivery includes the following parts:
� as pictured, incl. 1/8"NPT adapter on hose nozzle for cooling media.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Variable componentsCatalyst basket
149
12
Catalyst basket complete (without baffle rod), 6 ml 46.90082.0000 • • • • • •
Standard Hastelloy tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
The catalyst basket is installed on the baffle rod.
The basket is adjustable to position it perfectly within the flow path
of the medium.
The standard scope of delivery includes the following parts:
� Catalyst basket with set screw, 6 ml
� Cover with set screw
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Variable componentsDistillation system made of glass
150
12
Distillation system complete 46.90167.0000 • •Distillation system complete 46.90172.0000 •
Standard Hastelloy tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Distillation system
This application requires a welded flange for the ball valve on the cover plate.
Max. pressure: -1 to + 1 bar. Max. temperature: 200°C.
Total height from cover plate 1350 mm
The standard scope of delivery includes the following parts:
� complete glass overhead consisting of:
vapor duct DN25, holding rod with supports, reflux valve,
reflux condenser 0.075 m2, 4 liter receiver with bursting disc,
drain- and vent valve
� Ball valve DN22
For welded flange see chapter cover plates
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Instrumentation«bds md»
151
13
bds md 3 channel-display 22.08250.0000bds md 2 channel-display 22.08251.0000
Part number
The «bds md» is a 2 or 3 channel display which is available
in various configurations.
Standard version: 2 or 3 LED-displays
1 RS-232 Interface
The scope of delivery includes the instrument, without sensors.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Instrumentation«bds.sc»
152
13
te 94, Temperature instrument 48.00025.0000pr 94, Pressure instrument 48.00026.0000sm 94, Speed instrument 48.00028.0000
Options (add to base price)
Interface Master, incl. cable RS232 22.07800.0000Interface Slave, incl. connection cable 22.07810.0000
Ex i input, integrated into bds.sc 47.40045.0000
Part number
The «bds.sc» is a single channel instrument for the following parameters:
Temperature, pressure, vacuum, speed and pH.
Standard version: LED-display
2 alarm outputs
4...20mA analog output
These instruments are stackable and can be combined to a complete
measurement system with an internal bus system.
The scope of delivery includes the instrument, without sensors.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Instrumentation«bds mc»
153
13
bds mc measurement / control instrument 22.08050.0000
Part number
The «bds mc» is a multi channel instrument for the following
parameters:
Temperature, pressure, vacuum, torque, speed,
and pH. Speed control for all Büchi agitator drives
Standard version: LCD-Touch-screen display
1 speed input
5 sensor inputs
4 alarm outputs
4 analog outputs
1 RS-232 interface
The scope of delivery includes the instrument, without sensors,
a RS232-cable, and the configuration calibration
according to customer specification.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Instrumentation«bds mc Ex-Box»
154
13
Part number
The «bds mc Ex-Box» is connected between the «bds mc» outside the Ex-area and the
sensors in the Ex-area. The «bds mc Ex-Box» must be placed outside the Ex-area.
The system consists of the base unit and Ex-transmitters.
Transmitters can be selected depending on the configuration for the following parameters:
Temperature, pressure, vacuum, and speed
The scope of delivery includes the Ex-Box and the connection cables to the bds mc.
Ex-Box base unit for EExi transmitters 47.40046.0000Channel set EEx i te (Pt100), installed in Ex-Box 47.40047.0000Channel set EEx i pr (4..20mA), installed in Ex-Box 47.40048.0000Channel set EEx i rpm (Namur), installed in Ex-Box 47.40050.0000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
InstrumentationpH-Measurement
155
13
bds pH-amplifier / sensor / adapter
The pH- measurement system consist of:
� pH amplifier with connection cable and plug
� pH sensor with cable
� pH adapter for pH sensor
� Pt100 temperature sensor
� bds mc
All components must be ordered separately.
bds pH-amplifier 22.08072.0000
pH-sensor for max. 60 bar / 110°C, cable 3 m 46.90065.0000
Adapter for pH- sensor 3/8" NPT, length 180 mm 46.90059.0000 46.90061.2200Adapter for pH- sensor 3/8" NPT, length 210 mm 46.90062.0000 46.90064.2200
Plug coax for pH-sensor, mounted 40.20171.0000
HastelloyStandard
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
InstrumentationTemperature controller «btc»
156
13
Part number
Temperature controller for electric heating on Büchi pressure
reactors.
