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City of Detroit 2 Woodward Avenue, Suite 401, Detroit, MI 48226 June 30, 2015 NTH Project No. 62-140614-100B Report Baseline Environmental Assessment 3801 West Jeerson Property Detroit, Michigan NTH Consultants, Ltd. 2990 W. Grand Blvd. Suite M-10 Detroit, MI 48202

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Page 1: Baseline Environmental Assessment for Riverside Park

City of Detroit 2 Woodward Avenue, Suite 401, Detroit, MI 48226

June 30, 2015NTH Project No. 62-140614-100B

ReportBaseline Environmental Assessment

3801 West Jeff erson PropertyDetroit, Michigan

NTH Consultants, Ltd.2990 W. Grand Blvd.

Suite M-10Detroit, MI 48202

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TABLE OF CONTENTS

Page No.

1.0 INTRODUCTION AND DISCUSSION 1

1.1 OWNER/OPERATOR INFORMATION 1 1.2 INTENDED USE OF THE PROPERTY 1 1.3 EXECUTIVE SUMMARY – ALL APPROPRIATE INQUIRY 1 1.4 AAI EXCEPTIONS OR DELETIONS 2 1.5 AAI DATA GAPS 3 1.6 PHASE II ENVIRONMENTAL SITE ASSESSMENT 3 1.7 KNOWN CONTAMINATION AND MEDIA AFFECTED 4 1.8 BASIS FOR FACILITY DETERMINATION 6

2.0 PROPERTY INFORMATION 7

2.1 LEGAL DESCRIPTION 7 2.2 SURVEY MAP 7 2.3 SCALED SITE MAP 7 2.4 SCALED AREA MAP 7 2.5 PROPERTY LOCATION 7 2.6 SPATIAL DATA 7

3.0 FACILITY STATUS 8

3.1 ANALYTICAL SUMMARY TABLE 8 3.2 LABORATORY DATA 8

4.0 IDENTIFICATION OF THE AUTHOR 9 5.0 ALL APPROPRIATE INQUIRY REPORT 10 6.0 REFERENCES 11 7.0 ATTACHMENTS 12

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1.0 INTRODUCTION AND DISCUSSION

On behalf of City of Detroit, NTH Consultants, Ltd. (NTH) has prepared this Baseline

Environmental Assessment (BEA) report for the 3801 West Jefferson property located in

Detroit, Wayne County, Michigan. The subject property is approximately 4.7 acres in size

and contains a warehouse building, paved parking lot and ship dock, and grass-covered areas.

The building is used for storage of aluminum ingots.

1.1 OWNER/OPERATOR INFORMATION

City of Detroit (2 Woodward Avenue, Suite 401, Detroit, Michigan 48226) intends to acquire

the property around July 10, 2015.

1.2 INTENDED USE OF THE PROPERTY

The property will be used for general recreational purposes. The property will be prepared for

expansion of adjacent Riverside Park by demolishing the existing building and adding

landscape improvements.

1.3 EXECUTIVE SUMMARY – ALL APPROPRIATE INQUIRY

NTH performed a Phase I Environmental Site Assessment (ESA) for the property in accordance

with the scope and limitations of American Society for Testing and Materials (ASTM) Practice

E1527-13, which is consistent with United States Environmental Protection Agency’s All

Appropriate Inquiries (AAI) Final Rule. The findings of the Phase I ESA are presented in

NTH’s report dated May 19, 2015, which is included as Attachment I.

The Phase I ESA revealed the following evidence of recognized environmental conditions

(RECs) at the property:

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x The property was formerly a part of Detroit River and was reclaimed to support the

current development. No information on the backfill soil used for land reclamation

purposes is readily available. As such, the environmental nature and origin of the

backfill soil are unknown.

x Past uses of the property include lumber yard, coal yard and warehouse with an oil house.

No information is readily available regarding the past occupants’ hazardous material

handling, storage or waste disposal practices implemented on the premises.

x Railroad spur is located at the property and railroad ties were noted to be stored east of

the building.

x One closed-in-place UST is located inside the building. No documented information was

available to evaluate the environmental status of the UST and its impact on the

surrounding soils.

x One vent pipe was noted on the north exterior wall of the building. The significance of

this pipe could not be determined.

x Based on the information provided by the current property owners regarding a previous

subsurface investigation, the property is a “facility” as defined by Part P.A. 451, Part

201, as amended.

x Soil and/or groundwater contamination was identified on the westerly and easterly

adjacent sites.

1.4 AAI EXCEPTIONS OR DELETIONS

No deviations, deletions or additions from the ASTM Practice E1527-13 were made during

performance of the Phase I ESA.

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1.5 AAI DATA GAPS

No significant data gaps were encountered during the Phase I ESA.

1.6 PHASE II ENVIRONMENTAL SITE ASSESSMENT

NTH performed a Phase II ESA at the property in accordance with ASTM E1903-11 to

evaluate the Phase I ESA-identified RECs. The results of the Phase II ESA were presented in

NTH’s report dated June 9, 2015, and a copy of which is included as Attachment II.

During Phase II ESA, a visual survey was conducted to determine the significance of the vent

pipe observed on the exterior north wall of the building and to confirm the location of the

1,000-gallon gasoline underground storage tank (UST) which was closed-in-place and filled

with concrete in 1987. The vent pipe was traced using a utility locating device and it

terminated in an area inside the building that is covered with a concrete patch. This area was

further evaluated by geoprobe borings and an obstruction indicative of UST was encountered.

The subsurface investigations comprised of advancing 11 geoprobe borings, designated as

GP-1 through GP-11, three exploratory probes, designated as P-1 through P-3, and analysis of

soil. The borings were advanced at the approximate locations depicted on the Boring

Location Plan included in Attachment II. Subsurface conditions observed at each explored

location are presented on the Log of Geoprobe Borings included in Attachment II.

The subsurface conditions at the explored locations comprised of up to 19 feet of sandy and

clayey fill soil with pieces of brick, coal, porcelain, roofing materials, slag and wood. The fill

soil is underlain by native clayey soils to the explored depths. Obstructions were encounter at

P-1 at a depth of about 2 feet and at GP-5, P-2 and P-3 at depths of about 12 feet. As

previously indicated, a closed-in-place UST is present at the location of P-1. The significance

of obstructions at GP-5, P-2 and P-3 could not be precisely determined, but appear to be

rubble materials in the fill soil. No groundwater was encountered in any of the borings.

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The soil samples were analyzed for Volatile Organic Compounds (VOCs), Polynuclear

Aromatics (PNAs), and the Michigan 10 metals (arsenic, barium, cadmium, chromium,

copper, lead, mercury, selenium, silver and zinc). Laboratory data for the analyzed samples

are included in Attachment II.

The results of soil analytical results were compared to MDEQ-established - Revised Part 201

Generic Cleanup Criteria and Screening Levels - Table 2; Soil: Residential, published on

December 30, 2013, which have been established pursuant to 1994 P.A. 451, Part 201, as

amended. Specifically, the results of the soil analysis were compared to the Part 201

residential direct contact (DC) criteria, drinking water protection (DWP) criteria,

groundwater/surface water interface protection (GSIP) criteria, soil volatilization to indoor air

criteria (SVIIC), infinite source soil volatilization to ambient air criteria (VSIC), particulate

soil inhalation criteria (PSIC), and soil saturation concentration screening levels (SSCSL).

The results of the metals analyses were also compared to the statewide default background

(SWDB) concentrations, as established by MDEQ.

Results of VOCs, PNAs and PCBs were also compared to Residential Vapor Intrusion Soil

Screening Levels. , and residential vapor intrusion soil screening levels. The results of the

soil analyses are summarized on Table 1 in Attachment II.

1.7 KNOWN CONTAMINATION AND MEDIA AFFECTED

The Phase II ESA identified the following hazardous substances in the soil samples above the

Part 201 generic residential cleanup criteria (GRCC):

Contaminant CAS Nos. Sample Location

Criteria Exceeded

Arsenic 7440382

S-3 from GP-3

DWP and GSIP GP-2, S-1 from GP-3, GP-4, S-1 and S-3 from GP-5, GP-6, GP-8, GP-9, GP-10 and S-2 from GP-

11

DWP, GSIP and DC

Chromium 7440473 GP-2 and GP-6 GSIP S-3 from GP-5, GP-9 and GP-10 DWP and GSIP

Copper 7440508 S-3 from GP-3, S-1 and S-3 from GSIP

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Contaminant CAS Nos. Sample Location

Criteria Exceeded GP-5, GP-6, GP-7 and GP-8

Lead 7439921 GP-6 DC S-3 from GP-5 DWP and DC

Mercury 7439976

S-3 from GP-3, GP-4, GP-6, GP-9 and GP-10

GSIP

Selenium 7782492

GP-2, S-1 from GP-3, GP-4, S-1 from GP-5, GP-8, GP-9 and GP-

10

GSIP

Zinc 7440666

S-3 from GP-3, GP-4, S-3 from GP-5, GP-6 and GP-8

GSIP

Benzene 71432 S-1 from GP-3

DWP

GP-2, and S-2 from GP-11

DWP and SVIIC S-1 from GP-11

DWP, GSIP and SVIIC n-Butylbenzene 104518 S-1 from GP-11

DWP

Ethylbenzene 100414 S-2 from GP-11 DWP GP-2, GP-6 and S-1 from GP-11 DWP and GSIP

Naphthalene 91203 GP-2, S-3 from GP-5 and S-1

from GP-11 GSIP

GP-6 DWP and GSIP n-Propylbenzene 103651 S-1 from GP-11 DWP

Toluene 108883 S-1 from GP-11 GSIP Trichloroethylene 79016 GP-9 DWP

1,2,4-Trimethylbenzene 95636 GP-2, GP-6 and S-1 and S-2 from GP-11 DWP and GSIP

1,3,5-Trimethylbenzene 108678 GP-2 and S-1 from GP-11 DWP and GSIP

Xylenes 1330207 S-1 from GP-3, GP-6 and S-2

from GP-11 GSIP

GP-2 and S-1 from GP-11 DWP and GSIP Acenaphthene 83329 GP-6 GSIP

Benzo(a)pyrene 50328 S-3 from GP-3, GP-4 and GP-6 DC Fluoranthene 206440 S-3 from GP-3, GP-4 and GP-6 GSIP

Fluorene 86737 GP-6 GSIP

2-Methylnaphthene 91576 S-1 from GP-3, S_1 from GP-5

and S-1 from GP-11 GSIP

GP-6 DWP and GSIP

Phenanthrene 85018

S-1 and S-3 from GP-3, GP-4, S-1 and S-3 from GP-5, GP-8 and

GP-10 GSIP

GP-6 DWP and GSIP

The locations of the above contamination exceeding Part 201 GRCC are depicted on the

Sample Exceedance Plan in Attachment III.

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1.8 BASIS FOR FACILITY DETERMINATION

Based on the hazardous substances identified in Section 1.7, the property is a “facility.”

According to Section 20101(1)(s) of Part 201 of NREPA (1994 P.A. 451, as amended),

“facility” means any area, place, or property where a hazardous substance in excess of the

concentrations that satisfy the cleanup criteria for unrestricted residential use has been

released, deposited, disposed of, or otherwise comes to be located.

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2.0 PROPERTY INFORMATION

2.1 LEGAL DESCRIPTION

Legal description and plat map for the property are included in Attachment I.

2.2 SURVEY MAP

A plat map depicting property boundaries is included in Attachment III.

2.3 SCALED SITE MAP

A scaled site map in the form of a Sample Exceedance Plan with boring locations, sample

depths and detected contaminant concentrations above the Part 201 GRCC is included in

Attachment III.

2.4 SCALED AREA MAP

A scaled area map in the form of a Site Location Map of the property is included in

Attachment I.

2.5 PROPERTY LOCATION

The property is located at 3801 West Jefferson Avenue, Detroit, Wayne County, Michigan

48216. The property is identified as Parcel No. 14000001-3.

2.6 SPATIAL DATA

The property is located in the Northeast ¼ of Section 24, Township 1 South, Range 11 East,

Detroit, Wayne County, Michigan.

According to Google Earth webpage, the property coordinates are:

x Latitude: 42.310819 N / Longitude: -83.081639 W.

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3.0 FACILITY STATUS

3.1 ANALYTICAL SUMMARY TABLE

Tables listing the hazardous substance concentrations, sample identification, sample depths,

media affected and the Part 201 GRCC are included in Attachment II.

3.2 LABORATORY DATA

Laboratory analytical data and chain-of-custody documents are included in Attachment II.

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4.0 IDENTIFICATION OF THE AUTHOR

Author: Cliff J. Andrews Senior Project Professional

NTH Consultants, Ltd. Phone: 248-662-2741 Email: [email protected]

Reviewer: Bhushan C. Modi Project Manager

NTH Consultants, Ltd. Phone: 248-662-2740 Email: [email protected]

The resumes of the above NTH personnel are included in Attachment I.

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5.0 ALL APPROPRIATE INQUIRY REPORT

NTH conducted a Phase I ESA at the property in accordance with the scope and limitations of

ASTM Practice E1527-13, entitled: “Standard Practice for Environmental Site Assessments:

Phase I Environmental Site Assessment Process”, which is consistent with EPA’s AAI Rule

40 CFR Part 312. NTH’s Phase I ESA report is included in Attachment I.

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6.0 REFERENCES

x Attachments I, II and III in Section 7.0.

x MDEQ’s - Revised Part 201 Generic Cleanup Criteria and Screening Levels - Table 2;

Soil: Residential, published on December 30, 2013.

x Environmental Remediation, Part 201 of the Natural Resources and Environmental

Protection Act 451 P.A. 1994, as amended, and the Part 201 Rules promulgated

thereunder, for the purpose of establishing an exemption to liability pursuant to Section

20126(1)(c) for a new owner or operator of property that is a facility as defined by Section

20101(1)(s).

x MDEQ’s document entitled: “Contents of BEA Report,” dated February 2015.

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7.0 ATTACHMENTS Attachment I: Phase I ESA Report Attachment II: Phase II ESA Report Attachment III: Sample Exceedance Plan Plat Map

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ATTACHMENT IPHASE I ESA REPORT

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City of DetroitBuildings, Safety Engineering and Environmental Department

2 Woodward Avenue, Suite 401, Detroit, Michigan 48226

May 19, 2015NTH Project No. 62-140614-100

ReportPhase I Environmental Site Assessment

3801 West Jeff erson PropertyDetroit, Michigan

NTH Consultants, Ltd.2990 W. Grand Blvd.

Suite M-10Detroit, MI 48202

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TABLE OF CONTENTS

Page No. 1.0 EXECUTIVE SUMMARY 1 2.0 INTRODUCTION 3

2.1 Purpose 3 2.2 Detailed Scope of Services 4 2.3 Significant Assumptions 4 2.4 Limitations and Exceptions 5 2.5 Special Terms and Conditions 5 2.6 User Reliance 5

3.0 USER PROVIDED INFORMATION 6

3.1 Title Records, Environmental Liens and Activity and Use Limitations 6

3.2 Specialized Knowledge 6 3.3 Valuation Reduction for Environmental Issues 6 3.4 Commonly Known or Reasonably Ascertainable Information 6 3.5 Reason for Performing the Phase I ESA 7

4.0 RECORDS REVIEW 7

4.1 Physical Setting Sources 7 4.1.1 Topography 7

4.1.2 Geology 8 4.1.3 Hydrology 8 4.1.4 Hydrogeology 8 4.1.5 Oil and Gas Wells 8

4.2 Standard Federal, State and

Tribal Environmental Record Source 8

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TABLE OF CONTENTS (cont.)

Page No.

4.3 Historical Use Information 14

4.3.1 Local Governmental Agency Records 14 4.3.2 Sanborn Fire Insurance Maps 15 4.3.3 City Directories 16 4.3.4 Aerial Photographs 17 4.3.5 USGS Topographic Maps 17 4.3.6 Past Use Summary 18

4.4 Historical Uses of Adjoining Properties 19

5.0 SITE RECONNAISSANCE 20

5.1 Location and Legal Description 20 5.2 Site and Vicinity Characteristics 20 5.3 Current Uses of the Property 20 5.4 Description of Structures, Roads and Other Improvements 21 5.5 Current Uses of Adjoining Properties 21 5.6 Methodology and Limiting Conditions 21 5.7 General Site Setting 22 5.8 Exterior Observations 22 5.9 Interior Observations 23 5.10 Storage Tanks 24 5.11 Polychlorinated Biphenyls (PCBs) 24

6.0 INTERVIEWS 24

6.1 Property Owner Information 24 6.2 Interview with Site Manager 25 6.3 Interviews with Occupants 26 6.4 Interviews with Local Government Officials 26

7.0 EVALUATIONS 26

7.1 Findings and Opinions 26 7.2 Conclusions 28

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TABLE OF CONTENTS (cont.)

Page No. 8.0 ADDITIONAL SERVICES 29 9.0 REFERENCES 29 10.0 QUALIFICATIONS OF ENVIRONMENTAL PROFESSIONALS 31

APPENDICES Site Location Plan, Figure 1; Site Plan, Figure 2; and Legal Description APPENDIX A Property Photographs APPENDIX B User Questionnaire APPENDIX C EDR Radius Map Report APPENDIX D Sanborn Maps APPENDIX E Owner Questionnaire APPENDIX F Resumes of Environmental Professionals APPENDIX G

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1.0 EXECUTIVE SUMMARY

This report presents the results of a Phase I Environmental Site Assessment (ESA) for the

3801 West Jefferson property located in Detroit, Michigan. The subject property is

approximately 4.7 acres in size and contains a warehouse building, paved parking lot and ship

dock, and grass-covered areas.

The Phase I ESA was performed in accordance with the scope and limitations of American

Society for Testing and Materials (ASTM) Practice E1527-13, which is consistent with

United States Environmental Protection Agency (EPA) All Appropriate Inquiries (AAI) Final

Rule. This assessment has revealed the following evidence of recognized environmental

conditions (RECs) in connection with the property:

x The property was formerly a part of Detroit River and was reclaimed to support the

current development. No information on the backfill soil used for land reclamation

purposes is readily available. As such, the environmental nature and origin of the

backfill soil are unknown.

x Past uses of the property include lumber yard, coal yard and warehouse with an oil house.

No information is readily available regarding the past occupants’ hazardous material

handling, storage or waste disposal practices implemented on the premises.

x Railroad spur is located at the property and railroad ties were noted to be stored east of

the building.

x One underground storage tank (UST) was located inside the building and is reportedly

closed-in-place. No information is available to evaluate the environmental status of the

UST and surrounding soils.

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x One vent pipe was noted on the north exterior wall of the building. The significance of

this pipe could not be determined.

x Based on the information provided by the current property owners regarding a previous

subsurface investigation, the property is a “facility” as defined by Part P.A. 451, Part

201, as amended.

x Soil and/or groundwater contamination was identified on the westerly and easterly

adjacent sites.

This executive summary should not be reviewed separately from the remainder of the report,

and is not a substitute for a thorough review of the entire report.

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2.0 INTRODUCTION

NTH Consultants, Ltd. (NTH) was retained by the City of Detroit to perform a Phase I

Environmental Site Assessment (ESA) of the 3801 West Jefferson property located in Detroit,

Wayne County, Michigan. A map depicting the location of the property is included as Figure

1 in Appendix A.

NTH conducted this Phase I ESA in accordance with the scope and limitations of American

Society for Testing and Materials (ASTM) Practice E1527-13 entitled: “Standard Practice for

Environmental Site Assessments: Phase I Environmental Site Assessment Process,” which is

consistent with the All Appropriate Inquiries (AAI) Final Rule (40 CFR Part 312).

2.1 Purpose

City of Detroit intends to acquire the property as part of the Riverside Park expansion. Thus,

the objective of this Phase I ESA is to provide the City of Detroit with a professional opinion

regarding recognized environmental conditions (RECs), if any, associated with the property.

According to ASTM Practice E1527-13, the term recognized environmental conditions means

the presence or likely presence of any hazardous substances or petroleum products in, on, or at

a property: (1) due to any release to the environment; (2) under conditions indicative of a release

to the environment; or (3) under conditions that pose a material threat of a future release to the

environment.

De minimis conditions are not RECs, and are defined as a condition that generally does not

present a threat to human health or the environment and that generally would not be the subject

of an enforcement action if brought to the attention of appropriate governmental agencies.

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2.2 Detailed Scope of Services

The scope of services for the Phase I ESA comprised of the following key tasks:

x A visual survey of the property and accessible portions of the building was conducted to

identify RECs. Color photographs were taken to document surface features indicative of

RECs. These photographs are presented in Appendix B and are referenced in the text of

the report.

x The neighboring properties were observed to assess whether surface features or activities

on these properties may have a negative environmental impact on the property. The

previous uses of the adjacent properties were determined through review of information

compiled during the Phase I ESA.

x Past use history of the property was developed from reasonably ascertainable

information.

x Readily available information was reviewed relating to geology, hydrogeology and

topographic setting for the property.

x A regulatory agency file search was performed to identify sites of known or potential

environmental concerns located within the minimum search distances from the property,

as specified in the ASTM Practice E1527-13.

x Local governmental agency personnel were contacted to determine their knowledge of

reported environmental incidents at the property.

x The information developed during this study was evaluated and this report was prepared.

2.3 Significant Assumptions

During the course of this study, various documents and other information published by and

obtained from private organizations, as well as Municipal, State and Federal regulatory

agencies have been relied upon. No independent verification or confirmation of the accuracy

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of this information has been performed. Additionally, information provided by the property

owner and NTH’s client was presumed to be factual, unless written documentation was

available indicating otherwise.

2.4 Limitations and Exceptions

The evaluations and opinions presented in this report have been made to assist the client in

making a reasonable assessment of risk with respect to the presence of RECs at the property.

This study has been performed in accordance with a standard of care and diligence, which is

considered to be representative of the local environmental engineering practice at the present

time.

The evaluations and opinions presented in this report are based on the scope of services

defined herein, and should not be misconstrued as those pertaining to a formal environmental

compliance audit. The results of this investigation cannot be construed as a certification of

the absence of any contaminants on the property, but rather a diligent and prudent review of

available data within an established work scope, and time and budgetary constraints.

Limiting conditions encountered during the performance of the Phase I ESA are described in

appropriate sections of this report.

2.5 Special Terms and Conditions

The services for this study were performed in accordance with the project purchase order

issued by City of Detroit.

2.6 User Reliance

This report is intended for the exclusive use of the City of Detroit and/or its affiliates,

subsidiaries and authorized agents. This report presents NTH’s opinion of the property as of

this date, based on the results of this study and on the information provided during the course

of the study. The results of this study may not be relied upon by parties other than those

identified above without the prior knowledge and written consent of NTH.

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3.0 USER PROVIDED INFORMATION

NTH’s Phase I ESA User’s Questionnaire was completed by Raymond Scott of City of

Detroit. Mr. Scott indicated that this Phase I ESA is requested for intended acquisition of the

property. A copy of this completed questionnaire is included in Appendix C.

3.1 Title Records, Environmental Liens and Activity and Use Limitations

Title records for the property were not provided to NTH during the current study. The

information obtained from Michigan Department of Environmental Quality (MDEQ) –

Remediation Division website did not identify any environmental liens recorded against the

property. Additionally, a regulatory agency database search by EDR, Inc. (discussed later)

did not identify any environmental liens or activity use limitations (AULs) associated with the

property.

Actual Knowledge of the User

Mr. Scott is not aware of any environmental liens or AULs associated with the property.

3.2 Specialized Knowledge

Mr. Scott indicated that he has no specialized knowledge or experience related to the property

or nearby properties, other than the property has been used for warehouse purposes and is

located downstream from a former manufactured gas plant.

3.3 Valuation Reduction for Environmental Issues

Mr. Scott did not identify any significant reduction in the purchase price of the property in

relationship with its fair market value.

3.4 Commonly Known or Reasonably Ascertainable Information

Mr. Scott is not aware of any commonly known or reasonably ascertainable information

indicative of RECs at the property.

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3.5 Reason for Performing the Phase I ESA

The reason for performing the Phase I ESA was to provide the authorized users of this report

with an independent evaluation of the environmental risks associated with the property, and to

satisfy the requirement to perform “all appropriate inquiry” in order to qualify for liability

protection pursuant to Part 201 of the Natural Resources and Environmental Protection Act as

well as to the Comprehensive Environmental Response, Compensation and Liability Act

(CERCLA).

4.0 RECORDS REVIEW

NTH reviewed readily available records to determine 1) the local geology and hydrogeology

of the area; 2) the potential risk to the property from offsite sources of environmental concern;

3) historical uses of the property; and 4) historical uses of adjacent properties. These records

were reviewed to help identify RECs, if any, associated with the property.

Environmental Data Resources, Inc. (EDR), a private environmental information agency, was

retained to provide physical setting information, regulatory agency database search, historical

Sanborn maps, aerial photographs, and topographic maps.

4.1 Physical Setting Sources

The physical setting sources for the property were determined based on a review of EDR

provided information, readily available published information and visual observations made

during site reconnaissance. As described in the following subsections, the physical setting

includes topography, soil, general geology, hydrology, hydrogeology, and related attributes.

4.1.1 Topography

Information on the topography of the property was obtained from the USGS “Detroit,

Michigan” topographic map. Based on this map, the property exhibits a level topography

with a USGS elevation of approximately 580 feet above mean sea level.

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4.1.2 Geology

The USDA Soil Survey of Wayne County Area, Michigan does not cover the property. Based

on historical information the property was part of Detroit River and is man-made land

comprised of unknown fill soil underlain by native clayey soil. According to published

sources of generalized subsurface information, the geology of the area is characterized by

about 85 to 135 feet of non-homogeneous glacial lacustrine clay deposits. Underlying these

glacial deposits is the Traverse bedrock formation, which is comprised of limestone and shale.

4.1.3 Hydrology

Detroit River is located immediately south of the property. According to the EDR report,

which searched the FEMA database, the property is not located within a 100-year or 500-year

flood zone.

4.1.4 Hydrogeology

Groundwater in the area is generally present in both the glacial deposits and in the underlying

bedrock; however, shallow groundwater in the area of the property is expected to be erratic

and almost negligible due to the high clay content of the glacial soils. Intermittent

accumulations of perched water may be encountered where granular soils overlie the clay.

4.1.5 Oil and Gas Wells

According to information provided in the EDR report, no oil or gas wells are located at or in

the immediate vicinity of the property.

4.2 Standard Federal, State and Tribal Environmental Record Source

EDR, Inc. provided a regulatory agency database search report (The EDR Radius Map

Report) identifying sites of environmental concerns located within the ASTM Practice E1527-

13-specified minimum search distances from the property. A list of the regulatory agency

databases researched by EDR for the current study, along with the respective search distances

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and a brief description of each database are presented in the EDR report, dated April 29,

2015, and is included in Appendix D.

The EDR report identified 74 sites, of which 72 sites were plotted on a street map and 2 sites

were listed as “orphan sites.” The orphan sites could not be plotted by EDR on a map due to

lack of proper addresses or other pertinent information required for precise computer plotting,

and as such could only be located within the city, county or zip code area of the property.

The following tables list the ASTM –recommended databases researched by EDR along with

their respective search distances:

FEDERAL DATABASES

SEARCH RADIUS (in miles)

National Priorities List (NPL) - Identifies the nation's most hazardous sites that warrant further investigation. Sites are first identified as a CERCLIS Site and the degree of contamination determines whether the site will be included on the NPL. Also known as Superfund.

1.0

Delisted NPL – Sites deleted from the NPL where no further response is appropriate 0.5 Comprehensive Environmental Response. Compensation Liability Index System (CERCLIS) - Compilation of properties that the EPA has identified as having actual or suspected releases of contamination. The sites are reported to the EPA through states, municipalities, and private companies/citizens. Each site undergoes a series of reviews that determine the severity of the contamination from the discovery and preliminary assessment to the site inspection and the hazard ranking system, which will determine whether the site will be included on the NPL.

0.5

CERCLIS No Further Remedial Action Planned (CERC-NFRAP) - CERCLIS Sites where no further remedial action is planned at the federal level.

0.5

Corrective Action Report (CORRACTs) List - Includes hazardous waste handlers with RCRA corrective action activities.

1.0

Resource Conservation Recovery Act (RCRA) Treatment Storage and/or Disposal (TSD) Facilities - RCRA provides for the cradle to grave management of hazardous wastes by regulating the operations of those who operate treatment, storage or disposal facilities.

0.5

RCRA Large Quantity Generator (LQG) - RCRA provides for the management of properties that generate more than 1,000 kilograms of hazardous waste or over 1 kilogram of acutely hazardous waste per month.

property and

adjacent RCRA Small Quantity Generator (SQG) - RCRA provides for the management of properties that generate more than 100 kilograms and less than 1,000 kilograms of hazardous waste.

property and

adjacent RCRA Conditionally Exempt Small Quantity Generator (CESQG) - RCRA provides for the management of properties that generate less than 100 kilograms of hazardous waste or less than 1 kilogram of acutely hazardous waste per month.

property and

adjacentRCRA Non-Generators (NonGen) – Non-generators do not presently generate hazardous waste, but may have in the past.

property and

adjacentEmergency Response Notification Sites (ERNS) List - Records information about property

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FEDERAL DATABASES

SEARCH RADIUS (in miles)

reported releases of hazardous substances and/or petroleum products. These sites are maintained by the EPA and the MDEQ.

only

STATE/TRIBAL DATABASES SEARCH RADIUS (in miles)

State Hazardous Waste Sites (SHWS) - Known as Part 201 Sites in Michigan, SHWS are Michigan's equivalent to CERCLIS. The sites are reported to the State through municipalities, private companies/citizens. The State has developed a numerical ranking model for determining the present and potential hazard that each site poses to public health, safety, welfare and/or the environment. Each site is scored using this model once identified and annually thereafter.

1.0

State Landfill and/or Solid Waste Disposal Site List (SWF/LF) - Part 115 of Act 451, as amended, regulates and maintains an inventory of solid waste disposal facilities or landfills.

0.5

Leaking Underground Storage Tank (LUST) List - Part 213 of Act 451, as amended, regulates and details the corrective action required due to releases from leaking USTs. Part 213 also prescribes the powers and duties of certain State agencies and officials, and provides penalties and remedies.

0.5

Underground Storage Tank (UST) List - Part 211 of Act 451, as amended, regulates certain UST systems, requires the registration of certain UST systems, prescribes the powers and duties of certain state and local agencies and officials, imposes fees, and prescribes penalties and remedies.

property and

adjacent

Above Ground Storage Tank (AST) List - Listing of registered ASTs. property and

adjacent Activity and Use Limitations (AUL) – Sites with institutional control and/or engineering control.

property only

Brownfields - BEA or leaking UST sites which have been redeveloped by private entities using the BEA process.

0.5

U.S. Brownfields - List of brownfields properties addressed by Cooperative Agreement Recipients and/or Targeted Brownfields Assessments

0.5

Baseline Environmental Assessment (BEA) List - Sites which have been identified as a facility (i.e., soil and/or groundwater contamination exceeding Part 201 generic residential cleanup criteria) and BEA reports have been submitted to MDEQ.

0.5

Following review of the EDR report, a drive-through reconnaissance was conducted to

confirm the locations of the plotted and orphan sites. The following EDR-identified sites

were determined to be located in close proximity (i.e., less than one-eighth of a mile) to the

property and were further evaluated:

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x Riverview Trenton Railroad Company/The Jeneric Group, LLC, Coughlin FX Co.,

and Quality Mailing & Fulfillment (4000 West Jefferson Avenue): This site is

located approximately 150 feet west of the property and is an unimproved vacant land.

The site is listed in the RCRA-CESQG, RCRA-NonGen and BEA databases. According

to the EDR report, no RCRA compliance violations have been issued against the site.

A review of MDEQ files for this site contained a BEA report prepared by Stephens

Environmental LLC, dated January 27, 2011. The BEA report indicated that a Phase II

ESA was conducted to evaluate historical industrial uses of the site. The Phase II ESA

comprised of drilling six soil borings to depths of up to 16 feet and analysis of soil

samples. Subsurface conditions at the site comprised of up to 11.5 feet of fill soil

comprised of sandy soil with pieces of glass, brick, and wood. No groundwater was

encountered at the boring locations. The soil analytical data identified heavy metals,

volatile organic compounds (VOCs) and semi-VOCs (SVOCs) above Part 201 generic

residential cleanup criteria (GRCC). The site is located cross-gradient from the property

and no offsite migration of contamination was reported. Thus, this site is not considered

as an offsite source of potential environmental concern.

x General Mill Supply Co. (189 Vinewood Street): This site is located approximately

350 north of the property and is listed in the UST and LUST databases. According to

the EDR report, one 1,000-gallon gasoline UST was installed on March 25, 1966 and

removed on July 1, 1998; and one 6,000-gallon gasoline UST was installed on March

25, 1966 and removed on July 8, 1998. A gasoline release was reported on July 8, 1998

and the LUST incident was closed on August 15, 2000. Based on the closed LUST

status and its distance from the property, this site is not considered as an offsite source of

potential environmental concern.

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x Nicholson Terminal and Port of Detroit Property (4105 West Jefferson) and

Ambassador Port Company (4461 W. Jefferson): This site is located immediately to

the west of the property and is listed in the RCRA NonGen, UST and LUST databases.

The site is also listed in the BEA database. According to the EDR report, no RCRA

compliance violations have been issued for the site. According to the EDR report, one

10,000-gallon diesel UST and a 3,000-gallon gasoline UST were installed in 1976 and

both USTs were removed in 1997. The site contains one 10,000-gallon diesel UST and

one 2,500-gallon gasoline UST, which were installed in 1997. The existing USTs are

located over 800 feet southwest of the property.

MDEQ personnel could not locate the BEA report for this site, but had a copy of the

LUST closure report, dated March 1998, prepared by CEI Environmental (CEI). The

report indicated that 10,000-gallon and 3,000-gallon USTs were removed from the site.

The USTs were located over 1,000 feet southwest and down-gradient from the property.

A confirmed release was reported by CEI based on the presence of petroleum odors in the

excavated soils. On January 8, 1998, CEI completed a subsurface investigation at the site

with 16 geoprobe borings and 4 monitoring wells. The subsurface conditions at the site

comprised of up to 13 feet of sandy fill soil with construction debris and fly ash underlain

by native clayey soils. Groundwater was encountered at a depth of 4 to 6 feet. Thirteen

soil samples and four groundwater samples were submitted for laboratory analysis.

Elevated levels of lead and polynuclear aromatics (PNA) were detected throughout the

site. The soil contamination was determined by CEI to be associated with fill soil at the

site. Based on its close proximity, the neighboring site is considered as an offsite source

of potential environmental concern and an REC.

x DIB Detroit LLC (215 Vinewood): This site is located approximately 600 feet north of

the property and is listed in the BEA database. A review of MDEQ files for this site

contained a BEA report prepared by Stephens Environmental LLC, dated January 19,

2012. The BEA report included information on the subsurface investigation at the

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property, which comprised of four borings and analysis of soil samples. The soil

conditions at the site comprised of up to 7.5 feet of sandy fill soil with slag, foundry sand

and brick underlain by native clayey soils. No groundwater was encountered in the

borings. Analytical results identified heavy metals above Part 201 GRCC. Considering

its distance and lack of shallow groundwater, this site is not considered as an offsite

source of potential environmental concern.

x City of Detroit Riverside Park (3621 West Jefferson): This site is located immediately

east of the property and is listed in the RCRA NonGen database. According to the EDR

report, no RCRA compliance violations have been issued for the site.

In 2001, NTH was retained by the City of Detroit to conduct a Preliminary

Environmental Assessment (PEA) of the park and in the proximity of a former coal

gasification plant. The study was requested due to the evidence of contaminated soils

discovered during a geotechnical investigation for construction of a concrete walkway at

the southern portion of the park, along the Detroit River. The PEA comprised of drilling

19 geoprobe borings and installation of four groundwater monitoring wells. The

subsurface conditions at the explored locations comprised of up to 20 feet of fill material

containing pieces of concrete, brick, slag, coal, metal, glass and wood. Groundwater was

encountered at each boring at depths of about 6 and 13 feet. The soil and groundwater

analyses identified heavy metals, VOCs and PNAs above Part 201 GRCC. Based on its

close proximity and up gradient location, this site is considered as an offsite source of

potential environmental concern and an REC.

x O-J Transport Co and Former John James Site (4005-4117 W. Fort Street): This

site is located approximately 480 feet northwest of the property and is listed in the UST,

LUST and Brownfield databases. According to the EDR report, two 10,000-gallon diesel

USTs were removed from the site on November 9, 2006. A diesel release was reported

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on February 27, 2007. Considering that its distance and down-gradient location, this site

is not considered as an offsite source of potential environmental concern.

x Detroit City Gas Company Station (Jefferson Avenue): This site is located

approximately 650 feet northeast of the property and is listed as a manufactured gas

plant. Manufactured gas sites typically produces combustible gas from coke, coal, and

oil. These types of plants yield large quantities of hazardous byproducts including tars,

sludges, oils and other chemicals, which were typically disposed of in unlined pits at the

site. MDEQ had no records for this site. Considering its distance from the property, this

site is not considered as an offsite source of potential environmental concern.

x 24th Street Incinerator (3565 West Jefferson): This site is located approximately 550

feet northeast of the property and is listed in the Historical Landfill database. MDEQ had

no records for this site. Considering its distance from the property, this site is not

considered as an offsite source of potential environmental concern.

The remaining EDR-identified sites are located more than one-eighth of a mile from the

property; thus, based on the considerable distances and known subsurface conditions in the

area, these sites are not expected to have a negative environmental impact on the property.

4.3 Historical Use Information

A historical search was conducted to determine the previous uses of the property. Only

historical sources, which could be reasonably ascertained and judged likely to be useful, were

obtained and reviewed during the current study. The following sections present the results of

the historical searches conducted during this study.

4.3.1 Local Governmental Agency Records

A visit was made to the City of Detroit municipal offices to review readily available records

for the property.

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Assessor’s Records

The assessment records identified the property by Parcel No. 14000001-3 and its address as

3801 West Jefferson Avenue. The property is recorded as approximately 4.71 acres in size

and contains a warehouse building that is approximately 80,116 square feet in size. The

building was constructed in 1949 and 1970. Additionally, the available records indicate that

Detroit Newspaper Agency sold the property to Detroit International Bridge Co. on

September 22, 2006.

Buildings, Safety Engineering & Environmental Department

Buildings, Safety Engineering & Environmental Department (BSEED) did not have any

records indicative of environmental concerns at the property.

Fire Department

City of Detroit Fire Department (DFD) records for the property included an inspection report

dated June 27, 1949 for the installation of one 1,000-gallon gasoline UST. The UST was

installed for Detroit Evening News Terminal under the building and at 96 feet from the

nearest property line (no direction was provided). A letter dated June 26, 1987 indicated that

on June 24 and 25, 1987, Parks Installation Co. filled one 1,000-gallon tank will lean

concrete. MDEQ has no records of this 1,000-gallon UST.

4.3.2 Sanborn Fire Insurance Maps

NTH retained EDR to conduct a search of Sanborn fire insurance maps for the property.

Sanborn maps are primarily used by insurance companies to assess fire risks, and when

available for a particular property can provide relevant information about its history.

Thirteen maps covering the property, dated 1884, 1897, 1918, 1921, 1950, 1952, 1957, 1961,

1977, 1988, 1991, 1996, and 2002 were provided by EDR. Copies of these maps are included

in Appendix E.

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A review of the referenced Sanborn maps is summarized in the following table:

Year Prominent Features 1884 The property is depicted as part of the Detroit River with a log boom, a lumber dock owned by

Morton & Backus, and another lumber dock. West Jefferson Avenue is identified as West Woodbridge Street.

1897 The majority of the property is depicted as part of the Detroit River and some portions of the property have been filled. Five boat houses and a boat building with a bridge to another boat house are depicted on the northern portion of the property. A vacant dock is depicted on the western portion of the property.

1918 Additional portions of the property has been filled. One residential dwelling and an office building are depicted on the northern portion of the property and Grace Harbor Lumber Co. is depicted on the western portion of the property.

1921 Additional portions of the property have been filled. One residential dwelling and an office building are depicted on the northern portion of the property and Great Lakes Navigation Co. Docks is depicted on the western portion of the property.

1950 The entire property has been filled or reclaimed. The eastern portion of the existing building is identified as Commercial Marine Terminal and The Detroit Evening News Association. The building is divided into a paper warehouse, shipping and receiving, office and lockers and an “oil house.” Champion Fuel Co. with an office building and a coal yard is depicted on the western portion of the property.

1952 Similar features as depicted on the 1950 map. 1957 Similar features as depicted on the 1952 map.1961 Similar features as depicted on the 1957 map.1977 The existing building identified as Commercial Marine Terminal and The Detroit Evening News

Association. The building is divided into a paper warehouse, shipping and receiving, office and lockers and an oil house. The west building addition was constructed in 1970 and is identified as warehouse. The western portion of the property is depicted as vacant land.

1988 Similar features as depicted on the 1977 map.1991 Similar features as depicted on the 1988 map. 1996 Similar features as depicted on the 1991 map. 2002 Similar features as depicted on the 1996 map.

4.3.3 City Directories

NTH reviewed historic address directories dating back to 1888 (i.e., the date of the earliest

directory) for the property address at Bressers Company and City of Detroit Public Library to

determine past occupants. The following tables summarize information on listed past

property occupants:

Year Occupants 2014 Metro International Trade Services 2009 Detroit News Warehouse

1994-2004 No listing 1959-1993 Commercial Marine Terminal 1888-1954 No listing

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4.3.4 Aerial Photographs

NTH obtained copies of historical aerial photographs dated 1937, 1949, 1952, 1956, 1961,

1966, 1972, 1981, 1983, 1997, 1999, 2005, 2009, 2010, and 2012 from EDR. Additional

aerial photographs dated 1999, 2002, 2005, 2007 and 2010 were reviewed on the Google

webpage. These aerial photographs were reviewed to determine past uses and changes in

surface features that might indicate possible environmental concerns.

The scales on the aerial photographs range from 1” = 100’ to 1” = 500’. Thus, certain

photographs, particularly those with larger scales, did not clearly identify all the surface

features at the property.

A review of the above aerial photographs is summarized below.

Year Scale Prominent Features 1937 1” = 500’ Unidentified building in the northeast corner of the property. The remainder of the

property is covered with mounds of soil or coal. A portion of the central portion of the property is part of the Detroit River and has not been filled or reclaimed.

1949 1” = 500’ The eastern existing building is under construction. The remainder of the property is covered with mounds of soil or coal.

1952 1” = 500’ The eastern existing building and two large coal mounds. 1956 1” = 500’ The eastern existing building and vacant land. 1961 1” = 500’ Similar features as depicted on the 1956 aerial photograph. 1966 1” = 500’ The eastern existing building with a crane and unknown materials on the western portion

of the property. 1972 1” = 500’ Existing building, parking lot and vacant land. 1981 1” = 500’ Similar features as depicted on the 1972 aerial photograph. 1983 1” = 500’ Similar features as depicted on the 1981 aerial photograph. 1997 1” = 500’ Similar features as depicted on the 1983 aerial photograph. 1999 1” = 100’ Similar features as depicted on the 1997 aerial photograph. 2002 1” = 100’ Similar features as depicted on the 1999 aerial photograph. 2005 1” = 100’ Similar features as depicted on the 2002 aerial photograph. 2007 1” = 100’ Similar features as depicted on the 2005 aerial photograph. 2009 1” = 500’ Similar features as depicted on the 2007 aerial photograph. 2010 1” = 100’ Similar features as depicted on the 2009 aerial photograph. 2012 1” = 500’ Similar features as depicted on the 2010 aerial photograph.

4.3.5 USGS Topographic Maps

Historical USGS “Grosse Pointe, Michigan” topographic maps dated 1936, 1940, 1947, 1952,

1968, 1973, 1980 were reviewed to determine past uses of or changes in the surface features

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at the property. The 1936 map depicts the property as vacant land. The 1940 and 1952 maps

depict three unknown structures on the northern portion of the property. The 1968 depicts the

eastern portion of the existing building and the remainder of the property as vacant land. The

1973 and 1980 maps depict the existing building and vacant land.

4.3.6 Past Use Summary

The historical research to determine the past uses of the property was conducted in

accordance with ASTM Practice E1527-13. The following table summarizes the past uses of

the property:

Year Property Uses Sources RECs

1884-1890 Detroit River with docks Sanborn maps and street address directories

None

1890-1918 Detroit River and boat houses Aerial photographs, Sanborn maps, street address

directories and municipal records.

None

1918-1930s Detroit River, residential, office and lumber company

and docks

Sanborn maps and street address directories

None

1930s-1949 Residential and coal yard Aerial photographs, Sanborn maps, and street address

directories

Unknown origin of backfill material to fill Detroit River

and coal storage 1949-1970s Newspaper warehouse with

oil house, UST, and coal yard Aerial photographs, Sanborn

maps, street address directories, and municipal

records

Unknown origin of backfill material to fill Detroit River,

oil house, UST and coal storage

1970s-1987 Newspaper warehouse with oil house and UST

Aerial photographs, Sanborn maps, street address

directories, and municipal records

Same as above

1987-2006 Newspaper warehouse with oil house

Aerial photographs, Sanborn maps, street address

directories, and municipal records

Unknown origin of backfill material to fill Detroit River,

and oil house

2006-Present

Warehouse Aerial photographs, street address directories, municipal

records

Unknown origin of backfill material to fill Detroit River

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4.4 Historical Uses of Adjoining Properties

Past uses of adjacent properties, as determined through a review of the previously referenced

historical Sanborn maps and aerial photographs, are as follows:

Year Source North East South West 1884 Sanborn Foundry and

machine shop, log boom, hair storage, and carbon works

warehouse

Detroit River and lumber docks

Detroit River Lumber docks and Detroit River

1897 Sanborn Vacant buildings and carbon works

warehouse

Detroit River Same as above Vacant docks and Detroit River

1919 Sanborn Lumber company, residential dwelling

and dye storage building

No coverage Same as above Lumber company

1921 Sanborn Lumber company and storage warehouse

Park Same as above Same as above

1937 Aerial Vacant land and storage warehouse

Same as above Same as above Several ASTs

1949 Aerial Same as above Same as above Same as above Coal storage 1950 Sanborn Same as above No coverage Same as above Coal yard 1952 Sanborn,

Aerial Same as above Park Same as above Same as above

1956 Aerial Trucking company buildings and

storage warehouse

Same as above Same as above Same as above

1957 Sanborn Same as above No coverage Same as above Same as above 1961 Sanborn,

Aerial Same as above Park Same as above Same as above

1966 Aerial Same as above Same as above Same as above Commercial building and

material storage 1972 Aerial Same as above Same as above Same as above Same as above 1977 Sanborn Same as above No coverage Same as above Scrap metal yard1981 Aerial Same as above Park Same as above Commercial

building and material storage

1983 Aerial Same as above Same as above Same as above Same as above 1988 Sanborn Vacant warehouse

and storage warehouse

No coverage Same as above Scrap metal yard

1991 Sanborn Warehouse and storage warehouse

Same as above Same as above Same as above

1996 Sanborn Same as above Same as above Same as above Warehouse 1997 Aerial Same as above Same as above Same as above Same as above

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Year Source North East South West 1999 Aerial Same as above Same as above Same as above Same as above 2002 Sanborn,

Aerial Same as above Same as above Same as above Same as above

2005 Aerial Same as above Same as above Same as above Same as above 2007 Aerial Same as above Same as above Same as above Same as above 2009 Aerial Same as above Same as above Same as above Same as above 2010 Aerial Same as above Same as above Same as above Same as above 2012 Aerial Vacant land and

storage warehouse Same as above Same as above Same as above

5.0 SITE RECONNAISSANCE

A site reconnaissance of the property was conducted to observe surface features indicative of

RECs.

5.1 Location and Legal Description

The property is located in the Northeast ¼ of Section 24, Township 1 South, Range 11 East,

Detroit, Wayne County, Michigan. A map showing the location of the property is presented

as Figure 1 in Appendix A of this report. The legal description of the property, obtained from

City of Detroit, is included in Appendix A.

5.2 Site Vicinity and Characteristics

The property is located in a recreational and industrial use area, which is serviced by the

municipal potable water supply and sanitary sewer systems provided by Detroit Water and

Sewerage Department, as well as natural gas and electric utilities.

5.3 Current Uses of the Property

The property is occupied by Metro International and is used to store aluminum ingots.

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5.4 Description of Structures, Roads and Other Improvements

The improvements at the property include a warehouse building, paved parking lot, paved

ship dock with two overhead cranes, steel seawall and railroad spur within the building.

5.5 Current Uses of Adjoining Properties

During the visual survey, the adjoining properties were observed and identified from the

boundaries of the property and readily accessible public right-of-ways. Observed land uses at

the adjoining properties are listed below:

Locations Features Environmental

Concerns North, across W. Jefferson

Avenue Vacant land and Composite Forgings None noted

East Riverside Park None noted South Detroit River None noted West Port of Detroit, Nicholson Terminal None noted

5.6 Methodology and Limiting Conditions

A visual survey of the property was conducted on May 7, 2015 by Jesse Veenkant of NTH.

Access to the property was provided by John Hochstein of Stephens Environmental LLC

(SE), the property owner’s consultant. Mr. Veenkant was accompanied by Joe Jeffery of

Metro International and Mr. Hochstein with during the visual survey of the building.

During the survey, the property was observed for evidence of RECs such as stressed

vegetation, stained surface soil, and improper waste disposal practices. The visual survey was

conducted by walking the interior of the building, the perimeter of the property, and randomly

traversing the property, where accessible. The following limiting conditions were

encountered during the visual survey:

x Aluminum ingot and other items in the building obscured observations of surface

features.

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x Parked vehicles in the parking lot obscured observations of surface features.

x Portions of the building had limited lighting which obscured observations of surface

features in those areas.

x A door on the north side of the building was locked and that area could not be accessed.

The above limiting conditions impeded observations of surface features but are not expected

to significantly affect NTH’s ability to render an opinion regarding the property.

5.7 General Site Setting

The property is located in a recreational and industrial use area. A map showing the location

of the property is presented as Figure 1 in Appendix A of this report. The approximate

configuration of the property, along with prominent surface features observed by NTH during

the recent site visit, is shown on Figure 2 included in Appendix A. This plan was prepared

from a recent aerial photograph and observations made during the visual survey. NTH’s site

plan should be considered as a preliminary reference drawing and should not be used as a

legal boundary survey. Color photographs of the property taken during the visual survey are

included in Appendix B.

5.8 Exterior Observations

The warehouse building, paved parking lot and paved ship dock is located on the east portion

of the property (Photographs 1 and 2). A railroad spur enters the building from the northeast

corner (Photograph 3). The western portion of the property is grass-covered (Photograph 4).

The ship dock contains two overhead cranes and metal carts (Photograph 5). Stacked railroad

ties were noted on the west side of the building (Photograph 6). A refuse dumpster and

storage rack containing propane gas cylinders used for forklift are located in the parking lot

(Photograph 7). No evidence of material spillage or leakage was observed around the

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dumpster at the time of the visual survey. One vent pipe was noted on the north exterior wall

of the building, approximately 200 feet southwest of the northeast corner (Photograph 8).

The significance of this pipe is unknown.

The following evidence of RECs was noted on the exterior portions of the property during the

visual survey on May 7, 2015:

x A vent pipe possibly associated with former equipment or 1,000-gallon closed-in-place

gasoline UST.

x Stored railroad ties on the east side of the building.

5.9 Interior Observations

The warehouse building is a single-story, slab-on-grade structure with a mezzanine. The

mezzanine is comprised of offices and restrooms (Photograph 9). The warehouse is used to

store aluminum ingots and is comprised of storage room, railroad car loading and unloading

area, office, restrooms, break room, boiler room (inactive), mechanical room (former oil

house) and an office (Photographs 10 through 13). The storage room contains tools, office

supplies, cleaning supplies and automotive fluids (Photographs 14 and 15). No evidence of

material spillage or leakage was noted near the containers. The mechanical room contains

tools, a scale, and propane tanks (Photograph 16).

The following evidence of RECs was noted in the accessible portions of the building during

the visual survey on May 7, 2015:

x Railroad spur in the building.

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5.10 Storage Tanks

A vent pipe was noted on the north side of the building. Municipal records indicated that a

1,000-gallon gasoline UST was installed in the building in 1949 and was closed-in-place in

1987. No other details on this UST were readily available.

5.11 Polychlorinated Biphenyls (PCBs)

The property was surveyed to identify liquid-cooled electrical units, such as transformers and

capacitors. These types of units are of possible concern because they may be potential PCB

sources. PCB units may subject the owner/operator to various regulatory requirements under

Toxic Substances Control Act (TSCA). The release of PCB fluids or their combustion

products (in case of spill or fire) are potential environmental liabilities and may require costly

remediation. Two-pole-mounted electrical transformers were observed on the east side of the

building. Labels on the transformers indicated that they are “Non-PCB” units.

6.0 INTERVIEWS

Interviews were conducted with various individuals to determine historical uses of the

property and to determine environmental concerns associated with the property.

6.1 Property Owner Information

NTH’s Phase I ESA Owner’s Questionnaire was completed by Todd White of Crown

Enterprises. A copy of the completed questionnaire is included in Appendix F.

Mr. White indicated that the building is owned by Riverview Trenton Railroad Company, a

subsidiary of Crown Enterprises since last 4 to 5 years. The property is occupied by Metro

International for storage of aluminum ingots and was formerly used as Detroit News

warehouse. The original portion of the building was constructed in 1949 with additions

constructed in about 1952 and 1972. The building is heated by natural gas.

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Mr. White provided information on a subsurface investigation conducted at the property in

March 2015 by SE. The information included boring location plan, boring logs, analytical

summary table and summary memo. The subsurface investigation comprised of six soil

borings to depths of up to 20 feet and analyses of soil samples. The borings were located

within the grass-covered southern and western portions of the property. The subsurface

conditions at the boring locations consisted of up to 4 feet of sandy fill soil with asphalt

millings, slag and brick fragments. The fill was underlain by native sands and clays.

Groundwater was encountered in two borings at a depth of approximately 11 feet. The boring

logs indicated that insufficient amount of groundwater was encountered for sampling

purposes. Analytical results identified heavy metals and polynuclear aromatics above Part

201 GRCC. SE concluded that the metals are consistent with background levels found in

Detroit area. Furthermore, the detected PNAs were determined to be associated with the

asphalt millings in the fill soil. Based on this analytical data, the property is a “facility” as

defined by 1994 P.A. 451, Part 201, as amended. According to Section 20101(1)(s) of Part

201 of NREPA (1994 P.A. 451, as amended), "Facility” means any area, place, or property

where a hazardous substance in excess of the concentrations that satisfy the cleanup criteria

for unrestricted residential use has been released, deposited, disposed of, or otherwise comes

to be located.

No rationale for selecting the boring locations was provided. The depth of fill soil reported

on the boring logs appears to be much shallower than those found on the westerly adjacent

site, especially when the property was reclaimed from Detroit River. Groundwater was

encountered in two borings that were located farthest from the river. As such, the limited data

provided by the property owner does not provide sufficient information to evaluate subsurface

conditions at the property.

6.2 Interview with Site Manager

Refer to Section 6.1.

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6.3 Interviews with Occupants

Mr. Jeffery indicated that the property is used for storage of aluminum ingots and is occupied

by Metro International for the past 18 months. Mr. Jeffery is not aware of the UST inside the

building and any RECs at the property.

6.4 Interviews with Local Government Officials

Information obtained from local government offices is described in appropriate sections

throughout this report.

7.0 EVALUATIONS

7.1 Findings and Opinions

The property was part of the Detroit River and reclaimed between 1890s and the early 1930s.

Between 1890s and 1930s, the property was occupied by ship docks, a residential dwelling,

boat houses and an office for a lumber yard. From the early 1930s to about 1949, the property

was occupied by a residential dwelling and coal yard. The coal yard remained at the property

until the mid-1970s. In 1949, the east portion of the existing building was constructed with a

1,000-gallon gasoline UST, oil house and railroad spur. An addition was constructed to the

building in 1970. Between 1949 and about 2006, the building was operated as the Detroit

Newspaper warehouse. Since about 2006, the property has been used for storage of

aluminum ingots. No information on the origin, type and environmental status of the backfill

material used to reclaim the property was readily available, which is an REC.

The property was occupied by lumber company, coal yard and warehouse with an oil room.

No information was readily available regarding the past occupants, hazardous material

handling, storage or waste disposal practices implemented on the premises. Thus, these past

uses of the property are RECs.

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A railroad spur is located within the building. Additionally, railroad ties are stored on the east

side of the building. Typically, heavy metals, PCBs and creosote are associated with

railroads. As such, the presence of the railroad spur and ties are an REC.

Municipal records indicate that one 1,000-gallon gasoline UST was installed in the building

in 1949. In 1987, the UST was filled with lean concrete and closed in-place. The only

information available for the UST was that it was located 96 feet from the nearest property

line (specific property boundary is unknown). During the visual survey, a vent pipe was

noted on the north side of the building, approximately 200 feet southwest of the northeast

corner of the building. It is unknown if this vent pipe is associated with the 1,000-gallon UST

or any previous equipment in the building. No documentation on the UST closure was

readily available. Thus, the UST and vent pipe are RECs.

In 2015, a subsurface investigation was conducted at the property. Based on analytical

results, the property is a facility, as defined in Part 201 rules of MI PA 451.

Extensive fill soil with soil and water contamination exceeding Part 201 GRCC was identified

at the easterly and westerly adjacent sites. Based on their close proximity, these neighboring

sites are considered as an offsite sources of potential environmental concern and RECs.

No historical RECs, controlled RECs (CRECs), de minimis conditions or significant data

gaps were identified at the property.

Based on the results of this Phase I ESA, an additional environmental due diligence study

(i.e., Phase II ESA) to evaluate the above RECs and understand future owner’s continuing

obligations under Part 201 is warranted for the property.

