case no: : 13383 · the samples collected on december 19, 1989, were designated as case 13383. case...

UNITED STATES ENVIRONMENTAL PROTECTION AGENC'• REGION III

CENTRAL REGIONAL LABORATORY839 BESTGATE ROAD

ANNAPOLIS. MARYLAND 21*01,(301)286-9180 -

DATE: ^ — 3-^ o

SUBJECT: Region HI CLP Data QA Review

FROM: Patricia J. Krantz (3ES23)Chief, Quality AssuranceT Region III

TO: QAO, AOB (OS 230)

Attached is a Region III CLP Data Review by reviewers at CH2M HILL.

SITE: " Raymark

CASE NO: : 13383 " '.-'..

SDGNO: CAW50

LABORATORY: Versar Inc.

REVIEWER: Gayle Lytle

Attachments —_ _ __ :

cc: EPA Site RPM: Mike TowleEdward Kantor, EMSL-LVRegional DPO: Tmn Dciujell,

DATA VALIDATION EVALUATION CHECKLIST

Case/SAS Number: l_339__3_____ Site Name: RjGL\fmOf /<-Assignment #:______;___ Revision Number; $ ] G nalysis Type; ______Reviewer; fay/g. LjJ-tf g.______ Contractor; . CHlM lj ILL_____ Sdtfr f: f/JTAnalytical Laboratory; V(s£gj~_______" " ""_____________________Information Informationrequest date: _________ ___ _______ received date:Date submitted to EPA:EPA DPO; Cfru fc. Cayirf.S _________________ Number of hours spentEPA RPMt Mik*. TptVJC on review: H 5

cc: Joe, CUOjry [r.ti 3M HILL _________ Number of_____________________________ samples : 1 3

CRITERIA YES NO COMMENTS

Format according toRegion III protocol

Clarity of report

Qualifiers appliedcorrectly

Consistency betweennarrative, data summaryform(s), and DPO report

Error-free transcription - <&A+J'

EFFICIENCY OF YE5 : NO COMMENTSCONTRACTOR .._ _. , ... -. -.-.....-,— -.,',..-, ... ——.-=..- - - • -----— ~

Approval recommendedfor current submission

Time spent on reviewis reasonable

ESP OVERSIGHT .... , . ... - • - •MONITOR/ ^ /-

DATES AFC/DPO EVALUATOR Jj ~~ ESAT

Received at EPA (j?~~\ I ____Oversight assigned _ . /^^Oversight rec'd by TM JLJN | 3 iy J //ty/.f£Oversight completeFeedback given _-r • 3 • S pMailed to RPM

EVALUATOR SIGNATURE:___________

revised 01/90

MEMORANDUM

TO: Mike Towle/EPA RPM

COPY: Claudia Walters/EPA (3ES23)QA SectionJoe Cleary/CH2M HILL

FROM: Dean R. Charpentier/CH2M HILL OcuGayle Lytle/CH2M HILL JUJ*

DATE: May 15, 1990

RE: Organic Data Validation for RAS Case 13383, SDG CAW50Site: Raymark

OVERVIEW

This data validation report discusses the quality of the data generated from the Raymark site.The samples collected on December 19, 1989, were designated as Case 13383. Case 13383consists of Organic Sample Delivery Group (SDG) CAW50 which includes iO soil samples,1 field duplicate (soil), 1 trip blank (aqueous), and 1 field blank (aqueous) for a total of 13samples. These samples were analyzed through the Contract Laboratory Program (CLP)Routine Analytical Services (RAS) for semivolatiles, volatile organics, and pesticides/PCBs.The requested analyses were performed using approved EPA methodology.

SUMMARY

All the Target Compound List (TCL) organics were successiully analyzed. Areas of concernare listed below under major and minor problems.

MAJOR PROBLEMS

No major problems were encountered during the analyses.

MINOR PROBLEMS

1. -The volatile analysis included five (5) method blanks. The tentatively identifiedcompound (TIC) carbon dioxide (ACN) was found in four (4) of the blanks.This TIC was not found'in any of the samples so no action was taken.

Method blank VBLK89 was contaminated with 3 ug/L methylene chloride. Thisblank affected all samples. All associated results less than ten (10) times the methodblank concentration were qualified possible blank contamination "B".

Acetone was detected in the field blank at 6 ug/L. All associated results less thanten (10) times the method blank concentration were qualified possible blankcontamination "B". _

2. The semivolatile internal standard for CAW57 had an area of 62700 greater than theupper limit of 58800 for perylene-d!2. Since results for all compounds in thissample were non-detect, all compounds associated with perylene-d!2 were qualifiedestimated "UJ".

3. The holding time for several samples was exceeded for volatile analysis. Allaromatic compounds in these samples were qualified biased low "L" or "UL".

4. Extraction holding times were exceeded for soil using the water holding time criteriafor semi-volatiles. All results exceeding 7 day holding time criteria have beenflagged estimated "J" or MUJ".

5. The instrument used for the water sample analysis for volatiles yielded an initialcalibration for acetone (40.6%) that was outside the relative standard deviationcontrol limit (30%). All water sample results for acetone were qualified asestimated "J" or "UJ".

6. Several compounds had values below the Contract Required Quantitation Limit(CRDL) and therefore, were qualified as estimated "J".

7. Several TICs were found in both soil and water semivolatile method blanks. Anyof these TICs found in a sample were crossed off Form IPs. All other TICs wereflagged estimated "J". ...... ...... ..._._. ... _

NOTES

1. The semivolatile MS/MSD recovery for soil was outside of control limits for 4-nitrophenol. The percent recovery for this compound was 121 % and the limit is 114 %.No qualification was made for this reason alone.

2. The semivolatile initial calibration relative standard deviation for benzoic acid (36.2%)was greater than the control limit of 30 %. Since there were no positive results for thiscompound, no flags were applied.

3. The volatile continuing calibration yielded several percent differences greater than thecontrol limit of 25%. Since there were no positive results in the associated samples,it was the reviewer's professional judgment not to apply flags to this data due tocalibration problems.

4. The matrix spike (MS) sample for soil pesticides had percent recoveries below thecontrol limit (75%) for dieldrin (19%), endrin (1956), 4,4'DDT (0%), lindane (17%),and heptachlor (31 %). No action was taken.

5. The matrix spike duplicate (MSD) for soil pesticides also had recoveries outside thecontrol limits for dieldrin (24%), endrin (26%), and 4,4'DDT (0%). The resultantrelative percent difference between MS and MSD results exceeded QA criteria forlindane (117%) and heptachlor (75%). No action was taken.

6. Reproducibility of the aroclor-1260 peaks exceeded the 20% difference QA/QC limit.Percent difference for aroclor-1260 equaled 25 % and 33 % on successive runs. Aroclorwas not detected in any samples. No action was required.

7. In the semivolatile analysis of CAW54, benzo(b)fluoranthene and benzo(k)fluoranthenedid not meet EPA CLP criteria for confirmation. It Was determined after inspection ofthe mass spectra for these two compounds that there was enough agreement among thepeaks to consider the compound present, and no further action was taken.

8. This validation was performed using the Laboratory Data Validation FunctionalGuidelines for Evaluating Qrganics Analyses (February 1988) and the Region IIIModifications (June 1988).'

ATTACHMENTS

Appendix A Glossary of Data Qualifier Codes

Appendix B Data Summary Forms

Appendix C Results as Reported by Laboratory (Form I)

Appendix D Reviewed and Corrected Tentatively Identified Compounds

Appendix E DPO Report

Appendix F Document Support

Sample Cross-Reference TableEPA Case 13383Versar Inc.Raymark

Date Sampled CLP Sample SampleNumber Type

12-19-89 .. CAW50 Water Field Handling Blank

12-19-89 CAW51 Water Trip Blank

12-19-89 CAW52 Soil

12-19-89 CAW53 Soil

12-19-89 - CAW54 Soil

12-19-89 CAW55 Soil

12-19-89 - - CAW56 Soil

12-19-89 CAW57 Soil

12-19-89 - CAW58 Soil

12-19-89 CAW59 Soil

12-19-89 CAW60 Soil

12-19-89 CAW61 Soil

12-19-89 CAW62 Soil Duplicate of CAW55

Appendix A

Glossary of Data Qualifier Codes

GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)

CODES RELATING TO IDENTIFICATION(confidence concerning presence or absence of compounds):

U = Not detected. The associated number indicates approximate sampleconcentration necessary to be detected.

(NO CODE) = Confirmed identification.

B * Not detected substantially above the level reported in laboratory or fieldblanks.

R = Unreliable result. Analyte may or may not be present in the sample.Supporting data necessary to confirm result.

N - Tentative identification. Consider present. Special methods may be neededto confirm its presence or absence in future sampling efforts.

CODES RELATED TO QUANnTATION .(can be used for both positive results and sample quantitation limits):

J = Analyte present. Reported value may not be accurate or precise.

K * Analyte present. Reported value may be biased high. Actual value isexpected lower.

L * Analyte present. Reported value may be biased low. Actual value isexpected to be higher.

UJ « Not detected, quantitation limit may be inaccurate or imprecise.

UL - Not detected, quantitation limit is probably higher.

OTHER CODES

Q - No analytical result.

AR3Q0053

Appendix B

Data Summary Forms

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FOR CODE DEFINITIONS

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Appendix C ;

Results as Reported by_.Laboratory (Form I)

330

1AVOLATILE QRGrtNICS ANALYSIS DATA SHEET ^ SflMPLE

Lab Name: VERSAR TNC ' - : ^ ' . I CAWSOLont racts GS -D 1-74 7.1 ;

Lab Code: VERSftR Case No. s ^oe MHo.: SDG No.: CAWSO

Matrix: tsoi I/water) "WATER " ' "~I" "Lab Sample ID: 93374A "

Sample Vfc/voi: : """" 5. 0 a,/mL) ML ^ * r-• ,B U' '^L L^^ f-ile IDs U1GQ5

Levei: (low/med) LOWDate Received: 1S/HO/89

% Moistu-res not dec-_ _ Date Anal/zeds 12/S8/a9

Column: (pack/cap)" PACK~ ~ ",Dilution Factor: 1.0

NO. OUND" - - COHCENTRATIOH UNITS,OUND Cug/L or ug/Kg) UG/L Q

chloride

Chloride

Disul f ide

— ,l-Pichloroethane

_1,1, 1-Trichloroethan

:-CaT,boiT___Ietrachloride

3~Dichlo-ropropeneTTit?hlcrroethene

Bromoform

-2-Hexanone

I f ci—1 ,ii —Q~—"•i •? =: ~_ T? "=; „ A ._,_——.__——j / >j i-ji-i * T — ^ ^i "7"=:—"3'=: J_"a_-——__I l *J OiJ —j—•—•——•_ (

1 540-59-0-————-1, £H5ichlproethene 7total7__I_J! 67-& £-3———"™———Chloroform,_,_^._i___.I 107-0'6-H----——^~:l,H:-Dichlor,pethane1 73-93-3— " ""_' "'"I "71 _-K-er_£___",""_I^jJ / J. iJfcJ — D ———I 1 - ! iC -^ C} Tf ,^ f"T .^»ot> cu—c> —I 10a-05~4——t -r-rr " o "i1 "'/.~ ~ll~—— ") / i..' i_ / ~^~ — — ——

J 7G-87-5--100&10-1-5——~*O_A 1 _fi _-»_,/ 3 —*U J, ~ti —

124-48-79-00-5"——71-43-2—-1 OOol ~OS"ci~-—"

i / .3—55— S"""10S-10-1o91~i7fl—6—~—•127-1S-4————-79-34-5——1 Ail — &.Q —"^ — _,ii__.™._—_. .TJ-Vo CJCJ O — —— I __

J.Ofl-9.0-7————~-CTilo.robei _100-41-4—————-—Ethyl benze1100-42-5---"" "" . ,..-_ « ^1330-20-7-—---^tQtaY'Xxlenes.

1/S7 Rev.

-103.02

1A _ _ .t 3 .. , EPA SAMPLE HO.VOLATILE ORGftNICS ANALYSIS DATA SHEET

I CAWS1Lab Names VERSflR INC Contracts cia-01-7471 !______

L.ab Codes VERSAR Case No. : 13333 SftS No. : " SDG Ho. : CAW50

Matrix: (soil/water) WATER Lab Sample ID: 93375A

Sample wt/vol: 5.0 <g/mL> ML Lab File IDs 01686

Level: (low/med) LOW Date Received: 12/20/89

% Moisture: not dec. Date Analyzed: 12/2S/S9

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND Cug/LioT ug/Kg) UG/L Q

74—37-3——————=——Chl or ome thane,74-83-9————————Bromomethane__75-01-4---————-Vinyl Chloride,75-00-3-—--"—"————Chloroethane_______75-09-2—————-^Hlethylene Chloride67-&4-1————————Acetone____________75-15-0————————Carbon Disulfide

_.„. .,- 10 . I.U10 IU10 IU10 IU5 iy

10 i.u5 IU

75-35-4 ———————— 1,1-Dichloroethene_____;____ _ , 5 I"U"75-35-3————————l,l~Dichloroethane_I__~____I1 S IU

I 540-59-0———————1,2-Dichloroethene (tot^lT__I . : 5 I.U1 67-66-3--—^—^-Chloroform__________________1 .". . . ., _5 IUI 107-06-2————————1,2-Dichloroethane___________! „. . 5 IU

I 71-55-6———r-——-1, 1, l-Tric'ill oetliAnelllllll Ii .—-,... ... .5 J,U_I 56-23-5———~- ~-Carbon Tetrachloride___^_Z_i. . ~~ .1 3 1UI 10S—05-4———-———Vinyl Acetate____-_____,|_]_s_ I....__._,_ _ 1Q I U.I 75-27-4——————*-Bromodachloromethane___j____ I 5 I UI 7S-a7-S—.—-—-—!, S-Dichloropropanej___'^__1 ........ S ' U'1 100610-1-5————— cis-i, 3-Dichloroprop"@ne_L~___.! _. - S JLCI 79-01-6——————-—^Trichloroethene____;___\___^! __, _ 5.JUI 124-48-1————————Dibromochloromethisne____;_____ I _.._ ,r ... 5 I.UI 79-OO-5——————«—1, 1, 2-Trichloroethane__^__J^__ I . .. . .5 1 UI 71-43-2————•———Benzene___.___;__.____„_„!__I ,= 5 IU_I 10061-02-6—————brans-1, 3-Dichlordpropene_.;__ I "... 5 IUI 75-2S-S————————Bromoform______________.____ I ,. ... _. S I UJ 100-10-1—————=~~4-Methyl-H-PentAnoneI_______I ^ / , 10 IUI 531-7S-6———————2-Hexanone_____:_________„_.!_ I .i . . . . . . 10 IUI 127-1S-4———————Tetrachloroethene_^_-____"__ I ,..„.. ,„ .5 1'UI 79-34-5———————;-l, 1,2,2-Tetrachloroethane___I .. _. . S IUI 108-SS-3——————Toluene_______________J____I .__.,_... 5 IUI 10Q-9O-7——————-Chlorobenzene_.____.._.. _..' .... I 5 ..1 Ui 100-41-4———————Ethyl benzeneI 1OO-42-5————————Styrene.I 1330-20-7——————Total Xylenes.

FORM I VOft 1/B7 Rev,i r\ . .-* — »,-jLOulj*!,-

VOLATILE O R G A W r c - S ' SHEET ™ SAMPLE NO.

