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Cambridge Analytical Associates 222 Arsenal Street / Watertown, Massachusetts 02172/ (617)923-9378 March 28, 1984 Ms. Elleen' O1 Connor U.S. Environmental Protection Agency Contract Laboratory Program Sample Management Office (SMQ) P. 0. Box 818 Alexandria, VA 22313 Dear Elleen: Enclosed 1s the sample data package for Case 2427 received by Cambridge Analytical Associates under Contract No. 68-01-6808 (Inorganics Analysis), on February 21, 1984. ' Problems Encountered 1. Procedural .blanks showed presence of contamination for tin (Sn) at concentrations (20>21 ug/1) slightly above the contract required detection Unit. The source of the blank was apparently the hydrogen peroxide used for digestion. We recognize that certain vendors stabilize .hydrogen peroxide with Sn confounds and have attempted to avoid use of stabilized reagents when performing Sn analyses. Me will continue to Investigate sources of hydrogen peroxide of suitable purity for these determinants. 2. No other problems were encountered during the analyses. I apologize for the delay 1n forwarding this package to you. Please call If you have any questions. Sincerely, Keith A. Hausknecht Director, Inorganic Chemistry Laboratory n & 600001

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Cambridge Analytical Associates222 Arsenal Street / Watertown, Massachusetts 02172 / (617)923-9378

March 28, 1984

Ms. Elleen' O1 ConnorU.S. Environmental Protection AgencyContract Laboratory ProgramSample Management Office (SMQ)P. 0. Box 818Alexandria, VA 22313

Dear Elleen:Enclosed 1s the sample data package for Case 2427 received by Cambridge

Analytical Associates under Contract No. 68-01-6808 (Inorganics Analysis), onFebruary 21, 1984. 'Problems Encountered •

1. Procedural .blanks showed presence of contamination for tin (Sn) atconcentrations (20>21 ug/1) slightly above the contract requireddetection Unit. The source of the blank was apparently the hydrogenperoxide used for digestion. We recognize that certain vendorsstabilize .hydrogen peroxide with Sn confounds and have attempted toavoid use of stabilized reagents when performing Sn analyses. Me willcontinue to Investigate sources of hydrogen peroxide of suitablepurity for these determinants.

2. No other problems were encountered during the analyses. •I apologize for the delay 1n forwarding this package to you. Please call

If you have any questions.Sincerely,

Keith A. HausknechtDirector, Inorganic ChemistryLaboratory

n

& 600001

r] Cimwwv An«rwn Atxxum''

\ WiMftnm, M«, 0917!

Document Inventory: Case May fobo I?Project Number 84-iao

Lab Manager

Item £291

Cover Page - Inorganic Analyses Data PackageInorganic Analyses Data Sheet(s)q.C, Report • Initial and Continuing Calibration *•»»?••>'Q.C. Report - Blanksq.C. Report • ICP-Interference Check Sample *'*7q.C. Report - Spike Sample RecoveryQ.C. Report • Duplicates •q.C. Report - Instrument Detection Limits and Aya7-3/

Laboratory Control StandardRaw Data - Summary Data Slieet(s) - ICP Elements • —Raw Data - Sample Preparation Log(s) AW-31Raw Data - ICP lutings tftf'Raw Data - Summary Data Sheet(s) - AAS ElementsRaw Data - Working' Standard Preparation Log(s)Raw Data - Sb Worksheets) and AA TracingsRaw Data - As Horkiheet(s) and AA TracingsRaw Data . Cd Horksheet(s) and AA TracingsRaw Data • Pb uorksheet(s) and AA TracingsRaw Data . Sa HorkJheet(s) and AA Tracings .~Raw Data • Sn Horksheet(s) and AA Tracings j.f>>'3" *Raw Data - TV Horksneet(s) and AA Tracings )$an-»\~l*tRaw Data - Hg Horksheet(s) and AA'Tracings j.y»>/»1-W7Raw Data > Worksheets for Other Constituents - —-

Page 5 of 12U.S. EPA Contract Laboratory PrcgranSample Management OfficeP.O. Box 813 - Alexandria, VA 22313 , ,703/557-2490 PISi 8-557-2490 . Date l/toWf

COVER PAGEPPRGAMIC ANALYSES DMA PACKAGE

Lab Nona (anthrfJof UnaluKeAtJtece.* Case No.Q.C. Report No. 84-igo

i•EPA NO. Lab ID N , No. Lab ID No.

fflft. n^TV tfitloofgo | Jf ojj L ftWea f>gUa««p«H I M

M«- afTaOH. otf77ma-fla-O-o

1 Old. o<Aft

SDDBn l

ICP Intanleoent and badcgnund corrections applied? yea / No _, _ ,.

• net required by contract at this time j, .„C - blank corncted 2°HVb • not detected due to blank.Mm ItValue - If the nault la a value) greater than or equal to the Inatrunent

detection limit but lesa than the contract required detection limit,report the value in bracket* (i.e., (10) ). indicate the analyticalnetted used with P (for ICP/AA) or p ( tot furnace) .

<: • Indicates element wai analywd for but not detected. Report with thedetection limit value («.g., <10). ,

B - Indicates a value estimated or not reported due to the presence of 'interference, ficplanatory note included on cover page.nt 1708

• - indicates value determined by Method of Standard Additittf * '

Exhibit 8Page 6 of 12

U.S. EPA Contract Laboratory Program ^ ~ EPA Sarple No.Sonple Managarant Office k fl/iQ <-/i-P.O. Box flia - Alexandria. VA 22313 „ lll1.'ivO5Col (,703/557-2490 PIS 1 8-557-2490

Date 3 111 ft"/

LAB NAME Px«VA.,. VN?\

LAB SAMPLE ID. NO. gqoft'

Matrix Ksv/?vi*,

1. Altfflinum ti&e2. Anttaonv < 5Lo

3. Arsenic < *4. Barium \.*V1a5. Barvlliun <.«•

6. Cadoium • ^ 17. Calciun NR

8. ChttiuiuQi \lo i

9. Cobalt <yo

10. CoDoer <I6o

11. Iron ffjl&t

12. Lead <«•Cyanide

iINORGANIC ANALYSIS BOA SHEET

\A-icA\ tasot.. CftSENO. aAll ''labR

ft\ CC REPORT NO. fp\"\&°

Elemnts Identified and Measured

X£/yor rag/Kg (circle One)i f 13. Maqnesiun NR

$ 14. Manganese <k* P

T P 15. Mercury '9 16. Nickel <1o 9

t 17. Potasaiuo NR

P 18. Seleniun < 1 F

19. Silver <io f '20. Scdiun, NR

P 21. Thalliun <\0 t? 22. Tin - oS

5 f 23. Vanadiun <-a.<io f

P. 24. Zinc 4-3_P

Percent Solids NR

Footnotes* For reporting results to EPA, standard result qualifiers are used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags oust be explicitand contained on Cover Page, however.

^ .Lab Manager "fttM. tf, fflMsft+*>&CA

Porral

Exhibit BPage 6 of 12

U.S. EPA Contract Laboratory Program aftSample Managerent Office uy >P.O. Box 818 - Alexandria, VA 22313 "'703/557-2490 PIS: 8-557-2490 . .

Date 3/aj/gd

INORGANIC ANALYSIS, DATA SHEET

LAB NAME >f>i?a&. aUffJ/. dce.. CASE NO.L?Ja&.

ID.

ifl»(

LAB SAMPLE ID. NO. ftfoaoft ._ QC REPORT NO.

Elements Identified and MeasuredMatrix

rag/Kg (Circle One)1. Aluninun /<loft p 13, Maonesiun NR2. Antimony <ae F 14. Manganese

3. Arsenic <"S P ______ 15. Mercury4. Bariun _____ <7S" (> _____ 16. Nickel «/o5, BervUiun ____ <5* p _____ 17, poi-n««iun'

' 6. Cadmium, ____ • l.flla P 18. Selenium <0. C.7. Calcium ' HR ______ • 19, Silver <|Q >*8. Chremiun 4 ID 9 20, Sodium, NR

9. frhilt _____ <ro f ' _____ 21. ThalliuB ^lo P

10. Copper <fo P _____ 22, Tin

11. Iron <* i" 23. Vanadiun

12. Lead ______ <g P ______ 24, Zinc

Cyanide ______________ Percent Solids NR

Footnotes: POT reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

«Can»nts»

Lab Manager

U.S. EPA Contract LaboratcSample Management officeP.O. Box 813 - Alexandria,703/557-2490 PIS: 8-557-2

LAB NAME (h L9 ™^

LAB SAMPLE ID. NO\

Exhibit B^ Page 6 of 12

ry Prcgram \ EPA Sample" No.VA 22313 H R- OtTTJ490

Date 3/4J/&</

INORGANIC ANALYSIS QVTA SHEET

V>,A\ «XL. CASE NO. ,at\a.i. 91.0 R\T OC REPORT NO. SI-lftD

L Elements Identified and Measuredu**i*\

1. Aluninun

2. Antimony

3. Arsenic

S. Bervlliun

6. C&omium7. Calciun8. QuranluB

9. Cobalt

10. Cooper

11. Inn12. Lead

Cvanide

<1«R P

4fto V/< C

[.me P

<* 9

<\ £

NR'<1B P4.SD 9

<St> ?

•a«< 98.3 C

/uBA/br rag/kg (circle om)13. Magnesium NR14. Manganese >V\ 9

IS. Mercury «A2o16. Nickel Wo ?n&vetMdf aJi«« UD

18. Selehiun <a ?'

19. Silver <vo P20. Sodiun NR21. Dulliun <lo ?22. Tin *2o f

23. Vanadiun <iaa f

24. Zinc I3&P

Percent Solids NR

Footnotes: Per reporting results to EPA, standard result qualifiers an used asdefined on Cover Page, Additional flags or footnotes explainingresults an encouraged. Definition of such flags oust be explicitand contained on Cover Page, however,

sj ' Lab Manager

Form I - i

Exhibit BPage 6 of 12

U.S. EPA Contract Laboratory Program ., * 5Sanple Management: officeP.O. Box 818 - Alexandria, VA 22313703/557-2490 PISi 8-557-2490

Date.

INORGANIC ANALYSIS DftIA SHEET

LAB NAME fLlAng. uAA-!tA\ iWj&c. CASE NO. Q\a.t jqtad R

LAB SAMPLE ID.

Matrix Lv.tovx.\

1. Alufflimn

2. Antimony

3. Arsenic4. Barim

5. Bervlliun

6. Cadmium

7. ''"'cium • •

8. Chmniun9. Cobalt

10. Comer

11. Iron12. Lrad

Cvanide

NO. CjHOfthl'V QC DEPORT NO. .jWjjfcO

Elements Identified and Measuredq S* \.

f ug/ljor ng/kg (Circle One)co 9 13. Magntsiun NR<ao ? 14. Manaanese Hf ?

< 5 P 15. Mercury *ft284iM 9 16. Nickel Alb P

< 1 ? 18. Selenium < 9. C

NR 19. Silver <\o P

<sa P 21. Thalliun < lo F<soP 22. Tin <2cB?

aai 9 23. Vanadiun <ooa Pb.'S P 24. Zinc \15" P

Percent Solids NR

footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Cements:.

Lab Manager

U.S. EPA Centract Laboratory Program ^ Z?A Ssrpie ,v!o.Sanple Management Office /M' J /v, nP.O. Box flia - Alexandria. VA 22313 AH .oV (rU-OS'76> _703/557-2490 FTSi 8-557-2490

S Date 3/Srt«t)f ' i

INORGANIC ANALYSIS DATA SHEET

tAB NAME 0,-wA ka«j JkeA &MOC.. CASE NO. a.MO.1 lll.aft

LAB SAMPLE ID. NO. 840&.W\ _.

» ElementsMatrix iWflvLfi —

1. Aluninun t'Aoo 9

2. Antimany <1c C

3. Arsenic <«• C4. f>>"*iun <* 100 9

5. Bervlliun <«• o6. Ca&nium <l P

7« Cfl\dun • • MR

8. Chremium <\o 9

9. Cobalt <sa P

10. Coner <Sto P11. Iron <srn P12. Lead <S ?

Cvanide .

iQC REPORT NO. BU-lftO

Identified ant) Measured

r rag/kg (circle One)13. Maqnesiun NR

14. Mamansse <nT P15. Mercury *o.2o

16, Nickel <Ma P

17. Potassium NR

18. Selenium U F

19. Silver <\o P20. Scdlun NR21. Thalliun <»« F

22. Tin *&> Bf23. Vanadiun <2oiP

24. Zinc iff P

Percent Solids NR

pectnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of, such flags must be explicitand contained on Cover Page, however.

.Cannta: 1— . ,'• •" " .