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7.2 Conclusions

We have performed a Phase I Environmental Site Assessment in conformance with the scope

and limitations of ASTM Practice E1527-13 for the 3801 West Jefferson Property in Detroit,

Wayne County, Michigan. Any exceptions to, or deletions from, this practice is described in

appropriate sections throughout this report. This assessment has revealed no evidence of

recognized environmental conditions in connection with the property, except for the

following:

x The property was formerly a part of Detroit River and was reclaimed to support the

current development. No information on the backfill soil used for land reclamation

purposes is readily available. As such, the environmental nature and origin of the

backfill soil are unknown.

x Past uses of the property include lumber yard, coal yard and warehouse with an oil house.

No information is readily available regarding the past occupants’ hazardous material

handling, storage or waste disposal practices implemented on the premises.

x Railroad spur is located at the property and railroad ties were noted to be stored east of

the building.

x One underground storage tank (UST) was located inside the building and is reportedly

closed-in-place. No information is available to evaluate the environmental status of the

UST and surrounding soils.

x One vent pipe was noted on the north exterior wall of the building. The significance of

this pipe could not be determined.

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x Based on the information provided by the current property owners regarding a previous

subsurface investigation, the property is a “facility” as defined by Part P.A. 451, Part

201, as amended.

x Soil and/or groundwater contamination was identified on the westerly and easterly

adjacent sites.

8.0 ADDITIONAL SERVICES

No additional or non-ASTM Practice E1527-13 scope items were requested by the City of

Detroit during the current study.

9.0 REFERENCES

1) American Society for Testing and Materials (ASTM) Designated: E1527-13 – Standard

Practice for Environmental Site Assessments: Phase I Environmental Site Assessment

Process.

2) Environmental Data Resources, Inc. (EDR):

x Radius Map Report

x Sanborn Maps

x Aerial Photography

x Topographic maps

x City Directory

3) United States Department of Agricultural (USDA) Soil Survey of Wayne County Area,

Michigan

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4) Department of Geology, College of Arts and Sciences, Western Michigan University -

Hydrogeologic Atlas of Michigan

5) Department of Geological Sciences, The University of Michigan – Quaternary Geology of

Southern Michigan

6) City of Detroit – Municipal Offices (Assessment, BSEED & DFD)

7) Google Earth website (aerial photographs)

8) MDEQ - Remediation Division website for environmental liens

9) MDEQ records for various sites in the area

10) Stephens Environmental LLC - subsurface investigation documents

11) Raymond Scott (User Representative)

12) Todd White (Owner Representative)

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APPENDIX ASITE LOCATION PLAN, FIGURE 1;SITE PLAN, FIGURE 2; ANDLEGAL DESCRIPTION

Page 56: Baseline Environmental Assessment for Riverside Park

NTH Consultants, Ltd. Professional Engineering & Environmental Services

Northville · Detroit · Cleveland · Indianapolis · Grand Rapids · Lansing

PROJECT NO. 62-140614-100

DRAWN BY: JAV

CHECKED BY:

LOCATION: 3801 West Jefferson Property Detroit, Michigan

TITLE: Site Location Map

DATE: 5/11/2015

SHEET: 1 OF 1

FIGURE NO:

1

SITE

Page 57: Baseline Environmental Assessment for Riverside Park

5176*�5

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APPENDIX BPROPERTY PHOTOGRAPHS

Page 61: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�1:��North�and�east�side�of�the�warehouse�building�

�������Photograph�2:��South�portion�of�the�property�and�east�side�of�the�warehouse�building�

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PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�3:��Railroad�entrance�at�northeast�corner�of�the�building�

�������Photograph�4:��Western�portion�of�the�property�

Page 63: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�5:��Ship�dock,�overhead�cranes�and�metal�carts�

�������Photograph�6:��Stacked�railroad�ties�

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PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�7:��Propane�storage�racks�

��������Photograph�8:��Vent�pipe�on�north�side�of�the�building�

Page 65: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�9:��Mezzanine�office�

�������Photograph�10:��Stored�aluminum�ingots�

Page 66: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

������Photograph�11:�Railroad�box�car�loading�area�

�������Photograph�12:�Office�area�

Page 67: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

������Photograph�13:�Boiler�room�

�������Photograph�14:�Storage�room�

Page 68: Baseline Environmental Assessment for Riverside Park

PROPERTY�PHOTOGRAPHS�NTH�Project�No.�62Ͳ140614Ͳ100�

�������Photograph�15:�Stored�automotive�and�cleaning�fluids�in�the�storage�room�

������Photograph�16:�Mechanical�room��

Page 69: Baseline Environmental Assessment for Riverside Park

APPENDIX CUSER QUESTIONNAIRE

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APPENDIX DEDR RADIUS MAP REPORT

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FORM-LBC-HRM

®kcehCoeG htiw tropeR ™paM suidaR RDE ehT

6 Armstrong Road, 4th floorShelton, CT 06484Toll Free: 800.352.0050www.edrnet.com

3801 W. Jefferson Aveune Property3801 W. Jefferson AveuneDetroit, MI 48216

Inquiry Number: 4278659.2sApril 29, 2015

Page 74: Baseline Environmental Assessment for Riverside Park

SECTION PAGE

Executive Summary ES1

Overview Map 2

Detail Map 3

Map Findings Summary 4

Map Findings 8

Orphan Summary 91

Government Records Searched/Data Currency Tracking GR-1

GEOCHECK ADDENDUM

Physical Setting Source Addendum A-1

Physical Setting Source Summary A-2

Physical Setting Source Map A-7

Physical Setting Source Map Findings A-8

Physical Setting Source Records Searched PSGR-1

TC4278659.2s Page 1

Thank you for your business.Please contact EDR at 1-800-352-0050

with any questions or comments.

Disclaimer - Copyright and Trademark NoticeThis Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental DataResources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist fromother sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTALDATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION,MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALLENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE,ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL,CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLYLIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings,environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, norshould they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase IEnvironmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for anyproperty. Additionally, the information provided in this Report is not to be construed as legal advice.

Copyright 2015 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in wholeor in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All othertrademarks used herein are the property of their respective owners.

TABLE OF CONTENTS

Page 75: Baseline Environmental Assessment for Riverside Park

EXECUTIVE SUMMARY

TC4278659.2s EXECUTIVE SUMMARY 1

A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR).The report was designed to assist parties seeking to meet the search requirements of EPA’s Standardsand Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice forEnvironmental Site Assessments (E 1527-13) or custom requirements developed for the evaluation ofenvironmental risk associated with a parcel of real estate.

TARGET PROPERTY INFORMATION

ADDRESS

3801 W. JEFFERSON AVEUNEDETROIT, MI 48216

COORDINATES

42.3111000 - 42˚ 18’ 39.96’’Latitude (North): 83.0816000 - 83˚ 4’ 53.76’’Longitude (West): Zone 17Universal Tranverse Mercator: 328440.7UTM X (Meters): 4686202.5UTM Y (Meters): 577 ft. above sea levelElevation:

USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY

42083-C1 DETROIT, MI CA08Target Property Map:1980Most Recent Revision:

AERIAL PHOTOGRAPHY IN THIS REPORT

20120629Portions of Photo from:USDASource:

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4278659.2s Page 2

39 DET/WAYNE CO PORT AU 4300, 4461, & 4500 W INVENTORY Higher 1378, 0.261, SW

H38 FORMER JOHN JAMES SI 4005-4117 WEST FORT US BROWNFIELDS, FINDS Higher 1288, 0.244, NW

H37 4005 W FORT ST EDR US Hist Auto Stat Higher 1288, 0.244, NW

H36 O-J TRANSPORT CO 4005 W FORT ST RCRA NonGen / NLR, FINDS, INVENTORY, LUST, UST,... Higher 1288, 0.244, NW

G35 NEITZER HENRY J 705 25TH EDR US Hist Cleaners Higher 1265, 0.240, North

H34 PEZZANI & REID EQUIP 3960 W FORT ST LUST, UST, WDS Higher 1254, 0.237, NW

H33 PEZZANI AND REID EQU 3960 W FORT ST RCRA NonGen / NLR, FINDS Higher 1254, 0.237, NW

G32 CARRIERE LESTER J 3650 W FORT EDR US Hist Auto Stat Higher 1228, 0.233, North

G31 REEDYS MARATHON (FOR 3650 W FORT ST INVENTORY, LUST, UST, WDS Higher 1223, 0.232, North

G30 FORT BOULEVARD SHELL 3650 W FORT ST EDR US Hist Auto Stat Higher 1223, 0.232, North

F29 ACTON S SUPER SERVIC 3910 W FORT EDR US Hist Auto Stat Higher 1223, 0.232, NW

28 DETROIT CITY GAS CO- W. JEFFERSON AND 24T EDR MGP Higher 1201, 0.227, NNE

E27 NONE-VACANT LAND 401 SCOTTEN AVE INVENTORY, LUST, UST Higher 1191, 0.226, WNW

F26 BRENNAN SUPER SERVIC 3858 W FORT EDR US Hist Auto Stat Higher 1186, 0.225, NNW

F25 BRENNAN SERVICE STAT 3858 W FORT ST EDR US Hist Auto Stat Higher 1182, 0.224, NNW

F24 WARHURST HERSCHEL E 3841 W FORT EDR US Hist Auto Stat Higher 1178, 0.223, NNW

F23 BRENNAN LEO F 3800 W FORT EDR US Hist Auto Stat Higher 1172, 0.222, NNW

F22 DAN 0 MARATHON SERVI 3800 W FORT ST EDR US Hist Auto Stat Higher 1164, 0.220, NNW

F21 HOLZBAUGH GEORGE INC 3845 W FORT EDR US Hist Auto Stat Higher 1164, 0.220, NNW

D20 CULLON ALEXANDRINE P 243 24TH EDR US Hist Auto Stat Higher 1074, 0.203, NNE

E19 VACANT LAND 261 SCOTTEN INVENTORY, LUST, UST Higher 1023, 0.194, West

18 FIRE DEPT ENGINE #16 101 24TH ST UST Higher 857, 0.162, NNE

D17 24TH STREET INCINERA 3565 W JEFFERSON AVE HIST LF Higher 839, 0.159, NNE

C16 CITY OF DETROIT RIVE 3621 W JEFFERSON AVE RCRA NonGen / NLR, FINDS Higher 693, 0.131, NNE

C15 DETROIT CITY GAS CO- W. JEFFERSON EDR MGP Higher 629, 0.119, North

14 GREAT LAKES WATER BL 4120 W JEFFERSON AVE UST Higher 486, 0.092, WSW

13 CAPITOL TRUCKING INC 80 W GRAND BLVD LUST, UST, WDS Higher 420, 0.080, North

B12 DIB DETROIT LLC 215 VINEWOOD INVENTORY Higher 336, 0.064, NNW

B11 DIB DETROIT LLC 215 VINEWOOD BEA, WDS Higher 336, 0.064, NNW

A10 PORT OF DETROIT PROP 4105 W JEFFERSON AVE INVENTORY, LUST, UST, WDS Higher 327, 0.062, WSW

A9 NICHOLSON TERMINAL 4105 W JEFFERSON RCRA NonGen / NLR, FINDS Higher 327, 0.062, WSW

B8 GENERAL MILL SUPPLY 189 VINEWOOD ST INVENTORY, LUST, UST, WDS Higher 302, 0.057, NNW

A7 JENERIC GROUP, LLC T 4000 JEFFERSON AVENU BEA Higher 301, 0.057, West

A6 QUALITY MAILING & FU 4000 W JEFFERSON RCRA-CESQG, FINDS Higher 301, 0.057, West

A5 COUGHLIN FX CO 4000 W JEFFERSON AVE RCRA NonGen / NLR Higher 301, 0.057, West

A4 RIVERVIEW TRENTION R 4000 WEST JEFFERSON INVENTORY Higher 268, 0.051, WSW

B3 102 VINEWOOD ST EDR US Hist Auto Stat Higher 180, 0.034, NNW

A2 RIVERVIEW TRENTON RA 4000 WEST JEFFERSON BEA Higher 152, 0.029, WSW

A1 RIVERVIEW TRENTON RA 4000 WEST JEFFERSON INVENTORY Higher 152, 0.029, WSW

MAPPED SITES SUMMARY

Target Property Address:3801 W. JEFFERSON AVEUNEDETROIT, MI 48216

Click on Map ID to see full detail.

MAP RELATIVE DIST (ft. & mi.)ID DATABASE ACRONYMS ELEVATION DIRECTIONSITE NAME ADDRESS

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4278659.2s Page 3

72 HUBBARD-RICHARD HOUS 2661 BAGLEY STREET DEL PART 201 Higher 4749, 0.899, North

71 MI DEPT/TRANSPORTATI 5851 W JEFFERSON AVE CERC-NFRAP, RCRA NonGen / NLR, PART 201,... Higher 4317, 0.818, SW

70 WELCOME CENTER DEVEL NEAR VERNOR AND BAGL PART 201, INVENTORY, BROWNFIELDS Higher 3736, 0.708, North

69 CSX/NORFOLK & WESTER JEFFERSON AND 12TH S INVENTORY, PART 201 Higher 3310, 0.627, NE

68 AMBASSADOR BRIDGE CU HOWARD AND 21ST STRE INVENTORY, PART 201 Higher 3250, 0.616, North

O67 LETTS DROP FORGE 2714 W JEFFERSON AVE RCRA NonGen / NLR, ICIS, FINDS, PART 201,... Higher 2647, 0.501, NE

66 ARTIC RENTALS PROPER 4629 FORT ST LUST, UST Higher 2561, 0.485, West

O65 2781 CORPORATION 2781 WEST JEFFERSON BEA Higher 2531, 0.479, NE

N64 100 S. SUMMIT ST. INVENTORY Higher 2469, 0.468, WSW

N63 100 S. SUMMIT ST. BEA Higher 2469, 0.468, WSW

62 MI DEPT/NATURAL RESO 271 S SUMMIT ST CERCLIS, RCRA NonGen / NLR Higher 2458, 0.466, SW

M61 FORMER NICHOLSON TER 4685 W JEFFERSON INVENTORY, LUST, UST, WDS Higher 2440, 0.462, SW

60 AREF BAZZI 747 CLARK ST LUST, UST, WDS Higher 2318, 0.439, WNW

M59 ANACONDA BRASS 4610 W. JEFFERSON PART 201, INVENTORY, BROWNFIELDS Higher 2317, 0.439, SW

M58 ANACONDA BRASS 4610 WEST JEFFERSON AUL Higher 2317, 0.439, SW

57 AMBASSADOR BRIDGE FE 805 21ST ST INVENTORY, LUST, UST, WDS Higher 2274, 0.431, NNE

L56 CORNER OF FORT & CLA 4400 FORT ST. INVENTORY, LUST Higher 2135, 0.404, West

L55 DALRAY PORT AUTHORIT 4401-65 FORT ST INVENTORY, LUST, UST Higher 2128, 0.403, West

54 FORT AND CLARK SOUTHWEST CORNER OF US BROWNFIELDS, FINDS Higher 2069, 0.392, West

K53 ROCKWELL FORMER (FOR 4333-4335 WEST FORT BEA Higher 1988, 0.377, WNW

K52 ROCKWELL FORMER (FOR 4333-4335 WEST FORT INVENTORY Higher 1988, 0.377, WNW

L51 NONE-VACANT LAND 422 CLARK AVE INVENTORY, LUST, UST Higher 1978, 0.375, West

J50 GIB-SAR PROPERTIES I 4473 W JEFFERSON AVE LUST, UST, WDS Higher 1966, 0.372, SW

49 CROWN ENTERPRISES 3333 FORT STREET BEA Higher 1963, 0.372, NNE

L48 VACANT LAND 412 CLARK INVENTORY, LUST, UST, WDS Higher 1962, 0.372, West

K47 NONE-VACANT LAND 4301 W FORT ST INVENTORY, LUST, UST Higher 1933, 0.366, WNW

J46 AMBASSADOR PORT COMP 4461 W. JEFFERSON BEA, WDS Higher 1921, 0.364, SW

I45 VACANT LAND 4235 W FORT INVENTORY, LUST, UST Higher 1830, 0.347, WNW

I44 FORT & SCOTTEN STREE FORT & SCOTTEN STREE CERC-NFRAP Higher 1779, 0.337, WNW

43 24TH & SAVOY TRAILER 24TH AND SAVOY STREE CERC-NFRAP, PRP Higher 1778, 0.337, North

42 MIDWEST SUSPENSION A 3411 W FORT ST AIRS, BEA, WDS Higher 1658, 0.314, NNE

41 DETROIT GAS CO- STAT W. JEFFERSON AVE EDR MGP Higher 1577, 0.299, NNE

40 ROCKWELL FORMER (FOR 4333 FORT ST (FORT S INVENTORY Higher 1480, 0.280, West

MAPPED SITES SUMMARY

Target Property Address:3801 W. JEFFERSON AVEUNEDETROIT, MI 48216

Click on Map ID to see full detail.

MAP RELATIVE DIST (ft. & mi.)ID DATABASE ACRONYMS ELEVATION DIRECTIONSITE NAME ADDRESS

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TARGET PROPERTY SEARCH RESULTS

The target property was not listed in any of the databases searched by EDR.

DATABASES WITH NO MAPPED SITES

No mapped sites were found in EDR’s search of available ("reasonably ascertainable ") governmentrecords either on the target property or within the search radius around the target property for thefollowing databases:

STANDARD ENVIRONMENTAL RECORDS

Federal NPL site listNPL National Priority ListProposed NPL Proposed National Priority List SitesNPL LIENS Federal Superfund Liens

Federal Delisted NPL site listDelisted NPL National Priority List Deletions

Federal CERCLIS listFEDERAL FACILITY Federal Facility Site Information listing

Federal RCRA CORRACTS facilities listCORRACTS Corrective Action Report

Federal RCRA non-CORRACTS TSD facilities listRCRA-TSDF RCRA - Treatment, Storage and Disposal

Federal RCRA generators listRCRA-LQG RCRA - Large Quantity GeneratorsRCRA-SQG RCRA - Small Quantity Generators

Federal institutional controls / engineering controls registriesUS ENG CONTROLS Engineering Controls Sites ListUS INST CONTROL Sites with Institutional ControlsLUCIS Land Use Control Information System

Federal ERNS listERNS Emergency Response Notification System

State- and tribal - equivalent CERCLISSHWS This state does not maintain a SHWS list. See the Federal CERCLIS list and Federal NPL list.

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State and tribal landfill and/or solid waste disposal site listsSWF/LF Solid Waste Facilities Database

State and tribal leaking storage tank listsINDIAN LUST Leaking Underground Storage Tanks on Indian Land

State and tribal registered storage tank listsAST Aboveground TanksINDIAN UST Underground Storage Tanks on Indian LandFEMA UST Underground Storage Tank Listing

State and tribal voluntary cleanup sitesINDIAN VCP Voluntary Cleanup Priority Listing

ADDITIONAL ENVIRONMENTAL RECORDS

Local Lists of Landfill / Solid Waste Disposal SitesDEBRIS REGION 9 Torres Martinez Reservation Illegal Dump Site LocationsODI Open Dump InventorySWRCY Recycling FacilitiesINDIAN ODI Report on the Status of Open Dumps on Indian Lands

Local Lists of Hazardous waste / Contaminated SitesUS CDL Clandestine Drug LabsCDL Clandestine Drug Lab ListingUS HIST CDL National Clandestine Laboratory Register

Local Land RecordsLIENS 2 CERCLA Lien InformationLIENS Lien List

Records of Emergency Release ReportsHMIRS Hazardous Materials Information Reporting SystemSPILLS Pollution Emergency Alerting System

Other Ascertainable RecordsDOT OPS Incident and Accident DataDOD Department of Defense SitesFUDS Formerly Used Defense SitesCONSENT Superfund (CERCLA) Consent DecreesROD Records Of DecisionUMTRA Uranium Mill Tailings SitesUS MINES Mines Master Index FileTRIS Toxic Chemical Release Inventory System

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TSCA Toxic Substances Control ActFTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act)HIST FTTS FIFRA/TSCA Tracking System Administrative Case ListingSSTS Section 7 Tracking SystemsICIS Integrated Compliance Information SystemPADS PCB Activity Database SystemMLTS Material Licensing Tracking SystemRADINFO Radiation Information DatabaseFINDS Facility Index System/Facility Registry SystemRAATS RCRA Administrative Action Tracking SystemRMP Risk Management PlansUIC Underground Injection Wells DatabaseDRYCLEANERS Drycleaning EstablishmentsNPDES List of Active NPDES PermitsAIRS Permit and Emissions Inventory DataINDIAN RESERV Indian ReservationsSCRD DRYCLEANERS State Coalition for Remediation of Drycleaners ListingFinancial Assurance Financial Assurance Information ListingWDS Waste Data SystemUS AIRS Aerometric Information Retrieval System Facility SubsystemCOAL ASH EPA Coal Combustion Residues Surface Impoundments ListPCB TRANSFORMER PCB Transformer Registration DatabaseLEAD SMELTERS Lead Smelter SitesUS FIN ASSUR Financial Assurance InformationEPA WATCH LIST EPA WATCH LISTPRP Potentially Responsible Parties2020 COR ACTION 2020 Corrective Action Program ListCOAL ASH DOE Steam-Electric Plant Operation DataCOAL ASH Coal Ash Disposal Sites

EDR RECOVERED GOVERNMENT ARCHIVES

Exclusive Recovered Govt. ArchivesRGA LUST Recovered Government Archive Leaking Underground Storage TankRGA PART 201 Recovered Government Archive State Hazardous Waste Facilities ListRGA LF Recovered Government Archive Solid Waste Facilities List

SURROUNDING SITES: SEARCH RESULTS

Surrounding sites were identified in the following databases.

Elevations have been determined from the USGS Digital Elevation Model and should be evaluated ona relative (not an absolute) basis. Relative elevation information between sites of close proximityshould be field verified. Sites with an elevation equal to or higher than the target property have beendifferentiated below from sites with an elevation lower than the target property.Page numbers and map identification numbers refer to the EDR Radius Map report where detaileddata on individual sites can be reviewed.

Sites listed in bold italics are in multiple databases.

Unmappable (orphan) sites are not considered in the foregoing analysis.

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STANDARD ENVIRONMENTAL RECORDS

Federal CERCLIS listCERCLIS: The Comprehensive Environmental Response, Compensation and Liability Information Systemcontains data on potentially hazardous waste sites that have been reported to the USEPA by states,municipalities, private companies and private persons, pursuant to Section 103 of the ComprehensiveEnvironmental Response, Compensation and Liability Act (CERCLA). CERCLIS contains sites which are eitherproposed to or on the National Priorities List (NPL) and sites which are in the screening and assessment phasefor possible inclusion on the NPL.

A review of the CERCLIS list, as provided by EDR, and dated 10/25/2013 has revealed that there is 1 CERCLIS site within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

MI DEPT/NATURAL RESO 271 S SUMMIT ST SW 1/4 - 1/2 (0.466 mi.) 62 73

Federal CERCLIS NFRAP site ListCERC-NFRAP: Archived sites are sites that have been removed and archived from the inventory of CERCLISsites. Archived status indicates that, to the best of EPA’s knowledge, assessment at a site has been completedand that EPA has determined no further steps will be taken to list this site on the National Priorities List(NPL), unless information indicates this decision was not appropriate or other considerations require arecommendation for listing at a later time. This decision does not necessarily mean that there is no hazardassociated with a given site; it only means that, based upon available information, the location is not judgedto be a potential NPL site.

A review of the CERC-NFRAP list, as provided by EDR, and dated 10/25/2013 has revealed that there are 2 CERC-NFRAP sites within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

24TH & SAVOY TRAILER 24TH AND SAVOY STREE N 1/4 - 1/2 (0.337 mi.) 43 46 FORT & SCOTTEN STREE FORT & SCOTTEN STREE WNW 1/4 - 1/2 (0.337 mi.) I44 47

Federal RCRA generators listRCRA-CESQG: RCRAInfo is EPA’s comprehensive information system, providing access to data supportingthe Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA)of 1984. The database includes selective information on sites which generate, transport, store, treat and/ordispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionallyexempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg ofacutely hazardous waste per month.

A review of the RCRA-CESQG list, as provided by EDR, and dated 12/09/2014 has revealed that there is 1 RCRA-CESQG site within approximately 0.25 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

QUALITY MAILING & FU 4000 W JEFFERSON W 0 - 1/8 (0.057 mi.) A6 10

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State and tribal leaking storage tank listsLUST: The Leaking Underground Storage Tank Incident Reports contain an inventory of reportedleaking underground storage tank incidents. The data come from the Department of Environmental Quality’sLeaking Underground Storage Tank (LUST) Database.

A review of the LUST list, as provided by EDR, and dated 02/16/2015 has revealed that there are 19 LUST sites within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

GENERAL MILL SUPPLY 189 VINEWOOD ST NNW 0 - 1/8 (0.057 mi.) B8 12Release Status: ClosedSubstance Release: GasolineFacility Id: 00007807

PORT OF DETROIT PROP 4105 W JEFFERSON AVE WSW 0 - 1/8 (0.062 mi.) A10 15Release Status: OpenSubstance Release: UnknownFacility Id: 00013251

CAPITOL TRUCKING INC 80 W GRAND BLVD N 0 - 1/8 (0.080 mi.) 13 18Release Status: ClosedSubstance Release: GasolineFacility Id: 00009158

VACANT LAND 261 SCOTTEN W 1/8 - 1/4 (0.194 mi.) E19 25Release Status: OpenSubstance Release: UnknownFacility Id: 00038549

NONE-VACANT LAND 401 SCOTTEN AVE WNW 1/8 - 1/4 (0.226 mi.) E27 29Release Status: OpenSubstance Release: GasolineFacility Id: 00037969

REEDYS MARATHON (FOR 3650 W FORT ST N 1/8 - 1/4 (0.232 mi.) G31 31Release Status: OpenSubstance Release: Diesel,GasolineFacility Id: 00019967

PEZZANI & REID EQUIP 3960 W FORT ST NW 1/8 - 1/4 (0.237 mi.) H34 36Release Status: ClosedSubstance Release: UnknownFacility Id: 00036762

O-J TRANSPORT CO 4005 W FORT ST NW 1/8 - 1/4 (0.244 mi.) H36 38Release Status: OpenSubstance Release: Diesel,DieselFacility Id: 00014724

VACANT LAND 4235 W FORT WNW 1/4 - 1/2 (0.347 mi.) I45 48Release Status: OpenSubstance Release: UnknownSubstance Release: KeroseneFacility Id: 00037985

NONE-VACANT LAND 4301 W FORT ST WNW 1/4 - 1/2 (0.366 mi.) K47 51Release Status: OpenSubstance Release: OtherFacility Id: 00037968

VACANT LAND 412 CLARK W 1/4 - 1/2 (0.372 mi.) L48 52Release Status: OpenSubstance Release: UnknownSubstance Release: GasolineFacility Id: 00037976

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PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

GIB-SAR PROPERTIES I 4473 W JEFFERSON AVE SW 1/4 - 1/2 (0.372 mi.) J50 55Release Status: ClosedSubstance Release: UnknownFacility Id: 00008709

NONE-VACANT LAND 422 CLARK AVE W 1/4 - 1/2 (0.375 mi.) L51 56Release Status: OpenSubstance Release: OtherFacility Id: 00037988

DALRAY PORT AUTHORIT 4401-65 FORT ST W 1/4 - 1/2 (0.403 mi.) L55 63Release Status: OpenSubstance Release: UnknownFacility Id: 00040337

CORNER OF FORT & CLA 4400 FORT ST. W 1/4 - 1/2 (0.404 mi.) L56 64Release Status: OpenSubstance Release: GasolineFacility Id: 50001941

AMBASSADOR BRIDGE FE 805 21ST ST NNE 1/4 - 1/2 (0.431 mi.) 57 65Release Status: OpenSubstance Release: Gasoline,DieselFacility Id: 00006701

AREF BAZZI 747 CLARK ST WNW 1/4 - 1/2 (0.439 mi.) 60 68Release Status: ClosedFacility Id: 00016625

FORMER NICHOLSON TER 4685 W JEFFERSON SW 1/4 - 1/2 (0.462 mi.) M61 71Release Status: OpenSubstance Release: DieselFacility Id: 00037937

ARTIC RENTALS PROPER 4629 FORT ST W 1/4 - 1/2 (0.485 mi.) 66 78Release Status: ClosedSubstance Release: GasolineFacility Id: 00012168

State and tribal registered storage tank listsUST: The Underground Storage Tank database contains registered USTs. USTs are regulated underSubtitle I of the Resource Conservation and Recovery Act (RCRA). The data come from the Department ofEnvironmental Quality’s Michigan UST database.

A review of the UST list, as provided by EDR, and dated 03/01/2015 has revealed that there are 10 UST sites within approximately 0.25 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

GENERAL MILL SUPPLY 189 VINEWOOD ST NNW 0 - 1/8 (0.057 mi.) B8 12Facility Type: CLOSEDFacility Id: 00007807Tank Status: Removed from Ground

PORT OF DETROIT PROP 4105 W JEFFERSON AVE WSW 0 - 1/8 (0.062 mi.) A10 15Facility Type: ACTIVEFacility Id: 00013251Tank Status: Removed from GroundTank Status: Currently In Use

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PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

CAPITOL TRUCKING INC 80 W GRAND BLVD N 0 - 1/8 (0.080 mi.) 13 18Facility Type: CLOSEDFacility Id: 00009158Tank Status: Removed from Ground

GREAT LAKES WATER BL 4120 W JEFFERSON AVE WSW 0 - 1/8 (0.092 mi.) 14 20Facility Type: CLOSEDFacility Id: 00005507Tank Status: Closed in Ground

FIRE DEPT ENGINE #16 101 24TH ST NNE 1/8 - 1/4 (0.162 mi.) 18 25Facility Type: CLOSEDFacility Id: 00019098Tank Status: Removed from Ground

VACANT LAND 261 SCOTTEN W 1/8 - 1/4 (0.194 mi.) E19 25Facility Type: CLOSEDFacility Id: 00038549Tank Status: Removed from Ground

NONE-VACANT LAND 401 SCOTTEN AVE WNW 1/8 - 1/4 (0.226 mi.) E27 29Facility Type: CLOSEDFacility Id: 00037969Tank Status: Removed from Ground

REEDYS MARATHON (FOR 3650 W FORT ST N 1/8 - 1/4 (0.232 mi.) G31 31Facility Type: CLOSEDFacility Id: 00019967Tank Status: Removed from Ground

PEZZANI & REID EQUIP 3960 W FORT ST NW 1/8 - 1/4 (0.237 mi.) H34 36Facility Type: CLOSEDFacility Id: 00036762Tank Status: Removed from Ground

O-J TRANSPORT CO 4005 W FORT ST NW 1/8 - 1/4 (0.244 mi.) H36 38Facility Type: CLOSEDFacility Id: 00014724Tank Status: Removed from Ground

State and tribal institutional control / engineering control registriesAUL: A listing of sites with institutional and/or engineering controls in place.

A review of the AUL list, as provided by EDR, and dated 03/09/2015 has revealed that there is 1 AUL site within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

ANACONDA BRASS 4610 WEST JEFFERSON SW 1/4 - 1/2 (0.439 mi.) M58 66

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State and tribal Brownfields sitesBROWNFIELDS: Brownfields and USTfield Site Database.

A review of the BROWNFIELDS list, as provided by EDR, and dated 07/27/2012 has revealed that there is 1 BROWNFIELDS site within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

ANACONDA BRASS 4610 W. JEFFERSON SW 1/4 - 1/2 (0.439 mi.) M59 67Ernie Id Number: 82001505Site Id Number: 1000022

ADDITIONAL ENVIRONMENTAL RECORDS

Local Brownfield listsUS BROWNFIELDS: The EPA’s listing of Brownfields properties from the Cleanups in My Community program,which provides information on Brownfields properties for which information is reported back to EPA, as well asareas served by Brownfields grant programs.

A review of the US BROWNFIELDS list, as provided by EDR, and dated 12/22/2014 has revealed that there are 2 US BROWNFIELDS sites within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

FORMER JOHN JAMES SI 4005-4117 WEST FORT NW 1/8 - 1/4 (0.244 mi.) H38 42 FORT AND CLARK SOUTHWEST CORNER OF W 1/4 - 1/2 (0.392 mi.) 54 58

Local Lists of Landfill / Solid Waste Disposal SitesHIST LF: The database contains historical information and is no longer updated..

A review of the HIST LF list, as provided by EDR, and dated 03/01/1997 has revealed that there is 1 HIST LF site within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

24TH STREET INCINERA 3565 W JEFFERSON AVE NNE 1/8 - 1/4 (0.159 mi.) D17 23Status: INACTIVEFacility Id: 82000055

Local Lists of Hazardous waste / Contaminated SitesINVENTORY: The Inventory of Facilities has three data sources: Facilities under Part 201,Environmental Remediation, of the Natural Resources and Environmental Protection Act, 1994 PA 451, as amended(NREPA) identified through state funded or private party response activities (Projects); Facilities under Part

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213, Leaking Underground Storage Tanks of the NREPA; and Facilities identified through submittals of BaselineEnvironmental Assessments (BEA) submitted pursuant to Part 201 or Part 213 of the NREPA. The Part 201Projects Inventory does not include all of the facilities that are subject to regulation under Part 201because owners are not required to inform the Department of Environmental Quality (DEQ) about the facilitiesand can pursue cleanup independently. Facilities that are not known to DEQ are not on the Inventory, nor arelocations with releases that resulted in low environmental impact. Part 213 facilities listed here may havemore than one release; a list of releases for which corrective actions have been completed and list ofreleases for which corrective action has not been completed is located on the Leaking Underground StorageTanks Site Search webpage. The DEQ may or may not have reviewed and concurred with the conclusion that thecorrective actions described in a closure report meets criteria. A BEA is a document that new or prospectiveproperty owners/operations disclose to the DEQ identifying the property as a facility pursuant to Part 201 andPart 213. The Inventory of BEA Facilities overlaps in part with the Part 201 Projects facilities and Part 213facilities. There may be more than one BEA for each facility.

A review of the INVENTORY list, as provided by EDR, and dated 01/27/2015 has revealed that there are 22 INVENTORY sites within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

RIVERVIEW TRENTON RA 4000 WEST JEFFERSON WSW 0 - 1/8 (0.029 mi.) A1 8Facility ID: 82002548

RIVERVIEW TRENTION R 4000 WEST JEFFERSON WSW 0 - 1/8 (0.051 mi.) A4 8Facility ID: 82002548

GENERAL MILL SUPPLY 189 VINEWOOD ST NNW 0 - 1/8 (0.057 mi.) B8 12Facility ID: 00007807

PORT OF DETROIT PROP 4105 W JEFFERSON AVE WSW 0 - 1/8 (0.062 mi.) A10 15Facility ID: 00013251

DIB DETROIT LLC 215 VINEWOOD NNW 0 - 1/8 (0.064 mi.) B12 18 VACANT LAND 261 SCOTTEN W 1/8 - 1/4 (0.194 mi.) E19 25

Facility ID: 00038549 NONE-VACANT LAND 401 SCOTTEN AVE WNW 1/8 - 1/4 (0.226 mi.) E27 29

Facility ID: 00037969 REEDYS MARATHON (FOR 3650 W FORT ST N 1/8 - 1/4 (0.232 mi.) G31 31

Facility ID: 00019967 O-J TRANSPORT CO 4005 W FORT ST NW 1/8 - 1/4 (0.244 mi.) H36 38

Facility ID: 00014724 DET/WAYNE CO PORT AU 4300, 4461, & 4500 W SW 1/4 - 1/2 (0.261 mi.) 39 44

Facility ID: 82001733 ROCKWELL FORMER (FOR 4333 FORT ST (FORT S W 1/4 - 1/2 (0.280 mi.) 40 44

Facility ID: 82001482 VACANT LAND 4235 W FORT WNW 1/4 - 1/2 (0.347 mi.) I45 48

Facility ID: 00037985 NONE-VACANT LAND 4301 W FORT ST WNW 1/4 - 1/2 (0.366 mi.) K47 51

Facility ID: 00037968 VACANT LAND 412 CLARK W 1/4 - 1/2 (0.372 mi.) L48 52

Facility ID: 00037976 NONE-VACANT LAND 422 CLARK AVE W 1/4 - 1/2 (0.375 mi.) L51 56

Facility ID: 00037988 ROCKWELL FORMER (FOR 4333-4335 WEST FORT WNW 1/4 - 1/2 (0.377 mi.) K52 57

Facility ID: 82001482 DALRAY PORT AUTHORIT 4401-65 FORT ST W 1/4 - 1/2 (0.403 mi.) L55 63

Facility ID: 00040337

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PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

CORNER OF FORT & CLA 4400 FORT ST. W 1/4 - 1/2 (0.404 mi.) L56 64Facility ID: 50001941

AMBASSADOR BRIDGE FE 805 21ST ST NNE 1/4 - 1/2 (0.431 mi.) 57 65Facility ID: 00006701

ANACONDA BRASS 4610 W. JEFFERSON SW 1/4 - 1/2 (0.439 mi.) M59 67Facility ID: 82001505

FORMER NICHOLSON TER 4685 W JEFFERSON SW 1/4 - 1/2 (0.462 mi.) M61 71Facility ID: 00037937

Not reported 100 S. SUMMIT ST. WSW 1/4 - 1/2 (0.468 mi.) N64 77

PART 201: A Part 201 Listed site is a location that has been evaluated and scored by the DEQ usingthe Part 201 scoring model. The location is or includes a "facility" as defined by Part 201, where there hasbeen a release of a hazardous substance(s) in excess of the Part 201 residential criteria, and/or wherecorrective actions have not been completed under Part 201 to meet the applicable cleanup criteria forunrestricted residential use. The Part 201 List does not include all of the sites of contamination that aresubject to regulation under Part 201 because owners are not required to inform the DEQ about the sites and canpursue cleanup independently. Sites of environmental contamination that are not known to DEQ are not on thelist, nor are sites with releases that resulted in low environmental impact.

A review of the PART 201 list, as provided by EDR, and dated 10/01/2013 has revealed that there are 6 PART 201 sites within approximately 1 mile of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

ANACONDA BRASS 4610 W. JEFFERSON SW 1/4 - 1/2 (0.439 mi.) M59 67Facility Status: Interim Response conducted - No further activities anticipatedFacility ID: 82001505

LETTS DROP FORGE 2714 W JEFFERSON AVE NE 1/2 - 1 (0.501 mi.) O67 79Facility Status: Inactive - no actions taken to address contaminationFacility ID: 82001713

AMBASSADOR BRIDGE CU HOWARD AND 21ST STRE N 1/2 - 1 (0.616 mi.) 68 84Facility Status: Interim Response in progressFacility ID: 82000224

CSX/NORFOLK & WESTER JEFFERSON AND 12TH S NE 1/2 - 1 (0.627 mi.) 69 85Facility Status: Evaluation conductedFacility ID: 82002601

WELCOME CENTER DEVEL NEAR VERNOR AND BAGL N 1/2 - 1 (0.708 mi.) 70 85Facility Status: Interim Response conducted - No further activities anticipatedFacility ID: 82000145

MI DEPT/TRANSPORTATI 5851 W JEFFERSON AVE SW 1/2 - 1 (0.818 mi.) 71 86Facility Status: Interim Response conducted - No further activities anticipatedFacility ID: 82000136

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DEL PART 201: A deleted site has been removed from the Part 201 List because information known to theDEQ at the time of the evaluation does not support inclusion on the Part 201 List. This designation is oftenapplied to sites where changes in cleanup criteria resulted in a determination that the site no longer exceedsany applicable cleanup criterion. A delisted site has been removed from the Part 201 List because responseactions have reduced the levels of contaminants to concentrations which meet or are below the criteria forunrestricted residential use.

A review of the DEL PART 201 list, as provided by EDR, and dated 08/01/2013 has revealed that there is 1 DEL PART 201 site within approximately 1 mile of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

HUBBARD-RICHARD HOUS 2661 BAGLEY STREET N 1/2 - 1 (0.899 mi.) 72 90Facility Id: 82001763

Other Ascertainable RecordsRCRA NonGen / NLR: RCRAInfo is EPA’s comprehensive information system, providing access to data supportingthe Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA)of 1984. The database includes selective information on sites which generate, transport, store, treat and/ordispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non-Generators donot presently generate hazardous waste.

A review of the RCRA NonGen / NLR list, as provided by EDR, and dated 12/09/2014 has revealed that there are 5 RCRA NonGen / NLR sites within approximately 0.25 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

COUGHLIN FX CO 4000 W JEFFERSON AVE W 0 - 1/8 (0.057 mi.) A5 9 NICHOLSON TERMINAL 4105 W JEFFERSON WSW 0 - 1/8 (0.062 mi.) A9 14 CITY OF DETROIT RIVE 3621 W JEFFERSON AVE NNE 1/8 - 1/4 (0.131 mi.) C16 21 PEZZANI AND REID EQU 3960 W FORT ST NW 1/8 - 1/4 (0.237 mi.) H33 35 O-J TRANSPORT CO 4005 W FORT ST NW 1/8 - 1/4 (0.244 mi.) H36 38

BEA: A BEA is a document that new or prospective property owners/operations disclose to the DEQidentifying the property as a facility pursuant to Part 201 and Part 213. The Inventory of BEA Facilitiesoverlaps in part with the Part 201 Projects facilities and Part 213 facilities. There may be more than one BEAfor each facility.

A review of the BEA list, as provided by EDR, and dated 08/21/2013 has revealed that there are 9 BEA sites within approximately 0.5 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

RIVERVIEW TRENTON RA 4000 WEST JEFFERSON WSW 0 - 1/8 (0.029 mi.) A2 8 JENERIC GROUP, LLC T 4000 JEFFERSON AVENU W 0 - 1/8 (0.057 mi.) A7 12 DIB DETROIT LLC 215 VINEWOOD NNW 0 - 1/8 (0.064 mi.) B11 18 MIDWEST SUSPENSION A 3411 W FORT ST NNE 1/4 - 1/2 (0.314 mi.) 42 45 AMBASSADOR PORT COMP 4461 W. JEFFERSON SW 1/4 - 1/2 (0.364 mi.) J46 50 CROWN ENTERPRISES 3333 FORT STREET NNE 1/4 - 1/2 (0.372 mi.) 49 54 ROCKWELL FORMER (FOR 4333-4335 WEST FORT WNW 1/4 - 1/2 (0.377 mi.) K53 58 Not reported 100 S. SUMMIT ST. WSW 1/4 - 1/2 (0.468 mi.) N63 77 2781 CORPORATION 2781 WEST JEFFERSON NE 1/4 - 1/2 (0.479 mi.) O65 77

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EDR HIGH RISK HISTORICAL RECORDS

EDR Exclusive RecordsEDR MGP: The EDR Proprietary Manufactured Gas Plant Database includes records of coal gas plants(manufactured gas plants) compiled by EDR’s researchers. Manufactured gas sites were used in the United Statesfrom the 1800’s to 1950’s to produce a gas that could be distributed and used as fuel. These plants usedwhale oil, rosin, coal, or a mixture of coal, oil, and water that also produced a significant amount of waste.Many of the byproducts of the gas production, such as coal tar (oily waste containing volatile andnon-volatile chemicals), sludges, oils and other compounds are potentially hazardous to human health and theenvironment. The byproduct from this process was frequently disposed of directly at the plant site and canremain or spread slowly, serving as a continuous source of soil and groundwater contamination.

A review of the EDR MGP list, as provided by EDR, has revealed that there are 3 EDR MGP sites within approximately 1 mile of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

DETROIT CITY GAS CO- W. JEFFERSON N 0 - 1/8 (0.119 mi.) C15 21 DETROIT CITY GAS CO- W. JEFFERSON AND 24T NNE 1/8 - 1/4 (0.227 mi.) 28 31 DETROIT GAS CO- STAT W. JEFFERSON AVE NNE 1/4 - 1/2 (0.299 mi.) 41 45

EDR US Hist Auto Stat: EDR has searched selected national collections of business directories and has collectedlistings of potential gas station/filling station/service station sites that were available to EDRresearchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, includegas station/filling station/service station establishments. The categories reviewed included, but were notlimited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station,service station, etc. This database falls within a category of information EDR classifies as "High RiskHistorical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about pastsites and operations that typically create environmental concerns, but may not show up in current governmentrecords searches.

A review of the EDR US Hist Auto Stat list, as provided by EDR, has revealed that there are 12 EDR US Hist Auto Stat sites within approximately 0.25 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

Not reported 102 VINEWOOD ST NNW 0 - 1/8 (0.034 mi.) B3 8 CULLON ALEXANDRINE P 243 24TH NNE 1/8 - 1/4 (0.203 mi.) D20 27 HOLZBAUGH GEORGE INC 3845 W FORT NNW 1/8 - 1/4 (0.220 mi.) F21 27 DAN 0 MARATHON SERVI 3800 W FORT ST NNW 1/8 - 1/4 (0.220 mi.) F22 28 BRENNAN LEO F 3800 W FORT NNW 1/8 - 1/4 (0.222 mi.) F23 28 WARHURST HERSCHEL E 3841 W FORT NNW 1/8 - 1/4 (0.223 mi.) F24 29 BRENNAN SERVICE STAT 3858 W FORT ST NNW 1/8 - 1/4 (0.224 mi.) F25 29 BRENNAN SUPER SERVIC 3858 W FORT NNW 1/8 - 1/4 (0.225 mi.) F26 29 ACTON S SUPER SERVIC 3910 W FORT NW 1/8 - 1/4 (0.232 mi.) F29 31 FORT BOULEVARD SHELL 3650 W FORT ST N 1/8 - 1/4 (0.232 mi.) G30 31 CARRIERE LESTER J 3650 W FORT N 1/8 - 1/4 (0.233 mi.) G32 34 Not reported 4005 W FORT ST NW 1/8 - 1/4 (0.244 mi.) H37 41

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EXECUTIVE SUMMARY

TC4278659.2s EXECUTIVE SUMMARY 16

EDR US Hist Cleaners: EDR has searched selected national collections of business directories and has collectedlistings of potential dry cleaner sites that were available to EDR researchers. EDR’s review was limited tothose categories of sources that might, in EDR’s opinion, include dry cleaning establishments. The categoriesreviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash& dry etc. This database falls within a category of information EDR classifies as "High Risk HistoricalRecords", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites andoperations that typically create environmental concerns, but may not show up in current government recordssearches.

A review of the EDR US Hist Cleaners list, as provided by EDR, has revealed that there is 1 EDR US Hist Cleaners site within approximately 0.25 miles of the target property.

PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____

NEITZER HENRY J 705 25TH N 1/8 - 1/4 (0.240 mi.) G35 38

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EXECUTIVE SUMMARY

TC4278659.2s EXECUTIVE SUMMARY 17

Due to poor or inadequate address information, the following sites were not mapped. Count: 2 records.

Site Name Database(s)____________ ____________

ST. ANNE’S GATE PROPERTIES PART 201, DEL PART 201SPARETIME FAMILY ENTERTAINMENT CEN PART 201

Page 92: Baseline Environmental Assessment for Riverside Park

EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.

600

600600 600

6 0 0

Page 93: Baseline Environmental Assessment for Riverside Park

EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.

Page 94: Baseline Environmental Assessment for Riverside Park

MAP FINDINGS SUMMARY

SearchTargetDistance Total

Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted

STANDARD ENVIRONMENTAL RECORDS

Federal NPL site list 0 NR 0 0 0 0 1.000NPL 0 NR 0 0 0 0 1.000Proposed NPL 0 NR NR NR NR NR TPNPL LIENS

Federal Delisted NPL site list 0 NR 0 0 0 0 1.000Delisted NPL

Federal CERCLIS list 1 NR NR 1 0 0 0.500CERCLIS 0 NR NR 0 0 0 0.500FEDERAL FACILITY

Federal CERCLIS NFRAP site List 2 NR NR 2 0 0 0.500CERC-NFRAP

Federal RCRA CORRACTS facilities list 0 NR 0 0 0 0 1.000CORRACTS

Federal RCRA non-CORRACTS TSD facilities list 0 NR NR 0 0 0 0.500RCRA-TSDF

Federal RCRA generators list 0 NR NR NR 0 0 0.250RCRA-LQG 0 NR NR NR 0 0 0.250RCRA-SQG 1 NR NR NR 0 1 0.250RCRA-CESQG

Federal institutional controls /engineering controls registries

0 NR NR 0 0 0 0.500US ENG CONTROLS 0 NR NR 0 0 0 0.500US INST CONTROL 0 NR NR 0 0 0 0.500LUCIS

Federal ERNS list 0 NR NR NR NR NR TPERNS

State- and tribal - equivalent CERCLIS 0 NR 0 0 0 0 1.000SHWS

State and tribal landfill and/orsolid waste disposal site lists

0 NR NR 0 0 0 0.500SWF/LFState and tribal leaking storage tank lists

19 NR NR 11 5 3 0.500LUST 0 NR NR 0 0 0 0.500INDIAN LUST

State and tribal registered storage tank lists 10 NR NR NR 6 4 0.250UST

TC4278659.2s Page 4

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MAP FINDINGS SUMMARY

SearchTargetDistance Total

Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted

0 NR NR NR 0 0 0.250AST 0 NR NR NR 0 0 0.250INDIAN UST 0 NR NR NR 0 0 0.250FEMA UST

State and tribal institutionalcontrol / engineering control registries

1 NR NR 1 0 0 0.500AULState and tribal voluntary cleanup sites

0 NR NR 0 0 0 0.500INDIAN VCPState and tribal Brownfields sites

1 NR NR 1 0 0 0.500BROWNFIELDS

ADDITIONAL ENVIRONMENTAL RECORDS

Local Brownfield lists 2 NR NR 1 1 0 0.500US BROWNFIELDS

Local Lists of Landfill / SolidWaste Disposal Sites

0 NR NR 0 0 0 0.500DEBRIS REGION 9 0 NR NR 0 0 0 0.500ODI 1 NR NR 0 1 0 0.500HIST LF 0 NR NR 0 0 0 0.500SWRCY 0 NR NR 0 0 0 0.500INDIAN ODI

Local Lists of Hazardous waste /Contaminated Sites

0 NR NR NR NR NR TPUS CDL 22 NR NR 13 4 5 0.500INVENTORY 6 NR 5 1 0 0 1.000PART 201 1 NR 1 0 0 0 1.000DEL PART 201 0 NR NR NR NR NR TPCDL 0 NR NR NR NR NR TPUS HIST CDL

Local Land Records 0 NR NR NR NR NR TPLIENS 2 0 NR NR NR NR NR TPLIENS

Records of Emergency Release Reports 0 NR NR NR NR NR TPHMIRS 0 NR NR NR NR NR TPSPILLS

Other Ascertainable Records 5 NR NR NR 3 2 0.250RCRA NonGen / NLR 0 NR NR NR NR NR TPDOT OPS 0 NR 0 0 0 0 1.000DOD 0 NR 0 0 0 0 1.000FUDS 0 NR 0 0 0 0 1.000CONSENT

TC4278659.2s Page 5

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MAP FINDINGS SUMMARY

SearchTargetDistance Total

Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted

0 NR 0 0 0 0 1.000ROD 0 NR NR 0 0 0 0.500UMTRA 0 NR NR NR 0 0 0.250US MINES 0 NR NR NR NR NR TPTRIS 0 NR NR NR NR NR TPTSCA 0 NR NR NR NR NR TPFTTS 0 NR NR NR NR NR TPHIST FTTS 0 NR NR NR NR NR TPSSTS 0 NR NR NR NR NR TPICIS 0 NR NR NR NR NR TPPADS 0 NR NR NR NR NR TPMLTS 0 NR NR NR NR NR TPRADINFO 0 NR NR NR NR NR TPFINDS 0 NR NR NR NR NR TPRAATS 0 NR NR NR NR NR TPRMP 0 NR NR NR NR NR TPUIC 0 NR NR NR 0 0 0.250DRYCLEANERS 0 NR NR NR NR NR TPNPDES 0 NR NR NR NR NR TPAIRS 9 NR NR 6 0 3 0.500BEA 0 NR 0 0 0 0 1.000INDIAN RESERV 0 NR NR 0 0 0 0.500SCRD DRYCLEANERS 0 NR NR NR NR NR TPFinancial Assurance 0 NR NR NR NR NR TPWDS 0 NR NR NR NR NR TPUS AIRS 0 NR NR 0 0 0 0.500COAL ASH EPA 0 NR NR NR NR NR TPPCB TRANSFORMER 0 NR NR NR NR NR TPLEAD SMELTERS 0 NR NR NR NR NR TPUS FIN ASSUR 0 NR NR NR NR NR TPEPA WATCH LIST 0 NR NR NR NR NR TPPRP 0 NR NR NR 0 0 0.2502020 COR ACTION 0 NR NR NR NR NR TPCOAL ASH DOE 0 NR NR 0 0 0 0.500COAL ASH

EDR HIGH RISK HISTORICAL RECORDS

EDR Exclusive Records 3 NR 0 1 1 1 1.000EDR MGP 12 NR NR NR 11 1 0.250EDR US Hist Auto Stat 1 NR NR NR 1 0 0.250EDR US Hist Cleaners

EDR RECOVERED GOVERNMENT ARCHIVES

Exclusive Recovered Govt. Archives 0 NR NR NR NR NR TPRGA LUST 0 NR NR NR NR NR TPRGA PART 201 0 NR NR NR NR NR TPRGA LF

97 0 6 38 33 20 0- Totals --

TC4278659.2s Page 6

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MAP FINDINGS SUMMARY

SearchTargetDistance Total

Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted

NOTES: TP = Target Property NR = Not Requested at this Search Distance Sites may be listed in more than one database

TC4278659.2s Page 7

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

-83.08358Longitude:42.31055Latitude:BEAData Source:Southeast MIDistrict:DetroitTownship:201104841LVBea Number:

INVENTORY:

152 ft. Site 1 of 8 in cluster A0.029 mi.

Relative:Higher

Actual:579 ft.

< 1/8 WAYNE (County), MI 48209WSW 4000 WEST JEFFERSON AVENUE N/AA1 INVENTORYRIVERVIEW TRENTON RAILROAD COMPANY S114031541

RRDDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: Not reportedCategory: 0Petition Disclosure: No RequestPetition Determination: Riverview Trenton Railroad CompanySubmitter Name: 06/16/2011Date Received: Southeast MIDistrict: 4841BEA Number: Not reportedSecondary Address:

BEA:

152 ft. Site 2 of 8 in cluster A0.029 mi.

Relative:Higher

Actual:579 ft.

< 1/8 DETROIT, MI 48209WSW 4000 WEST JEFFERSON AVENUE N/AA2 BEARIVERVIEW TRENTON RAILROAD COMPANY S111121028

102 VINEWOOD STAddress: 2001Year: BOULEVARD COLLISIONName:

EDR Historical Auto Stations:

180 ft. Site 1 of 4 in cluster B0.034 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI 48216NNW 102 VINEWOOD ST N/AB3 EDR US Hist Auto Stat 1015129649

-83.08358Longitude:42.31055Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

268 ft. Site 3 of 8 in cluster A0.051 mi.

Relative:Higher

Actual:580 ft.

< 1/8 DETROIT, MI WSW 4000 WEST JEFFERSON N/AA4 INVENTORYRIVERVIEW TRENTION RAILROAD S114031540

TC4278659.2s Page 8

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 946-9510Contact telephone: USContact country: DETROIT, MI 48209 4000 W JEFFERSON AVEContact address: THERESA MENNAContact: TAYLOR, MI 48180 27050 WICK RDMailing address: MID106501646EPA ID: DETROIT, MI 48209 4000 W JEFFERSON AVEFacility address: COUGHLIN FX COFacility name: 12/31/2001Date form received by agency:

RCRA NonGen / NLR:

301 ft. Site 4 of 8 in cluster A0.057 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI 48209West 4000 W JEFFERSON AVE MID106501646A5 RCRA NonGen / NLRCOUGHLIN FX CO 1000234795

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: COUGHLIN FX COSite name: 04/20/1988Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: COUGHLIN FX COSite name: 04/05/2001Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer:

COUGHLIN FX CO (Continued) 1000234795

any residue or contaminated soil, waste or other debris resulting from time: 1 kg or less of acutely hazardous waste; or 100 kg or less of hazardous waste during any calendar month, and accumulates at any from the cleanup of a spill, into or on any land or water, of acutely of any residue or contaminated soil, waste or other debris resulting land or water, of acutely hazardous waste; or generates 100 kg or less other debris resulting from the cleanup of a spill, into or on any waste; or 100 kg or less of any residue or contaminated soil, waste or month, and accumulates at any time: 1 kg or less of acutely hazardous or generates 1 kg or less of acutely hazardous waste per calendar month, and accumulates 1000 kg or less of hazardous waste at any time; Handler: generates 100 kg or less of hazardous waste per calendarDescription: Conditionally Exempt Small Quantity GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 841-1040Contact telephone: USContact country: DETROIT, MI 48209 4000 W JEFFERSONContact address: PAUL NEUBURGERContact: DETROIT, MI 48209 4000 W JEFFERSON AVEMailing address: MIR000020289EPA ID: DETROIT, MI 48209 4000 W JEFFERSONFacility address: QUALITY MAILING & FULFILLMENTFacility name: 11/27/1996Date form received by agency:

RCRA-CESQG:

301 ft. Site 5 of 8 in cluster A0.057 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI 48209West FINDS4000 W JEFFERSON MIR000020289A6 RCRA-CESQGQUALITY MAILING & FULFILLMENT 1004724943

TC4278659.2s Page 10

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110003610496Registry ID:

FINDS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/1970Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: QUALITY MAILING & FULFILLMENTOwner/operator name:

Not reportedOwner/Op end date: 01/01/1970Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: QUALITY MAILING & FULFILLMENTOwner/operator name:

Owner/Operator Summary:

hazardous waste the cleanup of a spill, into or on any land or water, of acutely

QUALITY MAILING & FULFILLMENT (Continued) 1004724943

TC4278659.2s Page 11

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110009394887Registry ID:

QUALITY MAILING & FULFILLMENT (Continued) 1004724943

Storage Tank DivisionDivision Assigned: mitchelfReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 1Petition Disclosure: AffirmedPetition Determination: JENERIC GROUP, LLC THESubmitter Name: 01/16/1996Date Received: Southeast MIDistrict: 49BEA Number: Not reportedSecondary Address:

BEA:

301 ft. Site 6 of 8 in cluster A0.057 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI West 4000 JEFFERSON AVENUE N/AA7 BEAJENERIC GROUP, LLC THE S104909719

42.31261Latitude: General Mill Supply CoSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 554-1000Owner Phone: Not reportedOwner Contact: Detroit, MI 48216-1666Owner City,St,Zip: 189 Vinewood StOwner Address: General Mill Supply CoOwner Name: STATE OF MICHIGANSource: 00007807Facility ID:

LUST:

-83.08295Longitude:42.31262Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

302 ft. Site 2 of 4 in cluster B0.057 mi. WDS

Relative:Higher

Actual:584 ft.