Operating conditions: -100 to 500°C
Standard version: LCD and LED display
3 sensor inputs
Output for cooling valve
Output for electric heating
Over-temperature protection
RS-232 interface
The scope of delivery includes the controller with power cable.
Temperature controller «btc 01» configured for vessels Type 3E / 4E, incl. cable RS232 22.08112.0000Temperature controller «btc 02» configured for limbo, incl. cable RS232 22.08111.0000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
InstrumentationTemperature measurement
157
13
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Pt-100, Ø1/4", with cable
The scope of delivery includes the Pt-100 with
3 m cable and open ends
Pt-100, bendable1 x Pt-100, Ø 1/4", L=280 mm 46.60105.0000 46.60107.0000 • • • • • • • •1 x Pt-100, Ø 1/4", L=350 mm 46.60106.0000 46.60108.0000 • • • •1 x Pt-100, Ø 1/4", L=450 mm 46.60135.0000 46.60137.0000 • • • •2 x Pt-100, Ø 1/4", L=280 mm 46.60102.0000 46.60131.0000 • • • • • • • •2 x Pt-100, Ø 1/4", L=350 mm 46.60136.0000 46.60132.0000 • • • •2 x Pt-100, Ø 1/4", L=450 mm 46.60109.0000 46.60129.0000 • • • •
Pt-100, not bendable1 x Pt-100, Ø 1/4", L=250 mm 46.60096.0000 46.60097.0000 • • • • •2 x Pt-100, Ø 1/4", L=250 mm 46.60098.0000 46.60099.0000 • • • • •1 x Pt-100, Ø 1/4" HP, L=290 mm 60.10047.0000 46.60145.0000 •2 x Pt-100, Ø 1/4" HP, L=290 mm 46.60146.0000 46.60147.0000 •
Options (add to base price)
ATEX version 1 x Pt-100 47.40082.0000 47.40082.0000ATEX version 2 x Pt-100 47.40083.0000 47.40083.0000Cable with special length up to 20m 47.40051.0000
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Thermometer sleeve, Ø ¼"
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Thermometer sleeve, Ø ¼", L=140 mm for 100ml 52.50152.0000 52.50153.0000 • • •Thermometer sleeve, Ø ¼", L=180 mm for 200ml 52.50150.0000 52.50151.0000 • • •Thermometer sleeve, Ø ¼", L=205 mm for 250ml 52.50179.0000 52.50180.0000 • • •Thermometer sleeve, Ø ¼", L=230 mm for 300ml 46.60103.0000 46.60104.0000 • • •
Standard Hastelloy
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
InstrumentationTemperature measurement
158
13
tinyclave
steel
miniclave
steel
miniclave
drive
picoclave
ecoclave
polyclave
versoclave
kiloclave
midiclave
limbo
/lim
boli
limbo
ls
Pt-100 short, for vessel bottom
The scope of delivery includes the Pt-100, with Lemo plug.
The cable must be ordered separately.