Lab Manager /Tfew ' . Mw.fri./V

Fora I ttf 3 «.-•.-t"» * 'y «/W

Exhibit aPage 6 of 12

•v-U.S. EPA Contract Laboratory Prcgrra ,,1A EPA Sar?le NO.Sarole Management Office •X'Ap,Q, Boit BIB - Alexandria, VA 22313 ff\9i"OS'JI703/557-2490 FTSs 8-557-2490

Date 3/3J M _

INORGANIC ANALYSIS DATA SHEET

LAB NAME (LvvvUL i, \HV \ V=AOC.. CASE NO. 3.U2.7 Alfc&S\ ^

LAB SAMPLE ID. NO. .fJiAai'lftfc,,,.. OC REPOBS NO. 0 -180

. Elements Identified and MeasuredMatrix IW««A /. \ m/uot1. Aluninun < OK> 92. Antimony ^ao t

3. Arsenic « C

S. Beryllium <S* 9

6. Cadmium < 1 F"

7. Calcium NR8. Chroniun <io P

9. Cobalt <Sb P

10. Cocoer <So 9

11. Iron tot 912. Lead (f F

Cyanide „, ,_

rag/kg (Circle one)13. Magnesium NR14. Manganese H9 ?

15. Mercury *".2o16. Nickel <Ho f

17. Potassium NR

18. Selenium , • <i_ ?19. Silver <io' P20. Sodium NR

21. Thallium t ,o F22. Tin <2e"&f

23. Vanadium <lco 9

24. Zinc <ta 9Percent Solids NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Ccnatntst••N-T. §11714 (1

tab Manager jt&4<<n*"*r**w

Fom I 0 d .j s,

Exhibit BQ^r P<»S« 6 of 12

U.S. EPA Contract Laboratory Program J EPA Sample No.Simple Management Office *»• ' nP.a. Box 818 - Alexandria. VA 22313 IY\K-OS75" _703/557-2490 FTSi 8-557-2490

Date 3 2| SA

INORGANIC ANALYSIS DATA SHEET

LAB NAME (LwW.L«- VnoLVtiA {W*>. CASE NO. MM %OR\ ^

LAB SAMPLE ID. NO. pelv _ ,

. ElanentsMatrix {yufgyig /* ~\.

1. Aluminum taoe 92. Antimony < 0.0 C

3. Arsenic /..I f4. fun-turn 1U3 oS. Beryllium <«• P

6. Cadmium <l P

7. Calcium NR8. Omnium <i» P

9. Cobalt <5o P

10 . Cocoer < So P11. Iron 5B<^ 912. Lead <S" f

Cvanida

OC REPORT NO. &<\-\$O r

Identified and Measured

r ragAg (Circle one)13. Maqnesiutt NR14. Manganese \Aoo ^

15. Mercury 4-°< °16. Nickel <te P

17. Potassium NR

18. Selenium <ft P

19. Silver ' <\a P20. Sodium NR21. Thallium <io C

22. Tin tZt»^P23. Vanadium <aoo P

24. Zinc It P

Percent Solids MR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Ccnnents: „,„...,,'•vT .

\ *

\

Lab Manager nM$> wtM»4**£f

Form I 011715«H CGC«*0

U.S. EPA Contract Laboratory PrcgraiSarnie Manajsnent OfficeP.O. Box fl!3 - Alexandria, VA 2231703/557-2490 PTS: 8-557-2490

INORGANIC

LAB NAME (kA.'.L. \\,oL.Wltaio\ ^

LAB SAMPLE ID. NO. flUeo'ill

. Exhibit B»$iV Pa3a * °f 12

n ^\ EPA Sample No.j (HR-osV'/

Date 3/ai/fltj/ /ANALYSIS CftTA SHEET

CASE NO. .fl Jf /qioo91

OC REPORT NO. fll-ISo

. Elements Identified and MeasuredMatrix yiu,U£flA£i -s-v

\ /ug/tpr1. Aluminum (n$L> 9

2. Antimony /ao P

3. Arsenic <f P4. P iun t\tto P

5. Beryllium <«r 9

6. Cadmium < 1 P7. ''•'ciun NR8. Chromium <to P

10. Coocer (So P

11. Jron < s-o P12. Lead <S(?

Cvanide

raj/Xg (Circle one)13. Maonesiun NR

14. Manoanese / 17 PIS. Mercury 40.2o

16. Nickel <t\o P

17. Pctasaiun NR

18. Selenium O £19. Silver <io f

20. Sodium. NR

21. Thallium <\°122. Tin <2oBls

23. Vanadium ttoa P

24. Zinc 33 P

Percent Solids NR

Fcotnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Ccantnts: A««i9tR

Lnb Mtmacer "%*•**<. *<' f W>*T**'&{

porm i 19 G3::u

•Wiibit B7359 5 of 12

U.S. EPA Contract Laboratory Program 2?A Sample No.Sanple Wanagenent Office • .P.O. Box 818 - Alexandria. VA 22313 (Y1K-OS'I74703/557-2490

LAB NAME (j«\

LAB SAMPLE! ID.

Matrix \t\4iev\1. Aluninun

2. Antimony

3. Arsenic4. """"inn

5. Bervlliio

6 C&oniun

9. Cobalt

10. Cooper11. Iron

12. LeadCvanide

ETSi 8-557-2490Date 3/a.L/Ril

/ '"INORGANIC ANALYSIS DAIA SHEET

A\» Wrv;LW\ ,-ax.. CASE NO. fl>\J.f qi.ft 9\ \

NO. ft^OB^I W & CC REPORT NO. S4-I6O

Elements Identified and Measuredf, X"">K

(jjg/L>r mgAg (Circle One)^S^ P 13. Maqnesiun NRila ? 14. Manaanese i\f P

<S P 15. Mercury <0.io

lioo f 16. Nickel <i»o P

<ff P 17. Potossiun NR

<fo 9 21. Thallium < lo C

<«•<> ? 22. Tin <&t>"%f

\\ 9 23, Vanadium ' <a/se P

<S0 24. Zinc (.3 P

Percent Solids NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however,

Connents:011717

\J ' Lab Manager,

Form I

IiU.S. SPA Contract Laboratory Program \\"fSample Management office <<MP.O. Box 813 - Alexandria, VA 22313 '703/557-2490 PIS: 8-557-2490

I

• - ' INORGANIC ANALYSIS DATA SHEET

LAB NAME (LJ.w'.L. f i>L\.!tA (Uoe.. CASE NO. .\ ^

LAB SAMPLE ID. NO. fi pfl , ,

L Elementsstffl a . ^\ / ug/L,

1. Aluminum /2oo 9

2. Antimony <CLa C3. Arsenic <«• P

4. P"*"iun U*4 P

5. Berylliun <f P6n._iljiil__iu J \ 0• jff* BH11HH ^| \m

7» ''•'cium NRa Chromium <ia P9. cobalt <s-o P

10. Cower <fo9

11. iron 3M P

12. Lead <S" C

Cvanide

QC REPORT

Identified and Measured

&r rag/kg (Circle One)13. Maqmsiun

14. Manganese

ixhibit B'age 6 of 12

EPA Sample No.OlR-os'To

tote 3/a|/(}4

pNO. SM-180

NR

8**P

IS. Mercury <0l2°16. Nickel17. «*.«4,«

f4a fNR

<o C '19. Silver <\e> P

NR

21. Thallium <io C22. Tin <2oBI*

23. Vanadium iiix, 9

24. Zinc art 9

Percent Solids NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes, explainingresults an encouraged. Daf inition of such flags must be explicitand contained on Cover Page, however.

Ccnnents: . ,, _ -..,.,«-v j . — —— ""• ———— OUT*'" —

\s

Lab Manager

Form I ft

i£&#4k«&»4-

Co::*

U.S. EPA Contract Laboratory PrograSanple Management OfficeP.O. Box 818 - Alexandria, VA 2231703/557-2490 PTS: 8-557-2490

' " INORGANIC

LAB NAME (UJli Lfl Vi^»\Ava\ f\ ^

LAB SAMPLE! ID. NO. gUflfi'llS' „

Exhibit BPage 6 of 12

m Ji**'' EPA SamPie No>3 ^ P^R-OS1^

Date .3M./2J/

ANALYSIS DATA SHEET(K ,D<L. CASE NO. 2, afn((fi

CC REPORT NO. 84-lgD

. Elements Identified and MeasuredMatrix VkflfiSfcft cs

1. Aluninun ?0l? ^

2. Antimony <aa P

3. Arsenic < f P4. Barlun I'rS P5. Bervlliun tf P

6'. Cadmium < 1 P

7. Calciun NR8. Qii.Liiihin 5s" P

10. Copper S"o P

11. Iron t&iooo f12. Lead <S* P

Cvanide

rag/kg (circle One)13. Magnesium NR14. Manganese 3,530 P

15. Mercury *°2»16. Nickel IS f1^ r^>ha _• jili .11 MB

18. Selenium < 3 P

19. Silver t\o P20. Sodium, NR21. Thallium < lo C22. Tin BF

23. Vanadium <2ao i124. Zinc 5% P

Percent Solids MR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Pace, however. ..

.Cements: fl1l71<)"'"•s* . . ' " "

s\

Lab Manager 1$*# /)«a*£<**»r

. qP0"8 I *• » .•( ,-( n ,•, . |

|b •••• U w %•> u '.ft

Exhibit BPage 6 of 12

U.S. SPA Contract Laboratory Program \f^"Sample Management Office HP.O. Box 313 - Alexandria, VA 22313703/557-2490 ETS» 8-557-249,0 . . ,

Date slai/at/f~ I

• ' INORGANIC ANALYSIS DATA SHEET

LAB NAMEO^^iaa 'LxLVfaA ftwga. CASE NO.

LAB SAMPLE ID. NO.

Matrix Luft -4

1. Aluninun2. Antimony

3. Arsenic4. BartonS. Beryllium

6. Cadmium

9. Cobalt

10. Coooer

11. Iron12. Lead

Cyanide

flftBoMHn OC REPORTelements Identified and Measured>**"'\Q5 l)or rag/kg (Circle One)

<CL6f> 9 13. Maoneaiun<aa P 14. Manganese,

t f F 15. Mercury

(,810 9 16. Nickel

<y P 17. potassium

< 1 P 18. Seleniun

<\o P 20. Sodiun,

<Sb P 21. Thalliun

^So P 22. Tin <Yftlo P 23. Vanadium

<5 P 24. Zinc

Percent Solids

1

NO. 64- ISO

NR

*»fc10 f

o-a.C4t> PNR

<a ?<lo P

NR

<IO C

:2o-Bf:

ttoe fW PNR

Footnotes: For reporting' results to EPA, standard remit qualifiers an used adefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Dafinition of such flags must be explicitand contained on gover Page, however.

sCcmments:

Lab Manager

Ponal

ashibit B?ag<3 6 of 12

U.S. EPA Contract Laboratory ProgramSample Management OfficeP.O. Box 818 - Alexandria, VA 22313703/557-2490 ETS: 8-557-2490

Date 3INORGANIC ANALYSIS DATA SHEET

LAB NAME(jAs

LAB SAMPLE ID.

Matrix .ftyxoii

1. Aluninun2. Antiatnv

3. Arsenic4. Bariun5. BervUiun

6. Cadmium7 Caleiun

XoiAA-VeA. Woe. CASE NO. a a7/<i(.op\ - r A 1

NO. a iaBl * REPORT NO. fltt-lfiO

Elements Identified and Measured

(W/L)OT rag/kg (Circle one)<oooP 13. Maonesiun NR<lo p 14. Manaanese 1,00.0 f

«•£ 15. Mercury <0-2«it a P 16. Nickel <4o P<.«• P 17. Potassium MR

<•! P 18. Seleniun «f.1 F

8. Chnniun /to P 20. Sodiun NR

9. Cobalt

10. Caeeer11. Iron

12. Lead

Cyanide

<«3 P 21. Thallium < |o P<*»» 22. Tin <2«BP>

"A 9 23. Vanadiun ^looP

<f P 24. Zinc \»^ P

Percent Solids NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Lab Manager

Form I CJ*1 '.*"\

\

Page 6 of 12n

U.S. EPA Contract Laboratory Program ^p \ EPA Sample No.Sarole Management Office W* ton *•/ fP.O. Box 818 - Alexandria. VA 22313 V\ NK-OSXoS _703/557-2490 ETSs 8-557-2490

Date "3 /a/ /&dI i

' ' INORGANIC ANALYSIS DAIA SHEET

LAB NAME (jj<vbl ofl V,( ,Vriia.V i*oc.' CASE NO. iMa.1? /RlooR __ .\ \

LAB SAMPLE ID. NO. gHoVftft „ ,

ElementsMatrix jWfiu&__ r\

\ ^ ^ f\iJ/U

1. Aluninun <1oo t

2. Antimony < la £3. Arsenic <tfP4. Bariun <ioePS. Bervlliun <«T P6. Cadmium <| F

7. Caleiua NR8 Chremlun <io P9. Cobalt <.ffo?

10. Caccer <So911. Iron <6b P

12. Lead <S?

Cvanide

lOC REPORT NO. J3SL-.I &°. „ __ ^

Identified and Measured

or rag/kg (circle one)13. Maqnaslun NR

14. Manqanese o,ftP

15. Mercury *&2o16. Nickel L<\r>917. Potassium NR

18. Selenium < 9. 7>19. Silver <\e P20. sodiun, NR21. ThaUiua < la &22. Tin *S»B^

23. Vanadiun floo P

24. Zinc 3U P

Percent solids NR

Footnotes t For reporting results to EPA, standard result qualifiers an used as• defined on Cover Page. Additional flags or footnotes explaining

results an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Cements: 011722'•xT.

