bsc(honors) syllabus for applied chemistry and chemical ... · salts.modern process for manufacture...

Syllabus for Applied Chemistry and Chemical Engineering

Noakhali Science and Technology University

Year 1 : Term I

Course No Name of Course Credit Hour Page

ACCE 1101 Chemical Technology I 3.0 4

ACCE 1103 Chemical Engineering I 3.0 4

ACCE 1105 Inorganic Chemistry I 3.0 5

ACCE 1107 Physical Chemistry I 3.0 5

ACCE 1102 Applied Chemistry and Chemical Engineering Lab-I 1.0 6

ACCE 1102 Oral 1.0

PHYS 1101 Physics -I 2.0 6

CSTE 1131 Computer Fundamentals 3.0 8

MATH1101 Differential and Integral Calculus 2.0 9

Total 21.0

Year 1 : Term II

ACCE 1201 Chemical Technology -II 3.0 10

ACCE 1203 Chemical Engineering -II 2.0 10

ACCE 1205 Physical Chemistry II 3.0 11

ACCE 1207 Organic Chemistry I 3.0 11

ACCE 1202 Applied Chemistry and Chemical Engineering Lab-II 1.0 12

ACCE 1204 Applied Chemistry and Chemical Engineering Lab-III 1.0

ACCE 1206 Field Work 1.0 12

ACCE 1208 Oral 1.0 12

PHYS 1201 Physics –II 2.0 13

MATH 1203 Ordinary and Partial Differential Equations 2.0 14

PHYS 1202 Physics Practical 1.0

Total 20.0

Year 2 : Term I

ACCE 2101 Chemical Technology –III 3.0 15

ACCE 2103 Fundamentals of Technological Processes 3.0 16

ACCE 2105 Chemical Engineering –III 2.0 16

ACCE 2107 Inorganic Chemistry-II 3.0 16

ACCE 2102 Applied Chemistry and Chemical Engineering Lab-IV 2.0 17

ACCE 2104 Applied Chemistry and Chemical Engineering Lab-V 1.0 17

ACCE 2106 Applied Chemistry and Chemical Engineering Lab-VI 1.0

ACCE 2108 Field Work 1.0 17

ACCE 2110 Oral 1.0

MATH 2105 Numerical Analysis, Laplace Transform & Fourier Analysis

2.0 20

Total 19.0

Year 2: Term II

ACCE 2201 Analytical Chemistry 3.0 20

ACCE 2203 Organic Chemistry-II 3.0 21

ACCE 2205 Basic Electrochemistry 3.0 22

ACCE 2207 Chemical Technology –IV 2.0 22

ACCE 2209 Chemical engineering –IV 3.0 22

ACCE 2211 Metallurgy 2.0 23

ACCE 2202 Applied Chemistry and Chemical Engineering Lab – VII 1.0 23

ACCE 2204 Applied Chemistry and Chemical Engineering Lab – VIII 1.0 23

ACCE 2206 Field work 1.0 23

ACCE 2206 Oral 1.0 23

MATH 2207 Vector Analysis, Matrices and Statistics 2.0 23

Total 23.0

Year 3 : Term I

ACCE 3101 Fuel Technology 3.0 24

ACCE 3103 Corrosion Engineering 3.0 25

ACCE 3105 Instrumental Methods of Analysis- I 3.0 25

ACCE 3107 Applied Electrochemistry 3.0 26

ACCE 3109 Material Science and Engineering 3.0 27

ACCE 3111 Chemical Technology –V 3.0 27

ACCE 3102 Applied Chemistry and Chemical Engineering Lab –IX 2.0 28

ACCE 3104 Applied Chemistry and Chemical Engineering Lab –X 2.0 28


ACCE 3108 Oral 1.0

Total 24.0

Year 3 : Term II

ACCE 3201 Instrumental Methods of Analysis -II 3.0 28

ACCE 3203 Instrumental Methods of analysis-III 3.0 29

ACCE 3205 Chemical Engineering -V 3.0 29

ACCE 3207 Pharmaceutical Process and Technology 3.0 29

ACCE 3209 Chemical Technology - VI 3.0 30

ACCE 3211 Industrial Economics, Psychology and Management 3.0 30

ACCE 3202 Applied Chemistry and Chemical Engineering Lab -XI 2.0 31

ACCE 3204 Applied Chemistry and Chemical Engineering Lab -XII 2.0 31


ACCE 3208 Oral 1.0 32

Total 24.0

Year 4 : Term I

ACCE 4101 Environmental Chemistry 3.0 32

ACCE 4103 Pharmaceutical Technology & Pharmaceutics 3.0 32

ACCE 4105 Chemical Technology -VII 3.0 33

ACCE 4107 Chemical Engineering -VI 3.0 34

ACCE 4102 Applied Chemistry and Chemical Engineering Lab-XIII 2.0 34

ACCE 4104 Applied Chemistry and Chemical Engineering Lab -

XIV

2.0 34

ACCE 4106 Oral 1.0

ACCE 4108 Project & Presentation-I 1 .0

Total 17.0

Year 4 : Term II

ACCE 4201 Environmental pollution and industrial waste

management 3.0 34

ACCE 4203 Chemical Technology-VIII 3.0 35

ACCE 4205 Chemical Engineering -VII 3.0 35

ACCE 4207 Nuclear and Radiation Chemistry 3.0

ACCE 4202 In plant Training 2.0 36

ACCE 4204 Oral 2.0 36

ACCE 4206 Project & Presentation-II 1 .0 36

Total 17.0

Grand Total 166.0

References: 37-40

ACCE: Applied Chemistry and Chemical Engineering

Detail Course Contents

Year 1 : Term I

ACCE 1101: Chemical Technology- I 3 CH

1. Introduction to Chemical Technology: Chemical Technology. Development of Chemical

Technology. Importance of Chemical Technology for industry. 2. Basic principles of chemical technology: Classification of Chemical technological processes.

Importance of chemical industry for sustainable development of Bangladesh

3. Design and implementation of a chemical project. Methods of carrying out a design project. Process development. Design information from literature. Techno-economic feasibility study.

Selection of size of plant, plant site, technology, raw materials, utility services..

4. Materials of construction: Metals, alloys, non-metals, inorganic materials and organic materials.

5. Sulphur and Sulphuric Acid: Sources of sulphur and other raw materials of the sulphuric acid

industries.Frasch process for mining sulphur. Sulphur recovery from sulphide and sulphate ores. Sulphur recovery from waste sulphuric acid and wastes of natural gas plants and fuel gas plants.

Details of the manufacture of sulphuric acid by the Chamber and the Contact processes. Utilization

of hydrogen sulphide, sulphur dioxide, sulphur wastes of sulphuric acid and carbon disulphide plants. Sulphuric acid industry in Bangladesh.

6. Nitrogen Industries: Importance of nitrogen industries. Methods of nitrogen fixation. Outlines of

proceses for manufacture of nitrogen oxides, cyanamide, ammonia, nitric acid, urea and ammonium salts.Modern process for manufacture of Ammonia,Urea,ammonium chloride and ammonium

sulphate.Ammonia oxidation and nitric acid manufacture.Nitrogen industries in Bangladesh.

7. Phosphorus Industries:Importance of Phosphorus industries.Basic principles of the industrial processes for the manufacture of elementary Phosphorus,Phosphorus pentoxide,Phosphoric acid and

other important phosphorus compounds.Details of the processes for the manufacture of SSP, TSP

and other phosphatic fertilizers. Phosphorus industries in Bangladesh

ACCE 1103: Chemical Engineering -I 2 CH

1. Unit process and unit operation: Definition, Difference, Industrial application, Mills, Factories

and Industries (Chemical industry and Process industry)

2. Scope of chemical engineering; Principles of chemical engineering calculations; Systems of units, process variables, basis of calculation; Study of process flow sheets.

3. Material balance: Overall and component balance; recycle and bypass; simple reactive

systems and combustion reactions; Material balances with and without chemical reactions. 4. Fuels and Combustion: Classification of fuels, Calorific value of fuels, Theoretical and excess

air for combustion, Calculations of solid, liquid and gaseous fuels.

5. Energy balance: Forms of energy and the First Law of thermodynamics; Thermodynamic data and tables; Energy balance involving change of phases; Heat capacities; Heat of formation and heat

of reaction - effects of temperature and pressure; Energy balances on chemical processes.

6. Calculations with Chemical Formulas and Equations: The mole concept, Molar

interpretation of a chemical equation, Amounts of substances in a chemical reaction, Limiting

reactant, Yields of products: Theoretical and actual, Molar concentration, Diluting solutions.

ACCE 1105: Inorganic Chemistry I 3 CH

1. Electronic Structure of Atom: Bohr's Atom Model, Wave Nature of Electrons, The

Photoelectric Effect, Quantum Numbers, Shapes of the Atomic Orbitals, Effective Nuclear

Charge, Energies of Orbitals, Aufbau Principle, Pauli Exclusion Principle, Hund's Rule, Electron and Ion Electron Configurations, Magnetic Properties of Atoms.

2. Periodic classification of elements : Periodic properties. Modern Periodic Table, Ionization

potential, Electron affinity, Electronegativity, Position of hydrogen, Inert gases, Lanthanides and Actinides in the Periodic table, Properties of different types of elements in the light of electronic

configuration.

3. Chemical Bonds: Electronic concept of chemical bonds, types of bonds. Elementary treatments of valence bond and molecular orbital theories, Geometry of molecules, Hybridization,

Bond order. Other types of chemical bonds. Shapes of molecules on the basis of Valance Shell

Electron Pair Repulsion Theory (VSEPRT).

4. Molecular Geometry and Chemical Bonding Theory: VSEPR model, Dipole moment and

molecular geometry, Valence bond theory. Hybrid orbitals. Description of multiple bonding,

Principles of molecular orbital theory, MO diagram, Molecular orbitals, HOMO and LUMO orbitals 5. Inorganic Thermodynamics and Energetics: Bond Energy Terms, Enthalpy, Entropy,

Thermodynamics of the formation of Ionic and Covalent Compounds, The Driving Force of a

Reaction, Lattice Energy, Born-Haber Cycle, Energy of Hydration, Energy Change of the Solution Process, Ionization Energies, Electronegativity, Electron Affinity.

6. Oxidation and reduction: Electronic concept. Oxidation state and oxidation number. Writing of

equations involving oxidation-reduction reactions, equivalent weights of oxidizing and reducing agents.

7. Acids and bases: Acid-base concepts, measuring of acid-base strength. Hard and soft acids and

bases.

ACCE 1107: Physical Chemistry I 3 CH

1. Behavior of ideal and real gases: Kinetic theory of gases, Joule-Thompson effect,equation of

state for veal gases, liquefaction of gases, Vander waals equation and the critical state, law of corresponding state, vapour pressure, Trouton's law. 2. The liquids: Intermolecular forces in liquids (London Forces, Hydrogen Bonding)vapour

Pressure and its determination, surface tension, Capillary action, Measurement of Surface Tension, Interfacial Tension, Surface Tension and Temperature,Viscosity and Fluidity, Measurement of

Viscosity, Viscosity and Temperature, Refractive Index (Specific refraction, Molar refraction),

Determination of Refractive Index, Optical Activity, Specific Rotation, Measurement of Optical Activity.

3. Solid state: Types of solids, Solid crystals, Miller indices, crystal structure, classification of

crystals on the basis of bonds, structure of metal crystal, crystal defects, liquid crystal, Band Theory of Solids, simple Inorganic Compounds.