N.*., VERSftR INC Contract: 63-01-7471

L.ab Code: VERSAR Case NcuV 13383 SAS No.:

Lab Sample ID: 93337A

SDG No.: CAW50Matrix: <soil/w*t*r> SOIL '

Sample wt/vo'l: '" "" 5.0": (g/mL) G ' " . " Lab File IDs R37S1

Level.: (low/med) LOW"" , Date Received: 12/20/89

% Moistures not dec. 17 Date Analyzed: 1S/S1/S9

Column: <pack/caP) PACK Dilution Factor: 1.0

.....:. . .. ... CONCENTRATION UNITS:Cns N0- COMPOUND (ug/L or. ug/Kg) UG/KG Q

74-87-3——"- -- h loroinethane__________ _ \ 12 IU74-S3-9"--~^————Bromomethane________________ j _ 12 I U75-01-4-——— T VA*! Chloride.___*_________ j 12 I U75-00-3————————Chloroeth&ne '•75-09-2 ———————Methy 1 ene Ch_lorid.e.67-64—i------——Acetone.

12 JU7 !

_____________________, 12 IU! 75-15-0—-—~——darboV'DisLiff id&___;_Z___— ' 6 I UI 75-35-4—~ --~—1, 1 -Dich 1 oroeth^ne JT^__;__ZZ_ I 6 I UI 75-35-3————————-1, l-Dichloroe:thane__________ I 6 I UJ 54O-53-0———---"i,S-D.ichloroeth,ene.l,i-fcDt^l^ __ I 6 I Uf 67-66-3—- - R nlorof orm____'___________3—' -& ' uI 107-06-2—-—-'- —i, 2-l).ichloroethane_______!_ I S 1 UI 78-93-3——i-——- -p-ftM*!1 - - - :..._ ____________________, . 12 IUI 71-55-6—————-_^1", 1, l-TrichipTop^hane______^_ I, 6 I UI 56-23-5——•-——————Carbon Tetrachlpride___^___;— I 6 I UI 108-03-4—————-V_inyl" Acetate___u._,__~______^' 12 I Ui 7 5 —E'7—4 •—- —-^—- —— B r o.m o d i c h 1 or onie t h a n e.___. _ ____ J 6 I U7S-S7-5—-^—=^=^i=*i . p-n'i r-h i r*.^«n.K«-« — ~ - . . . . u___ __^ _ _,___1QO610-1-5— —— -~cis^l,3-DichlorppropeneI__ _ _l 6 IU79-01 -6----^----Trichloroethene_____._.__^_-_._ ___ J IS I

— ^ ™-—™.,.. J 6 ! U. ^ _ _ l l 6 I U

71-43~2--~::-~ -:-lSe"nzerte __ __" _ '_ __ __ ___ " ___ " I 6 I U10061-02-6— —^-—brans-1, 3-Dich lor opropene ___ ! 6 I U

- - - -75-£5-e—-^-^"^-Bromof orm___________________ ] 6 I UlOfl-10-1———*———4~Methyl-H-Pentancjne~_______I 12 1 U591-78-6———^-^-2-Hexanone_______-_____Z-IZ' 12 ' u127-18-4————-———————T*?-hTflf*h1 r»wn»+-K««-_ _ _ i79-34-5 — ——— -U -i , i 9 a"^ '"I-tetir ach loroeth ane1 08-88-3— — - _108-90-^7—— -—"-Chlorobenzene100-41-4 ——————— Ethyl benzene100-42-5 —— — -:; byreneL™,_J __ ,1330-20-7— -^^ — Total"Xylenes

FORM I VGA 1/S7 Rev.r,ui r, r*-L

1ft • EPA SAMPLE MO.VOLATILE ORGANICS ANALYSIS DATA SHEET . „ ___ ; ___________ -

II CAU53 _ _

Lab Name: VERSAR INC Contracts iSS-Or-7471 I _____

t_ab Code: VERSAR Case No.: 13383 SAS No. s SDG No.: CflUSO

Matrix s <soil/water) SOIL Lab Sample ID: 9338SA

Sample wt/vol s 5.0 Cg/mL) G Lab File ID: R3732

Level: Clow/med) LOW Date Received : 12/20/89

% Moisture: not dec. 31 Date Analyzed: 12/21/89


CONCENTRATION UNITS:CAS NO. COMPOUND <Lig/L 'or ug/K"g"> DO/KG Q

I I .._ - - II 74-37-3 —————— ——Chlorouiethane I .„. __ ,.. 14 '-U -74-33-9 ————————— Bromomethane ______ _ ________ 1 ^_ . ... 14 . LU I75-01-4 ———————— Vinyl Chloride _______ Z _____ !.._,. : , 14 IU I7S-OO-3-- —— — ~ — Chloroethane _ _ _________ j ____ I . . . . . 14 LU .175-09-2 ———— : ———— Methylene Chloride_~ ___ : ____ I _ „,., 22 I I67-64-1 ———————— Acetone ___________ I _______ Z1 - — . . . *4 IU '75-15-0 ———————— Carbon Bisulfide ___________ II ..__ ". .'. '_._ 7 IU I75-35—4 ———————— 1, "1-Dichioroethene ____ Z ____ ' ~ • ? 1U l75-35-3 —————— -1,1-Dichloroethane _____ ; ____ ! ,, 7 IU 154O-59-0 —————— -— 1, 2-Dichloroethene <totalT __ I _ 7 I U I&7_66-3 —————— __ chloroform^ ____________ | ____ I _.._.., „ ...7 ,.LU107-06-2 ——————— i,a-Dichloroethane_ ___ JZ_» _ i ..'. i. ' , - 3 ' u73-93-3 ——— '-. — ~ ~2

124-48—1 ——————— -D i bromoch 1 or ome thane ____ f __ ,79-00-5 —————— : — -1, 1,2-Trichloroethane ____ , _ _

71-55-6————————1,1,1-Trichloroethcine_____;_! __. .7. i.U56—E3-5———•———Carbon Tetrachlor ide___[____.1 _ ,. . 7 I U10S-05-4——————Vinyl Acetate?^____^___,___~ I __ . ... 14 IU73-27—4————~-^~--B-ronioaich ioroinethavie___|____ I _ __.. _ 7 I U78-87-5——————*•-"!, S-Dichloropropanei;___|____ I _!.:. , 7 I.U100610-1-5——-——cis-i,3-D-icbloropropene_:_Z_Z' ~~- - -7- l-u_79-01-6————————Trichloroethene_______: __„„"" I 7 IU

7. ILL7 IU7 IU7 LU7 IU

14_ I U14 IU7 (U7 IU7 IU

UU

Benzene10O61-08-6—————trans-1, 3-Dichloropropene__m75-25-2—-——————Bromoform___________________1 OS-10-1———••———-4~Methyl-H-Pentanone.591-78-6—————-—2-Hexanone_____________^1S7-1S-4———————Tetrachloroethene________79-34-5————- i, i, a, 2-f etrach 1 oroeth ane,10S-8S-3—————^--Toluene ___108-90-7——————-Chlorobenzene______________100-41-4———————Ethyl benzene______________w100-42-5———————-Sbyrene___;_____I__!Z-™Z^.____] - - -- 7. I U1330-20-7——————Total Xylenes____.___^ :

FORM I VOA 1/87 Rev.

1A . . . . , -- ..... - - EPA SAMPLE NO.VOLATILE ORGflNICS ANALYSIS DATA SHEET _____________

II CAW54Lab Name: VERSAR INC Contract: 68-01-7471 I

Code: VERSAR Case No. : 13383 SAS No. : SDG Mo. : CAU50

Matrix: (soil/water) SOIL . . . : . . . Lab sample ID: 93389C

Sample wt/vols 5.0 Cg/mL) G ' " Lab File ID: R3S13

Level: (low/medJ LOW Date Received: 12/20/S9

% Moisture: not dec. : Date Analyzed: 12/2S/fl3

Columns <pack/cap> PACK Dilution Factor: 1. 0

CONCENTRATION UNITS:NO. " COMPOUND (ug/L or ug/Kg> UG/KG 0

7 4 - a? - 3—-"• : ' ' -Cn74-83-9————r i. Bromomethane75-01-4-—-1——--Vinyl Chloride.^75-OO-3—--———~Ch 1 oroeth ane75-09-2-—————--—:Methylene Chloride.

I 67-64-1-——————"—-Acetone________f 75-15-0——————•—-Carbon DisulfideI 75-35-4——--——=~—i", 1 -Dichl oroeth ene.! 75-35-3————- -T, 1 -Dichl oroeth ane,_______I 540-59-0————~i,jr-jichloroeth_ene_ (total)I 67-66-3 ir - ^ ^ Cfflorb form________________f 1Q7-0&-2™±———^1,2-EfichlDroethane______I 73-93-3-——————^-2-Bu-fcanone " " : - : '1 "?1 _-nrtr _.r ,, -, ,__^ IIL _j -i " -I ' i! _j ( j_ — ,j,_j.~c.j — ~" r~ ~f—*± _ j. _ i —

56-S3-5.—~~^——-Carbon te-6"fachJ,oride'l^_10S-O5-4——•-—'-— Vinyl Acetate

i , j--cl/™-*t-»--*"-=-=—~——i<roi'rto'dich lproiii(i?than.e_^_^_,I 78 - S 7 •-• 5 -----1- —- - 1, 2 - D i c h 1 o •/- o p T d p a n e? _v_^-___^_,I 1 f\S\'£ "I ^ '•• "=•" " - - - - . . ^_- - : - - - -

I 79-01-6——-————-—Trichloroethene __J 124-48-1———————DibTomochlor-GiaethiI 73-00-5 —71-43"~2~-—-—•———-10061-OH-6-——:™trâr^s-l, 3~Dichlprqpropene_i__75-S5-S—-——^—=^Bromof orm____J___^____^___"_]___lOa-10-1———————4-Methyl~2-Pentanone_~_______591-78-6———=————2-Hexanone__._____'_______'_127-18-4——————~Tetra'chloroethene_i__________79-34-5-———————î,I,jB7r&-T®i?âcnl0ôe:thane____108-S8-3— ~ -~ —— Toluene_____________iOfl'~90-7'---*«iB==iiis --Ch IorjD_benz100--4"r-4—"--" —-E thyl benzene100-42-5— .- - ~1330-HO-7—^—-—-fotal" Xylenes

FORM I VOA ^-L

1A : • . EPA SAMPLE HO.VOLATILE ORGANICS ANALYSIS DATA SHE'ET - -^ ___ ____ __ -^

I1 CAW55 . _. ..

Lab Names VERSflR INC Contracts 6Q«01~"M7l ] ___

Lab Code: VERSAR Case Ho. s 133Q3 SAS No", s! - SDG Mo. : CAW50

Matrix: (soil/water) SOIL Lab Sample ID: 33390A

Sample wt/vol: 5.0 Cg/mL) G Lab File ID: R3784

Levels (low/med) LOW Date Received: 12/20/89

% Moistures not dec. 23 Date Analyzed: 1E/21/89

Column: <pack/cap) PACK Di lution Factor: 1.0

CONCENTRATION UNITS*CAS HO. COMPOUND <ug/L br ug/Kg) UG/.KG ... D

Ii 74-S7-3 —————— =— Chl orome thane ____ .I 74-53-9- ———— "^^Broroome thane. _____ fI 75-01-4 ———————— Vinyl Chloride ___ .I 75-00-3 — ; ——— — — Ch loroeth ane _____ tI 75-09-2 — " — -—— — Methylene Chloride'f 67-64-1 ———————— Acetone __________ ,I 75-15-0 ———————— Carbon Bisulfide _______ ___I 75-35-4 ———————— 1, l-BiehloroetheneZZ--ZZZZ__I 75-35-3 ———————— i, l-Dichloroethane_~ ___ —I 540-59-0 ——— -—— ~l,2-Dichloroethene Ttotal")I 67-66-3 ——————— — Ch lorof orm ________ 1_ a._ _J _I 107-06-2— — -^— —— 1, 2~DichIoroetharle *I 78-93-3 ——— --^ — -S-BI 71-55-6 —————— -—I, 1. l-Trichlorpeth"ane.I 56-23—5 ————————— Carbon TetrachT.oride_I 1OS-05-4 ——————— Vinyl flcetate_ ______ [i 75—e37-4— —— • ———— Bromodich lor ome thane ____ J _I 7S-87--5 —————— -«i, H-D i chl or o propane^ ___ J _1 10061O-1-5- ————— -cis-1, 3-Dichloropropene^ _ __I 79-01-6 ———————— Tri chl oroeth ene_. _______ _ _1 1 £4-48-1- —————— — DibromochloTome thane ____ . _I 79-00-5 ———— i_- i9 1,2-Tri chl oroeth ane __ ___I 71-43-2 ———— • —— -Benzene^. __ ^ ________ _ __ L"I 10061-02-6 — -—— --trans-1, 3-D ichloropr opensI 75-25-2 ———————— Bromoform _______________I 108-10-1 ———————— 4-ttethyl-2-Pentanone __ '__1 531-78-6 ————— —2-Hexanone _______ ; ______ _I 1E7-1S-4 ——————— Tetrachloroethene __ ._. ____I 79-34-5 ———————— 1, 1, 2,2-TetrachloroethaneI 108-88-3— ————— -Toluene _ - _ \ __ _ _____ ; ____ [_I 108-90-7 — —— — — Chlorobenzene _______ : ___ _! 100-41-4 ——— , — '— --=-Ethyl benzene ________ ___^.I 1OO-42-5 —————— -^Styrene ____ .___! _____ Z __ ZI 1330-SO-7 —————— Total Xylenes _____ Z ____ [

FORM I VOA ! ' 1/87 Rev.

1 U V.' L U J

1A ' iIPft 3AMPLE MO.VOLATILE ORGANICS ANALYSIS DATA SHEET

_ — i•* - -* iI CftW56

Lab Name: VERSflR INC " ' - - • Contract: £3-01-7471 i

uab Codes VERSAR Case No.: 13383 SAS No. s SDG No.: CAW50

Matrix: (soil/water) SOIL " Lab Sample ID: 93391A

Sample wt/vol: 5.0 Cg/mL) G ! - Lab File ID: R3790

Level: (low/med) LOW Date Received: 12/20/89


Column: Tpack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CflS NO. COMPOUND <ug/L or ug/Kg) UG/KG Q

1 .______. . . . . . . I II 74-S7~3--~™----~-CI-iloromethane_^i_____________ I 13 I U

I 75-01-4—--————^Vinyl""ChloTidelZZZZZZZZZZZZZZi 13 I U\ 75-00-3-----~~™~-C"hlDroethane____™__~_____ I 13 " I UI 75-09-2—-—————Hletbylene ChlorideZ___:_____I . 16 IBI 67-64-1———————Acetone____._______________ I 7 ! JI 75-15-0——————-—Carbon bisulfide____~______1 7 IUI 75-35-4————————-'l, 1-Dichloroethene______~_ I 7 I UI 75-35-3————-———1, 1-Dichlorpethane_________~l _ 7 IU1 540-59-0 ——————— l,E-Dichloroethene Xtotal) __ I 7 !UI £7~66-3---~-r---^-:-Chiofoform____J______'_________ i 7 I U

I 78-93-3——^—-^-2^Buj:anpne_'__*~_____________ I 13 I UI 71-55-6------~-~i7T, f'-frichlorpethane_^___ I 7 I UI 56-23-5—-———-—Carbon Tetrachlora.de_____^__ i 7 I US 108-05-4———————VinyT "Acetate________.__.,__"^J 13 I U

! 7S-fl7-5—-"— -r- —T, 2--DichlprppT:PpanE>____-____ I 7 i UI 100610-1-5—————cis~l, 3-Dichiorppropene_____,1 7 I UI 79-01-6—~————-Trich'l oroeth ene_____________J 7 IUI I24~4fi-i—•-—————Dibromochlorometbane________ I /" I UI 79-00-5———'—?-" "•. '-1, 1, H-Trichloroethavie^^^^^^^^^l 7 I UI 71-43—2——••———--^JSenzene_______\_______^^___ I 7 I Ut 10061-02-6—————-trans-1, 3-DichlpTopropene____I 7 !UI 7i3~* 25~ 2—'—————:—" "Br onto f or ni __ , J 7 I UI 108-10-1-——=————/*"iv(e'*'t"'>'1-2-Pentanone3ZZZZZZZZl 13 1U! 591-78-6————-.—-2-Hexanone._________12______ I 13 IUI 127-18-4———————Tetrachlo-rpethene__.?=_____2_Z-' -, 7 f'ui 79-34—5———•—•-—™i, 1, S, S-Te^trachlorpethanc___l_ . 7 JUI 108-88-3—-~-——--ToTuene__"___I______________I . 7 IUI 108-90-7———————Chlorobenzene_______________! 7 IUI 1 i^ri_Ji 1 ~A____ — — __™Cf'"'[""K v/1 f". /i •/•. -r r~.n ci " I "7 I I Ii .L \j\j -*i .i. ~*t——————— t. tfi t y j. LJt?iiz e j '£?_.__ _ l / i ui 100-42-5—>——»~-Styrene____._Z»_Z™_________;__ I 7 I UI 1330-20-7-——————Total Xylenes_ __ ~ ]


10 u o •' c

Ifl " ' - " . . . EPA" SAMPLE MO.VOLATILE DRGANICS ANALYSIS DATA SHEET "" " ._____;_________.

