analytical/chemical certificate of analysis...test lab cert. customer: stiriti ayurtherapies pvtltd...

Test Lab Cert

Customer: Stiriti Ayur Therapies PVT LTDAddress: Plot # 179 & 180, Cheekatmamidi (V), Bommalramaram (M)

Nalgonda Dist, Telangana State 508116Ph #: +919491042863

ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSIS

Accession #: 160719-0033

PO#: N/ASample Description: Bulk, 10 grams; US PharmacopeiaRush: N/A

Sample Date: 07/19/16Page:1/5

Test Performed:Pesticide Screen:

Pesticides

Bromophos-methyl

Flucythrlnate

Methoxychlor

Pyrettirums (Clnerin I, Cinerln II,Jasmolln I,Jasmolln II, Pyrethrin I, Pyrethrin II)

Acephate

Aldrin and dieidrln (sum of)

Azinphos-ethyl

Azinphos-methyl

Bromophos-ethyl

Bromopropylate

Chlordane

(sum of cis-trans-, and oxychlordane)Chlorfenvlnphos

Chlorpyrlphos-ethyl

Chlorpyriphos-methyl

Chlorthal-dimethyl

Cyfluthrin (sum of)

A-Cyhalothrin

Test Method Number:

MQLTM-0343 (USP<S61>Modifled)ByGC-MS

USP Limit Level:

MQLTM-0343 (USP<561> Modified) O.OSppmbvGC-MS

MQLTM-0343 {USP<561> Modified) O.OSppmby GC-MSMQLTM-0343 (USP<561> Modified) O.OSppmby GC-MS

MQLTM-0343 (USP<S61> Modified) 3ppmByGC-MS

MQLTM-0343 (USP<561> Modified) O.OO-O.lOmg/kgby GC-MS

MQLTM-0343 (USP<561> Modified) O.OO-O.OSmg/kgby GC-MSMQLTM-0343 (USP<561> Modified) 0.00-0.05mg/kgby GC-MSMQLTM-0343 (USP<561> Modified) O.OO-O.lOmg/kgby GC-MSMQLTM-0343 (USP<S61> Modified) O.OO-l.OOmg/kgby GC-MS

MQLTM-0343 (USP<561> Modified) 0.00-0.05mg/kgby GC-MSMQLTM-0343 (USP<S61> Modified) 0.00-3.00mg/kgby GC-MS

MQLTM-0343 (USP<561> Modified) O.OO-O.OSmg/kgby GC-MSMQLTM-0343 (USP<561> Modified) 0.00-0.5Qmg/kgby GC-MSMQLTM-0343 (USP<S61> Modified) 0.00-0.20mg/kgby GC-MSMQLTM-0343 (USP<561> Modified) O.OO-O.lOmg/kgby GC-MSMQLTM-0343 (USP<S61> Modified) O.OO-O.Olmg/kgby GC-MSMQLTM-0343 (LISP<561> Modified) O.OO-O.lOmg/kgby GC-MSMQLTM-0343 (USP<561> Modified) 0.00-l,00mg/kgby GC-MS

Results:

<O.OSppm

<O.OSppm

<O.OSppm

<0.10mg/kg

<0.05mg/kg

<0.05mg/kg

<0.10mg/kg

<1.00mg/kg

<0.05mg/kg

<3.00mg/kg

<0.0Smg/kg

<O.SOmg/kg

<0.20mg/kg

<0.10mg/kg

<0.01mg/kg

<0.10mg/kg

<1.00mg/kg

Form# 03B.2 Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR2015-0082

Sample Name: Spilanthes acmella

extract Produ de: N/A

Batch/Lot #: SEX64/003/16-17

DEEPA-SIDDHA

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Test Lab Cert

Customer: Stiriti Ayur Therapies PVT LTDAddress: Plot # 179 & 180, Cheekatmamidi (V), Bommalramaram (M)

Nalgonda Dist, Telangana State 508116Ph#: +919491042863

ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSISSample Name: Spilanthes acmella extractProduct Code:Batch/Lot #: EX64/003/16-17

Accession #: 160719-0033

PC#: N/A

Sample Description: Bulk,10 grams; US PharmacopeiaRush: N/A


Test Performed: Test Method Number:

Pesticide Screen:

Cvpermethfin and Isomers (sum oO

DDT (sum of o,p'-D0E,p,p'-DDE,o,p'-DDT,p,p'-DDT, o,p'-TDE, and p,p-TDE

Deltamethrin

Diarinon

Dichlofluanid

Dichlorvos

Dicofol

Dimethoate and omethoate (sum of)

Endosulfan (sum of isomers andendosulfan sulphate)Endrin

Ethion

Etrimphos

Fenctiiorophos (sum of fenchlorophos andfenchlorophos-oxon)