4. Thermodynamics: Introduction, first law of thermodynamics, reversible and Irreversible

processes, isothermal and adiabatic changes. Second law of thermodynamics, Carnot theorem, Entropy and free energy. Gibbs-Helmholtz equation, Classius-Clapeyron equation,Third law of

thermodynamics.

5. Thermochemistry: Laws of thermochemistry. Hess's law, Kirchoffs equation. Heat of reaction. Heat of formation, Heat of solution, Heat of neutralization. Heat of combustion. Bond energies.

6. Solution : Type of solutions, Units of concentration. Solution of gas in liquid, Henry's law.

Solution of solid in liquid, solubility curve. Distribution law and its application. Solvent extraction. 7. Dilute Solutions: Theory of Dilute Solutions, ideal Solution, Raoults Law, Colligative

Properties:(I) Lowering of vapour pressure (II) Elevation of Boiling point(III) Depression of

freezing point (IV) Osmosis and Osmotic pressure. Molecular Weight from Colligative properties, ideal and nonideal Solution.

ACCE 1102: Applied Chemistry and Chemical Engineering Lab I 1 CH

Inorganic Qualitative Analysis: Systematic analysis of samples containing upto four, of the

following ions/ radicals:

Pb2+, Ag+, Hg22+, Hg2+

Cu2+, Cd2+, Bi3+, Sn2+, Sb3+

Fe3+ Fe2+, Cr3+, Al3+

Co2+, Ni2+, Mn2+, Zn2+ Ca2+, Ba2+, Sr2+, Mg2+, Na+, K+, NH4

+

Cl-. Br -, I-, NO3-, SO4

2- PO43-, S2-, CO3

2-, CH3COO-

ACCE 1104: Oral 1 CH

PHYS 1101: PHYSICS-I 2 CH

Coulomb’s Law; Electric field; Gauss’s Law and its application; Electric potential; Capacitors and capacitance: Capacitors with dielectrics, Dielectrics an atomic view, Charging and discharging of a

capacitor; Magnetic field: Magnetic induction, Magnetic force on a current carrying conductor,

Torque on a current carrying loop, Hall effect; Faraday’s Law of electromagnetic induction; Lenz’s Law; Self induction; Mutual induction; Magnetic properties of matter: Hysteresis curve; Maxwell

equations.

Simple Harmonic Motion: Differential equation of a Simple harmonic oscillator, Total energy and average energy, Combination of simple harmonic oscillations, Lissajous’ figures, spring- mass

system, Time period of torsional pendulum; Damped oscillation: Determination of damping co-

efficient; Forced oscillation: Resonance, Two-body oscillations, Reduced mass, Differential equation of a progressive wave, Power and intensity of wave motion; Stationary wave: Group velocity and

phase velocity; Doppler effect.

Electronic: Diodes, Transistors, Integrated Circuits, Introduction to PLC.

Books: 1. Physics Vol-1 & 2, by D. Halliday & R. Resnick, Wiley Eastern Private Ltd., New Delhi.

2. Fundamental of Physics, by D. Halliday, R. Resnick & J Walker, John Wiley & Sons, Asia,

PTE Ltd., Singapore. 3. Physics Vol. l & 2 by D. Halliday, R. Resnick & K. S Krane, John Wiley & Sons, Inc., NY.

4. Concept of Modern Physics by A Beiser, TATA McGraw-Hill Publishing Company Ltd., New

Delhi. 5. Physics for Engineers by B. L. Theraja, India

6. Foundations of Electromagnetic Theory by R. R. Reitz and F. J. Milford, Addison

Wesley Publishing Company, London.

CSTE 1131 : Computer Fundamentals 3 CH

Introduction: Brief history and types of computers, application areas; Working principle of a

computer system, Single and multi-user systems.

Organization and Architecture: Motherboards & Microprocessor; Memory units; Primary memory, Secondary memory; I:O Devices: peripheral devices, AT:XT, ISA, EISA, PCI bus architecture;

Computer network: Basic concepts of Internet systems, LAN and WAN; Gateway, bridge, router,

Internet protocol; Multimedia systems. Maintenance: Power supply stability, grounding effects of surge, sag current and its protection.

Classification of Stabilizer and UPS, Effect of static charge on computer devices; Handing of

computers cards, chips, computer viruses and protections, software troubleshooting and maintenance.

Software: Classifications system software, operating system concepts, importance, components and

basic functions of DOS, Windows and UNIX operating systems; Application software: Introduction

to word processing and spreadsheet analysis.

Application: Introduction to Database, Concepts of data base systems; some applications using MS

Access and SQL;

Books: Sl Authors Name Edition Publisher

1 C. S. Frence Computer science 6th Thomson Learning

2 L. Rosch Hardware Bible 6th Braddy Publishing 3 Peter Norton Inside the PC 6th SAMS

MATH1101 : Differential and Integral Calculus 2CH

Differential Calculus: Limits, continuity and differentiability; Successive differentiation of various types of functions; Leibnitz’s Theorem; Rolle’s Theorem; Mean value Theorem; Expansion of

functions; Evaluation of indeterminate forms by L’Hospitals rule; Partial differentiation; Euler's Theorem; Tangent and Normal; Maximum and minimum values of functions of single variable;

Curvature, Asymptotes.

Integral Calculus: Definitions of integration; Integration by the method of substitutions; Integration

by parts; Standard integrals; Integration by the method of successive reduction; Definite integrals

and its use in summing series; Walli’s formula, Improper integrals, Beta function and Gamma function; Area under a plane curve; Area of the region enclosed by two curves; Volume of solids of

revolution; multiple integrals and its application.

Books:

1 Calculus and Analytic geometry by Thomas:Finney, 6th Edition; Narosa publishing house.

2 Calculus; Advanced Calculus by Schaum’s Series, SI, metric, edition, McGraw-Hill Book

Company.

3 Differential Calculus and Integral Calculus by Das & Mukerjee; 3rd edition; S. Chand and

Company limited

Year 1 : Term II

ACCE 1201: Chemical Technology - II 3 CH

1. Ceramics: Raw material; Ceramic chemistry; Classification of ceramic products;Methods of manufacture; Glazing and Decorating of porcelain and stonewares; Firing methods and Kilns for

ceramic and whitewares; Special ceramic products including ceramic composites; Enamels.

2. Glass: Definition, composition and classification; methods of manufacture; Raw material and manufacturing steps; Glass furnaces and their operation; Special glasses.

3. Cement: Definition of cement and cementing; Basis of classification and types of cement;

Constituents and properties of cement; Strength of cement; Method of manufacture of ordinary and other types of portland cement; Cement kilns - their design and operation; Present status and future

prospects of ceramic, glass and cement industry in Bangladesh.

4.Water conditioning and water treatment: Sources and impurities of water and water quality. Physical and chemical methods of treatment. Desalination of water. Practical applications.

Municipal water supply. Boiler-feed water. Water for various industries. Sewage treatment and

disposal. Industrial waste water treatment.

ACCE 1203: Chemical Engineering -II 2 CH

1. Size reduction and size enlargement: Properties of particulate solids, particle size and shape,

mean diameters; Methods and equipments for crushing and grinding, power requirement; Screen analysis, analytical size distribution functions; Agglomeration, granulating and compacting.

2. Material handling: Solid handling machinery, Fluid moving machinery, Pumps and compressors;

Pressure relieving devices; pneumatic and fluidized conveying; Storage devices for solid, liquid and gas.

3. Process instrumentation, Process measurement and Process control: Instrument for measurement, recording and control of pressure, temperature,level,flow and concentrations. Measuring instruments for transport of liquids and solids. Computer control.

ACCE 1205 : Physical Chemistry II 3 CH

1. Rates of Reactions : Defining reaction rates, Experimental determination of rate. Rate equation:

rate constant and order. Integrated rate equations. Determination of rate equation: experimental methods. Temperature dependence of reaction rates: Arrhenius equation. Collision theory of reaction

rates: activation energy. Transition state. Mechanism of reactions: elementary reactions;

molecularity of elementary reactions. Application of law of mass action to elementary reactions.

Rate law and mechanism. Catalysis. Application of catalysis in industries.

2. Chemical Equilibria : Chemical equilibrium : dynamic equilibrium. The equilibrium constant, Heterogeneous equilibria, Solvents in homogeneous equilibria, Qualitative interpretation of the

equilibrium constant, Predicting the direction of reaction, Calculating equilibrium concentration, Le

Chatelier's principle : changing concentrations of reactants and products, changing pressure and temperature, Effect of a catalyst.

3. Acid-base Equilibria: Relative strengths of acids and bases, Molecular structure and acid

strength, Self ionization of water, Solutions of strong acids or bases, The pH of a solution. Acid ionization equilibria, Polyprotic acids, Base ionization equilibria, Acid-base properties of salt

solutions, Common ion effect, Buffers, Acid-base titration curves.

4. Solubility and Complex-ion Equilibria : The solubility product constant, Solubility and the common ion effect, Precipitation calculations, Effect of pH on solubility, Complex-ion formation,

Complex ion and solubility, Qualitative analysis of metal ions.

5. Electrochemistry : Redox reactions, Constructions of Voltaic cells, Notation for Voltaic cells, Electromotive force, Standard electrode potential, Nernst equation. Equilibrium constant and emf,

Commercial Voltaic cells. Electrolytic cells: Electrolysis of metal salts.

6. Phase Equilibria: Phase rule and its application to one and two component system (including

phase diagram for systems of two volatile liquids in which Baoult's law obeyed), partially miscible liquid pairs, upper and lower consolute temperature,principle of fractional distillation, Constant

boiling mixture, Eutectic, periteetic, Entutoid and perifeetoid reactions.

7. Colloids : General methods of preparation, classification and general properties of colloid. Electrokinetic phenomena and their analytical applications. Colloidal electrolytes, preparation,

specific properties and stability of emulsion. use of colloids and emulsion.

ACCE 1207: Organic Chemistry I 3 CH

1. Introduction: Nomenclature of organic compounds by IUPAC system. Functional group and

their importance.

2.Alkanes: Structure, Preparation, Manufacture and uses. Variation of physical properties with increasing chain length and branching, sp3 Hybridisation, Reactions of alkanes-Alkylation, Nitration,

Halogenation, Sulfonation, Cracking and Isomerisation.

3. Alkenes: Structure, cis/trans and E/Z-isomerism, Preparation, Manufacture and synthesis, Uses. sp2 Hybridization, Reactions such as hydrogenation, bromination, hydrohalogenation and ozonolysis

with their mechanisms, Addition reactions to unsymmetrical alkenes with detailed mechanism in

light of Markovnikov rule, Reaction of alkenes with KMnO4, OSO-4, Epoxidation, Polymerization of

alkenes.

4. Alkynes: Structure, Preparation, Manufacture and uses. sp- Hybridization, Acidic properties,

Reactions. 5. Aromatic hydrocarbons, Arenes : Structure and resonance of benzene, Aromaticity,

Electrophilic substitution in aromatic systems like alkylation, Acylation, Nitration etc.

6. Alkyl and Aryl Halides: Structure, Preparation, Manufacture and Uses. Comparison of

the C-X bond strength of alkyl and aryl halides, Comparison of substitution reaction of

alkylhalide and aryl halides, Synthesis of alkyl and aryl halides, Reaction of alkylhalides with alkali in different conditions, Reaction with metals to obtain Grignard reagents, Safety and Conditions for

the synthesis of Grignard reagent, Use of Grignard reagents to obtain various organic compounds,

Wurtz reaction. 7. Alcohols and Phenols: Structure, Preparation, Manufacture, Physical properties and Uses.