< 1/8 USTDETROIT, MI 48216NNW LUST189 VINEWOOD ST N/AB8 INVENTORYGENERAL MILL SUPPLY CO U003321178

TC4278659.2s Page 12

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

Not reportedTank Release Detection: 07/08/1998Remove Date: 03/25/1966Install Date: GasolineProduct: 6000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 07/01/1998Remove Date: 03/25/1966Install Date: GasolineProduct: 1000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08295Longitude: 42.31261Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 554-1000Contact Phone: STUART ROTENBERGContact: (313) 554-1000Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48216-1666Owner City,St,Zip: 189 VINEWOOD STOwner Address: GENERAL MILL SUPPLY COOwner Name: CLOSEDFacility Type: 00007807Facility ID:

UST:

08/15/2000Release Closed Date: ClosedRelease Status: GasolineSubstance Released: 07/08/1998Release Date: C-0586-98Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08295Longitude:

GENERAL MILL SUPPLY CO (Continued) U003321178

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

WAYNEMailing County: 48216Mailing City/State/Zip: 189 VINEWOOD STMailing Address: GENERAL MILL SUPPLY COSite Specific Name: 455417WMD Id: MIG000016030Site Id:

WDS:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection:

GENERAL MILL SUPPLY CO (Continued) U003321178

06/14/2013Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NICHOLSON TERMINALOwner/operator name:

Not reportedOwner/Op end date: 06/14/2013Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NICHOLSON TERMINALOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (000) 000-0000Contact telephone: USContact country: Not reported Not reportedContact address: PATRICK SOMETHINGContact: RIVER ROUGE, MI 48218 P O BOX 18066Mailing address: MIK532831187EPA ID: DETROIT, MI 48209 4105 W JEFFERSONFacility address: NICHOLSON TERMINALFacility name: 06/14/2013Date form received by agency:

RCRA NonGen / NLR:

327 ft. Site 7 of 8 in cluster A0.062 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI 48209WSW FINDS4105 W JEFFERSON MIK532831187A9 RCRA NonGen / NLRNICHOLSON TERMINAL 1016453636

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110057073367Registry ID:

FINDS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date:

NICHOLSON TERMINAL (Continued) 1016453636

River Rouge, MI 48218Owner City,St,Zip: PO Box 18066Owner Address: Detroit Wayne County Port AuthorityOwner Name: STATE OF MICHIGANSource: 00013251Facility ID:

LUST:

-83.0842Longitude:42.30996Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

327 ft. Site 8 of 8 in cluster A0.062 mi. WDS

Relative:Higher

Actual:581 ft.

< 1/8 USTDETROIT, MI 48218WSW LUST4105 W JEFFERSON AVE N/AA10 INVENTORYPORT OF DETROIT PROPERTY U000268472

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Bare Steel,Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/08/1997Remove Date: 05/06/1976Install Date: DieselProduct: 10000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08420Longitude: 42.30995Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 331-3842Contact Phone: John StokerContact: (313) 259-5091Owner Phone: Not reportedOwner Contact: USAOwner Country: RIVER ROUGE, MI 48218Owner City,St,Zip: PO BOX 18066Owner Address: DETROIT WAYNE COUNTY PORT AUTHORITYOwner Name: ACTIVEFacility Type: 00013251Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 12/08/1997Release Date: C-1232-97Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08420Longitude: 42.30995Latitude: Detroit Marine Terminals IncSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 259-5091Owner Phone: Not reportedOwner Contact:

PORT OF DETROIT PROPERTY (Continued) U000268472

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

WAYNEMailing County: 48218Mailing City/State/Zip: P O BOX 18066Mailing Address: NICHOLSON TERMINALSite Specific Name: 493218WMD Id: MIK532831187Site Id:

WDS:

NoImpressed Device: Fiberglass Reinforced Plastic, Double WalledConstruction Material: Suction: No Valve At TankPiping Type: Fiberglass Reinforced Plastic, Double WalledPiping Material: Interstitial Monitoring Double Walled PipingPipe Realease Detection: Automatic Tank Gauging, Interstitial Monitoring Double Walled TankTank Release Detection: Not reportedRemove Date: 09/01/1997Install Date: GasolineProduct: 2500Capacity: Currently In UseTank Status: 4Tank ID:

NoImpressed Device: Fiberglass Reinforced Plastic, Double WalledConstruction Material: Suction: No Valve At TankPiping Type: Fiberglass Reinforced Plastic, Double WalledPiping Material: Interstitial Monitoring Double Walled PipingPipe Realease Detection: Automatic Tank Gauging, Interstitial Monitoring Double Walled TankTank Release Detection: Not reportedRemove Date: 09/01/1997Install Date: DieselProduct: 10000Capacity: Currently In UseTank Status: 3Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Bare SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/08/1997Remove Date: 05/06/1976Install Date: GasolineProduct: 3000Capacity: Removed from GroundTank Status:

PORT OF DETROIT PROPERTY (Continued) U000268472

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WAYNEMailing County: 48216Mailing City/State/Zip: 215 VINEWOOD STMailing Address: WEBSTER COLD FORGESite Specific Name: 444243WMD Id: MIG000038484Site Id:

WDS:

RDDivision Assigned: scheelsjReviewer: No RequestDetermination 20107A: Not reportedCategory: 0Petition Disclosure: No RequestPetition Determination: DIB Detroit LLCSubmitter Name: 05/04/2012Date Received: Southeast MIDistrict: 5173BEA Number: Not reportedSecondary Address:

BEA:

336 ft. Site 3 of 4 in cluster B0.064 mi.

Relative:Higher

Actual:584 ft.

< 1/8 DETROIT, MI 48216NNW WDS215 VINEWOOD N/AB11 BEADIB DETROIT LLC S111832660

Not reportedLongitude:Not reportedLatitude:BEAData Source:Southeast MIDistrict:DetroitTownship:201205173LVBea Number:

INVENTORY:

336 ft. Site 4 of 4 in cluster B0.064 mi.

Relative:Higher

Actual:584 ft.

< 1/8 WAYNE (County), MI 48216NNW 215 VINEWOOD N/AB12 INVENTORYDIB DETROIT LLC S114033982

Capitol Trucking IncSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 849-2100Owner Phone: Not reportedOwner Contact: Dearborn, MI 48120-1732Owner City,St,Zip: 1725 Miller RdOwner Address: Capitol Trucking IncOwner Name: STATE OF MICHIGANSource: 00009158Facility ID:

LUST:

420 ft.0.080 mi.

Relative:Higher

Actual:586 ft.

< 1/8 WDSDETROIT, MI 48216North UST80 W GRAND BLVD N/A13 LUSTCAPITOL TRUCKING INC U003321517

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05/18/1998Remove Date: 04/16/1981Install Date: GasolineProduct: 12000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/18/1998Remove Date: 04/16/1981Install Date: DieselProduct: 12000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.20720Longitude: 42.32685Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (248) 826-1199Contact Phone: EDWARD MURPHYContact: (313) 849-2100Owner Phone: Not reportedOwner Contact: USAOwner Country: DEARBORN, MI 48120-1732Owner City,St,Zip: 1725 MILLER RDOwner Address: CAPITOL TRUCKING INCOwner Name: CLOSEDFacility Type: 00009158Facility ID:

UST:

10/09/1998Release Closed Date: ClosedRelease Status: GasolineSubstance Released: 05/26/1998Release Date: C-0424-98Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.20720Longitude: 42.32685Latitude:

CAPITOL TRUCKING INC (Continued) U003321517

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WAYNEMailing County: 48216Mailing City/State/Zip: 80 W GRAND BLVDMailing Address: CAPITAL TRUCKINGSite Specific Name: 450539WMD Id: MIG000025176Site Id:

WDS:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/18/1998Remove Date: Not reportedInstall Date: DieselProduct: 12000Capacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection:

CAPITOL TRUCKING INC (Continued) U003321517

-83.08447Longitude: 42.31015Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 849-1800Contact Phone: GILBERT L. MAIUS JR.Contact: (313) 849-1800Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48209Owner City,St,Zip: 163 N MORRELLOwner Address: GREAT LAKES WATER BLASTINGOwner Name: CLOSEDFacility Type: 00005507Facility ID:

UST:

486 ft.0.092 mi.

Relative:Higher

Actual:581 ft.

< 1/8 DETROIT, MI 48209WSW 4120 W JEFFERSON AVE N/A14 USTGREAT LAKES WATER BLASTING U003320585

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 08/01/1984Remove Date: Not reportedInstall Date: DieselProduct: Not reportedCapacity: Closed in GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 11/01/1978Remove Date: Not reportedInstall Date: DieselProduct: Not reportedCapacity: Closed in GroundTank Status: 1Tank ID:

GREAT LAKES WATER BLASTING (Continued) U003320585

Alternate Name:MICHIGAN CONSOLIDATED GAS CO. No additional information availableManufactured Gas Plants:

629 ft. Site 1 of 2 in cluster C0.119 mi.

Relative:Higher

Actual:586 ft.

< 1/8 DETROIT, MI 48210North W. JEFFERSON N/AC15 EDR MGPDETROIT CITY GAS CO-STATION F 1008408095

USContact country: DETROIT, MI 48216 3621 W JEFFERSON AVEContact address: RICHARD HAUTAUContact: DETROIT, MI 48226 65 CADILLAC SQMailing address: MID980825202EPA ID: DETROIT, MI 48216 3621 W JEFFERSON AVEFacility address: CITY OF DETROIT RIVERSIDE PARKFacility name: 10/18/2002Date form received by agency:

RCRA NonGen / NLR:

693 ft. Site 2 of 2 in cluster C0.131 mi.

Relative:Higher

Actual:585 ft.

1/8-1/4 DETROIT, MI 48216NNE FINDS3621 W JEFFERSON AVE MID980825202C16 RCRA NonGen / NLRCITY OF DETROIT RIVERSIDE PARK 1000367045

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08/19/1983Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Small Quantity GeneratorClassification: CITY OF DETROIT RIVERSIDE PARKSite name: 01/11/2002Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/1970Owner/Op start date: OwnerOwner/Operator Type: MunicipalLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: CITY OF DETROITOwner/operator name:

Not reportedOwner/Op end date: 01/01/1970Owner/Op start date: OperatorOwner/Operator Type: MunicipalLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: CITY OF DETROITOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 224-1145Contact telephone:

CITY OF DETROIT RIVERSIDE PARK (Continued) 1000367045

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corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110003617355Registry ID:

FINDS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: CITY OF DETROIT RIVERSIDE PARKSite name:

CITY OF DETROIT RIVERSIDE PARK (Continued) 1000367045

Not reportedOwner Contact: CITY OF DETROITOwner Name: Not reportedOperator Email: Not reportedOperator Fax: Not reportedOperator Telephone: Not reportedOperator City,St,Zip: Not reportedOperator Address: Not reportedOperator Contact: Not reportedOperator Name: Not reportedExp Letters: Not reportedEnforcement: Not reportedNo Waste: Not reportedLicense No: / /License Date: Not reportedPermit Number: Not reportedPermit Date: NoActive: Not reportedStaff: 000055Facility Number: 82County Code: Not reportedFacility Contact: IncineratorFacility Type: Not reportedFacility is Open: Not reportedFacility Email: Not reportedFacility Type: Not reportedFacility Fax: Not reportedFacility Phone: Not reportedContact: INACTIVEStatus: 82000055Facility ID:

Historical LF:

839 ft. Site 1 of 2 in cluster D0.159 mi.

Relative:Higher

Actual:587 ft.

1/8-1/4 DETROIT, MI 48216NNE 3565 W JEFFERSON AVE N/AD17 HIST LF24TH STREET INCINERATOR S100344466

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Not reportedSite Monitorable Under Definition of New Rules: Not reportedReceived Waste on or After Oct. 9, 1991: Not reportedDate landill Certified Closed: Not reportedGroundwater Monitoring System Exists: Not reportedPerpetual Care Fund Agreement Signed: Not reportedPerpetual Care Fund Signed: Not reportedPerpetual Care Fund Type: Not reportedRestrictive Deed Covenant Filed: 0.000Acres Given in 3rd Construction Permit: Not reportedIssue of 3rd Construction Permit Date: 0.000Acres Given in 2nd Construction Permit: Not reportedIssue of 2nd Construction Permit Date: 0.000Acres Given in 1st Construction Permit: Not reportedIssue of 1st Construction Permit Date: 0.000Acres Certified Closed: 0.000Acreage Currently Licensed: Not reportedDate of Expiry of Current License: Not reportedComments: Not reportedLicensed: Not reportedExpiry: Not reportedExpires: Not reportedIssued Date: Not reportedFund Type: Not reportedFinancial Instrument: 0.00Amount: Not reportedReported Date: Not reportedLiner Type: Not reportedCounty 2 Description: Not reportedCounty Description: Not reportedBusiness Type: Not reportedDistrict: Not reportedTownship Section: Not reportedSection Number: Not reportedTownship: Not reportedNature of Wastes Allowed: Not reportedLiner Information: GovernmentApplication Type: Not reportedPermit Applicant Phone: DETROIT, MI 48226Permit Applicant City,St,Zip: 1550 ERSKINEPermit Applicant Address: JOSEPH GARRITYPermit Applicant Contact: DEPT OF PUBLIC WORKSPermit Applicant: Not reportedSection: S.E. MichiganDistrict: Not reportedOwner Email: Not reportedOwner Fax: Not reportedOwner Telephone: DETROIT, MI 48226Owner City,St,Zip: CITY-COUNTY BLDGOwner Address: Not reportedAttention:

24TH STREET INCINERATOR (Continued) S100344466

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NoImpressed Device: Asphalt Coated or Bare Steel,Cathodically Protected SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/08/1995Remove Date: 03/19/1956Install Date: DieselProduct: 1000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.07959Longitude: 42.31378Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 833-7296Contact Phone: RON BRUNDIDGEContact: (313) 224-3822Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48226Owner City,St,Zip: 65 CADILLAC SQUARE STE 900Owner Address: CITY OF DETROIT / DPW/CEDOwner Name: CLOSEDFacility Type: 00019098Facility ID:

UST:

857 ft.0.162 mi.

Relative:Higher

Actual:581 ft.

1/8-1/4 DETROIT, MI 48226NNE 101 24TH ST N/A18 USTFIRE DEPT ENGINE #16 U003324293

City Of Detroit / Planning Development DeptOwner Name: STATE OF MICHIGANSource: 00038549Facility ID:

LUST:

-83.08653Longitude:42.31136Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1023 ft. Site 1 of 2 in cluster E0.194 mi.

Relative:Higher

Actual:585 ft.

1/8-1/4 USTDETROIT, MI 48226West LUST261 SCOTTEN N/AE19 INVENTORYVACANT LAND U003326446

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Not reportedTank Release Detection: 06/03/1998Remove Date: Not reportedInstall Date: Hazardous SubstanceProduct: 12000Capacity: Removed from GroundTank Status: 2Tank ID:

-83.08652Longitude: 42.31136Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-9031Contact Phone: RAMSESH PATELContact: (313) 224-9031Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48226Owner City,St,Zip: 1602 CADILLAC TOWEROwner Address: CITY OF DETROIT / PLANNING DEVELOPMENT DEPTOwner Name: CLOSEDFacility Type: 00038549Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 07/09/1998Release Date: C-0590-98Leak Number:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 05/26/1998Release Date: C-0427-98Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08652Longitude: 42.31136Latitude: Vacant LandSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-9031Owner Phone: Not reportedOwner Contact: Detroit, MI 48226Owner City,St,Zip: 1602 Cadillac TowerOwner Address:

VACANT LAND (Continued) U003326446

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 11/30/1998Remove Date: Not reportedInstall Date: GasolineProduct: 1000Capacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection:

VACANT LAND (Continued) U003326446

AUTOMOBILE GARAGESType: 1926Year: CULLON ALEXANDRINE PName:

EDR Historical Auto Stations:

1074 ft. Site 2 of 2 in cluster D0.203 mi.

Relative:Higher

Actual:589 ft.

1/8-1/4 DETROIT, MI NNE 243 24TH N/AD20 EDR US Hist Auto StatCULLON ALEXANDRINE P 1009490005

2004Year: ENGINE PARTS WAREHOUESEName:

3845 W FORT STAddress: 2003Year: FORT BOULEVARD AUTOMOTIVEName:

3845 W FORT STAddress: 1999Year: FORT BOULEVARDAUTOMOTIVE COMPANYName:

AUTOMOBILE SERVICE STATIONSType: 1935Year: HOLZBAUGH GEORGE INC FORD DEALERSName:

AUTOMOBILE SERVICE STATIONSType: 1931Year: HOLZBAUGH GEORGE INCName:

EDR Historical Auto Stations:

1164 ft. Site 1 of 7 in cluster F0.220 mi.

Relative:Higher

Actual:591 ft.

1/8-1/4 DETROIT, MI NNW 3845 W FORT N/AF21 EDR US Hist Auto StatHOLZBAUGH GEORGE INC 1009491624

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3845 W FORT STAddress: 2010Year: ENGINE PARTS WAREHOUSE COName:

3845 W FORT STAddress: 2009Year: ENGINE PARTS WAREHOUSE COName:

3845 W FORT STAddress: 2008Year: ENGINE PARTS WAREHOUSE COName:

3845 W FORT STAddress: 2006Year: FORT BOULEVARD AUTOMOTIVEName:

3845 W FORT STAddress: 2005Year: FORT BLVD AUTOMOTIVEName:

3845 W FORT STAddress:

HOLZBAUGH GEORGE INC (Continued) 1009491624

GASOLINE STATIONSType: 1970Year: DAN 0 MARATHON SERVICEName:

EDR Historical Auto Stations:

1164 ft. Site 2 of 7 in cluster F0.220 mi.

Relative:Higher

Actual:590 ft.

1/8-1/4 DETROIT, MI NNW 3800 W FORT ST N/AF22 EDR US Hist Auto StatDAN 0 MARATHON SERVICE 1009491579

GASOLINE STATIONSType: 1965Year: DAN D MARATHON SERVICEName:

GASOLINE STATIONSType: 1956Year: DAN D SPEEDWAY SERVICEName:

GASOLINE AND OIL SERVICE STATIONSType: 1940Year: BRENNAN LEO FName:

EDR Historical Auto Stations:

1172 ft. Site 3 of 7 in cluster F0.222 mi.

Relative:Higher

Actual:590 ft.

1/8-1/4 DETROIT, MI NNW 3800 W FORT N/AF23 EDR US Hist Auto StatBRENNAN LEO F 1009491578

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GASOLINE AND OIL SERVICE STATIONSType: 1940Year: MADDOX ORVAL PName:

GASOLINE AND OIL SERVICE STATIONSType: 1935Year: WARHURST HERSCHEL EName:

EDR Historical Auto Stations:

1178 ft. Site 4 of 7 in cluster F0.223 mi.

Relative:Higher

Actual:591 ft.

1/8-1/4 DETROIT, MI NNW 3841 W FORT N/AF24 EDR US Hist Auto StatWARHURST HERSCHEL E 1009491616

GASOLINE STATIONSType: 1970Year: BRENNAN SERVICE STATIONName:

EDR Historical Auto Stations:

1182 ft. Site 5 of 7 in cluster F0.224 mi.

Relative:Higher

Actual:591 ft.

1/8-1/4 DETROIT, MI NNW 3858 W FORT ST N/AF25 EDR US Hist Auto StatBRENNAN SERVICE STATION 1009491635

GASOLINE STATIONSType: 1965Year: BRENNAN SERVICE STATIONName:

GASOLINE STATIONSType: 1956Year: BRENNAN SUPER SERVICEName:

EDR Historical Auto Stations:

1186 ft. Site 6 of 7 in cluster F0.225 mi.

Relative:Higher

Actual:591 ft.

1/8-1/4 DETROIT, MI NNW 3858 W FORT N/AF26 EDR US Hist Auto StatBRENNAN SUPER SERVICE 1009491634

LUST:

-83.08695Longitude:42.31195Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1191 ft. Site 2 of 2 in cluster E0.226 mi.

Relative:Higher

Actual:587 ft.

1/8-1/4 USTDETROIT, MI 48226WNW LUST401 SCOTTEN AVE N/AE27 INVENTORYNONE-VACANT LAND U003326292

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Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/09/1994Remove Date: 01/01/1955Install Date: GasolineProduct: 1000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08694Longitude: 42.31194Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-3894Contact Phone: RICHARD RYBINSKI/D FISHERContact: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: USAOwner Country: DETROIT, MI 48226-2619Owner City,St,Zip: 150 W MICHIGAN AVE7TTH FLOOROwner Address: CITY OF DETROITOwner Name: CLOSEDFacility Type: 00037969Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: GasolineSubstance Released: 04/20/1994Release Date: C-0347-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08694Longitude: 42.31194Latitude: City Of Detroit - Vacant LotSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: Detroit, MI 48226-2619Owner City,St,Zip: 150 W Michigan Ave7Tth FloorOwner Address: City of DetroitOwner Name: STATE OF MICHIGANSource: 00037969Facility ID:

NONE-VACANT LAND (Continued) U003326292

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material:

NONE-VACANT LAND (Continued) U003326292

Alternate Name:MICHIGAN CONSOLIDATED GAS CO. No additional information availableManufactured Gas Plants:

1201 ft.0.227 mi.

Relative:Higher

Actual:588 ft.

1/8-1/4 DETROIT, MI 48210NNE W. JEFFERSON AND 24TH STREET N/A28 EDR MGPDETROIT CITY GAS CO-STATION E 1008408094

GASOLINE STATIONSType: 1956Year: ACTON S SUPER SERVICEName:

GASOLINE AND OIL SERVICE STATIONSType: 1940Year: ACTON WM JName:

EDR Historical Auto Stations:

1223 ft. Site 7 of 7 in cluster F0.232 mi.

Relative:Higher

Actual:592 ft.

1/8-1/4 DETROIT, MI NW 3910 W FORT N/AF29 EDR US Hist Auto StatACTON S SUPER SERVICE 1009491686

GASOLINE STATIONSType: 1970Year: FORT BOULEVARD SHELL SERVICEName:

EDR Historical Auto Stations:

1223 ft. Site 1 of 4 in cluster G0.232 mi.

Relative:Higher

Actual:590 ft.

1/8-1/4 DETROIT, MI North 3650 W FORT ST N/AG30 EDR US Hist Auto StatFORT BOULEVARD SHELL SERVICE 1009491440

-83.08341Longitude:42.31542Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1223 ft. Site 2 of 4 in cluster G0.232 mi. WDS

Relative:Higher

Actual:590 ft.

1/8-1/4 USTDETROIT, MI 48089North LUST3650 W FORT ST N/AG31 INVENTORYREEDYS MARATHON (FORMER) U002303718

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Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/20/1994Remove Date: 06/23/1981Install Date: DieselProduct: 4000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08340Longitude: 42.31542Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 939-7000Contact Phone: MARK W TROTTIERContact: (313) 939-7000Owner Phone: Not reportedOwner Contact: USAOwner Country: WARREN, MI 48089-2010Owner City,St,Zip: 12225 STEPHENS RDOwner Address: MEXICAN TOWN REAL ESTATE COOwner Name: CLOSEDFacility Type: 00019967Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: Diesel,GasolineSubstance Released: 06/29/1994Release Date: C-0669-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08340Longitude: 42.31542Latitude: Mexican Town Real EstateSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 939-7000Owner Phone: Not reportedOwner Contact: Warren, MI 48089-2010Owner City,St,Zip: 12225 Stephens RdOwner Address: Mexican Town Real Estate CoOwner Name: STATE OF MICHIGANSource: 00019967Facility ID:

LUST:

REEDYS MARATHON (FORMER) (Continued) U002303718

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Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/29/1994Remove Date: 06/23/1976Install Date: GasolineProduct: 3000Capacity: Removed from GroundTank Status: 5Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/29/1994Remove Date: 06/23/1976Install Date: GasolineProduct: 3000Capacity: Removed from GroundTank Status: 4Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/29/1994Remove Date: 06/23/1976Install Date: GasolineProduct: 4000Capacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/29/1994Remove Date: 06/23/1976Install Date: GasolineProduct: 4000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Interier Asphalt Coated or Bare Steel,Fiberglass Reinforced plastic,LinedConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material:

REEDYS MARATHON (FORMER) (Continued) U002303718

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WAYNEMailing County: 48216Mailing City/State/Zip: 3650 W FORT STMailing Address: MEXICAN TOWN REALTYSite Specific Name: 416279WMD Id: MIG000039390Site Id:

WDS:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Gravity Fed?Piping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/30/1994Remove Date: Not reportedInstall Date: Used OilProduct: 500Capacity: Removed from GroundTank Status: 7Tank ID:

NoImpressed Device: Cathodically Protected Steel,Fiberglass Reinforced plasticConstruction Material: Not reportedPiping Type: Fiberglass reinforced plasticPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/29/1994Remove Date: 06/23/1981Install Date: GasolineProduct: 10000Capacity: Removed from GroundTank Status: 6Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material:

REEDYS MARATHON (FORMER) (Continued) U002303718

GASOLINE STATIONSType: 1965Year: FORT BOULEVARD SHELL SERVICEName:

GASOLINE AND OIL SERVICE STATIONSType: 1940Year: CARRIERE LESTER JName:

EDR Historical Auto Stations:

1228 ft. Site 3 of 4 in cluster G0.233 mi.

Relative:Higher

Actual:590 ft.

1/8-1/4 DETROIT, MI North 3650 W FORT N/AG32 EDR US Hist Auto StatCARRIERE LESTER J 1009491439

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NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 554-4000Contact telephone: USContact country: DETROIT, MI 48216 3960 W FORT STContact address: LORRAINE EASTONContact: MID016947541EPA ID: DETROIT, MI 48216 3960 W FORT STFacility address: PEZZANI AND REID EQUIPMENT CO INCFacility name: 12/31/2001Date form received by agency:

RCRA NonGen / NLR:

1254 ft. Site 1 of 5 in cluster H0.237 mi.

Relative:Higher

Actual:592 ft.

1/8-1/4 DETROIT, MI 48216NW FINDS3960 W FORT ST MID016947541H33 RCRA NonGen / NLRPEZZANI AND REID EQUIPMENT CO INC 1000443036

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corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110003587217Registry ID:

FINDS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Small Quantity GeneratorClassification: PEZZANI AND REID EQUIPMENT CO INCSite name: 09/22/1986Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter:

PEZZANI AND REID EQUIPMENT CO INC (Continued) 1000443036

UnknownSubstance Released: 12/29/1999Release Date: C-1391-99Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08553Longitude: 42.31450Latitude: Pezzani & Reid Equip Co IncSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 554-4000Owner Phone: Not reportedOwner Contact: Detroit, MI 48216-1655Owner City,St,Zip: 3960 W Fort StOwner Address: Pezzani & Reid CtrOwner Name: STATE OF MICHIGANSource: 00036762Facility ID:

LUST:

1254 ft. Site 2 of 5 in cluster H0.237 mi.

Relative:Higher

Actual:592 ft.

1/8-1/4 WDSDETROIT, MI 48216NW UST3960 W FORT ST N/AH34 LUSTPEZZANI & REID EQUIP CO INC U003325966

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Not reportedInstall Date: Petroleum ProductsProduct: Not reportedCapacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/29/1999Remove Date: Not reportedInstall Date: Petroleum ProductsProduct: 6000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/29/1999Remove Date: Not reportedInstall Date: UNKNOWNProduct: 6000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08553Longitude: 42.31450Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 554-4000Contact Phone: JAMES G SKALAContact: (313) 554-4000Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48216-1655Owner City,St,Zip: 3960 W FORT STOwner Address: PEZZANI & REID CTROwner Name: CLOSEDFacility Type: 00036762Facility ID:

UST:

06/26/2000Release Closed Date: ClosedRelease Status:

PEZZANI & REID EQUIP CO INC (Continued) U003325966

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WAYNEMailing County: 48216Mailing City/State/Zip: 3960 W FORT STMailing Address: PEZZANI AND REID EQUIPMENT CO INCSite Specific Name: 394640WMD Id: MID016947541Site Id:

WDS:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/29/1999Remove Date:

PEZZANI & REID EQUIP CO INC (Continued) U003325966

CLEANERS AND DYERSType: 1926Year: NEITZER HENRY JName:

EDR Historical Cleaners:

1265 ft. Site 4 of 4 in cluster G0.240 mi.

Relative:Higher

Actual:590 ft.

1/8-1/4 DETROIT, MI North 705 25TH N/AG35 EDR US Hist CleanersNEITZER HENRY J 1009482440

Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 841-0070Contact telephone: USContact country: DETROIT, MI 48209 4005 W FORT STContact address: WAYNE GUHYContact: MID001836881EPA ID: DETROIT, MI 48209 4005 W FORT STFacility address: O-J TRANSPORT COFacility name: 12/31/2001Date form received by agency:

RCRA NonGen / NLR:

WDS1288 ft. USTSite 3 of 5 in cluster H0.244 mi. LUST

Relative:Higher

Actual:592 ft.

1/8-1/4 INVENTORYDETROIT, MI 48209NW FINDS4005 W FORT ST MID001836881H36 RCRA NonGen / NLRO-J TRANSPORT CO 1000202772

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corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110003577763Registry ID:

FINDS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Small Quantity GeneratorClassification: O-J TRANSPORT COSite name: 01/17/1986Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 01/01/2002Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone:

O-J TRANSPORT CO (Continued) 1000202772

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-83.08580Longitude: 42.31406Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 841-0070Contact Phone: Patricia DennisContact: (313) 841-0070Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48209-3223Owner City,St,Zip: 4335 W FORT STOwner Address: O J LAND DEVELOPMENTOwner Name: CLOSEDFacility Type: 00014724Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: Diesel,DieselSubstance Released: 02/21/2007Release Date: C-0346-06Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08580Longitude: 42.31406Latitude: Motor City ExpressSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 841-0070Owner Phone: Not reportedOwner Contact: Detroit, MI 48209-3223Owner City,St,Zip: 4335 W Fort StOwner Address: O J Land DevelopmentOwner Name: STATE OF MICHIGANSource: 00014724Facility ID:

LUST:

-83.08581Longitude:42.31407Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

O-J TRANSPORT CO (Continued) 1000202772

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WAYNEMailing County: 48209Mailing City/State/Zip: 4005 W FORT STMailing Address: O J TRANSPORT CO INCSite Specific Name: 392901WMD Id: MID001836881Site Id:

WDS:

NoImpressed Device: Composite(Steel w/Fiberglass),Double WalledConstruction Material: PressurePiping Type: Double Walled,Fiberglass reinforced plasticPiping Material: Piping Automatic Line Leak Detectors,Interstitial Monitoring Double WalledPipe Realease Detection: Automatic Tank Gauging,Inter Monitoring Double Walled TankTank Release Detection: 11/09/2006Remove Date: Not reportedInstall Date: DieselProduct: 10000Capacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Composite(Steel w/Fiberglass),Double WalledConstruction Material: PressurePiping Type: Double Walled,Fiberglass reinforced plasticPiping Material: Piping Automatic Line Leak Detectors,Interstitial Monitoring Double WalledPipe Realease Detection: Automatic Tank Gauging,Inter Monitoring Double Walled TankTank Release Detection: 11/09/2006Remove Date: Not reportedInstall Date: DieselProduct: 10000Capacity: Removed from GroundTank Status: 2Tank ID:

O-J TRANSPORT CO (Continued) 1000202772

4005 W FORT STAddress: 2010Year: MOTOR CITY EXPRESSName:

EDR Historical Auto Stations:

1288 ft. Site 4 of 5 in cluster H0.244 mi.

Relative:Higher

Actual:592 ft.

1/8-1/4 DETROIT, MI 48209NW 4005 W FORT ST N/AH37 EDR US Hist Auto Stat 1015470039

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Not reportedAsbestos cleaned: YAsbestos found: Not reportedAir cleaned: Not reportedAir contaminated: Not reportedState/tribal NFA date: Not reportedState/tribal program ID: Not reportedState/tribal program date: Not reportedIC in place: Not reportedIC in place date: Not reportedIC cat. enforcement permit tools: Not reportedIC cat. gov. controls: Not reportedIC cat. info. devices: Not reportedIC Category proprietary controls: UInstitutional controls required: YesPhoto available: NoVideo available: YesCleanup required: NDid owner change: Ford Motor CompanyCurrent owner: PrivateOwnership entity: 96550501Cooperative agreement #: 0Accomplishment count: Phase I Environmental AssessmentAccomplishment type: HGrant type: Not reportedCleanup funding entity: Not reportedAssessment funding entity: Not reportedRedevelopment start date: Not reportedRedev. funding entity name: Not reportedRedev. funding source: Not reportedRedevelopment funding: US EPA - Brownfields Assessment Cooperative AgreementAssessment funding source: 2400Assessment funding: Not reportedCleanup funding source: Not reportedCleanup funding: Not reportedAcres cleaned up: Not reportedCompleted date: Not reportedStart date: 59041ACRES property ID: North American Datum of 1983Datum: Entrance Point of a Facility or StationPoint of reference: Not reportedMap scale: Address Matching-House NumberHCM label: -83.08643Longitude: 42.31392Latitude: Transport; Scotten Co tobacco business. fueling area. Past occupants: Fruehauf Co; Motor City Express; OJ Developed 1889. Site consists of large vacant building and smallProperty Description: 10.97Parcel size: 14/000033-5Property #: FORMER JOHN JAMES SITEProperty name: AssessmentGrant type: Detroit/Wayne County Port AuthorityRecipient name:

US BROWNFIELDS:

1288 ft. Site 5 of 5 in cluster H0.244 mi.

Relative:Higher

Actual:592 ft.

1/8-1/4 DETROIT, MI 48209NW FINDS4005-4117 WEST FORT ST N/AH38 US BROWNFIELDSFORMER JOHN JAMES SITE 1016347557

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Not reportedIron contaminant found: Not reportedCopper contaminant found: Not reportedChromium contaminant found: Not reportedCadmium contaminant found: Not reportedArsenic contaminant found: Not reportedUnknown clean up: Not reportedSVOCs cleaned up: Not reportedSelenium cleaned up: Not reportedPesticides cleaned up: Not reportedNo clean up: Not reportednickel cleaned up: Not reportedmercury cleaned up: Not reportedIron cleaned up: Not reportedCopper cleaned up: Not reportedChromium cleaned up: Not reportedCadmium cleaned up: Not reportedArsenic cleaned up: Not reportedSuperfund Fed. landowner flag: Not reportedGreenspace acreage and type: Not reportedFuture use industrial acreage: Not reportedFuture use commercial acreage: Not reportedFuture use residential acreage: Not reportedFuture use greenspace acreage: 10.97Past use industrial acreage: Not reportedPast use commercial acreage: Not reportedPast use residential acreage: Not reportedPast use greenspace acreage: Not reportedNum. of cleanup and re-dev. jobs: Not reportedCleanup other description: Not reportedVOCs cleaned: YVOCs found: Not reportedSurface water cleaned: Not reportedSoil cleaned up: YSoil affected: Not reportedSediments cleaned: Not reportedSediments found: Not reportedPetro products cleaned: YPetro products found: Not reportedPCBs cleaned up: Not reportedPCBs found: Not reportedPAHs cleaned up: YPAHs found: Not reportedOther contams found description: YOther contaminants found: Not reportedOther metals cleaned: YOther metals found: Not reportedOther cleaned up: Not reportedUnknown media affected: Not reportedNo media affected: Not reportedLead cleaned up: YLead contaminant found: Not reportedGroundwater cleaned: Not reportedGroundwater affected: Not reportedDrinking water cleaned: Not reportedDrinking water affected: Not reportedControled substance cleaned: Not reportedControled substance found:

FORMER JOHN JAMES SITE (Continued) 1016347557

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electronically submit data directly to EPA.is an federal online database for Brownfields Grantees toUS EPA Assessment, Cleanup and Redevelopment Exchange System (ACRES) Environmental Interest/Information System

110038724084Registry ID:

FINDS:

Not reportedPast Use: Multistory Not reportedUnknown media cleaned up: Not reportedIndoor air media cleaned up: Not reportedBuilding material media cleaned up: Not reportedMedia affected indoor air: Not reportedMedia affected Bluiding Material: Not reportedFuture Use: Multistory Not reportedUnknown contaminant found: Not reportedSVOCs contaminant found: Not reportedSelenium contaminant found: Not reportedPesticides contaminant found: Not reportedNo contaminant found: Not reportedNickel contaminant found: Not reportedMercury contaminant found:

FORMER JOHN JAMES SITE (Continued) 1016347557

-83.08623Longitude:42.30772Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

1378 ft.0.261 mi.

Relative:Higher

Actual:581 ft.

1/4-1/2 DETROIT, MI 48214SW 4300, 4461, & 4500 W. JEFFERSON AVE. N/A39 INVENTORYDET/WAYNE CO PORT AUTH WF DEV S114030890

-83.08799Longitude:42.31137Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

1480 ft.0.280 mi.

Relative:Higher

Actual:587 ft.

1/4-1/2 DETROIT, MI 48216West 4333 FORT ST (FORT STREET & CLARK) N/A40 INVENTORYROCKWELL FORMER (FORT & CLARK) S114030809

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stages of operation at the plant. 1866 to 1940. All three methods of gas production were employed at different Alternate Name:MICHIGAN CONSOLIDATED GAS CO. This site operated as an MGP from

Manufactured Gas Plants:

1577 ft.0.299 mi.

Relative:Higher

Actual:585 ft.

1/4-1/2 DETROIT, MI 48216NNE W. JEFFERSON AVE N/A41 EDR MGPDETROIT GAS CO- STATION A 1008408099

Not reported# Of Employees: Not reportedFederal Employer Id Number: Not reportedPermit Contact Person Phone Number: Not reportedPermit Contact Person Area Code: Not reportedPermit Contact Person: Not reportedEI Contact Phone Number: Not reportedEI Contact Area Code: Not reportedEmission Inventory Contact Person: Not reportedCompliance Phone Number: Not reportedCompliance Area Code: Not reportedCompliance Person: Not reportedMailing Zip 4 Extension: Not reportedMailing Zip: Not reportedMailing State: Not reportedMailing City: Not reportedMailing Street: Not reportedMailing Contact Person: Not reportedMailing Name: Not reportedUTM Vertical Coord: Not reportedUTM Horizontal Coord: Not reportedUTM Zone (Geo Coordinates Universal Transverse Mercator System): Not reportedPrincipal Product Description: Not reportedPrincipal Product: Not reportedBusiness Name: Not reportedDun & Brad Street Number: Not reportedSupplemental Location Text: Not reportedFacility Status: Not reportedTribal Code: Not reportedSIC Primary: Not reportedFacility Category: Not reportedState County FIPS: Not reportedRecord Type: SHOTBLAST MACHINE AND BAGHOUSEApplication Reason: Not reportedCountry: M4120State Registration Number: 02/15/1989Date Received: C-7627Permit Number: Not reportedContact City,St,Zip: Not reportedContact Address: Not reportedContact Phone: Not reportedContact Name: Not reportedNaics Code: M4120State Registration Number:

AIRS:

1658 ft.0.314 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 WDSDETROIT, MI 48216NNE BEA3411 W FORT ST N/A42 AIRSMIDWEST SUSPENSION AND BRAKE S108168789

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WAYNEMailing County: 48216Mailing City/State/Zip: 3411 W FORT STMailing Address: MIDWEST SUSPENSION AND BRAKESite Specific Name: 401331WMD Id: MID982617474Site Id:

WDS:

Environmental Response DivisionDivision Assigned: russeljeReviewer: PendingDetermination 20107A: No Hazardous Substance(s)Category: 1Petition Disclosure: AffirmedPetition Determination: BOULEVARD & TRUMBULL INVESTMENTS, INC.Submitter Name: 02/16/1999Date Received: Southeast MIDistrict: 840BEA Number: Not reportedSecondary Address:

BEA:

Not reportedDate Record Was Created: Not reportedReporting Year:

MIDWEST SUSPENSION AND BRAKE (Continued) S108168789

DISCOVERYAction:

Cleaned upPriority Level: 12/08/92Date Completed: 02/21/92Date Started: REMOVALAction:

Not reportedPriority Level: 03/04/92Date Completed: / /Date Started: Notice Letters IssuedAction:

Not reportedPriority Level: 03/04/92Date Completed: / /Date Started: Notice Letters IssuedAction:

CERCLIS-NFRAP Assessment History:

Great LakesDescription:Program Priority:

NFRAP-Site does not qualify for the NPL based on existing informationNon NPL Status: Not on the NPLNPL Status: Not a Federal FacilityFederal Facility: 0506622Site ID:

CERC-NFRAP:

1778 ft.0.337 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 DETROIT, MI 48216North PRP24TH AND SAVOY STREET. MID98563514343 CERC-NFRAP24TH & SAVOY TRAILER 1003873043

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WILES ENTERPRISES CAPITOL ALLIANCE CORPORATIONPRP name:

PRP:

NFRAP-Site does not qualify for the NPL based on existing informationPriority Level: 03/24/94Date Completed: / /Date Started: PRELIMINARY ASSESSMENTAction:

Not reportedPriority Level: 02/24/97Date Completed: / /Date Started: ARCHIVE SITEAction:

Search Complete, No Viable PRPsPriority Level: 05/16/96Date Completed: 02/14/92Date Started: NON-NATIONAL PRIORITIES LIST POTENTIALLY RESPONSIBLE PARTY SEARCHAction:

Not reportedPriority Level: 02/14/92Date Completed: / /Date Started:

24TH & SAVOY TRAILER (Continued) 1003873043

01/22/96Date Completed: / /Date Started: ARCHIVE SITEAction:

Cleaned upPriority Level: 04/16/84Date Completed: 03/28/84Date Started: REMOVALAction:

CERCLIS-NFRAP Assessment History:

Great LakesDescription:Program Priority:

DETROIT, MI 48209 FORT & SCOTTEN STREETAlias Address: FORT & SCOTTEN STAlias Name:

WAYNE, MI Not reportedAlias Address: FORT & SCOTTEN STAlias Name:

CERCLIS-NFRAP Site Alias Name(s):

NFRAP-Site does not qualify for the NPL based on existing informationNon NPL Status: Not on the NPLNPL Status: Not a Federal FacilityFederal Facility: 0505882Site ID:

CERC-NFRAP:

1779 ft. Site 1 of 2 in cluster I0.337 mi.

Relative:Higher

Actual:590 ft.

1/4-1/2 DETROIT, MI 48209WNW FORT & SCOTTEN STREET MID985567650I44 CERC-NFRAPFORT & SCOTTEN STREET 1003872819

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Not reportedPriority Level: 03/28/84Date Completed: / /Date Started: DISCOVERYAction:

NFRAP-Site does not qualify for the NPL based on existing informationPriority Level: 09/25/90Date Completed: / /Date Started: PRELIMINARY ASSESSMENTAction:

Not reportedPriority Level:

FORT & SCOTTEN STREET (Continued) 1003872819

OpenRelease Status: UnknownSubstance Released: 06/03/1997Release Date: C-0381-97Leak Number:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 04/07/1998Release Date: C-0316-98Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08743Longitude: 42.31336Latitude: Vacant LandSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-9031Owner Phone: Frederick RottachOwner Contact: Detroit, MI 48226-2862Owner City,St,Zip: 65 Cadillac Square Suite 1100Owner Address: City of Detroit Planning Development DeptOwner Name: STATE OF MICHIGANSource: 00037985Facility ID:

LUST:

-83.08743Longitude:42.31337Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1830 ft. Site 2 of 2 in cluster I0.347 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 USTDETROIT, MI 48226WNW LUST4235 W FORT N/AI45 INVENTORYVACANT LAND U002303761

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Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/03/1997Remove Date: Not reportedInstall Date: Hazardous SubstanceProduct: Not reportedCapacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: UnknownConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/10/1994Remove Date: 01/01/1940Install Date: MOTOR/OILProduct: 5000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08743Longitude: 42.31336Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-9031Contact Phone: RAMSESH PATELContact: (313) 224-9031Owner Phone: Frederick RottachOwner Contact: USAOwner Country: DETROIT, MI 48226-2862Owner City,St,Zip: 65 CADILLAC SQUARE SUITE 1100Owner Address: CITY OF DETROIT PLANNING DEVELOPMENT DEPTOwner Name: CLOSEDFacility Type: 00037985Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 06/04/1997Release Date: C-0389-97Leak Number:

Not reportedRelease Closed Date: OpenRelease Status: KeroseneSubstance Released: 04/25/1994Release Date: C-0387-94Leak Number:

Not reportedRelease Closed Date:

VACANT LAND (Continued) U002303761

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 04/07/1998Remove Date: Not reportedInstall Date: Hazardous SubstanceProduct: 11700Capacity: Removed from GroundTank Status: 4Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/04/1997Remove Date: Not reportedInstall Date: TRANSMISSION FLUIDProduct: Not reportedCapacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: UnknownPiping Material:

VACANT LAND (Continued) U002303761

No RequestPetition Determination: Ambassador Port CompanySubmitter Name: 09/21/2005Date Received: Southeast MIDistrict: 2912BEA Number: 4300 W. JeffersonSecondary Address:

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: Same Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: Nicholson Terminal and Dock Co.Submitter Name: 10/06/2005Date Received: Southeast MIDistrict: 2925BEA Number: 4300 W. JeffersonSecondary Address:

BEA:

1921 ft. Site 1 of 2 in cluster J0.364 mi.

Relative:Higher

Actual:581 ft.

1/4-1/2 DETROIT, MI 482SW WDS4461 W. JEFFERSON N/AJ46 BEAAMBASSADOR PORT COMPANY S105966638

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WAYNEMailing County: 48209Mailing City/State/Zip: 4461 W JEFFERSON AVEMailing Address: DETROIT MARINE TERMINALS INCSite Specific Name: 477657WMD Id: MIK857563316Site Id:

WDS:

Environmental Response DivisionDivision Assigned: thorntopReviewer: DeniedDetermination 20107A: Same Hazardous Substance(s)Category: 1Petition Disclosure: DeniedPetition Determination: Detroit Marine Terminals, IncSubmitter Name: 09/05/2003Date Received: Southeast MIDistrict: 2119BEA Number: Not reportedSecondary Address:

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: Same Hazardous Substance(s)Category: 0Petition Disclosure:

AMBASSADOR PORT COMPANY (Continued) S105966638

FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08806Longitude: 42.31309Latitude: City Of Detroit - Vacant LotSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: Detroit, MI 48226-2619Owner City,St,Zip: 150 W Michigan Ave7Tth FloorOwner Address: City of DetroitOwner Name: STATE OF MICHIGANSource: 00037968Facility ID:

LUST:

-83.08807Longitude:42.31309Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1933 ft. Site 1 of 3 in cluster K0.366 mi.

Relative:Higher

Actual:588 ft.

1/4-1/2 USTDETROIT, MI 48226WNW LUST4301 W FORT ST N/AK47 INVENTORYNONE-VACANT LAND U003326291

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/10/1994Remove Date: 01/01/1940Install Date: KeroseneProduct: 11750Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08806Longitude: 42.31309Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-3894Contact Phone: R RYBINSKI/D FISHERContact: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: USAOwner Country: DETROIT, MI 48226-2619Owner City,St,Zip: 150 W MICHIGAN AVE7TTH FLOOROwner Address: CITY OF DETROITOwner Name: CLOSEDFacility Type: 00037968Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: OtherSubstance Released: 04/27/1994Release Date: C-0373-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data:

NONE-VACANT LAND (Continued) U003326291

-83.08915Longitude:42.31108Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1962 ft. Site 1 of 4 in cluster L0.372 mi. WDS

Relative:Higher

Actual:586 ft.

1/4-1/2 USTDETROIT, MI 48226West LUST412 CLARK N/AL48 INVENTORYVACANT LAND U002303754

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Removed from GroundTank Status: 1Tank ID:

-83.08915Longitude: 42.31108Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-9031Contact Phone: RAMESH PATELContact: (313) 224-9031Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48226Owner City,St,Zip: 1602 CADILLAC TOWEROwner Address: CITY OF DETROIT / PLANNING DEVELOPMENT DEPTOwner Name: CLOSEDFacility Type: 00037976Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: GasolineSubstance Released: 04/21/1994Release Date: C-0355-94Leak Number:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 04/30/1998Release Date: C-0335-98Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08915Longitude: 42.31108Latitude: Vacant LandSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-9031Owner Phone: Not reportedOwner Contact: Detroit, MI 48226Owner City,St,Zip: 1602 Cadillac TowerOwner Address: City Of Detroit / Planning Development DeptOwner Name: STATE OF MICHIGANSource: 00037976Facility ID:

LUST:

VACANT LAND (Continued) U002303754

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WAYNEMailing County: 48209Mailing City/State/Zip: 412 CLARK STMailing Address: CITY OF DETROITSite Specific Name: 443073WMD Id: MIG000040964Site Id:

WDS:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 04/30/1998Remove Date: Not reportedInstall Date: GasolineProduct: 1370Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/10/1994Remove Date: 01/01/1952Install Date: GasolineProduct: 12000Capacity:

VACANT LAND (Continued) U002303754

Environmental Response DivisionDivision Assigned: temppmReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: CROWN ENTERPRISESSubmitter Name: 01/26/1996Date Received: Southeast MIDistrict: 53BEA Number: Not reportedSecondary Address:

BEA:

1963 ft.0.372 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 DETROIT, MI NNE 3333 FORT STREET N/A49 BEACROWN ENTERPRISES S104909741

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04/09/1982Install Date: GasolineProduct: 1000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08710Longitude: 42.30746Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 884-4887Contact Phone: MICHELLE LOWINContact: (313) 884-4887Owner Phone: Not reportedOwner Contact: USAOwner Country: GROSSE PTE, MI 48923Owner City,St,Zip: 17108 MACK AVEOwner Address: PHILIP BRUSHAOwner Name: CLOSEDFacility Type: 00008709Facility ID:

UST:

06/02/2000Release Closed Date: ClosedRelease Status: UnknownSubstance Released: 01/20/2000Release Date: C-0064-00Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08710Longitude: 42.30746Latitude: Gib-sar Properties IncSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 884-4887Owner Phone: Not reportedOwner Contact: GROSSE PTE, MI 48923Owner City,St,Zip: 17108 MACK AVEOwner Address: Philip BrushaOwner Name: STATE OF MICHIGANSource: 00008709Facility ID:

LUST:

1966 ft. Site 2 of 2 in cluster J0.372 mi.

Relative:Higher

Actual:581 ft.

1/4-1/2 WDSDETROIT, MI 48209SW UST4473 W JEFFERSON AVE N/AJ50 LUSTGIB-SAR PROPERTIES INC U003321379

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WAYNEMailing County: 48209Mailing City/State/Zip: 4473 W JEFFERSON AVEMailing Address: MICHELLE LOWINSite Specific Name: 424395WMD Id: MIG000059118Site Id:

WDS:

NoImpressed Device: Cathodically Protected SteelConstruction Material: Not reportedPiping Type: Bare SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 01/10/2000Remove Date:

GIB-SAR PROPERTIES INC (Continued) U003321379

Not reportedRelease Closed Date: OpenRelease Status: OtherSubstance Released: 04/20/1994Release Date: C-0348-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08918Longitude: 42.31112Latitude: City Of Detroit - Vacant LotSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: Detroit, MI 48226-2619Owner City,St,Zip: 150 W Michigan Ave7Tth FloorOwner Address: City of DetroitOwner Name: STATE OF MICHIGANSource: 00037988Facility ID:

LUST:

-83.08918Longitude:42.31112Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

1978 ft. Site 2 of 4 in cluster L0.375 mi.

Relative:Higher

Actual:586 ft.

1/4-1/2 USTDETROIT, MI 48226West LUST422 CLARK AVE N/AL51 INVENTORYNONE-VACANT LAND U002303760

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Suction: No Valve At TankPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 05/10/1994Remove Date: 01/01/1946Install Date: FUEL/OILProduct: 2000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08918Longitude: 42.31112Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 224-3894Contact Phone: RICHARD RYBINSKI/D FISHERContact: (313) 224-0154Owner Phone: Ramesh PatelOwner Contact: USAOwner Country: DETROIT, MI 48226-2619Owner City,St,Zip: 150 W MICHIGAN AVE7TTH FLOOROwner Address: CITY OF DETROITOwner Name: CLOSEDFacility Type: 00037988Facility ID:

UST:

NONE-VACANT LAND (Continued) U002303760

-83.08799Longitude:42.31137Latitude:BEAData Source:Southeast MIDistrict:DetroitTownship:201205408LVBea Number:

INVENTORY:

1988 ft. Site 2 of 3 in cluster K0.377 mi.

Relative:Higher

Actual:588 ft.

1/4-1/2 WAYNE (County), MI 48209WNW 4333-4335 WEST FORT STREET N/AK52 INVENTORYROCKWELL FORMER (FORT & CLARK) S114030810

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RRDDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: Not reportedCategory: 0Petition Disclosure: No RequestPetition Determination: JLK Real Estate Holdings, LLCSubmitter Name: 12/12/2012Date Received: Southeast MIDistrict: 5408BEA Number: Not reportedSecondary Address:

BEA:

1988 ft. Site 3 of 3 in cluster K0.377 mi.

Relative:Higher

Actual:588 ft.

1/4-1/2 DETROIT, MI 48209WNW 4333-4335 WEST FORT STREET N/AK53 BEAROCKWELL FORMER (FORT & CLARK) S113193123

UnknownCleanup required: NDid owner change: Mistro, LLCCurrent owner: PrivateOwnership entity: 96550501Cooperative agreement #: 1Accomplishment count: Phase I Environmental AssessmentAccomplishment type: HGrant type: Not reportedCleanup funding entity: Not reportedAssessment funding entity: Not reportedRedevelopment start date: Not reportedRedev. funding entity name: Not reportedRedev. funding source: Not reportedRedevelopment funding: US EPA - Brownfields Assessment Cooperative AgreementAssessment funding source: 2050Assessment funding: Not reportedCleanup funding source: Not reportedCleanup funding: Not reportedAcres cleaned up: Not reportedCompleted date: Not reportedStart date: 106423ACRES property ID: North American Datum of 1983Datum: Entrance Point of a Facility or StationPoint of reference: Not reportedMap scale: Address Matching-House NumberHCM label: -83.090200Longitude: 42.310000Latitude: Not reportedProperty Description: 7.86Parcel size: 14/010249-50Property #: FORT AND CLARKProperty name: AssessmentGrant type: Detroit/Wayne County Port AuthorityRecipient name:

US BROWNFIELDS:

2069 ft.0.392 mi.

Relative:Higher

Actual:588 ft.