\\

Lib Manaoer A* S. ,|3wtu»*VT**K7'

Fora I ^^ *tcc;;y

i, v. i

U.S. EPA Contract Laboratory Program x'U'"Sample Management office '•P.O. Box 818 - Alexandria, VA 22313703/557-2490 TO: 8-557-2490

I

INORGANIC ANALYSIS DATA SHEET

LAB NAME Pa«\».*.Lt V « a- ' CASE NO. _\ \

LAB SAMPLE ID. NO. &\H?.eff<S_.. CC REPORT

Elements Identified and MeasuredMatrix jWujfiufi — *

\ /ug/Liormg/kg (Circle One)1. Aluninun a<56 P 13. Maonesiun2. Antimsnv <io P 14. Manganese

Exhibit B'age 6 of 12SPA Ssriple No.P'lR-OS'iH

3ate 3/ai fuji

tt aT/lt.o (?iNO. aK-^eo

NR

«.Q30 P

3. Arsenic l<*P 15. Mercury *0>2o

4. Barium l,e<to P 16. Nickel5. Barvlliim <>** 9 17. Potassium6. Cadmium < 1 P 18. Seltniun

7. Calcium NR 19. SilverA fhfWfHtVfl QA P 9fl QM^flMI

9. Cobalt 61 P 21. Thalliun <

10. Cocoer <•£& 9 22. Tin ^11. Iron 3T (ooo P 23. Vanadiun

12. Lead <f P 24. Zinc

n<\ 9NR

<ap/ift pNR

10 C

2c B4

^loa*lot P

NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined en Cover Page. Additional flags or footnotes explainingresults an encouraged. DtCinitlon of such flags must be explicitand contained on Cover Page, however.

^.;» . 011723>' Lab Manner i . , 41

Form 1 V

r\ $&U.S. SPA Contract Laboratory Program USample Management Office > i 'P.O. Box 818 - Alexandria, VA 22313703/557-2490 PIS: 8-557-2490

INORGANIC ANALYSIS Dm SHEET1 / A l l I A

LAB NAME Ga LfdU ftfisLltisaJ //»<*•• CASE NO.

LAB SAMPLE! ID.

Matrix L eu,

1. Al|vninun2. Antimony

3. Arsenic

5. Berylliun

6. Cadmium •1. Calciun8. Chiiiiiliin

9. Cobalt

10. Ceceer11. Iron

12. LeadCvanide

/ /HO. flffOIJfll

Elm

<a.o 9<f G^<a P<«•<»

• < l FNR

•Si?P

83 P

<ffo P3L.f>pao f

« C

Exhibit BPage 5 of 12E?A Sample No.P1R-0S&3

Date Q/a;/p</i i

MM/leaO R/

CC HEMRT NO. »t-l«>

ents Identified and Measured

j/pcr rag/kg (Circle One)13. Maonesiun

14. Maraanase

15. Mercury16. Nickel

17. Potassiun18. Saleniun

19. Silver20. Sodiun,21. Thalliun

22. Tin

23. Vanadiun

24. Zinc

Percent solids

NR

3(.iTo 9t9.Zo

\ff)* 9NR

•< a-c13 P

NR

<\e> P<aocV

<acc p•3M P

NR

Footnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained on Cover Page, however.

Consents:-s:. Q117gi

Lab Manager

Fora I • *S '

Page 6 of 12U.S. EPA Contract Laboratory Program £?A Sample No.Sample Management Office •P.O. Box 818 - Alexandria. VA 22313 M-OttZ703/557-2490 PIS: 8-557-2490

Date 3/2//W

INORGANIC ANALYSIS DAIA SHEET

LAB NAME ( VaU ffaji / ' /hsec, CASE NO. MM/QbC R

LAB SAMPLE! ID. NO. fMftjfiftL.TW/

ZW QC REPORT NO. &M-IPOf

A ' Elements Identified and MeasuredMatrix fku£ffu&m 4-i.

1. Aluninun J2a A P

2. Antimony <lo C

3. Arsenic < tf 54. Bariua lt*S 05. Beryllium « 0ge i 4n4«fni 1.0 C

7. Calcium NR8. Omnium 4 10 P9. Cobalt tfo f

10. Coooer ^ $O P11. Iron V, 380 P

12. Laad << P

Cvanlde ,

' ng/kg (circle one)13. Maonesiun NR14. Manganese 3)3 ft15. Mercury *o>2o

16. Nickel <Mo Pnpr.fc-.i- 1 1 ... MB

18. Seleniun <Q. C19. Silver <lo P20. Sodium, NR

21. Thalliun <\o 22. Tin <56BfS

23. Vanadiun J£co f24. Zinc J O3o P

Percent Solids NR

Pootnotes: For reporting results to EPA, standard result qualifiers an used asdefined on Cover Page. Additional 'flags or footnotes explainingresults an encouraged. Definition of such flags must be explicitand contained en Cover Paga, however.

^- . t . *

Lab Manager £*«*&• £{•}&**>&***£(

Exhibit B?age 3 of 12

U.S. EPA Contract Laboratory Program \A? " ' " ^ Sss! ie No.Sample Management office I " /^ .9,0, Box BIB - Alexandria, VA 22313 nK"6SCo( .703/557-2490 ETS: 8-557-2490

Date 9la.iiBtl/ '

• ' INORGANIC ANALYSIS DATA SHEET

LAB NAMELL//v%A ti aLl"<3l /LfO.. CASE NO. SslS.? Mbo*

LAB SAMPLE ID. NO. fflff 0 m]l

A ElementsMatrix JiautB , _, A-L

1. AlJnun <«a 9

2. Antinonv <ae ?

3. Arsenic < f P

5. Beryllium <*" P

6.. CacMum . < 1 P7. Calciun NR8. Chrcmiun </o f'9, r/*wit 'ftfd P

10. Coocer <so f

11. Iron 5W</ P

12. Lead <S PCvanide

Footnotes: For reporting resultsdefined on Cover Page.results an encouragedand contained on Cover

.Cements:•s* .

OC REPORT NO. g<H&5>

Identified and Measured

r rag/kg (Circle One)' 13. Magnesiun NR14. Manganese itko f15. Mercury O.Zo

16. Nickel <«o P17. Potassium NR18. Selenium <a P

19. Silver </o P20. Sodium, NR21. Thallium ^la C22. Tin <2oB(*>

23. Vanadium {.CLon P

24. Zinc &o P

„_ Percent Solids . . NR .

to EPA, standard result qualifiers an used asAdditional flags or footnotes explaining

. Definition of such flags must be explicitPager. however. .

————————— OliTffi

Lab Manager A&A40wtw<fci\««/r

Bsrml o

„ *W'V?age 7 of 12

0. c. saprt r«, gjU-i^oINITIAL AND CCOTINUING CALIBPATICS VSRI?ICATICN

IABNAME1

DUE ^ 9

Metals:

R«wVip<Ae>(i I^^VVcAV VA'\ >

1 PkCj

Control LimitsICP/AA Furn.

1. Aluninun 85-1152. Antimony 85-1153. Arsenic 86-1144. Barium 84-1165. Berylliun 87-1136. Cadnlun 80-120

NR8. Chremiun 88-1129. Cobalt10. Coppsr11. Iron .12. Lead

78-12283-11788-112

78-122

lOC • CASE NO,

UNITS

Initial callb.lTrue Value IR*Ioo io/»fld. S"ft. a

toaaa

1S&

"i

ISO

ran

3*0(iOO

' '90

/Wloollfi

95la

inlotI0\

leS13 •

flia7M0«)0

Contimlro Calibration2True Value 1R 4R 3L.

lo loO la*)

ffa irf" i y3°O IQ ' Ijfl

lo Io3 |B!?3 lt>3 IMf

S InM 1^

la lal loif

l.b loO Ini

10 101 Iai

10 lea \n\

f ' lea Iai13.. Maonesiun NR ' '14. Manganese 90-11015. Mercury 80-12016. Nickel 89-111

3Se>1.09a*A

103/•7

101

IO |rf> 1 .

s.So 7•.0 l« H.1

17. Votassiun NR18. Selenium 85-11519. Silver20. Sodium

80-120NR

21. Thallium 88-11222. Tin 75-125

itleeo

as.a'• ft.

Irt

I0K

160

18

23. Vanadium 90-110 T&> IM24. Zinc

Other:Cyanide

75-125

80-120

aao

1 Initial Calibration Source £2fl wil.iLAi

la«

•WB «8»

*A < < <)tl

8.3 <W q

ri IOO Io4So lid. (04 hoIO lot (o-sl&. Ion Idff

0117271Ml»li. ,«ei-a

2 Continuing Calibration Source,_____

t »II

isuuuu B?2C,8 8 of 12

Q. C. Sacort :o.BLANKS

LAB NAME (jmhsL*. llaLl&al La*,. , CASE NO. fl- flT /Ho ff

DATE 5/lllfti• 1 i

PreparationCcmpound< _Metals:1. Aluninun2. Antimony

UNITS - / ,,. .

Initial Continuing Calibration*Calibration Blank Value Preparation Blank ,Blank Value i i i i i i $•

11o6 NR I'flpa flan <lc

^o» * , ^ao *Ae <&3. Arsenic if * <tr if <S

5. Berylliun6. Cadmium

8. Qirmilum

t\en * <IBB <i«» <i«/r « <* «• <s<l.o " /i.o /l.o <i.NR *^te " <ia <,» <ic

9. Cobalt <*b * t.Go tfo tt10. Copoer11. Iron12. Lead13. Mmwsiun

<SV» * • <«B • «b '<*

< *r» ^*a Klft ^ << • ** is 4SNR "

• J tA————————— ___ ———— • « • . ——14. Manganese <t# • <n? ^i* <«•15. Mercury16. Nickel17. Potassium

* 0,20 • 40.10 «0.20 > <«^

/Mo * <Uo ^0 <ieNR *

18. Selenlun la " <*2. •<£ 319. Silver20. Sodium21. Thalliun22. Tin23. Vanadium24. Zinc

Other:Cyanide

NR •<*ie> ' ^10 «lo ^ia

* 21 2O 2o/9dB * ta«> jfl, 4 .4

*

011728Not required at this time . f L .

« ^^Fomm

Page 9 of 12g. C. Report No. ev-&o

1C? ttJISRFERBCS CHECK SAMPLE

LAB NAME Q^AA** lUl.UuA Asset.

DATE 3/21/84

Control Limits3Comcund Mean* 2X Std. Cav.Metals:1. Aluninun

3. Arsenic

5. Bervlliun

CASE NO. QWl MttORCheck Sanple 'i.o.'jMP.auiCheck Sample Source tffl/<Units ^n/j r

Initial FinalTru&2 observed 4R Observed

3bc£O 90fl} In*! iMaoe 11 *

1 ooo »,* i 4< lab*9no l«.1 491 l ff

ri <.

4R

I1?

lainOQ

8. Chrcnltin9. Cobalt10. Ccocer11. Iron12. Lead

/jO» 431. 44 4tt

!J"» ( T ' IflU 9 0

l.tee 441 44 4«C, 196/000 I33.MB lu. OljiOO

Ifl

Itfl

1l

no

13. Maonesiun14. Manaanese /.o» <H£ W t«< 9415. Mercury16. Nickel 4M /tea 46 993 ...17. Potassium18. Seleniun19. Silver DM. M«4 ma «dV 10820. Scdlun

22. Tin23. Vanadiun24. Zinc

IBBO 4ftk 1h" Q/H

l.frv. 13<( 44 m4ft

111 Mean value based on n • __ . •2 True value of EPA. ICAP Quality Control Sample or contractor standard.3 Not required at this time. 011729

'Ran IV fc M« w^.J^j

/., .",--•>IPage 10 of 12

0. C, Rspart Ho. gu-^o

SPIXE SAMPLE RECOVER*

NAME Qj>m\..'.L._ A.WA ILec.. CASE NO. 3AM llt,oK_

DATE 3 9; \ EPA Sample So. m-pfrl-

\ gu Lab Sample ID No. a«an'rtfl_Units ^nLi __

Matrix kufiaua. - ''"Control Limit Soiked Sarnie Sarole Soiled

Cempound «R Result (SSS) Result (SR) Added (SA) tR*Metals:1. Aluninun 80-120 1*0.0 <aeo aw a 32. Antimony 75-1253. Arsenic 75-125

80-120 Joao <iao AAOA 1l5. Bervlliun 80-120 1.41 <#' 1.1.1 186. Cacmiun 75-1257. ''"Tciun NR8. Chrcmiun 80-120 "Jims < IB 3aae 9t9. Cobalt10. Cooper11. Iron .12. Lead

80—120 ^iao < So 3000 lo*80-120 9ict& <Set rCflfla l/<

80-120 3350 Tf 7-jfta IR75-125

13. Magnaaiua NR14. Manganese 80-120 ?sia IS ' MB* Q.<L13. Mercury 75-12516. Nickel 80-120 94oe /4a 3ooo 117. Pot»«»<««8 NR18. Seleniun 75-12519. Silver20. SodluB

80-120 3flLft <i« 2116 <ilNR

21. Thalliun 75-12522. Tin 75-12523. Vanadlun 80-120 3ilB <aoo mso <\f24. Zinc

Other:Cyanide

80-120 311.0 ff 333o °A

80-120

i IR • USSR - SR)/SAI x 100 011730Ccmments: •

PonnV

Page 10 of 120. C. Report No.