Pt-100Pt-100 short, 1/8"NPT, Lemo 0 46.60047.0000 46.60049.2200 • • • • •Pt-100 short, double, 1/8"NPT, Lemo 1 46.60050.0000 46.60052.2200 • • • • •
Options (add to base price)
ATEX version 47.40084.0000 47.40084.0000
Standard Hastelloy
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
InstrumentationTemperature measurement
159
13
Cable for Pt100 short, Lemo 0 / open ends 3m 46.60069.0000Cable for Pt100 short, Lemo 0 / open ends 10m 40.20926.0000
Cable for Pt100 short, doppelt, Lemo 1 / open ends 3m 46.60072.0000
Plug for bds-te (blue), mounted 40.20167.0000
Plug for bds-te Ex (white), mounted 40.20173.0000
Plug Lemo 1 4-pole, for «btc» or thermostat (*), mounted(*) Huber, Julabo, Lauda, according Namur 46.60087.0000
Plug Lemo 2 for Pt-1000, mounted 40.20017.0000
Cable with special length up to 20m 47.40051.0000
Part number
Part number
Cables and plugs for Pt-100
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
InstrumentationPressure measurement
160
13
Manometer Ø 63mmConnection Ga 1/4"
Vacuum-manometer -1/+15 bar 46.70004.0000 52.10138.0000Manometer 0/+40 bar 40.01745.0000 46.70019.0000Manometer 0/+60 bar 46.70014.0000 46.70018.0000Manometer 0/+100 bar 46.70015.0000 46.70020.0000Manometer 0/+200 bar 46.70022.0000 46.70023.0000Manometer 0/+400 bar 46.70016.0000 46.70017.0000
Standard Seal PFA coated
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Pressure transducer without cable and plug.Connection Ga 1/4"
Pressure transducer -1..16 bar 48.40052.0000 48.40046.2200Pressure transducer 0..40 bar 48.40054.0000 48.40048.2200Pressure transducer 0..60 bar 48.40055.0000 48.40053.0000Pressure transducer 0..100 bar 48.40056.0000 48.40050.2200Pressure transducer 0..200 bar 48.40074.0000 48.40075.2200Pressure transducer 0..400 bar 48.40057.0000 48.40063.0000Pressure transducer Ex i -1..16 bar 48.40068.0000 48.40068.2200Pressure transducer Ex i 0..40 bar 48.40070.0000 48.40070.2200Pressure transducer Ex i 0..60 bar 48.40071.0000 48.40071.2200Pressure transducer Ex i 0..100 bar 48.40072.0000 48.40072.2200Pressure transducer Ex i 0..200 bar 48.40076.0000 48.40078.2200
Standard Hastelloy
InstrumentationPressure measurement
161
13
Cable for transducer, open ends 2 m 22.07918.0000
Cable for transducer, plug for bds-pr, 2 m 22.07920.0000
Cable for transducer Ex i, plug for bds-pr Ex, 5 m 22.07924.0000
Cable with special length up to 20 m 47.40051.0000
Part number
Part number
Cables and plugs for pressure transducer
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Hall switch with cable, open ends 3 m 48.40010.0000 • • • •Hall switch with cable, open ends 5 m 48.40064.0000 • • • •
Hall switch with cable, for bds-rpm, 3 m 48.40058.0000 • • • •
Hall switch Ex i square, with cable, open ends, 10 m 48.40051.0000 •
Hall switch Ex i, M8x1, with cable, open ends, 2 m 48.40073.0000 •
Hall switch Ex i, M12x1 with plug M12 22.07909.0000 •
Pulse generator stainless steel, 3 pulse/revolution 48.40011.0000 • •Pulse generator Hastelloy C22, 3 pulse/revolution 48.40013.2200 • •
InstrumentationSpeed measurement
162
Part number bmd07
5
bmd30
0–12
00
bmd18
00
cyclon
e07
5
cyclon
e30
0
13
Hall switch / Pulse generator
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
InstrumentationSpeed measurement
163
13
Plug for bds-rpm (yellow), mounted 40.20170.0000
Plug for bds-rpm Ex (brown), mounted 40.20176.0000
Cable for hall switch Ex, M12 / open ends 5 m 31.01221.0000Cable for hall switch Ex, M12 / open ends 10 m 22.07910.0000
Cable for hall switch Ex i, M12 / plug for bds-rpm Ex 5 m 22.07913.0000Cable for hall switch Ex i, M12 / plug for bds-rpm Ex 10 m 22.07915.0000
Cable for hall switch Ex i, M12 / plug for bds-rpm 5 m 22.07912.0000Cable for hall switch Ex i, M12 / plug for bds-rpm 10 m 22.07914.0000
Cable with special length up to 20m 47.40051.0000
Part number
Part number
Cables and plugs for hall switch
Options (add to base price)
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Instrumentationbüchi pressflow gas controller «bpc»
164
13
bpc 1202 for max. 12 bar 48.90001.0000bpc 1210 for max. 12 bar 48.90006.0000bpc 6002 for max. 60 bar 48.90007.0000bpc 6010 for max. 60 bar 48.90008.0000bpc 9901 for max. 100 bar 48.90009.0000bhpc 20001 for max. 200 bar 48.90013.0000bhpc 40001 for max. 400 bar 48.90011.0000
Options (add to base price)
Software for ethylene, for reactions up to max. 50 bar 48.90014.0000Software for propylene, for reactions up to max. 17.5 bar 48.90015.0000Software for oxygen, for reactions up to max. 100 bar 48.90025.0000Analog input 4-20 mA, external setpoint for reaction pressure 48.90023.0000ATEX Version 47.40101.0000
Part numberType
The «bpc» is a hydrogenation instrument for dosing hydrogen,
ethylene, propylene or oxygen.