1/4-1/2 DETROIT, MI 48209West FINDSSOUTHWEST CORNER OF FORT AND CLARK N/A54 US BROWNFIELDSFORT AND CLARK 1016353355

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Not reportedArsenic cleaned up: Not reportedSuperfund Fed. landowner flag: Not reportedGreenspace acreage and type: Not reportedFuture use industrial acreage: Not reportedFuture use commercial acreage: Not reportedFuture use residential acreage: Not reportedFuture use greenspace acreage: 7.86Past use industrial acreage: Not reportedPast use commercial acreage: Not reportedPast use residential acreage: Not reportedPast use greenspace acreage: Not reportedNum. of cleanup and re-dev. jobs: Not reportedCleanup other description: Not reportedVOCs cleaned: Not reportedVOCs found: Not reportedSurface water cleaned: Not reportedSoil cleaned up: YSoil affected: Not reportedSediments cleaned: Not reportedSediments found: Not reportedPetro products cleaned: Not reportedPetro products found: Not reportedPCBs cleaned up: Not reportedPCBs found: Not reportedPAHs cleaned up: Not reportedPAHs found: Not reportedOther contams found description: Not reportedOther contaminants found: Not reportedOther metals cleaned: Not reportedOther metals found: Not reportedOther cleaned up: Not reportedUnknown media affected: Not reportedNo media affected: Not reportedLead cleaned up: Not reportedLead contaminant found: Not reportedGroundwater cleaned: Not reportedGroundwater affected: Not reportedDrinking water cleaned: Not reportedDrinking water affected: Not reportedControled substance cleaned: Not reportedControled substance found: Not reportedAsbestos cleaned: Not reportedAsbestos found: Not reportedAir cleaned: Not reportedAir contaminated: Not reportedState/tribal NFA date: Not reportedState/tribal program ID: Not reportedState/tribal program date: Not reportedIC in place: Not reportedIC in place date: Not reportedIC cat. enforcement permit tools: Not reportedIC cat. gov. controls: Not reportedIC cat. info. devices: Not reportedIC Category proprietary controls: Not reportedInstitutional controls required: YesPhoto available: NoVideo available:

FORT AND CLARK (Continued) 1016353355

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Not reportedCleanup funding entity: Not reportedAssessment funding entity: Not reportedRedevelopment start date: Not reportedRedev. funding entity name: Not reportedRedev. funding source: Not reportedRedevelopment funding: US EPA - Brownfields Assessment Cooperative AgreementAssessment funding source: 1000Assessment funding: Not reportedCleanup funding source: Not reportedCleanup funding: Not reportedAcres cleaned up: Not reportedCompleted date: Not reportedStart date: 106423ACRES property ID: North American Datum of 1983Datum: Entrance Point of a Facility or StationPoint of reference: Not reportedMap scale: Address Matching-House NumberHCM label: -83.090200Longitude: 42.310000Latitude: Not reportedProperty Description: 7.86Parcel size: 14/010249-50Property #: FORT AND CLARKProperty name: AssessmentGrant type: Detroit/Wayne County Port AuthorityRecipient name:

Not reportedPast Use: Multistory Not reportedUnknown media cleaned up: Not reportedIndoor air media cleaned up: Not reportedBuilding material media cleaned up: Not reportedMedia affected indoor air: Not reportedMedia affected Bluiding Material: Not reportedFuture Use: Multistory Not reportedUnknown contaminant found: Not reportedSVOCs contaminant found: Not reportedSelenium contaminant found: Not reportedPesticides contaminant found: Not reportedNo contaminant found: Not reportedNickel contaminant found: Not reportedMercury contaminant found: Not reportedIron contaminant found: Not reportedCopper contaminant found: Not reportedChromium contaminant found: Not reportedCadmium contaminant found: Not reportedArsenic contaminant found: Not reportedUnknown clean up: Not reportedSVOCs cleaned up: Not reportedSelenium cleaned up: Not reportedPesticides cleaned up: Not reportedNo clean up: Not reportednickel cleaned up: Not reportedmercury cleaned up: Not reportedIron cleaned up: Not reportedCopper cleaned up: Not reportedChromium cleaned up: Not reportedCadmium cleaned up:

FORT AND CLARK (Continued) 1016353355

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Not reportedPast use commercial acreage: Not reportedPast use residential acreage: Not reportedPast use greenspace acreage: Not reportedNum. of cleanup and re-dev. jobs: Not reportedCleanup other description: Not reportedVOCs cleaned: Not reportedVOCs found: Not reportedSurface water cleaned: Not reportedSoil cleaned up: YSoil affected: Not reportedSediments cleaned: Not reportedSediments found: Not reportedPetro products cleaned: Not reportedPetro products found: Not reportedPCBs cleaned up: Not reportedPCBs found: Not reportedPAHs cleaned up: Not reportedPAHs found: Not reportedOther contams found description: Not reportedOther contaminants found: Not reportedOther metals cleaned: Not reportedOther metals found: Not reportedOther cleaned up: Not reportedUnknown media affected: Not reportedNo media affected: Not reportedLead cleaned up: Not reportedLead contaminant found: Not reportedGroundwater cleaned: Not reportedGroundwater affected: Not reportedDrinking water cleaned: Not reportedDrinking water affected: Not reportedControled substance cleaned: Not reportedControled substance found: Not reportedAsbestos cleaned: Not reportedAsbestos found: Not reportedAir cleaned: Not reportedAir contaminated: Not reportedState/tribal NFA date: Not reportedState/tribal program ID: Not reportedState/tribal program date: Not reportedIC in place: Not reportedIC in place date: Not reportedIC cat. enforcement permit tools: Not reportedIC cat. gov. controls: Not reportedIC cat. info. devices: Not reportedIC Category proprietary controls: Not reportedInstitutional controls required: YesPhoto available: NoVideo available: UnknownCleanup required: NDid owner change: Mistro, LLCCurrent owner: PrivateOwnership entity: 96550501Cooperative agreement #: 0Accomplishment count: Supplemental AssessmentAccomplishment type: HGrant type:

FORT AND CLARK (Continued) 1016353355

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electronically submit data directly to EPA.is an federal online database for Brownfields Grantees toUS EPA Assessment, Cleanup and Redevelopment Exchange System (ACRES) Environmental Interest/Information System

110040216637Registry ID:

FINDS:

Not reportedPast Use: Multistory Not reportedUnknown media cleaned up: Not reportedIndoor air media cleaned up: Not reportedBuilding material media cleaned up: Not reportedMedia affected indoor air: Not reportedMedia affected Bluiding Material: Not reportedFuture Use: Multistory Not reportedUnknown contaminant found: Not reportedSVOCs contaminant found: Not reportedSelenium contaminant found: Not reportedPesticides contaminant found: Not reportedNo contaminant found: Not reportedNickel contaminant found: Not reportedMercury contaminant found: Not reportedIron contaminant found: Not reportedCopper contaminant found: Not reportedChromium contaminant found: Not reportedCadmium contaminant found: Not reportedArsenic contaminant found: Not reportedUnknown clean up: Not reportedSVOCs cleaned up: Not reportedSelenium cleaned up: Not reportedPesticides cleaned up: Not reportedNo clean up: Not reportednickel cleaned up: Not reportedmercury cleaned up: Not reportedIron cleaned up: Not reportedCopper cleaned up: Not reportedChromium cleaned up: Not reportedCadmium cleaned up: Not reportedArsenic cleaned up: Not reportedSuperfund Fed. landowner flag: Not reportedGreenspace acreage and type: Not reportedFuture use industrial acreage: Not reportedFuture use commercial acreage: Not reportedFuture use residential acreage: Not reportedFuture use greenspace acreage: 7.86Past use industrial acreage:

FORT AND CLARK (Continued) 1016353355

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Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 10/05/2004Date of Collection: (734) 654-9800Contact Phone: ROGER HOMRICHContact: (734) 654-9800Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48141Owner City,St,Zip: 200 MATLIN RDOwner Address: ROGER HOMRICHOwner Name: CLOSEDFacility Type: 00040337Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: UnknownSubstance Released: 01/27/2000Release Date: C-0111-00Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 10/05/2004Date of Collection: -83.09018Longitude: 42.31239Latitude: Dalray Port AuthoritySite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (734) 654-9800Owner Phone: Not reportedOwner Contact: DETROIT, MI 48141Owner City,St,Zip: 200 MATLIN RDOwner Address: Roger HomrichOwner Name: STATE OF MICHIGANSource: 00040337Facility ID:

LUST:

-83.09019Longitude:42.3124Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

2128 ft. Site 3 of 4 in cluster L0.403 mi.

Relative:Higher

Actual:586 ft.

1/4-1/2 USTDETROIT, MI 48141West LUST4401-65 FORT ST N/AL55 INVENTORYDALRAY PORT AUTHORITY U003758816

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NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Not reportedPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 01/26/2000Remove Date: Not reportedInstall Date: GasolineProduct: 1000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.09018Longitude: 42.31239Latitude: Address Matching-House NumberMethod of Collection:

DALRAY PORT AUTHORITY (Continued) U003758816

Not reportedRelease Closed Date: OpenRelease Status: GasolineSubstance Released: 11/15/1996Release Date: C-0941-96Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.09049Longitude: 42.31236Latitude: Corner Of Fort & Clark StSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: Not reportedOwner Phone: Not reportedOwner Contact: Unknown, MI 99999Owner City,St,Zip: UnknownOwner Address: Nrt OwnerOwner Name: STATE OF MICHIGANSource: 50001941Facility ID:

LUST:

-83.09049Longitude:42.31236Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

2135 ft. Site 4 of 4 in cluster L0.404 mi.

Relative:Higher

Actual:586 ft.

1/4-1/2 DETROIT, MI 99999West LUST4400 FORT ST. N/AL56 INVENTORYCORNER OF FORT & CLARK ST S102726357

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Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (312) 886-4170Contact Phone: MICHAEL GELBERContact: (312) 353-5610Owner Phone: Not reportedOwner Contact: USAOwner Country: CHICAGO, IL 60604-1492Owner City,St,Zip: 230 S DEARBORN ST STE 3670Owner Address: US GOVERNMENT - GSAOwner Name: CLOSEDFacility Type: 00006701Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: Gasoline,DieselSubstance Released: 06/07/1991Release Date: C-1097-91Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.07819Longitude: 42.31828Latitude: Ambassador Bridge Fed-fac #65Site Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (312) 353-5610Owner Phone: Not reportedOwner Contact: Chicago, IL 60604-1492Owner City,St,Zip: 230 S Dearborn St Ste 3670Owner Address: US Government - GsaOwner Name: STATE OF MICHIGANSource: 00006701Facility ID:

LUST:

-83.0782Longitude:42.31829Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

2274 ft.0.431 mi. WDS

Relative:Higher

Actual:588 ft.

1/4-1/2 USTDETROIT, MI 60604NNE LUST805 21ST ST N/A57 INVENTORYAMBASSADOR BRIDGE FED-FAC #65 U000266645

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Not reportedMailing County: 60604Mailing City/State/Zip: 230 S DEARBORN ST RM 3670Mailing Address: US CARGO INSPECTION FACILITYSite Specific Name: 391908WMD Id: MI2471490340Site Id:

WDS:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 07/01/1991Remove Date: Not reportedInstall Date: GasolineProduct: Not reportedCapacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 07/01/1991Remove Date: Not reportedInstall Date: DieselProduct: 12000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.07819Longitude: 42.31828Latitude: Address Matching-House NumberMethod of Collection:

AMBASSADOR BRIDGE FED-FAC #65 (Continued) U000266645

Not reportedProperty Or Description Restricted Area: NAER-ERD-00-005MDEQ Reference Number: 15220100005Based On The Deq Ref #: Not reportedLegal Description Of Property: Not reportedProgram Support Assigned Date: Not reportedProgram Support Assigned User: Part 201Program Type: NAERLand Use Restriction Type: Anaconda BrassProperty: Anaconda BrassSite Name: PendingStatus:

AUL:

2317 ft. Site 1 of 3 in cluster M0.439 mi.

Relative:Higher

Actual:582 ft.

1/4-1/2 DETROIT CITY, MI 48209SW 4610 WEST JEFFERSON AVENUE N/AM58 AULANACONDA BRASS S113406468

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Not reportedComment: YesMap Comments: Not reportedThere Is A Permanent Marker On The Site: Not reportedThere Is A Health And Safety Plan: Not reportedThere Is An Exposure Barrier In Place: Not reportedMonitoring Well Protected, No Tampering Or Removal: Not reportedThere Is A Restriction On All Construction: Not reportedSoil Movement Requirements: Not reportedExcavation And Soil Movement Restrictions: Not reportedSpecial Building Restrictions: Not reportedSpecial Well Construction Requirements: Not reportedGroundwater Contact Restrictions: Not reportedGroundwater Consumption Restrictions: Not reportedSite Specific Restrictions: Not reportedMultiple Land-Use Restrictions: Not reportedRecreational Land Use Restriction: Not reportedResidential Land Use Restriction: Not reportedIndustrial Land Use Restriction: Not reportedCommercial Iv Land Use Restriction: Not reportedCommercial Iii Land Use Restriction: Not reportedCommercial Ii Land Use Restriction: Not reportedCommercial I Land Use Restriction: Not reportedDate Legal Paperwork Stamped/Filed/Register Of Deeds: Not reportedProgram Used To Map Restricted Features: Not reportedIndividual Or Staff Assoc With The Mapping: Not reportedDate Data Entry Finished: Not reportedDate Data Entry Started: Not reportedMapped Polygons Area In Square Miles: Not reportedMapped Polygons Area In Acres: Not reportedFile Name Of Hyperlinked Legal Doc: ERDLead Division:

ANACONDA BRASS (Continued) S113406468

42.3071Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

Not reportedPollutants: Not reportedQuarter/Quarter: SEQuarter: 23Section: 11ERange: 02STownship: 04/14/1994SAM Score Date: 32SAM Score: Primary Metal ProductsSource: Interim Response conducted - No further activities anticipatedFacility Status: 82001505Facility ID:

PART 201:

2317 ft. Site 2 of 3 in cluster M0.439 mi.

Relative:Higher

Actual:582 ft.

1/4-1/2 BROWNFIELDSDETROIT, MI 48209SW INVENTORY4610 W. JEFFERSON N/AM59 PART 201ANACONDA BRASS S105144839

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82001505Ernie Id Number: NoBEA: Not reportedUse at Time of Listing: Not reportedProperry Use: Not reportedStatus: 1Region: Not reportedFacility ID:

BROWNFIELD:

-83.08897Longitude:

ANACONDA BRASS (Continued) S105144839

FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (248) 399-3300Contact Phone: John PoldermanContact: Not reportedOwner Phone: Not reportedOwner Contact: USAOwner Country: DEARBORN, MI 48126Owner City,St,Zip: 5960 REUTEROwner Address: AREF BAZZIOwner Name: ACTIVEFacility Type: 00016625Facility ID:

UST:

03/17/1992Release Closed Date: ClosedRelease Status: Not reportedSubstance Released: 05/07/1991Release Date: C-0851-91Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.09064Longitude: 42.31259Latitude: Mobil #03jt2-747 ClarkSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: Not reportedOwner Phone: Not reportedOwner Contact: Dearborn, MI 48126Owner City,St,Zip: 5960 ReuterOwner Address: Aref BazziOwner Name: STATE OF MICHIGANSource: 00016625Facility ID:

LUST:

2318 ft.0.439 mi.

Relative:Higher

Actual:585 ft.

1/4-1/2 WDSDETROIT, MI 48126WNW UST747 CLARK ST N/A60 LUSTAREF BAZZI U003426026

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Not reportedTank Release Detection: 06/01/1987Remove Date: 04/22/1967Install Date: Used OilProduct: 550Capacity: Removed from GroundTank Status: 4Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: Not reportedPiping Type: Fiberglass reinforced plasticPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/01/1987Remove Date: 04/22/1983Install Date: GasolineProduct: 10000Capacity: Removed from GroundTank Status: 3Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: Not reportedPiping Type: Fiberglass reinforced plasticPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/01/1987Remove Date: 04/22/1983Install Date: GasolineProduct: 6000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: Not reportedPiping Type: Fiberglass reinforced plasticPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 06/01/1987Remove Date: 04/22/1983Install Date: GasolineProduct: 8000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.09064Longitude: 42.31259Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum:

AREF BAZZI (Continued) U003426026

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Automatic Line Leak Detectors,Line Tightness TestingPipe Realease Detection: Automatic Tank GaugingTank Release Detection: Not reportedRemove Date: 05/01/1987Install Date: GasolineProduct: 10000Capacity: Currently In UseTank Status: 8Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: PressurePiping Type: Fiberglass reinforced plasticPiping Material: Automatic Line Leak Detectors,Line Tightness TestingPipe Realease Detection: Automatic Tank GaugingTank Release Detection: Not reportedRemove Date: 05/01/1987Install Date: GasolineProduct: 10000Capacity: Currently In UseTank Status: 7Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: PressurePiping Type: Fiberglass reinforced plasticPiping Material: Automatic Line Leak Detectors,Line Tightness TestingPipe Realease Detection: Automatic Tank GaugingTank Release Detection: Not reportedRemove Date: 05/01/1987Install Date: GasolineProduct: 10000Capacity: Currently In UseTank Status: 6Tank ID:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: PressurePiping Type: Fiberglass reinforced plasticPiping Material: Automatic Line Leak Detectors,Line Tightness TestingPipe Realease Detection: Automatic Tank GaugingTank Release Detection: Not reportedRemove Date: 05/01/1987Install Date: GasolineProduct: 10000Capacity: Currently In UseTank Status: 5Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Galvanized SteelPiping Material: Not reportedPipe Realease Detection:

AREF BAZZI (Continued) U003426026

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WAYNEMailing County: 48226Mailing City/State/Zip: 250 W LARNED STMailing Address: CITY OF DETROIT FIRE DEPARTMENTSite Specific Name: 483900WMD Id: MIK781789433Site Id:

WAYNEMailing County: 48209Mailing City/State/Zip: 747 CLARK STMailing Address: MOBIL OIL CORPSite Specific Name: 440215WMD Id: MIG000046398Site Id:

WDS:

NoImpressed Device: Fiberglass Reinforced plasticConstruction Material: PressurePiping Type: Fiberglass reinforced plasticPiping Material:

AREF BAZZI (Continued) U003426026

08/24/1994Release Date: C-0935-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.08909Longitude: 42.30581Latitude: Nicholson TerminalSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 237-4622Owner Phone: Not reportedOwner Contact: Detroit, MI 48226-4443Owner City,St,Zip: 150 W Jefferson Ave Ste 1000Owner Address: Detroit Economic Develop CorpOwner Name: STATE OF MICHIGANSource: 00037937Facility ID:

LUST:

-83.08909Longitude:42.30582Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

2440 ft. Site 3 of 3 in cluster M0.462 mi. WDS

Relative:Higher

Actual:582 ft.

1/4-1/2 USTDETROIT, MI 48226SW LUST4685 W JEFFERSON N/AM61 INVENTORYFORMER NICHOLSON TERMINAL U002303776

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MOTOR CITY BUILDING MATERIALSSite Specific Name: 391046WMD Id: MI0000372896Site Id:

WDS:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: Secondary ContainmentPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 08/25/1994Remove Date: 01/01/1988Install Date: GasolineProduct: 2000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 08/25/1994Remove Date: 01/01/1965Install Date: DieselProduct: 3000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.08909Longitude: 42.30581Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 841-0070Contact Phone: JAMES DANFORTHContact: (313) 237-4622Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48226-4443Owner City,St,Zip: 150 W JEFFERSON AVE STE 1000Owner Address: DETROIT ECONOMIC DEVELOP CORPOwner Name: CLOSEDFacility Type: 00037937Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: DieselSubstance Released:

FORMER NICHOLSON TERMINAL (Continued) U002303776

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WAYNEMailing County: 48209Mailing City/State/Zip: 4005 W FORT STMailing Address:

FORMER NICHOLSON TERMINAL (Continued) U002303776

Not reportedContact Email: On-Scene Coordinator (OSC)Contact Title: (734) 692-7689Contact Tel: ROSANNE ELLISONContact Name: 5270355.00000Contact ID:

Not reportedContact Email: On-Scene Coordinator (OSC)Contact Title: Not reportedContact Tel: GEORGE HUDAKContact Name: 5270182.00000Contact ID:

CERCLIS Site Contact Name(s):

Not reportedSite FUDS Flag: Not reportedAlias EPA ID: Not reportedCC Concurrence FY: / /CC Concurrence Date: 26163Site Fips Code: 01/27/00Non NPL Status Date: Referred to Removal - NFRAPNon NPL Status: Not reportedRResp Fed Agency Code: Not reportedRBRAC Code: Not reportedDMNSN Unit Code: Not on the NPLNPL Status: Not reportedSite Settings Code: Not reportedClassification: 05EPA Region: Not reportedRST Code: Not reportedParent ID: Not reportedNFRAP Flag: Not reportedSite Init By Prog: Not reportedUSGS Quadrangle: Not reportedRCRA ID: NSite Orphan Flag: 0.00000DMNSN Number: Not a Federal FacilityFederal Facility: Not reportedUSGC Hydro Unit: 2160SMSA Number: 05SKIFMS ID: 15Congressional District: ANACONDA INDUSTRIES BRASSShort Name: WAYNEFacility County: MID065608739EPA ID: 0507126Site ID:

CERCLIS:

2458 ft.0.466 mi.

Relative:Higher

Actual:584 ft.

1/4-1/2 DETROIT, MI 48209SW RCRA NonGen / NLR271 S SUMMIT ST MID06560873962 CERCLISMI DEPT/NATURAL RESOURCES AND ENVIRONMENT 1015731314

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Federal EnforcementPrimary Responsibility: SITEWIDEOperable Unit: Not reportedPriority Level: 11/22/95Date Completed: 04/07/95Date Started: NON-NATIONAL PRIORITIES LIST POTENTIALLY RESPONSIBLE PARTY SEARCHAction: 001Action Code:

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Not reportedUrgency Indicator: Not reportedPlanning Status: Federal EnforcementPrimary Responsibility: SITEWIDEOperable Unit: Not reportedPriority Level: 04/07/95Date Completed: / /Date Started: Notice Letters IssuedAction: 002Action Code:

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Not reportedUrgency Indicator: Not reportedPlanning Status: Federal EnforcementPrimary Responsibility: SITEWIDEOperable Unit: Not reportedPriority Level: 04/07/95Date Completed: / /Date Started: ISSUE REQUEST LETTERS (104E)Action: 002Action Code:

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Not reportedUrgency Indicator: Not reportedPlanning Status: EPA Fund-FinancedPrimary Responsibility: SITEWIDEOperable Unit: Not reportedPriority Level: 07/29/92Date Completed: / /Date Started: DISCOVERYAction: 001Action Code:

CERCLIS Assessment History:

Not reportedSite Description: Not reportedAlias Comments: MI Not reportedAlias Address: AMERICAN ANACONDAAlias Name: 101Alias ID:

CERCLIS Site Alias Name(s):

MI DEPT/NATURAL RESOURCES AND ENVIRONMENT (Continued) 1015731314

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Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (517) 373-9892Contact telephone: USContact country: DETROIT, MI 48209 271 S SUMMIT STContact address: PAUL GAUTHIERContact: LANSING, MI 48909 PO BOX 30028Mailing address: MID065608739EPA ID: DETROIT, MI 48209 271 S SUMMIT STFacility address: MI DEPT/NATURAL RESOURCES AND ENVIRONMENTFacility name: 09/13/2005Date form received by agency:

RCRA NonGen / NLR:

2 additional US CERCLIS Financial: record(s) in the EDR Site Report.Click this hyperlink while viewing on your computer to access

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Not reportedUrgency Indicator: Not reportedPlanning Status: State, Fund FinancedPrimary Responsibility: SITEWIDEOperable Unit: NFRAP-Site does not qualify for the NPL based on existing informationPriority Level: 09/26/96Date Completed: / /Date Started: PRELIMINARY ASSESSMENTAction: 001Action Code:

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Time CriticalUrgency Indicator: PrimaryPlanning Status: EPA Fund-FinancedPrimary Responsibility: SITEWIDEOperable Unit: Partially Cleaned upPriority Level: 11/22/95Date Completed: 09/07/95Date Started: REMOVALAction: 001Action Code:

For detailed financial records, contact EDR for a Site Report.:

Not reportedAction Anomaly: Not reportedUrgency Indicator: Not reportedPlanning Status:

MI DEPT/NATURAL RESOURCES AND ENVIRONMENT (Continued) 1015731314

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Not a generator, verifiedClassification: MI DEPT/NATURAL RESOURCES AND ENVIRONMENTSite name: 11/17/1980Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Large Quantity GeneratorClassification: MI DEPT/NATURAL RESOURCES AND ENVIRONMENTSite name: 09/22/1995Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/NATURAL RESOURCES AND ENVIRONMENTSite name: 11/13/2000Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 09/14/2005Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 09/14/2005Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported

MI DEPT/NATURAL RESOURCES AND ENVIRONMENT (Continued) 1015731314

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No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

MI DEPT/NATURAL RESOURCES AND ENVIRONMENT (Continued) 1015731314

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: American Tower CorporationSubmitter Name: 10/05/2001Date Received: Southeast MIDistrict: 1514BEA Number: Not reportedSecondary Address:

BEA:

2469 ft. Site 1 of 2 in cluster N0.468 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 DETROIT, MI 48209WSW 100 S. SUMMIT ST. N/AN63 BEA S105768267

Not reportedLongitude:Not reportedLatitude:BEAData Source:Southeast MIDistrict:DetroitTownship:200101514LVBea Number:

INVENTORY:

2469 ft. Site 2 of 2 in cluster N0.468 mi.

Relative:Higher

Actual:589 ft.

1/4-1/2 WAYNE (County), MI 48209WSW 100 S. SUMMIT ST. N/AN64 INVENTORY S114021788

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: 2781 CorporationSubmitter Name: 08/09/2004Date Received: Southeast MIDistrict: 2488BEA Number: Not reportedSecondary Address:

BEA:

2531 ft. Site 1 of 2 in cluster O0.479 mi.

Relative:Higher

Actual:586 ft.

1/4-1/2 DETROIT, MI NE 2781 WEST JEFFERSON N/AO65 BEA2781 CORPORATION S106521784

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05/02/1966Install Date: GasolineProduct: 2000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.05340Longitude: 42.40957Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: (313) 924-2705Contact Phone: ED BARNASContact: (313) 924-2700Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48211Owner City,St,Zip: 1921 E PERRYOwner Address: DEAN PERAKISOwner Name: CLOSEDFacility Type: 00012168Facility ID:

UST:

03/03/1995Release Closed Date: ClosedRelease Status: GasolineSubstance Released: 11/30/1994Release Date: C-1471-94Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.05340Longitude: 42.40957Latitude: Artic Rentals (former)Site Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 924-2700Owner Phone: Not reportedOwner Contact: DETROIT, MI 48211Owner City,St,Zip: 1921 E PERRYOwner Address: Dean PerakisOwner Name: STATE OF MICHIGANSource: 00012168Facility ID:

LUST:

2561 ft.0.485 mi.

Relative:Higher

Actual:584 ft.

1/4-1/2 DETROIT, MI 48211West UST4629 FORT ST N/A66 LUSTARTIC RENTALS PROPERTY U002303775

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NoImpressed Device: UnknownConstruction Material: Not reportedPiping Type: UnknownPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 12/13/1994Remove Date: 11/01/1947Install Date: GasolineProduct: 2000Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Bare SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 10/30/1990Remove Date:

ARTIC RENTALS PROPERTY (Continued) U002303775

01/01/1970Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: LETTS INDUSTRIES INCOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 496-1970Contact telephone: USContact country: DETROIT, MI 48216 2714 W JEFFERSON AVEContact address: JOSEPH FRYContact: MID985630706EPA ID: DETROIT, MI 48216 2714 W JEFFERSON AVEFacility address: LETTS DROP FORGEFacility name: 04/26/1999Date form received by agency:

RCRA NonGen / NLR:

WDSBEAUST

LUST2647 ft. INVENTORYSite 2 of 2 in cluster O0.501 mi. PART 201

Relative:Higher

Actual:588 ft.

1/2-1 FINDSDETROIT, MI 48216NE ICIS2714 W JEFFERSON AVE MID985630706O67 RCRA NonGen / NLRLETTS DROP FORGE 1000530553

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05-2000-0478Enforcement Action ID:

5EPA Region #: WAYNEFacility County: CERCLA 106 AO For Resp Action/Imm HazEnforcement Action Type: DETROIT, MI 48216-2034 2714 W JEFFERSON STFacility Address: LETTS DROP FORGEFacility Name: MichiganState: 2714 W JEFFERSON ST DETROIT MI 48216-2034Full Address: LETTS DROP FORGEAction Name: CERCLIS MIN000508055Program ID: 110003666667FRS ID: 05-2000-0478Enforcement Action ID:

ICIS:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: LETTS DROP FORGESite name: 12/30/1991Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 01/01/1970Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: LETTS INDUSTRIES INCOwner/operator name:

Not reportedOwner/Op end date:

LETTS DROP FORGE (Continued) 1000530553

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Conservation and Recovery Act (RCRA) program through the tracking ofRCRAInfo is a national information system that supports the Resource Environmental Interest/Information System

110003666667Registry ID:

FINDS:

Not reportedSIC Code: Not reportedNAIC Code: NoFed Facility: NTribal Indicator: 2714 W JEFFERSON STAddress: LETTS DROP FORGEFacility Name: RCRAINFO MID985630706Program ID:

Not reportedSIC Code: Not reportedNAIC Code: NoFed Facility: NTribal Indicator: 2714 W JEFFERSON STAddress: LETTS DROP FORGEFacility Name: FRS 110003666667Program ID:

Not reportedSIC Code: Not reportedNAIC Code: NoFed Facility: NTribal Indicator: 2714 W JEFFERSON STAddress: LETTS DROP FORGEFacility Name: CERCLIS MIN000508055Program ID:

5EPA Region #: WAYNEFacility County: CERCLA 106 AO For Resp Action/Imm HazEnforcement Action Type: DETROIT, MI 48216-2034 2714 W JEFFERSON STFacility Address: LETTS DROP FORGEFacility Name: MichiganState: 2714 W JEFFERSON ST DETROIT MI 48216-2034Full Address: LETTS DROP FORGEAction Name: FRS 110003666667Program ID: 110003666667FRS ID: 05-2000-0478Enforcement Action ID:

5EPA Region #: WAYNEFacility County: CERCLA 106 AO For Resp Action/Imm HazEnforcement Action Type: DETROIT, MI 48216-2034 2714 W JEFFERSON STFacility Address: LETTS DROP FORGEFacility Name: MichiganState: 2714 W JEFFERSON ST DETROIT MI 48216-2034Full Address: LETTS DROP FORGEAction Name: RCRAINFO MID985630706Program ID: 110003666667FRS ID:

LETTS DROP FORGE (Continued) 1000530553

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MAP FINDINGSMap IDDirection

EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

Not reportedOwner Contact: Detroit, MI 48207-3647Owner City,St,Zip: 1111 Bellevue StOwner Address: Letts Ind IncOwner Name: STATE OF MICHIGANSource: 00019364Facility ID:

LUST:

-83.07557Longitude:42.31774Latitude:Part 213Data Source:Southeast MIDistrict:Not reportedTownship:Not reportedBea Number:

INVENTORY:

Not reportedPollutants: Not reportedQuarter/Quarter: Not reportedQuarter: Not reportedSection: Not reportedRange: Not reportedTownship: 08/24/2004SAM Score Date: 32SAM Score: Automotive StampingSource: Inactive - no actions taken to address contaminationFacility Status: 82001713Facility ID:

PART 201:

Incident Tracking, Compliance Assistance, and Compliance Monitoring.that support Compliance and Enforcement programs. These include;has the capability to track other activities occurring in the Regionthat information with Federal actions already in the system. ICIS alsoCompliance System (PCS) which supports the NPDES and will integrateit Headquarters. A future release of ICIS will replace the Permitinformation is maintained in ICIS by EPA in the Regional offices andFederal Administrative and Judicial enforcement actions. Thisa single repository for that information. Currently, ICIS contains allreplace EPA’s independent databases that contain Enforcement data withinformation across most of EPA’s programs. The vision for ICIS is tocomplete, will contain integrated Enforcement and ComplianceCompliance Information System and provides a database that, whenICIS (Integrated Compliance Information System) is the Integrated

and financial information.including an inventory of sites, planned and actual site activities,system contains information on all aspects of hazardous waste sites,to support management in all phases of the Superfund program. TheLiability Information System) is the Superfund database that is usedCERCLIS (Comprehensive Environmental Response, Compensation, and

corrective action activities required under RCRA.program staff to track the notification, permit, compliance, andand treat, store, or dispose of hazardous waste. RCRAInfo allows RCRAevents and activities related to facilities that generate, transport,

LETTS DROP FORGE (Continued) 1000530553

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EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

Not reportedPiping Type: Bare SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 03/04/1990Remove Date: 02/19/1944Install Date: FUEL OILProduct: 15000Capacity: Removed from GroundTank Status: 1Tank ID:

-83.07557Longitude: 42.31773Latitude: Address Matching-House NumberMethod of Collection: Plant Entrance (Freight)Desc Category: POINTPoint Line Area: STATE OF MICHIGANSource: NAD83Horizontal Datum: FEETAccuracy Value Unit: 100Accuracy: 01/11/2001Date of Collection: ( ) -Contact Phone: Not reportedContact: (313) 579-1100Owner Phone: Not reportedOwner Contact: USAOwner Country: DETROIT, MI 48207-3647Owner City,St,Zip: 1111 BELLEVUE STOwner Address: LETTS IND INCOwner Name: CLOSEDFacility Type: 00019364Facility ID:

UST:

Not reportedRelease Closed Date: OpenRelease Status: Not reportedSubstance Released: 03/14/1990Release Date: C-0429-90Leak Number:

03/24/1994Release Closed Date: ClosedRelease Status: Not reportedSubstance Released: 03/05/1990Release Date: C-0377-90Leak Number:

Plant Entrance (Freight)Desc Category: POINTPoint Line Area: NAD83Horizontal Data: FEETAccuracy Value Unit: 100Accuracy: Address Matching-House NumberMethod of Collection: 01/11/2001Date of Collection: -83.07557Longitude: 42.31773Latitude: Letts IndustriesSite Name: Region 1 - SE Michigan District OfficeDistrict: USACountry: (313) 579-1100Owner Phone:

LETTS DROP FORGE (Continued) 1000530553

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EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

WAYNEMailing County: 48216Mailing City/State/Zip: 2714 W JEFFERSON AVEMailing Address: LETTS DROP FORGESite Specific Name: 406568WMD Id: MID985630706Site Id:

WDS:

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: Crown Enterprises, Inc.Submitter Name: 03/25/2002Date Received: Southeast MIDistrict: 1656BEA Number: Not reportedSecondary Address:

BEA:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material: Not reportedPiping Type: Bare SteelPiping Material: Not reportedPipe Realease Detection: Not reportedTank Release Detection: 03/04/1990Remove Date: 02/19/1948Install Date: GasolineProduct: 500Capacity: Removed from GroundTank Status: 2Tank ID:

NoImpressed Device: Asphalt Coated or Bare SteelConstruction Material:

LETTS DROP FORGE (Continued) 1000530553

General GovernmentSource: Interim Response in progressFacility Status: 82000224Facility ID:

PART 201:

-83.08015Longitude:42.3211Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

3250 ft.0.616 mi.

Relative:Higher

Actual:599 ft.

1/2-1 DETROIT, MI 48209North PART 201HOWARD AND 21ST STREET N/A68 INVENTORYAMBASSADOR BRIDGE CUSTOMS FAC S103085349

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EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

Benzene; Ethylbenzene; Pb; Toluene; Xylenes; PNAsPollutants: SWQuarter/Quarter: NWQuarter: 18Section: 12ERange: 02STownship: 08/19/1992SAM Score Date: 25SAM Score:

AMBASSADOR BRIDGE CUSTOMS FAC (Continued) S103085349

Not reportedPollutants: Not reportedQuarter/Quarter: Not reportedQuarter: Not reportedSection: Not reportedRange: Not reportedTownship: 03/07/2008SAM Score Date: 39SAM Score: RR Line-Haul OperatingSource: Evaluation conductedFacility Status: 82002601Facility ID:

PART 201:

-83.07196Longitude:42.31777Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

3310 ft.0.627 mi.

Relative:Higher

Actual:582 ft.

1/2-1 DETROIT, MI 48233NE PART 201JEFFERSON AND 12TH STREET N/A69 INVENTORYCSX/NORFOLK & WESTERN RAILROAD SITE S109149903

Benzene; Ethylbenzene; Toluene; XylenesPollutants: SEQuarter/Quarter: NWQuarter: 19Section: 12ERange: 02STownship: 09/07/2004SAM Score Date: 19SAM Score: Nonclassifiable EstablishmentsSource: Interim Response conducted - No further activities anticipatedFacility Status: 82000145Facility ID:

PART 201:

3736 ft.0.708 mi.

Relative:Higher

Actual:593 ft.

1/2-1 BROWNFIELDSDETROIT, MI 48216North INVENTORYNEAR VERNOR AND BAGLEY STREET OFF FISHER N/A70 PART 201WELCOME CENTER DEVELOPMENT S105144800

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EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

82000145Ernie Id Number: NoBEA: Not reportedUse at Time of Listing: Not reportedProperry Use: Not reportedStatus: 1Region: Not reportedFacility ID:

BROWNFIELD:

-83.0802Longitude:42.32174Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

WELCOME CENTER DEVELOPMENT (Continued) S105144800

RCRA NonGen / NLR:

NFRAP-Site does not qualify for the NPL based on existing informationPriority Level: 01/31/89Date Completed: / /Date Started: PRELIMINARY ASSESSMENTAction:

Not reportedPriority Level: 02/25/88Date Completed: / /Date Started: DISCOVERYAction:

StabilizedPriority Level: 04/17/88Date Completed: 03/15/88Date Started: REMOVALAction:

Not reportedPriority Level: 02/14/96Date Completed: / /Date Started: ARCHIVE SITEAction:

CERCLIS-NFRAP Assessment History:

Great LakesDescription:Program Priority:

NFRAP-Site does not qualify for the NPL based on existing informationNon NPL Status: Not on the NPLNPL Status: Not a Federal FacilityFederal Facility: 0505462Site ID:

CERC-NFRAP:

BEA4317 ft. BROWNFIELDS0.818 mi. INVENTORY

Relative:Higher

Actual:586 ft.

1/2-1 PART 201DETROIT, MI 48209SW RCRA NonGen / NLR5851 W JEFFERSON AVE MID00550999771 CERC-NFRAPMI DEPT/TRANSPORTATION 1000214658

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NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste:

Handler Activities Summary:

Not reportedOwner/Op end date: 04/28/2009Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 04/28/2009Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: NO ACTIVE O/OP AS NOT GENERATING WASTEOwner/operator name:

Not reportedOwner/Op end date: 01/01/1901Owner/Op start date: OwnerOwner/Operator Type: MunicipalLegal status: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: CITY OF DETROITOwner/operator name:

Owner/Operator Summary:

Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: 05EPA Region: Not reportedContact email: (313) 237-3900Contact telephone: USContact country: DETROIT, MI 48209 5851 W JEFFERSON AVEContact address: STEVE INNESContact: DETROIT, MI 48226 2000 BRUSH STMailing address: MID005509997EPA ID: DETROIT, MI 48209 5851 W JEFFERSON AVEFacility address: MI DEPT/TRANSPORTATIONFacility name: 04/27/2009Date form received by agency:

MI DEPT/TRANSPORTATION (Continued) 1000214658

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MI DEPT/TRANSPORTATIONSite name: 11/19/1980Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/TRANSPORTATIONSite name: 09/22/1995Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/TRANSPORTATIONSite name: 04/26/1999Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/TRANSPORTATIONSite name: 11/13/2000Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/TRANSPORTATIONSite name: 01/24/2007Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification: MI DEPT/TRANSPORTATIONSite name: 01/01/2008Date form received by agency:

IGNITABLE WASTE. Waste name: D001. Waste code:

Large Quantity GeneratorClassification: MI DEPT/TRANSPORTATIONSite name: 05/14/2008Date form received by agency:

Historical Generators:

IGNITABLE WASTE. Waste name: D001. Waste code:

NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption:

MI DEPT/TRANSPORTATION (Continued) 1000214658

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EDR ID NumberDistanceEPA ID NumberDatabase(s)SiteElevation

Environmental Response DivisionDivision Assigned: thorntopReviewer: No RequestDetermination 20107A: No Hazardous Substance(s)Category: 0Petition Disclosure: No RequestPetition Determination: B&C Land Development companySubmitter Name: 01/20/2006Date Received: Southeast MIDistrict: 3027BEA Number: Not reportedSecondary Address:

BEA:

82000136Ernie Id Number: NoBEA: Not reportedUse at Time of Listing: Not reportedProperry Use: Not reportedStatus: 1Region: Not reportedFacility ID:

BROWNFIELD:

-83.09242Longitude:42.30191Latitude:Part 201Data Source:Southeast MIDistrict:DetroitTownship:Not reportedBea Number:

INVENTORY:

Asbestos; PCB’s; Gasoline; PetroleumPollutants: SWQuarter/Quarter: SEQuarter: 23Section: 11ERange: 02STownship: 06/21/2004SAM Score Date: 39SAM Score: Primary Metal IndustriesSource: Interim Response conducted - No further activities anticipatedFacility Status: 82000136Facility ID:

PART 201:

No violations foundViolation Status:

IGNITABLE WASTE. Waste name: D001. Waste code:

Not a generator, verifiedClassification:

MI DEPT/TRANSPORTATION (Continued) 1000214658

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Delisted - no longer meets criteria specified in rulesStatus:82001763Facility ID:

DEL_PART201:

4749 ft.0.899 mi.

Relative:Higher

Actual:596 ft.

1/2-1 DETROIT, MI 48216North 2661 BAGLEY STREET N/A72 DEL PART 201HUBBARD-RICHARD HOUSING PROJECT S108633166

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Page 182: Baseline Environmental Assessment for Riverside Park

To maintain currency of the following federal and state databases, EDR contacts the appropriate governmental agencyon a monthly or quarterly basis, as required.

Number of Days to Update: Provides confirmation that EDR is reporting records that have been updated within 90 daysfrom the date the government agency made the information available to the public.

STANDARD ENVIRONMENTAL RECORDS

Federal NPL site list

NPL: National Priority ListNational Priorities List (Superfund). The NPL is a subset of CERCLIS and identifies over 1,200 sites for prioritycleanup under the Superfund Program. NPL sites may encompass relatively large areas. As such, EDR provides polygoncoverage for over 1,000 NPL site boundaries produced by EPA’s Environmental Photographic Interpretation Center(EPIC) and regional EPA offices.

Date of Government Version: 12/16/2014Date Data Arrived at EDR: 01/08/2015Date Made Active in Reports: 02/09/2015Number of Days to Update: 32

Source: EPATelephone: N/ALast EDR Contact: 04/08/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Quarterly

NPL Site Boundaries

Sources:

EPA’s Environmental Photographic Interpretation Center (EPIC)Telephone: 202-564-7333

EPA Region 1 EPA Region 6Telephone 617-918-1143 Telephone: 214-655-6659

EPA Region 3 EPA Region 7Telephone 215-814-5418 Telephone: 913-551-7247

EPA Region 4 EPA Region 8Telephone 404-562-8033 Telephone: 303-312-6774

EPA Region 5 EPA Region 9Telephone 312-886-6686 Telephone: 415-947-4246

EPA Region 10Telephone 206-553-8665

Proposed NPL: Proposed National Priority List SitesA site that has been proposed for listing on the National Priorities List through the issuance of a proposed rulein the Federal Register. EPA then accepts public comments on the site, responds to the comments, and places onthe NPL those sites that continue to meet the requirements for listing.

Date of Government Version: 12/16/2014Date Data Arrived at EDR: 01/08/2015Date Made Active in Reports: 02/09/2015Number of Days to Update: 32

Source: EPATelephone: N/ALast EDR Contact: 04/08/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Quarterly

NPL LIENS: Federal Superfund LiensFederal Superfund Liens. Under the authority granted the USEPA by CERCLA of 1980, the USEPA has the authorityto file liens against real property in order to recover remedial action expenditures or when the property ownerreceived notification of potential liability. USEPA compiles a listing of filed notices of Superfund Liens.

Date of Government Version: 10/15/1991Date Data Arrived at EDR: 02/02/1994Date Made Active in Reports: 03/30/1994Number of Days to Update: 56

Source: EPATelephone: 202-564-4267Last EDR Contact: 08/15/2011Next Scheduled EDR Contact: 11/28/2011Data Release Frequency: No Update Planned

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Federal Delisted NPL site list

DELISTED NPL: National Priority List DeletionsThe National Oil and Hazardous Substances Pollution Contingency Plan (NCP) establishes the criteria that theEPA uses to delete sites from the NPL. In accordance with 40 CFR 300.425.(e), sites may be deleted from theNPL where no further response is appropriate.

Date of Government Version: 12/16/2014Date Data Arrived at EDR: 01/08/2015Date Made Active in Reports: 02/09/2015Number of Days to Update: 32

Source: EPATelephone: N/ALast EDR Contact: 04/08/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Quarterly

Federal CERCLIS list

CERCLIS: Comprehensive Environmental Response, Compensation, and Liability Information SystemCERCLIS contains data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities,private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response, Compensation,and Liability Act (CERCLA). CERCLIS contains sites which are either proposed to or on the National PrioritiesList (NPL) and sites which are in the screening and assessment phase for possible inclusion on the NPL.

Date of Government Version: 10/25/2013Date Data Arrived at EDR: 11/11/2013Date Made Active in Reports: 02/13/2014Number of Days to Update: 94

Source: EPATelephone: 703-412-9810Last EDR Contact: 04/02/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Quarterly

FEDERAL FACILITY: Federal Facility Site Information listingA listing of National Priority List (NPL) and Base Realignment and Closure (BRAC) sites found in the ComprehensiveEnvironmental Response, Compensation and Liability Information System (CERCLIS) Database where EPA Federal FacilitiesRestoration and Reuse Office is involved in cleanup activities.

Date of Government Version: 07/21/2014Date Data Arrived at EDR: 10/07/2014Date Made Active in Reports: 10/20/2014Number of Days to Update: 13

Source: Environmental Protection AgencyTelephone: 703-603-8704Last EDR Contact: 04/08/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Varies

Federal CERCLIS NFRAP site List

CERCLIS-NFRAP: CERCLIS No Further Remedial Action PlannedArchived sites are sites that have been removed and archived from the inventory of CERCLIS sites. Archived statusindicates that, to the best of EPA’s knowledge, assessment at a site has been completed and that EPA has determinedno further steps will be taken to list this site on the National Priorities List (NPL), unless information indicatesthis decision was not appropriate or other considerations require a recommendation for listing at a later time.This decision does not necessarily mean that there is no hazard associated with a given site; it only means that,based upon available information, the location is not judged to be a potential NPL site.

Date of Government Version: 10/25/2013Date Data Arrived at EDR: 11/11/2013Date Made Active in Reports: 02/13/2014Number of Days to Update: 94

Source: EPATelephone: 703-412-9810Last EDR Contact: 04/02/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Quarterly

Federal RCRA CORRACTS facilities list

CORRACTS: Corrective Action ReportCORRACTS identifies hazardous waste handlers with RCRA corrective action activity.

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Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: EPATelephone: 800-424-9346Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Quarterly

Federal RCRA non-CORRACTS TSD facilities list

RCRA-TSDF: RCRA - Treatment, Storage and DisposalRCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservationand Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The databaseincludes selective information on sites which generate, transport, store, treat and/or dispose of hazardous wasteas defined by the Resource Conservation and Recovery Act (RCRA). Transporters are individuals or entities thatmove hazardous waste from the generator offsite to a facility that can recycle, treat, store, or dispose of thewaste. TSDFs treat, store, or dispose of the waste.

Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 312-886-6186Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Quarterly

Federal RCRA generators list

RCRA-LQG: RCRA - Large Quantity GeneratorsRCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservationand Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The databaseincludes selective information on sites which generate, transport, store, treat and/or dispose of hazardous wasteas defined by the Resource Conservation and Recovery Act (RCRA). Large quantity generators (LQGs) generateover 1,000 kilograms (kg) of hazardous waste, or over 1 kg of acutely hazardous waste per month.

Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 312-886-6186Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Quarterly

RCRA-SQG: RCRA - Small Quantity GeneratorsRCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservationand Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The databaseincludes selective information on sites which generate, transport, store, treat and/or dispose of hazardous wasteas defined by the Resource Conservation and Recovery Act (RCRA). Small quantity generators (SQGs) generatebetween 100 kg and 1,000 kg of hazardous waste per month.

Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 312-886-6186Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Quarterly

RCRA-CESQG: RCRA - Conditionally Exempt Small Quantity GeneratorsRCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservationand Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The databaseincludes selective information on sites which generate, transport, store, treat and/or dispose of hazardous wasteas defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators(CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month.

Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 312-886-6186Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

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Federal institutional controls / engineering controls registries

US ENG CONTROLS: Engineering Controls Sites ListA listing of sites with engineering controls in place. Engineering controls include various forms of caps, buildingfoundations, liners, and treatment methods to create pathway elimination for regulated substances to enter environmentalmedia or effect human health.

Date of Government Version: 09/18/2014Date Data Arrived at EDR: 09/19/2014Date Made Active in Reports: 10/20/2014Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 703-603-0695Last EDR Contact: 02/26/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Varies

US INST CONTROL: Sites with Institutional ControlsA listing of sites with institutional controls in place. Institutional controls include administrative measures,such as groundwater use restrictions, construction restrictions, property use restrictions, and post remediationcare requirements intended to prevent exposure to contaminants remaining on site. Deed restrictions are generallyrequired as part of the institutional controls.

Date of Government Version: 09/18/2014Date Data Arrived at EDR: 09/19/2014Date Made Active in Reports: 10/20/2014Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 703-603-0695Last EDR Contact: 02/26/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Varies

LUCIS: Land Use Control Information SystemLUCIS contains records of land use control information pertaining to the former Navy Base Realignment and Closureproperties.

Date of Government Version: 12/03/2014Date Data Arrived at EDR: 12/12/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 48

Source: Department of the NavyTelephone: 843-820-7326Last EDR Contact: 02/16/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: Varies

Federal ERNS list

ERNS: Emergency Response Notification SystemEmergency Response Notification System. ERNS records and stores information on reported releases of oil and hazardoussubstances.

Date of Government Version: 09/29/2014Date Data Arrived at EDR: 09/30/2014Date Made Active in Reports: 11/06/2014Number of Days to Update: 37

Source: National Response Center, United States Coast GuardTelephone: 202-267-2180Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Annually

State- and tribal - equivalent CERCLIS

SHWS: This state does not maintain a SHWS list. See the Federal CERCLIS list and Federal NPL list.This state does not maintain a SHWS list. See the Federal CERCLIS list and Federal NPL list.

Date of Government Version: N/ADate Data Arrived at EDR: 10/31/2013Date Made Active in Reports: 11/20/2013Number of Days to Update: 20

Source: Dept of Environmental QualityTelephone: 517-284-5103Last EDR Contact: 04/23/2015Next Scheduled EDR Contact: 08/10/2015Data Release Frequency: No Update Planned

State and tribal landfill and/or solid waste disposal site lists

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SWF/LF: Solid Waste Facilities DatabaseSolid Waste Facilities/Landfill Sites. SWF/LF type records typically contain an inventory of solid waste disposalfacilities or landfills in a particular state. Depending on the state, these may be active or inactive facilitiesor open dumps that failed to meet RCRA Subtitle D Section 4004 criteria for solid waste landfills or disposalsites.

Date of Government Version: 03/30/2015Date Data Arrived at EDR: 03/31/2015Date Made Active in Reports: 04/14/2015Number of Days to Update: 14

Source: Dept of Environmental QualityTelephone: 517-335-4035Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Semi-Annually

State and tribal leaking storage tank lists

LUST: Leaking Underground Storage Tank SitesLeaking Underground Storage Tank Incident Reports. LUST records contain an inventory of reported leaking undergroundstorage tank incidents. Not all states maintain these records, and the information stored varies by state.

Date of Government Version: 02/16/2015Date Data Arrived at EDR: 03/06/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 7

Source: Dept of Environmental QualityTelephone: 517-373-9837Last EDR Contact: 03/06/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: Annually

INDIAN LUST R9: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in Arizona, California, New Mexico and Nevada

Date of Government Version: 01/08/2015Date Data Arrived at EDR: 01/08/2015Date Made Active in Reports: 02/09/2015Number of Days to Update: 32

Source: Environmental Protection AgencyTelephone: 415-972-3372Last EDR Contact: 01/08/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

INDIAN LUST R7: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in Iowa, Kansas, and Nebraska

Date of Government Version: 09/23/2014Date Data Arrived at EDR: 11/25/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 65

Source: EPA Region 7Telephone: 913-551-7003Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN LUST R6: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in New Mexico and Oklahoma.

Date of Government Version: 01/23/2015Date Data Arrived at EDR: 02/10/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 31

Source: EPA Region 6Telephone: 214-665-6597Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN LUST R8: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in Colorado, Montana, North Dakota, South Dakota, Utah and Wyoming.

Date of Government Version: 01/28/2015Date Data Arrived at EDR: 01/30/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 42

Source: EPA Region 8Telephone: 303-312-6271Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

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INDIAN LUST R5: Leaking Underground Storage Tanks on Indian LandLeaking underground storage tanks located on Indian Land in Michigan, Minnesota and Wisconsin.

Date of Government Version: 01/30/2015Date Data Arrived at EDR: 02/05/2015Date Made Active in Reports: 03/09/2015Number of Days to Update: 32

Source: EPA, Region 5Telephone: 312-886-7439Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN LUST R1: Leaking Underground Storage Tanks on Indian LandA listing of leaking underground storage tank locations on Indian Land.

Date of Government Version: 02/01/2013Date Data Arrived at EDR: 05/01/2013Date Made Active in Reports: 11/01/2013Number of Days to Update: 184

Source: EPA Region 1Telephone: 617-918-1313Last EDR Contact: 01/30/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN LUST R4: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in Florida, Mississippi and North Carolina.

Date of Government Version: 09/30/2014Date Data Arrived at EDR: 03/03/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 10

Source: EPA Region 4Telephone: 404-562-8677Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Semi-Annually

INDIAN LUST R10: Leaking Underground Storage Tanks on Indian LandLUSTs on Indian land in Alaska, Idaho, Oregon and Washington.

Date of Government Version: 02/03/2015Date Data Arrived at EDR: 02/12/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 29

Source: EPA Region 10Telephone: 206-553-2857Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

State and tribal registered storage tank lists

UST: Underground Storage Tank Facility ListRegistered Underground Storage Tanks. UST’s are regulated under Subtitle I of the Resource Conservation and RecoveryAct (RCRA) and must be registered with the state department responsible for administering the UST program. Availableinformation varies by state program.

Date of Government Version: 03/01/2015Date Data Arrived at EDR: 03/12/2015Date Made Active in Reports: 03/19/2015Number of Days to Update: 7

Source: Dept of Environmental QualityTelephone: 517-335-4035Last EDR Contact: 03/12/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: Annually

UST 2: Underground Storage Tank ListingA listing of underground storage tank site locations that have unknown owner information.

Date of Government Version: 01/28/2015Date Data Arrived at EDR: 01/29/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 22

Source: Dept of Environmental QualityTelephone: 517-335-7211Last EDR Contact: 04/16/2015Next Scheduled EDR Contact: 08/03/2015Data Release Frequency: Annually

AST: Aboveground TanksRegistered Aboveground Storage Tanks.

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Date of Government Version: 03/02/2015Date Data Arrived at EDR: 03/03/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 10

Source: Dept of Environmental QualityTelephone: 517-373-8168Last EDR Contact: 02/27/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: No Update Planned

INDIAN UST R1: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 1 (Connecticut, Maine, Massachusetts, New Hampshire, Rhode Island, Vermont and ten TribalNations).

Date of Government Version: 02/01/2013Date Data Arrived at EDR: 05/01/2013Date Made Active in Reports: 01/27/2014Number of Days to Update: 271

Source: EPA, Region 1Telephone: 617-918-1313Last EDR Contact: 01/30/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN UST R4: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 4 (Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, Tennesseeand Tribal Nations)

Date of Government Version: 09/30/2014Date Data Arrived at EDR: 03/03/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 10

Source: EPA Region 4Telephone: 404-562-9424Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Semi-Annually

INDIAN UST R5: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 5 (Michigan, Minnesota and Wisconsin and Tribal Nations).

Date of Government Version: 01/30/2015Date Data Arrived at EDR: 02/05/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 36

Source: EPA Region 5Telephone: 312-886-6136Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN UST R6: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 6 (Louisiana, Arkansas, Oklahoma, New Mexico, Texas and 65 Tribes).

Date of Government Version: 01/23/2015Date Data Arrived at EDR: 02/13/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 28

Source: EPA Region 6Telephone: 214-665-7591Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Semi-Annually

INDIAN UST R7: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 7 (Iowa, Kansas, Missouri, Nebraska, and 9 Tribal Nations).

Date of Government Version: 09/23/2014Date Data Arrived at EDR: 11/25/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 65

Source: EPA Region 7Telephone: 913-551-7003Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

INDIAN UST R8: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 8 (Colorado, Montana, North Dakota, South Dakota, Utah, Wyoming and 27 Tribal Nations).

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Date of Government Version: 01/29/2015Date Data Arrived at EDR: 01/30/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 42

Source: EPA Region 8Telephone: 303-312-6137Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

INDIAN UST R10: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 10 (Alaska, Idaho, Oregon, Washington, and Tribal Nations).

Date of Government Version: 02/03/2015Date Data Arrived at EDR: 02/12/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 29

Source: EPA Region 10Telephone: 206-553-2857Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

INDIAN UST R9: Underground Storage Tanks on Indian LandThe Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indianland in EPA Region 9 (Arizona, California, Hawaii, Nevada, the Pacific Islands, and Tribal Nations).

Date of Government Version: 12/14/2014Date Data Arrived at EDR: 02/13/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 28

Source: EPA Region 9Telephone: 415-972-3368Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

FEMA UST: Underground Storage Tank ListingA listing of all FEMA owned underground storage tanks.

Date of Government Version: 01/01/2010Date Data Arrived at EDR: 02/16/2010Date Made Active in Reports: 04/12/2010Number of Days to Update: 55

Source: FEMATelephone: 202-646-5797Last EDR Contact: 04/13/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Varies

State and tribal institutional control / engineering control registries

AUL: Engineering and Institutional ControlsA listing of sites with institutional and/or engineering controls in place.

Date of Government Version: 03/09/2015Date Data Arrived at EDR: 03/10/2015Date Made Active in Reports: 03/19/2015Number of Days to Update: 9

Source: Dept of Environmental QualityTelephone: 517-373-4828Last EDR Contact: 03/03/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Varies

State and tribal voluntary cleanup sites

INDIAN VCP R1: Voluntary Cleanup Priority ListingA listing of voluntary cleanup priority sites located on Indian Land located in Region 1.

Date of Government Version: 09/29/2014Date Data Arrived at EDR: 10/01/2014Date Made Active in Reports: 11/06/2014Number of Days to Update: 36

Source: EPA, Region 1Telephone: 617-918-1102Last EDR Contact: 04/02/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

INDIAN VCP R7: Voluntary Cleanup Priority LisitngA listing of voluntary cleanup priority sites located on Indian Land located in Region 7.

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Date of Government Version: 03/20/2008Date Data Arrived at EDR: 04/22/2008Date Made Active in Reports: 05/19/2008Number of Days to Update: 27

Source: EPA, Region 7Telephone: 913-551-7365Last EDR Contact: 04/20/2009Next Scheduled EDR Contact: 07/20/2009Data Release Frequency: Varies

State and tribal Brownfields sites

BROWNFIELDS: Brownfields and USTfield Site DatabaseAll state funded Part 201 and 213 sites, as well as LUST sites that have been redeveloped by private entitiesusing the BEA process. Be aware that this is not a list of all of the potential brownfield sites in Michigan.

Date of Government Version: 07/27/2012Date Data Arrived at EDR: 07/31/2012Date Made Active in Reports: 09/20/2012Number of Days to Update: 51

Source: Dept of Environmental QualityTelephone: 517-373-4805Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 01/22/2015Data Release Frequency: Varies

BROWNFIELDS 2: Brownfields Building and Land Site LocationsA listing of brownfield building and land site locations. The listing is a collaborative effort of Michigan EconomicDevelopment Corporation, Michigan Economic Developers Association, Detrot Edison, Detroit Area Commercial Boardof Realtors

Date of Government Version: 04/09/2007Date Data Arrived at EDR: 04/10/2007Date Made Active in Reports: 05/01/2007Number of Days to Update: 21

Source: Economic Development CorporationTelephone: 888-522-0103Last EDR Contact: 02/26/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Varies

ADDITIONAL ENVIRONMENTAL RECORDS

Local Brownfield lists

US BROWNFIELDS: A Listing of Brownfields SitesBrownfields are real property, the expansion, redevelopment, or reuse of which may be complicated by the presenceor potential presence of a hazardous substance, pollutant, or contaminant. Cleaning up and reinvesting in theseproperties takes development pressures off of undeveloped, open land, and both improves and protects the environment.Assessment, Cleanup and Redevelopment Exchange System (ACRES) stores information reported by EPA Brownfieldsgrant recipients on brownfields properties assessed or cleaned up with grant funding as well as information onTargeted Brownfields Assessments performed by EPA Regions. A listing of ACRES Brownfield sites is obtained fromCleanups in My Community. Cleanups in My Community provides information on Brownfields properties for which informationis reported back to EPA, as well as areas served by Brownfields grant programs.