SPIKE SAMPLE RECOVERS

LAB NAME Ca j

DATE 3/3,/

lr'4f Hfl4/*-1' "*"•• CASE NO. MSf/fLO /?/ * EPA Sample (Jo. ' flU. nfffrg

i/Ai/ Lab Sample ID No. gftyrw' Unit3 ^T/g-Matrix /ftnuMu* //

/Control Limit Soiked Sairole Samnle Soiked

Metals:1. Aluninun2. Antimony3. Arsenic4. Barium5. Berylliun6. Cadmium

8. Qirniiluni9. Cobalt10. Copper11. Iron12. Lead13. Magneaiua14. Muflaneso15. Mercury16. Nickel17. Potassiun18. Selmiun19. Silver20. Sodlun21. Ihalliun22. Tin23. Vanadiun24. Zinc

Other:Cyanide

1 IR • ((SSR -

Concents: •

4R Result (SSR) Result (SR) Added ISA) «R'

BO-120 3(00 ^Ooo 3'3'3o 175-12575-12580-120 33Te </oo 39a PA80-120 6 9 «• I.L.*r <M75-125NR

BO-120 33oo <lo 1-iZo V\BO-120 J3ao . <$b *3ooe lol80-120 3 do <rf<9 <3?'9b 4.H80-120 '. ?Q-«ft <Sa 3390 "t75-125NR

80—120 357o ia' ' 3 30 875-12580-120 44qo <Vo <aeee 11NR

75-12580-120 3480 </o aiTo 106NR

75-12575-12580-120 3330 49aa 33?e A*I80-120 39<o <i "3 te <t*r

80-120

m"* * 10° 011731

AC) ,.,„.. .,m* v ••»--**Pormv

Page 10 of 120. C. r-seort No, gH-J[8o

'' SPIXS SAMPLE RECOVER*

LAB NAME A LVo.. ,iLl.AvJ>\ fUa-.. CASE NO.

N

DATE Q fll B^/ l EPA San le No. flU-a j./,,.,.

Lab Sample ID No. «//yifrflft_Units uilQ .. ..

Matrix Aai fl, (/Control Limit Spiked sarcole sample Spiked

Metals:1. Aluninun2. Antimony3. Arsenic4. Bariun5. Berylliun5, rju+nlim

7. Calciua8. Chromium

10. Copper11. Iron12. Lead13. Mamsiua14. Mammae13. Mercury16. Nickel17. Potassiun18. Seleniun19. Silver20. Sodium21. Ihallivm22. Tin23. Vanadiun24. Zinc

Other:Cyanide

1 IR • ((SSR -

Commits: •

«R Result (SSR) Result (SR) Added (SA) W-

80-12075-125 'itf ^ ^ "a 'nlT75-125 ifg.t -ts.6 fc "ITBO-12080-12075-125 <>3.Q In *. o ie«<NR

80-12080-12060-12080-12075-125 HU.8 <So ' «*o. 49NR

80-120 '75-12580-120 •NR

75—125 So la <2.o 9 loiBO-120NR

75-125 MI..8 ' '. <lo So <?<(75-125 *)!>.? l&d ?o lib80-12080-120

60-120

SRJ/SA) x 100 011732

Page 10 of 12Q, C. Report No. jW lfip

SPIXS SAMPLE RECOVER*

LAB NAME Af

DATE 3/ai

«U°Lt 'H\>W>\ flsMft. CASE HO. O.M?.Tffl ^1 \ EPA Sample Mo. ' ({.ajfiifl,,.

ft Lab Sample ID No. gjmoj%_" "" Unita *uaJJL •

Matrix (Waua ''Control Limit Spiked Sample Sample Spiked

«R Result (SSR) Result (SR) Added (SA) WMetalsT ~ '1. Aluninun 80-1202. Antimony 75-125 Sft.ft <lo s*a lao3. Arsenic 75-12$ Mt. M /<•« A qs*

BO-1205. BervUiun 80-120D • CAdoiiufi 75 125 ^r /i «? i ft ^Pi d i /^

NR8. Chranium 80-120

10. Cooper. „11. Iron-12. Lead

80-12080-12080-120 '75-125 qa.3 «r *» fi<

13. Maoneslua NR14. Manganese 80-120 '15. Mercury16. Nickel

75-125 2°3 <0,2o 2.oo /,„.80-120

17. Potassium NR18. Seleniun 75-125 <M.a il.o -so- 1ft19. Silver20. Sodium

BO-120NR

21. Thalliun 75-125 44,1 . <ia So °(&22. Tin , 75-125 »S.fc <?.T ffo «arTll23. Vanadlun 80-12024. Zinc

Other:Cvanide

80-120

80-120

1 IR • [(SSR - SRI/SA] X 100

Ccnmenta: • ,__ 0117*1

flora V :f

Page 10 of 12Q. C. Report No.

SPIKE SAMPLE RECOVERS

(L=\A;v.a\ A«.-ae..

DATE ^ 2\ \ EPA Sample No. mn~ "SStL,

j flU Lab Sample ID No. ftgooaoa.Units _M|JJ.

Matrix Juntas, HControl Limit Spiked Sample Sarnie Spiked

CCTOCUfriMetals:1. Aluninun2. Antimony3. Arsenic4. Barlun5. Berylliun6. Caoniun7. Caloiun8. Chromium9. Cobalt10. Copper11. Inn12. Lead.13. fiaqneaiua14. Manganese

16. Nickel

18. Seleniun19. Silver20. Sodiun21. Thalliun22. Tin23. Vanadlun24. Zinc

Other:Cyanide

1 IR • [(SSR •

Ccnmnts: •

IS Result 1S5R) Result (SR) Added (SA) W.

80-12075-125 tfa.ft *1a So laa.75-125 Uff.4 <5.o <a <)l80-120BO-12075-125 y.tl <i.a <-.o 4ftNR

80-120BO-12080-12080-12075-125 <4 T.'l <£,O So. <*UNR

80-120 '75-12580-120NR

V5-125 >s\A <i.o sa ia460-120NR

75-125 tb.u . <la S& <?S"75-125 (•''•I 1*10 J £o 11080-12080-120

60-120

- SR)/SA1 X 100

011734

flormv

?ags 11 of 12

CTOLICATSSLA3 NAME 0\j.'.Lt- La\,.V. \ taaec. CASE NO, 1M1T

DATE 3EPA Sanpla No __

»/_________ ' W° Sample ID No.

. 10. Copper*>* • 11. iron

12. Lead

units^

CompoundMetals:1. Aluninun2 . Ant p fiv3. Arsenic4. Barlun5. Berylliun6. Cadmium7. Calciun8 Oumiun9. Cobalt

Matrix L ^Control Limit* Sample) S) Duplicate! D)

/.<t. ffK

JQ*Q 2LO

ft'.e £f.o< laa <\oo

<•< *f

<l ^1

NR< in /IO

<a *o

S1,!0

oftoo

oo

13. Maonesiun NR14. Manganese Q< ' <i<-15, Mercury ' '____16. Nickel_______________i^_____ /qp17. Potassium .____NR18. Selenium19. Silver

Va4 lo

<0Ab

O

ft

20. Sodium_______NR21. Thalliun______;_____ Via22. Tin23. Vanadiun24. Zinc

SlT* Vfloo O31 an *3\.S

Other:Cyanide

• Out at Control '.1 To be added at a later date. j«| . 0*1735

2 RPD • t|S - D|)/((S •»• D)/2)J X 100 **

VT

« I" I V»

Page'n of 12

LAB NAMEjd

DATE 3a

0. C. ftocort No, af-jgO

DJFLICATES

wV»?Aao P1\Avi*a rf-AOh- CASE NO. { Jlfl /«|feftR

\ 04 ' Lab Saopla ID No. oaffioa _Units i^M

Matrix Unutet aCompound Control Limit* Sample) 51 Duplicate! D) RPD?

1. Aluninun /OBA 4*** o2. Ant<mnrtv /a /•. /ae O3. Arsenic /•? <sT o4. Bariua ins* iilo 9.95. Berylliun A* /«• a6. GflAnlum liOltf f.Oi 1.*.7. Caleiun NR81 Chrnn un ^i» /i* 09. Cobalt «o /ffo O

10 • uDPDBa? ri"Ta 4O A

11. Iron ' quw. uafio fl.S"12 fff <fi" S" a13.. Maonesiun NR14. MBnQanese 14 01 3 3 9kH15. Mercury16. Nickel Ma <Ho17. Potasslun NR18. Selenium <*a <1 o19. Silver <m /ta 020. sodium NR21. Thalliun • <io • <|o e>22. Tin23. Vanadlun ^Ooa oae o24. Zinc 1.Ma t| aia 1.7

Other:Cyanide

• out of control ^* To be added at a later date. ' ;' .2RPD" t|S-D|)/((S+ D)/2>!xlOO -

JflWon VT

LAB NAME £a«

CKTE 3/ai1

Metals:1. Aluninun2. Antimony3. Arsenic4. Barium5. Berylliun6. Cadniun7. Calciun8. Chromiun9. Cobalt10. Corner11. Iron12. Lead

Exhibit BPage 12 of 12

Q.C. Report No. giUgD

INSTWHENT DETECTION LIMITS ANDLABORATORY ONTROL STANDARD

A L,, ILLVrA VR.SCC.. CASE NO. Mtfht^R_\ *

BU

Reeuired DotectionLimits (CRDLl

200201010051NR105050505

1UNITS ug/L

Instrument Detection .Limits (IDL) fj|h Control Standard*

ICT/AA Rimace True »R17

*4H.S"

lo\f

or3.5*\*9£as" ' • ' • '

f.o13. Magnesiun NR14. Manganese15. Mercury16. Nickel17. PctassiuD18. Seleniun19. Silver20. sodiun21. Thalliun22. Tin23. Vanadlun24. Zinc

Other:Cyanide

150.240NR210NR102020010

10

toO.Zo

3b"

?.o/O

S.Olaif1,4

S ^-N •

1 Not required at this tine. '

Form Viz

a01

Is5=

s q o 8% 8 8d - (4

8 8rt 2

S'1

i*

and " a a 8 §

3 MJ.1

o°It M *5 a 8 8 aI i I I §^ • 3 - 3 ^ 1? * « S S

rtl

a t f800035

Hi 8

n

2'

rM,i : m: £ r> *r\

S

NV

Q

I ! !Si: ! i. . . . . . . . , . , . , -4_j_;_

\!8

i I

I I

i!i

' I I

I I I !

I i

i i I

1ATA > 36

STAlHJAPDUMION

W.WU.BNIUH il.JI'S C'EC nlllrt VOLTAGE

>ii.:i? :.v.,ii'j ,:oi iw7i',!,',42 i?ii.'i" !,:»'i! logo

:s7,6i s:uo,;:5 .on:;i.604 ii)n.i46 ,sa<;:n.,)49 373. 96:;. .07*,OB2 1000,04! IDOO

BLNK.9TD nCB QTHEN ftfl

I M. IOI S760

H.NK.STD <1ES OTHCK

: BA no 10:4DLNI..5TD nCS

UUNK.BTD TE9 OTHERIII B7U>,PLW.3TO n6S

H.NK.9TD t1E9 OTHER AOCU 49 13012

81.NN.aTD MES OTHER

FE mi. ::::«BI.NK.aTD I1ES OTHER AO

DUNX.9T8 1163 OTHER AS

•> M M7

. '"• •'

M'll'.IW, fit::, DIHBR _ ™>___ ____

ll.lll .HID .'I", ...