Differentiation of 1˚,2˚,3˚ alcohols, Test for the presence of -OH group, Reactions of alcohol and

Phenol including enolate alkylation. 8. Carbonyl compounds: Structure, Preparation, Manufacture, and Uses. Reactions of aldehyde and

ketones, Differentiting aldehyde from kelones, Orbital representation of C=O group and the

electrophilic character of the carbonyl compounds, Nucleophilic reacion of carbonyl compounds

with mechanisms, Oxidation, Reduction reactions, keto-enol tautomerism.

9.Carboxylic acids: Preparation, Properties, uses, Reactions of carboxylic acids to obtain acid

halides, acid anhydride and amides, comparison of reactivity of carboxylic acid and their derivatives. 10.Aliphatic and Aromatic Amines: Structure, Preparation, Manufacture, Properties and uses.

Quaternary amines, Diazotization of aromatic amines and their coupling to obtain diazocompounds

(dyes), Amino acids and proteins. 11.Heterocyclic compounds: Structure, Preparation, Manufacture, Properties and Uses of pyridine,

pyrole, furan, and thiophene. Synthesis of quinoline derivatives.

12.Cyclic compounds: Cyclopropane, cyclobutane Cyclopentane, Cyclohexane. Bayer- Strain theory, Sache-Mohr theory. Manufacture of aromatics from alicyclic compounds.

ACCE 1202: Applied Chemistry and Chemical Engineering Lab II 1 CH

Analysis of water

pH,Conductivity,TDS,TSS,Turbidity,m-alkalinity,p-alkalinity,metals, DO, Hardness, BOC,

COD.

ACCE 1204: Applied Chemistry and Chemical Engineering Lab III 1 CH

Organic Qualitative analysis: a. Detection of elements in organic compounds through Na-fusion

b. Determination of functional groups of organic samples.

c. Determination of physical constants such as m.p. and b.p. d. Identification of unknown organic compounds

e. Preparation of a suitable derivative of the sample under identification and determination

of the m.p.:b.p. of the derivative.

ACCE 1206: Field Work 1 CH


PHYS 1201: PHYSICS -II 2 CH

Theories of light: Interference of light, Young’s double slit experiment, Fresnel Bi-prism,

Interference at wedge shaped films, Newton’s rings, Interferometer; Diffraction of light: Fresnel and

Fraunhofer diffractions, Diffraction by single slit, Diffraction from a circular aperture, Resolving power of optical instruments, Diffraction at double slit and N-slits-diffraction grating; Polarization:

Production and analysis of polarized light, Brewster’s Law, Malus Law, Polarization by double

refraction, Retardation plates, Nicol prism, Optical activity, Polarimeters, Polartoids. Quantum theory of radiation: Photo-electric effect, Compton effect, Wave particle duality,

Interpretation of Bohr’s postulates; Radioactive disintegration; Properties of nucleus: Nuclear

reactions, Fission, Nuclear reactors.

MATH 1203 : Ordinary and Partial Differential Equations 2 CH

Ordinary Differential Equation, ODE: Degree and order of ordinary differential equations;

Formation of differential equations; Solution of first order differential equations by various methods; Solution of first order but higher degree ODEs; Solution of general linear equations of second and

higher orders with constant coefficients; Solution of homogeneous linear equations.

Partial Differential Equations, PDE: Rules for solving simultaneous equations of the form

;R

dz

Q

dy

P

dx Integral surfaces passing through a given curve, Nonlinear PDE of order one,

complete, particular, singular and general integrals: standard forms, Charpit's method; Second order

PDE: its nomenclature and classifications. Linear PDE with constant coefficients.

Books:

1 Differential Equations by H.T.H. Piaggio, Revised and enlarged edition; CBS publishers and

Distributors.

2 Differential Equations by Shapley L. Ross, 3rd edition; Blaisdell publishing company.

3 Advanced Differential Equations by M. D. Raisinghania, 8th edition; S. Chand and Company limited.

4 Ordinary and Partial Differential Equations by M. D. Raisinghania, Revised and enlarged edition; S. Chand and Company limited.

PHYS 1202: Physics Practical 2 CH

List of Experiments

1. Determination of the spring constant and the effective mass of a loaded spring.

Apparatus: A Spiral Spring, Convenient masses with hanging arrangement, Clamp or a hook attached to a rigid Framework of heavy metal rods, stopwatch, etc.

2. Determination of unknown resistances and verification of the laws of resistances by P.O Box.

Apparatus: Post Office Box, Galvanometer, Unknown resistances, Resistance, Connecting wires, Key, etc.

3. Comperison of EMF of two Cells.

Apparatus: Galvanometer, Potentiometer, Two cells, Battery, 6V, Connecting wires, Rheostat, 3 way key, etc.

4. Determination of the moment of inertia of a flywheel about its axis of rotation.

Apparatus: A flywheel with counter, thread, weight, etc.

5. Determination of rigidity modulus of the material of a wire by static method. Apparatus: Rigidity apparatus, Slide callipers, Screw gauge, Weights, Meter scale, Steel wires

etc.

6. Determination of the pressure-coefficient of air by Constant Volume Air Thermometer. Apparatus: Jolly’s thermometer, Hg-Barometer, Heating bath, Thermometers, Gas burner,

Stands and Clamps, etc.

7. Determination of the thermal conductivity of a bad conductor by Lee's method. Apparatus: Lec’s and Chorlton’s apparatus, Slide Callipers, Thermometers, Watch, Stands and

Clamps, Rubber tubes, etc.

8. To plot the thermo-electromotive force temperature, Calibration, curve for a given thermocouple.

Apparatus: Thermocouple, Resistance box, Potentiometer, Thermometer, Sensitive

Galvanometer, Wires, Ice, Water, Stands and Clamps, etc. 9. Determination of the melting point of a solid using the calibration curve obtained in

Experiment-8.

Apparatus: Thermocouple, Resistance box, Potentiometer, Sensitive Galvanometer, Wires, Solid, wax, Ice, Watch, beakers, etc.

10. Determination of mechanical equivalent of heat by electrical method.

Apparatus: Joule’s calorimeter, Voltmeter, Ammeter, Thermometer, Stopwatch, Connecting wires, balance, Stand and clamp, etc.

11. Determination of the focal length of i. a convex lens by displacement method and ii. a concave

lens by an auxiliary lens method. Apparatus: Optical bench, Convex lens, Concave lens, Screen, Index rod, Lamp, meter scale,

etc.

12. Determination of the refractive index of a liquid by plane mirror and a pin method using a

convex lens. Apparatus: A convex lens, Plane mirror, Pin, Spherometer, Slide Callipers, Stands and clamp,

Liquid, Water, etc.

13. Determination of the specific rotation of sugar solution by a Polarimeter. Apparatus: A Polarimeter or Sacharimeter, Sodium lamp, Sugar, Balance, Graduated cylinder,

Beaker, Filter paper, Thermometer, etc.

14. Measurement of the refractive index of the material of a prism with the help of a spectrometer. Apparatus: Spectrometer, Prism, sodium lamp arrangement, Spirit level, etc.

15. Determination of the radius of curvature of a plenoconvex lens by Newton’s method.

Apparatus: Newton’s Ring apparatus, Sodium lamp, Glass side, Stands and Clamps, etc.

Ref: Practical Physics for Degree students by Dr. Gias uddin Ahmad and Md. Shahbuddin

Year 2 : Term I

ACCE 2101: Chemical Technology -III 3 CH

1. Pulp and Paper Technology: Structural and Physical properties of pulpwood and other fibres

raw material, Chemistry of wood and fibres, preparation of pulpwood, manufacture of mechanical pulp, Bleaching mechanical pulp, Semi chemical, thermo chemical and chemi-mechanical pulping,

sulfite pulping, alkaline pulping, alkali recovery system, bleaching of wood pulps, treatment of pulp,

new pulping processes, solvent pulping, rag pulping, dissolving pulp.Wet processes, Foudriner machine, Jordan engine, dry process coated papers, speciality papers, re-use of waste paper,

structural board, Paper industry in Bangladesh.

2.Cellulosic fibres and fitness: Natural and synthetic fibres, Rayon and acetate, viscose manufacture, cellulose acetate manufacture, cuprammonium rayon, packaging fines, rayon industry

in Bangladesh.

3.Wood Chemicals: Hardwood distillation, naval stores, gum oleoresins, terpentines, sulphate pulp

rosin, tall oil, lignin, lignosulfates, hydrolysis of wood, wood extractives and conversion processes,

wood distillation.

4. Sugar Technology: Manufacture of sugar from sugar cane and sugar beet.Utilization of by products, miscellaneous sugars. Sugar industry in Bangladesh.

5. Starch Industry: Manufacture of starch, dextrin and dextrose, Manufacture from corn,

Miscellaneous starches, starch industry in Bangladesh.

ACCE 2103: Fundamentals of Technological Processes 3 CH

1. Thermodynamics: Estimation of thermodynamic properties; Heat effects: heat capacities of gases

as a function of temperature, heat capacities of solids and liquids; heat effects accompanying phase

change of pure substances; Effect of temperature on the standard heat of reaction.

2. Chemical Equilibrium: Homogeneous equilibria of some industrially important gas reactions.

Equilibria of parallel and consecutive reactions. Equilibria in non-ideal systems. Equilibria

calculations in industrial reactions. 3. Kinetics and mechanism: Reversible, consecutive, chain etc. reactions. Reactions in solution and

heterogeneous reactions. Kinetic models for non-elementary reactions; Testing kinetic models and

searching for a mechanism. 4. Catalysis: Characteristics of catalyzed reaction; Types of catalysis; Homogeneous and

heterogeneous catalysis; catalyst-inhibitors, reatardation and poisoning; Enzyme reactions.

5. Surface Chemistry: Absorption and desorption,Adsorption at gas-solid interface; Physical adsorption and chemisorption; Langmuir and BET isotherms; Adsorption from solution; Gibb's

adsorption isotherm.

6. Reactor Design: Classification of reactors; Ideal reactors; Space time and spacevelocity; Residence time; Distribution of fluids in vessels; Dispersion model; Principles of reactor design;

Design for single reactions and multiple reactions.

ACCE 2105: Chemical Engineering -III 2 CH

1. Fluid Mechanics: Fluid statics and manometry; Basic equation of hydrostatics and its practical application; Hydrostatic equilibrium; Differential equation of Euler; Fluid dynamics; Mechanism of

fluid flow; Distribution of velocities; Flow of fluids in closed conduits, laminar and turbulent flow,

Reynold’s number and its significance, friction factor, frictional losses in pipes and fittings, expansion contraction losses; Bernoulli theorem and its application; Differential equation of Euler

for fluid dynamics; viscosity; Poiseulle’s equation, motion in a viscous medium, determination of

coefficient of viscosity; Surface tension; surface tension as a molecular phenomenon, surface tension and surface energy, Capillarity and angle of contact, Quincke’s method. Fluid flow measuring

instruments. 2. Humidification operation: Theory; Humidity chart; Measurement of humidity; Adiabatic

saturation temperature and wet-bulb temperature; Calculation of humidification processes.

ACCE 2107: Inorganic Chemistry II 3 CH

1. Hydrogen : Occurrence, preparation and uses of hydrogen.Compounds of hydrogen.

2. Inert gases (elements of zero group): Isolation and industrial applications.

3. Group IA and IIA elements: Comparative study of the alkali and alkaline-earth metals. 4. Group III elements : Group properties of Boron, Aluminum,Gallium, Indium, Thallium.

5. Group IV elements : Carbon, Silicon, Germanium, Tin and Lead,

6. Chemistry of Group V elements : Nitrogen, Phosphorous, Arsenic, Antimony and Bismuth. 7. Group VI elements : Oxygen, Sulphur, Selenium, Tellurium & Pollonium.