There are several softwares available depending on the gas type.
The scope of delivery includes:
Gas control unit with 1/4" Swagelok-fittings for
gas connection, controller, powerbox, and various connection cables.
Software for hydrogen.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
InstrumentationSoftware «bls 2»
165
13
The software «bls 2» is used for data acquisition,
graphic display and saving and evaluating of up to
16 measurement parameters.
The following Büchi instruments are implemented in the software:
«bds md» / «bds sc» / «bds mc» / «btc» / «bpc»/ «cyclone 300»
as well as thermostats according to data sheet
Büchi software «bls 2»The newest version will be delivered 22.07892.0000
OptionsHydrogenation report 22.07893.0000
Cable RS232 SubD 9pol, straight, 3 m 40.20181.0000Cable RS232 SubD 9pol, straight, 10 m 40.20632.0000
Adapter Gender changer f-f 9pin 40.20673.0000Adapter crossed (Null modem) 9pin 40.20900.0000(for btc/Huber/cc300))
Converter USB for 4 x RS232 40.20901.0000
Converter USB for 1 x RS232 40.20626.0000
Part number
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Accessories166
Tool box with foam insert460 x 350 x 90 mm, blue, with Büchi- Logo 46.90057.0000
Part number
Heat transfer oil for thermostats, transparentin plastic canister
-40 to + 400°C 5 liter 48.50005.0000-73 to + 260°C 5 liter 48.50010.0000-90 to + 200°C 10 liter 31.00993.0000
Metal hose, flexible, for heat transfer oiltripple insulated, connections both endsM16 x 1 mm female, for max. 300°C.
length 1.5 m 45.30035.0000
Silicone hose,reinforced with polyester braiding.Ø inside 12.5 mm, outside 21 mm, for max. 200°C.
length 1.5 m 45.30046.0000
Assembly greaseFDA-conform for threads and general applications
Tube 250g 40.02513.0000
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
14
1. GeneralThe following terms and conditions serve as a clear arrangement for thereciprocal relationship between the buyer and Büchi AG. Supplementaryagreements, if any, must be in written form in order to be valid.
2. PricesOur official price lists include suggested prices. The right to make pricechanges as well as deviations in the sense of technical improvement re-mains reserved. The prices applicable on the day of delivery will be char-ged. The prices are in Swiss Francs, exclusive of value added tax, strictlynet, ex works and without packaging (Incoterms). All ancillary costs such asfreight, insurance, export permits, transit permits, import permits and otherapprovals, will be charged to the buyer. The buyer is likewise required topay all types of taxes, duties, fees, customs and similar tariffs that are le-vied in connection with the contract, or to reimburse Büchi AG for them inexchange for appropriate documentation if Büchi AG was obligated to paythem.
3. PackagingPackaging is billed at original cost. Export deliveries are made in speciallydeveloped packaging at the expense of the buyer.
4. Shipping and transfer of usufruct and riskWe deliver ex works (Incoterms). Usufruct and risk transfer to the buyerwhen the delivery is dispatched ex works. Without exception, shipping takesplace at the expense and risk of the buyer via our freight forwarder. A trans-portation insurance policy will be taken out at the expense of the buyer uponrequest. For deliveries by truck that are carriage paid breakage-free to theaddress of the recipient, we will invoice a share of transportation expenses.Complaints in connection with the shipment or transportation are to be dire-cted by the buyer to the most recent freight carrier without delay after re-ceipt of the consignment or freight documents. Büchi AG is to be informedwithout delay as well.
5. Customized productsFor customized products, we reserve the right to deliver the actual quantityof items produced.
6. Delivery dateIn the absence of an explicit written agreement, the delivery dates indica-ted by Büchi AG are target dates, and the failure to comply with them doesnot entitle the buyer to withdraw from the contract or to claim reductions orcompensation for damages.
7. AssemblyAssembly at the destination location shall be invoiced to the buyer on thebasis of time and expenses pursuant to our terms and conditions of assem-bly.