,, ., >"""" -"is;hum .UIC> ,1K!a OTItEi\

U ill !a U""o

011743O ._ . . -v.it-.-

fi -oooooa

.-.-: i t:.t DATE i 30-HAR-B4 USBi'KPCNriu i -:LP. c?u>i, cu:commons i FILE NANE«'.' ACT NflnE.'cu" DATE«'«'OTIM.I: miMO'i' cuDe.'i1 TVPE-'I'

Mf.nE CODE TYPE ANM.Y9I9 TIME

•..«', 1 :0"IMR-H4 10153.,.„., a 20«MfiR"i'i4 ioiS7noii 3 :o-nAR"B4 moi.X") S :0-HAR-94 ll|0f

9TD OuO 9 :0-tW)-94 lllldCAliE =437 BLANK ! I'nM 9 M-NAfl-34 I1|SOCASE S427 BLANK I 000 9 :0-t1ftR-94 11131CflEe 3497 BLANK 9 000 9 :o-nftR-34 11)36CASE S4S7 940r>7B8 ('0.) 9 30t1Afl-a4 11139CAliE !4S7 94IM79? I'nM 9 80-NAR-94 11|42CASE 3497 U4007TO vVl 9 SO-HAR-94 U|4Br.MX 5497 400791 000 9 !0-WAR"84 U|3JCASE S1S7 B40077I D OHO 9 SO-nAR-194 ll|37ME S497 8'W(i79= 000 9 SO-ttAR-a* IS|03Ch3E 34S7 9400799 SP 000 9 !0-NM)-a4 13)09CA9E S497 940i)7f3 000 9 9XMA-94 1S|13CA9B S497 84007M 000 9 :0-mH-94 13)17CALIS. CHECK 1 '») 9 JO-tlAfl-94 13|31OALIll. CHECK. 3 000 9 SO-IMR-B4 18)39liMl Z437 9400713 000 9 IO-nAR-94 I3|gfCASE 3497 Q4<,079o MOO 9 M-tUW-34 13) "CASE !)37 Q4IW97 «0 9 30-«*R-84 13|MClnH 3497 0400719 000 9 30-HAR-94 13)40Oi'.SE 3437 V'W>TTi 000 9 M-HAR-94 18)49CASE !4!7 9400?W 9P «i» 9 SO-hAR-B* IS|4?.•.ivii-: :<K7 avumiKi ouo a jii-twR-a4 isissPr.lir ;4?7 aWWil ntH> 9 50-nAR-B4 IS|5?CA9L S437 940001)4 I/ OuO 9 30-ttAR-a< 1)03CABE 34S7 9400901 1/000 9 :0-t1Afl-34 1|0*CASE 34'37 94MBOa 000 9 30-t1W-a4 It 10C..SE 3437 9400,9.}3 D 000 9 30-nAK-94 1)11ME 3437 94.MOO; OM 9 39-I1AR-94 1)17OALID, CHECK I 000 9 30-flAR-94 1)21CALIB. CHECK 3 <Xn) 9 :0-ttftR-94 1)39ICAP-INTER-CHECK 000 9 30-HM-B4 I|3B

O

r ,-„•-'• ,.. ' ,-.ii:37'' .-'' ".'X1'606 ,i»417S -.00115ii-.' ,,,,i-,'ii:i K'.W" .MM::: .,.110112 ,0111:5 ,0071:1•if-lNTLR-rHBCI 7I.1W.6 .'13)194 .192711 .976173 .514657 .940999

.',:;E ;:•:• r.Lf.iu : ,,',:4«7,i -'.(10070 '.oooi'»T -iixisC'6 -!ios?i ',000770.'E 3 :•* SLiW. I .-;,3I,|41 -,"i'i076 -.0001,4 -.01104 -.00331 -,00u77

• at. 2 I" BLrtNl 2 ,ir.7nl3 -.(10446 -.000(13 -.OOB37 -,00531 -.00039A 3 3 3" 44i)(i?9B .OW'tS .177503 -,00016 -.00231 -,00069 .001134

"".:,'.'• :«T 'MOu-'ll • '.Maim ',i.'7sia3 ,000*49 ,007467 -.00173 .001033C.'.tC 3.127 9400791 0 ..Sd-nu .097365 .000061 -.00733 -.00433 .004340CASE 3427 D400792 .'..71973 .043539 -.00004 -.01619 -.01333 .003662CASE 2437 0400792 9P 7.09009 3.01309 .631413 3.13646 3.11306 3.17699CASE 3437 9400793 .037601 .053933 -.00013 ,001733 ,003435 .005589CASE 3437 9400794 ,'176674 .433990 -.00003 -.00433 .007307 ,000579CAUB, CIIECl: I H'i.2703 10.3917 3.03433 10,3348 .029991 10,1013ClM.lt). CHECK 3 -.,'1990 .003330 -.OOD30 -.00993 9.1639B -.00037ilnOI! 3437 9400793 -.IU4703 ,275173 ,000399 ,034360 ,039329 .009299CA3E 3427 [1400794 .106195 1.90717 -,00004 -.00023 .006611 .001734COTE 3437 B4iW97 .075230 1.46339 .000041 -.00606 .001391 ,003973CAQE 2427 8400799 .127991 .271945 .000143 -.00037 .010091 ,006746CMK 3437 (HiW?! .,',77111 ,059911 -.00009 -.00006 -,00487 ,004819CASE 3437 B400799 3P 7.10735 3.36590 .658100 3,39798 3,31980 3,13949CA'JE 3437 9400900 .123070 1,83940 .000194 .03843? .096993 .006533CA3F. 3427 9400901 .134474 .331773 .000758 ,034610 ,093163 .014941CHdE 2437 B400900 UK ,019747 .229077 .000143 ,013434 ,011493 ,003303CASE 3437 9400901 III* .013334 .034302 .000093 .009300 .003937 .403011CASE 3437 94U0903 .'i'13234 .174580 .000061 -.00398 ,043844 .001734CASE 3437 9400903 0 .076674 ,163121 -.00036 -,00633 ,034101 -,00037CASE 3437 9400903 ,060194 ,493037 -,00010 -,00433 ,014366 ,405973CAMS. CHECK I 10.3971 10.3411 2,07161 10.4036 .023610 10.1497II.M.1B. CHECK 3 •••M470 .000461 .000441 -.00377 9,1130? -.00039ICAP-INTER-CHECK 77.99194 1.06117 .194032 .977303 ,343273 ,9S31?4

01*745

-l ...

6ATE I M-KAR-94 1 1 72

t'L.Mih 3TOCrrtfi :4'J? KAMI 7CASE Mi; tl.'M ICMI8 3457 QUID 2 .'024,

,71)503 .:tllQ-l -.(iiX'47 ,7:4923 ,:49343,,(''.'7,17 -.OI3"7 1.00227 -.00142 ,('03635.,Xi|i.mlJ -.00173 -.,.iOi)Q6 .006135 -.40073.976301 .079706 ,.1744!5 ,943073 .939417-,.',,..,,,,4 -, O'j'js: -.'.,0747 ,0 -,01)094,,,,11.975 -.0074! -.00743 .007077 -,001-71-,0'ioili -.011.77 -.00474 -.00414 ,047200

_. .... . _ . ..... ,,X'0709 -.04708 -.00474 -.04312 ,006589i'"E M" 14i..(.'M ,.".,|,1|.- .'.''71174 .'X'MII -.00794 .401023 ,04292?"Vl!i JI3" «.» ••-••' ,- "• " .--Mir/i! -,0'iMIII .001743 ,''• .014073,'...,g M:.' J.IO>.'-»., .IW.! l.|«944 ...,oo4'?7 ,408170 .404143 .071330CA'.S M27 MOOT1)! ,u4i.i7B? ,001234 -.00049 ,003473 ,412310 ,033945C.VJE 3'I27 9400791 D ,071267 .003533 .003697 -.00303 .009332 ,063878CASE 2437 9400793 .S2I630 ,044560 -.00371 -.00303 -.00303 ,134183ME 3.137 9440793 SP 3.3S4IO 3.31118 2,09372 2,06476 3.17090 3,16143CASE 3437 940<>7?3 .139773 ,046697 .406409 -.00390 -.00307 .139371CASE 3437 3400794 .369900 ,836696 .013904 -.00477 .003031 .211134CAL1B, CHECK I 10.1606 10.2412 ?. 10946 ,005208 10,1831 10,3336CilUB, CHECK 3 .019469 ,000604 .077136 9.36353 -.00303 .043398CAIIE 3437 8400795 101.123 3,33333 .079431 .004340 ,027697 ,033463rfiiE 3437 114110794 7.90849 4,06360 ,'102939 ,0 ,001023 .019637r.Mf. 3437 9440797 3,411337 ,967783 .11111973 -.00217 ,0 .0419*3I'.M'ii; 3437 0400798 .097667 1.03318 .020460 ,003478 .00312? .11237?CASE 2427 04407?? .433237 .029303 .0 -.00173 .001033 .034143CASE 3427 3400799 SP 3.22743 3,27213 2,92333 2.97588 3.31912 3,83313CASK 3487 9400800 143.169 6,23438 .114379 .004774 .043137 .101283CASE 3437 9400901 149,169 3,64671 .191849 .013433 ,068376 .034073CASE 3437 9401)900 I/It 37.0710 .733332 .010333 .003038 .001332 .011483CASE 3427 8400901 l/» 29.9916 .433198 .019327 .001736 ,007180 .014684CrtJR 3427 H4i'J08«2 4,60417 ,421303 .040180 -.00130 ,006133 4,37742CASE 3427 9400943 D 4,:7.9103 ,392773 .026129 -.00434 -.00307 4,22700(.iiiC 3437 94i'iii903 .344727 1.30466 -.00764 -.00320 -.00307 .020143CALIB, CHECK I 10,11119 10.336? 9.20090 ,406476 10,2964 10,3346iMUt. CHECK 3 .019015 .041626 .076170 8..36312 .001023 -.00263IW-INTER-CHECK 136,936 .993163 .923664 .430984 .181731 .912307

011746

• Mll,-,Ul'313 PILE DUMP -

22-MAR-94 9l39

FILENnne | CLP DATE CREATED I 80-MAR-94 10)92ART MM1E | CLP NO. CF OAKPtEB I 6

111 SAMPLE NAH6 CODE TVPE ANALYSIS TlltE BUNK? MOOS

I7S »3 440 3 20-IWR-94 10)3! N C

ELEI1 HAVE LEN CON/lriT 9T.DEV Kfl.9.0. BLANK BKO IE1 IE8 IE3 9LOPS Y-INT

AL :09.3I3 ,743041)3 .411644 1,36346 0 0 263,83 101,3OH !~.337 ,019336? .004092 21.2944 0 0 1689.32 110.3eC 713.043 ,6957937 ,003516 .793928 0 0 13190 66,29Cli 347,716 .1670003 .006994 4.12814 0 0 869.223 113.791:0 ::a.6i6 .506:021 .007331 1.43628 o o 718.444 14.3CU 721.734 .2519236 .'141898 ,749694 0 4 1397.02 42.249? jFF. :3?.94 ,431)9314 .4IJ6927 1.10170 4 4 3206,47 169.99?Wl :57,ol ,3619037 .1,06499 1.79793 0 0 5380,38 78.7411III 33l.6i'i4 .ISIoni.l ,418438 7,33510 0 4 1014.16 307.89nil ','MMiU -."'MJ4J4 ,1103604 -571,99 4 0 579,162 43'/ 592,403 .7509332 .439167 3.11469 0 0 ' 243.7 80'IN 313.936 ,2093432,4033791.96430 0 0 . '1337.9336.73

12 SAMRE NAUE CODE TVPB ANM.Y8I8 T1IH BUNK? NODI

ICAP-3 004 9 30-MAR-B4 10)37 N C

EL6H HAVE LEN CON/INT 3T.DEV ','.(!.3.0. BUNK BK9 IEI IBS IE3 SLOP8 Y-INT

HL 309.313 .0 .047302 -.3031E 4 4 368,99 101.3HA :33.327 .0032301 .003991 123.901 4 4 1623.32 110.3BB 313,043 .4 .00016? .6466B* 4 D 12190 66.29CP. S67.7I6 -.4H6067 .407933 -63.173 0 0 963.229 113.79CO 323.616 ,0441736 .009406 329.297 4 4 718.444 94.3CU 724.734 -.001150 ,404733 -63.938 0 0 1397,02 42.24HFE 3S1.94 -.4117969 .0117394 -90.631 0 0 3206.47 163.99?MM 337.nl ,00.17474 .404499 65,7499 0 0 9390,3279,74??Ml S3I.144 -.4130713 ,'Xi9349 -76.37B 0 4 1414.16307.29i.ti 720.111,0 I.-S92H3! .l'ii'8399 3.61413 4 0 373.962 43

011747

347,7 !4132','.'I T.I,73

(.•l.'iL'r'JU TlltS SLAW.? MODE

J...4W-84 llli'.l N C

cu,-i-ii no ici IE3 IE: SLOPE (-HIT'/".).r.1 I.'. -i7'I O 0 363.99 101,3.•.•Urn :..1.414' <i ''. 1623.33 110,3Oi'.c '..'. :?,<i447 4 0 13190 66.35 ,•.",.Ti'.i "'I.7SB7 il 0 (363.223 117.73•X'7721 13.7189 4 0 710,444 94.3,''-,.'.', '. ..IIIOI ,'> '., 1397.03 .13.3499,,,v.".',-.. -...i». .17 '., •', 3306.47 lal.iJ'Wwlllv |..,r.n7(, 0 0 3380,3378.7,199i)('40a: -i7!!.6U 4 0 1014.16 347,33001776 -199,19 0 0 ' 373,?63 4:! ,043297 06.0663 4 0 243.7 20«0';79Q -449,9? ') 0 1327,13 96.73