8. Group VII elements : Fluorine, Chlorine, Bromine & Iodine and some of their important

compounds. 9. Organometallics : Metal carbonyls, metal nitrosyls. metallocenes, catalysis by organometallic

compounds.

10. Transition and inner transition elements : Electronic configuration and general characteristics, Occurrence, Positions in the periodic table, Magnetic properties, Metal to metal bond, Oxidation

states and EMFs of the transition and inner transition metals.

11. Coordination compounds : Werner's postulates, Coordination bond and the elector neutrality principle, Strengths and weaknesses of VBT, Crystal field stabilization energy and 10Dq, Weak field

case and strong field case, Octahedral and tetrahedral symmetry, Parings energies, Factors affecting

10 Dq , Octahedral versus tetrahedral coordination, 12. Bioinorganic chemistry : Biological significance of Fe, Zn, Cu, Mo, Co, Cr, V and Ni,

Reactions of Zn enzyme as biological catalyst, Functions of Na+, K+, Mg2+ and Ca2+ ions in humans,

Hemoglobin as an oxygen carrier, Dioxygen reactions in biological systems, Metals in medicine.

ACCE 2102: Applied Chemistry and chemical engineering Lab-IV 2 CH

1. Qualitative analysis involving samples of natural ores, Minerals, Metals and Alloys.

(i) Analysis of Industrial water for iron content

(ii) Analysis of lime in limestone (iii) Analysis of Urea, mineral ores and alloys.

(iv) Analysis of iron in iron ore and scrap iron.

(v) Estimation of calcium in gypsum. (vi) Analysis of Bauxite.

(viii) Quantitative separation and determination of:

(a) Cu (Volumetrically) and Ni (Gravimetrically)

(b) Fe (Volumetrically), Mn (Gravimetrically) and Zn (Gravimetrically)

ACCE 2104: Applied Chemistry and Chemical Engineering Lab-V 1 CH

1. Determination of heat of solution calorimetrically and by measuring solubility.

2. Determination of heat of neutralization of a strong base by a strong acid.

3. Determination of the radius of glycerine molecule from viscosity measurements.

4. Determination of partition co-efficient of iodine between water and carbon tetrachloride.

5. Determination of the equilibrium constant of the reaction KI + I2 KI3.

6. Determination of energy of activation of the reaction 5KBr + KBrO3 + 3H2SO4 = 3K2SO4 + 3Br2 + 3H2O

ACCE 2106: Applied Chemistry and Chemical Engineering Lab-VI 1 CH

1. Engineering drawing ACCE 2108: Field Work 1 CH


MATH 2105 : Numerical Analysis, Vector Analysis, Matrices 2 CH

Numerical Analysis: Interpolation, Newton's formulae for forward and backward interpolation.

Newton and Lagrange's interpolation formulae. Inverse interpolation, Newton's forward and

backward formulae. Numerical integration. Trapezoidal rule, Simpson's rule, Weddle's rule. Gauss's

quadrature formula. Legendre polynomials. Principles of least squares. Curve fitting. Solution

Newton-Raphson method, Convergence. Solution of ordinary first order differential equations by

Picard's and Euler's method. Runge-Kutta's methods for solving differential equations.

Vector Analysis: Scalar and vector product of two vectors and their geometrical interpretation;

Triple products and multiple products; Linear dependence and independence of vectors. Differentiation and integration of vectors; Line, surface and volume integrals. Gradient, divergence

and curl of point functions, Gauss’s theorem, Stoke’s theorem, Green’s theorem.

Matrices: Definition of matrix; Different types of matrices-, Algebra of matrices, Adjoint and

inverse of a matrix; Elementary transformations of matrices; Matrix polynomials; Caley-Hamilton

theory with uses of rank and nullity; Normal and canonical forms; Eigen values and eigenvectors.

Definition and properties of vector spaces, subspaces, basis and dimension, change of basis.

Books for Numerical analysis:

1 Numerical Mathematical Analysis by J. B. Scarborough, 3rd edition; John Hopkins Press.

2 Study guide for Numerical Analysis by R. L. Burden and J.D. Faires; Cole Publishing Company.

Books for Matrices and Vectors:

1 Elementary Linear Algebra by Anton Rorrers, 8th edition; John Wiley and sons Int.

2 College Linear Algebra by Md. Abdur Rahman, 3rd edition; Nahar book depot and publications.

3 Linear Algebra by Schaum’s Series, SI, metric, edition; McGraw-Hill Book Company.

4 Vector Analysis with Applications by A. K. Hazra, 3rd edition; Wiley Eastern Company limited.

5 Vector Analysis by M. D. Raisinghania, 3rd edition; S. Chand and Company limited.

Year 2 : Term II

ACCE 2201: Analytical Chemistry 3 CH

1. Errors in measurements : Random and systematic errors. Precision and accuracy. The Gaussian

distribution of deviations. Confidence limits. Propagation of errors. Signal to noise ratio. Sensitivity and detection limits.

2. Statistical Measurements: Frequency distribution; Mean, median, mode and other measures of

central tendency; Standard deviation and other measures of dispersion; Moments, Skewness and Kurtosis; Elementary probability theory and discontinuous probability distribution;

Characteristics of distributions; Hypothesis testing and regression analysis.

3. Sampling and sample preparation methodology : Cleaning of apparatus. Dissolution of samples. Wet and dry ashing procedures.

4. Analytical reagents : Reagents, Purification of substances, Preparation and storage of standard

solutions.

5. Gravimetric methods of analysis : Conditions for analytical precipitation. Digestion of

precipitates. Washing, filtration, drying and igniting the precipitate. Homogeneous

precipitation. 6. Electrogravimetry: Theory of electro-gravimetric analysis, Decomposition potential, electrode

reaction, Effect of con. on electrode potential, Overpotential, completeness of deposition,

Electrolytic deposition of metals, character of deposit. Electrolytic separation of metals with controlled cathode potential, Electrolytic determinations at constant current. Internal

electrolysis.

7. Volumetric methods of analysis : Suitability of a reaction for use in volumetric analysis. Oxidation-reduction titrations, precipitation titrations, redox indicators, adsorption indicators.

Complexometric analysis. Formation constants of complexes. Chelates. EDTA titrations.

Effect of pH on EDTA equilibria. Masking and demasking agents. Metal ion indicators. Potentionmetric and conductometric methods of end point determination.

ACCE 2203: Organic Chemistry-II 3 CH

1. Nucleophilic substitution addition and Elimination Reaction: Mechanism of SN1, SN2

reactions with clear demonstration of the intermediates, Substrate effect on SN1 SN2

reactions, of E1, E2, reactions with clear understanding of the substrate effect and reaction conditions.Electrophilic and Nucleophilic addition.

2. Free radicals mechanism:

Formation of radicals by homolytic fission of weak bonds, Free radical initiators such as

Peroxides and AIBN, Radical stability, Radical chain reactions, Use of tributyltinhydride in

free radical reactions.

3. Stereochemistry:

a) Geometric and optical isomerism, Concept of enantiomers, diostereomers, epimers, Racemic

mixture and its modification, Relative and Absolute configuration,Determination of R,S configuration, Chirality of allenes and bi-phenyls.

b) Conformation and conformers: Conformation of ethane, butane, cyclohexane and substituted

cyclohexane.

4. Carbohydrates:

Definition and classification of carbohydrates, Nomenclature, Open chain and ring structure of

glucose, Mutarotation, Chain increasing and shortening reactions of monosaccharides, Oxidation reactions, Osazone formation, Chemistry of disaccharides, Starch and cellulose with

reference to the type of linkages between the anhydroglucose units.

5. Unit processes:

The general reaction, reaction conditions and mechanisms of the following:

Friedel Crafts Alkylation and acylation reactions, Alcoholysis, Ammination, Condensation,

Polymerisation, Halogenation, Esterification, Diels Alder reaction.

6. Amino acids, Peptides and Proteins: Definition, sources and classification.

7. Lipids and Nucleic Acids: Definition, sources and importance.

8. Natural Products: Occurance and methods of isolation of alkaloids, terpenoids and steroids.

ACCE 2205: Basic Electrochemistry 3 CH

1.Conductrometry: The conductance of electrolytic solutions. Strong and weak electrolytes.

Measurement of electrolytic conductance. Specific conductance. Molar conductance. Influence of

concentration. Law of independent migration of ions. Ion conductance. Applications of conductance measurements. Mobility of ions. Methods for the determination of conductance. Conductance cells.

Transport numbers. Theory of strong electrolytes. Debye-Hueckel Limiting law. Determination of

activity coefficient. 2. Amperometry: Amperometric titrations, Methodology, Advantages of ampero-metric titration,

Technique of amperometric titrations with the dropping mercury electrode. Titration to zero current,

Biamperometric titrations. 3. Coulometry: General discussion, fundamental principles, coulometry at controlled potential, the

general technique. Colulometry at constant current: Coulometric titration: general discussion, the

principle of coulometric titration instrumentation. 4. Potentiometry: Introduction, reference electrodes, Indicator electrodes, Instrumentation and

measurement of cell e.m.f.,potentiometer and pH meter.Direct potentiometry potentiometric titraions

classical methods, Differential Potentiometric titrations, Some experimental details for potentiometric titration

5. Chemical source of electrical energy: Leclanche's cell, Lead accumulator, accumulators, silver-

zinc. Accumulator. Fuel cell, Classification fuel cell, oxygen-hydrogen fuel cell. 6. Reference electrode: Standard hydrogen electrode, Calomel electrode, silver chloride electrode.

7. Electro winning, Electro refining, Electroplating: Importance and general principles;

Electroplating of Ni, Cr, Cu, AL, brass, bronze etc.; Electro winning of Zn, Al, Mg and Na; Application of electro refining in metallurgy

ACCE 2207: Chemical Technology -IV 2 CH

1. Oils, Fats and Waxes: Sources of fats, oils and waxes; Extraction, refining, bleaching,

deodourization and hydrogenation of fats and oils; Production of cooking oil, salad oil, margarine

and vanaspati; Saponification number and iodine value; Drying oil, essential oil and their uses; Waxes.

2. Soaps and Detergents: Surface active materials and principles of detergency; Splitting of fats;

Fatty alcohols; Manufacture of different types of soap; Recovery of glycerin; Classification of detergents; Manufacture of alkyl aryl sulphonate, Bio-degradability of detergents.

3.Fermentation industry: Enzymes - chemistry and mechanism of their action; Manufacture of

industrial and absolute alcohol, rectified spirit, acetic acid, citric acid and vinegar; Production of beer, wine and other liquors.

ACCE 2209: Chemical Engineering -IV 3 CH

1. Separation Processes: Filtration, centrifugation sedimentation - theory and application; Filters,

centrifuges, thickeners, classifiers, cyclones; Gravitational and centrifugal application. Membrane

separation.

2. Drying of solids: Principles of drying and industrial application; Mechanism of drying; Drying

rate curves; Drying time; Constant and variable drying conditions; Hygroscopic solid. 3. Refrigeration Principles: Basic theory; Compression and Absorption Refrigeration cycles;

Refrigerants; Application of refrigeration.

ACCE 2211: Metallurgy 3 CH

1. Metals and ores: a) Occurrence and Ore preparation. Physical methods of ore dressing : communication, Sorting

classifications, concentration, gravity concentration, Froth flotation methods.

b) Pyrometallurgical techniques : Calcining, roasting, Sintering, smelting, Reduction of ores with

carbon and metals, physical chemistry of thermal reduction process Slags, Fluxes. c) Hydro-metallurgy: principle of solvent extraction, leaching and their application in extraction

of metals.