II CAW57L&b Name: VERSAR INC Contract: G3-O1-7-471 J _________

i_ab Code: VERSAR Case No.: 13383 SAS Ho.: SDG No.: CAW50


Sample wt/vol: "~ 5.0 <g/wL> G 'Lab File IDs R3791

Level: Clow/med) LOW Date Received: 12/20/39


Columns Cpack/cap) PACK Dilution Factor: 1.6

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L or us/Kg) UG/KG Q

74-87-3————-——-ChJ-oromethane^74-83-9—-—~-———Bromomethane_75-01-4————————Vinyl Chloride75-00-3————————Chloroethane_____75-09-2———•———Methylene Chloride67-£4—1————————Acetone________75_15_0————————Carbon Bisulfide_75-35-4————————-1, 1-Dichloroethene75-35-3————————i, 1-Di chloroethane_______540-59-0———————1,2-Dichloroethene (total)67-66-3———-———-Chloroform_______1O7-O6-2-——-———i,2-Dichloroethane73-93-3———-———2-Butanone__________71-55-S ———————— 1, 1, l-Trichlordethane56—S3—5———•=—-"-—^Carbon Tetrachloride103-05-4———————Vinyl Acetate

7S-S7—5—————-—-i, 2-Dichloro pro pane___100610-1-5——:———cis-i , 3-Dichlorppropene73-01-6-^————^-^TrichloToethenfe____124—43-1--—————;—Di broniochloromethane__79-OO-5———————1, 1, a-Trichloroethane71-43-2————————Benzene_____„______________10061-02-6———'- — trans-i, 3-Dichioropropene_^_75-35-S———————-Bromoform_________103-10-1———"———4-l-1ethyl-£-Pentanone591-73-6——————^--2-Hexanone_______________1H7-1S-4———————Tetrachloroethene_______79-34-5————————1, 1,2,2-Tetrachloroethane103-88-3—————^-^"Toluene____________.____103-90-7———————Chlorobenzene^100-41-4———————Eth /I benzene_100-42-5———————Styrene_________1330-20-7——•—^^Total Xylenes___


Ifl , , .. , .- £PA SAMPLE NO.VOLATILE DRSflN'iCS"flNflLYSIS Dflfft SHEET _____________

" " " " fJ CAU58

Lab Names VERSAR INC Contract: 63-01-7471 :,______________

j_ab Code?: VERSAR Case No. s 13383 SAS Ho. : SDG No. : CAU50

Matrix: (soil/water) SOIL . . . . . _ . . Lafa sample ID: 93393A

Sample" wt/vols 5.0 <g/mL). G . . . . - —Lab File ID: R3794

Level: (low/med) LOW ... Date Received: 12/SO/39

% Moisture: not dec. 27 ; Date Analyzed: 12/22/89


CONCENTRATION UNITS:.CflS HO. COMPOUND <ug/L or ug/Kg) UG/KG Q

1[ "7/i — A "7 ~ -'3 _ ~.t f *\~~ o / ,i — —1 74-B"3~-9 —1 75-O1-4 —1 75-O.O-3 —1 75-09-2—I 67-64-1 —

I / £— ii_f— 4~—I 75-35-3 —! 540-59-0-1 £7-66-3—i 107-06-S-1 7Q--93-3--i ~7-t _«;•=:.-. c ——l / j, J vj t> —I •-J O 1Z. O •-!

1 103-05-4-i .' o "~d / "~st """~"j 7s-a7-5 —1 100610-1-[ ~7 Q — A -1 __ f __I / y U -L D

1 124~4G-i-

1 71-43-3—1 10061-02-t "7 "=• _ o <=: _ o _._1 / «J C«J C

: los-io-i-1 591-73-6-I 127-13-4-1 79-34-5—( 106-63-3-1 103-90 7-1 100-41-4-I 100-42-5-1 1330-20-71

—— _ —— Chloroniethancs 1— ——— ^ — Bromomethane"' . " * • • I—————— 'Vinyl Chloride.. _ ... _. • .- ... __ 1—————— Chloroethane ' .: . 1—— ^-—— -llethylene Chloride. _ _-. -— _:._l—————— Acetone I———— ' —— Carbon JHsulfide ... . .. ....- ... I—————— 1, 1— Di_chlproethene r__ ' . .. .... 1— _.: ——— i^ 1-Dichlproethane 1—————— -l,£-Dich_lproethene <total) __ I- — : ———— Chloroform !

1 "••' 1 5 d. -iJicn j.u f-pt- cffctni^- I-— •Lii-— —— S— Btitanone ; I— . —— r-»-*i, l, l-Jr,3;ch.lproeth.-t.Tie _. _ __._. ~J^-~ — — Carbon Te trach loride _ i—— —— — -yj-nyl Acetate , . ... . 1- - -i isssssjs pQ-jj ff QJ.J loTometh avie . I——— -—— -1, 2-Dichlpropropane !5-*- — : — cis-1, 3-Dichloropropene___>;__; _ f,„ — ,_ — Tricblorpeth.ene 1„— «« — •^JBi_b'ro_moch 1 prome'th ane. ________ 1— • ^^Afl "T'ric.h.le.Toethane _______ .1—— , ——— Benzene ! J6 ————— 'fcrans;-l,_3-DichlprqprDpene ___ J—— . — : — -Bromoform ._ . ... _. . . ----- 1———— ~~4--Methy 1 -S-Pent^none, __ __.__ _ I———— , — g-Hexanone 1—————— Tetrachlorpethene _. _. .,. 1— -rr— — —-="1", "1 , 2, 2— Tetrachloroethane ___ 1- : ————— Toluene . _ - - - - - - 1~—- - —— "-Chlorobenzene ••-'-• - " j————— — E' bhy 1 ben z ene* ___ ^__ __ . ______ __. _ _ !—————— Styrene . _ 1 1— -,^ —— -—Total Xy levies I

:! . : . ] . • - . . - - . - - • • • " . I

141414143314777777147714

•?777777771414

-7

77/7

I UIUIUIUIBIUIUIUIUIUIUIUIUJ UIUIUIUIUIUIUIU.IUIUIUmIUIUIUIUIUIUIU

I11I11!1111111J11111!J1I1II11111

fiR;309092!


1A ' EPA SAMPLE HO.VOLATILE ORGANICS ANALYSIS 0ATA SHEEt ______________

!I CAW59

Lab Name: VERSAR INC Contract: £8-01-7471 !._________.

Lab Code: VERSAR Case No.: 13333 SAS No- s ~ "S'BCJ Wo.: CAU50


Sample wt/vol: 5.0 <g/mL) G Lab File IDs R3305

Level: (low/roed) LOW Date Received: 1E/S7/69

% Moistures not dec.- - -39 Date Analyzed: 12/27/89

Column: Cpack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS HO. COMPOUND Cug/L or ug/Kg) .UG/KG Q

i74-37-3————————-Chl or ome thane74-83-9———————^Bromomethane75-01-4————————Vinyl Chloride___________75-00-3——:————— Chloroethane_____________75-0g_2———————^-Methylene Chloride______j.67—64—1————————Acetone____________:____75-15-0————————Carbon Bisulfide_J_______75—35-4—•:——————1, 1-Dichloroethene___;____75—35—3————————i, l-Dichloroethane_______540-59-0————————1,2-Dichloroethene < total)67—66—3-—————~—Ch lor of orm,_______.107-06-2—=————^T, H-Dichlproethane-78-93-3——-——~~—e-Butanone.._______71—55-6—————-———I, 1, i-Trichloroethane.36—23-5———————^Carbon Tetrachloride.103-05-4———————Vinyl Acetate,

7*3—07—5—-———-~—— 1, ST-Dich loropropane______'_._100S10-1-5—————cis-1, 3-DIchloropro'pene._J_79-01-6—————————-Trichlprp'ethene_____!_"l«-_j_1H4-48-1————————Dibromochloromethane_____;_79-00-5—————~—-1, 1, 2-Trichloroethane____j__71-43-E————————Benzene_________________^_10061-02-6—————trans-1,3-Dichloropropene^_75-25-2————————Bromoform________________1__108-10-1———————l-Methyl-2-Pentanone______591-73-6———————2-Hexanone______1H7-1S-4———————Tetrachl oroeth ene_______79-34-5———————=rl? 1,2, S-Tet-rachloToethane108-S8-3——————-Toluene__•____________10B-9O-7————————Chl pro benzene____________1OO-41-4———————'Ethyl benzene________._._100-42-5——————rr=Sbyrene,________________1330-20-7———————Total Xylenes_________ _

FORM I VQft 1/87 Rev.1 f\ M " "

in . EPfl SAMPLE HO,VOLATILE ORSANICS ANALYSIS DATA SHEET __________,

. . _ _ _ - - ! f

I CAW60Lab Names VERSAR INC Contract's.-. &S-01--7471 ! __________.

i_ab Code: VERSAR Case No.: 13383 ~SflS No.: SBG No.: CAU5O

Matrixs (soil/water) SOIL . Lab Sample ID: 93395ft

Sample wt/vol: """ " "" 5.0 "' Cg/mL) G ' Lab File IDs R3S1S

Level: <low/med> LOW Date Received: 12/SO/89

% Moistures not dec. 32 :. - Bate Analyzed: 12/H8/S9

Column: '<pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. "COMPOUND '• (ug/L or ug/Kg) UG/KG Q

I 74-37-3—-—-•^——-'CTilp-ronie thane.i 74-83-9—-----———Bromomethane__I 75-01-4 —————~^V i n yl C hl'o r±d <I * >j—OO—3"~'——*——••?••——\_,n l proetn ane_ _ II 75-09-S——T——-—Methylene Chiprid'e^_________Z_ JI 67-64-1—=-—==-*——Acetone _"... "_...._,....:_______________ II 75-is-o———————-Carbon Disulfide________.___ II 75—35-4———•————1, l~D,i-chloroethene__________ II 75-35-3-——-———-1, 1-Dichl oroeth ane_,_____:___ II 54O-59-0———————1, 2-Di ch 1 orpethene C total > "„ II 67-66-3r--—-T-~~~rCh 1 orof orm.___^^_________^^____ I

I 56-23-5——:—'—-——^Carbon f etrachloride___;____ ii 1 f\a_.A _A_____.......---...11•; •n'.j 'ii j. vc> w*j—"i———————v u. ny J.• 7S--£'7-'4.----- -.—-—Brombcl I

I 100610-1-5-—-_——ci.s-1, 3-DichlorpprPpene_____ Ii 79-0I--D"---—?——=—-Trichloroethent?___________;___ Ii 124-48-1-—————^jOil^rpmj^chlp-rp^methant?^__^^_=._^.-l.I 79-00-5-—*- -~> =l, 1, -lTrJ.chlprpethane,_ ^ , __ If 71 -43-2——™-——™-B'e'nz e'he_ 'f___^___________"____ lI 10061-OE-6—————trans~l , 3-Dich'lprpprppene___ I1 75-H5-S.—:—--—-~Bromoform_________;_________ IIOW —* 'I ») -" 1 ~™ •*——•-•**" — -i-. —•-*—- li i |V| jî " r> •.* T —* «J — L"*11X1 v^ *fr* "» v% Jî i.' 1J' *^ *-* J* w j* 7 j i tr L- *« > J. £*• r t. II w til 11U j I ti l

I 591-73-6—-——---2-Hexanone_____;____ZHIIZZZZ'1 127-18-4——•———™Tetracnlcjroethene___________ II 79-34-5--—-*-*- —'~-~-i,1,2, 2-fetrachioroethane___ 1j ios-88-3———————Toluene__^__________________I' 108-90-7———'——""Chlorobenzene_^_____________ I: lot) ;-41-~4™——————Êthyl benzene__________________ iI 100-42-5——-——-Sbyrerie „__..". ;.._"_ _„ _____Z'i 1330~£C)~7—^———-totar'Xyleines,

FORM I VOA

ift ' EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

I CAU61uab Name: VERSAR INC Contract: Ga-01-7471 I

uab Code: VERSAR Case No.: 133S3 SAS No.s" SDG HP.: CAW50

Matrix: (soil/water) SOIL. Lab Sample ID: 93396A

Sample wt/vols 5-0 Cg/mLi G Lab File IBs R3011

Level: Clow/med) LOU Bate Received: 12/20/89

% Moisture: not dec. 41 Bate Analyzed: 12/23/39

Column: (pack/cap) PACK Dilution"Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L or ug/Kg) UG/KG R

74—37—3———---—•"•-'Ch lorome thane74—S3-9————————Bromomethane_75-01-4—————:——Vinyl Chloride75-00-3—--——:———-Chloroethane_____________75-09-2————-——-Methylene Chloride____Z__£7-64-1——————=—Acetone_________________75-15-0————————Carbpn Disulf ideZ_._Z-_ZZjZ75-35-4—-—•———1, 1 -Dichl oroeth ene_______75—35-3————:——-—1, 1-Dichl oroeth ane_______54O-59-0———————1,2-Dichloroethene < total)67-66-3——————"—*»Ch lorof orm

78—93—3———'•-—-:=-2—But a none__________^71-55-6—————~—1, 1, 1-Trichloroethane

1 56—23—5——————"—Carbon Tetrachloride__I 103-05-4—————rr-vinyl Acetate! /?5—27-4——"———:——ctromod ich Iprometh ane__Mi^^._i 7S-37-5———————•**!, 2—Dichl OTo'propane_____^__I 100610-1-5——————cis-1, 3-Dich"lorppropene_\_\ 79-01-"6"—--——————T rich Iproeth ene_________;_! 124-4B-1——————=—Dibromoch lorome thaneI 79-OO-5——————^1, 1,'2-Tri chl oroeth ane_______I 71-43-2————————Benzene_________.___________I 10061-02-6————— trans-1, 3-Bichlorop-ropen^Z__I 75-25-2———————-Bromoform/______________,____108-10-1——————"-4-Hethyl-S-Pentanone____;___591-78-6———————2—Hexanone__________-___-_-'__127—18—4———————Tetrachl oroeth en©_______,___79-34-5————————1,1,2, 2-Tetrachloroethana___103-88-3—•—————^Toluene_________________'___103-90-7—=—-——^^Chlorobenzene_ ..... \X 00-41-4-——————Ethyl benzene__100-42-5-———————-Sfcyrene________1330-20-7——————Total Xylenes___


1. U J j. £ U

1AVOLATILE ORGANIC'S.ANALYSIS .MTfl SHEET

Lab Name: VERSAR TNC ' • • t ... . I CAU62" &3»01-7471 !

b Cod.: va»flR Case NO:; 13383 -, -—— HO--- SDQ HO_; ——^

Matrix: (soil/water) SOIL".""""* ' " ^" "" ---•=-- — •- —Lab Sample ID: 93397A

Sample wt/vol; 5 o fn/^\ i ' n : .::."^-0 <g/iaL) b Lab File IB: R3S1O

Level: (low/med> LOW =---- ——Date Keceiveds 12/20/39

% Moisture: not dec. 23Bate Analyzed: 12/2a/89

Column: (pack/cap) PACK ~ 'Dilution Factor: 1.0

CAS NO. COMPOUND ' CONCENTRATION UNITS:uum uuwo Cug/L ar ug/Kg) UG/KG Q

I

I ^4~S^~3~~"r^~~~^^c'ilorome'bhane _, ----- I ,J /jt — D > ft ^, - - — —J -«— —**«*i,: -M.___._ t r •( 1 I I t^ tiJ-,J——-.————±*rpmoTffethAne . ' ——————, il M,' ^™^~4——————'^iny ilh 1 oridi~———————————— f ! ni 75-00-3—— -—-rTVfrv r«4-V-:;;_" ~!—————————'- 13 i u i

_ ___________________ i iLf I U II 75-09-S-——~^~-^-Tiethx,i^ne_Chloride_Z_Z_Z__ ] - 6 I U II 67-64-1——"-—————Acetone_____________________ I . 13 I U II 75-15-0——~———-Carbon7Bij5W.lf.ideZ___^Z_Z_Z_Z_f. 6 IU 1I 75-35-4————~-~T,_i-Dic_hlprQe_then5___^__»„_ ' 6 I U II 75-35-3————————-1, l"-Dichloroethane_.____^_.____^.:_-_.,l 6 IU II 540-59-0——^-—— 1, E~Dichloroethene Ctotal) __ I 6 IU J

- — ' • ' - • ' - 6 1 U I

6 IU I13 IU 1

_ ________, 6 I U I-^-CaTbo^'tetrachlOTide . " i 6 IU 1

__ j n':: ; """ " "" 'f

I '/"l •—A i"i_*% " " _"" " - - - - j - - i ' ., _ _ , —™_.__—,,___,__ • .-j i .j- i - 2 = *~™"1'.-i-r2™Trichlprpethc(ne I n

I /!--*3-£————-"——-Benzene.. _ ___;_____~———————f P I

! i3!eiZpS"fi"" f*-:n"S 3-5Ichld °P op 5Zir"l ' 6 lu' o c-o e - ——"-^-^Bromoform . , ...