:.'.i,i(<4 ...XH7::::ii.,wi -.oixiaiB8V. 40! ,0061331:i;,'.!«4 -.(,047:3

114 TAMFLC NAME CODE TYPE ANALV919 TIME BLANK? HODS

IWif-INTCP-CHBCK 0*1 9 :4-flAR-94 11)01 N C

EI.EI1 UME LEU CUfllllir ST.DEV t',R,9,D. BLANK BK.B 161 IE2 IE3 SLOPS Y-INT •

AL 109.215 -.1.9606? .413783 1.30092 0 0 363.89 101.3 IBA 37-7,527 .1511943 .019704 3.07134 0 0 1683.32 110.3 !K 7J7.042 ,1927118 .0023:6 I.39B46 0 0 12190 66,29 •CR 2I.7.7II. ,9761736 ,OI(,67B I.7BIS9 0 4 963,233 113,73CO 37.1.616 .3146335 .4116l'l 3.23643 4 4 718.44414.3•III 774.734 ,94(l»999 .412953 1.37650 4 4 1217,03 43,3491 .ft 2S9.94 I.',S.413B 2.0278? 1.33301 0 4 82,04.47 143,19? iUN :;?,6I .=742617 .007-:07 .027182 0 0 33B0.38 78.7411HI .",l.n«4 ,13797963 .419679 2.336B4 4 4 1014.16 307.J3 -AO 730.069 ,4v44I)50 ,i'".''5B44 1,34660 4 0 979,163 43V :-)3,4'M ,94r,i)7S4 ,028!;99 :,;B944 4 4 343,7 30Z!l 313,936 ,4394|7>9 .006311 ,671963 0 • 4 . 1327.19 36.79

I!! 9AHF1E NAHE CODE TYPE ANALY313 TIME BtANK? HOOC

BLANK STO 400 9 20-HAR-94 11|I6 N ,C

ELEM UAVE LEN CQNMHT ST.BE1/ V.R.9.0, BLANK BKO IE1 IB3 IE3 3LQPC Y-INT

AL 7''.<9.2I5 -.006592 .007401 -54.710 4 0 263.83 101,3BA 277,527 -,002614 .001538 -59.02: 0 0 1623,32 110,9BE 713.042 .004U920 .000213 363.9?3 0 4 12190 66.35CR 347.716 .4409661! .U06639 743.942 0 4 065,229 113.79CO 238.616 -.00453:! .406363 -139.46 0 4 718.444 94,9SI! 734.754 ,0011!M .0047C3 77,3733 0 4 1297,02 43.2491re 559.'I* -.'Mil:.'; .043550 -310.6? 4 4 8246.47 t63.911MN ;!•.?,.11 -.oiiWA .4i»3".9 -516.44 4 4 9350.32 78.7499Nl 271..504 -.00962'' .402747 -57.203 4 4 1014.16 207.25HO Tfl.'V>a -.1111 47? ,Hil?.ViH -17.7T5 il 4 379.962 43

011748

3'ir. 7 !4I727.9S 56.75

<• .:,•.: >i> iinic c.im; tvir AN(,L(3I3 rim-- DLANK? HOOEr.SE 3.137 t'L,lHI 7 '\Vi 3 30-MW-94 U|34 'N C

SL3M W.'E LBH CUM-(FIT 3T.liE'.' 'm.3.U, 6U1NK SI'0 161 IE2 I S" SLOPE Y-INT

•.I. •••J.JIS .-'"-V174II .Ooio-l.' I5.M46 4 il 265,95 101,3Si ;",if> •,H,',,,7,-,? ,,.,,',.14! -1,72.4! 0 1 1625,73 110,3•-,- , r..,.i; , v,,x,,ii,i ,,-,,,,,,-.-.'.i pi,.in? ,'i o 1319,', »4,:s( -','u. -.,,"(,,.,.' ...,'T'.'.' -•>-.;,T'fl >:, 0 i36«.2«5 U7.72

CU r,i;.,>l6 '.0'W9I5 ,OOBa"-l -1411,!,: 0 0 719.444 94,SOi :.','.|.7S4 ,1,007709 .ilOHl-i IO>?,-:76 -0 " 1217.02 42.241?FE 3J9.9.1 .0424314 .405037 :96,483 4 4 ' S206j.47 163.9?? |Itl S57.ul .'Wi?7«7 .000971 0?.»41l 4 0 3380..32 78.749? IMi ::i,604 -.OU34SI .009223 -530,33 4 4 1014.16 307.33nil iTB.ilMl -."H"4"H .'Vi09Ml -:'8.!71 4 4 373.962 43 '•I 592.445 .0434773 ,006159 304,404 4 0 243.7 50 '7ii :i-,nri(. •.01117.17 ,«AIM -114.58 o o 1327.9356.73 •

• UNALYtiltl FILE DUnP -

32-HAR-94 lOlOO

FlLEIlnnE I CLP1 DATE CREATED I 30-flAR-84 11)21W HiHie t CLP NO. OP SAMPLES I 13

III SnHFLE NSHE COCL' TYPE ANALYSIS TIME BUNK? MODE

CASE 2457 BLANK I I'OO S 20-MAR-B4 II|31 N B

El.EI-1 UAVE LEN CDH/INT 3T.DEV W.S..D. BLANK BK8 161 IBS IK BLOPg Y-INT

>'4. 7,:i£l,:i,S .4244499 ,0'MI45 55.133? 4 . 0 363.93 101.39A 237.537 ' -.009767 ,0477311 -43.637 0 0 , 1623.32 110.3OS 717.442 -.004164 .000153 -94,648 0 4 12190 66,23CR 567,716 -.411846 .0113467 -29,268 0 0 869,223 113.79CO 538.616 -.00531? .003932 -73.434 0 0 718.444 14.3Cll 724.754 -.000770 .('111439 -199,3? 0 0 1317,02 42.349?CE 5i,'?,94 .0074779 .04364:! 34.9133 0 4 2806.47 163.991MM 557.6.1 -.404193 ,004779 -419,32 0 0 3350,33 79.7411HI 531.604 ".(111339 ,005115 -15,114 0 4 1014,16207.89A!) 558,060 -,004344 ,405241 -31,63? 4 4 379.162 43V 395,442 -.O'MIO.7 .044/70 -113.47 4 0 343.7 80ill 513.936 .0072004 .002079 63.7171 0 0 1327.13 36.73

•S SAMPLE NAME CODE TYPE ANALY9I9 TIME BLANK? MODE

CAHE 3437 BLANK 2 I'OO 3 50-MAR-84 IH26 N 0

ELEM HAVE LEM CQN/1NT 3T.OEV V.R.S.O. BLANK CKIi IEI IES IE3 SLOPE Y-INT

OU749" V

O

•'• .:': VI .•',.,•', '.'>

.,!•• .'ll.-'s'.l -!-••,„! JO

••••..: i-", ).»»:

,. '•• i -.1.1'-.'li, -Ml,"!••<•:•!•» :57.7'.'j..-, i 4 i!:.-ui7

.;.,,rvl •lO'l'.l.i0,:,7<58 -74.J94

'i ,,

0 "

0 n'I' 00 0

u::, :: no,:I319» 06,35•11,5.3:: 117.75

lR97,'i3 42, 24g93K6..I7 lnS.9993790. 7! 79.7499101,1.16 507,::S75.963 43243.7 34, -m .j »(j 75

,:'irc T1FE AIW.>9IS *!!'! OLANK" MODE

•:''") 5 20-,Wn-94 ll|7Q N C !I

Ci.EI'i HAVE I.EII COFI/INT CT.DEV '/.P..S.D. BLHNK EiKO IEI IE2 IE3 SLOPE Y-INT I

M, 108.213 .4791732 ,.W7S4 1,74143 0 4 363.83 101.3 'UH 333.357 .177,3477 ,00o059 3.49254 0 0 1623.32 114,3 iDE 31.7.043 -.04U164 ,0000/0 -47,971 0 4 12110 66.23 ;111! 7,47,716 -.045711 .01)5233 -350,67 0 4 863.233 113.73 ICO :2'J.ftli -,ij4'M93 .4011030 -IIS4.7 U 0 718.44494.3 !ttll 124,734 .OOH3I.4 ,004795 73,77™ 4 0 1217,42 42,241? jKB 2fH.?1 ..WI4I4I .003597 S.85773 0 4 2206.47 143.99?Illl .'!"'.61 ,"?9i;09 ,i,44!i7? 5.79691 0 0 3300.33 79.741?HI ,::i.A(i4 .(M34S11 .00/307 311.730 0 4 1414.16 307.33 Ihf> 729,460 -.403906 ,041662 -42,333 0 0 373,162 43 iV ?)2.442 .0010258 .405ini 204.00U 4 4 343.7 24 iI',* 217.956 .0429233 ,(•04492 14,4632 4 0 1327,93 36.79

44 .AHFLC IM15 COC'E TYPE ANALY913 TIME BLANK? MODE

Cn3E 2457 9404M9 -iOO 9 34-MAR-S4 IU42 N B

f.LEII'1 MW. LEI'I CON/IFIT 3T.UBV IR.3.D. BUNK BK8 IEI 1E2 IE3 SLOPE Y-INT

M. .709,313 ,432661ii .043761 7,14389 0 • 0 869,83 101.9DA 577,527 ,0194993 .00765? 39,9099 0 4 - 1629,39 110.3IX 7I3.04S -.'."X'OM ,('0'.'IS7 -535131 4 4' • '12110 66.29Cr. 4S7.7I.1 .OUI4447 .00:004 471.057 0 -4 - 963.329 113.79CCI 529,616 -,001311 .004357 -310.91 4 0 718,444 14,9CU 734,791 ,00,3(i622 ,041341 48,1033 0 0 1217,02 42.3411FE 351,14 ,0030511 .003319 92.3744 4 4 2206.47 163.919Ml) 237,61 .0017636 ,041087 61.6436 0 0 3380,3! 78.74??Ml 331.604 -,407999.007693-97,561 0 0 1014,16207.89flB 359.069 ,41)17031 .Ok'2184 167.774 0 4 373.963 43V 293.442 .4 4 • 4 4 4 243.7 50

,0149735 .041441 9.69546 0 0 1327.93 56.79

«", SAMPLE NAMF CODE TYPE ANALYSIS TIME BLANK? NODE

CA-iE 3457 0404794 "00 3 30-MAR-94 11)48 N 6

EUI1 UAVE LEN tQN.-INT fK.HF.V V.R.3.D, BLANK BKQ IEI IE2 IE3 SLOPE Y-INT

011750

•;,',is•«•criO)ftHIMlid711

. • .. . : 1 .

:;;•-',':r 3'.' ...I -i"3-1. '51SV.IIH7.61:;i. io47311.060: ",'. 402317,956

."Ti-jriii .

';'.!'.'!?'.'-;...,i n.i5'j. .T'ltia ,'SI1. l'?'*o4B":""i"";;.444|ft74".1.17175"!;

•"' ""' -'' '"

'"**'.i i'-al'-v,»-.,.^ •,101 !'.'!. !