2. Manufacture of pig iron : Raw material, Blast furnace design and operation, chemical reaction in Bose and Hearth. By-products of the blast furnace and its utilization, Heat recovery of blast furnace

and its efficiency.

3. Production of steel and wrought iron : Cement steel, and crucible steel, the Bessemer process, the open hearth process, basic and acid production of steel in electric furnace. Duplex process,

Deoxidation, alloying addition and steel ingots.Influence of minor elements in carbon steel, low steel

and high alloy steel. Nitrogen in the Bessemer steel; The use of oxygen in Bessemer converter; Classification and uses of steel. Heat treatment of steel: Annealing, normalizing, hardening, case

hardening, gas carburizing.

4. Phase diagram: General principles of the phase diagrams of alloys and solid solutions and intermetallic compounds; Study of the Fe-C, CuZn, Al-Cu, Al-Si and Cu-Sn systems.

5. Metallurgy of Uranium: Principle and new development in Uranium leaching and recovery of

Uranium there form, Reduction of Uranium tetra fluoride with Ca and Mg.

ACCE 2202: Applied Chemistry and Chemical Engineering Lab.- VII 1 CH

Inorganic Quantitative Analysis:

a. Acid-Base titrations

b. Oxidation-Reduction titrations

ACCE 2204: Applied Chemistry and Chemical Engineering Lab.- VIII 1 CH

Gravimetric Analysis

a.Precipitation titrations

b.Complexometric titrations



Year 3 : Term I

ACCE 3101: Fuel Technology 3 CH

1. Types of fuels: Definition, Classification of fuels; Calorific value of fuels.

2. Coal: Origin of formation and composition; classification; proximate and ultimate analysis of coal; moisture and mineral matters in coal; preparation and storage; destructive distillation,

carbonization, complete gasification of coal; manufacture of metallurgical coke, peat. Liquefaction

of coal; Utilization. 3. Petroleum: Origin; Composition; Classification; Preliminary processing of petroleum; Petroleum

emulsions and their destructions; Atmospheric-Vacuum distillation; Desulphurization of petroleum

products; Products from petroleum refinery in Bangladesh and their uses. 4. Different types of fuel gases: producer gas, water gas, coke-oven gas, oil gas, natural gas and

LPG. Natural gas industries in Bangladesh.

ACCE 3103: Corrosion Engineering 3 CH

1. Corrosion, Classification, Corrosion Damage Cost of Corrosion, Corrosion Engineering, Definition of Corrosion, Classification of Corrosion,

Environments, Corrosion Damage, Future Outlook.

2. Corrosion Principles: Introduction, Corrosion Rate Expressions. Electrochemical Aspects: Electrochemical Reactions, Polarization, Passivity.

Environmental Effects: Effect of Oxygen and Oxidizers, Effect of Velocity, Effect of

Temperature, Effect of Corrosive Concentration, Effect of Galvanic Coupling. Metallurgical and Other Aspects: Metallic Properties, Economic Considerations, Importance of

Inspection, Study Sequence.

3. Different Forms of Corrosion Uniform attack,Galvanic or Two-Metal Corrosion, Crevice Corrosion, Pitting Corrosion,

Intergranular Corrosion, Selective Leaching, Erosion Corrosion, Fretting Corrosion, Stress

Corrosion, Hydrogen Damage.

4. Corrosion Under various condition: Atmospheric Corrosion, Underground Corrosion, Immersion Corrosion, Marine Corrosion, Liquid

metal Corrosion.

5. Corrosion Testing Introduction, Classification, Purpose, Materials and Specimens, Surface Preparation, Measuring and

Weighing, Exposure Techniques, Duration Planned-Interval Tests, Aeration, Cleaning Specimens After Exposure, Temperature, Standard Expressions for Corrosion Rate, Galvanic Corrosion, High

Temperatures and Pressures, Different Corrosion Tests.

6. Corrosion Prevention Materiakls Selection, Alteration of Environment, Design, Cathodic and anodic Protection,Coatings.

7. Corrosion in Industries Corrosion in boiler plant, Chemical Industries, Petroleum Industry, Fertilizer Industries.

ACCE 3105: Instrumental Method of Analysis-I 3 CH

1. Chromatography-General Principles: Classification of chromatographic methods; Nature of

partition forces; Chromatographic behavior of solutes; Column efficiency and resolution; Column

processes and band broadening; Reduced variables; Time of analysis and resolution; Quantitative

analysis.

2. Paper Chromatography, PC: Principle; Valuation of PC as a separation method; Application.

3. Thin Layer Chromatography, TLC: Principle; Qualitative and quantitative analysis by TLC; Advantages and limitations; Application; Argentation TLC.

4. Liquid Column Chromatography: Adsorption Column Chromatography, LSC: Principle;

Methodology; Stationary phase; Mobile phases; Detectors; Application. 5. Partition Column Chromatography, LLC: Principle; mehodology; stationary phase; solid

supports, mobile phase; Application.

6. Gas Chromatography, GC: Principle; Instrumentation of GLC. Column efficiency and resolution. Sampling techniques, Column, packed column, capillary column; Column oven, Carrier

gas, Sample injection system; Detector of GC, TCD, FID, ECD etc.; Application; Overview of Gas

Solid Chromatography. 7. High Performance Liquid Chromatography, HPLC: Basic principle; modes of HPLC;

Instrumentation; Retention; Column efficiency, Band broadening and temperature effect; Column

packing and stationary phase; Solvents; Solvent delivery system; Pump; Sample introduction system; Detectors; Application.

8. Electrophoresis: Principle, Classification; Paper electrophoresis; Gel electrophoresis; application.

9. Ion exchange, Reverse Osmosis, Ultra filtration, and Electrodialysis.

ACCE 3107: Applied Electrochemistry 3 CH

1. Electrochemical Industries: Advantages and drawbacks of electrochemical manufacturing

process; Chlor-alkali industry; Importance of chlorine and caustic soda; Raw materials of chlor-

alkali industry; Chemistry and technology of manufacture of chlorine and caustic soda by brine electrolysis; Diaphragm, mercury and membrane cells; Modern technologival development and

environmental aspects; Caustic soda-chlorine industry in Bangladesh.

2. Polarization and Overvoltage: Nature of electrolytic polarization; Decomposition voltage; Types of polarization; Classification of overvoltage; Hydrogen and oxygen overvoltage;

Significance of polarization and overvoltage in electrochemical manufacturing processes.

3. Electrified interface, Electrical double layer; Helmholtz-parrin model, The Gaoy Chapman

model, stern model.

4. Electrodics: Charge transfer; Electrochemical devices: substance producer, substance destroyer and energy producer; Basic electrodic equation: The Butler-Volmer equation; Symmetry factor and

its significance; Exchange current density; Tafel equation.

5. Electrodic Reactions of special Interest: Electrocatalysis: A chemical catalyst and an electrocatalyst. Electrocatalysis in simple Redox

reaction, Reaction involving adsorbed species. Electrogrowth of metals on Electrodes.

6. Polarography : Basic principles. Direct current polarography: Residual current, Ilkovie equation, polarografic maxima, Half wave potentials, Equation of the polarografic wave. Quantitative

Technique: general consideration, evaluation of quantitative results, measurement of wave heights.

Equipment for polarography, Dropping mercury electrode assembly. Volatmetry: Cyclic voltametry,

Anodic stripping voltametry.

ACCE 3109: Material Science and Engineering 3 CH

1.Fundamentals on materials science and engineering, classification of materials, advanced materials, modern materials. Mechanical, electrical, thermal, magnetic and optical properties of

materials, materials selection and design considerations.

2.Fundamentals of structures of crystalline solids Crystal structures, unit cells, crystal system, crystallographic points, directions and planes, single

crystal, polycrystalline materials, anisotropy, noncrystalline solids. Metallic crystal structures (face-

centered, body-centered, hexagonal close-packed and closed-packed crystal structures), crystal structures of closed pack anions, polymer crystallinity, polymer crystals. Imperfections in solids

(Vacancies and self-interestials, impurities in solids, imperfections in ceramics, interfacial defects,

polymer defects. 3.Mechanical properties of metals

Types of metals and alloys (ferrous, non-ferrous and thermal processing of metals), deformation

(concept of stress-strain, plastic, elastic deformations and hardness), variability of materials properties, safety factors), Failure of metals (Fracture, Fatigue and Creep: Types and principles).

4.Polymers

Different types of polymeric materials (plastics, elastomers and fibers), mechanical behaviors of polymers, viscoelastic deformation and fracture of polymers. Deformation of elastomers,

Crystallization and melting, glass transition temperature, advanced polymeric materials.

5.Composites materials and ceramics Plastic reinforced composites, polymer-matrix composites, metal-matrix composites, carbon-carbon

composites, hybrid composites. Types and application of ceramics, mechanical and glass properties

of ceramics. 6.Processing of engineering materials

Fabrication of metals, fabrication and processing of ceramics, processing of plastics and processing

of composites. 7.Nano-Crabon compounds

Fullarene [60], Fullerene [70], synthesis, separation and applications, carbon nano-tubes: properties,

purification and application. Characterization of nano-materials by SEM, TEM and AFM and other techniques.

ACCE 3111: Chemical Technology-V 3 CH

1. Leather: Classification of hides and skins; Structure of animal skins; Pretannage processes; Tanning processes; Commercial preparation of tanning extract; Finishing of leather; Commercial

aspects of leather.

2. Glue, Gelatin and Adhesives: Manufacture of gelatin; By-products; Chemistry of Glue and Adhesives and their commercial importance.

3. Surface Coating Material: Paint, Varnish and lacquer - constituents and their functions;

Performance of surface coating; Properties of pigments, binders and volatile solvents; Manufacture of paints, varnish and lacquer.

4. Fragrances and Flavors: Constituents of perfumes; vehicles, the fixative and odoriferous

elements; Synthetics and semi-synthetics used in perfumes and flavors; Formulations; Natural fruit concentrates.

5. Food: Introduction, types of food additives, food processing, food processing equipments.

ACCE 3102: Applied Chemistry and Chemical Engineering Lab.-IX 2CH

Instrumental method of Analysis A) Conductometric Titrations:

i. Strong acid vs. strong base

ii. Weak acid vs Weak base

iii. Applications of single determinations of conductance, Determination of solubility of

sparingly soluble electrolytic

B) Potentiometric Titrations:

ACCE 3104: Applied Chemistry and Chemical Engineering Lab.-X 2CH

Experiments on

1. Separation of Food Dyes and Plant Pigments by Chromatography 2. A Cycle of Copper Reactions

3. Synthesis of Ferrous Sulfate from Iron

4. Paper Chromatography in Separation of FeII, CoII, Ni 2+ and CuII Ions



Year 3: Term II

ACCE 3201: Instrumental Methods of Analysis –II 3 CH

1. Ultraviolet and visible spectroscopy.-: Basic principles;different types of electronic transitions.

Beer-Lambert Law; The molar absorption coefficient and its significance. Instrumentation: Radiation sources, detectors; readout modules, filters, monochromators, grating monochromator

systems; Instrument for absorption photometry.

2.Fundamental laws of photometry; Spectrophotometric accuracy; photometric precision; quantitative methodology; Differencial or expanded scale spectroscopy; Spectra of solids;

Correlation of electronic absorption spectra with molecular structure.

3. Infrared spectrophotometry: Vibration in molecules: normal modes of vibration ; criterion for IR activity. Characteristic group vibrations. Correlation of infrared spectra with molecular structure;

Instrumentation; Sample handling, Quantitative analysis.

4. Raman spectroscopy: Theory. Importance of laser in Raman Spectroscopy. Instrumentation;

Sample handling and illumination; Diagnostic structural analysis; Quantitative analysis.