'«______ i 6 I Unene—_;__:________ I 4 j jX.emetha

I 1591— 7A—ft-___i___ o itOVA /o t. ——————2—Hexanone

J 79~34~ ---- - ~~r? i, a,2~Tetrachlproethane

431330---SO-7—

n

"

U

1/87 Rev

B IB _ EPA SAMPLE NO.SEMIVOLATILE QRGANICS ANALYSIS DATA SHEET ' _______________

I II CAU50 I

Lab Name: VERSAR INC Contract: 6S-O.1-7471 I_______________.1

b Codes VERSAR Case HP. : 13383 SAS No. : SBG Mo. : CAU50

Matrix: (soil/water) WATER Lab Sample IB: 93398

Sample wt/vpl: 1000 Cg/mL) ML Lab File ID: T1368

Level: (low/med) LOU Date Received: 12/20/89

% MPistures not dec. dec. Date Extracted: 12/2E/89

Extractipn: (SepF/Cont/Spnc) SEPF Date Analyzed: 01/24/90

GPC Cleanup: (Y/N) N pHs Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L or ug/Kg) UG/L Q

108-95-S———————-Phenol____________________„„111-44—4 ——————— bis<2-Ch loroethyl) Ether____.95-57-6————————=2-Chlorophenol________,____;__541-73-1 ——————— 1, 3-Dichlprpbenzene__-_m____.106-46-7———————1, 4-D i chl or P benzene.__t(__.__.__.100-51-6————————Benzyl ftlcphol___________;_,95-50-1-———————1,2-Dichlprpbenzene______,_,95-48-7—————————£-Methyl phenol_______.______,39638-32-9r-—————bis(£-Chlorpisopropy1)Ether,

10 IU10 IU10 IU10 IU10 iU10 IU10 IU10 IU10 IU

67-72-1—————-—:.-=Hexachl oroeth ane____________98-95-3—————————Nitrobenzene_________________78-59-1——;—-———Isdph prone______________:__38 75-5—————————e-Hitrophenol________________1O5-67-9————————2, 4-Dimethyl phenol_______|_;_65-85-0————————Benzoic Acid________________111-91-1———-—-bis(2-Chlproethoxy>Methane^_120-a3-2——————^E,4-Dichlprophenol_______'__12O-82-1————————1, 2, 4-TriChlorobenzene_______91-20-3————————Naphthalene________________106-47-8———'———4-Chloroaniline_____________87-68-3————————He xachloro butadiene_________59-50-7———————-4-Chloro-3-Methyl phenol______91-57-6————=——-S-Methylnaphthalene_________77-47-4————————Hexachlorocyclopentadiene_.__S8-O6-2--™——-—-=2,4,6-Trichlorophenol____,__95-95-4 ———————— 2,4,5-Trichlprophenol _______91-58-7 ———————— '-B— Chl oronaph thai ene _________88-74-4 ———————— S-Nitro.aniline __________ i __131-11-3 ——————— Dimethyl Phthalate __________20a~96~8 ——————— Acenaphthylene __________ _ _ ._606-20-S ————— . — 2,6-Binitrotoluene

106-44-5—————---4-Methylphenol________.___:__! . 10 IU621-64-7————:———N-Nitroso-Bi-n-Prppylamine,__1 10 I U 1

10 IU I10 IUJO iU10 !U10 IU50 -IU10 IU10 IU10 1U10 IU10 IU10 IU10 IU10 IU10 IU10 IU50 JU10 IU50 IU10 IU10 IU10 IU

FORM I SV-1 l/a7 Rev,

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____________

J /-_; _ I.__ - f CAU50 I

Lab Name: VERSAR INC - ~- Contract: 68-01-7471 I_______________I

'b Code: VERSAR Case No.: 13383 - SftS No.: SDG No.: CflWSO

Matrix: (soil/water) UATER^ "" Lab Sample ID: 93396

Sample wt/vol: 1000 <g/mL) ML Lab File ID: T1368

Level: Clow/med) LOU Date Received: 12/20/89

% Moisture: not dec. " dec. Date Extracted: 12/22/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 01/24/90

GPC Cleanup: <Y/N> N ' pH: Dilution Factor: l.O

CONCENTRATION UNITS:CAS NO. "COMPOUND <ug/L or ug/Kg) UG/L Q

99-09-2— - — :— — 3--NitroaniiineS3 -32-9 ——51-28-5 ——— -— — — S,"4"-i)iriitrophenp.l,1OO-O2-7 —— — -~ — 4-NitVophenoj, _ _ ;_ ____ __ -132-64-9 ——— — - — Dibenzofuran

_ _ _ _ , , , __———— -MM-^IM* ,- ___.*MI I I f.Hb-l - -VIM..

121-14-2- —————— 2, 4-Dihitrotpluen.e _______84-66-2 ——————— ~~Diethyiphthalate_ ______ ~ _ .7005-72-3 —— — ~- -4-Chlorcphenxl-phenylether.86-73-7 — --— —— — '-:rFluorene~-__| __ " __________ ,100-10-6 ——— - —— -4-Nitroaniline _ _: __ _ _ _„__]534-52-1——- - ™4, 6-Din"itrP-2-Metihyl.phenoI"86-3O-6 ——— • ———— N~Nitrpsodiphenylamine .(!>,101-55-3- ———— ; —— 4— Bromophenyl-phenxlether__118-74-1 ———— = ——— He xachl pro benzene,87-86-5: ——— - — = — '-Pen t ach 1 or o phenol,85-01 -8-- — —— : —— Phenanthrene120-12-784-74-2--£06-44- )—- — ^ — Fluor an thene129-00-O ——————— Pyrene_ _____ . ___ \ __ _ _____ _85-66-7—— — --;::: -Butylbenzylph thai ate _____ .91-94-1 — ; —— -^ —— 3, 3' -Dichlorobenzidine, ____56-55-3 ———————— Benzo (a) Anthracene _______ .£18-01-9 ——————— Chrysene ______ .f _____ i ____117-81-7 ——— : ——— bis (2-EthylhexylTph thai ate,117-84-0 ——————— Di-n-Octyl Phthalate _____ .305-99-2 ———— r: — -Benzo (b>Fluoranthene__. ____ ,£07-08-9 —— — : — — Benzo (k) Fluoranthene_. ____ .50-32-fl —— '— —— - — Benzo (a)Pyrene ___________ .193-39-5 ——————— Indeno < 1, 2, 3-cd7pyreneZ_IJ53-70-3------ — Dibenz (a, h) Anthracene ____ .191-24-2 ——————— Benzo (t|, h, i) Perylene_, ____ ,

50 IU10 IU50 IU50 iU10 IU10 IU10 IU10 IU10 IU50 IU50 IU10 IU10 IU10 IU50 IU10 IU10 IU10 IU10 IU10 IU10 iU20 IU10 IU10 IU10 IU10 IU10 IU10 IU10 IU10 IU10 IU10 IU

(1) - Cannot be separated from Diphenylamine

FORM I SV-£ 1/S7 Rev,

IB - - - - - - - -- :-; EPfl SAMPLE NO.SEN I VOLATILE ORGftNICS ANALYSIS DftTfi SHEET ...._..._ ________

I CflW5£3 Name: VJERSflft INC " "" ______ _ ,„ _Cor.tract : 6601_-7^

Lab Codes VERSflR Case~No. : 13363 SftS No.: r _ SDG NO. :

Mat r i x s ( moi 1 / wat er > SDIL Lab Samp 1 e ID: 4.376 _ .. _ ._

Sample wt/vol : 3gig J (g/rnL) G ___ ; Lab File ID: V44-S9

Lev&l : (low/mad) LOW Date Received: i£/agl/6S _

% Moisture: not dec. 1.7 dec. ___ Date Extracted: l£/£9/63

Extraction: (SepF/Cont/Sonc) SONG ; Date Analyzed: Ji9i

GPC Cleanup: CY/N) Y __ pH: 6. 3 _pilut ion Factor: 1 . 0

f'

CONCENTRATION UNITS:CflS NO. COMPOUND (uq/L or ug/Kg) UG/K6 Q

108-35-2—•—•-^3s=*r!henol________________1i1-44-4———————bis(£-Chloroethy1) Ether95-57-3———=——=——'i -Cn 1 oropneno 1 ________541-73-1———————1, 31 ®6-45-7———————1, 4—D i ch 1 orobenzene__.100-51-6—————-—-Benzyl Alcohol________.

95—46—7—————————2—Met hy 1 ph eno 1 _____________.3963S-3£-9—————bis<£-Chloroisopropyl)Ether,106—44-5————————4-Methy 1 pheno 1 ________.__. .r;r.6£ 1-S4-7———————^N-N i troso-D i —n-Propy 1 ami ne_.67—7£-l;——————^—^Hexaohloroethane__________.96—95-3——:——— - N i t robenzene______________.76—5S-1————-^^-—~lsophorone_.________________.68—75—5—————————^N11 rophenol ______________,105-67—9——————"fr, 4-D i met h y 1 pheno 1 _______._.

65-id—————————Benzoic Acid_______________.111-91-1———————ibis(£—Chloroethoxy) Methane__ i1 £0-83-2——-——— £, 4-Dichlorophenol_______.__.11 £0—62-1————=—-^1, £, 4—Trichlorobensene_____._ I91-£0-3—*-*—————Naphthalene________________t106—47-8———————'4—Ch loroani 1 ine__________p__1S7—S6-3——:——:— Hexach 1 orobut ad i ene______\__ I59-50-7————————4-Chloro-3-Methylphenol____._ I91 -57-6*————"•*—£-Met h y 1 napht h a 1 ene______:__ I77—47-4—-=-«————Hexach 1 orocyc 1 opent sd i ene,_ __„_. i88—06-£——:—— ^ £, 4, 6—Trichlorophenol_______I95-95—4————————£, 4, 5—Trichlorophenol_______I91-58—7————————£-Chloronaphthalene_________ I86—74—4—————————£—Nitroani 1 ine_ ,_____________ I131-11 -3—————=—*D i met hyl Ph thai at e__________ I£08—96—8————:—^^^^Aceriaphthylene____________._ i

£0-c:—-——— —£. 6-Dinitrotoluene __ I

FORM I SV-1 . r ^ A / Rev

1C : . fcPA SAMPLE NO.SEMIVOLATILE ORGANrCS ANALYSIS DATA SHEET _______________

I1 CAW5£

3 Name: VERSAR INC ._ ._.....L— V-'"-': "". Cpntf-_a(ft : 68-01-7471 I ___________.____

Lao Code: VERSAR Ca.se_Nc. : _.<k3383_ . SAS "No. : ".. . ' ". SDG No.: CAW50_

Matrix: (soil/water) SOIL .; .".,. . .. .""".""_....._. Lab Sample ID: 93376_____,_.

Sample wt/volT" '" "10..1 (.p/rnL) §.___,.... : ,=.,,.Lab File ID: V44£9

Level: (low/rued) L.OW . . . . .-. Date Received: 1

% Moisture: not dec, _.. —17 __ dec...___ Date Extracted: l£/£9/69

Extraction: (SepF/Cdnt/Sonc) SON£, , Date Analyzed: 01/84/90

GPC Cleanup: <Y/N> Y__ ..__.__,. pH: 6. 9 _ .Dilution Factor: 1.053

.CONCENTRATION. UNITS:CAS NO. COMPOUND" <ug/L or ug/Kg) US/KG Q

111f1i11111tiiili11l1ti1l111I1111t

S9_05_£_-___^

1 00-0£-7- — -—1 3£— 64— 9— —- — ~

84-66-2 ————— -7005-7£-3 ————

100-10-6 —————

_— — 13— fvj j t roan i i i ne—— Pcenaohthene- — £. 4— D i n i t ropheno 1— '— 4— Ni^rophenol ____ t __________-•— DiBenzof uran

1_1. 4 *r W -L M 1 U 1 f V wl A LH-*TJtr

-^--Diethvlphthalate—— 4— Ch 1 oropheny 1 —pheny 1 et her __—— Fluorene—— 4— N it roan i i i ne _____________ f

86-30-6 — —— — — —N-N~i~t~rosod i pheny 1 am i ne < 1 ) _ _ ,101-55-3 —— — — -— "— 4'— Bromophenvl — pheny lether ___116 74 1S7 — tJ'S — D ———————

84-74-S ———— —£06-44-0- ————1 £9-00-0 —————65-66-7 —————

i 1 f Oi — t —

117-84-0 —————£05-99-£—— -- -

—. — Pent acn 1 oropheno 1—— Phenanthrene~ — Anthracene—— D i -n— But y 1 pht ha 1 at e _________—— Fl uoranthene—— Pyrene—— Butvlbenzvlohthalate—— 3, 3' -Dichiorobenzidine ______- — Benzo < a Tflnt hracene—— —Chrysene-: — bis<£-Ethylhexyl)Phthalate __—— D i -n-Oc t y 1 Ph t h a 1 at e ________— •— "Benzo (b) Fl uoranthene

£07-06-9 —————— —Benzo < k) Fl uoranthene

193-39-5-----53-70-3 —————

1 ) — Cannot De

!JiLjri£. f \ d / ffyr L/ r i LJ _ _ _..

-^ — ^I ndeno (1 , £, 3-cd ) Pyrene ______—— Dibenz (a, h) Anthracene _______"—:— -^Benzo < p , h , i ) Pery 1 ene ________

400083040004000830830330830830

40006306306304000830630630630830630

830630630830£90830330830830

seoara t ed from D i pheny 1 am i ne

IIUIUIUIUIUIUIUIUIUiUIUIUIU1UIUIUIUIUIUiUIUIUIUmuIUJJiUIUIUIU

3J80 1 £

r rFORM I £V-£ 1/67 Rev.