Date of Government Version: 12/22/2014Date Data Arrived at EDR: 12/22/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 38

Source: Environmental Protection AgencyTelephone: 202-566-2777Last EDR Contact: 03/24/2015Next Scheduled EDR Contact: 07/06/2015Data Release Frequency: Semi-Annually

Local Lists of Landfill / Solid Waste Disposal Sites

DEBRIS REGION 9: Torres Martinez Reservation Illegal Dump Site LocationsA listing of illegal dump sites location on the Torres Martinez Indian Reservation located in eastern RiversideCounty and northern Imperial County, California.

Date of Government Version: 01/12/2009Date Data Arrived at EDR: 05/07/2009Date Made Active in Reports: 09/21/2009Number of Days to Update: 137

Source: EPA, Region 9Telephone: 415-947-4219Last EDR Contact: 04/23/2015Next Scheduled EDR Contact: 08/10/2015Data Release Frequency: No Update Planned

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ODI: Open Dump InventoryAn open dump is defined as a disposal facility that does not comply with one or more of the Part 257 or Part 258Subtitle D Criteria.

Date of Government Version: 06/30/1985Date Data Arrived at EDR: 08/09/2004Date Made Active in Reports: 09/17/2004Number of Days to Update: 39

Source: Environmental Protection AgencyTelephone: 800-424-9346Last EDR Contact: 06/09/2004Next Scheduled EDR Contact: N/AData Release Frequency: No Update Planned

HIST LF: Inactive Solid Waste FacilitiesThe database contains historical information and is no longer updated.

Date of Government Version: 03/01/1997Date Data Arrived at EDR: 02/28/2003Date Made Active in Reports: 03/06/2003Number of Days to Update: 6

Source: Dept of Environmental QualityTelephone: 517-335-4034Last EDR Contact: 02/28/2003Next Scheduled EDR Contact: N/AData Release Frequency: No Update Planned

SWRCY: Recycling FacilitiesA listing of recycling center locations.

Date of Government Version: 04/11/2015Date Data Arrived at EDR: 04/14/2015Date Made Active in Reports: 04/21/2015Number of Days to Update: 7

Source: Dept of Environmental QualityTelephone: 517-241-5719Last EDR Contact: 03/30/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

INDIAN ODI: Report on the Status of Open Dumps on Indian LandsLocation of open dumps on Indian land.

Date of Government Version: 12/31/1998Date Data Arrived at EDR: 12/03/2007Date Made Active in Reports: 01/24/2008Number of Days to Update: 52

Source: Environmental Protection AgencyTelephone: 703-308-8245Last EDR Contact: 02/02/2015Next Scheduled EDR Contact: 05/18/2015Data Release Frequency: Varies

Local Lists of Hazardous waste / Contaminated Sites

US CDL: Clandestine Drug LabsA listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides thisweb site as a public service. It contains addresses of some locations where law enforcement agencies reportedthey found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites.In most cases, the source of the entries is not the Department, and the Department has not verified the entryand does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example,contacting local law enforcement and local health departments.

Date of Government Version: 02/25/2015Date Data Arrived at EDR: 03/10/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 15

Source: Drug Enforcement AdministrationTelephone: 202-307-1000Last EDR Contact: 03/03/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Quarterly

PART 201: Part 201 Site ListA Part 201 Listed site is a location that has been evaluated and scored by the DEQ using the Part 201 scoringmodel. The location is or includes a "facility" as defined by Part 201, where there has been a release of a hazardoussubstance(s) in excess of the Part 201 residential criteria, and/or where corrective actions have not been completedunder Part 201 to meet the applicable cleanup criteria for unrestricted residential use. The Part 201 List doesnot include all of the sites of contamination that are subject to regulation under Part 201 because owners arenot required to inform the DEQ about the sites and can pursue cleanup independently. Sites of environmental contaminationthat are not known to DEQ are not on the list, nor are sites with releases that resulted in low environmentalimpact.

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Date of Government Version: 10/01/2013Date Data Arrived at EDR: 10/03/2014Date Made Active in Reports: 10/03/2014Number of Days to Update: 0

Source: Department of Environmental QualityTelephone: 517-284-5103Last EDR Contact: 04/23/2015Next Scheduled EDR Contact: 08/10/2015Data Release Frequency: No Update Planned

INVENTORY: Inventory of FacilitiesThe Inventory of Facilities has three data sources: Facilities under Part 201, Environmental Remediation, of theNatural Resources and Environmental Protection Act, 1994 PA 451, as amended (NREPA) identified through statefunded or private party response activities (Projects); Facilities under Part 213, Leaking Underground StorageTanks of the NREPA; and Facilities identified through submittals of Baseline Environmental Assessments (BEA)submitted pursuant to Part 201 or Part 213 of the NREPA. The Part 201 Projects Inventory does not include allof the facilities that are subject to regulation under Part 201 because owners are not required to inform theDepartment of Environmental Quality (DEQ) about the facilities and can pursue cleanup independently. Facilitiesthat are not known to DEQ are not on the Inventory, nor are locations with releases that resulted in low environmentalimpact. Part 213 facilities listed here may have more than one release; a list of releases for which correctiveactions have been completed and list of releases for which corrective action has not been completed is locatedon the Leaking Underground Storage Tanks Site Search webpage. The DEQ may or may not have reviewed and concurredwith the conclusion that the corrective actions described in a closure report meets criteria. A BEA is a documentthat new or prospective property owners/operations disclose to the DEQ identifying the property as a facilitypursuant to Part 201 and Part 213. The Inventory of BEA Facilities overlaps in part with the Part 201 Projectsfacilities and Part 213 facilities. There may be more than one BEA for each facility.

Date of Government Version: 01/27/2015Date Data Arrived at EDR: 01/28/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 23

Source: Department of Environmental QualityTelephone: 517-284-5136Last EDR Contact: 01/28/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Quarterly

DEL PART 201: Delisted List of Contaminated SitesA deleted site has been removed from the Part 201 List because information known to the DEQ at the time of theevaluation does not support inclusion on the Part 201 List. This designation is often applied to sites where changesin cleanup criteria resulted in a determination that the site no longer exceeds any applicable cleanup criterion.A delisted site has been removed from the Part 201 List because response actions have reduced the levels of contaminantsto concentrations which meet or are below the criteria for unrestricted residential use.

Date of Government Version: 08/01/2013Date Data Arrived at EDR: 08/01/2013Date Made Active in Reports: 09/11/2013Number of Days to Update: 41

Source: Dept of Environmental QualityTelephone: 517-373-9541Last EDR Contact: 04/23/2015Next Scheduled EDR Contact: 08/10/2015Data Release Frequency: Varies

CDL: Clandestine Drug Lab ListingA listing of clandestine drug lab locations.

Date of Government Version: 10/20/2008Date Data Arrived at EDR: 11/18/2008Date Made Active in Reports: 11/21/2008Number of Days to Update: 3

Source: Department of Community HealthTelephone: 517-373-3740Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

US HIST CDL: National Clandestine Laboratory RegisterA listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides thisweb site as a public service. It contains addresses of some locations where law enforcement agencies reportedthey found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites.In most cases, the source of the entries is not the Department, and the Department has not verified the entryand does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example,contacting local law enforcement and local health departments.

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Date of Government Version: 02/25/2015Date Data Arrived at EDR: 03/10/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 15

Source: Drug Enforcement AdministrationTelephone: 202-307-1000Last EDR Contact: 03/03/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: No Update Planned

Local Land Records

LIENS 2: CERCLA Lien InformationA Federal CERCLA (’Superfund’) lien can exist by operation of law at any site or property at which EPA has spentSuperfund monies. These monies are spent to investigate and address releases and threatened releases of contamination.CERCLIS provides information as to the identity of these sites and properties.

Date of Government Version: 02/18/2014Date Data Arrived at EDR: 03/18/2014Date Made Active in Reports: 04/24/2014Number of Days to Update: 37

Source: Environmental Protection AgencyTelephone: 202-564-6023Last EDR Contact: 01/30/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

LIENS: Lien ListAn Environmental Lien is a charge, security, or encumbrance upon title to a property to secure the payment ofa cost, damage, debt, obligation, or duty arising out of response actions, cleanup, or other remediation of hazardoussubstances or petroleum products upon a property, including (but not limited to) liens imposed pursuant to CERCLA42 USC * 9607(1) and similar state or local laws. In other words: a lien placed upon a property’s title dueto an environmental condition

Date of Government Version: 12/12/2014Date Data Arrived at EDR: 01/21/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 30

Source: Dept of Environmental QualityTelephone: 517-241-7603Last EDR Contact: 04/16/2015Next Scheduled EDR Contact: 08/03/2015Data Release Frequency: Varies

Records of Emergency Release Reports

HMIRS: Hazardous Materials Information Reporting SystemHazardous Materials Incident Report System. HMIRS contains hazardous material spill incidents reported to DOT.

Date of Government Version: 12/29/2014Date Data Arrived at EDR: 12/30/2014Date Made Active in Reports: 03/09/2015Number of Days to Update: 69

Source: U.S. Department of TransportationTelephone: 202-366-4555Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Annually

PEAS: Pollution Emergency Alerting SystemEnvironmental pollution emergencies reported to the Department of Environmental Quality such as tanker accidents,pipeline breaks, and release of reportable quantities of hazardous substances.

Date of Government Version: 03/13/2015Date Data Arrived at EDR: 03/17/2015Date Made Active in Reports: 04/01/2015Number of Days to Update: 15

Source: Dept of Environmental QualityTelephone: 517-373-8427Last EDR Contact: 03/09/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Quarterly

Other Ascertainable Records

RCRA NonGen / NLR: RCRA - Non Generators / No Longer RegulatedRCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservationand Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The databaseincludes selective information on sites which generate, transport, store, treat and/or dispose of hazardous wasteas defined by the Resource Conservation and Recovery Act (RCRA). Non-Generators do not presently generate hazardouswaste.

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Date of Government Version: 12/09/2014Date Data Arrived at EDR: 12/29/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 312-886-6186Last EDR Contact: 03/31/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

DOT OPS: Incident and Accident DataDepartment of Transporation, Office of Pipeline Safety Incident and Accident data.

Date of Government Version: 07/31/2012Date Data Arrived at EDR: 08/07/2012Date Made Active in Reports: 09/18/2012Number of Days to Update: 42

Source: Department of Transporation, Office of Pipeline SafetyTelephone: 202-366-4595Last EDR Contact: 02/03/2015Next Scheduled EDR Contact: 05/18/2015Data Release Frequency: Varies

DOD: Department of Defense SitesThis data set consists of federally owned or administered lands, administered by the Department of Defense, thathave any area equal to or greater than 640 acres of the United States, Puerto Rico, and the U.S. Virgin Islands.

Date of Government Version: 12/31/2005Date Data Arrived at EDR: 11/10/2006Date Made Active in Reports: 01/11/2007Number of Days to Update: 62

Source: USGSTelephone: 888-275-8747Last EDR Contact: 04/14/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Semi-Annually

FUDS: Formerly Used Defense SitesThe listing includes locations of Formerly Used Defense Sites properties where the US Army Corps of Engineersis actively working or will take necessary cleanup actions.

Date of Government Version: 06/06/2014Date Data Arrived at EDR: 09/10/2014Date Made Active in Reports: 09/18/2014Number of Days to Update: 8

Source: U.S. Army Corps of EngineersTelephone: 202-528-4285Last EDR Contact: 03/13/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Varies

CONSENT: Superfund (CERCLA) Consent DecreesMajor legal settlements that establish responsibility and standards for cleanup at NPL (Superfund) sites. Releasedperiodically by United States District Courts after settlement by parties to litigation matters.

Date of Government Version: 01/23/2015Date Data Arrived at EDR: 02/13/2015Date Made Active in Reports: 03/09/2015Number of Days to Update: 24

Source: Department of Justice, Consent Decree LibraryTelephone: VariesLast EDR Contact: 03/30/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

ROD: Records Of DecisionRecord of Decision. ROD documents mandate a permanent remedy at an NPL (Superfund) site containing technicaland health information to aid in the cleanup.

Date of Government Version: 11/25/2013Date Data Arrived at EDR: 12/12/2013Date Made Active in Reports: 02/24/2014Number of Days to Update: 74

Source: EPATelephone: 703-416-0223Last EDR Contact: 03/10/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Annually

UMTRA: Uranium Mill Tailings SitesUranium ore was mined by private companies for federal government use in national defense programs. When the millsshut down, large piles of the sand-like material (mill tailings) remain after uranium has been extracted fromthe ore. Levels of human exposure to radioactive materials from the piles are low; however, in some cases tailingswere used as construction materials before the potential health hazards of the tailings were recognized.

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Date of Government Version: 09/14/2010Date Data Arrived at EDR: 10/07/2011Date Made Active in Reports: 03/01/2012Number of Days to Update: 146

Source: Department of EnergyTelephone: 505-845-0011Last EDR Contact: 02/27/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Varies

US MINES: Mines Master Index FileContains all mine identification numbers issued for mines active or opened since 1971. The data also includesviolation information.

Date of Government Version: 12/30/2014Date Data Arrived at EDR: 12/31/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 29

Source: Department of Labor, Mine Safety and Health AdministrationTelephone: 303-231-5959Last EDR Contact: 03/06/2015Next Scheduled EDR Contact: 06/15/2015Data Release Frequency: Semi-Annually

TRIS: Toxic Chemical Release Inventory SystemToxic Release Inventory System. TRIS identifies facilities which release toxic chemicals to the air, water andland in reportable quantities under SARA Title III Section 313.

Date of Government Version: 12/31/2011Date Data Arrived at EDR: 07/31/2013Date Made Active in Reports: 09/13/2013Number of Days to Update: 44

Source: EPATelephone: 202-566-0250Last EDR Contact: 01/29/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Annually

TSCA: Toxic Substances Control ActToxic Substances Control Act. TSCA identifies manufacturers and importers of chemical substances included on theTSCA Chemical Substance Inventory list. It includes data on the production volume of these substances by plantsite.

Date of Government Version: 12/31/2012Date Data Arrived at EDR: 01/15/2015Date Made Active in Reports: 01/29/2015Number of Days to Update: 14

Source: EPATelephone: 202-260-5521Last EDR Contact: 03/27/2015Next Scheduled EDR Contact: 07/06/2015Data Release Frequency: Every 4 Years

FTTS: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act)FTTS tracks administrative cases and pesticide enforcement actions and compliance activities related to FIFRA,TSCA and EPCRA (Emergency Planning and Community Right-to-Know Act). To maintain currency, EDR contacts theAgency on a quarterly basis.

Date of Government Version: 04/09/2009Date Data Arrived at EDR: 04/16/2009Date Made Active in Reports: 05/11/2009Number of Days to Update: 25

Source: EPA/Office of Prevention, Pesticides and Toxic SubstancesTelephone: 202-566-1667Last EDR Contact: 02/23/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Quarterly

FTTS INSP: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act)A listing of FIFRA/TSCA Tracking System (FTTS) inspections and enforcements.

Date of Government Version: 04/09/2009Date Data Arrived at EDR: 04/16/2009Date Made Active in Reports: 05/11/2009Number of Days to Update: 25

Source: EPATelephone: 202-566-1667Last EDR Contact: 02/23/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Quarterly

HIST FTTS: FIFRA/TSCA Tracking System Administrative Case ListingA complete administrative case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. Theinformation was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA(Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regionsare now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarterswith updated records, it was decided to create a HIST FTTS database. It included records that may not be includedin the newer FTTS database updates. This database is no longer updated.

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Date of Government Version: 10/19/2006Date Data Arrived at EDR: 03/01/2007Date Made Active in Reports: 04/10/2007Number of Days to Update: 40

Source: Environmental Protection AgencyTelephone: 202-564-2501Last EDR Contact: 12/17/2007Next Scheduled EDR Contact: 03/17/2008Data Release Frequency: No Update Planned

HIST FTTS INSP: FIFRA/TSCA Tracking System Inspection & Enforcement Case ListingA complete inspection and enforcement case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPAregions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementationof FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). SomeEPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providingEPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records thatmay not be included in the newer FTTS database updates. This database is no longer updated.

Date of Government Version: 10/19/2006Date Data Arrived at EDR: 03/01/2007Date Made Active in Reports: 04/10/2007Number of Days to Update: 40

Source: Environmental Protection AgencyTelephone: 202-564-2501Last EDR Contact: 12/17/2008Next Scheduled EDR Contact: 03/17/2008Data Release Frequency: No Update Planned

SSTS: Section 7 Tracking SystemsSection 7 of the Federal Insecticide, Fungicide and Rodenticide Act, as amended (92 Stat. 829) requires allregistered pesticide-producing establishments to submit a report to the Environmental Protection Agency by March1st each year. Each establishment must report the types and amounts of pesticides, active ingredients and devicesbeing produced, and those having been produced and sold or distributed in the past year.

Date of Government Version: 12/31/2009Date Data Arrived at EDR: 12/10/2010Date Made Active in Reports: 02/25/2011Number of Days to Update: 77

Source: EPATelephone: 202-564-4203Last EDR Contact: 04/10/2015Next Scheduled EDR Contact: 08/10/2015Data Release Frequency: Annually

ICIS: Integrated Compliance Information SystemThe Integrated Compliance Information System (ICIS) supports the information needs of the national enforcementand compliance program as well as the unique needs of the National Pollutant Discharge Elimination System (NPDES)program.

Date of Government Version: 01/23/2015Date Data Arrived at EDR: 02/06/2015Date Made Active in Reports: 03/09/2015Number of Days to Update: 31

Source: Environmental Protection AgencyTelephone: 202-564-5088Last EDR Contact: 04/09/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Quarterly

PADS: PCB Activity Database SystemPCB Activity Database. PADS Identifies generators, transporters, commercial storers and/or brokers and disposersof PCB’s who are required to notify the EPA of such activities.

Date of Government Version: 07/01/2014Date Data Arrived at EDR: 10/15/2014Date Made Active in Reports: 11/17/2014Number of Days to Update: 33

Source: EPATelephone: 202-566-0500Last EDR Contact: 04/17/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Annually

MLTS: Material Licensing Tracking SystemMLTS is maintained by the Nuclear Regulatory Commission and contains a list of approximately 8,100 sites whichpossess or use radioactive materials and which are subject to NRC licensing requirements. To maintain currency,EDR contacts the Agency on a quarterly basis.

Date of Government Version: 12/29/2014Date Data Arrived at EDR: 01/08/2015Date Made Active in Reports: 01/29/2015Number of Days to Update: 21

Source: Nuclear Regulatory CommissionTelephone: 301-415-7169Last EDR Contact: 03/09/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Quarterly

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RADINFO: Radiation Information DatabaseThe Radiation Information Database (RADINFO) contains information about facilities that are regulated by U.S.Environmental Protection Agency (EPA) regulations for radiation and radioactivity.

Date of Government Version: 02/27/2015Date Data Arrived at EDR: 02/27/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 26

Source: Environmental Protection AgencyTelephone: 202-343-9775Last EDR Contact: 04/09/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Quarterly

FINDS: Facility Index System/Facility Registry SystemFacility Index System. FINDS contains both facility information and ’pointers’ to other sources that contain moredetail. EDR includes the following FINDS databases in this report: PCS (Permit Compliance System), AIRS (AerometricInformation Retrieval System), DOCKET (Enforcement Docket used to manage and track information on civil judicialenforcement cases for all environmental statutes), FURS (Federal Underground Injection Control), C-DOCKET (CriminalDocket System used to track criminal enforcement actions for all environmental statutes), FFIS (Federal FacilitiesInformation System), STATE (State Environmental Laws and Statutes), and PADS (PCB Activity Data System).

Date of Government Version: 01/18/2015Date Data Arrived at EDR: 02/27/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 26

Source: EPATelephone: (312) 353-2000Last EDR Contact: 03/09/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Quarterly

RAATS: RCRA Administrative Action Tracking SystemRCRA Administration Action Tracking System. RAATS contains records based on enforcement actions issued under RCRApertaining to major violators and includes administrative and civil actions brought by the EPA. For administrationactions after September 30, 1995, data entry in the RAATS database was discontinued. EPA will retain a copy ofthe database for historical records. It was necessary to terminate RAATS because a decrease in agency resourcesmade it impossible to continue to update the information contained in the database.

Date of Government Version: 04/17/1995Date Data Arrived at EDR: 07/03/1995Date Made Active in Reports: 08/07/1995Number of Days to Update: 35

Source: EPATelephone: 202-564-4104Last EDR Contact: 06/02/2008Next Scheduled EDR Contact: 09/01/2008Data Release Frequency: No Update Planned

RMP: Risk Management PlansWhen Congress passed the Clean Air Act Amendments of 1990, it required EPA to publish regulations and guidancefor chemical accident prevention at facilities using extremely hazardous substances. The Risk Management ProgramRule (RMP Rule) was written to implement Section 112(r) of these amendments. The rule, which built upon existingindustry codes and standards, requires companies of all sizes that use certain flammable and toxic substancesto develop a Risk Management Program, which includes a(n): Hazard assessment that details the potential effectsof an accidental release, an accident history of the last five years, and an evaluation of worst-case and alternativeaccidental releases; Prevention program that includes safety precautions and maintenance, monitoring, and employeetraining measures; and Emergency response program that spells out emergency health care, employee training measuresand procedures for informing the public and response agencies (e.g the fire department) should an accident occur.

Date of Government Version: 02/01/2015Date Data Arrived at EDR: 02/13/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 40

Source: Environmental Protection AgencyTelephone: 202-564-8600Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

BRS: Biennial Reporting SystemThe Biennial Reporting System is a national system administered by the EPA that collects data on the generationand management of hazardous waste. BRS captures detailed data from two groups: Large Quantity Generators (LQG)and Treatment, Storage, and Disposal Facilities.

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Date of Government Version: 12/31/2011Date Data Arrived at EDR: 02/26/2013Date Made Active in Reports: 04/19/2013Number of Days to Update: 52

Source: EPA/NTISTelephone: 800-424-9346Last EDR Contact: 02/24/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Biennially

UIC: Underground Injection Wells DatabaseA listing of underground injection well locations. The UIC Program is responsible for regulating the construction,operation, permitting, and closure of injection wells that place fluids underground for storage or disposal.

Date of Government Version: 01/30/2015Date Data Arrived at EDR: 01/30/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 21

Source: Dept of Environmental QualityTelephone: 517-241-1515Last EDR Contact: 01/26/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

DRYCLEANERS: Drycleaning EstablishmentsA listing of drycleaning facilities in Michigan.

Date of Government Version: 01/21/2015Date Data Arrived at EDR: 01/22/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 29

Source: Dept of Environmental QualityTelephone: 517-335-4586Last EDR Contact: 04/16/2015Next Scheduled EDR Contact: 08/03/2015Data Release Frequency: Annually

NPDES: List of Active NPDES PermitsGeneral information regarding NPDES (National Pollutant Discharge Elimination System) permits and NPDES StormWater permits.

Date of Government Version: 04/07/2015Date Data Arrived at EDR: 04/09/2015Date Made Active in Reports: 04/21/2015Number of Days to Update: 12

Source: Dept of Environmental QualityTelephone: 517-241-1300Last EDR Contact: 04/09/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Varies

AIRS: Permit and Emissions Inventory DataPermit and emissions inventory data.

Date of Government Version: 03/24/2015Date Data Arrived at EDR: 03/25/2015Date Made Active in Reports: 03/31/2015Number of Days to Update: 6

Source: Dept of Environmental QualityTelephone: 517-373-7074Last EDR Contact: 03/17/2015Next Scheduled EDR Contact: 07/06/2015Data Release Frequency: Varies

BEA: Baseline Environmental Assessment DatabaseA BEA is a document that new or prospective property owners/operations disclose to the DEQ identifying the propertyas a facility pursuant to Part 201 and Part 213. The Inventory of BEA Facilities overlaps in part with the Part201 Projects facilities and Part 213 facilities. There may be more than one BEA for each facility.

Date of Government Version: 08/21/2013Date Data Arrived at EDR: 08/23/2013Date Made Active in Reports: 09/12/2013Number of Days to Update: 20

Source: Dept of Environmental QualityTelephone: 517-373-9541Last EDR Contact: 02/16/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: No Update Planned

INDIAN RESERV: Indian ReservationsThis map layer portrays Indian administered lands of the United States that have any area equal to or greaterthan 640 acres.

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Date of Government Version: 12/31/2005Date Data Arrived at EDR: 12/08/2006Date Made Active in Reports: 01/11/2007Number of Days to Update: 34

Source: USGSTelephone: 202-208-3710Last EDR Contact: 04/14/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Semi-Annually

SCRD DRYCLEANERS: State Coalition for Remediation of Drycleaners ListingThe State Coalition for Remediation of Drycleaners was established in 1998, with support from the U.S. EPA Officeof Superfund Remediation and Technology Innovation. It is comprised of representatives of states with establisheddrycleaner remediation programs. Currently the member states are Alabama, Connecticut, Florida, Illinois, Kansas,Minnesota, Missouri, North Carolina, Oregon, South Carolina, Tennessee, Texas, and Wisconsin.

Date of Government Version: 03/07/2011Date Data Arrived at EDR: 03/09/2011Date Made Active in Reports: 05/02/2011Number of Days to Update: 54

Source: Environmental Protection AgencyTelephone: 615-532-8599Last EDR Contact: 02/18/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: Varies

2020 COR ACTION: 2020 Corrective Action Program ListThe EPA has set ambitious goals for the RCRA Corrective Action program by creating the 2020 Corrective ActionUniverse. This RCRA cleanup baseline includes facilities expected to need corrective action. The 2020 universecontains a wide variety of sites. Some properties are heavily contaminated while others were contaminated buthave since been cleaned up. Still others have not been fully investigated yet, and may require little or no remediation.Inclusion in the 2020 Universe does not necessarily imply failure on the part of a facility to meet its RCRA obligations.

Date of Government Version: 04/22/2013Date Data Arrived at EDR: 03/03/2015Date Made Active in Reports: 03/09/2015Number of Days to Update: 6

Source: Environmental Protection AgencyTelephone: 703-308-4044Last EDR Contact: 02/13/2015Next Scheduled EDR Contact: 05/25/2015Data Release Frequency: Varies

LEAD SMELTER 1: Lead Smelter SitesA listing of former lead smelter site locations.

Date of Government Version: 11/25/2014Date Data Arrived at EDR: 11/26/2014Date Made Active in Reports: 01/29/2015Number of Days to Update: 64

Source: Environmental Protection AgencyTelephone: 703-603-8787Last EDR Contact: 04/10/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Varies

LEAD SMELTER 2: Lead Smelter SitesA list of several hundred sites in the U.S. where secondary lead smelting was done from 1931and 1964. These sitesmay pose a threat to public health through ingestion or inhalation of contaminated soil or dust

Date of Government Version: 04/05/2001Date Data Arrived at EDR: 10/27/2010Date Made Active in Reports: 12/02/2010Number of Days to Update: 36

Source: American Journal of Public HealthTelephone: 703-305-6451Last EDR Contact: 12/02/2009Next Scheduled EDR Contact: N/AData Release Frequency: No Update Planned

PRP: Potentially Responsible PartiesA listing of verified Potentially Responsible Parties

Date of Government Version: 10/25/2013Date Data Arrived at EDR: 10/17/2014Date Made Active in Reports: 10/20/2014Number of Days to Update: 3

Source: EPATelephone: 202-564-6023Last EDR Contact: 02/13/2015Next Scheduled EDR Contact: 05/25/2015Data Release Frequency: Quarterly

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FEDLAND: Federal and Indian LandsFederally and Indian administrated lands of the United States. Lands included are administrated by: Army Corpsof Engineers, Bureau of Reclamation, National Wild and Scenic River, National Wildlife Refuge, Public Domain Land,Wilderness, Wilderness Study Area, Wildlife Management Area, Bureau of Indian Affairs, Bureau of Land Management,Department of Justice, Forest Service, Fish and Wildlife Service, National Park Service.

Date of Government Version: 12/31/2005Date Data Arrived at EDR: 02/06/2006Date Made Active in Reports: 01/11/2007Number of Days to Update: 339

Source: U.S. Geological SurveyTelephone: 888-275-8747Last EDR Contact: 04/14/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: N/A

COAL ASH DOE: Steam-Electric Plant Operation DataA listing of power plants that store ash in surface ponds.

Date of Government Version: 12/31/2005Date Data Arrived at EDR: 08/07/2009Date Made Active in Reports: 10/22/2009Number of Days to Update: 76

Source: Department of EnergyTelephone: 202-586-8719Last EDR Contact: 04/15/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Varies

US AIRS (AFS): Aerometric Information Retrieval System Facility Subsystem (AFS)The database is a sub-system of Aerometric Information Retrieval System (AIRS). AFS contains compliance dataon air pollution point sources regulated by the U.S. EPA and/or state and local air regulatory agencies. Thisinformation comes from source reports by various stationary sources of air pollution, such as electric power plants,steel mills, factories, and universities, and provides information about the air pollutants they produce. Action,air program, air program pollutant, and general level plant data. It is used to track emissions and compliancedata from industrial plants.

Date of Government Version: 10/16/2014Date Data Arrived at EDR: 10/31/2014Date Made Active in Reports: 11/17/2014Number of Days to Update: 17

Source: EPATelephone: 202-564-2496Last EDR Contact: 03/30/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Annually

US AIRS MINOR: Air Facility System DataA listing of minor source facilities.

Date of Government Version: 10/16/2014Date Data Arrived at EDR: 10/31/2014Date Made Active in Reports: 11/17/2014Number of Days to Update: 17

Source: EPATelephone: 202-564-2496Last EDR Contact: 03/30/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Annually

Financial Assurance 1: Financial Assurance Information ListingFinancial assurance information.

Date of Government Version: 01/09/2015Date Data Arrived at EDR: 01/16/2015Date Made Active in Reports: 02/20/2015Number of Days to Update: 35

Source: Dept of Environmental QualityTelephone: 517-335-6610Last EDR Contact: 04/06/2015Next Scheduled EDR Contact: 07/06/2015Data Release Frequency: Varies

Financial Assurance 2: Financial Assurance Information ListingA listing of financial assurance information for solid waste facilities. Financial assurance is intended to ensurethat resources are available to pay for the cost of closure, post-closure care, and corrective measures if theowner or operator of a regulated facility is unable or unwilling to pay.

Date of Government Version: 01/05/2011Date Data Arrived at EDR: 01/07/2011Date Made Active in Reports: 02/14/2011Number of Days to Update: 38

Source: Dept of Environmental QualityTelephone: 517-335-4034Last EDR Contact: 03/30/2015Next Scheduled EDR Contact: 07/13/2015Data Release Frequency: Varies

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US FIN ASSUR: Financial Assurance InformationAll owners and operators of facilities that treat, store, or dispose of hazardous waste are required to provideproof that they will have sufficient funds to pay for the clean up, closure, and post-closure care of their facilities.

Date of Government Version: 03/09/2015Date Data Arrived at EDR: 03/10/2015Date Made Active in Reports: 03/25/2015Number of Days to Update: 15

Source: Environmental Protection AgencyTelephone: 202-566-1917Last EDR Contact: 02/16/2015Next Scheduled EDR Contact: 06/01/2015Data Release Frequency: Quarterly

COAL ASH EPA: Coal Combustion Residues Surface Impoundments ListA listing of coal combustion residues surface impoundments with high hazard potential ratings.

Date of Government Version: 07/01/2014Date Data Arrived at EDR: 09/10/2014Date Made Active in Reports: 10/20/2014Number of Days to Update: 40

Source: Environmental Protection AgencyTelephone: N/ALast EDR Contact: 03/13/2015Next Scheduled EDR Contact: 06/22/2015Data Release Frequency: Varies

PCB TRANSFORMER: PCB Transformer Registration DatabaseThe database of PCB transformer registrations that includes all PCB registration submittals.

Date of Government Version: 02/01/2011Date Data Arrived at EDR: 10/19/2011Date Made Active in Reports: 01/10/2012Number of Days to Update: 83

Source: Environmental Protection AgencyTelephone: 202-566-0517Last EDR Contact: 01/30/2015Next Scheduled EDR Contact: 05/11/2015Data Release Frequency: Varies

EPA WATCH LIST: EPA WATCH LISTEPA maintains a "Watch List" to facilitate dialogue between EPA, state and local environmental agencies on enforcementmatters relating to facilities with alleged violations identified as either significant or high priority. Beingon the Watch List does not mean that the facility has actually violated the law only that an investigation byEPA or a state or local environmental agency has led those organizations to allege that an unproven violationhas in fact occurred. Being on the Watch List does not represent a higher level of concern regarding the allegedviolations that were detected, but instead indicates cases requiring additional dialogue between EPA, state andlocal agencies - primarily because of the length of time the alleged violation has gone unaddressed or unresolved.

Date of Government Version: 08/30/2013Date Data Arrived at EDR: 03/21/2014Date Made Active in Reports: 06/17/2014Number of Days to Update: 88

Source: Environmental Protection AgencyTelephone: 617-520-3000Last EDR Contact: 02/09/2015Next Scheduled EDR Contact: 05/25/2015Data Release Frequency: Quarterly

WDS: Waste Data SystemThe Waste Data System (WDS) tracks activities at facilities regulated by the Solid Waste, Scrap Tire, HazardousWaste, and Liquid Industrial Waste programs.

Date of Government Version: 03/04/2015Date Data Arrived at EDR: 03/06/2015Date Made Active in Reports: 03/13/2015Number of Days to Update: 7

Source: Dept of Environmental QualityTelephone: 517-284-6562Last EDR Contact: 02/23/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Quarterly

COAL ASH: Coal Ash Disposal SitesCoal fired power plants in Southeast Michigan that have coal ash handling on site.

Date of Government Version: 10/15/2014Date Data Arrived at EDR: 10/16/2014Date Made Active in Reports: 11/26/2014Number of Days to Update: 41

Source: Dept of Environmental QualityTelephone: 586-753-3754Last EDR Contact: 04/06/2015Next Scheduled EDR Contact: 07/20/2015Data Release Frequency: Varies

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EDR HIGH RISK HISTORICAL RECORDS

EDR Exclusive Records

EDR MGP: EDR Proprietary Manufactured Gas PlantsThe EDR Proprietary Manufactured Gas Plant Database includes records of coal gas plants (manufactured gas plants)compiled by EDR’s researchers. Manufactured gas sites were used in the United States from the 1800’s to 1950’sto produce a gas that could be distributed and used as fuel. These plants used whale oil, rosin, coal, or a mixtureof coal, oil, and water that also produced a significant amount of waste. Many of the byproducts of the gas production,such as coal tar (oily waste containing volatile and non-volatile chemicals), sludges, oils and other compoundsare potentially hazardous to human health and the environment. The byproduct from this process was frequentlydisposed of directly at the plant site and can remain or spread slowly, serving as a continuous source of soiland groundwater contamination.

Date of Government Version: N/ADate Data Arrived at EDR: N/ADate Made Active in Reports: N/ANumber of Days to Update: N/A

Source: EDR, Inc.Telephone: N/ALast EDR Contact: N/ANext Scheduled EDR Contact: N/AData Release Frequency: No Update Planned

EDR US Hist Auto Stat: EDR Exclusive Historic Gas StationsEDR has searched selected national collections of business directories and has collected listings of potentialgas station/filling station/service station sites that were available to EDR researchers. EDR’s review was limitedto those categories of sources that might, in EDR’s opinion, include gas station/filling station/service stationestablishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station,filling station, auto, automobile repair, auto service station, service station, etc. This database falls withina category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presentsunique and sometimes proprietary data about past sites and operations that typically create environmental concerns,but may not show up in current government records searches.

Date of Government Version: N/ADate Data Arrived at EDR: N/ADate Made Active in Reports: N/ANumber of Days to Update: N/A

Source: EDR, Inc.Telephone: N/ALast EDR Contact: N/ANext Scheduled EDR Contact: N/AData Release Frequency: Varies

EDR US Hist Cleaners: EDR Exclusive Historic Dry CleanersEDR has searched selected national collections of business directories and has collected listings of potentialdry cleaner sites that were available to EDR researchers. EDR’s review was limited to those categories of sourcesthat might, in EDR’s opinion, include dry cleaning establishments. The categories reviewed included, but werenot limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database fallswithin a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effortpresents unique and sometimes proprietary data about past sites and operations that typically create environmentalconcerns, but may not show up in current government records searches.

Date of Government Version: N/ADate Data Arrived at EDR: N/ADate Made Active in Reports: N/ANumber of Days to Update: N/A

Source: EDR, Inc.Telephone: N/ALast EDR Contact: N/ANext Scheduled EDR Contact: N/AData Release Frequency: Varies

EDR RECOVERED GOVERNMENT ARCHIVES

Exclusive Recovered Govt. Archives

RGA LUST: Recovered Government Archive Leaking Underground Storage TankThe EDR Recovered Government Archive Leaking Underground Storage Tank database provides a list of LUST incidentsderived from historical databases and includes many records that no longer appear in current government lists.Compiled from Records formerly available from the Department of Environmental Quality in Michigan.

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Date of Government Version: N/ADate Data Arrived at EDR: 07/01/2013Date Made Active in Reports: 12/24/2013Number of Days to Update: 176

Source: Department of Environmental QualityTelephone: N/ALast EDR Contact: 06/01/2012Next Scheduled EDR Contact: N/AData Release Frequency: Varies

RGA LF: Recovered Government Archive Solid Waste Facilities ListThe EDR Recovered Government Archive Landfill database provides a list of landfills derived from historical databasesand includes many records that no longer appear in current government lists. Compiled from Records formerly availablefrom the Department of Environmental Quality in Michigan.

Date of Government Version: N/ADate Data Arrived at EDR: 07/01/2013Date Made Active in Reports: 01/13/2014Number of Days to Update: 196

Source: Department of Environmental QualityTelephone: N/ALast EDR Contact: 06/01/2012Next Scheduled EDR Contact: N/AData Release Frequency: Varies

RGA PART 201: Recovered Government Archive State Hazardous Waste Facilities ListThe EDR Recovered Government Archive State Hazardous Waste database provides a list of SHWS incidents derivedfrom historical databases and includes many records that no longer appear in current government lists. Compiledfrom Records formerly available from the Department of Environmental Quality in Michigan.

Date of Government Version: N/ADate Data Arrived at EDR: 07/01/2013Date Made Active in Reports: 12/24/2013Number of Days to Update: 176

Source: Department of Environmental QualityTelephone: N/ALast EDR Contact: 06/01/2012Next Scheduled EDR Contact: N/AData Release Frequency: Varies

OTHER DATABASE(S)

Depending on the geographic area covered by this report, the data provided in these specialty databases may or may not becomplete. For example, the existence of wetlands information data in a specific report does not mean that all wetlands in thearea covered by the report are included. Moreover, the absence of any reported wetlands information does not necessarilymean that wetlands do not exist in the area covered by the report.

CT MANIFEST: Hazardous Waste Manifest DataFacility and manifest data. Manifest is a document that lists and tracks hazardous waste from the generator throughtransporters to a tsd facility.

Date of Government Version: 07/30/2013Date Data Arrived at EDR: 08/19/2013Date Made Active in Reports: 10/03/2013Number of Days to Update: 45

Source: Department of Energy & Environmental ProtectionTelephone: 860-424-3375Last EDR Contact: 11/17/2014Next Scheduled EDR Contact: 03/02/2015Data Release Frequency: No Update Planned

NJ MANIFEST: Manifest InformationHazardous waste manifest information.

Date of Government Version: 12/31/2011Date Data Arrived at EDR: 07/19/2012Date Made Active in Reports: 08/28/2012Number of Days to Update: 40

Source: Department of Environmental ProtectionTelephone: N/ALast EDR Contact: 04/14/2015Next Scheduled EDR Contact: 07/27/2015Data Release Frequency: Annually

NY MANIFEST: Facility and Manifest DataManifest is a document that lists and tracks hazardous waste from the generator through transporters to a TSDfacility.

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Date of Government Version: 01/01/2015Date Data Arrived at EDR: 02/04/2015Date Made Active in Reports: 02/27/2015Number of Days to Update: 23

Source: Department of Environmental ConservationTelephone: 518-402-8651Last EDR Contact: 02/04/2015Next Scheduled EDR Contact: 05/18/2015Data Release Frequency: Annually

PA MANIFEST: Manifest InformationHazardous waste manifest information.

Date of Government Version: 12/31/2013Date Data Arrived at EDR: 07/21/2014Date Made Active in Reports: 08/25/2014Number of Days to Update: 35

Source: Department of Environmental ProtectionTelephone: 717-783-8990Last EDR Contact: 04/16/2015Next Scheduled EDR Contact: 08/03/2015Data Release Frequency: Annually

RI MANIFEST: Manifest informationHazardous waste manifest information

Date of Government Version: 12/31/2013Date Data Arrived at EDR: 07/15/2014Date Made Active in Reports: 08/13/2014Number of Days to Update: 29

Source: Department of Environmental ManagementTelephone: 401-222-2797Last EDR Contact: 02/23/2015Next Scheduled EDR Contact: 06/08/2015Data Release Frequency: Annually

WI MANIFEST: Manifest InformationHazardous waste manifest information.

Date of Government Version: 12/31/2014Date Data Arrived at EDR: 03/19/2015Date Made Active in Reports: 04/07/2015Number of Days to Update: 19

Source: Department of Natural ResourcesTelephone: N/ALast EDR Contact: 03/13/2015Next Scheduled EDR Contact: 06/29/2015Data Release Frequency: Annually

Oil/Gas Pipelines: This data was obtained by EDR from the USGS in 1994. It is referred to by USGS as GeoData Digital Line Graphsfrom 1:100,000-Scale Maps. It was extracted from the transportation category including some oil, but primarilygas pipelines.

Sensitive Receptors: There are individuals deemed sensitive receptors due to their fragile immune systems and special sensitivityto environmental discharges. These sensitive receptors typically include the elderly, the sick, and children. While the location of allsensitive receptors cannot be determined, EDR indicates those buildings and facilities - schools, daycares, hospitals, medical centers,and nursing homes - where individuals who are sensitive receptors are likely to be located.

AHA Hospitals:Source: American Hospital Association, Inc.Telephone: 312-280-5991The database includes a listing of hospitals based on the American Hospital Association’s annual survey of hospitals.

Medical Centers: Provider of Services ListingSource: Centers for Medicare & Medicaid ServicesTelephone: 410-786-3000A listing of hospitals with Medicare provider number, produced by Centers of Medicare & Medicaid Services,a federal agency within the U.S. Department of Health and Human Services.

Nursing HomesSource: National Institutes of HealthTelephone: 301-594-6248Information on Medicare and Medicaid certified nursing homes in the United States.

Public SchoolsSource: National Center for Education StatisticsTelephone: 202-502-7300The National Center for Education Statistics’ primary database on elementaryand secondary public education in the United States. It is a comprehensive, annual, national statisticaldatabase of all public elementary and secondary schools and school districts, which contains data that arecomparable across all states.

TC4278659.2s Page GR-23

GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING

Page 205: Baseline Environmental Assessment for Riverside Park

Private SchoolsSource: National Center for Education StatisticsTelephone: 202-502-7300The National Center for Education Statistics’ primary database on private school locations in the United States.

Daycare Centers: Day Care Centers, Group & Family HomesSource: Bureau of REgulatory ServicesTelephone: 517-373-8300

Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the FederalEmergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA.

NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDRin 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service.

State Wetlands Data: Wetlands InventorySource: Department of Natural ResourcesTelephone: 517-241-2254

Scanned Digital USGS 7.5’ Topographic Map (DRG)Source: United States Geologic SurveyA digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map imagesare made by scanning published paper maps on high-resolution scanners. The raster imageis georeferenced and fit to the Universal Transverse Mercator (UTM) projection.

STREET AND ADDRESS INFORMATION

© 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protectionand other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subjectto the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material.

TC4278659.2s Page GR-24

GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING

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TC4278659.2s Page A-1

geologic strata.of the soil, and nearby wells. Groundwater flow velocity is generally impacted by the nature of theGroundwater flow direction may be impacted by surface topography, hydrology, hydrogeology, characteristics

2. Groundwater flow velocity. 1. Groundwater flow direction, and

Assessment of the impact of contaminant migration generally has two principal investigative components:

forming an opinion about the impact of potential contaminant migration.EDR’s GeoCheck Physical Setting Source Addendum is provided to assist the environmental professional in

1980Most Recent Revision:42083-C1 DETROIT, MI CA08Target Property Map:

USGS TOPOGRAPHIC MAP

577 ft. above sea levelElevation:4686202.5UTM Y (Meters): 328440.7UTM X (Meters): Zone 17Universal Tranverse Mercator: 83.0816 - 83˚ 4’ 53.76’’Longitude (West): 42.3111 - 42˚ 18’ 39.96’’Latitude (North):

TARGET PROPERTY COORDINATES

DETROIT, MI 482163801 W. JEFFERSON AVEUNE3801 W. JEFFERSON AVEUNE PROPERTY

TARGET PROPERTY ADDRESS

®GEOCHECK - PHYSICAL SETTING SOURCE ADDENDUM®

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should be field verified.on a relative (not an absolute) basis. Relative elevation information between sites of close proximitySource: Topography has been determined from the USGS 7.5’ Digital Elevation Model and should be evaluated

SURROUNDING TOPOGRAPHY: ELEVATION PROFILES

Elev

atio

n (ft

)El

evat

ion

(ft)

TP

TP0 1/2 1 Miles

✩Target Property Elevation: 577 ft.

North South

West East

571

571

571

571

571

571

570

570

570

577

583

588

589

589

589

598

593

591

594589

585

589

587

585

587

586

585

582

577 570

570

570

571

571

571

571

571

573

General SEGeneral Topographic Gradient:TARGET PROPERTY TOPOGRAPHY

should contamination exist on the target property, what downgradient sites might be impacted.assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or,Surface topography may be indicative of the direction of surficial groundwater flow. This information can be used toTOPOGRAPHIC INFORMATION

collected on nearby properties, and regional groundwater flow information (from deep aquifers).sources of information, such as surface topographic information, hydrologic information, hydrogeologic datausing site-specific well data. If such data is not reasonably ascertainable, it may be necessary to rely on otherGroundwater flow direction for a particular site is best determined by a qualified environmental professionalGROUNDWATER FLOW DIRECTION INFORMATION

®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY®

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TC4278659.2s Page A-3

For additional site information, refer to Physical Setting Source Map Findings.

Not Reported1/2 - 1 Mile NNE2

GENERAL DIRECTIONLOCATIONGROUNDWATER FLOWFROM TPMAP ID

hydrogeologically, and the depth to water table.authorities at select sites and has extracted the date of the report, groundwater flow direction as determinedflow at specific points. EDR has reviewed reports submitted by environmental professionals to regulatoryEDR has developed the AQUIFLOW Information System to provide data on the general direction of groundwater

AQUIFLOW®

Search Radius: 1.000 Mile.

Not found Status:1.25 miles Search Radius:

Site-Specific Hydrogeological Data*:

* ©1996 Site−specific hydrogeological data gathered by CERCLIS Alerts, Inc., Bainbridge Island, WA. All rights reserved. All of the information and opinions presented are those of the cited EPA report(s), which were completed undera Comprehensive Environmental Response Compensation and Liability Information System (CERCLIS) investigation.

contamination exist on the target property, what downgradient sites might be impacted.environmental professional in forming an opinion about the impact of nearby contaminated properties or, shouldof groundwater flow direction in the immediate area. Such hydrogeologic information can be used to assist theHydrogeologic information obtained by installation of wells on a specific site can often be an indicatorHYDROGEOLOGIC INFORMATION

YES - refer to the Overview Map and Detail MapDETROIT

NATIONAL WETLAND INVENTORYNWI ElectronicData CoverageNWI Quad at Target Property

2602220030B - FEMA Q3 Flood dataAdditional Panels in search area:

2602220045B - FEMA Q3 Flood dataFlood Plain Panel at Target Property:

YES - refer to the Overview Map and Detail MapWAYNE, MI

FEMA FLOOD ZONEFEMA FloodElectronic DataTarget Property County

and bodies of water).Refer to the Physical Setting Source Map following this summary for hydrologic information (major waterways

contamination exist on the target property, what downgradient sites might be impacted.the environmental professional in forming an opinion about the impact of nearby contaminated properties or, shouldSurface water can act as a hydrologic barrier to groundwater flow. Such hydrologic information can be used to assistHYDROLOGIC INFORMATION

®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY®

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> 0 inchesDepth to Bedrock Max:

> 0 inchesDepth to Bedrock Min:

Not ReportedCorrosion Potential - Uncoated Steel:

Hydric Status: Soil does not meet the requirements for a hydric soil.

Not reportedSoil Drainage Class:

Not reportedHydrologic Group:

variableSoil Surface Texture:

URBANLAND Soil Component Name:

The following information is based on Soil Conservation Service STATSGO data.in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO) soil survey maps.for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patternsSurvey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey informationThe U.S. Department of Agriculture’s (USDA) Soil Conservation Service (SCS) leads the National Cooperative Soil

DOMINANT SOIL COMPOSITION IN GENERAL AREA OF TARGET PROPERTY

Map, USGS Digital Data Series DDS - 11 (1994).of the Conterminous U.S. at 1:2,500,000 Scale - a digital representation of the 1974 P.B. King and H.M. BeikmanGeologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology

ROCK STRATIGRAPHIC UNIT GEOLOGIC AGE IDENTIFICATION

Stratified SequenceCategory:PaleozoicEra:DevonianSystem:Middle DevonianSeries:D2Code: (decoded above as Era, System & Series)

at which contaminant migration may be occurring.Geologic information can be used by the environmental professional in forming an opinion about the relative speedGEOLOGIC INFORMATION IN GENERAL AREA OF TARGET PROPERTY

move more quickly through sandy-gravelly types of soils than silty-clayey types of soils.characteristics data collected on nearby properties and regional soil information. In general, contaminant plumesto rely on other sources of information, including geologic age identification, rock stratigraphic unit and soilusing site specific geologic and soil strata data. If such data are not reasonably ascertainable, it may be necessaryGroundwater flow velocity information for a particular site is best determined by a qualified environmental professionalGROUNDWATER FLOW VELOCITY INFORMATION

®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY®

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FEDERAL USGS WELL INFORMATION

LOCATIONFROM TPWELL IDMAP ID

1.000State DatabaseNearest PWS within 1 mileFederal FRDS PWS1.000Federal USGS

WELL SEARCH DISTANCE INFORMATION

SEARCH DISTANCE (miles)DATABASE

opinion about the impact of contaminant migration on nearby drinking water wells.professional in assessing sources that may impact ground water flow direction, and in forming anEDR Local/Regional Water Agency records provide water well information to assist the environmental

LOCAL / REGIONAL WATER AGENCY RECORDS

silty clayclay loamsandsilt loamDeeper Soil Types:

silty claysandShallow Soil Types:

loamy sandloamy fine sandclay loamSurficial Soil Types:

loamy sandloamy fine sandclay loamSoil Surface Textures:

appear within the general area of target property.Based on Soil Conservation Service STATSGO data, the following additional subordinant soil types may

OTHER SOIL TYPES IN AREA

Min: 0.00Max: 0.00

Min: 0.00Max: 0.00Not reportedNot reportedvariable60 inches 0 inches 1

Soil Layer Information

Boundary ClassificationPermeabilityRate (in/hr)

Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction(pH)

®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY®

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TC4278659.2s Page A-6

No Wells Found

STATE DATABASE WELL INFORMATION

LOCATIONFROM TPWELL IDMAP ID

Note: PWS System location is not always the same as well location.

No PWS System Found

FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION

LOCATIONFROM TPWELL IDMAP ID

1/4 - 1/2 Mile NEUSGS40000481767 1

FEDERAL USGS WELL INFORMATION

LOCATIONFROM TPWELL IDMAP ID

®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY®

Page 212: Baseline Environmental Assessment for Riverside Park

EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.

6 00600

600600 60

0

6 0 0

60 0

MI

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TC4278659.2s Page A-8

Date: 07/23/1996Average Water Table Depth: Not ReportedDeepest Water Table Depth: 11Shallowest Water Table Depth: 2Groundwater Flow: Not ReportedSite ID: Not Reported2

NNE1/2 - 1 MileHigher

36177AQUIFLOW

Ground-water levels, Number of Measurements: 0

Not ReportedWellholedepth units:Not ReportedWellholedepth:Not ReportedWelldepth units:Not ReportedWelldepth:Not ReportedConstruction date:

Not ReportedAquifer type:Not ReportedFormation type:Not ReportedAquifername:

USCountrycode:Not ReportedVert coord refsys:Not ReportedVertcollection method:Not ReportedVert accmeasure units:

Not ReportedVertacc measure val:Not ReportedVert measure units:Not ReportedVert measure val:NAD83Horiz coord refsys:

Interpolated from mapHoriz Collection method:minutesHoriz Acc measure units:1Horiz Acc measure:Not ReportedSourcemap scale:-83.0763104Longitude:42.3142049Latitude:Not ReportedContrib drainagearea units:Not ReportedContrib drainagearea:Not ReportedDrainagearea Units:Not ReportedDrainagearea value:Not ReportedHuc code:

Not ReportedMonloc desc:WellMonloc type:WAYNE CO (MICH CON RIVERSIDE, P1)Monloc name:USGS-421851083043501Monloc Identifier:USGS Michigan Water Science CenterFormal name:USGS-MIOrg. Identifier:

1NE1/4 - 1/2 MileHigher

USGS40000481767FED USGS

Map IDDirectionDistanceElevation EDR ID NumberDatabase

®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS®

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TC4278659.2s Page A-9

0%3%97%1.398 pCi/LBasementNot ReportedNot ReportedNot ReportedNot ReportedLiving Area - 2nd Floor0%0%100%0.853 pCi/LLiving Area - 1st Floor

% >20 pCi/L% 4-20 pCi/L% <4 pCi/LAverage ActivityArea

Number of sites tested: 159

Federal Area Radon Information for WAYNE COUNTY, MI

: Zone 3 indoor average level < 2 pCi/L. : Zone 2 indoor average level >= 2 pCi/L and <= 4 pCi/L. Note: Zone 1 indoor average level > 4 pCi/L.

Federal EPA Radon Zone for WAYNE County: 3

1.511/19/200748216

_________________________ResultLT SignTest DateZipcode

Radon Test Results

State Database: MI Radon

AREA RADON INFORMATION

®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGSRADON

®

Page 215: Baseline Environmental Assessment for Riverside Park

TOPOGRAPHIC INFORMATION

USGS 7.5’ Digital Elevation Model (DEM)Source: United States Geologic SurveyEDR acquired the USGS 7.5’ Digital Elevation Model in 2002 and updated it in 2006. The 7.5 minute DEM correspondsto the USGS 1:24,000- and 1:25,000-scale topographic quadrangle maps. The DEM provides elevation datawith consistent elevation units and projection.

Scanned Digital USGS 7.5’ Topographic Map (DRG)Source: United States Geologic SurveyA digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map imagesare made by scanning published paper maps on high-resolution scanners. The raster imageis georeferenced and fit to the Universal Transverse Mercator (UTM) projection.

HYDROLOGIC INFORMATION

Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the FederalEmergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA.

NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDRin 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service.

State Wetlands Data: Wetlands InventorySource: Department of Natural ResourcesTelephone: 517-241-2254

HYDROGEOLOGIC INFORMATION

AQUIFLOW Information SystemRSource: EDR proprietary database of groundwater flow informationEDR has developed the AQUIFLOW Information System (AIS) to provide data on the general direction of groundwater

flow at specific points. EDR has reviewed reports submitted to regulatory authorities at select sites and hasextracted the date of the report, hydrogeologically determined groundwater flow direction and depth to water tableinformation.

GEOLOGIC INFORMATION

Geologic Age and Rock Stratigraphic UnitSource: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology of the Conterminous U.S. at 1:2,500,000 Scale - A digitalrepresentation of the 1974 P.B. King and H.M. Beikman Map, USGS Digital Data Series DDS - 11 (1994).

STATSGO: State Soil Geographic DatabaseSource: Department of Agriculture, Natural Resources Conservation ServicesThe U.S. Department of Agriculture’s (USDA) Natural Resources Conservation Service (NRCS) leads the nationalConservation Soil Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soilsurvey information for privately owned lands in the United States. A soil map in a soil survey is a representationof soil patterns in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO)soil survey maps.

SSURGO: Soil Survey Geographic DatabaseSource: Department of Agriculture, Natural Resources Conservation Services (NRCS)Telephone: 800-672-5559SSURGO is the most detailed level of mapping done by the Natural Resources Conservation Services, mappingscales generally range from 1:12,000 to 1:63,360. Field mapping methods using national standards are used toconstruct the soil maps in the Soil Survey Geographic (SSURGO) database. SSURGO digitizing duplicates theoriginal soil survey maps. This level of mapping is designed for use by landowners, townships and countynatural resource planning and management.

TC4278659.2s Page PSGR-1

PHYSICAL SETTING SOURCE RECORDS SEARCHED

Page 216: Baseline Environmental Assessment for Riverside Park

LOCAL / REGIONAL WATER AGENCY RECORDS

FEDERAL WATER WELLS

PWS: Public Water SystemsSource: EPA/Office of Drinking WaterTelephone: 202-564-3750Public Water System data from the Federal Reporting Data System. A PWS is any water system which provides water to at

least 25 people for at least 60 days annually. PWSs provide water from wells, rivers and other sources.

