case narrative - ida ore

Client: Ida Ore Zeolite, LLC Lab Order: 17061608Project: Zeolite Mix Samples Report Date: 6/30/2017

This data package consists of the following:

Case Narrative - 1 Page

Sample Analysis Reports - 5 Pages

Chain of Custody and Sample Log-in Report - 2 Pages

CASE NARRATIVE

Some parameters were sub-contracted to Pace Analytical for analysis.

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Lab ID: 17061608-01

Customer Sample ID: Horizontal Brine-Zeo Mix

Matrix: Soil

Notes:

Customer Name: Ida-Ore Zeolite, LLC

Project ID: Zeolite Mix

Order ID: 17061608

Report Date: 6/30/2017

LABORATORY ANALYTICAL REPORT

Analyses Method Analysis Date/Time AnalystResult Units RL Qual.

Collection 6/13/2017

Received: 6/16/2017 2:05 PM

Date Time

Organic Compounds

Benzene 290 ug/Kg 200 EPA 8021 B 6/22/2017 TMC1:59

4-Bromofluorobenzene (PID)Surr: 99.4 % 70-130 EPA 8021 B

Toluene 530 ug/Kg 200 EPA 8021 B 6/22/2017 TMC1:59


Ethyl Benzene 540 ug/Kg 200 EPA 8021 B 6/22/2017 TMC1:59


m,p-Xylene 18000 ug/Kg 400 EPA 8021 B 6/22/2017 TMC1:59


o Xylene 7400 ug/Kg 200 EPA 8021 B 6/22/2017 TMC1:59


Gasoline Range Organics (GRO) 555900 ug/Kg 22000 EPA 8015 D 6/22/2017 TMC1:59

4-Bromofluorobenzene (FID)Surr: 99.2 % 70-130 EPA 8015 D

Diesel Range Organics (DRO) 2494 mg/kg 500 EPA 8015 D 6/22/2017 TMC0:40

o-TerphenylSurr: 93.8 % 70-130 EPA 8015 D

Total Petroleum Hydrocarbons 3050 mg/kg 5.5 EPA 8015 D 6/28/2017 JS16:14

Definitions:

ND-Not Detected at the reporting limit

RL-Analyte Reporting Limit

H-Holding times for preparation or analysis exceeded

S-Spike Recovery outside accepted recovery limits

M-Matrix Effect

J-Analyte detected below quantitation limits

D-Diluted out of recovery limits

L-Analyzed by a contract laboratory

Documentation will be kept for five (5) years.

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Laboratory Analytical ReportCustomer Name: Ida-Ore Zeolite, LLC


Order ID: 17061608


Analyses Method AnalystResult Units RL

Lab Sample ID: 17061608-01

Collection: 6/13/2017

Received: 6/16/2017


Matrix: Soil

Qual.

2:05 PM

Date Time

Notes:

Arsenic EPA 6010 C MMCND mg/kg 0.05

Barium EPA 6010 C MMC1080 mg/kg 5

Cadmium EPA 6010 C MMCND mg/kg 0.05

Chloride EPA 300.0 TMC681.4 mg/kg 1

Chromium MMCND mg/kg 0.05

Conductivity measured JS2400 uS/cm 1

Lead MMCND mg/kg 0.05

Mercury CL0.042 mg/kg 0.029 L

Selenium MMCND mg/kg 0.05

Silver

EPA 6010 C

WREP-125: S-1.20

EPA 6010 C

EPA 7471

EPA 6010 C

EPA 6010 C MMCND mg/kg 0.05

Analysis Date/Time

6/26/2017 5:04:15 PM

6/26/2017 5:04:15 PM

6/26/2017 5:04:15 PM

6/19/2017 8:32:00 PM

6/26/2017 5:04:15 PM

6/20/2017 1:30:00 PM

6/26/2017 5:04:15 PM

6/25/2017 4:24:00 PM

6/26/2017 5:04:15 PM

6/26/2017 5:04:15 PM

Definitions:





M-Matrix Effect





29 Country Acres Rd., Riverton, WY 82501 • E-mail: [email protected] • www.Precision-Labs.com

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Lab ID: 17061608-02


Matrix: Leachate

Notes:



Order ID: 17061608





Received: 6/16/2017 2:05 PM

Date Time

Organic Compounds

Oil & Grease (HEM) by WY Leachate 12.8 mg/L 1 EPA 1664 A 6/26/2017 TMC12:30

Definitions:





M-Matrix Effect





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Lab ID: 17061608-03

Customer Sample ID: Horizontal Brine

Matrix: Aqueous

Notes:



Order ID: 17061608





Received: 6/16/2017 2:05 PM

Date Time

Organic Compounds

Benzene 664.0 ug/L 100 EPA 8021 B 6/22/2017 TMC2:28

4-BromofluorobenzeneSurr: 91.5 % 70-130 EPA 8021 B

Toluene 1260 ug/L 100 EPA 8021 B 6/22/2017 TMC2:28


Ethyl Benzene 1043 ug/L 100 EPA 8021 B 6/22/2017 TMC2:28


m,p-Xylene 6278 ug/L 200 EPA 8021 B 6/22/2017 TMC2:28


o Xylene 1728 ug/L 100 EPA 8021 B 6/22/2017 TMC2:28


Gasoline Range Organics (GRO) 86130 ug/L 11000 EPA 8015 D 6/22/2017 TMC2:28

4-Bromofluorobenzene (FID)Surr: 99.7 % 70-130 EPA 8015 D

Diesel Range Organics (DRO) 26640 mg/L 4100 EPA 8015 D 6/22/2017 TMC3:38

o-TerphenylSurr: 0.0 % 70-130 EPA 8015 D

Oil & Grease (HEM) 13700 mg/L 1 EPA 1664 A 6/26/2017 TMC12:30

TPH as DRO + GRO 26730 mg/L 0.1 Calculation 6/28/2017 JS16:14

Definitions:





M-Matrix Effect





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Laboratory Analytical ReportCustomer Name: Ida-Ore Zeolite, LLC


Order ID: 17061608


Analyses Method Analysis Date/Time AnalystResult Units RL

Lab Sample ID: 17061608-03

Collection: 6/13/2017

Received: 6/16/2017

Customer Sample ID: Horizontal Brine

Matrix: Aqueous

Qual.

2:05 PM

Date Time

Notes:

Arsenic EPA 200.7 MMCND mg/L 0.05 6/28/2017 12:07:40 PM

Barium EPA 200.7 MMC8.99 mg/L 0.05 6/28/2017 12:07:40 PM

Cadmium EPA 200.7 MMCND mg/L 0.05 6/28/2017 12:07:40 PM

Chloride EPA 300.0 TMC2235 mg/L 100 6/19/2017 7:57:00 PM

Chromium EPA 200.7 MMCND mg/L 0.05 6/28/2017 12:07:40 PM

Conductivity SM 2510 B JS13900 µS/cm 5 6/20/2017 1:30:00 PM

Lead EPA 200.7 MMCND mg/L 0.05

Mercury CLND ug/L 0.20 L

Selenium MMCND mg/L 0.05

Silver MMC0.57 mg/L 0.05

TPH as DRO + GRO

EPA 245.1

EPA 200.7

EPA 200.7

Calculation JS26730 mg/L 0.1

6/28/2017 12:07:40 PM

6/26/2017 7:20:00 PM

6/28/2017 12:07:40 PM

6/28/2017 12:07:40 PM

6/28/2017 4:14:12 PM

Definitions:





M-Matrix Effect





29 Country Acres Rd., Riverton, WY 82501 • E-mail: [email protected] • www.Precision-Labs.com

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Login Report

Order ID: 17061608Customer Name: Ida-Ore Zeolite, LLC


Comment:

Order Date: 6/16/2017

SAMPLE CONDITION RECORD

Number of cooler/packages received: 1

Number of bottles received: 16

Were the samples received intact? (no broken bottles, leaks, etc.) Yes

Were the samples received with custody seals? No

Were custody seals intact? N/A

Did signature match? N/A

Is the COC properly completed, legible, and signed? Yes

Were all samples received accounted for on the COC? Yes

Were all requested analyses understood and appropriate? Yes

Did the bottle labels correspond with the COC information? Yes

Were Samples collected in proper containers? Yes

Were the Temp and Pressure recorded for cylinders? N/A

Were all containers properly preserved, and pH checked - should be <=2? Yes

Do VOA vials have <6mm headspace? No

Was a trip blank present? No

Were all analyses within holding time at time of receipt? Yes

Have rush or project due dates been checked and accepted? Yes

Login verification: Client Name: Yes

Login verification: Project Name: Yes

Login Verification: Matrix: Yes

Sample/Cooler Temperature(s): 21.3

Were cylinder valves leaking? N/A

Were pressurized liquid samples collected at a rate of <50 ml/min? N/A

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case narrative - ida ore

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