IB : ; EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________._____

I1 CAW53

3 Name: VERSRR INC_______________ _ Contract: 68-01-7471 1 ___

Lao Code: vERSAR Case No.: 13365 SAS No..; _______ SDG No. : CAUI50

Matrix: (soil/water) SOIL Lab Sample ID: 95577____

Sample wt/vol: 3.0, 0 (g/mL) G__ Lab File ID: T137£

Level: (low/med) uOW__ Date Received: l£/£0/89

% Moistures not oec. 3-1 dec. ___ Date Extracted: i£/£9/69

Extraction: (SeoF/Cont/Sonc) SQNl_ Date Analyzed: 01/£4/90

GPC Cleanuo: (Y/N) Y DH: 6.9 Dilution Factor: 1.063

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG_/KG _ Q

1 tf 6-35-S* — —111-44-4 ——— •Q^_s-"7__c_ ____,-jj— j f — £j— —— —— ..

541-73-1 ———1 0S-46-7 ——— •100-51 -& —— -

S=— 4 A— 7—— - — ;.i_>_'L>i_ibJ kj C. -J

1 06-44-5 ——6£l-S4-7 ———

/O -J3 1~-

66— / «j- -j "~ —105-67-3 ———65-BS-iZi ——— =

1 £0—83—2 ———

91-20-3 ————10S-47-S ———

59—50-7 — ——S J. *J t O"•77—47—4. ————S6-06-£ ———

6i2i6-£0-£ ——

1——— ^-Phenol 1———— DIS (£-Chloroethyl) Ether 1——— -^Sr-ChioroDhenol 1———— 1, 3— Di Chlorobenzene 1— : — -1, 4— Dichlorobenzene 1——— —&&rizyl Alcohol———— 1 , £— Di ch lorcbenzene

———— bis (£— Chloroisopropy 1 ) Ether _————— 4— Methyl phenol— = — N— N i t roso— D i — n-Propy 1 am i ne, __———— Hexachlorbetharie———— N i t roben zene————— .isophorone .—— : —— -4_ NitroDhenol— , —— ,-4— Dimethvlphenoi— -— — Benzoic Acid———— bis(£-Chloroethoxy) Methane _

———— 1, £, 4-Trichlorobenzene———— Naphthalene———— 4— Chloroani 1 ine '.——— -Hexacnlorobut ad iene———— -4— Chloro-3-Methyl phenol——— -— £— Met hy 1 na ph t h a 1 ene ;———— -Hexach 1 orocyc 1 opent ad i ene__. __———— S, 4, 6-Trichlorophenol——— — £, 4, 5— Trichlorophenol———— S— Chl oronaph thai ene————— £— N i t roan i 1 i ne———— D i met hy 1 Ph t h a 1 at e———— Acenaph thy Iene _ :———— £, 6— Dinitrotol uene _ . _____ ; _ _

1000100010001000100010001000100010001000100010001000

^ 10I?0

IWtftf

: 10004900

1015010001000

1000

1000Itf #0

100010001000

10004901121*T _7t&i<L'

100049001000

i«*R100®-

1

IUIUIUIUIUIUtuIUIUIUIUIU!UIUIU iIU iIUIUIUIUIUIUIUIUIUIUIUIUIUIU

li JQ \{iu • •!

I 5V-1 . _-_ - p.i^T Rev,

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________I iI CAW53 I

Name: VERSfiR INC _ .... .. ....-.-. :..Contract: 66-01-7471 I ___ I

Lab Code: VERSflR .Case No, : 13383 S,AS No. : ______ SDG No. : CAUJ50

Matrix: (soil/water) SOIL 1 . . . . Lab Sample ID: 93377____

Sample wt/vol: 30. 0 .(o/mL). G__ Lab File ID: T137£

Level: (low/med) LOUl ... . ._._. Date Received: l£/£0/69

Date Extracted: l£/£9/89

-t'io'n:""" "(SepF/Cont/Sonc)" SONC Date fnalysed: 01/£4/90

ieanuo: <Y/J\J) Y pH: 6.9 Dilution Factor: 1.053

CONCENTRATION UNITS:COS NO. 1 :: "COMPOUND <ug/l_ or up"/Kg) UG/KG

i^9 05 ci —•— . .... -"*" i -Nit v*o3Ki i 1 i ' _.*. . ___ .._.... _M "^ ™* "*• '" -.— - _ - - - -_** - ----- iirt.± CK7'l=l IT rOil- ^_/w- .J . -- -J lin. t? r PCI kJi i u l i t?r ft?

51 -£6-5 — : —————— «=!, 4— Dim trophenol.1 00-0£-7— —————— 4-N i t ropherro 1 __ ____________1 3£-64— S"— -—— — - — Di Senzof uran1£1 — 14— £ ——————— £, 4— DinTtrotoluene84-56-£ —— — • ——— -Diethyiphthalate_ _ m _________7005-7£-3- — -- — -4— Chlorophenyl— pheny let her __66-73-7 ———————— F 1 uorene1 00- 1 0-6 ——————— 4-N it roan i 1 i ne534-52-1 ———————— 4, 6— Di n i t ro— £— Met hy 1 pheno 1 _ . _66— 30— 6 — - — -—"—"- — N— N i t r6s"dd i ph eny 1 am i ne C 1- ) ___101-55-3— — — ——— "4— Bromop'henyl -pheny let her ____1 16-74—1 ——————— HexachlorobenseneS7-B6- D-— —— — — r Pent ach 1 bropheno.l ___________65—01—6 — s -!- -? — ^-Phenanthrene1 £0- 1 £-7— —————— Ant h racrene84-74-2 — -::-~* — ---T) i -n-But y 1 ph t h a 1 a t e£06—44—0 ———————— Fl uoranthenel£9-00-0 ——————— Pyrene65-68-7 ——————— —But y 1 benzy 1 pht ha 1 at e ________91-94-1 — r —— ..—-•. "3-..-S* — Dithlorobenzidine56-55—3 — • ————— —Benzo (a) Anthracene£16-01-9 ————— - — Chrysene, ... s .._ r .., . _ ....1 17-61-7 ——————— bis<£-Ethylhexyl)Phthalate __117-64-0 ——————— Di-n-Octyl Phthalate£05-99— £ — " — — ——"-Benzo <b)Fl uoranthene£07-06-9 ——————— Benzo < k ) F 1 uorant hene _ _ ______50-3£-8 —————— —Benso <a) Pyrene _____________193-39-5 ——————— Indeno < 1, £, 3-cd> Pyrene _____ __53-70-3 ———————— Dibenz (a, h) Anthracenel91-£4-£— — —— ——Benzo <g, h, i ) Perylene

-

4900" "~ 1000

490049001000

10001000100010004900490010001000

1000490037003901000

610044001000£000

£40030007001000£300£000190013001000890

1

Q

iiUIUIUIUIUIUIUIUIUIUiuIU(UtuIU1IJIU"11IUIU11IJIU1111

"1"102

"_i_________"CJ~i-<] "-"(1) - CarinoT De separated" from Di pheny lam ine

FORM I £JV-£ ^rritl^'v 1/S7 Rev.

IB EPA SAMPLE"NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___.____________

tI CAW54

Names VERSAR INC _______ Contract: 66-01-7471 i____________

Lab Code: VERSAR Case^No- : 13383 SA.S No...: ' SDG,; No. : CftW50

Matrix: (soil/water) SQlL Lab Sample IDs 95378_____

Sample wt/voli 30. £ (g/mL) G___ Lab File IDs. V4430

Level: (low/med) LOW.. Date Received: l£/£0/69

% Moisture: not aec. 19 dec. ___ Date Extracted: l£/£9/69

Extraction: (SepF/Cont/Sonc) SDNC Date Analyzed: 01/£4/90

GPC Cleanup: (Y/N) Y__ pH: 7. 0 _ Dilution Factor: 1. 053

CONCENTRATION UNITS:CftS NO. COMPOUND Cuo/L or ug/Kg) UG/KG G

1 06-46-7 ———I 100-51-6 ———

&£ 1-64-7 ———£7-7£- 1 ————

/ O W :3 1

ti 6 *~ 7 j — D — — "—

111-91-1 ——

31 C.*tl ^— — — —

1(36-47-6 ——

77—47—4 ———

95-95-4 ———3 1 iJO / • •»—

tio f *r •"+

131-11-3 ——

———— Phenol———— bis <£-Ch loroethyl ) Ether ___ ; _ _———— £^Ch loroohenoi L———— 1. 3— Di Chlorobenzene———— i , 4-D i ch 1 or o bens ene '.————— genzyl Alcohol———— 1, £— Di Chlorobenzene————— 2-Met hy 1 ph eno 1———— bis(£-Chloroisopropyl ) Ether _———— 4-Met h y 1 pheno 1————— N— N i t romo— D i — n— Pr opy 1 am i ne_, _————— :He"x ach 1 oroet h ane———— N i t robenz ene

———— £-N i t rooh eno 1 - -———— £, 4— Dimethyl phenol

J_t L_B J 1 d* W ^ L« tmt W X U

———— bis <£— Chloroethoxy) Methane __—— • —— £, 4— Dichlorophenol

—— ——Naphthalene— — — — 4-Chloroani 1 ine—— -— —Hex ach 1 or o but ad i ene———— 4-Ch loro— 3-^Met hy 1 pheno 1———— £— Met hy 1 naph t h a 1 ene—— - —— Hexachlorocyclopentadiene ___———— £, 4, 6— Trichlorophenol———— £, 4, 5— Trichlorophenol———— £— Chloronaphthalene _________———— £-N i t r o an i 1 i ne

•^•tlilEViiT r~ll\r>*OhJh^lfK

r-n_fer l idk-1' l 1 l y ± ferl Itr

• ——— — £, B— D i n 1 1 rot o 1 uene

860860660850B60860660860660860660860660860660660410086066086086086©66066017066086041006604100660860660

i

1IUIUiUIUIUIUiU)UiUIUIU)UIUIUIUIUIUIUIUiuIUIUtufUIJiUiUIUIUIU

• iu - •1

I03<t -

FORM I SV-1 . .. .. .. I-/67 Rev,o r* 'N . J-.T, —•f-.t-M i r* f

-C _ _ . . . . . . . EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA"SHEET

I CAW545 Name: VE.RS.flR INC.______ - -- "• .Contract: 66-01-7471 I

Lab Code: VEftSAR .Case' Mo". :: 1 .363__ " !SAS No. : _^_^_ SDG No. : CAW50.

Matrix: (soil/water) SOIL „ ,.., ., .___...,......_... Lab-Sample ID: 93378

Sample wt/vbi :"""" "30. £ Cg/mL). g___ Lab.. .File" ID.: V4430

uevei: (low/med) LOW .... . —...„_ . .Date Received: !£/

% Moisture: not dec. 19 . __ dec. _____ pate Extracted: l£/£9/69

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 01/24/98

GPC Cleanup: (Y/NT V___ '.'_... ; pH: 7. 0 Dilution Factor: 1. 053

CONCENTRATION UNITS:CAS NO. "" COMPOUND" ~ "" <ug/L or ug/Kg) UG/KG Q

f 9S-09-£————-——3~Ni t roani 1 i ne______________ I . 4100 I Ut 63-3£-S-—:——-=^=ftcenap"hth"ene_____.______„.„_i _ £30 I JI 51^36-5————————£,"4-f>init"rophenoV___________ \ ..„ 4100 I U\ 100-0£-7———----T 4-N i t roph eno 1 ________________ t 4100 I Ul 13£-64-9———————Di benzof uran___,________________ I 160 I Ji i £ i -.14-£———————^£, 4-D in i t rot o 1 uene____.___.___ I 860 I UI S4_££_2-———_—H3iethylphthalate_^______"' I .,_ 660 IUI 7005-7£-3--- ——---4-Ch 1 oropheny 1 -pheny 1 ether__ t 860 IUI aS-73-7——:-——•——-Fl uorene____________________I 860 t Uj 100-10-6———————4-N i t roan i"l i ne__i__________ 1 4100 1 Ui 534-52-1—————~-4, 6-Dinitro-£-Methyl phenol__,1 4100 IUl 86-30-6————-——=—N-Nitrosodi pheny lam ine (1)__I. 860 IUi 101 -55—5———•—--r-—-^4V—Bronic-bnenyf—pheny let her___ I 660 I Ut 116-74-1————————MexachlbrobenzeneJ____t_______i 860 i Ui , 67-66-5———---——Pent ach 1 oropheno 1J______-___ I 4100 I U

"~" "" " 3000 i\ 85—01—e-————————Phenanthrene_______t 1S0-12-7———————Anthracene_-________i s4-74-£-———-———D i -n-But y 1 ph tha 1 ate.I £06-44-0———:———FI uorant hene________________t 1 £9-00-0———————Pyrene_____________________i 65-68-7——————•——But y 1 benzy 1 pht ha 1 at e________i 91 -94-1——1—™—3, 3' -Dich lorobenz i d ine______* 56-55-3————-———Benzo (a'i Anthracene__________i 218-01 -9———————Chrysene___________________i 117-61-7—————•-~bis~<£-Ethylhexyl )Phthalate__I 117-64-0———————Di-n-Qctyl Phthalate_________l 205-99-2———•——Benzo (b)Fl uorant hene________I £07-06-9————•—-Benzo <k)Fl uorantheneI 50-32-6————————Benzo (a)i 193-39-5———————IndenoTi, £, 3-cd) Pyrene____.I 53-70-3——————-—Diben"z"<a, h> Anthracene______

410 IJ860 IU9600 I9100 1660 IU1700 IU5100 I5400 I860 iU860 IU6300 IX6600 IX6900 I3400 I860 I U>

I 191-£4-£———-——Benzo <g, h, i ) Perylene________ I £500

Cannot be separated from Diphenylamine

O r-* —v

FURM I SV-c; ** ' *' ' J-/W7 Rev.

IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

I CAW55I 3 Name: VERSAff INC ___________ Contract : £8-01-7471 i

i_ab Coae: VERSAR Case No.: 15585 SAS No.: " : " St)G No. : CAW50

Matrix: (soil/water) SOIL __ Lab Sample ID: 93379 ____

Sample wt/vols 30. I <Q/mL) G__ Lab File IDs V44£'£

Level: <low/med> LOW Date Received: 12/20/69

% Moisture: not aec. £3 dec. ___ _.."... Date; Extracted: 12/5:9/69

Extraction! (SepF/Cont/Sonc) SONC Date Analyzed: 01/24/90

GPC Cleanup: <Y/N) Y__ pH: 6. 9 Dilution Factor: 1. 053

CAS NO.

c

33 «J f O

W f «i f ? .b

1 06-46-7 ——— -100-51-6 ———

t_l 1 O /

106-44-5 ———

67-72- 1 ————

105-&7-9 ——

l£0-63-£ ———C.IS' OC. i.