5. X-Ray Methods:

Introduction Production of X-rays and X-ray spectra. X-ray Methods and Applications: i) Direct X-ray methods, ii) X-ray absorption methods, iii) X-ray fluorescence methods iv) X-ray diffraction.

ACCE 3203: Instrumental Methods of Analysis -III 3 CH

1. Nuclear Magnetic Resonance Spectroscopy: Theory; instrumentation; Relaxation process; Information from NMR spectra; chemical shift; factors influencing chemical shifts; spin-spin

coupling; spin-spin splitting patterns; factors affecting spin-spin coupling; Shift reagents; spin de-

coupling; chemical shifts in case of proton exchange reaction; restricted rotation etc.; Introduction to 13C NMR; Application of NMR spectroscopy.

2. Mass Spectroscopy: Introduction; Instrumentation; Determination of molecular formula. Mc

Lafferty rearrangement; Meta-stable ions; Fragmentation process; Interpretation of mass spectra. Identification of Compounds by combined UV. IR, NMR and mss Spectroscopy.

3. Atomic spectroscopy: Flame emission spectrometry, FES; flame characteristics; flame processes

quantitative measurements, interference; Applications Atomic absorption spectrometry, AAS: absorption of characteristic radiation; instrumentation;

sample vaporization; qualitative measurements; Application.

4. Fluorescence and Phosphorescence spectroscopy: Theory and Application of fluorescence and phosphorescence spectroscopy, Emission spectroscopy and Electron Spectroscopy. Mossbuer

Spectroscopy.

ACCE 3205: Chemical Engineering- V 3 CH

1. Heat transfer: Modes of heat transfer; Basic equations for conduction, convection and radiation

heat transfer; heat exchangers and condensers; Mean temperature difference in different flow

arrangements; extended surfaces; Construction and principle of operation of heat exchangers and condensers.

2. Evaporation: Evaporators, Types of evaporators, single effect evaporator, multiple effect

evaporators. 3. Boiler: Definition, classification, construction and operation of fire tube boiler, water tube boiler,

High pressure boiler, Boiler mountings, Industrial application of boiler.

4. Distillation and Rectification: Binary distillation principles; Equilibrium, flash and differential distillation; Continuous distillation with reflux, rectification; McCabe-Thiele method for stage

calculation; Economic Reflux Ratio; Constructional features of fractionating column; Efficiency of

rectification; Multi-component distillation.

ACCE 3207: Pharmaceutical Process and Technology 3 CH

1. Raw Materials for pharmaceutical industries: Classification of raw materials and sources;

Specification analysis and testing of raw materials; Procurement of raw materials; preliminary

processing and storage of raw materials.

2.Processing steps in pharmaceutical industries: Formulation of drugs and

medicines; preliminary processing of different components; Mixing and blending. Equipment used for preliminary processing, mixing and blending. Final packaging methods and equipment employed

there in.

3. Quoting and non drug ingredients: definition of quoting, necessity of quoting, types of quoting, sugar quoting,film quoting. Application of special quoting, use of preservatives and excipients and

their specific roles.

4. Enzymes, Vitamins, Hormones and Alkaloids: Definition, classification, nomenclature and structural features of enzymes, mechanism of enzymatic reactions, Optimum condition for

enzymatic reaction, Inhibition of enzymatic reaction. . Specificity and optimum condition for

enzyme action; enzymic hydrolysis of protein; Water and fat soluble vitamins, Source of different vitamins, Vitamin deficiencies. Drugs for type I and type II diabetes - thioureas, biguanidines,

thiazolidinediones, Insulin preparation. Thyroid hormone and its function, Sex hormones,

Adrenalines - mineralocorticoids and glucocorticoids, Belladona, Cinchona, Tropane, Nux-vomica alkaloids.

5. Preparation, Properties, action, uses and assays of the following drugs:

i) Promethazine Hydrochloride, ii) Piperazine, iii) Chloropheniramine maleate, iv) Calcium

Gluconate, v) Isoniazide, vi) Para Amino Salicylic Acid and vii) Thiomersol. 6. Gastric Antacids: Chemistry, biological action and uses of Non-systemic antacids such as

aluminium hydroxide, aluminium carbonate, magnesium hydroxide and oxide, Chemistry, biological

action and uses of Systemic drugs such as H2 receptor antagonists, like ranitidine, cimitidine,

omeprazole etc.

7. Histamines and Antihistamins: Mode of action of histamine on cardiovascular system, histamine releasing components, allergic effect, Definition, General structure, examples, mode of action of H-1

Blockers Sedative hypnotics-Definition, Biological action and synthesis of benzodiazepines.

ACCE 3209: Chemical Technology - VI 3 CH

1. Introduction to fertilizer: History of chemical fertilizer; role of fertilizers in agriculture; factors influencing choice of fertilizers; Fertilizer industry in Bangladesh.

2. Nitrogenous fertilizer: Ammonia and urea Manufacturing technology; Prospects of urea fertilizer

industries in Bangladesh.

3. Phosphate fertilizer: Raw material, chemistry and technology of phosphates and super

phosphates; Triple super phosphate; Prospects of phosphatic fertilizer industries in Bangladesh.

4. Potash fertilizer: Production and uses of murate of potash and other potassium fertilizers. 5. Complex and mixed fertilizers: NPK fertilizers, mixed fertilizers, bio fertilizers.

6. Agro-chemicals: Raw materials, manufacturing processes and uses of pesticides, insecticides etc.

7. Bio fertilizer: Introduction, sources, manufacturing processes, applications.

ACCE 3211: Industrial Economics, Psychology and Management 3 CH

1. Interest & Investment costs : Cost estimation. Factors affecting investment and production costs. Capital investments. Cost factors in capital investment. Methods for estimating capital investment.

Estimation of total production cost. Gross-earning costs.

2. Taxes & Insurance.

3. Depreciation: Physical & functional depreciations. Methods for determining depreciation.

Evaluation of depreciation methods. service value, salvage value and present value of an equipment.

4.Profitability, Alternative Investments & Replacements : Bases for evaluating project

profitability. Mathematical methods for profitability evaluation. Determining Acceptable Returns. Principles of Alternative Investments by different profitability methods. Replacement policy.

Methods of profitability evaluation for replacements.

5. Price-cost volume relationship. Computation of break-even point. Managerial use of break-even analysis. Principal accounting tools/statements.

6. Principles of management-Functions of Management. Management Theories. Patterns of

management. Inventory management 7. Behavior as a science : Industrial psychology as branch of knowledge, Ways in which

psychologists can help, Management of an enterprise in changing human behavior, Organizational

psychology, Psychological problems and informal organization, Management attitude towards informal organization.

8. Perceptions and attitudes: Determinations and method of change, Committees, Consultative

direction and participate management as tools of influencing behavior, Attitude training, Attitude formation, Conditions favoring attitude change, Lenin and schein models.

9. Work and work environment : Impact of environment on workers performance, Job satisfaction,

Productivity, Group solidarity and cohesiveness, Impact of repetitive work, Rest, Recreational facilities and boredom, How to eliminate boredom, Length or work period, Measuring workers

efficiency, Work and pay and impact of incentives.

10. Ethics, Morality & Counseling : Meaning and significance Ethics, Meaning and significance of morality, Causes of low and high moral, Moral and productivity, Moral components, Group morale,

Maintaining morale, Measurement of morale, Diagnosis of morale, Meaning and significance of

counseling, Counseling types, Causes of mental maladjustment, Ways of handling maladjusted employees, Directive vs, Non-directive counseling.

ACCE 3202: Applied Chemistry and Chemical Engineering Lab - XI 2CH

Analysis of Industrial Products. Complete analysis of

1.Soap and detergents

2.Fertilizers, Urea, TSP and Murate of Potash 3.Bleaching powder and Cement.

4.Vegetable oils

5.hydrogenated fats 6.Milk and milk products

7.Sugar and confectionary materials

8.Glass

ACCE 3204: Applied Chemistry and Chemical Engineering Lab -XII 2CH

1.Batch (continuous) distillation of Methanol-water binary mixture.

2.Fractional distillation of Methanol-water mixture using a fractionating column

3.Determination of batch-settling curve

4.Measurement of fluid flow in pipes using an Orifice:Venturimeter. 5.Extractive distillation of Tolune-n-Heptane mixture using phenol as additive.

6.Phase diagram of the ternary systems i. anilne-n-heptane-toluene and ii. acetic acid-chloroform-

water. 7.Determination of Viscocity-Index of Motor oil by, ASTM D2270-87:IP 226-84, methods.



Year 4 : Term I

ACCE 4101: Environmental Chemistry: 3 CH

1. Nomenclature: Pollution, pollutant, contaminant; receptor; sink; pathways of pollutants; speciation; DO, COD, BOD and TLV.

2. The environmental segments: Atmosphere, Hydrosphere, Lithosphere and Biosphere.

The atmosphere: Structure and properties of the atmosphere; Temperature inversion and air pollution episodes; Atmospheric photochemistry; Possible depletion of stratospheric ozone; Natural versus

polluted air.

3. Air pollution - Industry and Energy related: Particulate matter; analysis and control of particulates; Sulphur oxides; effects of sulphur oxides and particulates; Control technology of

sulphur oxides.

4. Air pollution - Transportation related: Carbon monoxide; Nitrogen oxides; Hydrocarbons; Photochemical smog; Control of automobile emissions.

5. Water-General principles: Unique physical and chemical properties. Criteria of water quality.

Natural water-eutrophication. 6. Water pollution: Water pollutants-organic pollutants, pesticides, organochlorine insecticides,

organophosphates and carbamates; Detergents; Toxic organic chemicals. Inorganic pollutants -

sediments, radio active materials. Thermal pollution; Oil pollution; Monitoring and control of water pollution; BOD and COD.

7. Municipal waste water treatment: The importance of micro organisms in water purification;

Primary and secondary treatments; Tertiary or advanced treatments. Removal of nitrogen, phosphorous, bacteria and viruses; Disposal of treated water in soil.

ACCE 4103: Pharmaceutical Technology and Pharmaceutics 3 CH

A. Pharmaceutical Technology:

1. Unit process and unit operation in pharmaceutical industry: Design, construction and safety measures of pharmaceutical manufacturing plants. Principles involved and techniques employed in

drying, granulation, mixing, clarification, filtration, milling, distillation. Control of humidity,

refrigeration and air-conditioning. 2. Ointments, emulsions and Aerosol: Definition, classification and preparation of ointments;

emulsion and aerosol; Factors affecting skin adsorption; Ophthalmic ointments; Emulsifying agents;

stability of emulsions; industrial preparation of emulsions; Aerosol for typical use. Packing and storage of ointments, emulsions and aerosols.

3. Parenteral products: Types of parenteral products. Advantages and disadvantages; Vehicles for

parenteral products. Containers, closures, cleaning equipment and preparation of parenteral products including clarification, filling, sterilization, sealing and capping; Control requirements for parenteral

products; pyrogen test; sterility test; inspection of foreign particles, inspection for leakage, identity,

labeling, storage and administration of parenteral products. 4. Tablet making: Weights and measures; Formula, ingredients and excipients; Compounding of

tablets by i. dry and ii. wet granulation methods. Slagging and capping of tablets; disintegration test

for compressed tablets. Essential quality of good tablets.Advantages and disadvantages of tablets as medicinal dosage form.

5. Antibiotics: Definition. Gram positive and gram negative bacteria; Production of antibiotics.

Action and uses of different penicillin, streptomycin, chloramphenicol and tetracycline.