,',l-,,57 jo,./:;.: i

, .47-l •',1'iJii1):".'.' i .'USS47

•:«,:;79 I44.-I54i,io,,-n i-i,:r,i3

" •:*

;. >tn «,:, 44 01 •'!4 04 44 0

m::,:2 no,!06S.225 1!7?75719,444 94,51597.02 42,2 93506.47 165.49933B0.32 70.74191014. 16 207,:S37S.962 4.3243.7 541337,99 56,75

liu .nhl'LE N>IME CMDE TYPE ANALYSIS TIME BLANK? FIODE

CASf. 5427 9404791 Owl 9 24-MAR-94 11)52 N C

ELEM MhVK LEN CON/INT ST.DEV 7.R.S.D. BUNK BKS IEI IE2 193 SLOPS Y-INT

04,513 ,6563931 .417030 1.19313 0 4 269.85 101.377,327 ,0756931 ,409799 57.4602 0 4 1633.38 110.3DA

DEr.r<i.n1:11FK

13,443 ,0047496 ,004157 43,0933 D 0 18190 66,23i.V.716 .0474677 .00=2(»1 150.1)00 0 4 969.329 113.79M.6I6 -,.li.i|779 .046367 -331.99 0 4 71B.444 14,3 i'.'4.794 ,4430939 .000170 71.4376 4 6 1297,08 42.8411 i

._ ..71.74 .0447990 .44JR66 7.03739 I) 4 3306.47169.99?MN 257.61 ,0413543 .000977 77.9243 0 0 93B0.32 78,74??Nl 531,644 -.000493 .000339 -1668.3 0 4 1014. U 207.33 IAO ;.5fl.069 ,0034724 ,0(>4495 129.09? 0 0 379.962 43 |V 39.!.4l» .4123103 ,004738 78,4900 0 4 243,7 20 IIN 5I7.!I56 ,0759433 ,0475'?3 33.0469 0 4 1337.93 36.73 i

«/ 'rtl'IPLE IWME CODE TYPE ANALYSIS TIME BLANK? nODE

CASE 3437 94047?! D 004 9 20-MAR-94 1U97 N B

ELEM.MAVS LEFI CON/INT ST.DEV '/.R.3.D. BLANK BKfl IEI 1E2 IB3 SLOPE Y-INT

AL :>M.213 ,»94?I63 .01737- 2.9742? 4 4 . 363.93 101.3~~ — .0933639 ,045511 5.9032B 0 0 1633,32 110.9

,0000611! .000149 243.433 0 4 18110 66.89-.407233 .009173 -136.91 0 ' 0 869.829 113.79-.004323.414491-324.13 0 0 719.44414.9,0042404 ,1)00309 1.09090 4 0 1217.03 42.841?,0715679 ,042149 3.04438 0 0 2206,47 169,91?.'M23336 ,0114616 34,1249 4 4 9390,32 78.741?,0076976.40394194,9473 0 4 1014,1*207.89-.443039 .1)01662 -94.710 0 4 979,162 43,0095356 ,4113958 42.3333 0 4 243.7 20.0629799.0496149.95065 0 4 1327.1996.75

»5 SAMPLE NAME CODE TYPE ANALYSIS TIME BLANK? FIODE

CASE 545'' 9400795 000 9 20-MAR-94 13)03 N B

ELEM UAVE LEN CQN/INT ST.DEV KR.9.D. BUNK BKQ IEI IE2 1E3 SLOPE Y-INT

,1 265,'.1C 101,3•/ 1635,73 114,:,, 18i?u ati.ilo 043.555 117.75.;, 719,444 14.5

,l,7,',4,l 0 c ti.17.,1,5 43.2499. 19,100 " 0 2206.47 165,999i,;:96Qs o o 5780.53 711.74*9• Ml,91 ... " 1014,16 347,23•54,710 u " 375,'I62 43 '.•199.9? 4 0 547.7 SOi:.S967 >', 4 i:27.95 S6.79

niiR nis AiiiiUY'Ji" line BLAFI»? minen'" 9 30-NAH-84 12)49 N C

EUI1 MAVE LEN CDNClNT ST.OEV V.R.3.D. BUNK BKQ IEI IE! IE3 9LOPE Y-INT

>',L 709.215BA 333,5:7ne :.i7.o43iV 267.7IUCIJ 559.416Oil -,34.754FP 339.'14111! P.57.61HI 2:i.,io4,',Q 739,069V 395,405ttl 913.996

,490090 ,."I647A I.S('406 4 4 369.95 101,9 ;,013099 ,1144116 7.71714 0 0 16.33.33 110,96514150 .044703 .732387 4 0 12190 66.39,136467 ,022141 ,704634 4 4 949,333 113.73.113067.0844095.70973 4 4 719.44494.3 '.176893 .431066 .177082 0 4 1817.02 42.8491.331103 ,,j79941 2.33060 4 4 8846.47 163.911 !.-IIIU4 .059070 .947733 4 4 9380,32 78,7411 !.915727 .014153 2.47740 0 4 1014,16 307,23 :,064769 ,040718 1,43133 0 0 979.962 43 ', 1701116 ,1)46714 1,47311 4 4 343,7 20 I.161431,.UI5I1S .414834 >> 4 1327.9336,79 I

HI" tlAMFLE tir.HE CODE TYPE AKAUY813 Tint BLANK? NODE

CASE 2457 940U79.7 t"X> S 24-MAfl-94 15)13 N C

SLCM WAVE LEN CCM/INT SI.DEV »R,9,D. BLANK BKO IBI 1(2 IB3 SLOPE Y-INT

AL 308.213 ,0536416,01542823.1862 0 "iT ' 263.83 101,9fA 237,327 ',0330333 .444604 8,55239 0 4 1689,32 110,9, S-IT 713,045 -.000123 ,004362 -215,43 4 .0 12110 66,39CR 567.716 ,4417336 ,009861 561,275 4 4 • 963.223 113,79CO 238.,11ft ,0024338.043146344,114 0 0 718.44414.3CD 324.754 .4053997 .041940 34,7118 0 0 1217.02 42,2411PI! 339.14 .3387736 .003317 1.36963 0 4 2306.47 169.???I"M 237,1,1 ,|14'M79 ,('(i|'(?4 4,36111 0 0 ' 3300,32 78,7411111 251,.404 ,4064049.04498777,8133 0 4 1014.16807,23>iO 330,068 -,003106 ,043041 -98.341 4 4 379.162 43V 313.402 -.043477 .006133 -191.91 0 4 243.7 20.-II 217.956 ,1303711 .011047 7,93501 0 0 1327,1396.79

llll SAMPLE NAME CODE TYPE ANAUY9I9 TIME BUNK? FIOOE

CASE 3437 0400794 004 S 80-tlAR-B4 12)17 N C

ELEM WAVK LEII CUN.'IMT ST.DEV XR.S.D. BLANK BKO IEI IE2 IE3 SLOPE Y-INT

.,.-.12451',;i'MM7

tr"T«.T • TV

its.js 101.a. , , ..i.- -17.1..'i (. •:• on!.::! 1i:.7S

•''-.' .'I 'IQ.H l I 0 u 713.4>U 1.1. S..••I'.l.ll 3U.IH* 0 0 I3«7.02 45.5499•,,,-,i'"> i.:uw o o 5:00,47 ; j'i.ni,...1 ••:". ?.,(l»*"* " •' 5700.T5 '.'11.7419.I'V'.-.y; "'1,1S>»4 c ' 1014,to 307,25.,,,:';.'? -H.'liiS " '., 573.11,2 ,13•)",|1,17 504,'JO') 4 o 543,7 300"i-..i!> :,!;ioa <> " 1737.95 86.75 •

,-illir tvre MIALY8I3 TIIC

"On 5 2(.i-Mfifi-84 15151 N C

EI.F.I1 WI.VK I,Ell CON/HIT 3T.ORV V.R.3,Q. BLANK BKO IEI IE2 1E3 SLOPE Y-INT j

"L •.'},].213 14,57439 ,0001114 ,789946 4 4 863.09 141.3 IOil ::77.I27 14.50170 .3151132 5,46989 4 0 1629,33 110,9 •NT 717,44: S.iB4fi56 .427331 1,33798 4 0 13110 66,29IT -,<,7,7lfi I4..-.3I1HH , i:.7l.'7 I.::sa4 4 4 069,235 II3,79|,II ..-••J,6lo ,4-JlllUII) .'jil/l.'.l 54,4114 4 0 718.444 94.9ClI .'.M.7S4 l'i,14i;U ,<>!fflWi2 ,503707 0 4 1397,03 42,2499 .ft. .r/).9,| I". 14066 .'.'(,')913 3.63649 0 -4 3306.47 165,991 (Ill'l .37,lit 10,24159 ,i:47d7 1,31761 0 4 9380,33 70,7411 'III :7I.644 9,1.IWJ .220713 2.42444 0 4 1414.16207,23 <All -,39,06(1 ,,,0j::0l)6 .005075 34.4331 0 4 979.163 43 i</ 593.443 10.13513 .0-,OM6 ,300300 0 4 243,7 20III 513.036 10.33361 .MV47 1.41464 0 0 1387.15 36.79

»'.: V.I1PLE NAME CODE TYPE ANALYSIS TIME BLANK? MODE

I'.'.LID. aim, ?, ,»" S 50-FMR-04 13)35 N C

61.111 WAVE LOI COH/INT -iUK',1 »R,3.D. BLANK BKO IEI 162 1E3 SLOPj Y-INT

AL :,/a,215 -.DI9907 .43BU12 -193.62 '4 0 269,93 101.3BA 577.357 ,0032701 ,441368 79,5676 0 0 '1623,32 110.3

' f'R :i7,,44: -.vOfOj'J ,iji)4l23 -60 0 0 12190 44,23'.-R :47'.7I6 -,o(,a937 .006998 -70,132 0 0 863,339 113,75CO 323.416 9.165993 .181094 1.97371 It 0 ' 719.444 94,9CU 734,754 -.004578 .041333 -330.94 0 0 1317.02 42,241?FE ::?.?4 .0194693 .003493 13.4161 0 0 3206,47 169.9??I'lN 237.61 ,0006<)40 .004993 164.742 0 0 3380.32 79.7419'II 231.004 ,477196? .014333 13.3039 4 0 '1014,16 207.29AQ 739,41.9 0.363556 .123337 1.49234 0 0 973.962 43V 392.405 -.005431 .00:769 -113.47 0 0 343.7 20ZN 513.036 .4433BD6 .404493 134.867 4 0 1337.99 56.79

- ANALYSIS PILE DUHP -

92-MAR-B4 IDlOIl

HI.EN'IME i CLP3 DATE CREATED I 34-MAR-94 12)29At' NI'.HE i CUP Ml. IF SAMPLES I 16

011753

tr

,Vl,M,v;i5 '."i: :i,.,Mll " r-UI)S

:.--M,-.r,-34 ir.iJ'' N c, si.w :i-j '.£1 tiss IE7 SLOPE (-INT

'R I'll,'4 |,.i|,i;.5BHM .:•'•.:.\ ".77777!,.i:1 '"..I",! . :7,,7i'.'.• 'J .:(i.ivi .-,,-171,,':.. -•'•:,,i,.: ,02769/9ill 1,17.531. ,45746tiQ

.10,17351 . .•'16.1:4 a,!M33 0 " 515.03 101,Sul'i'I! 7."0!l!; v " 1635.35 114,5,«:,",',vi 17,11194 0 0 12114 66,35• •I :•.-•! 44,J'.-'I9 0 o 043.25: 117.7!.,"1 '"It 4.M759 0 d 719,44494,5"0"aS? 7.S9S7I 0 0 1397.42 4S.S4997"7i.'07. ,740753 0 t 3306,47 145,99?•.,IH"VI I.7n,.i77 ,, ') 5794,72 70.7499•..•,,l'.i .1 S, "?«' 0 •' 101.1.16 SO1,'.25",-t'>."'; 2*. 094H 0 0 -75,762 4!,>iJ6i:S 35.5222 0 0 243.7 20'Meal 7,12307 0 d . 1337,95 S6.7S

US flAMPLE NAME CODE TYPE ANALYSIS TIME BUNK? HOPE

f.liie. S'I27 0444794 000 8 80-MAR-84 12)33 N C

'SLFH tWVE IEFI r.OFI/INT <3T.IIEV V.R.9.D. BLANK BKO IEI IE2 IE3 SLOPE Y-INT

i',l. :oQ.2IU ,IUdl?S3 ,IX'«I43 i,S9817 4 0 869,89 101.9BA 373.557 1,947177 ,059903 1.65394 0 0 1639.32 110.9BE 313.442 -.000041 .004133 -300 0 i) 12190 64,29 |CD 267,716 -.000299 .009779 -1911.1 0 4 849.239 113.79r.l) .'M,.6I/, .OOMII3 ,iK.r,'l46 89,9768 4 4 718,444 14.9CU ' 334,7S4 ,0<il77*7 ,(ni4774 44,4444 0 0 1317.4! 48.2491KB ;;9.-M 7.8(1,1413 ,172446 3.50332 0 4 2346,47 169,11?MFI 557.01 4.069fii'll .047026 1,13668 4 0 9390.32 79.741?Fll 371.644 .4029390 .006916 233.134 0 0 1014.16 807.29t<> 7311.06'J .4 .042453 -734134 0 0 579.163 43V .192.405 .')ol02!'l .00203! 20".000 0 4 343,7 20III 217.836 ,,;,|J6".77 ,402950 13.3947 0 0 1327.13 96.79

»-; SAMPLE nAHE CODE TYPE ANALYSI9 TlnE BLANK? MODE ,

CASE 3457 9400797 «» 9 24-NAR-84 12)36 N C

ELEM WAVE LEN CQN/IMT ST.DEV W.3.D. BLANK BKO 161 IE2 IE3 BtOPg V-INT

AL 700.315 .0732303 ,043761 4,1111? 0 0 '269,89 101.3EA 333.937 1.465319 ,025001 1,70663 4 0 1639,32 110.9BE 317.042 ,4004410 .000203 300 4 4 18110 66.89CR 267.716 -.046067 .409253 -136.0S 4 0 ' 869,289 113.79CO 259,616 .4013118 ,005302 331.661 0 0 718.444 14.9CU 724,734 .0059733 ,001790 21,7197 0 4 1217,02 42.2411FE 531.94 5.49227.7 .098432 1,79398 4 0 8306,47 163.99?FIN 257.61 .9677854 ,007916 .819013 0 0 9380.32 78.741?HI 531.644 ,,MI?7:4 ,0(1,1907 532.819 0 4 1014,16 307.23AO 350.468 -.01,2170 ,(,42184 -140,66, 0 4 379.968 43V 595.403 , 4 0 4 4 0 843.7 307N rn.ivift .(i4i9Fni .oiV""w i.nniiA o o

011754,'»•'*.' '.