3 J. C.W O

106-47—6 — — •87— SS-3 ——— —

-i « r*-"T r*9 1 —57—6- ——— —77-47-4 ————

95-95-4 ————91-58-7 ————88-74-4 ————

C.tTlC ~'J7i ~'

1

CONCENTRATION UNITS:COMPOUND <ug/l_ or u"g/Kg) "OG/KG

— . — Phenol———— b"is<£-Chloroethyl) Ether——— — 2— Ch 1 orcpneno 1 '••———— -1, 3— Dichlorobenzene

* *^4^tt^i_pr <*• wt^r J^»GT icr

——— :— Ben zy 1 A 1 coh o 1———— 1, £-Dichlorobenzene———— £— Met h y 1 pheno 1———— bis <£— Chloroimopropyl ) Ether _———— 4— Met hy 1 pheno 1— -. —— if\j_ jxj j roso— D i — n— Propy 1 am i ne __———— Hexachloroethane——— —Nitrobenzene———— tsoohorone————— £— N i t ropneno 1 _ _______ _____ _————— c_, 4— Dimethylphenol———— Benz o i c Ac i d———— b i s < £— Ch 1 oroet hox y ) Met h ane __— - — :— 2, 4— Dichlorophenol———— 1, 2, 4— Tri Chlorobenzene———— Naphthalene——— :_ 4— chloroani 1 ine—— — -^Hexachlorofautadiene————— 4— Chl oro—j— Methyl phenol———— £-Met hy 1 na ph t h a 1 ene———— Hexach 1 orocyc lopent ad i ene ___

ci, 4, 6 Trichlorophenol———— £, 4, 5— Trichlorophenol———— £— Ch 1 orona ph t ha 1 ene _________———— £— IM it roan i 1 ine———— D i met hy 1 Pht ha 1 at e———— Acenaph thy Iene———— 2, fc»-Diriitrotoluene

900900

900

900900900900

900900

9-00900900300

9004400900900900900900900900

900900

90044009004400

900-9013

Q

1IUIUIUIUtuIUIUIUIUIUIUIUIUIUiUlUiUIUIUIUIUIUIUIUIUiUIUIUIU

^OiC-m •IU1

"

is1 '1t

FORM I SV-1 . _: : _^*-vn •->--_•/67 Rev'

1C - - - - ----- -SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

I CAW55Name: VERSflfi IMC ______"____ Contract: 68- 1-7471 I

Lab Code: vERSflR __C_ase No. : 13383 SAS WoY: _______ SDG No. : CAI-J50

Matrix: (soil/water) SOIL , . ...... .,..._,.,.. ,.„.. Lab Sample ID: 93579

Sarnole wt/vol: 50. 1 (a/rnL> G__; Lab File ID: V4422

Levels .low/rued) i-OW _ ... ....... .Date Received: 12/20/89

% Moisture: not dec. £3 dec/ ____ " D a t e Extracted: 12/29/69

Extraction's "" = ""(SeoFTCont/Sonc) SQNC Date Analyzed: 01/24/90

GPC Cleanup: (Y/N) Y__ pH: 6. 9 =...." ...Dilution Factor: 1.053

CONCENTRATION UNITS:CAS NO. .-- COMPOUND (uo/L or un/Ko) UG/KG Q

39-09-2——————--3-Wt ro~ani 1 i ne.65—32—S————-——Acenapht'hene51 -£6—5 ———————— £V"4— D i n'i t ro pheno 1

4400 IU900 IU4400 !U4400 IU900 IU900 IU900 IU900 IU

4400 IU_ 4400 IU

900 IU900 IU300 IU

.4400 l U900 IU900 IU900 IU900" iU9130 IU

S5-6S-7--————-——Butyl benzyl phthal ate______ I 90S I U31 -94-1 -—•——:~;37 S -D i ch I or obenz i d i ne______ I 1800 I U

z. --/— •--- -~ — 4-N i t ropheno 1 ____ _- ___________132-64"— 9- ——— --—— — Dioenzof uran ________________1 2 1 - 14-2— ———— : —— •£ , 4— D i n i t rot o 1 uene _ _________84— 66-£— — - ~— - — — -D" ilet hy I pht ha 1 at e ____________7005-72-3- — — — "--— 4— Chlorbphenyl— phenylether __86-73-7 ———————— Fluorene ______ __ __________ ._1 00- 1 0-6 ————— — 4-N itroan i IJ e __ ', ____ _ ____ . _534-5S- 1 — ——— :— 4,~S-Di>ii"t "ro -Met hy 1 pheno 1__ ^66-50-6— —--—-7- — HxT-N i t r osoa i pheny 1 am i ne < 1 ) __101-55-3 — ~~- — '— — 4— Brornophenyl -pheny letner ___1 18-74— 1 — ——TV-- — :Hexach lore benzene __________ ,_67-66-5- — — ———pent ach Ic-ropnenol ___________85—01-6- ————— — rPnenan1;h120-12-7-.- —— --.—- Ant h"r a ce"rie84-74-2——————--Di-n-Butylphtha_late,£06-44-0——•— ---Fl uoranthene. "~129-00-0———————Pyrene__^_

56—55-3—:—————-Benzo <a) Anthracene.£16-01-9—————--Chrysene________.

I 117-81-7———————bis(£-Ethy!hexyl> Phthal ate__I 117-84-0———————Di-n-Octyl Phthalate________I £05-99-2——-----Benzo(b)Fluoranthene________I 207-06-9———————Benzo<k)Fluoranthene_________I 5S-32-6——~————Benzo<a7Pyrene______________I 193-39-5———-———Indeno (1, £, 3-cd) Pyrene_____^t 53^70-3—;——--=——Difoenz<a, h)Anthracene_______1 191-24—2——•————Benzc. Cg7~h,~"i) Perylene^_______I______________________________(1) - Cannot be separated from Di pheny larn ine

300 I U

900 tU900 IU900 IU900 IU900 tu900 IU900 IU9900-

FORM I SV-2 1/67 Rev,

IB EPA 'SAMPLE "NO.SEMIVOLATILE ORGftNICS ANALYSIS DATA SHEET ________

i Ii CAW56

( 3 Name: VERSA R INC______________ Contract: fe8-gi 1-7471 i_____________

Lab Code: VERSAR Case No. : 13565 SAS No, : '____ SDG No. : CAW50

Matrix: (moil/water) SOIL Lab Sample ID: 95360_________

Safnple wt/vols 30, 1 <g/rnL) G___ ._ Lab.File IDs . V4427

Levels (low/Hied) LOW Date Received: 12/20/89

% Moimture: not dec. £5 dec. ___ Pate Extracted: 18/29/69

Extraction: <SepF/Cont/Sonc) SDNC Date Analyzed: 01/24/30

GPC CleanuDS <Y/N> Y__ pH: 6.9 ___Diliation Factor: 1.053

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L or uq/Kg> UG/KG Q

c-

.LJ.jp I I J

95-57-6 ———541-73-1 —1 06-45-7 ——1 0O— 5 1 —6——<* -.--.- -**t .k *_J

55—50— 1 - ———95— 4fi— 7 ———*J*J T W 1

6£ 1 — £4— 7 ——S7-7£-l — --98-95-3 ———76-59-1 ———

105-67-9 —

120-82-1 —

106-47-6 —

77-47-4 ———Q Q RlC -^

•r * ^ "1

131-11-3 —20S-9&-S—

i

1+- neno i i

————— bis(£-Chloroethyl )Ether 1————— £— Chlorophenol 1————— 1, 3— Di Chlorobenzene 1————— 1, 4— Dicnlorobenzerie 1——— --Benzyl Alcohol 1————— 1, 2— Dichlorobenzene 1—— r —— £-Methy 1 pheno 1 1————— bis<2-Chloroisopropyl) Ether _ J————— 4— Met h y 1 pheno 1 1————— N— N i t r omo— D i — n— Propy 1 am i ne __ 1—————— Hexach loroettnane 1-- ——— -— NitroPenzene 1————— Isoonorone 1——— _. — ci^Nitropnenol 1————— 2, 4-Dimethylphenol 1————— Benzoic Acid 1————— bis <£— Chloroethoxy) Methane _ __ 1— • ———— £, 4— Dichlorophenol 1————— i. £, 4— Trichlorobenzene 1————— Napnthalene 1————— 4-Chloroanil ine 1————— Hex ach 1 orob ut ad i ene 1————— 4— Ch 1 oro-3-Met hy 1 pheno 1 _____ 1————— 2-Methyl naphthalene 1— ———— -Hexach 1 orocycl opent ad a ene _ _ _ 1-; ———— £•- 4^ 6-Trichlorophenol 1—————— £i 4, 5-Trichlorophenol 1————— 2-Ch 1 oronapht ha 1 ene 1————— 2— N i t roan i 1 i ne 1————— Dimethyl Phthalate " " 1————— Acenaph t h y 1 ene )——— — — ;i= ~6— Dinitrotoluene f

1

9£0920

9209209209£0920920920920920920920

~ 92092045009209209209209£09£09209209£09£045009204500920

9p8-

1IUIUIUIUiUIUIUIUIUIUIUIUIUIUIUIUiUIUIUIUIUIUtufUIUIUIUtuIUIUIU3€0i-iu - -

fni

. FORM I SV-1 : . -----rrr:?.rtrl/&7 Rev.

1C- - - —— ——— ———----- EPrt SflWPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

.- . . I CAW563 Name: VERSAR IMC__ . . .. ". . !.'"" Contract: 68-01-7471 I

Lao Code: VERSfiR ,Case_..N.Q, !___.!55.83 _,J$A.S .No. : " SDG No. : CAW50

Matrix: (soil/water) SOIL "' . Lab Sample ID: 93380____

Sample wt/voi : ' " 50. 1 vg/rnL) .G___ ~ .._.;.. Lap File ID: V44£7

i-evel: (low/rned) LOW : ..._'. ...... Date Received: ia/eg/89

"A Moisture: not dec. £5 . " _dec. ___ Date Extracted: l£/29/69

Extraction: "<SepF/Cont/Sonc> SQNC Date Analysed: 01/24/90

GPC Cleanup": (Y/N) Y__ .. .pH: 6,9 Dilution Factor: 1.053

__ _ CONCENTRATION UNITS:CAS NO. ^•-" COMPOUND '-••"'• ""• """(ug/L or ug/Kg) UG/KG Q

f 7 » iI 4500 IU

920 IU4500 IU4500 IU920 IU920 IU920 tU9£0 )U920 IU4500 IU4500 IU920 IU920 IU920, IU4500 IU9£0 IU9£l3 IU3£0 1U340 IJ300 IJ9£0 IU1800 IU9£0 IU9£0 IU920 IU920 IU920 IU920 JU920 IU920 IU9£0 IU

S 3 —"3£ -9—--—•——-™?ft c ena "ph't'hene^__________„__51— 28-S————————-^^-4— DI nitrc< phenol_________100-02-7-——---~4-Ni t ropnenp 1 _!_„_ "• -:--132-64-9——;—•-—- Dibenzof u'ran_____^--~____121-14—£-——.————,__, !4-D i n i t rot o 1 uene_______64-66—2-———--——-Diethylphthaiate_________7005-72-5—--———4-Chlorophenyl-phenylether_SS-75-7-^—"—————-F 1 uoren'e______.___100-10-6————--—-A-NTt roan i"l i ne534-52-1-——--"-"-"4, 6-D-initro-£-Methyl phenol__86-50—6—————————N—Nitrosodiphenylamine <1)__101 -55-3———•"—"—4-~0rorn6pheny 1 -pheny 1 et her___

I 116—74— 1 —————:—Hexach 1 orobenzene,l 67-66-5——————-—PentfacnToropheno-.i 85-01 —6————~r~—Phenant hrene___________t 1 £0— 1 £-7——-—-"——Ant hrace;ne_____.______i 64-74-£—--——^----Di-n-Butylphthalate___I £06-44-0———————F1 uorant hene_~________J 1 £9-00-0———————Pyrene_______]________t 85-68-7—:——•———B"utyl benzyl phthal ate__i 91 -94- i ———-———5, 3'~—D i ch 1 orobenz i d i ne.I 56-55-3-——------Benzo <a)Anthracene£18-01-9————-——Chrysene___________________117-61-7———————b is (2-Ethylhexyl) Phthal ate__117-64-0———————D i -n-Oct y 1 Ph t h a 1 at e______£05—99-£————-——BenzoTb) Fl uoranthene________£07-08-9———————Benzo (k) Fluor ant hene_^.______50-5£-8-——•———•—Benzo <a) Pyrene______________193—39—5———•———Indeho < 1 f £, 3—cd) Pyrene_^___53-70-3-———————Dibenz (a, h ) Anthracene,

t 191-24-2——————-Benzo (gIh,i)Perylene^___II__ I 9 ?R3I8Q II _____ •-_______________ ___________________________ I ___________^ -_-! _-____ "" ..<1) — Cannot be "separatee)" from Dipheriyiamine

FORM I 5V-£ " ^'---la7 ftev

IB EPA SAMPLE NO.SEMI VOLATILE ORGANICS ANALYSIS DATA SHEET

I CAW573 Name: VgRSAR INC __________ Contract:. 66-01-7471 I _

Code: VERSAR Came No. : 13565 SAS No. : ____ ' SDG No. : C.AW50

Matrix: (soil /water) SQIi- Lat? Sample ID: 93381 ____

Sample wt/vols 3g!U.0 (g/mi_) G___ . . Lat? File ID: V44£3

Level: tlow/rned) uOt*i Date Received: 12/2B/89

% Moisture: not aec. 58 dec. ___ Date Extracted: i£/£9/89

Extraction: (SepF/Cont/Sonc) IsQNC .Date Analysed:

GPC Cleanup: <Y/N> Y __ pH: 7. 0 __; Dilution Factor: 1. 0 S3

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG ___ Q

1 lAfi— 55— 2 ———^ *<J**J ._* <hv* IM

111--H-4-4 ———3o— 5 / — 6— ~ "— "—vJT^ J- ' i_> J.

1 lilt) *ttS /

100-51-6 ———

j 95_4£_7 ————OzroiiiQ *ic. s1 06— 44— 5 ———A -_' j T r ^j

621-64-7 ———67-72-1 ————np j— r- --— '-J -mSlmJ O

^- ^-_r J^l ^ 1 J ]_

- ___ .___£.. .___

w _<} r *_P •bJ

105-67—9 ———

111-S1-1 ———

120-82-1 ———9 1 -20-3 ————

l?t ~ A — Q.

59-50-7 ———

86—06-2 ————95-95-4 ————

86-74-4 ———

4,*ld*u (LI w

—— ---Phenol———— bis <£-Ch loroethyl ) Ether——— -H-Chloropnenol—— - — 1 . 3-D i ch 1 orobenz ene———— 1 , 4-Di Chlorobenzene———— Ben zy 1 A 1 coho 1———— 1, £— Di Chlorobenzene———— £-Methyl phenol— - —— bis <£— Chloroisopropyl ) Ether _———— 4— Met hy 1 pheno 1———— N-N i t roso-D i -n-Propy 1 am i ne_ __———— Hexach loroethane———— Nitrobenzene———— Isoohorone———— £— Nitroonenol '.— - —— 2, 4-Dirnethylphenol———— Benzoic Acid—— - — bis (2-Chloroethoxy) Methane __———— £, 4— Dichlorophenol———— 1, £, 4— Trichlorobenzene———— Naphthalene———— 4— Chloroani line_, _________ _____———— Hexach lorobut ad iene———— -4— Chloro-3— Methyl phenol— — • = -* £— Me t hylnaphthal ene ______ __—

J )l_.k ^ JI J J^^>l 'L. j' L- ± U LJ w i 1 v l LU L.T rrUT

———— £, 4, 6— Trichlorophenol _______———— £, 4, 5-Trichlorophenol———— £-Chlorona phthal ene ______ __— - —— £— Nitroani 1 ine———— D i m et h y 1 Ph t h a 1 at e _________——— —fiTcenaph thy Iene _____________ _———— £, 6-Dinitrotoluene

1100

1100

1100110011001100110011001 IBClA •Vb'

1100110011001100

ff\&\J. L •L»<L'