B. Pharmaceutics:

1. History of Pharmacy: History. Code of ethics. Pharmacopoeias, formularies and codex officially

recognized in Bangladesh; Raw materials used in Pharmacy; general properties of drug constituents; solvents used in extracting drugs.

2. Dispensing: The prescription; Proper handling of prescription. Prescriptions in compatibility.

3. Pharmaceutical dosage forms: Quality assurance, packaging and packing of tablets, capsule,

suspension, emulsion, ointment, ear, nose and throat medication. 4. Pharmaceutical necessities: Pharmaceutical solvents, coloring, flavoring, sweetening and

diluting agents. Antioxidants and preservatives.

ACCE 4105: Chemical Technology - VII 3 CH

1. Importance of petro-chemical industry for national development. 2. Secondary petroleum refining processes: Thermal cracking; Catalytic cracking; Catalytic

reforming; Pyrolysis; Hydrocracking.

3. Chemistry and technology of manufacturing paraffins, olefins, aromatic hydrocarbons, acetylene, synthesis gas from petroleum and natural gas.

4. Halogenation processes

Radical-chain chlorination-Chemistry and technology of liquidphase and gas-phase chlorination. Ionic-catalytic halogenation, decomposition reactions of chloroderivatives. Flourination processes.

Liquid-phase and gas-phase chlorination; Chloroderivatives.

5. Alkylation processes Theory and technology of C-alkylation- alkylation of aromatic hydrocarbons, phenols and

paraffins,alkylation at oxygen, sulphur and nitrogen atoms. -Ethoxylation and other syntheses

based on - oxides vinylation processes. Alkylation at atoms of other elements. 6. Oxidation processes

Homogeneous oxidation at saturated carbon atom, heterogeneous-catalytic oxidation of

hydrocarbons and their derivatives. Oxidation of olefins catalysed by metal complexes. Scientific and engineering foundations of the processes.

6.Theoretical basis, chemistry and technology of hydrolysis, hydration, dehydration, esterification,

amidation, sulphation, sulphonation, nitration, dehydrogenation and hydrogenation processes. 7. Synthesis based on carbon monoxide.

ACCE 4107: Chemical Engineering- VI 3 CH

1. Liquid-liquid extraction: Liquid-liquid extraction in single and multiple contact extractor; Selection of solvents; Use of triangular diagram for stage calculations; Different extraction

equipments; Application of solvent extraction.

2. Leaching: Types of leaching, Principles of leaching, leaching equipments, Industrial applications.

3. Gas-liquid Absorption: Principles of absorption and desorption processes; constructional

features of absorbers and desorbers.

4. Crystallization: Theory of crystallization and crystallization equipments; Industrial application.

ACCE 4102: Applied Chemistry and Chemical Engineering Lab -XI II 2 CH

Study of unit operations e.g. Absorption, Drying, Heat Transfer, Fluid flow Phenomena etc. using

equipments of pilot plant scale either in Departmental laboratories or at laboratories of other

industrial training organizations.

ACCE 4104: Applied Chemistry and Chemical Engineering Lab.-XIV 2 CH

1. Analysis of some industrially important inorganic and organic materials

1. Common salt 2. Sand. 3. Cellulosic raw materials 4.Water; 5.Coal; 6.Natural gas; 7. fuel oil;

5.sulphur; 6. Oil seeds


ACCE 4108: Project & Presentation-I 1 CH

Year 4 : Term II

ACCE 4201: Environmental Pollution and Industrial Waste Management 3 CH

1. Deposition of atmospheric pollutants and their effects: Acid rain; Some air pollution case

study, London smog; Bhopal disaster; Chernobyl disaster etc. Air quality standards; Sampling and monitoring.

2. Disposal of solid wastes: i. Population X Affluence X Technology. ii. Municipal wastes;

reclamation, recycling and reuse. iii. Incineration, pyrolysis and sanitary landfill. iv. Toxic chemicals; incineration, chemical treatment, solidification, encapsulation and landfill.

3. Industrial waste water treatment: Activated carbon adsorption; Ultra filtration; Electrodialysis.

Heavy metals and their removal. Sources and effects of mercury, lead, arsenic and chromium. Case studies of bio-amplification, Minamata disease etc.

4. Waste treatment of various industries: i. Pulp and paper industries, ii. breweries, wineries and

distilleries. iii. Tannery, iv. Textile mills, v. Dairy, vi. Fertilizers, vii. Sugar industries, viii. Steel plants, ix. Oil refineries and x. Pharmaceutical industries.

5. Industrial monitoring: Concept of TLV, time weighted average and short term exposure limits;

Methods of sampling, preservation, monitoring techniques and methodology of various environmental samples.

6. Current industrial environmental status: Formulation of guidelines and discharge standards of

various industries; State of global environment; Environmental protection act-95, EPA-95, of Bangladesh.

7. Environmental problems and regulatory systems: Definition of laws and protocols, Major

international conventions, Treaties and protocols in the field of environment, the agenda 21 adopted at the UNCED, 1992, Kyoto protocol; Sectoral environmental legislation’s in Bangladesh and their

limitations, Conservation act 1995, Environmental conservation rules,1997; Environmental court act

2000; environmental policy,1992, Environmental Action plan of Bangladesh, 1992, and the role of DoE in the implementation of existing national and international rules in Bangladesh, Bangladesh

position on the Environmental ICTPs to be signed, ratified or accessed, implementation status,

action to be taken for implementation.

ACCE 4203: Chemical Technology -VIII 3 CH

1. Polymerization and Polymer properties.

Chain and step growth polymerization, types of polymers, copolymers, structure and properties of

polymers, methods of polymerization, polymer degradation. Radical Chain (addition)

Polymerization, ionic & coordination chain (addition) Polymerize.

2.Rubber

Natural rubber, synthetic rubber, monomer production, synthetic rubber polymerization, sterespecific rubbers, rubber processing chemicals, Rubber compounding, rubberication, latex

compounds, reclenical rubber, vulcanization. Elastomer Technology

3.Synthetic fibres industries Fibre forming polymers and polymer structure, fibre properties. Polyamide fibers polyester, acrylics

and modacrylics, vinyls and vinylidanes, spandex polyolefins, glass fibres. Fibre Technology.

5. Thermoplastic Manufacture: Polyethylene , polypropylene, polyvinyl chloride, polyvinyl acetate, polytetrafluoroethylene,

polymethyl methacrylate, polystyrene.

6. Thermosetting: Phenolic plastics, polyurethene, aminoplastics, epoxyresins unsaturated polyester resins,

miscellaneous thermosetting resins.

7. Additives for polymers: Fillers, plasticizers and softeners, lubricants and flow promoters, antiaging additions,flame retarders,

cross linking agents.

ACCE 4205: Chemical Engineering -VII 3 CH

1. Mass Transfer: Introduction to mass transfer; Phase equilibria; Equilibrium stage concept; Basic

theories of mass transfer; Diffusion of gases and liquids; Diffusion through stagnant layer and

equimolar counter diffusion; Mass transfer between gas and liquid phases; Two-film and other

theories; Application of mass transfer correlations to transfer units; HTU and NTU concept; Mass

transfer coefficients. 2. Dimensional Analysis Method: Basic concepts of dimensional Analysis- Dimension and Unit of

physical quantity, Primary Dimension, Dimensional formula, Dimensionless group of variables;

Principles of Dimensional Analysis; Application of Dimensional Analysis method for evaluation of heat transfer coefficients in heat transfer equipments; Dimensionless correlations for forced and free

convection.

ACCE 4207: Nuclear and Radiation Chemistry 3 CH

1. Introduction: Basic Concepts of Nuclear, Radiochemistry and Radiation Chemistry, Definition and scope of nuclear chemistry; Modern ideas in nuclear science and technology.

2. Atomic Nucleus: (i) Composition, (ii) Size, (iii) Density, (iv) Mass and Energy correlation, (v)

Nuclear binding energy, (vi) Stable and unstable nuclei, (vii) Factors responsible for the stability of a nucleus.

3. Modes of Decay: Radioactivity, (i) Laws governing radioactive decay, (ii) Half-life and average

life, (iii) Successive decay and branching decay, (iv) Radioactive equilibria. 4. Nuclear Reaction: (i) Basic concepts, (ii) Potential barrier, (iii) Elastic and inelastic scattering, (iv)

Q-value and threshold energy for nuclear reaction, (v) Reaction cross section, (vi) Excitation

function, (vii) Reaction mechanism at low and high energy. 5. Types of Nuclear Reaction: (i) Radiative capture, (ii) Photonuclear reaction, (iii) Reaction

mechanism of low and high energy, Special reaction: (i) Evaporation, (ii) Spallation, (iii) Fission, (iv) Fusion, (v) Fragmentation, (vi) Transfer reaction.

6. Nuclear Fission: The process of nuclear fission, Fission Fragment and their mass distribution,

Fission energy, Fission cross section and thresholds, Fission Neutrons, Theory of nuclear fission. 7. Nuclear Fusion and Nuclear Reactor: Basic principle, The natural uranium reactor, The four factor

formula, The classification of reactors, Reactor power, Critical size of thermal reactor; The Breeder

reactor; Nuclear waste management; Nature’s nuclear reactor. 8. Interaction of radiation with Matter: Interactions of charged particles with matters and energy loss

mechanism, Interaction of gamma radiation with matters, Photoelectric and Compton effects and

pair production, Radiolysis of water spur reaction. 9. Radiation detection: Ionization current measurement, Ionization chamber, Multificative ion-

collection, G.M. counter, Scintillation counter: operation principles of NaI (T1) Scintillation

detector, Proportional counter, Semiconductor gamma radiation detector-Ge (Li) and Hyperpure Germanium, Health physics instruments, Radio isotopes and their uses: Production and separation of

radio isotopes, The Szilard – Shalmers reaction, Isotope dilution analysis, Activation analysis,

Tracer technique for reaction kinetics and for industrial, agriculture and medical uses. 10. Nuclear and Radiomechanical Analytical Techniques: (i) Neutron activation analysis, (ii)

Isotope, isotope dilution analysis, (iii) Radiomechanical tracer techniques, Production of

radioisotopes and labeled compounds, Radiation protection. 11. Radiation Protection: (i) External and internal radiation sources, (ii) Radiation effects, (iii) Safety

recommendation and regulations.

ACCE 4202: In plant Training 2 CH


ACCE 4206: Project & Presentation-II 1 CH

Book references:

1. A text book of physical chemistry -S. Glasstone.

2. Chemical Thermodynamics - Steiner.

3. Thermodynamics for chemistry - S. Glasstone. 4. Phase Rule - A. Findlay (Revised by campbell)

5. Physical chemistry

6. Practical Physical Chemistry - Findlay 7. Introduction to electrochemistry - S. Glasstone.

8. Physical Chemistry - Borrow.

9. Molecular spectroscopy - Barrow 10. Molecular spectroscopy - Banwell

11. Chemical Kinetics - Laidler.

12. Physical Chemistry -Haque & Nwab 13. Organic Chemistry - Feiser & Feiscer.

14. Principles of organic chemistry - English & Cassidy.

15. Organic Reaction Mechanism - Peter Sykes. 16. Organic Reactions - Vol. I-IV by R. Adams

17. Organic Chemistry - Ahmed & Jabbar.

18. Practical Organic Chemistry - J.B. Cohen. 19. Organic Identification - Clarke.

20. A. Text Book of Practical organic Chemistry - Vogel

21. Organic Chemistry - Vol. I & II-I.L. Fine 22. Organic Chemistry - Morrison & Boyd

23. Advanced organic chemistry - Wheland.

24. Advanced Inorganic Chemistry - Cotton & Wilkinson

25. Inorganic Chemistry - T. Moeller.

26. Valency and Molecular Structure - Cartmell & Fowels. 27. Fundamental concepts of Inorganic Chemistry E.S. Gilreath.

28. Quantitative Inorganic Analysis - Vogel

29. Standard Methods of chemical analysis (Vol. I.III) Etd. by welcher. 30. Instrumental Methods of analysis - Willared, Merritt, Dean, & Scttle.