PWS ENF: Public Water Systems Violation and Enforcement DataSource: EPA/Office of Drinking WaterTelephone: 202-564-3750Violation and Enforcement data for Public Water Systems from the Safe Drinking Water Information System (SDWIS) after

August 1995. Prior to August 1995, the data came from the Federal Reporting Data System (FRDS).

USGS Water Wells: USGS National Water Inventory System (NWIS)This database contains descriptive information on sites where the USGS collects or has collected data on surfacewater and/or groundwater. The groundwater data includes information on wells, springs, and other sources of groundwater.

OTHER STATE DATABASE INFORMATION

RADON

State Database: MI RadonSource: Department of Environmental QualityTelephone: 517-335-9551Radon Test Results

Michigan Radon Test ResultsSource: Department of Environmental QualityTelephone: 517-335-8037These results are from test kits distributed by the local health departments and used byMichigan residents. There is no way of knowing whether the devices were used properly, whether there are duplicates(or repeat verification) test (i.e., more than one sample per home), etc.

Area Radon InformationSource: USGSTelephone: 703-356-4020The National Radon Database has been developed by the U.S. Environmental Protection Agency(USEPA) and is a compilation of the EPA/State Residential Radon Survey and the National Residential Radon Survey.The study covers the years 1986 - 1992. Where necessary data has been supplemented by information collected atprivate sources such as universities and research institutions.

EPA Radon ZonesSource: EPATelephone: 703-356-4020Sections 307 & 309 of IRAA directed EPA to list and identify areas of U.S. with the potential for elevated indoorradon levels.

OTHER

Airport Landing Facilities: Private and public use landing facilitiesSource: Federal Aviation Administration, 800-457-6656

Epicenters: World earthquake epicenters, Richter 5 or greaterSource: Department of Commerce, National Oceanic and Atmospheric Administration

Earthquake Fault Lines: The fault lines displayed on EDR’s Topographic map are digitized quaternary faultlines, preparedin 1975 by the United State Geological Survey

TC4278659.2s Page PSGR-2

PHYSICAL SETTING SOURCE RECORDS SEARCHED

Page 217: Baseline Environmental Assessment for Riverside Park

STREET AND ADDRESS INFORMATION

© 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protectionand other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subjectto the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material.

TC4278659.2s Page PSGR-3

PHYSICAL SETTING SOURCE RECORDS SEARCHED

Page 218: Baseline Environmental Assessment for Riverside Park

APPENDIX ESANBORN MAPS

Page 219: Baseline Environmental Assessment for Riverside Park

&HUWLILHG�6DQERUQ��0DS�5HSRUW

3801 W. Jefferson Aveune Property3801 W. Jefferson AveuneDetroit, MI 48216

Inquiry Number: 4278659.3April 29, 2015

Page 220: Baseline Environmental Assessment for Riverside Park

Certified Sanborn® Map Report 4/29/15

Site Name:3801 W. Jefferson Aveune3801 W. Jefferson AveuneDetroit, MI 48216

Client Name:NTH Consultants Ltd.41780 6 Mile RoadNorthville, MI 48168

Contact: Cliff AndrewsEDR Inquiry # 4278659.3

The Sanborn Library has been searched by EDR and maps covering the target property location as provided by NTHConsultants Ltd. were identified for the years listed below. The Sanborn Library is the largest, most complete collectionof fire insurance maps. The collection includes maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow, andothers. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction ofmaps by the Sanborn Library LLC, the copyright holder for the collection. Results can be authenticated by visitingwww.edrnet.com/sanborn.

The Sanborn Library is continually enhanced with newly identified map archives. This report accesses all maps in thecollection as of the day this report was generated.

Certified Sanborn Results:

Site Name: 3801 W. Jefferson Aveune PropertyAddress: 3801 W. Jefferson AveuneCity, State, Zip: Detroit, MI 48216Cross Street:P.O. # 62-140614-100Project: 62-140614-100Certification # 1B1A-4518-806D

Library of Congress

University Publications of America

EDR Private Collection

The Sanborn Library LLC Since 1866™

The Sanborn Library includes more than 1.2 millionfire insurance maps from Sanborn, Bromley, Perris &Browne, Hopkins, Barlow and others which trackhistorical property usage in approximately 12,000American cities and towns. Collections searched:

Sanborn® Library search resultsCertification # 1B1A-4518-806D

Maps Provided:200219961991198819771961

195719521950192119181897

1884

Limited Permission To Make CopiesNTH Consultants Ltd. (the client) is permitted to make up to FIVE photocopies of this Sanborn Map transmittal and each fire insurance mapaccompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request madedirectly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission isconditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request.

Disclaimer - Copyright and Trademark noticeThis Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot beconcluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED ORIMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THEMAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALLRISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OFERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL,INCIDENTAL CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLYLIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risklevels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providingany facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by anenvironmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to beconstrued as legal advice.

Copyright 2015 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map ofEnvironmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.

EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein arethe property of their respective owners.

4278659 - 3 page 2

Page 221: Baseline Environmental Assessment for Riverside Park

Sanborn Sheet ThumbnailsThis Certified Sanborn Map Report is based upon the following SanbornFire Insurance map sheets.

2002 Source Sheets

Volume 1, Sheet 109

1996 Source Sheets

Volume 1, Sheet 109

1991 Source Sheets

Volume 1, Sheet 109

1988 Source Sheets

Volume 1, Sheet 109

4278659 - 3 page 3

Page 222: Baseline Environmental Assessment for Riverside Park

1977 Source Sheets

Volume 1, Sheet 109

1961 Source Sheets

Volume 1, Sheet 109

1957 Source Sheets

Volume 1, Sheet 109

1952 Source Sheets

Volume 1, Sheet 109

4278659 - 3 page 4

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1950 Source Sheets

Volume 1, Sheet 86 Volume 1, Sheet 109

1921 Source Sheets

Volume 1, Sheet 109

1918 Source Sheets

Volume 1, Sheet 82

1897 Source Sheets

Volume 1, Sheet 80 Volume 1, Sheet 82

4278659 - 3 page 5

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1884 Source Sheets

Volume 1, Sheet 23

4278659 - 3 page 6

Page 225: Baseline Environmental Assessment for Riverside Park

2002 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 2002

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 7

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1996 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1996

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 8

Page 227: Baseline Environmental Assessment for Riverside Park

1991 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1991

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 9

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1988 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1988

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 10

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1977 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1977

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 11

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1961 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1961

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 12

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1957 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1957

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 13

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1952 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1952

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 14

Page 233: Baseline Environmental Assessment for Riverside Park

1950 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1950

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 86Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 15

Page 234: Baseline Environmental Assessment for Riverside Park

1921 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1921

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 109

0 Feet 150 300 600

4278659 - 3 page 16

Page 235: Baseline Environmental Assessment for Riverside Park

1918 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1918

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 82

0 Feet 150 300 600

4278659 - 3 page 17

Page 236: Baseline Environmental Assessment for Riverside Park

1897 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1897

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 80Volume 1, Sheet 82

0 Feet 150 300 600

4278659 - 3 page 18

Page 237: Baseline Environmental Assessment for Riverside Park

1884 Certified Sanborn Map

1B1A

-451

8-80

6D

Order Date:EDR Inquiry:

Client:

Site Name:Address:

City, ST, ZIP:

Certification #

Copyright: 1884

4/29/2015 11:52:00 AM4278659.3

NTH Consultants Ltd.

3801 W. Jefferson Aveune Property3801 W. Jefferson Aveune

Detroit MI 48216

1B1A-4518-806D

This Certified Sanborn Map combines the following sheets.Outlined areas indicate map sheets within the collection.

Volume 1, Sheet 23

0 Feet 150 300 600

4278659 - 3 page 19

Page 238: Baseline Environmental Assessment for Riverside Park

APPENDIX FOWNER QUESTIONNAIRE

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APPENDIX GRESUMES OF ENVIRONMENTALPROFESSIONALS

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Cliff J. Andrews Senior Project Professional Expertise Mr. Andrews has more than 26 years of experience in performing and managing soil investigations, remedial investigations, environmental due diligence assessments, demolition and construction oversight. His project work has included Phase I and II environmental site assessments, baseline environmental assessments and Compliance Analysis (Due Care) Plans, soil and groundwater contamination remedial studies, storm water illicit discharge studies, geotechnical investigations, building demolition, restoration of concrete structures, and construction monitoring. Education Associates Degree, Applied Science; Schoolcraft College (1993) Experience Environmental Investigations Performed or managed over 3500 Phase I and Phase II Environmental Site Assessments for property transfers in Michigan and several other states. Additionally, served as a team member and field leader for Phase I and Phase II ESA’s for the dual stadiums in Detroit, and the expansion of international terminal at Metro Airport. Prepared Baseline Environmental Site Assessments and Compliance Analysis (Due Care) Plans for Brownfield sites. Provided field monitoring, environmental consulting and project management for underground storage tank (UST) removal projects, including remedial investigation, and pilot studies for leaking UST’s. Carried out geophysical surveys to identify buried UST’s and drums on previously developed properties. Presented field monitoring, environmental consulting and project management for petroleum hydrocarbon and chlorinated solvent soil and groundwater remediation projects, including remedial investigation, pilot studies, design, installation, and operation of air water separator and liquid phase carbon units, a soil vapor extraction and air sparge blowers. Performed and managed storm water management for a local school district including illicit discharge investigations, preparation of storm water management plan and annual as management plans. Demolition/Site Redevelopment Activities Completed and managed demolition of commercial and educational structures including bid specification preparation, trade contractor procurement, and management for waste / debris removal, hazardous materials surveys and hazardous materials abatement, building demolition oversight, and site restoration. Geotechnical Investigations Performed more than 500 soil/geotechnical and hydrogeologic investigations, including the supervision of drilling operations, rock coring, monitoring well installation, and cross-hole, vane shear, and cone penetration testing. Performed Shelby and piston tube, soil/sediment and groundwater sampling.

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Cliff J. Andrews Geotechnical Investigations (cont’d) Served as team leader for a combination geotechnical and concrete investigation for ten hydro-dams in northern Michigan. Collected vertical and horizontal concrete cores, and conducted a soil investigation, including soil borings and the installation of a piezometer along the concrete retaining walls and on sloped earthen embankments providing difficult access. Completed work under budget, ahead of schedule, and without interruption to the service provided by the dams. Construction Restoration/Monitoring Supervised investigations and restorations of parking structures and buildings. Investigated the structures to identify areas requiring repair by the contractor. Monitored the repairs, and assisted with contractor’s invoicing. Monitored more than 200 construction projects, including inspection of caissons, auger piles, grade beams, concrete placement, soil balancing and structural steel. Facilitated interaction between the general contractor and the various trades, including preparation of daily reports. Certifications State Michigan Certified Asbestos Inspector 40-Hour Hazardous Waste Activities Health and Safety Training per 29 CFR 1910.120, with yearly 8-hour refresher courses as required.

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Bhushan C. Modi Vice President/ Senior Principal Engineer Expertise Mr. Modi has over 25 years of experience in performing and managing a wide variety of environmental, geotechnical and construction projects. He has extensive experience in soil investigations, remedial investigations, environmental due diligence assessments, hazardous materials inventory/demolition surveys, industrial hygiene studies and Brownfield projects. His project work has included site redevelopment, building demolition support, underground storage tanks, property transfers, and soil and groundwater remediation activities. He has successfully managed multi-disciplined teams addressing all phases of projects from coordinating and planning through construction and operation/implementation. Education Graduate Certificate, Environmental Auditing; Wayne State University Master of Science, Civil Engineering; University of Detroit Bachelor of Science, Civil Engineering; University of Bombay Experience Environmental Due Diligence Assessments / Brownfield Redevelopment Performed and managed over 5,000 Phase I and Phase II environmental site assessments for private and public sector clients in US, Canada and Mexico. Prepared and reviewed over 250 Baseline Environmental Assessments and Compliance Analysis or Due Care Plans for Brownfield redevelopment projects. Provided management and engineering services for waste removal and industrial hygiene projects. Project tasks have included coordinating and managing asbestos and lead-based paint surveys, mold investigations and indoor air quality studies. Monitored implementation of Due Care Plans and Construction Sequencing Plans at Brownfield sites. Monitored installation of environmental barriers and engineering controls. Developed a program of annual inspections of environmental barriers. Managed and oversaw implementation of environmental remediation and cleanups Geotechnical/Hydrogeological Investigations Performed and managed over 500 soil/geotechnical investigations and construction monitoring projects for residential, recreational, commercial and industrial developments. Implemented various phases of geotechnical and hydrogeologic investigations, including supervising drilling operations, monitoring well installations, performing soil/sediment and groundwater sampling, as well as conducting aquifer testing and geophysical surveys. Underground Storage Tank (UST) Removal/Closure Services Managed and provided environmental consulting services for underground storage tank (UST) removal and closure projects. Prepared UST removal specifications and bid packages, participated in selecting subcontractors on client's behalf, and

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Bhushan C. Modi communicated with appropriate regulatory agencies to achieve site closures and no further action letters. Oversaw investigation and remediation of leaking USTs at several various educational facilities in Michigan. Performed contract review, processed contractor invoices/change orders and engineering oversight. Remediation Services Provided engineering services in a project involving remediation of soil and groundwater impacted with petroleum hydrocarbons at a former gasoline service station site. Assisted in developing a work plan for performing pilot studies and a feasibility analysis to evaluate several corrective action alternatives. Managed a large remediation project at a dry cleaning facility with tetrachloroethene (PCE) or “Perc” contamination. Responsibilities included development of subsurface environmental investigation work plan to determine the severity and extent of PCE contamination in soil and groundwater, provide remedial alternatives, design air sparge (AS) and soil vapor extraction (SVE) system, based on design parameters and cleanup objectives designed a pilot system, and developed bid package for the construction of a remediation system. Demolition/Site Redevelopment Activities Performed project management and demolition oversight for various Brownfield Redevelopment Projects entailing asbestos abatement, lead-based paint evaluation, and removal and disposal of PCB/Mercury-containing equipment and other hazardous materials prior to building demolition or rehabilitation activities. Prepared and reviewed Technical Specifications and Bidding Documents for abatement/removal of hazardous materials and demolition of commercial and educational structures. Certifications 24-hour Asbestos Inspectors Program Radon Diagnostician Certification Course 40-hour OSHA HAZWOP Program

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ATTACHMENT IIPHASE II ESA REPORT

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City of DetroitBuildings, Safety Engineering and Environmental Department

2 Woodward Avenue, Suite 401, Detroit, Michigan 48226

June 9, 2015NTH Project No. 62-140614-100A

ReportPhase II Environmental Site Assessment

3801 West Jeff erson PropertyDetroit, Michigan

NTH Consultants, Ltd.2990 W. Grand Blvd.

Suite M-10Detroit, MI 48202

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TABLE OF CONTENTS Page No.

1.0 EXECUTIVE SUMMARY 1 2.0 INTRODUCTION 2 3.0 SCOPE OF SERVICES 3 4.0 FIELD INVESTIGATION 4 5.0 SUBSURFACE DATA 6 6.0 ANAYTICAL TESTING 6 7.0 EVALUATION OF ANALYTICAL TEST RESULTS 7

7.1 SOIL ANALYTICAL DATA 7 7.1.1 Volatile Organic Compounds (VOCs) 8 7.1.2 Polynuclear Aromatics (PNAs) 8 7.1.3 Polychlorinated Biphenyls (PCBs) 9

7.1.4 Heavy Metals 9

8.0 CONCLUSIONS 10 9.0 LIMITATIONS 13

APPENDICES BORING LOCATION PLAN, FIGURE 1; LOG OF GEOPROBE BORINGS, FIGURE 2; and SUMMARY OF CHEMICAL ANALYSES, TABLE 1 APPENDIX A LABORATORY DATA APPENDIX B

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1.0 EXECUTIVE SUMMARY

This report presents the results of a Phase II Environmental Site Assessment (ESA) for the

3801 West Jefferson property located in Detroit, Wayne County, Michigan. The subject

property is approximately 4.7 acres in size and contains a warehouse building, paved parking

lot and ship dock, and grass-covered areas. The building is used for storage of aluminum

ingots.

The Phase II ESA was performed in accordance with the American Society for Testing and

Materials (ASTM) Practice E1903-11. This study entailed a visual survey to determine the

significance of the vent pipe observed on the exterior north wall of the building and to confirm

the location of the 1,000-gallon gasoline underground storage tank (UST) which was closed-in-

place and filled with concrete in 1987. The vent pipe was traced using a utility locating device

and it terminated in an area inside the building that is covered with a concrete patch. This area

was further evaluated by geoprobe borings and an obstruction indicative of UST was

encountered.

The Phase II ESA also included drilling of geoprobe borings and analysis of soil samples.

The results of analytical testing identified volatile organic compounds (VOCs), polynuclear

aromatics (PNAs) and heavy metals in soil samples above Michigan Department of

Environmental Quality (MDEQ) Part 201 generic residential cleanup criteria. Thus, based

upon these soil analytical results, the property is a “facility”  as defined by 1994 P.A. 451, Part

201, as amended. Additionally, certain VOCs and PNAs were detected in soil samples above

Residential Vapor Intrusion Soil Screening Levels and may require further evaluation based

on the future use of the property.

This Executive Summary should not be reviewed separately from the remainder of the

report. The Executive Summary provides an overview and is not a substitute for a

thorough review of the entire report.

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2.0 INTRODUCTION

NTH Consultants, Ltd. (NTH) was retained by City of Detroit to perform a Phase II

Environmental Site Assessment (ESA) for the 3801 West Jefferson property located in

Detroit, Wayne County, Michigan. The subject property is approximately 4.7 acres in size

and contains a warehouse building, paved parking lot and ship dock, and grass-covered areas.

The warehouse building is used for storage of aluminum ingots.

NTH performed a Phase I ESA for the property in accordance with ASTM E1527-13, and the

results of this study were presented to City of Detroit in a report dated May 19, 2015 (NTH

Project No. 62-140614-100). The Phase I ESA revealed the following evidence of recognized

environmental conditions (RECs):

x The property was formerly a part of Detroit River and was reclaimed to support the

current development. No information on the backfill soil used for land reclamation

purposes is readily available. As such, the environmental nature and origin of the backfill

soil are unknown.

x Past uses of the property include lumber yard, coal yard and warehouse with an oil house.

No information is readily available regarding the past occupants’  hazardous material

handling, storage or waste disposal practices implemented on the premises.

x Railroad spur is located at the property and railroad ties were noted to be stored east of

the building.

x One closed-in-place UST is located inside the building. No documented information was

available to evaluate the environmental status of the UST and its impact on the

surrounding soils.

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x One vent pipe was noted on the north exterior wall of the building. The significance of

this pipe could not be determined.

x Based on the information provided by the current property owners regarding a previous

subsurface investigation, the property is a “facility” as defined by Part P.A. 451, Part

201, as amended.

x Soil and/or groundwater contamination was identified on the westerly and easterly

adjacent sites.

This Phase II ESA was performed in accordance with the ASTM Practice E1903-11, and the

objective of this study was to evaluate the above-identified RECs.

3.0 SCOPE OF SERVICES

x Vent pipe noted on the exterior wall of the building was further evaluated by tracing its

alignment using a hand-held utility locating device.

x Eleven geoprobe borings and three exploratory probes were advanced at the property to

evaluate the Phase I ESA-identified RECs, and to facilitate the collection of soil and

water samples for analyses.

x Soil samples were screened in the field for the presence of total volatile organic

compounds using a portable photoionization detector.

x Soil samples were submitted  to  NTH’s  subcontracted  laboratory  for  analyses.

x Information gathered during the study was evaluated and this report was prepared.

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4.0 FIELD INVESTIGATION

Visual Survey

Municipal records identified one 1,000-gallon gasoline UST in the building. The UST was

installed 1949 and was closed-in-place by filling with concrete in 1987. During the Phase I

ESA, a vent pipe was observed on the exterior north wall of the building. At that time the visual

survey of the interior of the building was limited due to stored pallets of ingots in that area.

Thus, on May 27, 2015, another site visit was made to determine the significance of the noted

vent pipe. NTH personnel observed a hole or an opening in the wall behind the pallets of ingots.

Observations through the opening revealed another room which contained several pipes and

valves. A utility pipe locator was attached to the vent pipe to trace the alignment of this pipe.

The vent pipe extended beneath the floor slab and terminated in an area that was patched with

concrete, which was located under pallets of ingots. The pallets were removed by the building

owner’s  representative  and one exploratory probe (P-1) was advanced within the patched floor

surface. The probe encountered an obstruction at a depth of approximately two feet. Based on

the depth of the obstruction, it was confirmed that the patched area is the location of closed-in-

place UST.

Subsurface Exploration

On May 27 and 28, 2015, 11 geoprobe borings, designated as GP-1 through GP-11, and three

exploratory probes, designated as P-1 through P-3, were advanced at the property by Fibertec

under the observation of Jesse Veenkant of NTH. The following rationale was used for

locating the borings and probes:

Boring No. REC GP-1 Railroad spur

GP-2, GP-11 & P-1 Closed-in-place UST GP-3 Fill soil

GP-4, GP-5, P-2 & P-3 Oil house GP-6 Stored railroad ties

GP-7 thru GP-10 Fill soil

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The borings were located at the approximate locations depicted on the Boring Location Plan,

Figure 1 in Appendix A.

Subsurface conditions observed in each boring are presented on the Log of Geoprobe Borings,

Figure 2 in Appendix A. The stratification shown on the logs represents the approximate

boundary between soil types; the actual transition may be more gradual. In addition, the soil

layers are described based on field classification of observed soil samples. As such, the soil

layer descriptions should be considered generalized.

The geoprobe drilling technique involves mechanically driving or pushing a two-inch outside

diameter stainless steel sampling tool, with a disposable clear acetate liner, to a desired

sampling depth. This technique does not generate soil cuttings because the geoprobe rods

push soils away from the rods as the tool string advances through the hole. The geoprobe

tools and equipment were steam-cleaned prior to arrival at the project site. Furthermore,

between each successive geoprobe location, the tools and equipment were steam-cleaned and

new sample liners were used to minimize the possibility of cross-contamination. Upon

completion of drilling activities and after collecting samples, the boreholes were backfilled

with excavated soil and hydrated bentonite chips. The boreholes were capped with concrete

patch.

Soil samples retrieved from the borings were screened in the field with RAE Systems

MiniRae™  photoionization detector (PID). The PID is capable of detecting total volatile

organic compounds (VOCs) to a detection level of one part per million (ppm). The field PID

measurements on the soil samples are shown on the boring logs in Appendix A. As indicated,

PID readings ranged from than the detection limit of the instrument to 241 ppm. Petroleum

odors were noted in soil samples collected from GP-2 (4.5 to 6 feet), GP-4 (5 to 11.5 feet),

GP-5 (8 to 10.5 feet), GP-11 (5.5 to 7 feet), and P-2 and P-3 (8 to 10.5 feet). Additionally, a

solvent odor indicative of VOCs was noted in the soil sample from GP-6 (10.5 to 11 feet).

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5.0 SUBSURFACE DATA

The subsurface conditions at the explored locations comprised of up to 19 feet of sandy and

clayey fill soil with pieces of brick, coal, porcelain, roofing materials, slag and wood. The fill

soil is underlain by native clayey soils to the explored depths. Obstructions were encounter at

P-1 at a depth of about 2 feet and at GP-5, P-2 and P-3 at depths of about 12 feet. As

previously indicated, a closed-in-place UST is present at the location of P-1. The significance

of obstructions at GP-5, P-2 and P-3 could not be precisely determined, but appear to be

rubble materials in the fill soil. No groundwater was encountered in any of the borings.

6.0 ANALYTICAL TESTING

Soil samples for analysis were selected based on the results of the field screening, including

visual and olfactory observations, and PID measurements. The rationale for selecting soil

samples for analyses is presented in the following table:

Geoprobe No.

Sample No.

Sample Depth (ft.) Rationale

GP-1 S-1 1.0 – 3.0 Fill soil directly beneath the railroad spur. GP-2 S-1 4.5 – 6.0 Fill soil with petroleum odor and highest PID reading. GP-3 S-1 0.5 – 1.5 Fill soil directly beneath the floor. GP-3 S-3 11.0 – 12.5 Fill soil. GP-4 S-1 7.0 – 9.0 Fill soil with petroleum odor and highest PID reading. GP-5 S-1 2.0 – 3.0 Fill soil. GP-5 S-3 9.0 – 10.5 Fill soil with petroleum odor and highest PID reading. GP-6 S-3 10.5 – 11.0 Fill soil with solvent odor and highest PID reading. GP-7 S-1 5.0 – 7.0 Fill soil. GP-8 S-1 2.0 – 3.0 Fill soil. GP-9 S-1 1.5 – 3.5 Fill soil.

GP-10 S-1 4.0 – 5.0 Fill soil. GP-11 S-1 5.5 – 7.0 Fill soil with petroleum odor and highest PID reading. GP-11 S-2 8.0 – 9.5 Fill soil.

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The soil samples were analyzed for VOCs, polynuclear aromatics (PNAs), and the Michigan

10 metals (arsenic, barium, cadmium, chromium, copper, lead, mercury, selenium, silver and

zinc). Additionally, soil samples from GP-1, GP-3 (S-1) and GP-4 were also analyzed for

polychlorinated biphenyls (PCBs). These samples were selected based on their locations (i.e.,

beneath the railroad track, beneath the floor of the building and near the former oil house).

The soil samples for VOC testing were prepared in the field using Michigan-modified

methanol preservation (EPA Method 5035).

The soil samples selected for analyses were placed in laboratory-supplied containers and

stored in a cooler packed with ice. The samples were then released to Fibertec’s  laboratory  in  

accordance  with  NTH’s  standard  chain-of-custody procedures. Laboratory data for the

analyzed samples are included in Appendix B.

7.0 EVALUATION OF ANALYTICAL TEST RESULTS

The results of analyses were compared to the MDEQ-established generic residential cleanup

criteria (GRCC) dated December 30, 2013, pursuant to 1994 P.A. 451, Part 201, as amended.

7.1 SOIL ANALYTICAL DATA

The results of the soil analysis were compared to the Part 201 residential direct contact (DC)

criteria, drinking water protection (DWP) criteria, groundwater/surface water interface

protection (GSIP) criteria, soil volatilization to indoor air criteria (SVIIC), infinite source soil

volatilization to ambient air criteria (VSIC), particulate soil inhalation criteria (PSIC), soil

saturation concentration screening levels (SSCSL).

The results of VOCs, PNAs and PCBs were also compared to Residential Vapor Intrusion Soil

Screening Levels. The results of the metals analyses were also compared to the statewide

default background (SWDB) concentrations, as established by MDEQ.

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The soil analytical data is summarized in tables included in Appendix A and discussed in the

sections below.

7.1.1 Volatile Organic Compounds (VOCs)

No VOCs were detected above laboratory method detection limits (MDLs) in the soil samples

collected from GP-1 and GP-10. VOCs were detected in the remaining samples, but at

concentrations below Part 201 GRCC; except the following:

Contaminant Sample/Boring Location Criteria Exceeded

Benzene S-1 from GP-3 DWP GP-2, and S-1 and S-2 from GP-11 DWP and SVIIC

n-Butylbenzene S-1 from GP-11 DWP

Ethylbenzene S-2 from GP-11 DWP GP-2, GP-6 and S-1 from GP-11 DWP and GSIP

Naphthalene GP-2, S-3 from GP-5 and S-1 from GP-11 GSIP GP-6 DWP and GSIP

n-Propylbenzene S-1 from GP-11 DWP Toluene S-1 from GP-11 GSIP

Trichloroethylene GP-9 DWP 1,2,4-Trimthylbenzene GP-2, GP-6 and S-1 and S-2 from GP-11 DWP and GSIP 1,3,5-Trimthylbenzene GP-2 and S-1 from GP-11 DWP and GSIP

Xylenes S-1 from GP-3, GP-6 and S-2 from GP-11 GSIP GP-2 and S-1 from GP-11 DWP and GSIP

Additionally, the above contaminants plus sec-butylbenzene, cis-1,2-dichloroethylene,

isopropylbenzene and 1,2,3-trimthylbenzene in certain soil samples also exceed residential

vapor intrusion soil screening levels developed by MDEQ.

7.1.2 Polynuclear Aromatics (PNAs)

PNAs were not detected in the soil sample from GP-1 above laboratory MDLs. Certain PNAs

were detected in the remaining samples, but at concentrations below Part 201 GRCC; except

for the following:

Contaminant Sample/Boring Location Criteria Exceeded Acenaphthene GP-6 GSIP

Benzo(a)pyrene S-3 from GP-3, GP-4 and GP-6 DC Fluoranthene S-3 from GP-3, GP-4 and GP-6 GSIP

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Contaminant Sample/Boring Location Criteria Exceeded Fluorene GP-6 GSIP

2-Methylnaphthalene S-1 from GP-3, S_1 from GP-5 and S-1 from GP-11 GSIP

2-Methylnaphthalene GP-6 DWP and GSIP

Phenanthrene S-1 and S-3 from GP-3, GP-4, S-1 and S-3 from GP-5, GP-8 and GP-10 GSIP

Phenanthrene GP-6 DWP and GSIP

Additionally, 2-methylnaphthalene and phenanthrene in certain soil samples also exceeded

residential vapor intrusion soil screening levels.

7.1.3 Polychlorinated Biphenyls (PCBs)

PCBs were not detected in the soil samples from GP-1, S-1 from GP-3 and GP-4 above

laboratory MDLs.

7.1.4 Heavy Metals

Cadmium in the soil sample from GP-1, Mercury in soil samples GP-1 and S-1 from GP-11,

Selenium in soil samples GP-1, GP-7 and S-1 from GP-11, and Silver in soil samples GP-1,

GP-2, S-1 from GP-5, GP-7, GP-9, GP-10 and GP-11 were not detected above laboratory

MDLs.

Heavy metals were detected in the remaining soil samples at concentrations at or below

SWDB levels and/or Part 201 GRCC; except for the following:

Contaminant Sample/Boring Location

Criteria Exceeded

Arsenic S-3 from GP-3

DWP and GSIP GP-2, S-1 from GP-3, GP-4, S-1 and S-3 from GP-5,

GP-6, GP-8, GP-9, GP-10 and S-2 from GP-11

DWP, GSIP and DC

Chromium GP-2 and GP-6

GSIP S-3 from GP-5, GP-9 and GP-10 DWP and GSIP

Copper S-3 from GP-3, S-1 and S-3 from GP-5, GP-6, GP-7 and GP-8

GSIP

Lead GP-6

DC S-3 from GP-5

DWP and DC Mercury S-3 from GP-3, GP-4, GP-6, GP-9 and GP-10

GSIP

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Contaminant Sample/Boring Location

Criteria Exceeded

Selenium GP-2, S-1 from GP-3, GP-4, S-1 from GP-5, GP-8, GP-9 and GP-10 GSIP

Zinc S-3 from GP-3, GP-4, S-3 from GP-5, GP-6 and GP-8 GSIP

8.0 CONCLUSIONS

A visual survey, utility locating device and geoprobes confirmed the location of the 1,000-gallon

closed-in-place gasoline UST inside the building. This UST should be removed during the

demolition of the building.

Soil samples collected and analyzed from the geoprobe borings at the property identified

following contaminants above Part 201 GRCC:

Contaminant CAS Nos. Sample Location

Criteria Exceeded

Arsenic 7440382

S-3 from GP-3

DWP and GSIP GP-2, S-1 from GP-3, GP-4,

S-1 and S-3 from GP-5, GP-6, GP-8, GP-9, GP-10 and S-2

from GP-11

DWP, GSIP and DC

Chromium 7440473 GP-2 and GP-6 GSIP

S-3 from GP-5, GP-9 and GP-10 DWP and GSIP

Copper 7440508 S-3 from GP-3, S-1 and S-3 from GP-5, GP-6, GP-7 and

GP-8

GSIP

Lead 7439921 GP-6 DC S-3 from GP-5 DWP and DC

Mercury 7439976

S-3 from GP-3, GP-4, GP-6, GP-9 and GP-10

GSIP

Selenium 7782492

GP-2, S-1 from GP-3, GP-4, S-1 from GP-5, GP-8, GP-9

and GP-10

GSIP

Zinc 7440666

S-3 from GP-3, GP-4, S-3 from GP-5, GP-6 and GP-8

GSIP

Benzene 71432 S-1 from GP-3

DWP

GP-2, and S-1 and S-2 from GP-11

DWP and SVIIC

n-Butylbenzene 104518 S-1 from GP-11

DWP

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Contaminant CAS Nos. Sample Location

Criteria Exceeded

Ethylbenzene 100414 S-2 from GP-11 DWP

GP-2, GP-6 and S-1 from GP-11 DWP and GSIP

Naphthalene 91203 GP-2, S-3 from GP-5 and S-1

from GP-11 GSIP

GP-6 DWP and GSIP n-Propylbenzene 103651 S-1 from GP-11 DWP

Toluene 108883 S-1 from GP-11 GSIP Trichloroethylene 79016 GP-9 DWP

1,2,4-Trimethylbenzene 95636 GP-2, GP-6 and S-1 and S-2 from GP-11 DWP and GSIP

1,3,5-Trimethylbenzene 108678 GP-2 and S-1 from GP-11 DWP and GSIP

Xylenes 1330207 S-1 from GP-3, GP-6 and S-2

from GP-11 GSIP

GP-2 and S-1 from GP-11 DWP and GSIP Acenaphthene 83329 GP-6 GSIP

Benzo(a)pyrene 50328 S-3 from GP-3, GP-4 and GP-6 DC

Fluoranthene 206440 S-3 from GP-3, GP-4 and GP-6 GSIP

Fluorene 86737 GP-6 GSIP

2-Methylnaphthene 91576 S-1 from GP-3, S_1 from GP-

5 and S-1 from GP-11 GSIP

GP-6 DWP and GSIP

Phenanthrene 85018

S-1 and S-3 from GP-3, GP-4, S-1 and S-3 from GP-5, GP-8

and GP-10 GSIP

GP-6 DWP and GSIP

Based on the above analytical data, the property is a “facility” as defined by 1994 P.A. 451,

Part 201, as amended. According to Section 20101(1)(s) of Part 201 of NREPA (1994 P.A.

451,  as  amended),  "Facility”  means  any  area,  place,  or  property  where  a  hazardous  

substance in excess of the concentrations that satisfy the cleanup criteria for unrestricted

residential use has been released, deposited, disposed of, or otherwise comes to be located.

City of Detroit intends to acquire the property and redevelop it into a public park. Thus, as a

new owner, the City is recommended to submit a Baseline Environmental Assessment (BEA)

report to MDEQ, provided this report is prepared within 45 days of acquiring the property.

The BEA provides certain statutory protection to the new (non-liable) owners and operators of

the “facility” against existing subsurface contamination.

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Additionally, as part of continuous obligations under Part 201, Section 7a(1), a person who

owns or operates property that he/she has knowledge is a “facility” must do the following:

1. Prevent exacerbation of the existing contamination.

2. Prevent unacceptable human exposure and mitigate fire and explosion hazards to allow

for the intended use of the facility in a manner that protects the public health and safety.

3. Take reasonable precautions against the reasonably foreseeable acts or omissions of a

third party.

4. Provide reasonable cooperation, assistance, and access to the persons that are

authorized to conduct response activities at the property.

5. Comply with any land use or resource use restrictions established or relied on in

connection with the response activities.

6. Not impede the effectiveness or integrity of any land use or resource use restriction.

A Due Care Plan meeting above objectives is recommended for the property once the future

use and redevelopment plans are finalized. Furthermore, all future site redevelopment and

subsurface construction activities at the property should be monitored for evidence of

potential environmental concerns (such as discolored soil, soil with chemical odors or debris

materials). Such conditions, if encountered, will require further evaluation by NTH to

formulate an appropriate response. Any offsite relocation of soils would require proper

characterization prior to their removal from the property.

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Additionally, certain VOCs and PNAs were detected soil samples above Residential Vapor

Intrusion Soil Screening Levels. Thus, there is a potential risk from vapor intrusion into the

existing building or future buildings. Further evaluation comprising of soil-gas sampling and

analysis will be required based on the future use of the property.

9.0 LIMITATIONS

The evaluations and conclusions presented in this report have been made to assist the users of

this study in making a reasonable assessment of risk with respect to subsurface contamination

at the property from the RECs identified  during  NTH’s  Phase  I  ESA. Considering the limited

scope of the present investigation, data collection and testing, our findings should not be

construed as absolute certainties, but rather as probabilities based on our professional

judgment. NTH Consultants, Ltd. cannot offer any form of warranty or guarantee with respect

to the type and extent of hazardous substances on the property, other than those identified and

discussed in this report.

This report is intended for the exclusive use of The City of Detroit and/or its affiliates,

subsidiaries and authorized agents. This report presents NTH's opinion of the property as of

this date, based on the results of this study. The results of this study may not be relied upon by

parties other than those identified above without the prior knowledge and written consent of

NTH.

Page 264: Baseline Environmental Assessment for Riverside Park

APPENDIX ABORING LOCATION PLAN, FIGURE 1;LOG OF GEOPROBE BORINGS,

FIGURE 2; ANDSUMMARY OF CHEMICAL ANALYSES,

TABLE 1

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 1 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-1 N/A 0.0 – 1.0 FILL: DARK BROWN SAND WITH PIECES OF RAILROAD GRAVEL 0.0 1.0 <1

1.0 – 4.0 FILL: BROWN SAND S-1* 1.0 3.0 <1

3.0 4.0 <1

4.0 – 7.0 FILL: GRAY SAND 4.0 6.0 <1

S-2 6.0 7.0 <1

7.0 – 16.0 BROWN AND GRAY CLAY 7.0 9.0 <1

9.0 11.0 <1

11.0 13.0 <1

13.0 15.0 <1

15.0 16.0 <1

NO GROUNDWATER ENCOUNTERED

GP-2 N/A 0.0 – 2.0 CONCRETE FLOOR SLAB 0.0 2.0 ---

2.0 – 4.5 FILL: BROWN SAND 2.0 3.0 2.0

3.0 4.5 4.5

4.5 – 6.0 FILL: BLACK AND GRAY CLAY WITH PIECES OF SLAG (PETROLEUM ODOR) S-1* 4.5 6.0 99.0

6.0 – 9.5 FILL: BROWN AND GRAY CLAY 6.0 8.0 2.0

8.0 9.5 3.0

9.5 – 10.0 FILL: BLACK SAND WITH PIECES OF ROOFING MATERIAL S-2 9.5 10.0 2.0

10.0 – 17.0 BROWN CLAY 10.0 12.0 2.0

12.0 14.0 1.0

14.0 16.0 2.0

16.0 17.0 1.0

17.0 – 25.0 GRAY CLAY 17.0 19.0 <1

19.0 21.0 <1

21.0 23.0 <1

23.0 25.0 <1

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 2 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-3 N/A 0.0 – 0.5 CONCRETE FLOOR SLAB 0.0 0.5 ---

0.5 – 1.5 FILL: BLACK AND BROWN SAND WITH PIECES OF COAL AND BRICK S-1* 0.5 1.5 5.0

1.5 – 2.0 FILL: BROWN CLAY 1.5 2.0 <1

2.0 – 8.0 FILL: BLACK AND BROWN SAND WITH PIECES OF COAL AND PORCELAIN 2.0 4.0 <1

4.0 6.0 <1

S-2 6.0 8.0 <1

8.0 – 11.0 FILL: GRAY CLAY 8.0 10.0 <1

10.0 11.0 <1

11.0 – 12.5 FILL: BLACK SAND S-3* 11.0 12.5 <1

12.5 – 15.0 BROWN CLAY 12.5 14.0 <1

14.0 15.0 <1

NO GROUNDWATER ENCOUNTERED

GP-4 N/A 0.0 – 0.5 CONCRETE FLOOR SLAB 0.0 0.5 ---

0.5 – 5.0 FILL: BROWN SAND 0.5 2.0 2.0

2.0 3.0 4.0

3.0 5.0 5.0

5.0 – 11.5 FILL: BLACK AND GRAY CLAY WITH SAND SEAMS AND PIECES OF BRICK (PETROLEUM ODOR)

5.0 7.0 32.0

S-1* 7.0 9.0 44.0

9.0 10.0 12.0

S-2 10.0 11.5 24.0

11.5 – 20.0 BROWN CLAY 11.5 13.0 <1

13.0 15.0 <1

15.0 17.0 <1

17.0 19.0 <1

19.0 20.0 <1

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 3 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-5 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 3.0 FILL: BLACK SAND 0.5 2.0 <1

S-1* 2.0 3.0 <1

3.0 – 5.0 FILL: BROWN SAND WITH PIECES OF WOOD 3.0 4.0 <1

S-2 4.0 5.0 <1

5.0 – 8.0 FILL: BROWN AND GRAY CLAY 5.0 7.0 <1

7.0 8.0 <1

8.0 – 10.5 FILL: BLACK AND GRAY CLAY WITH SAND SEAMS AND PIECES OF WOOD (PETROLEUM ODOR)

8.0 9.0 6.0

S-3* 9.0 10.5 8.0

10.5 – 12.0 FILL: GRAY CLAY WITH PIECES OF WOOD 10.5 12.0 <1

REFUSAL AT 12 FEET / NO GROUNDWATER ENCOUNTERED

GP-6 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 3.5 FILL: BLACK AND BROWN SAND WITH PIECES OF BRICK S-1 0.5 2.0 2.0

2.0 3.5 1.0

3.5 – 7.0 FILL: GRAY CLAY WITH PIECES OF WOOD AND BRICK 3.5 5.0 <1

S-2 5.0 7.0 <1

7.0 – 10.5 FILL: BROWN CLAY 7.0 9.0 <1

9.0 10.5 <1

10.5 – 11.0 FILL: BLACK AND GRAY CLAY WITH SAND SEAMS AND PIECES OF BRICK (SOLVENT ODOR)

S-3* 10.5 11.0 10.0

11.0 – 16.0 BROWN AND GRAY CLAY 11.0 13.0 <1

13.0 15.0 <1

15.0 16.0 <1

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 4 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-7 N/A 0.0 – 0.5 ASPHALT PAVEMENT 0.0 0.5 ---

0.5 – 1.0 FILL: BROWN SAND 0.5 1.0 <1

1.0 – 4.0 FILL: GRAY CLAY WITH PIECES OF WOOD 1.0 3.0 <1

3.0 4.0 <1

4.0 – 7.0 FILL: BLACK AND GRAY SAND WITH PIECES OF WOOD 4.0 5.0 <1

S-1* 5.0 7.0 <1

7.0 – 10.5 FILL: GRAY CLAY WITH PIECES OF WOOD 7.0 9.0 <1

S-2 9.0 10.5 <1

10.5 – 16.0 BROWN AND GRAY CLAY 10.5 12.0 <1

12.0 14.0 <1

14.0 16.0 <1

NO GROUNDWATER ENCOUNTERED

GP-8 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 3.0 FILL: BLACK AND GRAY SAND WITH PIECES OF BRICK, COAL AND SLAG 0.5 2.0 3.0

S-1* 2.0 3.0 5.0

3.0 – 5.0 FILL: BROWN AND GRAY CLAY WITH PIECES OF WOOD 3.0 5.0 1.0

5.0 – 9.0 FILL: BLACK AND BROWN SAND WITH PIECES OF WOOD 5.0 7.0 3.0

S-2 7.0 9.0 <1

9.0 – 16.0 BROWN AND GRAY CLAY 9.0 11.0 <1

11.0 13.0 <1

13.0 15.0 <1

15.0 16.0 <1

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 5 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-9 N/A 0.0 – 0.5 TOPSOIL: BROWN SAND 0.0 0.5 <1

0.5 – 3.5 FILL: BLACK AND GRAY SAND WITH PIECES OF BRICK AND COAL 0.5 1.5 <1

S-1* 1.5 3.5 <1

3.5 – 7.5 FILL: BROWN CLAY 3.5 5.5 <1

5.5 7.5 <1

7.5 – 11.0 FILL: GRAY CLAY 7.5 9.0 <1

9.0 11.0 <1

11.0 – 12.0 FILL: GRAY CLAY WITH PIECES OF WOOD S-2 11.0 12.0 <1

12.0 – 16.0 BROWN CLAY 12.0 14.0 <1

14.0 16.0 <1

NO GROUNDWATER ENCOUNTERED

GP-10 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 5.0 FILL: BLACK AND GRAY CLAY WITH PIECES OF BRICK AND WOOD 0.5 2.0 <1

2.0 4.0 <1

S-1* 4.0 5.0 2.0

5.0 – 19.0 FILL: GRAY CLAY WITH PIECES OF WOOD 5.0 7.0 <1

7.0 9.0 <1

S-2 9.0 11.0 <1

11.0 13.0 <1

13.0 15.0 <1

15.0 17.0 <1

S-3 17.0 19.0 <1

19.0 – 25.0 BROWN CLAY 19.0 21.0 <1

21.0 23.0 <1

23.0 25.0 <1

25.0 – 28.0 GRAY CLAY 25.0 27.0 <1

27.0 28.0 <1

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

Page 271: Baseline Environmental Assessment for Riverside Park

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PROJECT NO: 62-140614-100A NTH CONSULTANTS, LTD. SHEET 6 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

GP-11 N/A 0.0 – 0.5 CONCRETE FLOOR SLAB 0.0 0.5 ---

0.5 – 5.5 FILL: BROWN SAND 0.5 2.0 <1

2.0 4.0 <1

4.0 5.5 212

5.5 – 7.0 FILL: GRAY SAND (PETROLEUM ODOR) S-1* 5.5 7.0 241

7.0 – 9.5 FILL: GRAY CLAY 7.0 8.0 54

S-2* 8.0 9.5 5.0

9.5 – 10.5 FILL: BLACK SAND 9.5 10.5 <1

10.5 – 15.0 BROWN CLAY 10.5 12.0 <1

12.0 14.0 <1

14.0 15.0 <1

NO GROUNDWATER ENCOUNTERED

P-1 N/A 0.0 – 1.0 CONCRETE FLOOR SLAB 0.0 1.0 ---

1.0 – 2.0 FILL: BROWN SAND 1.0 2.0 <1

2.0 REFUSAL

NO GROUNDWATER ENCOUNTERED

P-2 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 3.0 FILL: BLACK SAND 0.5 2.0 <1

2.0 3.0 <1

3.0 – 5.0 FILL: BROWN SAND WITH PIECES OF WOOD 3.0 4.0 <1

4.0 5.0 <1

5.0 – 8.0 FILL: BROWN AND GRAY CLAY 5.0 7.0 <1

7.0 8.0 <1

8.0 – 10.5 FILL: BLACK AND GRAY CLAY WITH SAND SEAMS AND WOOD (PETROLEUM ODOR) 8.0 9.0 6.0

9.0 10.5 8.0

10.5 – 12.0 FILL: GRAY CLAY WITH PIECES OF WOOD 10.5 12.0 <1

12.0 REFUSAL

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

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PROJECT NO: NTH CONSULTANTS, LTD. SHEET 7 OF 7

LOG OF GEOPROBE BORINGS

PROBE NO.

GROUND SURFACE

ELEV.

DEPTH (FT.) SOIL DESCRIPTION

DISCRETE SAMPLE INFO.

SAMPLE NO.

DEPTH (FT) PID READING

(PPM) FROM TO

P-3 N/A 0.0 – 0.5 FILL: BROWN SAND 0.0 0.5 <1

0.5 – 3.0 FILL: BLACK SAND 0.5 2.0 <1

2.0 3.0 <1

3.0 – 5.0 FILL: BROWN SAND WITH PIECES OF WOOD 3.0 4.0 <1

4.0 5.0 <1

5.0 – 8.0 FILL: BROWN AND GRAY CLAY 5.0 7.0 <1

7.0 8.0 <1

8.0 – 10.5 FILL: BLACK AND GRAY CLAY WITH SAND SEAMS AND WOOD (PETROLEUM ODOR) 8.0 9.0 6.0

9.0 10.5 8.0

10.5 – 12.0 FILL: GRAY CLAY WITH PIECES OF WOOD 10.5 12.0 <1

12.0 REFUSAL

NO GROUNDWATER ENCOUNTERED

NOTES:

[1] GEOPROBES BACKFILLED WITH SOIL CUTTINGS AND PATCHED WITH CONCRETE AS NECESSARY AFTER OBTAINING SOIL SAMPLES. [2] GEOPROBE DRILLING OBSERVED BY J. VEENKANT OF NTH CONSULTANTS, LTD. [3] SOIL CLASSIFICATION BASED SOLELY ON VISUAL OBSERVATION. [4] * - SAMPLE SUBMITTED FOR ANALYTICAL TESTING.

DRILLED BY: J. STROMBERGER AND R. MOORE OF FIBERTEC ENVIRONMENTAL SERVICES DATE: MAY 27-28, 2015 FIGURE NO: 2

Page 273: Baseline Environmental Assessment for Riverside Park

Tabl

e 1:

SU

MM

ARY

OF

CH

EMIC

AL A

NAL

YSES

- SO

IL38

01 W

est J

effe

rson

Pro

pert

yN

TH P

roje

ct N

o. 6

2-14

0614

-100

A

Mic

higa

n 10

Met

als

Vola

tile

Org

anic

Com

poun

ds

7440

-38-

274

40-3

9-3

7440

-43-

974

40-4

7-3

7440

-50-

874

39-9

2-1

7439

-97-

677

82-4

9-2

7440

-22-

474

40-6

6-6

71-4

3-2

104-

51-8

135-

98-8

156-

59-2

100-

41-4

98-8

2-8

91-2

0-3

103-

65-1

108-

88-3

79-0

1-6

526-

73-8

95-6

3-6

108-

67-8

1330

-20-

7V

ario

us

(1.0

' - 3

.0')

5/28

/201

51,

900

6,10

0<5

03,

500

3,10

02,

300

<50

<200

<100

8,70

0<5

0<5

8<5

8<5

0<5

0<2

90<3

30<1

00<5

0<5

8<1

00<1

20<1

00<1

50N

D

(4.5

' - 6

.0')

5/27

/201

512

,000

94,0

0030

020

,000

72,0

0062

,000

100

560

<100

120,

000

3,10

018

0<6

1<5

05,

000

<310

1,90

01,

000

1,40

0<6

12,

000

8,50

02,

300

24,0

00N

D

(0.5

' - 1

.5')

5/27

/201

518

,000

190,

000

500

10,0

0054

,000

220,

000

110

1,40

027

012

0,00

019

0<5

8<5

8<5

014

0<2

9059

0<1

001,

200

<58

140

260

<100

1,30

0N

D

(11.

0' -

12.5

')5/

27/2

015

6,40

068

,000

620

7,90

016

0,00

016

0,00

032

034

038

037

0,00

0<5

0<6

5<6

5<5

0<5

0<3

20<3

30<1

0062

<65

<100

<130

<100

<150

ND

(7.0

' - 9

.0')

5/27

/201

513

,000

110,

000

600

12,0

0034

,000

300,

000

180

810

100

530,

000

<50

160

450

<50

<50

500

<330

240

<50

<50

<100

420

<100

<150

ND

(2.0

' - 3

.0')

5/28

/201

515

,000

65,0

0049

06,

300

110,

000

58,0

0088

1,30

0<1

0011

0,00

0<5

0<6

0<6

0<5

0<5

0<3

00<3

30<1

0031

0<6

0<1

00<1

20<1

0046

0N

D

(9.0

' - 1

0.5'

)5/

28/2

015

11,0

0013

0,00

01,

000

33,0

0018

0,00

087

0,00

073

380

130

390,

000

<50

160

98<5

0<5

0<3

502,

500

<100

<50

<70

280

330

370

<150

ND

(10.

5' -

11.0

')5/

28/2

015

13,0

0021

0,00

057

022

,000

150,

000

530,

000

790

380

420

260,

000

6321

0<6

3<5

01,

500

<310

60,0

00<1

0015

0<6

373

02,

400

750

1,40

0N

D

(5.0

' - 7

.0')

5/28

/201

54,

000

28,0

0096

5,90

017

0,00

085

,000

120

<200

<100

46,0

00<5

0<6

0<6

0<5

0<5

0<3

00<3

30<1

0060

<60

<100

<120

<100

<150

ND

(2.0

' - 3

.0')

5/28

/201

514

,000

100,

000

1,60

018

,000

120,

000

140,

000

581,

700

200

210,

000

59<5

7<5

7<5

086

<280

410

<100

320

64<1

0017

0<1

0053

0N

D

(1.5

' - 3

.5')

5/28

/201

513

,000

97,0

0068

034

,000

45,0

0060

,000

220

1,00

0<1

0012

0,00

0<5

0<6

0<6

014

0<5

0<3

00<3

30<1

0018

061

0<1

00<1

20<1

0018

0N

D

(4.0

' - 5

.0')

5/28

/201

514

,000

93,0

0067

045

,000

57,0

0014

0,00

018

01,

500

<100

170,

000

<50

<63

<63

<50

<50

<310

<330

<100

<50

<63

<100

<130

<100

<150

ND

(5.5

' - 7

.0')

5/27

/201

51,

700

15,0

0073

5,20

07,

300

28,0

00<5

0<2

00<1

0018

,000

4,90

06,

400

890

<50

9,20

088

07,

400

3,30

014

,000

<62

12,0

0046

,000

23,0

0072

,000

ND

(8.0

' - 9

.5')

5/27

/201

58,

200

62,0

0015

018

,000

17,0

0015

,000

9033

0<1

0052

,000

1,70

035

015

0<5

037

0<3

0046

040

031

0<6

046

02,

400

640

1,10

0N

DS

WD

B5,

800

75,0

001,

200

18,0

0032

,000

21,0

0013

041

01,

000

47,0

00N

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AV

ario

usD

WP

4,60

01.

30E

+06

6,00

030

,000

5.80

E+0

67.

00E

+05

1,70

04,

000

4,50

02.

40E

+06

100

1,60

01,

600

1,40

01,

500

91,0

0035

,000

1,60

016

,000

100

NA

2,10

01,

800

5,60

0V

ario

usG

SIP

4,60

04.

40E

+05

3,00

03,

300

73,0

002.

50E

+06

5040

010

01.

70E

+05

4,00

0ID

ID12

,000

360

3,20

073

0ID

5,40

04,

000

NA

570

1,10

082

0V

ario

usS

VIIC

NLV

NLV

NLV

NLV

NLV

NLV

48,0

00N

LVN

LVN

LV1,

600

IDID

22,0

0087

,000

4.00

E+0

52.

50E

+05

ID3.

30E

+05

1,00

0N

A4.

30E

+06

2.60

E+0

66.

30E

+06

Var

ious

VS

ICN

LVN

LVN

LVN

LVN

LVN

LV52

,000

NLV

NLV

NLV

13,0

00ID

ID1.

80E

+05

7.20

E+0

51.

70E

+06

3.00

E+0

5ID

2.80

E+0

611

,000

NA

2.10

E+0

71.

60E

+07

4.60

E+0

7V

ario

usV

SIC

5M

NLV

NLV

NLV

NLV

NLV

NLV

52,0

00N

LVN

LVN

LV34

,000

IDID

4.20

E+0

51.

00E

+06

1.70

E+0

63.

00E

+05

ID5.

10E

+06

25,0

00N

A5.

00E

+08

3.80

E+0

86.

10E

+07

Var

ious

VS

IC 2

MN

LVN

LVN

LVN

LVN

LVN

LV52

,000

NLV

NLV

NLV

79,0

00ID

ID9.

90E

+05

2.20

E+0

62.

80E

+06

3.00

E+0

5ID

1.20

E+0

757

,000

NA

5.00

E+0

83.

80E

+08

1.30

E+0

8V

ario

usP

SIC

7.20

E+0

53.

30E

+08

1.70

E+0

62.

60E

+05

1.30

E+0

81.

00E

+08

2.00

E+0

71.

30E

+08

6.70

E+0

6ID

3.80

E+0

82.

00E

+09

4.00

E+0

82.

30E

+09

1.00

E+1

05.

80E

+09

2.00

E+0

81.

30E

+09

2.70

E+1

01.

30E

+08

NA

8.20

E+1

08.

20E

+10

2.90

E+1

1V

ario

usD

C7,

600

3.70

E+0

75.

50E

+05

2.50

E+0

62.

00E

+07

4.00

E+0

51.

60E

+05

2.60

E+0

62.

50E

+06

1.70

E+0

81.

80E

+05

2.50

E+0

62.

50E

+06

2.50

E+0

62.

20E

+07

2.50

E+0

71.

60E

+07

2.50

E+0

65.

00E

+07

1.10

E+0

5N

A3.

20E

+07

3.20

E+0

74.

10E

+08

Var

ious

SS

CS

LN

AN

AN

AN

AN

AN

AN

AN

AN

AN

A4.

00E

+05

1.00

E+0

71.

00E

+07

6.40

E+0

51.

40E

+05

3.90

E+0

5N

A1.

00E

+07

2.50

E+0

55.

00E

+05

NA

1.10

E+0

594

,000

1.50

E+0

5V

ario

us

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

5045

050

5019

825

044

314

110

,100

503,

180

2,20

01,

660

291

Var

ious

NOTE

S:[1]

Part

201 C

RITE

RIA

EFFE

CTIV

E DA

TE: D

ECEM

BER

30, 2

013

[2]SA

MPLE

S CO

LLEC

TED

BY N

TH C

ONSU

LTAN

TS P

ERSO

NNEL

AND

ANA

LYZE

D BY

FIB

ERTE

C EN

VIRO

NMEN

TAL S

ERVI

CES

OF H

OLT,

MIC

HIGA

N.[3]

ALL V

ALUE

S PR

ESEN

TED

AS µ

G/KG

- MI

CROG

RAMS

PER

KILO

GRAM

(§ P

ARTS

PER

BILL

ION)

.[4]

ID -

INAD

EQUA

TE D

ATA

TO D

EVEL

OP C

RITE

RION

/ NA

- CRI

TERI

A NO

T AV

AILA

BLE

[5]NL

V - C

HEMI

CAL I

S NO

T LIK

ELY

TO V

OLAT

ILIZE

UND

ER M

OST

COND

ITIO

NS[6]

ND -

NOT

DETE

CTED

ABO

VE LA

BORA

TORY

REP

ORTE

D ME

THOD

DET

ECTI

ON LI

MITS

[7]SW

DB -

STAT

E-W

IDE

DEFA

ULT

BACK

GROU

ND[8]

DWP

- RES

IDEN

TIAL

DRI

NKIN

G W

ATER

PRO

TECT

ION

CRIT

ERIA

[9]GS

IP -

GRO

UNDW

ATER

/ SUR

FACE

WAT

ER IN

TERF

ACE

PROT

ECTI

ON C

RITE

RIA

BASE

D ON

WAT

ER H

ARDN

ESS

OF 15

0mg C

aCO 3

/L.[10

]SV

IIC -

SOI

L VOL

ATILI

ZATI

ON T

O IN

DOOR

AIR

INHA

LATI

ON C

RITE

RIA.