8. WarrantyBüchi AG guarantees that the products will be free of defects, i.e. withflawless fusion zones, including tension-free cooling and damage-freeglass surfaces. Flats shall be precision-ground. Glass breakage, in particu-lar when due to surfaces damaged between the time of delivery or assem-bly and commissioning shall be excluded from the warranty.Büchi AG is obligated to repair or replace all parts that become damaged orunusable as a result of poor materials, incorrect design or defective work-manship.Damage not caused by Büchi AG (normal wear and tear, lack of maintenan-
ce, disassembly errors for which Büchi AG is not accountable, and so forth)is excluded from the warranty. The warranty expires prematurely if the buy-er or a third party makes improper modifications or repairs or, if a defect isdiscovered, if the buyer does not immediately take appropriate steps to re-duce the scope of damage and in writing provide Büchi AG with the oppor-tunity to remedy the defect. The warranty period amounts to one year andcommences upon dispatch of the delivery ex works, or upon completion ofassembly, if it was carried out by Büchi AG. If assembly is delayed for rea-sons that are beyond the control of Büchi AG, the warranty period ends nolater than 18 months after delivery to the buyer. The warranty period startsanew for replaced parts. The buyer is required to examine the consignmentimmediately upon receipt. If the buyer does not carry out the examinationof the goods, or if the buyer fails to provide notice of the defects to BüchiAG immediately after examination or discovery, rights to claim defects shallbe forfeited. Returns shall be accepted only with prior approval from BüchiAG.
9. LiabilityBüchi AG is liable for contractual performance. Any further liability with res-pect to the buyer for any damages whatsoever is waived by the buyer.
10. PaymentInvoices are to be paid by the buyer without any deductions (such as dis-counts, etc.) whatsoever, and for a delivery amount
of up to CHF 30,000within 30 days after the date of the invoice, strictly net;
of more than CHF 30,000 up to CHF 150,000one-third at the time the order is placed and two-thirds within 30 days af-ter the date of the invoice, strictly net;
of more than CHF 150,000, the negotiated terms and conditions of pay-ment are applicable.
The minimum invoice amount is CHF 50 net.
The material that we deliver remains our property until payment in full isreceived. The buyer is obligated to cooperate with us upon first requestwith respect to steps that may be necessary to protect our ownership inte-rest. The buyer does not have a right of offset against Büchi AG.
11. Applicable law and court of jurisdictionSwiss law exclusively is applicable to all legal relationships established bythese terms and conditions.Uster is the place of performance and the court of jurisdiction for both par-ties.
Viton® and Kalrez® are registered trademarks of DuPont ElastomersSwagelok® is a registered trademark of the Swagelok CompanySantotrac® is a registered trademark of the Findett CorporationNovapress® is a registered trademark of the Frenzelit-Werke GmbH & Co. KGFlex-O-Form® is a registered trademark of Merkel Freudenberg Fluidtechnic GmbH
General terms and conditions of sale and delivery
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
Inertautoclaves
(non-m
etallic)
Autoclaves
(metal/glass)
Drives
Magnetic
couplings
Mixingelem
ents
Vessels
Coverplates
Burstingdiscs
Reliefvalves
Valves
Fittings
andtubes
Seals
Variable
components
Instrumentation
Accessories
Specials are our specialty
70 liter 10 barreactor with distillationoverhead stainless steel
1 liter parallel reactor for hydrogenationstainless steel / glass
chlorine dioxid pilot plant, fully automatedtitanium / glass
100 liter 60 barhydrogenation reactor with sparging tubeHastelloy C22
10 liter 400 barreactor with electricheating and lift
3x 20 liter 20 barpilot plant for suspension-polymerizationwith automation, Ex proof
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Custom pressure reactors and pilot plants up to 200 liter / 500 bar / 500°CWe build reactors for the highest demands made of Hastelloy, tantalum, titanium and other exotic materials. Your requirementes are our challenge. Our ex-
perience in manufacturing reactors guarantees good, practical and economic solutions. Whatever needs you have for experimental reactors - we have an
answer. Do not hesitate to ask us.
Büchi AG Geschwaderstrasse 12 CH-8610 Uster/Switzerland Phone +41 44 905 51 11 Fax +41 44 905 51 22 www.buchiglas.ch
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