31. Treaties on analytical chemistry - Editted by I.M. Kolthoff.

32. Source bok of atomic energy - Glasstone. 33. Introduction to Modern Inorganic Chemistry - S.Z. Haider.

34. Advance Inorganic Chemistry S.Z. Haider.

35. Basic Inorganic Chemistry - Cotton & Wilkinson.

36. Nuclear & Radiochemistry - Friedlander & Kannedy.

37. Qualitative Inorganic Analysis - Vogel.

38. Quantitation Inorganic Analysis - Vogel. 39. Hand Book of Chemical Engineering - Perry.

40. Unit operations of chemical engineering - McCabe & Smith.

41. Elements of chemical Engineering - Padger & McCabe. 42. Liquid - Liquid Extraction - Alders.

43. Stoichiometry - Bhatt & Bora.

44. Principles of Industrial Chemistry - Clausen & Mattson. 45. Elementary Principles of Chemical Processes -Pelder & Rousseal.

46.A Text book of Engineering Chemistry - M.M. Uppal.

47.Petrochemical Digest - M.G. Menon.

48. Petroleum Chemicals Industry - R.R. Gold Steam & Al. L. Waddams.

49.Chemical Process Industries - Shreve.

50.Fuel - Brame & King. 51.Petroleum Refining Engineering - Nelson.

52.Modern Plastic Technology- Seymour.

53.Chemistry and Technology of Basic Organic and Petrochemical. Synthesis- N.N. Lebedev.

54.Applied Chemistry for Engineers - L.L. Shriev. 55.Principles of Sugar Technology - P. Honig, Vols. I & II.

56.Introduction to chemical Technology - Dryden.

57.Industrial Chemistry - R.K.Das. Vols. I & II. 58.Water Treatment - James.

59.Method of Cellulosic Chemistry -Doree

60.Refining of fats and oils - Anderson. 61.Paint and Varnish Technology - Fisher.

62.Food and Food Products - Jacob.

63. Chemistry of cellulose -Heuser. 64.Pulp and Paper -Casey.

65.Chemical Refining of Petroleum - Kalichosky.

66.Petroleum Chemical Industry-Glodstein. 67.Petrochemical Industry-Hahy and Loillams.

68.Natural gas and natural gasoline-Hunlington.

69.Modern Plastics-Harry and Brown. 70.Fundamentals of anslytical chemistry-douglas a Sleoogy, & Donable West.

71.Analytical Chemistry-Robert V. Dilts.

72.Modern Methods of Chemical Analysis -Pecsole, Shields, Cairng Mewillam. 73.Spectroscopic Methods in Organic Chemistry-Williams & Fleuing.

74.Application of spectroscopy to Organic Chemistry- J.C.D. Brand & G.Eglinton.

75.Seperation Methods in Chemical Analysis- James M. Miller. 76.Industrial Methods of Analysis - Willered, herritto & Deon.

77.Qualitative Inorganic Analysis-A.I. Vogel.

78.Thin-layer Chromatography-George allen & Unwin.

79.Gas Chromatography- G.G. Ververy.

80.Ion-exchange Technology-Nachod & Schubert. 81.The design & Analysis of Industrial Experiments -Davies.

48.An Introduction to Industrial Chemistry - C.A. Heaton.

83.Hand Book of Industrial Chemistry - J.A. Kent & V.N. Reinhold. 84.The Chemical Industry-D. Sharp & T.F. West.

85.Industrial Organic Chemicals in Perspective-H.A. Wittcoff & B.G. Reuben. Part I & II.

86.Introduction to Industrial organic Chemistry- P.Wiseman. 87.Industrial Minerals and Rocles - S.J. Lefond.

88.Industrial Chemistry- R.W. Thomes & P.J. Farage.

89.Environmental Chemistry-By John W. Moore & Eligabeth A. Moore.

90.Environmental Chemistry: Air & Water Pollution.By H. Stephen Stoker and Speucer L. Seager.

91.Environmental Chem

92.Industrial Waste Water Management. By Seven Erik Jogensen. 93.Wastewater Treatment, By Donald W. Sundstrom & Herbert E. Klei.

94.Industrial Environmental Chemistry.By Donald T. Sawyer and Arthur E. Martell.

95.Recent Advances in Environmental Analysis. By R.W. Frei. 96.Introduction to Environmental Toxicolosy. By Guthrie & Parry.

97.The Industrial Environment & its control. By J.M. Dall avalle.

100.Environmental Plammuf & Management in India. By R.K. Sapru. 101.Friedel-Crafts Chemistry,- G.A. Olah,

102.Fluid Catalytic Cracking role in Modern Refining Mario L.Occelli, Editor American Chemical

society, Washington, DC.

103.Introduction to Material and Energy Balances - G.V. Reklaitis.

104.Catalytic Reforming By Donald M Little.

105.Petrochemical Technology Assessment. 106.The Petrochemical Industry Market and Economics - Albert V. Hahn.

107.Physical Chemistry of Petroleum solvents.- W.W. Reynolds.

108.Origin and Refining of Petroleum - H.G. MeGrath and M.E. Charles Advances in Chemistry

Series American Chemical society. 109.Chemistry of Catalytic Processes - Bruce C. Gates, James R. Katzer G.C.A. Sehuit.

110.Applied Industrial Catalysis Vol. 1-3. Edited by Brucl F.Leach.

111.Characterisation of Catalysts - J.M. Thomas and R.M. Lambert. 112.Catalyst Manufacture - Alvin B. Stiles, Tecodore A Koch Marcel Dekken.

113.Design of Industrial Catalysts- David l.

114.The Natural Gas Industry- M. MEDICI, DRING, MIME. 115.Fuel Science and Technology Handbook edited - James G.

116.Chromatography in petroleum analyses,- Altgelt. K.H. ed K.H. Algett & T.H. Gouw.

117.Mass transfer operations - Robert E. Treybel Internal Student Edition. 118.The Chemistry and Technology of Petroleum. - James G.

119.Laboratory fractional distillation - Thomas P. Carney.

120.Advances in Petroleum Chemistry and Refining. - Kobe and Meketta. 121.Petrochemical Technology - H.L. List.

122.Theories and Practices of Industrial Waste Treatment - Nelson Leonard.

123.Industrial waste Disposal - R.d. ross. 124.Handbook of Separation Technology - Rousseau.

125.Liquid Extraction - Trcybal.

126.Plastics - J. Harry DuBols FREDERICK . 127.Handbook of solvent Extraction - LO, BIRD and HANSON.

128.Text Book of Polymer Science - W. BILLMEYE.

129.Plastic materials - J. A. Brydson, London ILIFFE Books. 130.Petroleum Refining Technology and economics - James H. Gary, GLENN E.

131.Herbicides Chemistry, Degradation and Mode of action P.C. Kearrey and d.d. Kaufman .

132.Elements of Chemical Reaction Engineering - H. SCOTT FOGLER.

133.Principles of Industrial Instrumentation - D. PATRA NABIS

134.An Introduction to thermodynamics Y.V.C. RAO. 135. Encyclopedia of Chemical Processing and Design. (all the volumes).

136.A text on Petrochemicals, 4th Edition 2002.

DR. B.K. BHASKARARAO KHANNA PUBLISHERS, DELHI

137.Introduction to Petrochemicals, 1992. SUKUMAR MAITI

Oxford & IBH PUBLISHING CO. PVT. LTD.

New Delhi, Bombay, Calcutta.

138.Alkylation with olefins

A.V. TOPCHIEV, S.V. ZAVGORODNI AND V.G. KRYUCHKOVA

EISEVIER PUBLISHING COMPANY

AMSTERDAM-LONDON-NEW YORK 1964

139.Chromatography of Polymers Petroleum and Petrochemicals, 1979,

Sukumar Maiti Symposium and workshop organising committee Calcutta 1979

140. Chemistry and Technology of Basic Organic and Petrochemical Synthesis (Volume 1 and

N.N. LEBEDEV

MIR PUBLISHERS MOSCOW, 1984

141.Modern Petroleum Refining Processes, 1990. B.K. Bhaskara Rao

Oxford and IBH Publishing Co. Pot. Ltd. New Delhi, Bombay, Calcutta.

142.CHAUVEL, A. AND G. LEFEBVRE, Petrochemical Processes, Vol. 1 and 2,

France : Pierre leprinee, Imprimene Nouvella, 1989.

143.BROWNSTEIN, M., Trends in Petrochemical Technology, Tulsa, Lklahoma: Petroleum

Publishing Co., 1976

144.FRIED, J.R., Polymer Science and Technology, 3rd ed., New Delhi, Prentice-Hall of India,

2002

Englewood cliffs, N.J. New Yourk: Prentice-Hall, 1995.

145.ODIAN, G., Principles of Polymerization, 2nd ed. New York: John Wiley and Sons, 1981.

146.BILLMEYER, F.W., Textbook of Polymer Science, 3rd ed. New York: John Wiley and sons,

1984.

147.HAHN, A.V., The Petrochemical Industry, New York: McGraw-Hill, 1970.

148.McGranth H.G. and M.E. Charles, Origin and Refining of Petroleum: Advances in Chemistry series, American Chemical Sockty.

149.KOBE and Mcketta, Advances in Petroleum Chemistry and Refining, New York: Interscience Publishers, Inc.

150.List, H.L., Petrochemical Technology, Englewood Cliffs, New York: Prentice-Hall, 1986.

151.Goldstein and Waddams, The Petroleum Chemicals Industry, London: E. and F.N. SPOW Ltd., 1967.

152.Speight, J.G., The Chemistry and Technology of Petroleum, New York and Basel: Marcel Dekkers.

153.Gary J.H. and E. GLENN, Petroleum Refining, New York: Marcel Dekker, 1975.

154.HOBSON, Modern Petroleum Technology.

155.SPEIGHT, J.G., Fuel Science and Technology. (Hand Book), New York: New and Basel Mercel

Dekker, 1990.

156.British Pharmacopoeia

157.Dispensing of medicine - Husa & Martin

158.Pharmaceutical practice- Aulton

159.Bentle'ys Textbook of Pharmaceutics

160.An introduction of Pharmaceutical productions- Poldeman

161.A textbook of pharmaceutical chemistry - Wilson & Gisvold.

162.I.L. Finar, Organic chemistry vol. I & II,

163.Clayden, Greeves, Warren, Wothers, Organic chemistry, Oxterd Univ. Press.

164.Morrison and Boyd; Organic Chemistry, Prentice-Hall.

165.Peter sykes, Mechanism of Organic Reaction

166.E.E liel, Stereochemistry of Carbon compounds.

167.Ian Fleming, Frontier Molecular Orbital Theory,

168.Bentleys Hand book of Pharmaceutical Technology- E.A. Rawlins.

169.The Theory and Practice of Industrial Pharmacy- L. Lachman, H.A. Lieberman, J.L. Kaning.

170American Pharmacy- 1.Good Man Gillman's

171.Essentials of Medicinal Chemistry, 2nd Ed.- Andrejus Korolkovas.

172.Biotransformations in Organic Chemistry, 5th Ed.- Kurt Faber.

173.An Introduction to Medicinal Chemistry, 2nd Ed.- Graham L. Patrick.

bsc(honors) syllabus for applied chemistry and chemical ... · salts.modern process for manufacture...

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