[11]

VSIC

- V

OLAT

ILE S

OIL I

NHAL

ATIO

N CR

ITER

IA (

AMBI

ENT

AIR;

INFI

NITE

SOU

RCE)

.[12

]VS

IC 5M

- FI

NITE

VSI

C FO

R 5 M

ETER

SOU

RCE

THIC

KNES

S[13

]VS

IC 2M

- FI

NITE

VSI

C FO

R 2 M

ETER

SOU

RCE

THIC

KNES

S[14

]PS

IC -

PART

ICUL

ATE

SOIL

INHA

LATI

ON C

RITE

RIA

[15]

DC -

DIRE

CT C

ONTA

CT C

RITE

RIA

[16]

SSCS

L - S

OIL S

ATUR

ATIO

N CO

NCEN

TRAT

ION

SCRE

ENIN

G LE

VELS

[17]

- REP

ORTE

D CO

NCEN

TRAT

ION

EXCE

EDS

ONE

OR M

ORE

APPL

ICAB

LE P

ART

201 C

RITE

RIA

Benzene

1,3,5-Trimethylbenzene

Sample Designation

Sample Depth (ft)

Collect Date

1,2,4-Trimethylbenzene

n-Butylbenzene

Arsenic

Barium

Cadmium

Chromium, Total

Copper

Lead

Isopropylbenzene

Mercury, Total

Selenium

Silver

Zinc

n-Propylbenzene

Toluene

Trichloroethylene

1,2,3-Trimethylbenzene

Other Volatile Organic Compounds

Xylenes

sec-Butylbenzene

cis-1,2-Dichloroethylene

Ethylbenzene

Naphthalene

GP

-9 S

-1

GP

-1 S

-1

GP

-2 S

-1

GP

-3 S

-1

GP

-3 S

-3

GP

-4 S

-1

GP

-5 S

-1

GP

-5 S

-3

GP

-6 S

-3

GP

-7 S

-1

GP

-8 S

-1

GP

-10

S-1

G

P-1

1 S

-1

GP

-11

S-2

PA

RT

201

RE

SID

EN

TIA

L S

OIL

CLE

AN

UP

C

RIT

ER

IA

Res

iden

tial V

apor

Intru

sion

S

oil S

cree

ning

Lev

els

1 of

2

Page 274: Baseline Environmental Assessment for Riverside Park

Tabl

e 1:

SU

MM

ARY

OF

CH

EMIC

AL A

NAL

YSES

- SO

IL (C

ON

TIN

UED

)38

01 W

est J

effe

rson

Pro

pert

yN

TH P

roje

ct N

o. 6

2-14

0614

-100

A

PCB

s

83-3

2-9

208-

96-8

120-

12-7

56-5

5-3

50-3

2-8

205-

99-2

191-

24-2

207-

08-9

218-

01-9

53-7

0-3

206-

44-0

86-7

3-7

193-

39-5

91-5

7-6

85-0

1-8

129-

00-0

(1.0

' - 3

.0')

5/28

/201

5<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30N

D

(4.5

' - 6

.0')

5/27

/201

5<3

30<3

30<3

3057

050

061

040

0<3

3038

0<3

3064

0<3

3037

01,

800

550

750

---(0

.5' -

1.5

')5/

27/2

015

<330

<330

340

930

730

1,10

069

033

01,

200

<330

1,20

0<3

3055

05,

800

3,10

01,

500

ND

(11.

0' -

12.5

')5/

27/2

015

860

460

1,90

04,

100

4,20

04,

100

2,50

01,

400

4,40

055

07,

300

770

2,20

034

06,

500

10,0

00---

(7.0

' - 9

.0')

5/27

/201

51,

600

<330

3,30

04,

100

4,00

04,

900

2,40

01,

400

4,10

060

010

,000

2,10

02,

400

920

11,0

009,

700

ND

(2.0

' - 3

.0')

5/28

/201

5<3

30<3

3076

02,

300

1,90

02,

800

1,30

090

03,

100

390

4,10

061

01,

200

8,10

07,

000

4,60

0---

(9.0

' - 1

0.5'

)5/

28/2

015

1,20

0<3

301,

800

1,30

076

01,

000

440

<330

1,30

0<3

304,

200

1,80

044

02,

700

7,50

04,

100

---(1

0.5'

- 11

.0')

5/28

/201

557

,000

3,20

037

,000

18,0

0016

,000

12,0

007,

100

4,70

017

,000

1,70

034

,000

29,0

006,

200

74,0

0011

0,00

063

,000

---(5

.0' -

7.0

')5/

28/2

015

340

<330

<330

620

470

560

340

<330

410

<330

840

<330

<330

<330

760

1,10

0---

(2.0

' - 3

.0')

5/28

/201

5<3

30<3

3040

02,

800

3,50

02,

400

2,80

051

03,

500

780

2,20

0<3

301,

500

2,30

02,

500

4,70

0---

(1.5

' - 3

.5')

5/28

/201

5<3

30<3

3037

01,

100

870

1,40

036

044

01,

100

<330

2,10

0<3

3043

01,

000

1,80

01,

800

---(4

.0' -

5.0

')5/

28/2

015

<330

<330

660

1,70

01,

600

2,00

01,

000

670

1,60

0<3

303,

300

<330

1,00

0<3

302,

200

3,40

0---

(5.5

' - 7

.0')

5/27

/201

5<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

30<3

307,

600

<330

<330

---(8

.0' -

9.5

')5/

27/2

015

<330

<330

<330

<330

<330

<330

<330

<330

<330

<330

<330

<330

<330

740

<330

<330

---S

WD

BN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AD

WP

3.00

E+0

55,

900

41,0

00N

LLN

LLN

LLN

LLN

LLN

LLN

LL7.

30E

+05

3.90

E+0

5N

LL57

,000

56,0

004.

80E

+05

NLL

GS

IP8,

700

IDID

NLL

NLL

NLL

NLL

NLL

NLL

NLL

5,50

05,

300

NLL

4,20

02,

100

IDN

LLS

VIIC

1.90

E+0

81.

60E

+06

1.00

E+0

9N

LVN

LVID

NLV

NLV

IDN

LV1.

00E

+09

5.80

E+0

8N

LV2.

70E

+06

2.80

E+0

61.

00E

+09

3.00

E+0

6V

SIC

8.10

E+0

72.

20E

+06

1.40

E+0

9N

LVN

LVID

NLV

NLV

IDN

LV7.

40E

+08

1.30

E+0

8N

LV1.

50E

+06

1.60

E+0

56.

50E

+08

2.40

E+0

5V

SIC

5M

8.10

E+0

72.

20E

+06

1.40

E+0

9N

LVN

LVID

NLV

NLV

IDN

LV7.

40E

+08

1.30

E+0

8N

LV1.

50E

+06

1.60

E+0

56.

50E

+08

7.90

E+0

6V

SIC

2M

8.10

E+0

72.

20E

+06

1.40

E+0

9N

LVN

LVID

NLV

NLV

IDN

LV7.

40E

+08

1.30

E+0

8N

LV1.

50E

+06

1.60

E+0

56.

50E

+08

7.90

E+0

6P

SIC

1.40

E+1

02.

30E

+09

6.70

E+1

0ID

1.50

E+0

6ID

8.00

E+0

8ID

IDID

9.30

E+0

99.

30E

+09

ID6.

70E

+08

6.70

E+0

66.

70E

+09

5.20

E+0

6D

C4.

10E

+07

1.60

E+0

62.

30E

+08

20,0

002,

000

20,0

002.

50E

+06

2.00

E+0

52.

00E

+06

2,00

04.

60E

+07

2.70

E+0

720

,000

8.10

E+0

61.

60E

+06

2.90

E+0

71,

200

SS

CS

LN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

AN

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AN

A

4.32

E+0

51.

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+05

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7N

AN

AN

AN

AN

AN

AN

AN

A7.

09E

+05

NA

7,48

05,

140

6.47

E+0

71,

940

NOTE

S:[1]

PART

201 C

RITE

RIA

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CTIV

E DA

TE: D

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BER

30, 2

013

[2]SA

MPLE

S CO

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LYZE

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CES

OF H

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HIGA

N.[3]

ALL V

ALUE

S PR

ESEN

TED

AS µ

G/KG

- MI

CROG

RAMS

PER

KILO

GRAM

(§ P

ARTS

PER

BILL

ION)

.[4]

ID -

INAD

EQUA

TE D

ATA

TO D

EVEL

OP C

RITE

RION

/ NA

- CRI

TERI

A NO

T AV

AILA

BLE

[5]NL

V - C

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CAL I

S NO

T LIK

ELY

TO V

OLAT

ILIZE

UND

ER M

OST

COND

ITIO

NS[6]

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NOT

DETE

CTED

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VE LA

BORA

TORY

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ORTE

D ME

THOD

DET

ECTI

ON LI

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DB -

STAT

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IDE

DEFA

ULT

BACK

GROU

ND[8]

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G W

ATER

PRO

TECT

ION

CRIT

ERIA

[9]GS

IP -

GRO

UNDW

ATER

/ SUR

FACE

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ER IN

TERF

ACE

PROT

ECTI

ON C

RITE

RIA

BASE

D ON

A W

ATER

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S of

150m

g CaC

O 3/L.

[10]

SVIIC

- S

OIL V

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ILIZA

TION

TO

INDO

OR A

IR IN

HALA

TION

CRI

TERI

A.[11

]VS

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ATILE

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L INH

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ERIA

(AM

BIEN

T AI

R; IN

FINI

TE S

OURC

E).

[12]

VSIC

5M -

FINI

TE V

SIC

FOR

5 MET

ER S

OURC

E TH

ICKN

ESS

[13]

VSIC

2M -

FINI

TE V

SIC

FOR

2 MET

ER S

OURC

E TH

ICKN

ESS

[14]

PSIC

- PA

RTIC

ULAT

E SO

IL IN

HALA

TION

CRI

TERI

A[15

]DC

- DI

RECT

CON

TACT

CRI

TERI

A[16

]SS

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SOI

L SAT

URAT

ION

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ATIO

N SC

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ING

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]- R

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CONC

ENTR

ATIO

N EX

CEED

S ON

E OR

MOR

E AP

PLIC

ABLE

PAR

T 20

1 CRI

TERI

A

Sample Designation

Sample Depth (ft)

Collect Date

2-Methylnaphthalene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(g,h,i)perylene

Benzo(k)fluoranthene

Chrysene

Dibenzo(a,h)anthracene

GP

-7 S

-1

Fluoranthene

Fluorene

Indeno(1,2,3-cd)pyrene

Acenaphthene

Acenaphthylene

AnthraceneG

P-1

1 S

-1

Polychlorinated Biphenyls

GP

-1 S

-1

GP

-5 S

-1

GP

-5 S

-3

GP

-6 S

-3

Phenanthrene

Benzo(a)anthracene

Poly

nucl

ear A

rom

atic

s

Res

iden

tial V

apor

Intru

sion

S

oil S

cree

ning

Lev

els

Pyrene

GP

-2 S

-1

GP

-3 S

-1

GP

-3 S

-3

GP

-4 S

-1

GP

-10

S-1

GP

-8 S

-1

GP

-9 S

-1

GP

-11

S-2

PA

RT

201

RE

SID

EN

TIA

L S

OIL

CLE

AN

UP

C

RIT

ER

IA

2 of

2

Page 275: Baseline Environmental Assessment for Riverside Park

APPENDIX BLABORATORY DATA

Page 276: Baseline Environmental Assessment for Riverside Park

Thursday, June 04, 2015

62-140614-100A /62-140614-100AProject Identification:Fibertec Project Number: 68075

41780 Six Mile RoadNTH Consultants, Ltd. - Northville

Northville, MI 48168-3459

Mr. Cliff Andrews

Thank you for selecting Fibertec Environmental Services as your analytical laboratory. The samples you submitted have been analyzed in accordance with NELAC standards and the results compiled in the attached report. Any exceptions to NELAC compliance are noted in the report. These results apply only to those samples submitted. Please note TO-15 samples will be disposed of 14 days after the reporting date. All other samples will be disposed of 30 days after the reporting date.

Dear Mr. Andrews,

Submittal Date: 05/28/2015

If you have any questions regarding these results or if we may be of further assistance to you, please contact me at (517) 699-0345.

Sincerely,

Daryl P. Strandbergh Laboratory Director

Enclosures

DPS/arp

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 277: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-001

Analytical Laboratory Report 680752 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-2 S-1 (4.5-6.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 09:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

%1. 18 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

µg/kg1. 12000 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 94000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 300 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 20000 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 72000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 62000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. 560 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. U 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 120000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

µg/kg1. 100 50 8.9 06/01/15 PM15F01C 06/02/15 M615F02AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-001A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. 3100 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 278: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-001

Analytical Laboratory Report 680753 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-2 S-1 (4.5-6.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 09:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-001A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

E1 µg/kg10. 180 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

µg/kg11. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. 5000 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

µg/kg38. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. 1900 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. 1000 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 279: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-001

Analytical Laboratory Report 680754 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-2 S-1 (4.5-6.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 09:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-001A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

µg/kg47. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. 1400 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 61 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. 2000 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 8500 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. 2300 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. 23000 610 10 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. 840 610 10 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. 24000 1200 10 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-2 S-1 (4.5-6.0)

µg/kg1. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 570 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 500 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 610 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 400 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 380 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 640 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 370 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 1800 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 550 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 750 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 280: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-003

Analytical Laboratory Report 680755 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-1 (0.5-1.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

%1. 13 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg1. 18000 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 190000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 500 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 10000 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 54000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 220000 1000 40 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. 1400 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. 270 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 120000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg1. 110 50 9.1 06/01/15 PM15F01C 06/02/15 M615F02AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polychlorinated Biphenyls (PCBs) (EPA 3546/EPA 8082A) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg1. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1016 PM

µg/kg2. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1221 PM

µg/kg3. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1232 PM

µg/kg4. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1242 PM

µg/kg5. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1248 PM

µg/kg6. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1254 PM

µg/kg7. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1260 PM

µg/kg8. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1262‡ PM

µg/kg9. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1268‡ PM

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 281: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-003

Analytical Laboratory Report 680756 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-1 (0.5-1.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-003A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

V- µg/kg1. U 1000 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcrylonitrile‡ DAR

µg/kg3. 190 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Butanone DAR

µg/kg10. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Butylbenzene DAR

µg/kg11. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Asec-Butylbenzene DAR

µg/kg12. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atert-Butylbenzene DAR

L+ µg/kg13. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Disulfide DAR

µg/kg14. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Tetrachloride DAR

µg/kg15. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChlorobenzene DAR

µg/kg16. U 290 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroform DAR

µg/kg18. U 290 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromochloromethane DAR

µg/kg21. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,4-Dichlorobenzene DAR

L+ µg/kg26. U 290 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,2-Dichloroethene DAR

µg/kg32. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloropropane DAR

µg/kg33. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,3-Dichloropropene DAR

µg/kg34. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,3-Dichloropropene DAR

µg/kg35. 140 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylbenzene DAR

µg/kg36. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Hexanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 282: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-003

Analytical Laboratory Report 680757 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-1 (0.5-1.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-003A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg38. U 290 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMTBE DAR

µg/kg42. 590 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ANaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Propylbenzene DAR

µg/kg44. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2,2-Tetrachloroethane DAR

µg/kg47. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATetrachloroethene DAR

µg/kg48. 1200 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1-Trichloroethane DAR

µg/kg51. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2-Trichloroethane‡ DAR

µg/kg52. U 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trichloropropane DAR

µg/kg55. 140 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 260 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AVinyl Chloride DAR

µg/kg59. 860 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Am&p-Xylene DAR

µg/kg60. 430 58 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Ao-Xylene DAR

µg/kg61. 1300 150 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg1. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 340 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 930 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 730 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 1100 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 690 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 283: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-003

Analytical Laboratory Report 680758 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-1 (0.5-1.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-1 (0.5-1.5)

µg/kg8. 330 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 1200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 1200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 550 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 5800 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 3100 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 1500 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 284: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-005

Analytical Laboratory Report 680759 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-3 (11.0-12.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

%1. 23 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

µg/kg1. 6400 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 68000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 620 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 7900 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 160000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 160000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. 340 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. 380 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 370000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

µg/kg1. 320 50 9.3 06/01/15 PM15F01C 06/02/15 M615F02AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

V- µg/kg1. U 1000 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcetone DAR

µg/kg2. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromodichloromethane DAR

µg/kg7. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 285: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-005

Analytical Laboratory Report 6807510 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-3 (11.0-12.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

µg/kg10. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Butylbenzene DAR

µg/kg11. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Asec-Butylbenzene DAR

µg/kg12. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atert-Butylbenzene DAR

L+ µg/kg13. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Disulfide DAR

µg/kg14. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Tetrachloride DAR

µg/kg15. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChlorobenzene DAR

µg/kg16. U 320 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroform DAR

µg/kg18. U 320 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Chlorotoluene DAR

µg/kg20. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromochloromethane DAR

µg/kg21. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,4-Dichlorobenzene DAR

L+ µg/kg26. U 320 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,2-Dichloroethene DAR

µg/kg32. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloropropane DAR

µg/kg33. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,3-Dichloropropene DAR

µg/kg34. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylbenzene DAR

µg/kg36. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Hexanone DAR

µg/kg38. U 320 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMTBE DAR

µg/kg42. U 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ANaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Propylbenzene DAR

µg/kg44. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AStyrene DAR

µg/kg45. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 286: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-005

Analytical Laboratory Report 6807511 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-3 S-3 (11.0-12.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 10:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

µg/kg47. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATetrachloroethene DAR

µg/kg48. 62 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1-Trichloroethane DAR

µg/kg51. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2-Trichloroethane‡ DAR

µg/kg52. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichlorofluoromethane DAR

µg/kg54. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 130 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AVinyl Chloride DAR

µg/kg59. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Am&p-Xylene DAR

µg/kg60. U 65 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Ao-Xylene DAR

µg/kg61. U 150 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-3 S-3 (11.0-12.5)

µg/kg1. 860 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. 460 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 1900 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 4100 340 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 4200 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 4100 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 2500 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. 1400 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 4400 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. 550 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 7300 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. 770 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 2200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 340 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 6500 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 10000 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 287: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-006

Analytical Laboratory Report 6807512 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-4 S-1 (7.0-9.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 14:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

%1. 21 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg1. 13000 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 110000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 600 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 12000 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 34000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 300000 1000 100 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. 810 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. 100 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 530000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg1. 180 50 8.9 06/01/15 PM15F01C 06/02/15 M615F02AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polychlorinated Biphenyls (PCBs) (EPA 3546/EPA 8082A) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg1. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1016 PM

µg/kg2. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1221 PM

µg/kg3. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1232 PM

µg/kg4. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1242 PM

µg/kg5. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1248 PM

µg/kg6. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1254 PM

µg/kg7. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1260 PM

µg/kg8. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1262‡ PM

µg/kg9. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1268‡ PM

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 288: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-006

Analytical Laboratory Report 6807513 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-4 S-1 (7.0-9.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 14:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-006A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg1. U 1000 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BAcetone DAR

µg/kg2. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBenzene DAR

µg/kg4. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBromobenzene DAR

µg/kg5. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBromochloromethane DAR

µg/kg6. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBromodichloromethane DAR

µg/kg7. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBromoform DAR

µg/kg8. U 200 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BBromomethane DAR

µg/kg9. U 750 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B2-Butanone DAR

µg/kg10. 160 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bn-Butylbenzene DAR

E1 µg/kg11. 450 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bsec-Butylbenzene DAR

µg/kg12. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BCarbon Disulfide DAR

µg/kg14. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BCarbon Tetrachloride DAR

µg/kg15. U 63 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BChlorobenzene DAR

µg/kg16. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BChloroethane DAR

µg/kg17. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BChloroform DAR

µg/kg18. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BChloromethane DAR

µg/kg19. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B2-Chlorotoluene DAR

µg/kg20. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BDibromochloromethane DAR

µg/kg21. U 32 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BDibromomethane DAR

µg/kg23. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,4-Dichlorobenzene DAR

µg/kg26. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1-Dichloroethane DAR

µg/kg28. U 63 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Btrans-1,2-Dichloroethene DAR

µg/kg32. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2-Dichloropropane DAR

µg/kg33. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bcis-1,3-Dichloropropene DAR

µg/kg34. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BEthylbenzene DAR

µg/kg36. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B2-Hexanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 289: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-006

Analytical Laboratory Report 6807514 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-4 S-1 (7.0-9.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 14:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-006A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg38. 500 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BIsopropylbenzene DAR

µg/kg39. U 130 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BMethylene Chloride DAR

µg/kg40. U 2500 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BMTBE DAR

µg/kg42. U 330 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BNaphthalene DAR

µg/kg43. 240 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bn-Propylbenzene DAR

µg/kg44. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BStyrene DAR

µg/kg45. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 63 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1,2,2-Tetrachloroethane DAR

µg/kg47. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BTetrachloroethene DAR

µg/kg48. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BToluene DAR

µg/kg49. U 330 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1,1-Trichloroethane DAR

µg/kg51. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BTrichloroethene DAR

µg/kg53. U 130 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BTrichlorofluoromethane DAR

µg/kg54. U 130 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 420 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BVinyl Chloride DAR

µg/kg59. U 100 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bm&p-Xylene DAR

µg/kg60. U 50 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28Bo-Xylene DAR

µg/kg61. U 150 1.0 05/28/15 VJ15E28B 05/29/15 VJ15E28BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg1. 1600 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 3300 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 4100 340 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 4000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 4900 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 2400 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 290: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-006

Analytical Laboratory Report 6807515 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-4 S-1 (7.0-9.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 14:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-006

P. Date P. Batch A. Date A. Batch Init.

Description: GP-4 S-1 (7.0-9.0)

µg/kg8. 1400 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 4100 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. 600 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 10000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. 2100 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 2400 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 920 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 11000 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 9700 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 291: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-008

Analytical Laboratory Report 6807516 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-1 (5.5-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

%1. 19 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

µg/kg1. 1700 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 15000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 73 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 5200 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 7300 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 28000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. U 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. U 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 18000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

µg/kg1. U 50 8.8 06/03/15 PM15F03B 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. 4900 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 292: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-008

Analytical Laboratory Report 6807517 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-1 (5.5-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

E1 µg/kg10. 6400 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

E1 µg/kg11. 890 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. 9200 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

µg/kg38. 880 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. 7400 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. 3300 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 293: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-008

Analytical Laboratory Report 6807518 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-1 (5.5-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

µg/kg47. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. 14000 310 10 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 62 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. 12000 310 10 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 46000 1200 10 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. 23000 620 10 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. 50000 620 10 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. 23000 620 10 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. 72000 1200 10 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-1 (5.5-7.0)

µg/kg1. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthene RDK

µg/kg2. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthylene RDK

µg/kg3. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAnthracene RDK

µg/kg4. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)anthracene RDK

µg/kg5. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)pyrene RDK

µg/kg6. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(b)fluoranthene RDK

µg/kg7. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(ghi)perylene RDK

µg/kg8. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(k)fluoranthene RDK

µg/kg9. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AChrysene RDK

µg/kg10. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ADibenzo(a,h)anthracene RDK

µg/kg11. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluoranthene RDK

µg/kg12. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluorene RDK

µg/kg13. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AIndeno(1,2,3-cd)pyrene RDK

µg/kg14. 7600 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02A2-Methylnaphthalene RDK

µg/kg15. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APhenanthrene RDK

µg/kg16. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APyrene RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 294: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-009

Analytical Laboratory Report 6807519 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-2 (8.0-9.5)

Sample No: S-2

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68075-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

%1. 17 0.1 1.0 06/01/15 MC150601 06/02/15 MC150601Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68075-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

µg/kg1. 8200 100 20 06/02/15 PT15F02B 06/02/15 T415F02AArsenic JLP

µg/kg2. 62000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ABarium JLP

µg/kg3. 150 50 20 06/02/15 PT15F02B 06/02/15 T415F02ACadmium JLP

µg/kg4. 18000 500 20 06/02/15 PT15F02B 06/02/15 T415F02AChromium JLP

µg/kg5. 17000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ACopper JLP

µg/kg6. 15000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02ALead JLP

µg/kg7. 330 200 20 06/02/15 PT15F02B 06/02/15 T415F02ASelenium JLP

µg/kg8. U 100 20 06/02/15 PT15F02B 06/02/15 T415F02ASilver JLP

µg/kg9. 52000 1000 20 06/02/15 PT15F02B 06/02/15 T415F02AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68075-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

µg/kg1. 90 50 9.0 06/03/15 PM15F03B 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

V- µg/kg1. U 1000 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AAcrylonitrile‡ DAR

µg/kg3. 1700 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ABromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 295: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-009

Analytical Laboratory Report 6807520 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-2 (8.0-9.5)

Sample No: S-2

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

E1 µg/kg10. 350 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Butylbenzene DAR

E1 µg/kg11. 150 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Asec-Butylbenzene DAR

µg/kg12. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atert-Butylbenzene DAR

L+ µg/kg13. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Disulfide DAR

µg/kg14. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ACarbon Tetrachloride DAR

µg/kg15. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChlorobenzene DAR

µg/kg16. U 300 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloroform DAR

µg/kg18. U 300 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromochloromethane DAR

µg/kg21. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,4-Dichlorobenzene DAR

L+ µg/kg26. U 300 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ADichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,2-Dichloroethene DAR

µg/kg32. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2-Dichloropropane DAR

µg/kg33. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Acis-1,3-Dichloropropene DAR

µg/kg34. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Atrans-1,3-Dichloropropene DAR

µg/kg35. 370 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylbenzene DAR

µg/kg36. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A2-Hexanone DAR

µg/kg38. U 300 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AMTBE DAR

µg/kg42. 460 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ANaphthalene DAR

µg/kg43. 400 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02An-Propylbenzene DAR

µg/kg44. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 296: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68075-009

Analytical Laboratory Report 6807521 of 22

Order:Page:Date: 06/04/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-11 S-2 (8.0-9.5)

Sample No: S-2

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141396

Collect Time: 16:00

Laboratory Project Number: 68075

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/27/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68075-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

µg/kg47. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATetrachloroethene DAR

µg/kg48. 310 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,1-Trichloroethane DAR

µg/kg51. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,1,2-Trichloroethane‡ DAR

µg/kg52. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02ATrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trichloropropane DAR

µg/kg55. 460 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 2400 120 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,2,4-Trimethylbenzene DAR

µg/kg57. 640 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02A1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AVinyl Chloride DAR

µg/kg59. 1100 100 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Am&p-Xylene DAR

µg/kg60. U 60 1.0 06/02/15 VH15F02A 06/02/15 VH15F02Ao-Xylene DAR

µg/kg61. 1100 150 1.0 06/02/15 VH15F02A 06/02/15 VH15F02AXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68075-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-11 S-2 (8.0-9.5)

µg/kg1. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthene RDK

µg/kg2. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthylene RDK

µg/kg3. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAnthracene RDK

µg/kg4. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)anthracene RDK

µg/kg5. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)pyrene RDK

µg/kg6. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(b)fluoranthene RDK

µg/kg7. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(ghi)perylene RDK

µg/kg8. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(k)fluoranthene RDK

µg/kg9. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AChrysene RDK

µg/kg10. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ADibenzo(a,h)anthracene RDK

µg/kg11. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluoranthene RDK

µg/kg12. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluorene RDK

µg/kg13. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AIndeno(1,2,3-cd)pyrene RDK

µg/kg14. 740 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02A2-Methylnaphthalene RDK

µg/kg15. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APhenanthrene RDK

µg/kg16. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APyrene RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 297: Baseline Environmental Assessment for Riverside Park

Spike recovery or precision unusable due to dilution.

Definitions/ Qualifiers:

The analyte was detected in the associated method blank.The analyte was detected at a concentration greater than the calibration range, therefore the result is estimated.The concentration is an estimated value.

The analyte was not detected at or above the reporting limit.Matrix Interference has resulted in a raised reporting limit or distorted result.Results reported on a wet-weight basis.Value reported is outside QA limits

A:B:E:J:

U:X:W:*:

Analytical Laboratory Report 6807522 of 22

Order:Page:Date: 06/04/15

Laboratory Project Number: 68075

Exception Summary:

Modified MethodM:

The reported value is estimated due to the presence of interference.E1 :Recovery in the associated laboratory sample (LCS) exceeds the upper control limit. Results may be biased high.L+ :Recovery in the associated continuing calibration verification sample (CCV) exceeds the lower control limit. Results may be biased low.

V- :

T104704518-15-3 (TX)Accreditation Number(s):

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68075-150604165325

Page 298: Baseline Environmental Assessment for Riverside Park

Cold Vapor Atomic Absorption Spectrometry

Quality Control Report

PM15F01CPreparation Batch: 06/01/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PM15F01C1 of 1

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Mercury U 50 194 200 97 85 - 115 MB-4 LCS-4

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:50 PM

MB-4 06/02/15 13:20M615F02ALCS-4 06/02/15 13:22M615F02A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PM15F01C-150604165621

Page 299: Baseline Environmental Assessment for Riverside Park

Cold Vapor Atomic Absorption Spectrometry

Quality Control Report

PM15F03BPreparation Batch: 06/03/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PM15F03B1 of 1

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Mercury U 50 203 200 102 85 - 115 MB-8 LCS-8

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:50 PM

MB-8 06/04/15 12:18M615F04ALCS-8 06/04/15 12:20M615F04A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PM15F03B-150604165621

Page 300: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F02A1 of 1

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acenaphthene U 330 4,025 5,333 75 50 - 114 MB-5 LCS-5.2 Acenaphthylene U 330 4,050 5,333 76 53 - 115 MB-5 LCS-5.3 Anthracene U 330 3,862 5,333 72 48 - 119 MB-5 LCS-5.4 Benzo(a)anthracene U 330 4,152 5,333 78 56 - 120 MB-5 LCS-5.5 Benzo(a)pyrene U 330 4,321 5,333 81 57 - 122 MB-5 LCS-5.6 Benzo(b)fluoranthene U 330 4,274 5,333 80 50 - 131 MB-5 LCS-5.7 Benzo(ghi)perylene U 330 4,107 5,333 77 41 - 132 MB-5 LCS-5.8 Benzo(k)fluoranthene U 330 4,321 5,333 81 39 - 137 MB-5 LCS-5.9 Chrysene U 330 4,360 5,333 82 53 - 124 MB-5 LCS-5.10 Dibenzo(a,h)anthracene U 330 4,265 5,333 80 53 - 126 MB-5 LCS-5.11 Fluoranthene U 330 4,473 5,333 84 48 - 135 MB-5 LCS-5.12 Fluorene U 330 4,195 5,333 79 49 - 126 MB-5 LCS-5.13 Indeno(1,2,3-cd)pyrene U 330 4,402 5,333 83 51 - 132 MB-5 LCS-5.14 2-Methylnaphthalene U 330 3,744 5,333 70 46 - 105 MB-5 LCS-5.15 Phenanthrene U 330 3,939 5,333 74 53 - 119 MB-5 LCS-5.16 Pyrene U 330 4,024 5,333 75 55 - 127 MB-5 LCS-5

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 2-Fluorobiphenyl(S) 4,048 3,951 5,333 74 49 - 1155,333 76 MB-5 LCS-5.2 4-Terphenyl-d14(S) 4,488 4,432 5,333 83 48 - 1175,333 84 MB-5 LCS-5.3 1-Fluoronaphthalene(S) 4,164 4,087 5,333 77 46 - 1145,333 78 MB-5 LCS-5

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:50 PM

MB-5 06/02/15 13:35S115F02ALCS-5 06/02/15 14:23S115F02A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F02A-150604165621

Page 301: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F02A1 of 1

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Aroclor-1016 U 100 1,056 1,333 79 60 - 122 MB-6 LCS-6.2 Aroclor-1260 U 100 1,102 1,333 83 70 - 131 MB-6 LCS-6

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Decachlorobiphenyl-PCB(S) 50.6 54.8 66.7 82 40 - 14366.7 76 MB-6 LCS-6.2 2,4,5,6-Tetrachloro-m-xylene-PCB(S) 49.3 48.8 66.7 73 42 - 13366.7 74 MB-6 LCS-6

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:50 PM

MB-6 06/02/15 14:10SA15F02BLCS-6 06/02/15 14:29SA15F02B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F02A-150604165621

Page 302: Baseline Environmental Assessment for Riverside Park

Inductively Coupled Plasma - Mass Spectrometry

Quality Control Report

PT15F02BPreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PT15F02B1 of 1

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Arsenic U 100 9,827 10,000 98 85 - 115 MB-2 LCS-2.2 Barium U 1000 44,650 50,000 89 85 - 115 MB-2 LCS-2.3 Cadmium U 50 9,616 10,000 96 85 - 115 MB-2 LCS-2.4 Chromium U 500 18,683 20,000 93 85 - 115 MB-2 LCS-2.5 Copper U 1000 20,382 20,000 102 85 - 115 MB-2 LCS-2.6 Lead U 1000 18,409 20,000 92 85 - 115 MB-2 LCS-2.7 Selenium U 200 9,594 10,000 96 85 - 115 MB-2 LCS-2.8 Silver U 100 9,392 10,000 94 85 - 115 MB-2 LCS-2.9 Zinc U 1000 48,242 50,000 96 85 - 115 MB-2 LCS-2

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:50 PM

MB-2 06/02/15 09:29T415F02ALCS-2 06/02/15 09:33T415F02A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PT15F02B-150604165621

Page 303: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02A1 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acetone U 1000 3,810 5,000 76 70 - 150 2082 8 MB-3 LCS-3 LCD-2.2 Acrylonitrile U 100 5,777 5,000 116 70 - 134 20116 0 MB-3 LCS-3 LCD-2.3 Benzene U 50 5,176 5,000 104 70 - 134 2099 5 MB-3 LCS-3 LCD-2.4 Bromobenzene U 100 5,178 5,000 104 70 - 134 20100 4 MB-3 LCS-3 LCD-2.5 Bromochloromethane U 100 5,426 5,000 109 70 - 134 20105 4 MB-3 LCS-3 LCD-2.6 Bromodichloromethane U 100 5,770 5,000 115 70 - 134 20111 4 MB-3 LCS-3 LCD-2.7 Bromoform U 100 4,583 5,000 92 70 - 134 2090 2 MB-3 LCS-3 LCD-2.8 Bromomethane U 200 6,115 5,000 122 70 - 134 20118 3 MB-3 LCS-3 LCD-2.9 2-Butanone U 750 5,453 5,000 109 70 - 150 20105 4 MB-3 LCS-3 LCD-2.10 n-Butylbenzene U 50 4,909 5,000 98 70 - 134 2093 5 MB-3 LCS-3 LCD-2.11 sec-Butylbenzene U 50 5,064 5,000 101 70 - 134 2096 5 MB-3 LCS-3 LCD-2.12 tert-Butylbenzene U 50 5,008 5,000 100 70 - 134 2095 5 MB-3 LCS-3 LCD-2.13 Carbon Disulfide U 250 7,655 5,000 153 70 - 134 * 20142 7 MB-3 LCS-3 LCD-2.14 Carbon Tetrachloride U 50 5,751 5,000 115 70 - 134 20108 6 MB-3 LCS-3 LCD-2.15 Chlorobenzene U 50 4,890 5,000 98 70 - 134 2094 4 MB-3 LCS-3 LCD-2.16 Chloroethane U 250 5,406 5,000 108 70 - 134 20100 8 MB-3 LCS-3 LCD-2.17 Chloroform U 50 5,218 5,000 104 75 - 134 20100 4 MB-3 LCS-3 LCD-2.18 Chloromethane U 250 6,117 5,000 122 70 - 134 20118 3 MB-3 LCS-3 LCD-2.19 2-Chlorotoluene U 50 5,077 5,000 102 70 - 134 2093 9 MB-3 LCS-3 LCD-2.20 Dibromochloromethane U 100 4,983 5,000 100 70 - 134 2097 3 MB-3 LCS-3 LCD-2.21 1,2-Dibromo-3-chloropropane U 50 4,853 5,000 97 70 - 134 2097 0 MB-3 LCS-3 LCD-2.22 Dibromomethane U 250 5,358 5,000 107 70 - 134 20106 1 MB-3 LCS-3 LCD-2.23 1,2-Dichlorobenzene U 100 4,830 5,000 97 70 - 134 2093 4 MB-3 LCS-3 LCD-2.24 1,3-Dichlorobenzene U 100 4,805 5,000 96 70 - 134 2092 4 MB-3 LCS-3 LCD-2.25 1,4-Dichlorobenzene U 100 4,410 5,000 88 70 - 134 2085 3 MB-3 LCS-3 LCD-2.26 Dichlorodifluoromethane U 250 8,004 5,000 160 70 - 134 * 20151 6 MB-3 LCS-3 LCD-2.27 1,1-Dichloroethane U 50 5,053 5,000 101 70 - 134 2097 4 MB-3 LCS-3 LCD-2.28 1,2-Dichloroethane U 50 5,028 5,000 101 70 - 134 2099 2 MB-3 LCS-3 LCD-2.29 1,1-Dichloroethene U 50 5,736 5,000 115 75 - 134 20106 8 MB-3 LCS-3 LCD-2.30 cis-1,2-Dichloroethene U 50 5,219 5,000 104 70 - 134 20101 3 MB-3 LCS-3 LCD-2.31 trans-1,2-Dichloroethene U 50 5,407 5,000 108 70 - 134 20102 6 MB-3 LCS-3 LCD-2.32 1,2-Dichloropropane U 50 5,111 5,000 102 75 - 134 2098 4 MB-3 LCS-3 LCD-2.33 cis-1,3-Dichloropropene U 50 4,615 5,000 92 70 - 134 2089 3 MB-3 LCS-3 LCD-2.34 trans-1,3-Dichloropropene U 50 4,719 5,000 94 70 - 134 2092 2 MB-3 LCS-3 LCD-2.35 Ethylbenzene U 50 5,339 5,000 107 75 - 134 20102 5 MB-3 LCS-3 LCD-2.36 Ethylene Dibromide U 50 5,433 5,000 109 70 - 134 20107 2 MB-3 LCS-3 LCD-2.37 2-Hexanone U 2500 4,249 5,000 85 70 - 150 2087 2 MB-3 LCS-3 LCD-2.38 Isopropylbenzene U 250 5,179 5,000 104 70 - 134 2099 5 MB-3 LCS-3 LCD-2.39 Methylene Chloride U 100 4,896 5,000 98 70 - 134 2094 4 MB-3 LCS-3 LCD-2.40 4-Methyl-2-pentanone U 2500 5,119 5,000 102 70 - 134 20103 1 MB-3 LCS-3 LCD-2.41 MTBE U 250 4,203 5,000 84 70 - 134 2085 1 MB-3 LCS-3 LCD-2.42 Naphthalene U 330 5,003 5,000 100 70 - 134 20100 0 MB-3 LCS-3 LCD-2.43 n-Propylbenzene U 100 5,145 5,000 103 70 - 134 2097 6 MB-3 LCS-3 LCD-2.44 Styrene U 50 5,533 5,000 111 70 - 134 20107 4 MB-3 LCS-3 LCD-2.45 1,1,1,2-Tetrachloroethane U 100 5,429 5,000 109 70 - 134 20104 5 MB-3 LCS-3 LCD-2.46 1,1,2,2-Tetrachloroethane U 50 5,340 5,000 107 70 - 134 2095 12 MB-3 LCS-3 LCD-2.47 Tetrachloroethene U 50 4,914 5,000 98 70 - 134 2094 4 MB-3 LCS-3 LCD-2.48 Toluene U 50 5,072 5,000 101 75 - 134 2098 3 MB-3 LCS-3 LCD-2.49 1,2,4-Trichlorobenzene U 330 4,176 5,000 84 70 - 134 2081 4 MB-3 LCS-3 LCD-2.50 1,1,1-Trichloroethane U 50 5,258 5,000 105 70 - 134 20100 5 MB-3 LCS-3 LCD-2.51 1,1,2-Trichloroethane U 50 5,088 5,000 102 70 - 134 2098 4 MB-3 LCS-3 LCD-2

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02A-150604165621

Page 304: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02A2 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.52 Trichloroethene U 50 5,316 5,000 106 70 - 134 20102 4 MB-3 LCS-3 LCD-2.53 Trichlorofluoromethane U 100 6,182 5,000 124 70 - 134 20117 6 MB-3 LCS-3 LCD-2.54 1,2,3-Trichloropropane U 100 5,131 5,000 103 70 - 134 20102 1 MB-3 LCS-3 LCD-2.55 1,2,3-Trimethylbenzene U 100 4,856 5,000 97 70 - 134 2093 4 MB-3 LCS-3 LCD-2.56 1,2,4-Trimethylbenzene U 100 5,155 5,000 103 70 - 134 2098 5 MB-3 LCS-3 LCD-2.57 1,3,5-Trimethylbenzene U 100 5,095 5,000 102 70 - 134 2097 5 MB-3 LCS-3 LCD-2.58 Vinyl Chloride U 40 6,500 5,000 130 75 - 134 20122 6 MB-3 LCS-3 LCD-2.59 m&p-Xylene U 100 10,868 10,000 109 70 - 134 20104 5 MB-3 LCS-3 LCD-2.60 o-Xylene U 50 5,404 5,000 108 70 - 134 20104 4 MB-3 LCS-3 LCD-2

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 5,212 5,212 5,000 104 75 - 125 20104 05,000 104 MB-3 LCS-3 LCD-2.2 1,2-Dichloroethane-d4(S) 5,152 5,026 5,000 101 62 - 134 20101 05,000 103 MB-3 LCS-3 LCD-2.3 Toluene-d8(S) 5,061 5,060 5,000 101 50 - 150 20102 15,000 101 MB-3 LCS-3 LCD-2.4 4-Bromofluorobenzene(S) 4,895 5,091 5,000 102 64 - 136 20102 05,000 98 MB-3 LCS-3 LCD-2

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:51 PM

MB-3 06/02/15 13:01VH15F02ALCS-3 06/02/15 11:40VH15F02ALCD-2 06/02/15 12:07VH15F02A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02A-150604165621

Page 305: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02BPreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02B1 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acetone U 1000 3,853 5,000 77 70 - 150 2074 4 MB-7 LCS-7 LCD-3.2 Acrylonitrile U 100 5,555 5,000 111 70 - 134 20109 2 MB-7 LCS-7 LCD-3.3 Benzene U 50 4,964 5,000 99 70 - 134 2099 0 MB-7 LCS-7 LCD-3.4 Bromobenzene U 100 4,988 5,000 100 70 - 134 2099 1 MB-7 LCS-7 LCD-3.5 Bromochloromethane U 100 5,196 5,000 104 70 - 134 20101 3 MB-7 LCS-7 LCD-3.6 Bromodichloromethane U 100 5,486 5,000 110 70 - 134 20108 2 MB-7 LCS-7 LCD-3.7 Bromoform U 100 4,250 5,000 85 70 - 134 2084 1 MB-7 LCS-7 LCD-3.8 Bromomethane U 200 5,876 5,000 118 70 - 134 20116 2 MB-7 LCS-7 LCD-3.9 2-Butanone U 750 5,026 5,000 101 70 - 150 2098 3 MB-7 LCS-7 LCD-3.10 n-Butylbenzene U 50 4,728 5,000 95 70 - 134 2093 2 MB-7 LCS-7 LCD-3.11 sec-Butylbenzene U 50 4,884 5,000 98 70 - 134 2096 2 MB-7 LCS-7 LCD-3.12 tert-Butylbenzene U 50 4,895 5,000 98 70 - 134 2097 1 MB-7 LCS-7 LCD-3.13 Carbon Disulfide U 250 6,296 5,000 126 70 - 134 20126 0 MB-7 LCS-7 LCD-3.14 Carbon Tetrachloride U 50 5,454 5,000 109 70 - 134 20108 1 MB-7 LCS-7 LCD-3.15 Chlorobenzene U 50 4,726 5,000 95 70 - 134 2094 1 MB-7 LCS-7 LCD-3.16 Chloroethane U 250 5,032 5,000 101 70 - 134 2099 2 MB-7 LCS-7 LCD-3.17 Chloroform U 50 5,019 5,000 100 75 - 134 2099 1 MB-7 LCS-7 LCD-3.18 Chloromethane U 250 5,634 5,000 113 70 - 134 20111 2 MB-7 LCS-7 LCD-3.19 2-Chlorotoluene U 50 4,673 5,000 93 70 - 134 2097 4 MB-7 LCS-7 LCD-3.20 Dibromochloromethane U 100 4,683 5,000 94 70 - 134 2092 2 MB-7 LCS-7 LCD-3.21 1,2-Dibromo-3-chloropropane U 50 4,514 5,000 90 70 - 134 2084 7 MB-7 LCS-7 LCD-3.22 Dibromomethane U 250 5,243 5,000 105 70 - 134 20103 2 MB-7 LCS-7 LCD-3.23 1,2-Dichlorobenzene U 100 4,749 5,000 95 70 - 134 2093 2 MB-7 LCS-7 LCD-3.24 1,3-Dichlorobenzene U 100 4,667 5,000 93 70 - 134 2091 2 MB-7 LCS-7 LCD-3.25 1,4-Dichlorobenzene U 100 4,288 5,000 86 70 - 134 2085 1 MB-7 LCS-7 LCD-3.26 Dichlorodifluoromethane U 250 7,296 5,000 146 70 - 134 * 20144 1 MB-7 LCS-7 LCD-3.27 1,1-Dichloroethane U 50 4,958 5,000 99 70 - 134 2098 1 MB-7 LCS-7 LCD-3.28 1,2-Dichloroethane U 50 4,941 5,000 99 70 - 134 2097 2 MB-7 LCS-7 LCD-3.29 1,1-Dichloroethene U 50 5,220 5,000 104 75 - 134 20103 1 MB-7 LCS-7 LCD-3.30 cis-1,2-Dichloroethene U 50 5,066 5,000 101 70 - 134 20100 1 MB-7 LCS-7 LCD-3.31 trans-1,2-Dichloroethene U 50 5,045 5,000 101 70 - 134 20101 0 MB-7 LCS-7 LCD-3.32 1,2-Dichloropropane U 50 5,148 5,000 103 75 - 134 20101 2 MB-7 LCS-7 LCD-3.33 cis-1,3-Dichloropropene U 50 4,514 5,000 90 70 - 134 2088 2 MB-7 LCS-7 LCD-3.34 trans-1,3-Dichloropropene U 50 4,544 5,000 91 70 - 134 2090 1 MB-7 LCS-7 LCD-3.35 Ethylbenzene U 50 5,069 5,000 101 75 - 134 20100 1 MB-7 LCS-7 LCD-3.36 Ethylene Dibromide U 50 5,290 5,000 106 70 - 134 20105 1 MB-7 LCS-7 LCD-3.37 2-Hexanone U 2500 4,049 5,000 81 70 - 150 2077 5 MB-7 LCS-7 LCD-3.38 Isopropylbenzene U 250 4,982 5,000 100 70 - 134 2099 1 MB-7 LCS-7 LCD-3.39 Methylene Chloride U 100 4,648 5,000 93 70 - 134 2092 1 MB-7 LCS-7 LCD-3.40 4-Methyl-2-pentanone U 2500 5,072 5,000 101 70 - 134 2098 3 MB-7 LCS-7 LCD-3.41 MTBE U 250 4,726 5,000 95 70 - 134 2095 0 MB-7 LCS-7 LCD-3.42 Naphthalene U 330 4,837 5,000 97 70 - 134 2094 3 MB-7 LCS-7 LCD-3.43 n-Propylbenzene U 100 4,897 5,000 98 70 - 134 2097 1 MB-7 LCS-7 LCD-3.44 Styrene U 50 5,412 5,000 108 70 - 134 20107 1 MB-7 LCS-7 LCD-3.45 1,1,1,2-Tetrachloroethane U 100 5,217 5,000 104 70 - 134 20104 0 MB-7 LCS-7 LCD-3.46 1,1,2,2-Tetrachloroethane U 50 4,217 5,000 84 70 - 134 2088 5 MB-7 LCS-7 LCD-3.47 Tetrachloroethene U 50 4,741 5,000 95 70 - 134 2093 2 MB-7 LCS-7 LCD-3.48 Toluene U 50 4,920 5,000 98 75 - 134 2097 1 MB-7 LCS-7 LCD-3.49 1,2,4-Trichlorobenzene U 330 4,252 5,000 85 70 - 134 2083 2 MB-7 LCS-7 LCD-3.50 1,1,1-Trichloroethane U 50 5,096 5,000 102 70 - 134 20101 1 MB-7 LCS-7 LCD-3.51 1,1,2-Trichloroethane U 50 4,884 5,000 98 70 - 134 2096 2 MB-7 LCS-7 LCD-3

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02B-150604165621

Page 306: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02BPreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02B2 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.52 Trichloroethene U 50 5,298 5,000 106 70 - 134 20105 1 MB-7 LCS-7 LCD-3.53 Trichlorofluoromethane U 100 5,750 5,000 115 70 - 134 20113 2 MB-7 LCS-7 LCD-3.54 1,2,3-Trichloropropane U 100 5,065 5,000 101 70 - 134 2097 4 MB-7 LCS-7 LCD-3.55 1,2,3-Trimethylbenzene U 100 4,709 5,000 94 70 - 134 2093 1 MB-7 LCS-7 LCD-3.56 1,2,4-Trimethylbenzene U 100 5,003 5,000 100 70 - 134 2099 1 MB-7 LCS-7 LCD-3.57 1,3,5-Trimethylbenzene U 100 4,939 5,000 99 70 - 134 2097 2 MB-7 LCS-7 LCD-3.58 Vinyl Chloride U 40 6,033 5,000 121 75 - 134 20120 1 MB-7 LCS-7 LCD-3.59 m&p-Xylene U 500 10,359 10,000 104 70 - 134 20103 1 MB-7 LCS-7 LCD-3.60 o-Xylene U 500 5,230 5,000 105 70 - 134 20104 1 MB-7 LCS-7 LCD-3

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 5,062 5,071 5,000 101 75 - 125 20101 05,000 101 MB-7 LCS-7 LCD-3.2 1,2-Dichloroethane-d4(S) 5,080 5,022 5,000 100 62 - 134 2099 15,000 102 MB-7 LCS-7 LCD-3.3 Toluene-d8(S) 5,051 5,075 5,000 102 50 - 150 20101 15,000 101 MB-7 LCS-7 LCD-3.4 4-Bromofluorobenzene(S) 4,915 5,118 5,000 102 64 - 136 20103 15,000 98 MB-7 LCS-7 LCD-3

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:51 PM

MB-7 06/03/15 02:56VH15F02BLCS-7 06/03/15 00:15VH15F02BLCD-3 06/03/15 00:42VH15F02B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02B-150604165621

Page 307: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VJ15E28BPreparation Batch: 05/28/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

VJ15E28B1 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acetone U 1000 7,150 5,000 143 70 - 150 20121 17 MB-1 LCS-1 LCD-1.2 Acrylonitrile U 100 4,927 5,000 99 70 - 134 2098 1 MB-1 LCS-1 LCD-1.3 Benzene U 50 4,883 5,000 98 70 - 134 2096 2 MB-1 LCS-1 LCD-1.4 Bromobenzene U 100 4,534 5,000 91 70 - 134 2090 1 MB-1 LCS-1 LCD-1.5 Bromochloromethane U 100 4,144 5,000 83 70 - 134 2082 1 MB-1 LCS-1 LCD-1.6 Bromodichloromethane U 100 4,806 5,000 96 70 - 134 2095 1 MB-1 LCS-1 LCD-1.7 Bromoform U 100 5,221 5,000 104 70 - 134 20101 3 MB-1 LCS-1 LCD-1.8 Bromomethane U 200 4,448 5,000 89 70 - 134 2088 1 MB-1 LCS-1 LCD-1.9 2-Butanone U 750 5,818 5,000 116 70 - 150 20101 14 MB-1 LCS-1 LCD-1.10 n-Butylbenzene U 50 4,825 5,000 96 70 - 134 2093 3 MB-1 LCS-1 LCD-1.11 sec-Butylbenzene U 50 5,042 5,000 101 70 - 134 2098 3 MB-1 LCS-1 LCD-1.12 tert-Butylbenzene U 50 5,110 5,000 102 70 - 134 20100 2 MB-1 LCS-1 LCD-1.13 Carbon Disulfide U 250 4,463 5,000 89 70 - 134 2086 3 MB-1 LCS-1 LCD-1.14 Carbon Tetrachloride U 50 5,145 5,000 103 70 - 134 20100 3 MB-1 LCS-1 LCD-1.15 Chlorobenzene U 50 4,988 5,000 100 70 - 134 2096 4 MB-1 LCS-1 LCD-1.16 Chloroethane U 250 5,136 5,000 103 70 - 134 20100 3 MB-1 LCS-1 LCD-1.17 Chloroform U 50 4,523 5,000 90 75 - 134 2089 1 MB-1 LCS-1 LCD-1.18 Chloromethane U 250 4,215 5,000 84 70 - 134 2082 2 MB-1 LCS-1 LCD-1.19 2-Chlorotoluene U 50 5,064 5,000 101 70 - 134 2094 7 MB-1 LCS-1 LCD-1.20 Dibromochloromethane U 100 5,149 5,000 103 70 - 134 20100 3 MB-1 LCS-1 LCD-1.21 1,2-Dibromo-3-chloropropane U 25 5,137 5,000 103 70 - 134 20100 3 MB-1 LCS-1 LCD-1.22 Dibromomethane U 250 4,939 5,000 99 70 - 134 2098 1 MB-1 LCS-1 LCD-1.23 1,2-Dichlorobenzene U 100 4,821 5,000 96 70 - 134 2095 1 MB-1 LCS-1 LCD-1.24 1,3-Dichlorobenzene U 100 4,810 5,000 96 70 - 134 2095 1 MB-1 LCS-1 LCD-1.25 1,4-Dichlorobenzene U 100 4,630 5,000 93 70 - 134 2091 2 MB-1 LCS-1 LCD-1.26 Dichlorodifluoromethane U 250 4,584 5,000 92 70 - 134 2088 4 MB-1 LCS-1 LCD-1.27 1,1-Dichloroethane U 50 4,450 5,000 89 70 - 134 2087 2 MB-1 LCS-1 LCD-1.28 1,2-Dichloroethane U 50 4,800 5,000 96 70 - 134 2095 1 MB-1 LCS-1 LCD-1.29 1,1-Dichloroethene U 50 4,620 5,000 92 75 - 134 2089 3 MB-1 LCS-1 LCD-1.30 cis-1,2-Dichloroethene U 50 4,580 5,000 92 70 - 134 2089 3 MB-1 LCS-1 LCD-1.31 trans-1,2-Dichloroethene U 50 4,594 5,000 92 70 - 134 2089 3 MB-1 LCS-1 LCD-1.32 1,2-Dichloropropane U 50 4,754 5,000 95 75 - 134 2095 0 MB-1 LCS-1 LCD-1.33 cis-1,3-Dichloropropene U 50 4,845 5,000 97 70 - 134 2096 1 MB-1 LCS-1 LCD-1.34 trans-1,3-Dichloropropene U 50 4,714 5,000 94 70 - 134 2094 0 MB-1 LCS-1 LCD-1.35 Ethylbenzene U 50 4,826 5,000 97 75 - 134 2093 4 MB-1 LCS-1 LCD-1.36 Ethylene Dibromide U 50 4,900 5,000 98 70 - 134 2096 2 MB-1 LCS-1 LCD-1.37 2-Hexanone U 2500 6,052 5,000 121 70 - 150 20107 12 MB-1 LCS-1 LCD-1.38 Isopropylbenzene U 250 5,225 5,000 104 70 - 134 20100 4 MB-1 LCS-1 LCD-1.39 Methylene Chloride U 100 4,585 5,000 92 70 - 134 2091 1 MB-1 LCS-1 LCD-1.40 4-Methyl-2-pentanone U 2500 5,311 5,000 106 70 - 134 20103 3 MB-1 LCS-1 LCD-1.41 MTBE U 250 4,902 5,000 98 70 - 134 2097 1 MB-1 LCS-1 LCD-1.42 Naphthalene U 330 5,295 5,000 106 70 - 134 20104 2 MB-1 LCS-1 LCD-1.43 n-Propylbenzene U 100 4,858 5,000 97 70 - 134 2095 2 MB-1 LCS-1 LCD-1.44 Styrene U 50 5,283 5,000 106 70 - 134 20103 3 MB-1 LCS-1 LCD-1.45 1,1,1,2-Tetrachloroethane U 100 4,988 5,000 100 70 - 134 2096 4 MB-1 LCS-1 LCD-1.46 1,1,2,2-Tetrachloroethane U 50 4,647 5,000 93 70 - 134 2096 3 MB-1 LCS-1 LCD-1.47 Tetrachloroethene U 50 5,147 5,000 103 70 - 134 2098 5 MB-1 LCS-1 LCD-1.48 Toluene U 50 4,883 5,000 98 75 - 134 2096 2 MB-1 LCS-1 LCD-1.49 1,2,4-Trichlorobenzene U 330 5,028 5,000 101 70 - 134 2099 2 MB-1 LCS-1 LCD-1.50 1,1,1-Trichloroethane U 50 4,886 5,000 98 70 - 134 2095 3 MB-1 LCS-1 LCD-1.51 1,1,2-Trichloroethane U 50 4,970 5,000 99 70 - 134 2097 2 MB-1 LCS-1 LCD-1

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VJ15E28B-150604165621

Page 308: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VJ15E28BPreparation Batch: 05/28/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

VJ15E28B2 of 2

Batch ID:Page:Date: 06/04/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.52 Trichloroethene U 50 5,250 5,000 105 70 - 134 20101 4 MB-1 LCS-1 LCD-1.53 Trichlorofluoromethane U 100 4,245 5,000 85 70 - 134 2078 9 MB-1 LCS-1 LCD-1.54 1,2,3-Trichloropropane U 100 5,056 5,000 101 70 - 134 20100 1 MB-1 LCS-1 LCD-1.55 1,2,3-Trimethylbenzene U 100 4,954 5,000 99 70 - 134 2097 2 MB-1 LCS-1 LCD-1.56 1,2,4-Trimethylbenzene U 100 4,943 5,000 99 70 - 134 2096 3 MB-1 LCS-1 LCD-1.57 1,3,5-Trimethylbenzene U 100 4,970 5,000 99 70 - 134 2097 2 MB-1 LCS-1 LCD-1.58 Vinyl Chloride U 40 4,527 5,000 91 75 - 134 2086 6 MB-1 LCS-1 LCD-1.59 m&p-Xylene U 100 10,013 10,000 100 70 - 134 2096 4 MB-1 LCS-1 LCD-1.60 o-Xylene U 50 5,208 5,000 104 70 - 134 20100 4 MB-1 LCS-1 LCD-1

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 2,359 2,363 2,500 95 75 - 125 2094 12,500 94 MB-1 LCS-1 LCD-1.2 1,2-Dichloroethane-d4(S) 2,380 2,335 2,500 93 62 - 134 2094 12,500 95 MB-1 LCS-1 LCD-1.3 Toluene-d8(S) 2,470 2,440 2,500 98 50 - 150 2099 12,500 99 MB-1 LCS-1 LCD-1.4 4-Bromofluorobenzene(S) 2,474 2,479 2,500 99 64 - 136 2099 02,500 99 MB-1 LCS-1 LCD-1

Thursday, June 04, 2015

Amanda PetrovskyClient Services Representative

4:56:51 PM

MB-1 05/29/15 07:38VJ15E28BLCS-1 05/29/15 05:36VJ15E28BLCD-1 05/29/15 06:00VJ15E28B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VJ15E28B-150604165621

Page 309: Baseline Environmental Assessment for Riverside Park

Monday, June 08, 2015

62-140614-100A /62-140614-100AProject Identification:Fibertec Project Number: 68109

41780 Six Mile RoadNTH Consultants, Ltd. - Northville

Northville, MI 48168-3459

Mr. Cliff Andrews

Thank you for selecting Fibertec Environmental Services as your analytical laboratory. The samples you submitted have been analyzed in accordance with NELAC standards and the results compiled in the attached report. Any exceptions to NELAC compliance are noted in the report. These results apply only to those samples submitted. Please note TO-15 samples will be disposed of 14 days after the reporting date. All other samples will be disposed of 30 days after the reporting date.