/•>":

..1

.un•'iL

[R

iioni.'E'III .Ill..nV:H

.•i»i..- it..'.•« '..i:'n.v.-t! I.EII

B'SIS71 *.,.;ni;-I*.". 716M-U.1II6

i;4. T54:r-'. 14.". 1 . fli)4::n,n60:95,402213. B36

C

.1H""'")I|

,:i;n.';tir,l'J7.»Ui

.'.„.,''.' 14""•lo'k'577

i"H674ij:

l^l-^fjqp>0' ",|6"1,40''4754, 0051595, 1 133793

::r.c......

"..I'l'.J;.•14ST).,„.,. ,1 1,,.;FIIUj. l-r.,0, ,1)9, ,„,--.-,..I!!"1

,'.,,! .'0,.J03750006ISI!410104

I'fHC

3

V>.. 1,3

j'. T6D2l.'.S'l-06". n14.11."-

., 7.91.1

. . :,'>'.' si ;, C71)iua, oi124,4019.4466V

,-.«,l.

::o-r

01 u

,.>:.44,;,M...004

5IS Tlrif.

ft-at I5|44

NK DIU 1EI

440440

i1,.-,4U0

a.'.M " ROUE

M 5

IE: IE: SLCFE565.031635,3512110065.:::7IS1.44.11317,022246.475780.321014.16375.962243.71327.13

Y-IHT

101.5114.360.33113.7594,542. 2419165.91170.7491:o7.:s435056.79

•5 SAMPLE NAME CODE TYPE ANALYSIS TIME BUNK? MODE

CASE 5427 B400799 044 9 20-MAR-84 I2|49 N C

EI.EH WAVE LEU CON/INT ttr.OEV Vfl.a.D. BLANK BKO IEI IE2 IE3 SLOPE Y-INT

AL 709.3113 .4771111,0473331.73601 0 0 869.93 I01.3OA 333.337 ,4301112 ,04645? 10,3819 0 0 1639,38 110,9BE 313.042 -.01)01182 .000078 -19.742 0 0 12110 66.33Cf 567.716 -.040966 ,009648 -117,77 0 0 869,329 113,79CO '338.616 -.004871 ,006412 -141.94 4 0 ' 718.444 14.9CU 734.734 .0048197 ,000770 13.19?? 0 0 1297.02 42.341?F5 339.94 ,4332373 ,004307 IS.7118 0 4 2206.47 163,99?Ill 537.61 .0295036 ,001494 5.03847 0 0 3380.32 78.749?MI 351.604 ,0 ,009673 ,63476* 4 4 1014,16307,83A(i 359.M -.IXU736 ,004232 -244.94 0 0 973.962 43V I"??, 102 .0014558 ,002051 200.004 4 4 243.7 307M SI7,H56 ,47.4143? ,ill.|900 5,47107 0 (I • 1387,13 36,73

•6 SAMPLE NAMi CODE TYPE ANALYSIS TIME BUNK? MODE '

CASE 2427 8440799 SP 000 8 30-tlM-84 15)41 N C

ELEM HAVE L6N CON/INT ST.DEV XR.9.0. BUNK BKO IEI IE2 IE3 SLOPR Y-INT

AL 308,313 3.143333 .037677 1,81413 0 0 263.83 101.3BA 373,327 3.265008 .061962 1.91424 0 0 1653.32 110.3BE 71.7,1)43 .6391001 .405347 .942992 0 4 13190 66.89CP 567,716 3.297986 ."39004 1.18368 0 0 869.229 113.79CO 2:9,616 3.3I9B03 .442:61 1,31369 4 0 719,444 94,3CU 534,734 3.139493,437430,873419 0 0 1817,0842,2411FE 559,94 3,227433 .032239 1,61919 0 4 2246,47 163.919MFI 257,61 5,573133 ,041040 1,34470 0 0 3380.33 78,749?NI 531,604 3,953336 .063931 2.13342 0 4 1414.16 247,23nO 329.469 2.975S97 ,043717 1.46904 0 0 S73.962 43V 293.443 .7.219131 .434549 1,06314 0 4 243,7 24ill 513,936 7,:s:.|34 ,1148693 I.496U7 I) H IJJ7.9FI *6.7!i

011755

O

il? "Ml* IB "(,M6 (.'HUH Tvlf .WU2I3 TIPE

C-.'.E 315" ll4,,,,ui"J •,(',) 3 Sd-MAh-14 12155

FLfiM tai'/H LBN "111. HIT STiliE'.' '.'.ft.'J.O. CLilllf till IK!

iiL 7''J.513 .ltWo5 ,4i:4:u -I.1769S u •)M r-.-ir"1 i. ii704i)i .oswi 1,73119 o o:r •'•,04: .,'-,,:-!-5,r/ .oo-ior, 77.777: o o• t ''•'.•;' ..,"M7'i: ,, '.,',-.. "I 4, S'.i7:7 ,, •',t'l . I.SIi. .OMol.'JS ,0"'.,|, .1 J.9l'MO 0 "01 72',. 7B4 .OU6SM4 , 401 156 17.6474 4 0FE 5V. 94 143.1691 0 0 4 0FIN :37.6I 6.274791.1397.743.53374 0 4III 571.604 .1143796 .403791 7.33739 0 4AO -.30.068 ,''.'447746 ,005163 62, 1037 4 0V .«?:.- 102 .4451774 , ••.iMfWS 12,9564 4 0,'H Sl"..f)56 ,1019939.4055465.80403 4 4

M SAMPLE NAME CODE TYPE ANALY913 TIME

W36 8457 3400801 1140 9 30-HAR-94 12)39

EL6I1 HAVE LEN COIKIIIT ST.DEV 'iW.S.O. BUNK BK8 IEI

HI. ' Ida, 313 ,1744743,4064244,77713 0 4ftft 277.52? .7S1775/ .045032 1.43074 4 4if. 717.443 ,4007nOO ,0i»l93 25,7340 4 0«. :o7.7lo .4M6IOO .012267 33.4644 4 4CO 333, 4U ,01)31637 .414633 13.7733 4 4Oil 754,754 .-,140111. , 01.0770 3,19490 0 4PF :S?,»4 145.1691 t> 4 0 4Mil .'17.01 7..M67I3 .o:.|7-,3 ,070342 4 dN! 331,604 .1519438 ,0')S99I ",,94339 4 4AO 329,468 ,4134597 ,002943.22.4364 4 4'/ .595.402 .Oi:S769 .,X,1I63 8,55110 4 4:H 513.856 .Ii34u'/S(i .007'13'1 21.11773 0 4

»9 9AMTLE FIAFIE CODE TYPE ANALYSIS TIME

CASE 3437 8441)600 I/ 044 9 50-nAR-84 1)03

ELEM HAVE LEN CON/INT ST.DEV 3R.3.D. BLANK BKQ IEI

AL 708.213 .4197477 ,003601 18.3367 0 4BA 373.337 ,3:99773 ,446493 3.03216 4 4HP. 713.045 .«',', H33 ,444149 104.339 4 4CP 267,710 ,4154545 .'M4765 38,7:44 4 0CO :50.616 ,0114031 .'XiliaS 69,5430 0 0CII 724,754 ,0423037 ,400445 17,7646 0 0PS 339,94 27,8714" ,331210 1,10836 0 4MM 557.61 .7553335 ,043474 .387937 0 4FII 53I.604 .01073" ,41.17438 71.3304 0 4A3 359.069 .M70303 ,1X0849 126.706 4 4'.' 392.449 .0495356 ,.X>7958 42,9323 4 47N 213* Pifln .(MI4nin , .lfi|fl44 l/,.l)ft?? n 4

fLAMf' FIOOS

N C

IE2 IE" SL3PE Y-IMT

565,33 101,31635.32 110. 315194 16.23965,22: 117,73710,444 '"I,';1297,42 43.34998306.47 165.9113300.38 79.74111014.16 307.39979.162 43843.7 SO1337.99 56.79

BLANK? MODE

N C

118 IR3 SLOPE Y-INT

869,99 101.91623,35 110.912110 66.29969.283 113.79718.444 14.91817,08 48.24??3346.47 169.11?5390.32 78.749?1414,16 3.07,89379.962 43243.7 301327.19 36.79

BUNK?, MCDB

U C

IE2 IE3 SLOPE Y-INT

369,83 141,91689,32 110.912194 66.89969.229 113.79718,444 94.91217.02 42.24??2206.47 163.99993B4.32 78.74111014.16 807,99373.168 45243.7 201337.13 94. 79

011756

, I*

HO IE! IE2 IE7 3LOF5

it. . . • •»: • i :•o :!•!

7:11;-,! ;"7,

Mi .'•>1,7j:f"'"•' .",..'-,(1.1

•.i , isM'iu;1I'-l .AI13S7S•-.-'I ,':-n77ii:Ji.i .oi-iuo'i:

»• s.i: i/i. i",73• ••.":•;; 17. 710:•.«>li ' Soil, 1 S3"..[jvs; ir.5.,i53•.«H(|? 74.-16S5,•,.",770 l'l.7:'7i

.tl--4'7 S.,|l9''i7-'":;!7 14.9477-"vl-!: I'll, ,151

o-;,l/ir? 11.7710

4 0,) 0') 04 00 0

0 04 00 -'

4 0

1655. 75 110,512190 66,55963.3:5 113.75719,444 I').:1397.03 42.8499

3300.32 79.749?1014,16 507,53S73,962 47

1327.93 56.75

il l ! SAMPLE I ME CODE TYPE ANALYSIS TIME BLANK? MODE

CASE 2137 04W.5 O'X' S :0-«AR-94 I) 10 N C

ELttl HiWIi LEFI CON/INT ST.DE1.' 'IS.fl.D. BLANK BKO IEI IE2 IE3 SLOPE Y-INT

.,L -uO.313 .4122249 ,,">7wil 21.4593 0 0 365.89 11)1.9 jr,(, :••,:,.527 .17450114.^17/383.14130 o o 1629.32110.9DC 717.045 ,4440615 ,,X"1I33 317.732 4 0 12190 66.53Cft V.7.710 -.0030159 ,04?749 -268.07 4 0 963,239 113.79 iCO 350,61,'j ,0439447 .0434:9 11.2331 0 0 718,444 14,9CU 72'l,734 ,0017747 ,000770 44,4444 4 I) 1297.42 42.2491 'FE ;S«,')4 4.644176 .444778 .884917 4 4 3246.47 1*3.919MM 257,61 ,4213435 .00'531 1,96332 0 4 • 5:80.3! 78.7419 ,HI ..71.404 .4441607 ,4097al 34.3932 4 0 1414.16207.23>,0 1?0."4b -.04i:45 .>:<4318'l -167.77 0 0 573.968 43'.' 3?:,402 .4061351 .047107 113.474 4 4 343.7 20 i ':n :.i7.oric 4.37743- .OIIM? .955777 o ' o 1327,13 34,73 <

»I3 3AMPL6 NAME CODE TYPE ANW.Y8IS TIME BLANK? MODI

iWiili 3427 O4':".'fl45 'D I.XH) S 50-MAR-B4 1'|14 N' C 'I

ELEM HAVE LEN CON/INT 13T.DEV 7 ,8,0. BUNK BKO IB1 IE2 IE3 9UOPB Y-INT I

AL 709.513 ,4366740 .049992 26,973? 04 ' 260.83 101,9BA 577,557 .1631214 ,447193 4,43664 0 0 1623.38 110.3BE 3I7.043 -,0002o6 ,400116 -43.514 4 0 12110 66.83CR 267.716 -.006336 .043362 -40.315) 0 0 963.883 113.79CD 559.6I6 ,4341414 .415457 73.2493 0 4 718.444 14.9CU 724,754 -.000370 ,1100774 -133,33 0 0 1297,02 42.2499FE :.".!.1-t 4.7B44Sn ,447471 1.09191 4 4 3806,47 169.111 jnil 337.01 .3957734 .044547 I.IB792 0 4 9590.3878.741?Ill ;.7l.o44 ,113615911 .0493W 32.iin24 4 4 1414,16807,39All 320.048 •.004340 .OI17"'''? •61,:B2 0 4 373,143 45'/ .".•,4ii.1 -.oiil'l// .'XiMSfi -199.9? 4 4 343.7 24JN 317.036 4.5r7iXi4 ,'17Str.FI I.7H707 (I « liW.I!! fl/,,7rt '

m

1*"* • <5 i

,.. ,. i'.l ''."'. ''i.i'.Mi ' iilie

-; .• TI1--11 it i' N C. VI.in H-.1 IRI IE5 \e.~ 9WI1B (-III'

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. . .'.• -

.,,:;•:, 14 '3

•SAMPLE HAFie

I-.ALIG. CHECK 1

HAVE LCN

703,215237.557313.443567.710

72l'.-!4259. '14557.111

"29,06039-. 4i>-317. US/,

,,;?. ,- , 1 ' .' ' "i-,,,,,! ..•;-!',/4,1"0

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