1 1 00

1100=r4P.pii.J'TlL lLk

1100110011001100

....... 11 001100110011001100

11005400

1100" """" 5400

. j fana^lD

1 1 1 00 ~

UuuuuuuuuuruuuIUU"IUtuIUIUIUIUIUIUIUIUIUIUIUJU1 1 IithniI Ui

u *.39V <Jri

FORM I SV-1 . - oo WS-.K Rev

1C . ••-"' --SEMJVOLATILE ORGANICS ANALYSIS'DATA SHEET

I CAW57h Name: VERSQR INC________________ Contract: 66-01-7471 I

Lab Code: v'E.RSftR Case No. ; 13385 SAS No. : _______ SDG No.: CAW50

Matrix: (soil/water) SOIL ._,... ..._„. . . Lab Sample ID: 95581____

Sample wt/vol; 50. 0 (g/mL) G "" ' Lab File ID: V44£3

Level: ilow/medr" L.OW .".._" .._,...! .Jl .... Date^-Re.peiveds l£/£0/69

% Moisture: not dec. 36 .dec. ___ Date Extracted: l£/£9/89

Extraction: <SepF/Cont/Sonc> SONC. Date Analyzed: 01/84/90

GPC Cleanup: (Y/N) Y __ pH; 7. 0 _ Dilution Factor: 1. 053

CONCENTRATION UNITS:COS NO. COMPOUND (ug/L or ug/Kq) UG/KG U

I 99—129-2—————————3-N i t roan i I i ne___.I 65-5£-9————>———Acenaphthene_"_"_._.I 51—23-5———-.-=—*.£ 4-i_ Dinitrophenol__,i 100-02-7————————4-N i t ro ph eno 1 _____.I 132-64-9-——— ---D i ben z o f ur an______I l £ 1 -14-£——————£, 4—D i n i t ro t o 1 uene,I 64-66-2——-----Diethylp~hthalate_J7005-7£-3————--4-Chloropheny1-phenylether.86-73-7————————F1 uorene

I 100-10-6——————4-N i t roan i 1 i neI 534-52-1 ——-—--4, 6-D i n i t ro-2-Met h y 1 pheno 1 _.i 86-30-6——•—"——N—Nitrosbdiphen"yl^ami"ne Q ) _.I 101-55-5— ^^^—*•%—Brornophenyl-Qheny let her___I ilb-74—l—————r—Hex"acm'brobenzene'67—66-5———-———'-—P^nt~ach'16rophenoi^__85—0 1 -6-———rr—r-T-Phenanthrene__:_;__:_120-1 £-7———————Anthracene________S4—74-2———- r—:—D i —n—But y 1 ph t h a 1 at e.£06-44-0————————Fl uoranthene

t 1 £9-00-065-68-7—————•—-Butyl benzyl phthal ateSi—54-1——————————37-3' —Dich lorobenzidine____m56—55—3—————-——Benso (a) Anthracene_______.218-01-9———————Chrysene_________________117-61 -7———————b i s (£-Et hy 1 hexy 1) Pht halat e.117-64-0———————Di-n-Octyl Phthalate

1 £05—99-£—•——:———Benzo (b) Fl uoranthene.I 207-06-9———————Benzo <k)Fl uorant hene_.I 50-3£-8—:——————Benzo (a) Pyrene_______.I 193—39-5—————Indeno(l,2, 3—cd) Pyrene.I 53-70-3————————Dibenz <a, h) Anthracene_.I 191-24-2———-——Benzo < g, h, i ) Per y Iene_.

5400 i U1100 IU5400 )U5400 IU1100 IU1100 IU1100 I U1100 )U1100 IU5400 IU5400 t U1100 IU1100 IU

"1100 IU5400 IU1100 IU1100 IU1100 IU1100 IU

1 100 1 U

1100 IU2200 1U1100 IU1100 IU1100 IU1100 IU1100 IU1100 IU1100 i U1100 IU1100

11 •„.-.____^___________________1_"_1___ f ""

(1) — Cannot be" separated" from D i pheny lam ine

FORM I SV-2 __ i/S7_Rev

IB : - .£PA SfliwPu£ NO.SEMIVQLftTlLE DRGANICS ANALYSIS DftTtf SHEET " "' :: : _._!"!_ __ ... __ .1 _ _

i:o Name: VERSAR INC ______________ ContraJct: £5-r"8 1-7V71 "i" r*"! : " — "<D'T

Lab Cod^s VERSAR Case No. : 15385 SAS No. : ______ _. SDG No. ;

Matrix s (soil /water) SOIL. Lab Sample ID: 95582

Sample wt/vols 30. £ (g/rnL) G__ ^ " l_"4tb ;Fi le ID_: V4425

Levels <low/mea) LQuJ Date Received: l£/20/S9

% Moisture: not aec. £7 dec. ___ Date Extracted: i£/£9/69

Extraction: CSepF/Cont/Sonc) SONC Date Analyzed: 01/24/90

GPC Cleanup: (Y/N) Y__ pH: 6. 9 Dilution .Fact or: 1 ,_0.53

CONCENTRATION UNITSCAS NO. COMPOUND iua/L or ua/Ka) 'UG/KG u

1 1 1—44—4— —————Jh ih .k PI 1

1 06-46-7 ——————

"3QA™A ~"~* Q

Jp v U ' P ' P -sj

ft;* 1 A4 7—67-72-1 ——————— -

1 78-39- 1 ———————

i 111 -?i i

I *f •*• ^ V *»/

1 106-47-8 ——————

1 59-50-7 ———————

1 77-47-4 ————— ——

t 131-11-3 ——————i •*"• iTt n T" rt1 i^ L'U Jw ii

I 606-20— £ —————• -'f \mJ !• t' L-*

1

i-^Phenol i— bis <£-Chloroethyl) ether J 1— £— Chlorophenol 1— 1, 3-D i Chlorobenzene 1— 1, 4— Dichlorobenzene 1— Benzyl Alcohol i— 1 , £— D i en 1 oro Dens ene _________ 1— -£— Methyl pnenol i— bis (£— Chloroisopropy 1 J Ether _ _ i— -4-Methyl phenol l— N— N i t roso— D i — n— Pro py i am i n4 _ .„ 1— Hexacn loroethane i— --N 1 1 ro benzene _______________ .J_— Isophorone I— 2— Nitroohenol , f— -2, 4-Dirnethylphenol . 1— Benzoic Acid _________________ 1— bis (£-Chloroethoxy) Methane __ 1-—2, 4-Dicnloroonenol 1— 1. £, 4- Trichlorobenzene 1— Naphthalene 1— !-4— Chloroani 1 ine 1— Hexach lorodut ad iene 1— -4-Chloro— 3— methyl pnenol i- — £— Methylnaphthalene _________ 1-^Hexach lorc-cyclopentaaierie_ __ 1—Hi', 4, 6-Trichlorophenol ____ _ __ 1— £, 4, 5— Trichlorophenol \ t— 2— Chl orone phthal ene _________ 1— £— Ni troani 1 ine ' 1— Dimethyl Phthal ate 1— Acenaph thy Iene . i— 2, 5-Dinitrotoluene 1

i

950- - i.icr.T!— '*— 'k-i

•asa950950950S3®3 -J^

950Z'O «."

'550'350550 .95095095046009503'i—JVl'

950950«• hJt*

950S50950

?u

460095046009*$>r-Si',• "i/*i.

950

i iiU iIU JIU 1

- iu tIU 1IU t

. I U . 1IU iiU

iU 1IU i

, iu , '' 1 U " " ilU (IU Ii l l

IU IiU iIU 1iU fIU !IU tIU l

„. ' - * _ , _ iiU I

"iU " " tiU tIU 1IU f

Oi« n i |i tW|Ul %/ Ifl

• 1 t* _ .1 *

iU 11 1

FORM I SV-1 . ^ - - ou

iC ' ; ' _ |: " .." cPfl0"R"&AN"ICSL ANALY"SISlJ5ATA "SHEET"" " „_,.__,

iI CAW56

3 Name: VERSA R INC_______________ Contract.: £6-01-7471 i

Lab Code: VERSflR _r Case No.,;. 13385., '. _SAS No. : ______ SDG No. : C0w50_

Matrix: (soil/water) SOIL ----- - - / "" Uab _Sarnple ID:

Sample wt/vol : 50. £ Co/mL) G____._ . ...Lab File ID: V4425

Level: (low/med) LDUJ ^ 1 __ ..__"...""_! Date Received: l£/£,0/6.9

% Moisture: not dec. "27 dec. ___ Date Extracted: 1S/S9/89

Extraction: XSepF7Cont/~S"onc> ""SONG ....._bate Analyzed: 01/24/90

GPC Cleanup: (Y/N) Y__ pH; 6.9 Dilution Factor: 1.053

CONCENTRATION UNITS:CAS NO. COMPOUND "' "(ua'/L or ua/Ka) UG/KG Q

^ 1 . -"-n , =;_ _ _._,...,„

132-64-9 ————— -

7005-72-3-----

100-ltf-6 —— - — :-554 52-1- —— ——

101-55-5—— - r———1 1 0 / *+' i

1 85-01-6 — -----1 128-12-7 ———— ——1 84-74-2 —————— -| £06-44- 0 ——————1 129-00-0 ——— —

1 117-81-7 ———— —

1 f^l "7l7l 7 _ _

t

t 1 ) - Cannot be

1— -3— N i t roan i 1 i ne 1- ML* l_' 1 JCL LJJ J L» J J L.* 1 Ibr \

— 2, 4-Dinitrophenbl i— 4— Nitrophenol - - . 1— -Dibenzof uran 1— 2^ 4-D i n i t rot o 1 u'ene _____ ___ __ 1-^Diethyiphthalate i— ~— 4-Chloropheny I'-— bheriylether___ 1— Fl uorene 1——4-N i f roan 1 1 i ne i— -^Vci-Dirritro— £'— Methyl onenol __ 1— N-N it rosodi pheny lam ine \ 1 ) _ __ i— 4— Sr ohio pheny I —pheny let ner _ I- — riexachiorobenzene . i-— -— Penta'chlorooheno 1 " ~~ ~ i_— — Phenanthrene ' i——Anthracene ~- - 1— Di—n— Butyl phthal ate i— Fl uoranthene 1— Pyrene - 1— Butyl benzyl phthal ate 1-• RT, "51 — Dich-Torobenzidine 1—Benzo (a) Anthracene 1— Chrysene ___________________ 1— —5 jTs <£— Ethyl hexyl ) P'hthalate __ 1— D i -n-Oct y 1 Ph t ha 1 at e ________ 1— Bert-zc*(b}Fi uorant hene ________ i— Benzo <k)Fi uorant hene 1— Benzo <a) Pyrene 1— Intienc < 1. 2, 3-ca') Pyrer.e i— Dibenz <a, h) Anthracene ____ ____. i•—— Benzd <q, h, i )Perylene. ________ i

" 1separates from Di phenvlarnme

460095046004600950

I?5?•4-000

950

9509509509509509501900950950950950950950950950

i iIU 1IU iIU lIU 1IU 1lU lIU 1!U 1iU ItU 1i U 1IU 1iU iIU IIU 1lU lIU 1IU 1fU 1IU 1iU iIU 1IU 1IU iIU lIU IiU iIU 1(U 1IU 1

"l 1r

FORM I SV-2 . 1 / 6 ? Rev.

l& . : _ . — EPrt SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATS SHEET ______________.

ii CAW59

( 3 Name: VgRSAR INC______________ Contract: 66-01-7471 J________

Lab Codes VERSAR Case No. : 15583 SAS No. : ______ SDG NO. :

Matrix: (soil/water) SOIL Lab Sample ID:" 33583

Sample wt/vols 30. 1 (g/raL) S__ Lao File ID: V4426

Level: tlow/r.ied) U3U Date Received: 12/20/SS.

% Moistures not dec. 59 dec. ___ - .. Date Extractec"; l£7'29/a9

Extractions <SepF/Corit/SoncJ SQNC Date Analyzed: ^1/

GPC Cleanup: (Y/N) Y __ DHS 6. 9 Di l.ut ion^pactor : 1.

CONCENTRATION UNITSCAS NO. COMPOUND (ug/L or ug/Kq) LJG/K'G

108-95-2 ——111 -44-4 ———

541-73-1 ———106-46-7 ———

1 100-51-6 ———

o&.— /i n.-.T... .... _.,,.,kl> 3OOO *iC. 3106-44-5 ———Sr*i C.A. ~7

C.Q ~7

111-91-1 ——120-63-2 ———

91-20-3 ————

1 S7-68-3 ———

1 91-57-6 ————

i 91-58-7 ————I < " % Q *» A J.

1 131—11-3 ———

1

r" M EM H— * 1

———— bis <£-Ch loroethyl ) Ether———— 2— Chl oro phenol———— 1, 3— Dichl orobenzen© ____ , ____———— i, 4— Di Chlorobenzene————— Benzyl Alcohol————— 1, 2— Dichlorobenzene— -— — - £— Me t h y 1 ph eno 1

bis <£ Chloroisopropy 1 ) Etner _— — — —4— Methyl oh eno 1————— N— Nitroso— Di— n— t-rropy lam ane __———— riexachloroerhane———— Nitrobenzene———— Isopnorone . .———— -2— Nitrc-Dnenol :— — — - — Si 4 D"irnetrTy 1 phenol _ ___ : ______

— Bensoic ficid ______________ ; _———— bis <2— Chl oroeth ox y) Methane^ _——— --2, 4— Dichlorophenol - -———— :1, 2, 4-Trichlorobenzene ! '.———— Naphthalene—— . — _4_Ef1 \ oroan i 1 i ne——— —Hexach 1 orobut ad i ene———— 4— Ch 1 oro— 3— Met h y 1 ph eno 1————— 2— Met hy 1 naph thai ene— ——— Hexach lorocyclopent ad iene _ ; _____

—2, 4, 6— Trichlorophenol2,4,5 Trichlorophenol

———— 2— Ch 1 oronaoh thai ene————— 2— N i t roan i 1 i r.e—— —Dimethyl Phtnalate————— Acenapnthy Iene———— £, 6-Dinitrotoluene

1100

1 1 00_

1.1 aa11001100i i 001100

1 1 00110131 100i lii'01 10011 id 1311 00

1 10KJ

1100110011 00

iiea110011001100

1100550131100

5500

i"i a§ -1100

1IUIU

iuIUIUIUIUlUIUIU1UIUIU

iUiU

iulUIUIUIUIUiUIUJUiu

iu. ." '

1i11111111111111

1i111111I111

!1i

FORM I SV-i , i/67 Rev

200C48

lC~-,= . . :.--.:_.. - . . : J..-H5EMIVQLATiLE"'ORGAiVJlCSv=A.>IALVSIS --DATA SHEET _._______

iLAW59

'3 Name: VERSAR INC - - - - - - - - ---Contraci: : "66-01-7471 t

Lab Code: VERSAR Case No. ; 13363 SAS No. : _______ SDG No. ; CAW50

Matrix: (soil/water) SOIL" "' "" " -—^ . Lab samp;_e u_j. 93365____

Sample wt/voi: " .J..0. 1 (g/rnL) G___ Lab File ID: v44£6

Level: (low/med) ..OW Date Receivea: IS/

% Moisture: not dec. 39 __._._..dec. ____ r Date Extracted: I2/29/69

Extraction: (SepF/Cont/Sonc) SQNC . . Date Analyzes: i3l/£4/90

GPC Cleanup: (Y/N) Y__ pH: 6.9 Dilution Factor: i. 053

CONCENTRATION UNITS: 'CflS NO. COMPOUND (ua/L or uo/Ka) UC3/XG Q

99-S9-£ —— — -

H3121-I32-7— ——

l£l-i"4-£— --

7005-72-3 ——

100-10-0 ————— -taj j*.- -Jl_ •" j.

101-55-3 —— -118-74-1 —— -O f OO — kJ

O*J V) 1 O .......