Dear Mr. Andrews,

Submittal Date: 06/01/2015

If you have any questions regarding these results or if we may be of further assistance to you, please contact me at (517) 699-0345.

Sincerely,

Daryl P. Strandbergh Laboratory Director

Enclosures

DPS/arp

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 310: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-001

Analytical Laboratory Report 681092 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-1 S-1 (1.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 09:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

%1. 14 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg1. 1900 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 6100 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. U 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 3500 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 3100 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 2300 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. U 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. U 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 8700 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg1. U 50 8.6 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polychlorinated Biphenyls (PCBs) (EPA 3546/EPA 8082A) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg1. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1016 PM

µg/kg2. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1221 PM

µg/kg3. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1232 PM

µg/kg4. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1242 PM

µg/kg5. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1248 PM

µg/kg6. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1254 PM

µg/kg7. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1260 PM

µg/kg8. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1262‡ PM

µg/kg9. U 100 5.0 06/02/15 PS15F02A 06/03/15 SA15F03AAroclor-1268‡ PM

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 311: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-001

Analytical Laboratory Report 681093 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-1 S-1 (1.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 09:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-001A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

µg/kg10. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

µg/kg11. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 290 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 290 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 290 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 312: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-001

Analytical Laboratory Report 681094 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-1 S-1 (1.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 09:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-001A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg38. U 290 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

µg/kg47. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. U 58 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. U 150 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg1. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthene RDK

µg/kg2. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAcenaphthylene RDK

µg/kg3. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AAnthracene RDK

µg/kg4. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)anthracene RDK

µg/kg5. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(a)pyrene RDK

µg/kg6. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(b)fluoranthene RDK

µg/kg7. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(ghi)perylene RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 313: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-001

Analytical Laboratory Report 681095 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-1 S-1 (1.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 09:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-001

P. Date P. Batch A. Date A. Batch Init.

Description: GP-1 S-1 (1.0-3.0)

µg/kg8. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ABenzo(k)fluoranthene RDK

µg/kg9. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AChrysene RDK

µg/kg10. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02ADibenzo(a,h)anthracene RDK

µg/kg11. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluoranthene RDK

µg/kg12. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AFluorene RDK

µg/kg13. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02AIndeno(1,2,3-cd)pyrene RDK

µg/kg14. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02A2-Methylnaphthalene RDK

µg/kg15. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APhenanthrene RDK

µg/kg16. U 330 1.0 06/02/15 PS15F02A 06/02/15 S115F02APyrene RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 314: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-003

Analytical Laboratory Report 681096 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

%1. 17 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg1. 15000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 65000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 490 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 6300 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 110000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 58000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. 1300 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. U 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 110000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg1. 88 50 8.6 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-003A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 315: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-003

Analytical Laboratory Report 681097 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-003A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg10. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

µg/kg11. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 300 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 300 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 300 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

µg/kg38. U 300 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 316: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-003

Analytical Laboratory Report 681098 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-003A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg47. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. 310 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 120 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. 290 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. 170 60 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. 460 150 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-003

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-1 (2.0-3.0)

µg/kg1. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 760 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 2300 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 1900 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 2800 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 1300 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. 900 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 3100 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. 390 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 4100 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. 610 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 1200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 8100 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 7000 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 4600 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 317: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-005

Analytical Laboratory Report 681099 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-3 (9.0-10.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

%1. 28 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

µg/kg1. 11000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 130000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 1000 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 33000 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 180000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 870000 1000 200 06/03/15 PT15F03D 06/04/15 T415F04ALead JLP

µg/kg7. 380 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. 130 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 390000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

µg/kg1. 73 50 8.5 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 318: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-005

Analytical Laboratory Report 6810910 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-3 (9.0-10.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

E1 µg/kg10. 160 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

µg/kg11. 98 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 350 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 350 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 350 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

µg/kg38. U 350 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. 2500 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 319: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-005

Analytical Laboratory Report 6810911 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-5 S-3 (9.0-10.5)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 10:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-005A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

µg/kg47. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. 280 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 330 140 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. 370 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. U 70 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. U 150 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-005

P. Date P. Batch A. Date A. Batch Init.

Description: GP-5 S-3 (9.0-10.5)

µg/kg1. 1200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 1800 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 1300 370 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 760 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 1000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 440 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 1300 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 4200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. 1800 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 440 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 2700 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 7500 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 4100 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 320: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-008

Analytical Laboratory Report 6810912 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-6 S-3 (10.5-11.0)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 11:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

%1. 21 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

µg/kg1. 13000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 210000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 570 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 22000 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 150000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 530000 1000 100 06/03/15 PT15F03D 06/04/15 T415F04ALead JLP

µg/kg7. 380 200 10 06/03/15 PT15F03D 06/04/15 T415F04ASelenium JLP

µg/kg8. 420 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 260000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

µg/kg1. 790 50 9.2 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

µg/kg1. U 1000 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcetone DAR

µg/kg2. U 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcrylonitrile‡ DAR

µg/kg3. 63 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBenzene DAR

µg/kg4. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromobenzene DAR

µg/kg5. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromochloromethane DAR

µg/kg6. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromodichloromethane DAR

µg/kg7. U 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromoform DAR

µg/kg8. U 200 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromomethane DAR

µg/kg9. U 750 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 321: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-008

Analytical Laboratory Report 6810913 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-6 S-3 (10.5-11.0)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 11:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

E1 µg/kg10. 210 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Butylbenzene DAR

µg/kg11. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bsec-Butylbenzene DAR

µg/kg12. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Disulfide DAR

µg/kg14. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Tetrachloride DAR

µg/kg15. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChlorobenzene DAR

µg/kg16. U 310 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroethane DAR

µg/kg17. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroform DAR

µg/kg18. U 310 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloromethane DAR

µg/kg19. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Chlorotoluene DAR

µg/kg20. U 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromochloromethane DAR

µg/kg21. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromomethane DAR

µg/kg23. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,4-Dichlorobenzene DAR

µg/kg26. U 310 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,2-Dichloroethene DAR

µg/kg32. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloropropane DAR

µg/kg33. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,3-Dichloropropene DAR

µg/kg34. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,3-Dichloropropene DAR

µg/kg35. 1500 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylbenzene DAR

µg/kg36. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Hexanone DAR

µg/kg38. U 310 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMTBE DAR

µg/kg42. 60000 630 10 06/03/15 VH15F03A 06/03/15 VH15F03ANaphthalene DAR

µg/kg43. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Propylbenzene DAR

µg/kg44. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BStyrene DAR

µg/kg45. U 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 322: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-008

Analytical Laboratory Report 6810914 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-6 S-3 (10.5-11.0)

Sample No: S-3

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 11:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-008A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

µg/kg47. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTetrachloroethene DAR

µg/kg48. 150 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BToluene DAR

µg/kg49. U 330 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1-Trichloroethane DAR

µg/kg51. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichloroethene DAR

µg/kg53. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichlorofluoromethane DAR

µg/kg54. U 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trichloropropane DAR

µg/kg55. 730 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 2400 130 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trimethylbenzene DAR

µg/kg57. 750 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BVinyl Chloride DAR

µg/kg59. 840 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bm&p-Xylene DAR

µg/kg60. 530 63 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bo-Xylene DAR

µg/kg61. 1400 150 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-008

P. Date P. Batch A. Date A. Batch Init.

Description: GP-6 S-3 (10.5-11.0)

µg/kg1. 57000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. 3200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 37000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 18000 340 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 16000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 12000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 7100 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. 4700 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 17000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. 1700 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 34000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. 29000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 6200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 74000 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 110000 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 63000 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 323: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-009

Analytical Laboratory Report 6810915 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-7 S-1 (5.0-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

%1. 17 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg1. 4000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 28000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 96 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 5900 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 170000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 85000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. U 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. U 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 46000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg1. 120 50 8.7 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg1. U 1000 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcetone DAR

µg/kg2. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBenzene DAR

µg/kg4. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromobenzene DAR

µg/kg5. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromochloromethane DAR

µg/kg6. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromoform DAR

µg/kg8. U 200 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromomethane DAR

µg/kg9. U 750 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 324: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-009

Analytical Laboratory Report 6810916 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-7 S-1 (5.0-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg10. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Butylbenzene DAR

µg/kg11. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bsec-Butylbenzene DAR

µg/kg12. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Disulfide DAR

µg/kg14. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Tetrachloride DAR

µg/kg15. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChlorobenzene DAR

µg/kg16. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroethane DAR

µg/kg17. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroform DAR

µg/kg18. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloromethane DAR

µg/kg19. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromochloromethane DAR

µg/kg21. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromomethane DAR

µg/kg23. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,4-Dichlorobenzene DAR

µg/kg26. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,2-Dichloroethene DAR

µg/kg32. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloropropane DAR

µg/kg33. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,3-Dichloropropene DAR

µg/kg34. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylbenzene DAR

µg/kg36. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Hexanone DAR

µg/kg38. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMTBE DAR

µg/kg42. U 330 1.0 06/03/15 VH15F03A 06/03/15 VH15F03ANaphthalene DAR

µg/kg43. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Propylbenzene DAR

µg/kg44. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BStyrene DAR

µg/kg45. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 325: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-009

Analytical Laboratory Report 6810917 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-7 S-1 (5.0-7.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-009A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg47. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTetrachloroethene DAR

µg/kg48. 60 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BToluene DAR

µg/kg49. U 330 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1-Trichloroethane DAR

µg/kg51. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichloroethene DAR

µg/kg53. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BVinyl Chloride DAR

µg/kg59. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bm&p-Xylene DAR

µg/kg60. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bo-Xylene DAR

µg/kg61. U 150 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-009

P. Date P. Batch A. Date A. Batch Init.

Description: GP-7 S-1 (5.0-7.0)

µg/kg1. 340 330 20 06/04/15 PS15F04D 06/04/15 S715F04AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04AAcenaphthylene (SIM) RDK

µg/kg3. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04AAnthracene (SIM) RDK

µg/kg4. 620 330 20 06/04/15 PS15F04D 06/04/15 S715F04ABenzo(a)anthracene (SIM) RDK

µg/kg5. 470 330 20 06/04/15 PS15F04D 06/04/15 S715F04ABenzo(a)pyrene (SIM) RDK

µg/kg6. 560 330 20 06/04/15 PS15F04D 06/04/15 S715F04ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 340 330 20 06/04/15 PS15F04D 06/04/15 S715F04ABenzo(ghi)perylene (SIM) RDK

µg/kg8. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 410 330 20 06/04/15 PS15F04D 06/04/15 S715F04AChrysene (SIM) RDK

µg/kg10. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 840 330 20 06/04/15 PS15F04D 06/04/15 S715F04AFluoranthene (SIM) RDK

µg/kg12. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04AFluorene (SIM) RDK

µg/kg13. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. U 330 20 06/04/15 PS15F04D 06/04/15 S715F04A2-Methylnaphthalene (SIM) RDK

µg/kg15. 760 330 20 06/04/15 PS15F04D 06/04/15 S715F04APhenanthrene (SIM) RDK

µg/kg16. 1100 330 20 06/04/15 PS15F04D 06/04/15 S715F04APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 326: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-011

Analytical Laboratory Report 6810918 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-8 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-011

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

%1. 12 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-011

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg1. 14000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 100000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 1600 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 18000 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 120000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 140000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. 1700 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. 200 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 210000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-011

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg1. 58 50 9.0 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-011A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg1. U 1000 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcetone DAR

µg/kg2. U 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcrylonitrile‡ DAR

µg/kg3. 59 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBenzene DAR

µg/kg4. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromobenzene DAR

µg/kg5. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromochloromethane DAR

µg/kg6. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromodichloromethane DAR

µg/kg7. U 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromoform DAR

µg/kg8. U 200 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromomethane DAR

µg/kg9. U 750 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 327: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-011

Analytical Laboratory Report 6810919 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-8 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-011A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg10. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Butylbenzene DAR

µg/kg11. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bsec-Butylbenzene DAR

µg/kg12. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Disulfide DAR

µg/kg14. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Tetrachloride DAR

µg/kg15. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChlorobenzene DAR

µg/kg16. U 280 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroethane DAR

µg/kg17. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroform DAR

µg/kg18. U 280 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloromethane DAR

µg/kg19. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Chlorotoluene DAR

µg/kg20. U 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromochloromethane DAR

µg/kg21. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromomethane DAR

µg/kg23. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,4-Dichlorobenzene DAR

µg/kg26. U 280 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,2-Dichloroethene DAR

µg/kg32. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloropropane DAR

µg/kg33. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,3-Dichloropropene DAR

µg/kg34. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,3-Dichloropropene DAR

µg/kg35. 86 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylbenzene DAR

µg/kg36. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Hexanone DAR

µg/kg38. U 280 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMTBE DAR

µg/kg42. 410 330 1.0 06/03/15 VH15F03A 06/03/15 VH15F03ANaphthalene DAR

µg/kg43. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Propylbenzene DAR

µg/kg44. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BStyrene DAR

µg/kg45. U 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 328: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-011

Analytical Laboratory Report 6810920 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-8 S-1 (2.0-3.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 13:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-011A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg47. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTetrachloroethene DAR

µg/kg48. 320 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BToluene DAR

µg/kg49. U 330 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1-Trichloroethane DAR

µg/kg51. U 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2-Trichloroethane‡ DAR

µg/kg52. 64 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichloroethene DAR

µg/kg53. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichlorofluoromethane DAR

µg/kg54. U 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. 170 110 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BVinyl Chloride DAR

µg/kg59. 330 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bm&p-Xylene DAR

µg/kg60. 190 57 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bo-Xylene DAR

µg/kg61. 530 150 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-011

P. Date P. Batch A. Date A. Batch Init.

Description: GP-8 S-1 (2.0-3.0)

µg/kg1. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 400 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 2800 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 3500 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 2400 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 2800 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. 510 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 3500 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. 780 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 2200 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 1500 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. 2300 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 2500 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 4700 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 329: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-013

Analytical Laboratory Report 6810921 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-9 S-1 (1.5-3.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-013

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

%1. 16 0.1 1.0 NA NA 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-013

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg1. 13000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 97000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 680 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 34000 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 45000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 60000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. 1000 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. U 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 120000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-013

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg1. 220 50 8.8 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-013A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg1. U 1000 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcetone DAR

µg/kg2. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBenzene DAR

µg/kg4. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromobenzene DAR

µg/kg5. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromochloromethane DAR

µg/kg6. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromodichloromethane DAR

µg/kg7. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromoform DAR

µg/kg8. U 200 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BBromomethane DAR

µg/kg9. U 750 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 330: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-013

Analytical Laboratory Report 6810922 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-9 S-1 (1.5-3.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-013A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg10. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Butylbenzene DAR

µg/kg11. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bsec-Butylbenzene DAR

µg/kg12. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Disulfide DAR

µg/kg14. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BCarbon Tetrachloride DAR

µg/kg15. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChlorobenzene DAR

µg/kg16. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroethane DAR

µg/kg17. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloroform DAR

µg/kg18. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BChloromethane DAR

µg/kg19. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Chlorotoluene DAR

µg/kg20. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromochloromethane DAR

µg/kg21. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDibromomethane DAR

µg/kg23. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,4-Dichlorobenzene DAR

µg/kg26. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1-Dichloroethene DAR

µg/kg30. 140 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,2-Dichloroethene DAR

µg/kg32. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2-Dichloropropane DAR

µg/kg33. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bcis-1,3-Dichloropropene DAR

µg/kg34. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylbenzene DAR

µg/kg36. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B2-Hexanone DAR

µg/kg38. U 300 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BMTBE DAR

µg/kg42. U 330 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BNaphthalene DAR

µg/kg43. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bn-Propylbenzene DAR

µg/kg44. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BStyrene DAR

µg/kg45. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 331: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-013

Analytical Laboratory Report 6810923 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-9 S-1 (1.5-3.5)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:00

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-013A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg47. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTetrachloroethene DAR

µg/kg48. 180 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BToluene DAR

µg/kg49. U 330 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,1-Trichloroethane DAR

µg/kg51. U 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,1,2-Trichloroethane‡ DAR

µg/kg52. 610 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichloroethene DAR

µg/kg53. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BTrichlorofluoromethane DAR

µg/kg54. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 120 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BVinyl Chloride DAR

µg/kg59. 120 100 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bm&p-Xylene DAR

µg/kg60. 61 60 1.0 06/01/15 VH15F01B 06/01/15 VH15F01Bo-Xylene DAR

µg/kg61. 180 150 1.0 06/01/15 VH15F01B 06/01/15 VH15F01BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-013

P. Date P. Batch A. Date A. Batch Init.

Description: GP-9 S-1 (1.5-3.5)

µg/kg1. U 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AAcenaphthene RDK

µg/kg2. U 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AAcenaphthylene RDK

µg/kg3. 370 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AAnthracene RDK

µg/kg4. 1100 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ABenzo(a)anthracene RDK

µg/kg5. 870 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ABenzo(a)pyrene RDK

µg/kg6. 1400 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ABenzo(b)fluoranthene RDK

µg/kg7. 360 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ABenzo(ghi)perylene RDK

µg/kg8. 440 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ABenzo(k)fluoranthene RDK

µg/kg9. 1100 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AChrysene RDK

µg/kg10. U 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02ADibenzo(a,h)anthracene RDK

µg/kg11. 2100 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AFluoranthene RDK

µg/kg12. U 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AFluorene RDK

µg/kg13. 430 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02AIndeno(1,2,3-cd)pyrene RDK

µg/kg14. 1000 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02A2-Methylnaphthalene RDK

µg/kg15. 1800 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02APhenanthrene RDK

µg/kg16. 1800 330 1.0 06/02/15 PS15F02A 06/03/15 S115F02APyrene RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 332: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-015

Analytical Laboratory Report 6810924 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-10 S-1 (4.0-5.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Dry Weight Determination (ASTM D 2974-87) Soil/SolidMatrix:68109-015

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

%1. 20 0.1 1.0 06/02/15 MC150602 06/03/15 MC150602Percent Moisture (Water Content)‡ BMG

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Michigan 10 Elements by ICP/MS (EPA 0200.2-M/EPA 6020A) Soil/SolidMatrix:68109-015

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg1. 14000 100 20 06/03/15 PT15F03D 06/03/15 T415F03AArsenic JLP

µg/kg2. 93000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ABarium JLP

µg/kg3. 670 50 20 06/03/15 PT15F03D 06/03/15 T415F03ACadmium JLP

µg/kg4. 45000 500 20 06/03/15 PT15F03D 06/03/15 T415F03AChromium JLP

µg/kg5. 57000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ACopper JLP

µg/kg6. 140000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03ALead JLP

µg/kg7. 1500 200 20 06/03/15 PT15F03D 06/03/15 T415F03ASelenium JLP

µg/kg8. U 100 20 06/03/15 PT15F03D 06/03/15 T415F03ASilver JLP

µg/kg9. 170000 1000 20 06/03/15 PT15F03D 06/03/15 T415F03AZinc JLP

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Mercury by CVAAS (EPA 7471B) Soil/SolidMatrix:68109-015

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg1. 180 50 9.0 06/03/15 PM15F03D 06/04/15 M615F04AMercury JWS

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-015A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg1. U 1000 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcetone DAR

µg/kg2. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BAcrylonitrile‡ DAR

µg/kg3. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBenzene DAR

µg/kg4. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromobenzene DAR

µg/kg5. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromochloromethane DAR

µg/kg6. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromodichloromethane DAR

µg/kg7. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromoform DAR

µg/kg8. U 200 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BBromomethane DAR

µg/kg9. U 750 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Butanone DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 333: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-015

Analytical Laboratory Report 6810925 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-10 S-1 (4.0-5.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-015A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg10. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Butylbenzene DAR

µg/kg11. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bsec-Butylbenzene DAR

µg/kg12. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btert-Butylbenzene DAR

µg/kg13. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Disulfide DAR

µg/kg14. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BCarbon Tetrachloride DAR

µg/kg15. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChlorobenzene DAR

µg/kg16. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroethane DAR

µg/kg17. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloroform DAR

µg/kg18. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BChloromethane DAR

µg/kg19. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Chlorotoluene DAR

µg/kg20. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromochloromethane DAR

µg/kg21. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dibromo-3-chloropropane (SIM)‡ DAR

µg/kg22. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDibromomethane DAR

µg/kg23. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichlorobenzene DAR

µg/kg24. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3-Dichlorobenzene DAR

µg/kg25. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,4-Dichlorobenzene DAR

L+ µg/kg26. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BDichlorodifluoromethane DAR

µg/kg27. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethane DAR

µg/kg28. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloroethane DAR

µg/kg29. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1-Dichloroethene DAR

µg/kg30. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,2-Dichloroethene DAR

µg/kg31. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,2-Dichloroethene DAR

µg/kg32. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2-Dichloropropane DAR

µg/kg33. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bcis-1,3-Dichloropropene DAR

µg/kg34. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Btrans-1,3-Dichloropropene DAR

µg/kg35. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylbenzene DAR

µg/kg36. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BEthylene Dibromide DAR

µg/kg37. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B2-Hexanone DAR

µg/kg38. U 310 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BIsopropylbenzene DAR

µg/kg39. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMethylene Chloride DAR

µg/kg40. U 2500 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B4-Methyl-2-pentanone DAR

µg/kg41. U 250 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BMTBE DAR

µg/kg42. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BNaphthalene DAR

µg/kg43. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bn-Propylbenzene DAR

µg/kg44. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BStyrene DAR

µg/kg45. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1,2-Tetrachloroethane DAR

µg/kg46. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2,2-Tetrachloroethane DAR

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 334: Baseline Environmental Assessment for Riverside Park

Laboratory Sample Number: 68109-015

Analytical Laboratory Report 6810926 of 27

Order:Page:Date: 06/08/15

Client Identification: NTH Consultants, Ltd. - Northville

Client Project Name: 62-140614-100A

Client Project No: 62-140614-100A

Sample Description: GP-10 S-1 (4.0-5.0)

Sample No: S-1

Sample Matrix: Soil/Solid

Collect Date:

Chain of Custody: 141511

Collect Time: 14:30

Laboratory Project Number: 68109

Sample Comments: Soil results have been calculated and reported on a dry weight basis unless otherwise noted.

Q: Qualifier (see definitions at end of report) NA: Not ApplicableDefinitions:

05/28/15

: Parameter not included in NELAC Scope of Analysis.‡

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Volatile Organic Compounds (VOCs) by GC/MS, 5035 (EPA 5035A/EPA 8260B) Soil/SolidMatrix:68109-015A

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg47. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTetrachloroethene DAR

µg/kg48. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BToluene DAR

µg/kg49. U 330 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trichlorobenzene DAR

µg/kg50. U 50 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,1-Trichloroethane DAR

µg/kg51. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,1,2-Trichloroethane‡ DAR

µg/kg52. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichloroethene DAR

µg/kg53. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BTrichlorofluoromethane DAR

µg/kg54. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trichloropropane DAR

µg/kg55. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,3-Trimethylbenzene‡ DAR

µg/kg56. U 130 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,2,4-Trimethylbenzene DAR

µg/kg57. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02B1,3,5-Trimethylbenzene DAR

µg/kg58. U 40 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BVinyl Chloride DAR

µg/kg59. U 100 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bm&p-Xylene DAR

µg/kg60. U 63 1.0 06/02/15 VH15F02B 06/03/15 VH15F02Bo-Xylene DAR

µg/kg61. U 150 1.0 06/02/15 VH15F02B 06/03/15 VH15F02BXylenes‡ DAR

AnalysisReporting Limit Parameter(s) Result

PreparationUnitsQ Dilution

Aliquot ID: Polynuclear Aromatic Hydrocarbons (PNAs) (EPA 3546/EPA 8270C) Soil/SolidMatrix:68109-015

P. Date P. Batch A. Date A. Batch Init.

Description: GP-10 S-1 (4.0-5.0)

µg/kg1. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthene (SIM) RDK

µg/kg2. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAcenaphthylene (SIM) RDK

µg/kg3. 660 330 20 06/02/15 PS15F02A 06/02/15 S715F02AAnthracene (SIM) RDK

µg/kg4. 1700 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)anthracene (SIM) RDK

µg/kg5. 1600 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(a)pyrene (SIM) RDK

µg/kg6. 2000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(b)fluoranthene (SIM) RDK

µg/kg7. 1000 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(ghi)perylene (SIM) RDK

µg/kg8. 670 330 20 06/02/15 PS15F02A 06/02/15 S715F02ABenzo(k)fluoranthene (SIM) RDK

µg/kg9. 1600 330 20 06/02/15 PS15F02A 06/02/15 S715F02AChrysene (SIM) RDK

µg/kg10. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02ADibenzo(a,h)anthracene (SIM) RDK

µg/kg11. 3300 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluoranthene (SIM) RDK

µg/kg12. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02AFluorene (SIM) RDK

µg/kg13. 1000 330 20 06/02/15 PS15F02A 06/02/15 S715F02AIndeno(1,2,3-cd)pyrene (SIM) RDK

µg/kg14. U 330 20 06/02/15 PS15F02A 06/02/15 S715F02A2-Methylnaphthalene (SIM) RDK

µg/kg15. 2200 330 20 06/02/15 PS15F02A 06/02/15 S715F02APhenanthrene (SIM) RDK

µg/kg16. 3400 330 20 06/02/15 PS15F02A 06/02/15 S715F02APyrene (SIM) RDK

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 335: Baseline Environmental Assessment for Riverside Park

Spike recovery or precision unusable due to dilution.

Definitions/ Qualifiers:

The analyte was detected in the associated method blank.The analyte was detected at a concentration greater than the calibration range, therefore the result is estimated.The concentration is an estimated value.

The analyte was not detected at or above the reporting limit.Matrix Interference has resulted in a raised reporting limit or distorted result.Results reported on a wet-weight basis.Value reported is outside QA limits

A:B:E:J:

U:X:W:*:

Analytical Laboratory Report 6810927 of 27

Order:Page:Date: 06/08/15

Laboratory Project Number: 68109

Exception Summary:

Modified MethodM:

The reported value is estimated due to the presence of interference.E1 :Recovery in the associated laboratory sample (LCS) exceeds the upper control limit. Results may be biased high.L+ :

T104704518-15-3 (TX)Accreditation Number(s):

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-610.15 (10/09/13) RSN: 68109-150608132534

Page 336: Baseline Environmental Assessment for Riverside Park

Cold Vapor Atomic Absorption Spectrometry

Quality Control Report

PM15F03DPreparation Batch: 06/03/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PM15F03D1 of 1

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Mercury U 50 196 200 98 85 - 115 MB-7 LCS-7

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-7 06/04/15 13:53M615F04ALCS-7 06/04/15 13:55M615F04A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PM15F03D-150608135613

Page 337: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F02A1 of 1

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acenaphthene U 330 4,025 5,333 75 50 - 114 MB-2 LCS-2.2 Acenaphthylene U 330 4,050 5,333 76 53 - 115 MB-2 LCS-2.3 Anthracene U 330 3,862 5,333 72 48 - 119 MB-2 LCS-2.4 Benzo(a)anthracene U 330 4,152 5,333 78 56 - 120 MB-2 LCS-2.5 Benzo(a)pyrene U 330 4,321 5,333 81 57 - 122 MB-2 LCS-2.6 Benzo(b)fluoranthene U 330 4,274 5,333 80 50 - 131 MB-2 LCS-2.7 Benzo(ghi)perylene U 330 4,107 5,333 77 41 - 132 MB-2 LCS-2.8 Benzo(k)fluoranthene U 330 4,321 5,333 81 39 - 137 MB-2 LCS-2.9 Chrysene U 330 4,360 5,333 82 53 - 124 MB-2 LCS-2.10 Dibenzo(a,h)anthracene U 330 4,265 5,333 80 53 - 126 MB-2 LCS-2.11 Fluoranthene U 330 4,473 5,333 84 48 - 135 MB-2 LCS-2.12 Fluorene U 330 4,195 5,333 79 49 - 126 MB-2 LCS-2.13 Indeno(1,2,3-cd)pyrene U 330 4,402 5,333 83 51 - 132 MB-2 LCS-2.14 2-Methylnaphthalene U 330 3,744 5,333 70 46 - 105 MB-2 LCS-2.15 Phenanthrene U 330 3,939 5,333 74 53 - 119 MB-2 LCS-2.16 Pyrene U 330 4,024 5,333 75 55 - 127 MB-2 LCS-2

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 2-Fluorobiphenyl(S) 4,048 3,951 5,333 74 49 - 1155,333 76 MB-2 LCS-2.2 4-Terphenyl-d14(S) 4,488 4,432 5,333 83 48 - 1175,333 84 MB-2 LCS-2.3 1-Fluoronaphthalene(S) 4,164 4,087 5,333 77 46 - 1145,333 78 MB-2 LCS-2

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-2 06/02/15 13:35S115F02ALCS-2 06/02/15 14:23S115F02A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F02A-150608135613

Page 338: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F02APreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F02A1 of 1

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Aroclor-1016 U 100 1,056 1,333 79 60 - 122 MB-3 LCS-3.2 Aroclor-1260 U 100 1,102 1,333 83 70 - 131 MB-3 LCS-3

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Decachlorobiphenyl-PCB(S) 50.6 54.8 66.7 82 40 - 14366.7 76 MB-3 LCS-3.2 2,4,5,6-Tetrachloro-m-xylene-PCB(S) 49.3 48.8 66.7 73 42 - 13366.7 74 MB-3 LCS-3

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-3 06/02/15 14:10SA15F02BLCS-3 06/02/15 14:29SA15F02B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F02A-150608135613

Page 339: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F04DPreparation Batch: 06/04/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F04D1 of 2

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acenaphthene U 330 3,162 5,333 59 50 - 114 MB-9 LCS-8.2 Acenaphthene U 330 3,162 5,333 59 50 - 114 MB-8 LCS-8.3 Acenaphthylene U 330 3,311 5,333 62 53 - 115 MB-8 LCS-8.4 Acenaphthylene U 330 3,311 5,333 62 53 - 115 MB-9 LCS-8.5 Anthracene U 330 3,608 5,333 68 48 - 119 MB-8 LCS-8.6 Anthracene U 330 3,608 5,333 68 48 - 119 MB-9 LCS-8.7 Benzo(a)anthracene U 330 3,531 5,333 66 56 - 120 MB-9 LCS-8.8 Benzo(a)anthracene U 330 3,531 5,333 66 56 - 120 MB-8 LCS-8.9 Benzo(a)pyrene U 330 3,981 5,333 75 57 - 122 MB-8 LCS-8.10 Benzo(a)pyrene U 330 3,981 5,333 75 57 - 122 MB-9 LCS-8.11 Benzo(b)fluoranthene U 330 3,937 5,333 74 50 - 131 MB-8 LCS-8.12 Benzo(b)fluoranthene U 330 3,937 5,333 74 50 - 131 MB-9 LCS-8.13 Benzo(ghi)perylene U 330 3,636 5,333 68 41 - 132 MB-8 LCS-8.14 Benzo(ghi)perylene U 330 3,636 5,333 68 41 - 132 MB-9 LCS-8.15 Benzo(k)fluoranthene U 330 3,800 5,333 71 39 - 137 MB-8 LCS-8.16 Benzo(k)fluoranthene U 330 3,800 5,333 71 39 - 137 MB-9 LCS-8.17 Chrysene U 330 3,430 5,333 64 53 - 124 MB-9 LCS-8.18 Chrysene U 330 3,430 5,333 64 53 - 124 MB-8 LCS-8.19 Dibenzo(a,h)anthracene U 330 3,485 5,333 65 53 - 126 MB-8 LCS-8.20 Dibenzo(a,h)anthracene U 330 3,485 5,333 65 53 - 126 MB-9 LCS-8.21 Fluoranthene U 330 3,321 5,333 62 48 - 135 MB-8 LCS-8.22 Fluoranthene U 330 3,321 5,333 62 48 - 135 MB-9 LCS-8.23 Fluorene U 330 3,324 5,333 62 49 - 126 MB-9 LCS-8.24 Fluorene U 330 3,324 5,333 62 49 - 126 MB-8 LCS-8.25 Indeno(1,2,3-cd)pyrene U 330 3,934 5,333 74 51 - 132 MB-8 LCS-8.26 Indeno(1,2,3-cd)pyrene U 330 3,934 5,333 74 51 - 132 MB-9 LCS-8.27 2-Methylnaphthalene U 330 3,017 5,333 57 46 - 105 MB-8 LCS-8.28 2-Methylnaphthalene U 330 3,017 5,333 57 46 - 105 MB-9 LCS-8.29 Phenanthrene U 330 3,390 5,333 64 53 - 119 MB-8 LCS-8.30 Phenanthrene U 330 3,390 5,333 64 53 - 119 MB-9 LCS-8.31 Pyrene U 330 3,968 5,333 74 55 - 127 MB-9 LCS-8.32 Pyrene U 330 3,968 5,333 74 55 - 127 MB-8 LCS-8

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F04D-150608135613

Page 340: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Semivolatiles)

Quality Control Report

PS15F04DPreparation Batch: 06/04/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PS15F04D2 of 2

Batch ID:Page:Date: 06/08/15

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 2-Fluorobiphenyl(S) 3,613 2,871 5,333 54 49 - 1155,333 68 MB-9 LCS-8.2 4-Terphenyl-d14(S) 4,439 3,710 5,333 70 48 - 1175,333 83 MB-9 LCS-8.3 1-Fluoronaphthalene(S) 3,716 2,784 5,333 52 46 - 1145,333 70 MB-9 LCS-8

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-9 06/05/15 11:10S515F05AMB-8 06/04/15 14:11S715F04ALCS-8 06/04/15 15:00S715F04A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PS15F04D-150608135613

Page 341: Baseline Environmental Assessment for Riverside Park

Inductively Coupled Plasma - Mass Spectrometry

Quality Control Report

PT15F03DPreparation Batch: 06/03/15Preparation Date:

Soil/Solid

Preparation Batch QC Summary

PT15F03D1 of 1

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Arsenic U 100 10,275 10,000 103 85 - 115 MB-5 LCS-6.2 Barium U 1000 48,361 50,000 97 85 - 115 MB-5 LCS-6.3 Cadmium U 50 10,225 10,000 102 85 - 115 MB-5 LCS-6.4 Chromium U 500 18,386 20,000 92 85 - 115 MB-5 LCS-6.5 Copper U 1000 20,259 20,000 101 85 - 115 MB-5 LCS-6.6 Lead U 1000 20,071 20,000 100 85 - 115 MB-5 LCS-6.7 Selenium U 200 9,827 10,000 98 85 - 115 MB-5 LCS-6.8 Silver U 100 9,725 10,000 97 85 - 115 MB-5 LCS-6.9 Zinc U 1000 49,119 50,000 98 85 - 115 MB-5 LCS-6

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-5 06/03/15 16:13T415F03ALCS-6 06/03/15 16:15T415F03A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: PT15F03D-150608135613

Page 342: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F01BPreparation Batch: 06/01/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F01B1 of 2

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acetone U 1000 3,635 5,000 73 70 - 150 2074 1 MB-1 LCS-1 LCD-1.2 Acrylonitrile U 100 5,428 5,000 109 70 - 134 20108 1 MB-1 LCS-1 LCD-1.3 Benzene U 50 4,915 5,000 98 70 - 134 20100 2 MB-1 LCS-1 LCD-1.4 Bromobenzene U 100 4,973 5,000 99 70 - 134 20100 1 MB-1 LCS-1 LCD-1.5 Bromochloromethane U 100 5,436 5,000 109 70 - 134 20109 0 MB-1 LCS-1 LCD-1.6 Bromodichloromethane U 100 5,499 5,000 110 70 - 134 20111 1 MB-1 LCS-1 LCD-1.7 Bromoform U 100 4,237 5,000 85 70 - 134 2085 0 MB-1 LCS-1 LCD-1.8 Bromomethane U 200 5,474 5,000 109 70 - 134 20110 1 MB-1 LCS-1 LCD-1.9 2-Butanone U 750 5,164 5,000 103 70 - 150 20102 1 MB-1 LCS-1 LCD-1.10 n-Butylbenzene U 50 4,748 5,000 95 70 - 134 2093 2 MB-1 LCS-1 LCD-1.11 sec-Butylbenzene U 50 5,050 5,000 101 70 - 134 20100 1 MB-1 LCS-1 LCD-1.12 tert-Butylbenzene U 50 5,072 5,000 101 70 - 134 20102 1 MB-1 LCS-1 LCD-1.13 Carbon Disulfide U 250 6,720 5,000 134 70 - 134 20135 1 MB-1 LCS-1 LCD-1.14 Carbon Tetrachloride U 50 5,509 5,000 110 70 - 134 20112 2 MB-1 LCS-1 LCD-1.15 Chlorobenzene U 50 4,636 5,000 93 70 - 134 2094 1 MB-1 LCS-1 LCD-1.16 Chloroethane U 250 4,580 5,000 92 70 - 134 2094 2 MB-1 LCS-1 LCD-1.17 Chloroform U 50 5,239 5,000 105 75 - 134 20106 1 MB-1 LCS-1 LCD-1.18 Chloromethane U 250 4,692 5,000 94 70 - 134 2096 2 MB-1 LCS-1 LCD-1.19 2-Chlorotoluene U 50 4,720 5,000 94 70 - 134 20100 6 MB-1 LCS-1 LCD-1.20 Dibromochloromethane U 100 4,689 5,000 94 70 - 134 2095 1 MB-1 LCS-1 LCD-1.21 1,2-Dibromo-3-chloropropane U 50 4,014 5,000 80 70 - 134 2081 1 MB-1 LCS-1 LCD-1.22 Dibromomethane U 250 5,121 5,000 102 70 - 134 20103 1 MB-1 LCS-1 LCD-1.23 1,2-Dichlorobenzene U 100 4,637 5,000 93 70 - 134 2094 1 MB-1 LCS-1 LCD-1.24 1,3-Dichlorobenzene U 100 4,721 5,000 94 70 - 134 2095 1 MB-1 LCS-1 LCD-1.25 1,4-Dichlorobenzene U 100 4,212 5,000 84 70 - 134 2085 1 MB-1 LCS-1 LCD-1.26 Dichlorodifluoromethane U 250 5,349 5,000 107 70 - 134 20111 4 MB-1 LCS-1 LCD-1.27 1,1-Dichloroethane U 50 5,084 5,000 102 70 - 134 20103 1 MB-1 LCS-1 LCD-1.28 1,2-Dichloroethane U 50 4,900 5,000 98 70 - 134 2099 1 MB-1 LCS-1 LCD-1.29 1,1-Dichloroethene U 50 5,692 5,000 114 75 - 134 20117 3 MB-1 LCS-1 LCD-1.30 cis-1,2-Dichloroethene U 50 5,277 5,000 106 70 - 134 20108 2 MB-1 LCS-1 LCD-1.31 trans-1,2-Dichloroethene U 50 5,300 5,000 106 70 - 134 20108 2 MB-1 LCS-1 LCD-1.32 1,2-Dichloropropane U 50 4,975 5,000 99 75 - 134 20102 3 MB-1 LCS-1 LCD-1.33 cis-1,3-Dichloropropene U 50 4,588 5,000 92 70 - 134 2092 0 MB-1 LCS-1 LCD-1.34 trans-1,3-Dichloropropene U 50 4,420 5,000 88 70 - 134 2088 0 MB-1 LCS-1 LCD-1.35 Ethylbenzene U 50 4,973 5,000 99 75 - 134 20101 2 MB-1 LCS-1 LCD-1.36 Ethylene Dibromide U 50 5,009 5,000 100 70 - 134 20102 2 MB-1 LCS-1 LCD-1.37 2-Hexanone U 2500 4,072 5,000 81 70 - 150 2083 2 MB-1 LCS-1 LCD-1.38 Isopropylbenzene U 250 4,985 5,000 100 70 - 134 20101 1 MB-1 LCS-1 LCD-1.39 Methylene Chloride U 100 5,007 5,000 100 70 - 134 20102 2 MB-1 LCS-1 LCD-1.40 4-Methyl-2-pentanone U 2500 4,650 5,000 93 70 - 134 2095 2 MB-1 LCS-1 LCD-1.41 MTBE U 250 4,138 5,000 83 70 - 134 2084 1 MB-1 LCS-1 LCD-1.42 Naphthalene U 330 4,572 5,000 91 70 - 134 2093 2 MB-1 LCS-1 LCD-1.43 n-Propylbenzene U 100 5,124 5,000 102 70 - 134 20103 1 MB-1 LCS-1 LCD-1.44 Styrene U 50 5,432 5,000 109 70 - 134 20109 0 MB-1 LCS-1 LCD-1.45 1,1,1,2-Tetrachloroethane U 100 5,104 5,000 102 70 - 134 20105 3 MB-1 LCS-1 LCD-1.46 1,1,2,2-Tetrachloroethane U 50 4,822 5,000 96 70 - 134 2086 11 MB-1 LCS-1 LCD-1.47 Tetrachloroethene U 50 4,658 5,000 93 70 - 134 2096 3 MB-1 LCS-1 LCD-1.48 Toluene U 50 4,866 5,000 97 75 - 134 2099 2 MB-1 LCS-1 LCD-1.49 1,2,4-Trichlorobenzene U 330 4,264 5,000 85 70 - 134 2085 0 MB-1 LCS-1 LCD-1.50 1,1,1-Trichloroethane U 50 5,422 5,000 108 70 - 134 20110 2 MB-1 LCS-1 LCD-1.51 1,1,2-Trichloroethane U 50 4,931 5,000 99 70 - 134 2099 0 MB-1 LCS-1 LCD-1

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F01B-150608135613

Page 343: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F01BPreparation Batch: 06/01/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F01B2 of 2

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.52 Trichloroethene U 50 5,073 5,000 101 70 - 134 20104 3 MB-1 LCS-1 LCD-1.53 Trichlorofluoromethane U 100 5,453 5,000 109 70 - 134 20112 3 MB-1 LCS-1 LCD-1.54 1,2,3-Trichloropropane U 100 4,798 5,000 96 70 - 134 2097 1 MB-1 LCS-1 LCD-1.55 1,2,3-Trimethylbenzene U 100 4,869 5,000 97 70 - 134 2097 0 MB-1 LCS-1 LCD-1.56 1,2,4-Trimethylbenzene U 100 4,835 5,000 97 70 - 134 2097 0 MB-1 LCS-1 LCD-1.57 1,3,5-Trimethylbenzene U 100 5,038 5,000 101 70 - 134 20102 1 MB-1 LCS-1 LCD-1.58 Vinyl Chloride U 40 5,163 5,000 103 75 - 134 20108 5 MB-1 LCS-1 LCD-1.59 m&p-Xylene U 100 10,314 10,000 103 70 - 134 20104 1 MB-1 LCS-1 LCD-1.60 o-Xylene U 50 5,349 5,000 107 70 - 134 20108 1 MB-1 LCS-1 LCD-1

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 5,481 5,548 5,000 111 75 - 125 20110 15,000 110 MB-1 LCS-1 LCD-1.2 1,2-Dichloroethane-d4(S) 5,147 5,084 5,000 102 62 - 134 20101 15,000 103 MB-1 LCS-1 LCD-1.3 Toluene-d8(S) 5,086 5,104 5,000 102 50 - 150 20102 05,000 102 MB-1 LCS-1 LCD-1.4 4-Bromofluorobenzene(S) 4,943 5,126 5,000 103 64 - 136 20103 05,000 99 MB-1 LCS-1 LCD-1

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:36 PM

MB-1 06/01/15 13:39VH15F01BLCS-1 06/01/15 11:52VH15F01BLCD-1 06/01/15 12:19VH15F01B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F01B-150608135613

Page 344: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02BPreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02B1 of 2

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Acetone U 1000 3,853 5,000 77 70 - 150 2074 4 MB-4 LCS-4 LCD-2.2 Acrylonitrile U 100 5,555 5,000 111 70 - 134 20109 2 MB-4 LCS-4 LCD-2.3 Benzene U 50 4,964 5,000 99 70 - 134 2099 0 MB-4 LCS-4 LCD-2.4 Bromobenzene U 100 4,988 5,000 100 70 - 134 2099 1 MB-4 LCS-4 LCD-2.5 Bromochloromethane U 100 5,196 5,000 104 70 - 134 20101 3 MB-4 LCS-4 LCD-2.6 Bromodichloromethane U 100 5,486 5,000 110 70 - 134 20108 2 MB-4 LCS-4 LCD-2.7 Bromoform U 100 4,250 5,000 85 70 - 134 2084 1 MB-4 LCS-4 LCD-2.8 Bromomethane U 200 5,876 5,000 118 70 - 134 20116 2 MB-4 LCS-4 LCD-2.9 2-Butanone U 750 5,026 5,000 101 70 - 150 2098 3 MB-4 LCS-4 LCD-2.10 n-Butylbenzene U 50 4,728 5,000 95 70 - 134 2093 2 MB-4 LCS-4 LCD-2.11 sec-Butylbenzene U 50 4,884 5,000 98 70 - 134 2096 2 MB-4 LCS-4 LCD-2.12 tert-Butylbenzene U 50 4,895 5,000 98 70 - 134 2097 1 MB-4 LCS-4 LCD-2.13 Carbon Disulfide U 250 6,296 5,000 126 70 - 134 20126 0 MB-4 LCS-4 LCD-2.14 Carbon Tetrachloride U 50 5,454 5,000 109 70 - 134 20108 1 MB-4 LCS-4 LCD-2.15 Chlorobenzene U 50 4,726 5,000 95 70 - 134 2094 1 MB-4 LCS-4 LCD-2.16 Chloroethane U 250 5,032 5,000 101 70 - 134 2099 2 MB-4 LCS-4 LCD-2.17 Chloroform U 50 5,019 5,000 100 75 - 134 2099 1 MB-4 LCS-4 LCD-2.18 Chloromethane U 250 5,634 5,000 113 70 - 134 20111 2 MB-4 LCS-4 LCD-2.19 2-Chlorotoluene U 50 4,673 5,000 93 70 - 134 2097 4 MB-4 LCS-4 LCD-2.20 Dibromochloromethane U 100 4,683 5,000 94 70 - 134 2092 2 MB-4 LCS-4 LCD-2.21 1,2-Dibromo-3-chloropropane U 50 4,514 5,000 90 70 - 134 2084 7 MB-4 LCS-4 LCD-2.22 Dibromomethane U 250 5,243 5,000 105 70 - 134 20103 2 MB-4 LCS-4 LCD-2.23 1,2-Dichlorobenzene U 100 4,749 5,000 95 70 - 134 2093 2 MB-4 LCS-4 LCD-2.24 1,3-Dichlorobenzene U 100 4,667 5,000 93 70 - 134 2091 2 MB-4 LCS-4 LCD-2.25 1,4-Dichlorobenzene U 100 4,288 5,000 86 70 - 134 2085 1 MB-4 LCS-4 LCD-2.26 Dichlorodifluoromethane U 250 7,296 5,000 146 70 - 134 * 20144 1 MB-4 LCS-4 LCD-2.27 1,1-Dichloroethane U 50 4,958 5,000 99 70 - 134 2098 1 MB-4 LCS-4 LCD-2.28 1,2-Dichloroethane U 50 4,941 5,000 99 70 - 134 2097 2 MB-4 LCS-4 LCD-2.29 1,1-Dichloroethene U 50 5,220 5,000 104 75 - 134 20103 1 MB-4 LCS-4 LCD-2.30 cis-1,2-Dichloroethene U 50 5,066 5,000 101 70 - 134 20100 1 MB-4 LCS-4 LCD-2.31 trans-1,2-Dichloroethene U 50 5,045 5,000 101 70 - 134 20101 0 MB-4 LCS-4 LCD-2.32 1,2-Dichloropropane U 50 5,148 5,000 103 75 - 134 20101 2 MB-4 LCS-4 LCD-2.33 cis-1,3-Dichloropropene U 50 4,514 5,000 90 70 - 134 2088 2 MB-4 LCS-4 LCD-2.34 trans-1,3-Dichloropropene U 50 4,544 5,000 91 70 - 134 2090 1 MB-4 LCS-4 LCD-2.35 Ethylbenzene U 50 5,069 5,000 101 75 - 134 20100 1 MB-4 LCS-4 LCD-2.36 Ethylene Dibromide U 50 5,290 5,000 106 70 - 134 20105 1 MB-4 LCS-4 LCD-2.37 2-Hexanone U 2500 4,049 5,000 81 70 - 150 2077 5 MB-4 LCS-4 LCD-2.38 Isopropylbenzene U 250 4,982 5,000 100 70 - 134 2099 1 MB-4 LCS-4 LCD-2.39 Methylene Chloride U 100 4,648 5,000 93 70 - 134 2092 1 MB-4 LCS-4 LCD-2.40 4-Methyl-2-pentanone U 2500 5,072 5,000 101 70 - 134 2098 3 MB-4 LCS-4 LCD-2.41 MTBE U 250 4,726 5,000 95 70 - 134 2095 0 MB-4 LCS-4 LCD-2.42 Naphthalene U 330 4,837 5,000 97 70 - 134 2094 3 MB-4 LCS-4 LCD-2.43 n-Propylbenzene U 100 4,897 5,000 98 70 - 134 2097 1 MB-4 LCS-4 LCD-2.44 Styrene U 50 5,412 5,000 108 70 - 134 20107 1 MB-4 LCS-4 LCD-2.45 1,1,1,2-Tetrachloroethane U 100 5,217 5,000 104 70 - 134 20104 0 MB-4 LCS-4 LCD-2.46 1,1,2,2-Tetrachloroethane U 50 4,217 5,000 84 70 - 134 2088 5 MB-4 LCS-4 LCD-2.47 Tetrachloroethene U 50 4,741 5,000 95 70 - 134 2093 2 MB-4 LCS-4 LCD-2.48 Toluene U 50 4,920 5,000 98 75 - 134 2097 1 MB-4 LCS-4 LCD-2.49 1,2,4-Trichlorobenzene U 330 4,252 5,000 85 70 - 134 2083 2 MB-4 LCS-4 LCD-2.50 1,1,1-Trichloroethane U 50 5,096 5,000 102 70 - 134 20101 1 MB-4 LCS-4 LCD-2.51 1,1,2-Trichloroethane U 50 4,884 5,000 98 70 - 134 2096 2 MB-4 LCS-4 LCD-2

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02B-150608135613

Page 345: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F02BPreparation Batch: 06/02/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F02B2 of 2

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.52 Trichloroethene U 50 5,298 5,000 106 70 - 134 20105 1 MB-4 LCS-4 LCD-2.53 Trichlorofluoromethane U 100 5,750 5,000 115 70 - 134 20113 2 MB-4 LCS-4 LCD-2.54 1,2,3-Trichloropropane U 100 5,065 5,000 101 70 - 134 2097 4 MB-4 LCS-4 LCD-2.55 1,2,3-Trimethylbenzene U 100 4,709 5,000 94 70 - 134 2093 1 MB-4 LCS-4 LCD-2.56 1,2,4-Trimethylbenzene U 100 5,003 5,000 100 70 - 134 2099 1 MB-4 LCS-4 LCD-2.57 1,3,5-Trimethylbenzene U 100 4,939 5,000 99 70 - 134 2097 2 MB-4 LCS-4 LCD-2.58 Vinyl Chloride U 40 6,033 5,000 121 75 - 134 20120 1 MB-4 LCS-4 LCD-2.59 m&p-Xylene U 100 10,359 10,000 104 70 - 134 20103 1 MB-4 LCS-4 LCD-2.60 o-Xylene U 50 5,230 5,000 105 70 - 134 20104 1 MB-4 LCS-4 LCD-2

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 5,062 5,071 5,000 101 75 - 125 20101 05,000 101 MB-4 LCS-4 LCD-2.2 1,2-Dichloroethane-d4(S) 5,080 5,022 5,000 100 62 - 134 2099 15,000 102 MB-4 LCS-4 LCD-2.3 Toluene-d8(S) 5,051 5,075 5,000 102 50 - 150 20101 15,000 101 MB-4 LCS-4 LCD-2.4 4-Bromofluorobenzene(S) 4,915 5,118 5,000 102 64 - 136 20103 15,000 98 MB-4 LCS-4 LCD-2

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:37 PM

MB-4 06/03/15 02:56VH15F02BLCS-4 06/03/15 00:15VH15F02BLCD-2 06/03/15 00:42VH15F02B

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F02B-150608135613

Page 346: Baseline Environmental Assessment for Riverside Park

Gas Chromatography - Mass Spectrometry (Volatiles)

Quality Control Report

VH15F03APreparation Batch: 06/03/15Preparation Date:

Soil/Solid

Preparation Batch QC SummaryVH15F03A1 of 1

Batch ID:Page:Date: 06/08/15

MB LCS LCDQRPD UCLRec.

% % Q%Result RL

Parameter %%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kgµg/kgµg/kgµg/kg.1 Naphthalene U 330 4,549 5,000 91 70 - 134 2089 2 MB-6 LCS-5 LCD-3

Exception Summary:

Exceptions have been properly noted on reported results or affected samples have been scheduled for reanalysis when appropriate.

Report Generated By:

Run Code (Analysis Sequence/Run Time):Definitions/ Qualifiers:

The analyte was not detected at or above the Reporting Limit (RL).Value reported is outside QC limits

U:*:

%Rec.SpikeSystem Monitoring Compounds

(Surrogates): MB LCS LCDQRPD UCLRec.

% % Q%Result

%%SpikeResult

QRec. LCL - UCL

Laboratory Control Sample (LCS)Method Blank (MB) LCS Duplicate (LCD) Run Code

µg/kg µg/kg µg/kg µg/kg.1 Dibromofluoromethane(S) 4,986 5,116 5,000 102 75 - 125 20101 15,000 100 MB-6 LCS-5 LCD-3.2 1,2-Dichloroethane-d4(S) 5,022 4,967 5,000 99 62 - 134 2098 15,000 100 MB-6 LCS-5 LCD-3.3 Toluene-d8(S) 5,031 5,056 5,000 101 50 - 150 20100 15,000 101 MB-6 LCS-5 LCD-3.4 4-Bromofluorobenzene(S) 4,991 5,070 5,000 101 64 - 136 20102 15,000 100 MB-6 LCS-5 LCD-3

Monday, June 08, 2015

Amanda PetrovskyClient Services Representative

1:56:37 PM

MB-6 06/03/15 16:16VH15F03ALCS-5 06/03/15 14:01VH15F03ALCD-3 06/03/15 14:28VH15F03A

1914 Holloway Drive Holt, MI 48842 T: (517) 699-034511766 E. Grand River Brighton, MI 48116 T: (810) 220-33008660 S. Mackinaw Trail Cadillac, MI 49601 T: (231) 775-8368

[email protected]

F: (517) 699-0388F: (810) 220-3311F: (231) 775-8584

DCSID: G-6014.0 (09/08/14) RSN: VH15F03A-150608135613

Page 347: Baseline Environmental Assessment for Riverside Park
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ATTACHMENT IIISAMPLE EXCEEDANCE PLAN ; AND PLAT MAP

Page 353: Baseline Environmental Assessment for Riverside Park
Page 354: Baseline Environmental Assessment for Riverside Park