MQLTM-0343 (USP<561> Modified)by6C-MSMQLTM-0343 (USP<561> Modified)byGC-MSMQLTM-0343 (USP<561> Modified)

byGC-MSMQLTM-0343 (USP<561> Modified)byGC-MS

MQLTM-0343 (USP<561> Modified)

by GC-MSMQLTM-0343 (USP<561> Modified)

byGC-MS

MQLTM-0343 (USP<561> Modified)by GC-MSMQLTM-0343 (USP<561> Modified)by GC-MSMQLTM-0343 (USP<S61> Modified)by GC-MSMQLTM-0343 (USP<S61> Modified)byGC-MS

MQLTM^)343 (USP<561> Modified)byGC-MSMQLTM-0343 (USP<561> Modified)byGC-MSMQLTM-0343 (USP<551> Modified)

by GC-MS

USP Limit Level:

O.OO-l.OOmg/kg <1.00mg/kg


O.OO-O.SOmg/kg <0.S0mg/kg

O.OO-O.SOmg/kg <0.50mg/kg

O.OO-O.lOmg/kg <0.10mg/kg


0.5mg/kg <0.5mg/kg


0.00-3.00mg/kg <3.00mg/kg

0.00-0.OSmg/kg <0.05mg/kg

0.00-2.00mg/kg <2.00mg/kg

O.OO-O.OSmg/kg <0.05mg/kg


Fenitrothlon MQLTM-0343 (USP<561> Modified)by GC-MS

O.OO-O.SOmg/kg <0.50mg/kg

Fenpropathrin ' MQLTM-0343 (USP<561> Modified) 0.00-0.03mg/kg <0.03m6/kgbyGC-MS

Fensuifothlon

(sum of fensuifothlon, fensulfothion-oxon,fensulfothion-oxonsuifon, and

fensulfothion-suifon)

Fenthion (sum of fenthion, fenthion-oxon, fenthion-oxon-suifon,fenthion-

oxon-sulfoxid, fenthion-sulfon, and

fenthion-sulfoxid)

MQLTM-0343 (USP<561> Modified)by GC-MS

MQLTM-0343 (USP<561> Modified)ByGC-MS

0.00-0,OSmg/kg <0.05mg/kg

0.00-0.05mg/kg <0.05mg/kg

Form#038.2 Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR201S-0082

DEEPA-SIDDHA

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Test Lab Cert

Customer: Stiriti Ayur Therapies PVT LTDAddress: Plot tf 179 & 180, Cheekatmamldi (V), Bommalramaram (M)

Nalgonda Dist, Telangana State 508116Ph U: +919491042863

ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSISSample Name: Spilanthes acmeiia extract

Product Code:Batch/Lot #: EX64/003/16-17

Accession #: 160719-0033

PC#: N/ASample Description: Bulk, 10 grams; US PharmacopeiaRush: N/ASample Date: 07/19/16Page:3/5

Test Performed: Test Method Number:

Pesticide Screen:

Fenvalerate

Tau-Fluvslinate

Fonophos

Hept3chlor(sum of heptachlor, os-

MQLTM-0343 (USP<S61> Modified)by GC-MS

MQLTM-0343 (USP<561> Modified)byGC-MS


MQLTM-0343 (USP<S61> Modified)

heptachlorepoxide, andtrans-heptachiorepoxide) j byGC-MSHexachlorobenzene

Hexachlorocyclohexane (sum of isomers a, P-, 6,and E-)

Lindan (T-hexachlorocyclohexane)

Malathion and malaoxon (sum of)

Mecarbam

Methacriphos

Methamidophos

Methidathion

Mirex

Monocrotophos

Parathion-ethyl and Paraoxon-ethyl (sum of)

Parathlon-methyl and Paraoxon-methyl (sum of)

Pendlmethalin

MQLTM-0343 (U5P<561> Modified)by GC-MSMQLTM-0343 (USP<S61> Modified)

by GC-MS

MQLTM-0343 (U5P<S61> Modified)by GC-MSMQLTM-0343 (USP<561> Modified)byGC-MS


MQLTM-0343 (USP<561> Modified)by GC-MSMQLTM-0343 (USP<S61> Modified)

byGC-MSMQLTM-0343 (USP<561> Modified)

byGC-MS

MQLTM-0343 (USP<561> Modified)

by GC-MSMQLTM-0343 (LISP<561>Modified)byGC-MS

MQLTM-0343 (USP<S61> Modified)

by GC-MS

MQLTM-0343 (USP<561> Modified)by GC-MSMQLTM-0343 (USP<561> Modified)

byGC-MS

USP Limit Level: Results:

O.OO-l.SOmg/kg <1.50mg/kg

O.OO-O.OSmg/kg <0.05mg/kg

O.OO-O.QSmg/kg <0.05mg/kg

0.00-0.05mg/kg <O.OSmg/kg

O.OO-O.lmg/kg <0.1mg/kg

0.00-0.30mg/kg <0.30mg/kg

0.00-0.60mg/kg <0.60mg/kg

O.O-l.OOmg/kg <1.00mg/kg

O.GO-O.OSmg/kg <0.05mg/kg

0.00-0.05mg/kg <0.05mg/kg

0.00-0.05mg/kg <0.05mg/kg

0.00-0.20mg/kg <0.20mg/kg

Q.OO-O.Olmg/kg <0.01mg/kg

0.00-0.lOmg/kg <0.10mg/kg

0.00-0.50mg/kg <0.50mg/kg

0.00-0.20mg/kg <0.20mg/kg

O.lmg/kg cO.lmgAs

Pentachloranisol MQLTM-0343 (USP<561> Modified)by GC-MS

O.OO-O.Olmg/kg <0.01mg/kg

Permechrin and Isomers (sum of) MQLTM-0343 {USP<551> Modified)

by GC-MS

0.00-1.00mg/kg <1.00mg/kg

Phosalone MQLTM-0343{USP<561> Modified) O.OO-O.lOmg/kg <0.10mg/kgby GC-MS

Form# 038.2 Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR201S-0082

DEEPA-SIDDHA

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Test Lab Cert

Customer: Stiriti Ayur Therapies PVTLTDAddress: Plot # 179 &180, Cheekatmamidi (V), Bommalramaram (M)


ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSISSample Name: Spllanthes acmelia extractProduct Code:Batch/Lot #: EX64/003/16-17

Accession ft: 160719-0033

PO#: N/ASample Description: Bulk,10 grams;Rush: N/ASample Date: 07/19/16Page:4/5

Test Performed:

Pesticide Screen:

Phosmet

PIperonyl butoxide

Pirimiphos-ethyl

Pirimiphos-methyl (sum of pirlmiphos-methyl and N-desethyl-pirimiphos-methyl)

Procymidone

Profenophos

Quintozene (sum of quintozene,pentachloranillne, and methylpentachlorphenyl sulflde)

5-421

US Pharmacopeia

Test Method Number:

(USP<561> Modified) O.OO-O.OSmg/kgMQLTM-0343

byGC-MS

USP Limit Levei:

(USP<561> Modified) 0.00-3.00mg/kgMQLTM-0343

by GC-MS


by GC-MS


ByGC-MS

(USP<561> Modified) 0,00-0.10mg/kgMQLTM-0343

byGC-MS

(USP<561> Modified) O.OO-O.lOmg/kgMQLTM-0343

by GC-MS


by GC-MS

(USP<561> Modified) O.OO-O.OSmg/kgMQLTM-0343

by GC-MS

(USP<561> Modified) O.OO-l.OOmg/kgMQLTM-0343

By GC-MS

MQLTM-G343 (USP<561> Modified) 0.00-0.02mg/kgby GC-MSMQLTM-0343 (USP<561> Modified) O.OO-O.OSmg/kgbyGC-MSMQLTM-0343 (USP<S61> Modified) 0.00-0.30mg/kgby GC-MSMQLTM-0343 (USP<S61> Modified) 0.00-0.40mg/kgBy GC-MS

<O.OSmg/kg

<3.00mg/kg

<O.OSmg/kg

<4.00mg/kg

<0.10mg/kg

<0.10mg/kg

<0.05mg/kg

<O.OSmg/kg

<1.00mg/kg

<0.02mg/kg

<O.OSmg/kg

<0.30mg/kg

<0.40mg/kg

Form# 03B.2 Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR2015-0082

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Customer: Stirltl Ayur Therapies PVTLTDAddress: Plot # 179 & 180, Cheekatmamidi (V), Bommalramaram (M)


ACCREDITED

Test Lab Cert

ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSIS

Sample Name: Spilanthes acmella extractProduct Code:

Batch/Lot #: EX64/003/16-17Accession #: 160719-0033

PO#: N/ASample Description: Bulk, 10 grams; USPharmacopeiaRush: N/A


Prepared By:

Lisa Ha/Document Control

Reviewed By:

Danielle Dobrow/Document Control Supervisor

AU6 0 3 201608/03/16

08/03/16

, i5onA2LA ISO 17025 accredited testing laboratory (Certificate Number ). Therequirements of ISO 17025 werefollowedfor the test, results and preparation of thiscertificate of analysis.

'sscope of accreditation may be found on A2LA or websites.

The aforementioned resultson thisreport are representative of the samplessubmittedand maynot be indicative of the entiremanufacture, batch, and/or lot.Applicable current CMP's shallalwaysbe usedwhensampling. GLP's shallalwaysbe practicedby

to ensure the most accurate results.

Form# 03B.2 Analytical / Chemical Certificate ofAnalysis, Revised 06/29/15 DCR2015-0082

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analytical/chemical certificate of analysis...test lab cert. customer: stiriti ayurtherapies pvtltd...

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