120-1 £-7 ————

129-00-0 ————Owl CO l

91-94-l: ——— -RC.— *?. =•_•?_.— -« —fcJD hJ^ o

1 £05-99-2- —— -

1 Jit) tlfC O

1 53-70-3 ———— -

i———— 3— Nit roan i 1 ine i _ji00

— — : — 2, 4^Dinitrophenol 1——— 4— Ni trophenol 1— • —— -Dibenzofuran 1— — r^_— £y 4— Di"ri i trot o 1 uene f——— D iethylph thai ate 1— 4 Chlorophenyl pheny lether __— — — Fluoriene— _ — 4— M i t r can i 1 i ne— - —— 4, 6— Di nit ro^-d— Methyl pnenol ___— • —— :N— Ni trosod'i pheny lam me ( 1 ) __—— — 4— Brornopneny l-pnenylether ___——— — Hexach lorooenzene—«--**--Pent ach i orooheno 1— — — P'henarifPir-'ene """ " " ~ "" "~ "~

r i r t l t r l r L^LhLJr ILJ

— — — -D i — n— But ylphthalate——— Fl uoranthene———— Pyrene— - —— Butyl benzyl pht ha late———3, 3' -Dichlorobenzidine ...—— •— Benzo < a ) Ant hracene___.~ _ ""„ _ „— — — Chrysene——— bis(£-Ethylhexyl)Phthalate __ ,——— D i -n-Oct y 1 Ph t h a 1 at e _______ _— ^^-Benzb < b) Fl uoranthene ___ ] _ . ___— _. — Benzo (k) Fl uoranthene— —-Benzo <a> Pyrene =—— — Iridenb'Cl, £, 3-ca) Pyrene——— Di'benz (a, h) Anthracene—-' —— &en z 6 ( g , h , i ) Pery 1 ene

1 * "

11 ida55005500110011001100

11001100

5500DD0011001 1 014

1100

DbOid1 10011001100

4003201100

2 aa1 1001100

3201100

110W

1100

1100i 1130

llljftp

I

!UiUIUIU(UIUIUIUiUIU,uIUiUIUiUIUlUIUIJ1 JtuiUiUIUi JIUiUIUIU

3801-IU • •1

II*1 -i

<1) - Cannot be separated from Diphenylamine

FORM I SV-£

IB aPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA ShiEET 'L " '. ____, ____._ _--__

(• %3 Name: VERSAR INC____________ Contract.: .66rJ4i-74_7i_ .. i .____-~~^_."**«- ~ " " , -_ - - ——

Lab Code: VERSAR Case No. : 13363 SAB No. : "" "SD6 No.": CAW50" _

Matrix: (soil/water) SOIL Lab Sample ID: 93384.. _....

Sample wt/vol: 30.0 <g/mL) G__ Lab. File ID: V44£4

Level: (low/med) LOW Date Received: 12/20/.Q9

•A Moisture: not dec. SE dec. ___ Bate Extracted: l£/£9/89

Extraction:" (SepF/Cont/Sonc) SQNC Date Analysed: 0l/£4/30

GPC Cleanup: (Y/N> Y__ pH: 6. 9 pi lut ion _Factor: 1. 053

CONCEN TRATI ON.UNIT5:CAS NO. COMPOUND (uo/L or ua/Ko) OG/KG Q

c

1111.1

11I

111I111t1t1\It1,

1f1f1JIJ11

111-44-4 ——95-57-8 ———E? J • ^~- 1lJ-4- 1 /W 1

106-46-7 ——100-51-6 ——j*j tajw j.9s! 4A 7

106-44-5 —6£ 1-64-7 —O / / 1± 1

98-95-3 ——7S-53-1 ——S6-75-5 ——

65-85-0 ——111-91-1 —

91-20-3 ———10S-47-6 —87-68-3 ———1= t T— - — -•53—50—7 ———

77-47-4 ——86-06-2——95-95-4 ——O 1 ^O "7

88-74-4 ——131-1 1—3 —

606-20-2—

i———— —Pheno 1 (————— bis(£-Chloroethyl ) Ether _____ 1————— £— Ch 1 oropheno 1 !————— 1, 3— Dichlorobenzene 1————— 1, 4— Dichlorobenzene I————— Ben zy 1 A 1 coho 1 ______________ 1—————— 1, £— Dichl orocenz ene l——— . — £— Me t h y 1 ph eno 1 ______________ 1————— bis <£— Chloroisopropy 1 ) Et her _ i———— ;==2p viet h y 1 ph eno 1 ___________ , __ __ 1————— N— N 1 1 roso— D i — n— Propy I am i ne __ 1—————— Hexach loroethane _______ .._____ '————— N i t robenzene I————— I soph or one i————— .-2-NitroDhenol 1——— ^ 2_- 4-D i rnet n y 1 pheno 1 I——— : — Benzole Acid I————— bis<£~Chloroethoxy) Metnane_ _ 1—————— £, 4— Dichlorophenol ' 1

- l.i-, 4 Trichlorobenzene 1—————— Naphthalene 1—————— 4-Chloroani 1 ine !————— Hexach 1 orobut ad i ene 1————— 4-Ch 1 oro-3-Met hy 1 ph eno 1 _ ; ___ 1——— — £— Methyl naphtha Iene _________ 1

Mexachlorocyclopentaaiene ___ i— . ——— 2 4, 6-Trichlorophenol ___ _ _ _ 1————— £, 4, 5— Trichlorophenol 1—————— 2— Chloronaphthalene __________ 1————— 2— N i t r oan Hi ne J————— Dimethyl Phthalate ' i——— — ftcenaphthy Iene i— 2,6 Dinitrotoluene ___________ 1

. _._ f

1000

1000

1000100010001 *c'*C**tl

10001000

; T000

.,.t?00- 1130010130

1C001000490010001000

1000

10001000

1 000"1000

.____ 10IZICI ,

: 1000""4300.,,,__

" ~ IPfl 0, __j-i.P| *V1 Wv* VItfBS "1000"

I

JU1 1

IUIUiuiuIUIUIU

IU

iu"IU.IUIUIUIUIUIUIUIUIUiuIUiUIUI , .

rt-h'iij Lf 1 1<i _W * •

ru1l i t1

1111tM*™1f

FORM I 3V-i 1/67 Rev,

1C • --_ - e_PA. SAMPLE NO.SEft'IVGLATILt CTRGfWrcS ANALYSES SfiTft1 "" ""

., -. ...:. __,__ _,-_-, ,. ..-.:-- .,- - I CAW60

'I. b Name; VERSAR INC____________ Contract: 6S-0l_-747l i

Lab Code: VERSAR Case .No. ; .13363 _ : SAS No. : ______ SDG No. : CfiWSft

Matrix: (soil/water) SOIL "" '- . Lab Sample ID: 93384_

Sample wt/vol : 30. 0' <g/mL) G __ .Lab pile ID: V44£4

Level: (low/med J LOW ._._... _ . __ ...._ ... __.._.JDate Received: 12/20/89

% Moisture: not dec. 32. ... dec. ____ Date Extracted: .2/29/63

Extraction: (SddF/Cont/Sonc) SONC Date Analyzed: 01/24/90

X£

leanup: (Y/N)

CAS NO.

51-28-5 —————100-02-7 ————132-64-9 —————121-14-2 —————84-66-2 —— ----

86-73-7 ———— ——100-10-6— ———

86-30-6 —— — --101-55-3 —————

84-74-2"———- -£06-44-0 —————1 £9-00-0 — ' ——55-68-7 —— - ——

1 117-81-7 ——— -t 117-64-0 —————

1 £07-06-9 —————

Y "'"oH: 6.9 Dilution

CONCENTRATIONCOMPOUND •"•"••" ' (ug/L or ug/Kg

l. _3 N it roan i i ine I_ - = - _ . • • - ; , . - - - - - • '

J-tcenapntriSKiS 1—— £, 4— Dinitrophenol 1—— 4-Nitrophenol _______________ 1—— Dibensofuran 1——2^ 4-D i n i t rot o 1 uene __________ i— —DiethVlphthaiate 1——— 4— ChlorOpiheny 1— pheny letner__ _ 1— Fluorene " i— — 4— Nit roar, i i me - - i— —4, Q-Dinitro-^-Methylpnenoi^ _ i—— N-Nitrosod i pheny 1 am me < 1 ) _ __ l .,- — 4-Bromophenyl -pheny let her ___ i— — — riexach lorooenzene ___________ i— ——Pent ach lorophenoi 1— '— T-Phenanthrene '. 1— - •Ar.thracene " ' 1— -D i -n-eU t y 1 ph t h a 1 a t e 1—— -F 1 uorant hene 1—— Pyrene 1—— Butyl benzyl phthal ate 1—— 3, 3' -Dichlorobensidine ______ i—— Benzo (a) Anthracene 1

t-*t • • Y-^t^riu.1 i--"-bis"(£-Ethylhexyl)Phthalate __ 1— — Di-rr-dctyl Phthalate " 1—— -Benzo < b) Fl uoranthene ________ 1— - Behz6"<t<) Fl uorant hene 1—— Benzo fa) Pyrene 1—— Indenb "(1,2, 3-cd ) Pyrene ___ _ __ i—— Dibenz <a, h) Anthracene 1—— Benzp^j ht i jPerylene ________ i- 1

Fact or : l

UNITS:> UG/K6

490010004900490010001000

1000

1000

490049001000

10004 '300

100010001000

10001 000

1000£0001000

100010001000

1000

10001000

053

Q

1IUIUIUIUiu1UIUiUIUtU1 UIUiU - .ILilUIUiUiu •fUIUIUiuIUIUlU!UIUIUIUIU

1

11111iiitiiiii

iiiiIllliiii1i1i

1(1) - Cannot be separated from Dipnenylarnine

FORM I SV-2

IB . . EPA SAMPLE MO.SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET . _______________

i CAWS!._ Name: VERSAR INC______________ Contract: 66-01-7471 i_____

Lab Code: VERSAR Case No. : 13383 SAS No. : ______ _ _SDG .No. : CAUJ50

Matrix: (soil/watgr) SOIL Lab Samoie ID: 933B5

Sample wt/voi: 30* 1 (g/rnL) G___ Lab_File ID: .._ V4428

<low/med> uQd Date Receivea: i£/£0/89

% Moisture: not dec. 41 dec. ___ Date Extractea: i2-/i£9/89

Extraction: (SepF/Cont/Sonc) SO___C: Date Analyzeas 0i"/

GPC Cleanup: (Y/N) Y __ pH: 6. 9 __ Dilution Factor: 1. 053

CONCENTRATION UNITS:CAS NO. COMPOUND (uo/L or ua/Ko) UG/KG Q

=14 1 _7"5— 1 —— —

_7O *tO t

1- ——— Phenol 1- ——— b i s < £-Ch loroet hy 1 ) Et her ___ __ 1- ——— £-Ch 1 oropheno 1 1- ——— 1, 3— Dichlorobenzene t• ——— 1, 4— Dichlorobenzene 1———— Benzy 1 A 1 coho 1 ______________ 1- ——— 1, £— Dichlorobensene 1- ——— "£-Met hy 1 pneno 1 1- , i-, _. , . , _ , , • - - .

106-44-5 ———————— 4-methyloherrol - - i6£ 1-64-7 ———

78-59-1 ———— -

65-85-0 ———— -111-91-1 ———

120-62-1 ———91-20-3 —— —

———— N— N 1 1 roso— D i — n— Pr opy 1 am i ne _ _ i———— H^xachloroethane I—— •— -N i t robenzene i—— -— Isophorone t—— ^ — 2— Nitropnenol -- - i———— c , 4-D i met h y i ph eno 1 ______ ! __ _ i———— Benzoic Acid 1••*»"»» ™ *fr T 1 **•*—— 1^^ 1 i"hlV i£5 rt fc*™! —f \.f \ rrt al" fr"l 3 Xi CA \u A. ? \ LI t^i i ± "— ' r v c? v l J i—1 f\ y / l* )CT v i > d ' > " J

———— 2, 4-Dichlorophenol )———— 1, 2, 4— Tri Chlorobenzene 1———— Naphthalene 1

1 06-47-6 ———————— 4-Ch 1 or oan 1 1 i ne i87-68-3 ———— -

86-74-4 ——— -

606-£0-£ ——— -

———— Hexachlorobutadiene ' . " 1———— 4— Ch 1 or o— 3— Met h y 1 ph eno 1 _ ', __ __._ l———— £-Methy 1 napht hal ene 1———— Hexach lorocyclopentadiene _ ^ 1—— -" 2, 4, 6— Trichlorophenol ________ i———— 2, 4, 5-Trichlorophenol '. ... 1———— 2-Ch 1 oronmpht ha 1 ene _____ , _ _ _ 1———— £-N i t roan i 1 i ne 1———— Dimethyl Phthal ate , . i———— Acenaph thy Iene I— ; —— £-^ s— Dinitrotol uene 1_ _ _ _ __ 1

FORM I SV^-1 :

120012001200120012001£001200l£001£00

l£00"1£00

1200

D7S0

1200

~ 1200120012001£00

1£00

57001200

1200

<->o

1IUIUIUIUIU

lUtUiUIUIUIUiui UfU"'!-...

IUIUIUIU1UIUm"IUIUIUIUiuiu"

IU1

uoi

11

- 111111tIIi

- 1

111i

11111f1111

IT11

TO Rev.

5EMIVGLATILE ORGANICS "ANALYSIS DATA SHEETl

Name: VERSAR INC ..... .. ... .._..,„'.. .Contract :'" 68-01-7471 I _______________ 1

Lab Code: vERSAR Case No. : 13363 SAS No. : ______ SDG No. : CAW50

Matrix: (soil/water) SOIL ' _;!_... Lab Sample ID: 93385_______

Sample wt/vol : .—'. 30. 1 (g/rnL) G__ Lab File ID: V44£8_____

Level: (low/med) LOW ; .. "' .'. . '. Date Received: l£/£gi/89

% Moisture: not dec. 41 dec. ___ ___ Date Extracted: 12/29/69

Extraction: (SepF/Cont/Sonc) SQNC Date Analyzed: 01/24/90

GPC Cleanup: <Y/N) Y__ . _ = pH: 6. 9 _ Dilution Factor: l. 053

CONCENTRATION UNITS:CAS NO. " COMPOUND (uq/L-or uo/Kg) UGA1G Q

99-09-2-83-32-9-

100-02-7132-64-91 2 1 - 1 4— £84-66-2-

OO t -J- r11210-10 — 6

So-30-S-101-55-3116-74-167—66—5—-11= IT. f -

120-12-784-74-£-206-44-0- _ _ .;.,•» .j.ltiJ"1liHj tl

3 1 3*T i

tilO l£l 1 3*

117-61-7

£05-99-2207-08-950-3S-8-1-93 -.i 9 -553-70-3-

i- .. . . . i Nitroaniline !—— • — "— •--- — Acenaphthene ' 1——— . ——— £",~4— D i n i t r o ph eno 1 1—— . ——————— 4_jvj 3^ t r o p j-, en 0 1 |

——————— Dibenzofuran 1— £-, 4— Dinitrotoluene 1—— — • — — -Diethyl phthalate i3 —— ——• -— — 4— Chlorophenyl— phenylether __ 1— - — — F 1 uorene 1... -j,- - u r .- , — — . ... — , — , — — . - _. . ,•4— l>J 1 1 roan i i i ne 1— — " —— ——4 , S-D i n 1 1 ro-£-met h y 1 pheno 1 __ 1

N-Nitrosodi pheny larnine < 1 ) ^^ !-.— ~— — ~ — 4— Bromopheny I -pheny let her ___ 1

Hexach lorobenzene I——— —- r-r^Pent acfi 1 oro ph eno 1 *———————— 'Phenant hrene i——————— Ant hracene 1

- - «—— ___ — __£) t _n_t, ut y 1 ph t ha 1 at e 1———————— Fl uoranthene 1——————— Pyrene 1—-- —— — -—But vl, benzyl oh thai ate i—————— —3, 3' — Dichlorobenzidine ______ i— — — Benzo (a) Anthracene i—— --_ — r— —Chrysene i——————— bis <2-Ethylhexyl) Phthalate __ 1—————— ._ £)i_n_Qctyi Phthalate 1——————— Benzo ( b) Fl uoranthene . ._ J—————— ~ Benzo <k)Fl uoranthene 1—— — —— r— Benzo < a) Pyrene 1— —.— — — — •=-—! ndeno < 1 , £, 3— ca ) Pyrene t————— -—-Da beriz (a, h ) Anthracene 1

— Benzo <g, h, i ) Perylene 1.... . . .. _ ....... i

j i <di|(,i1£0057l3WW -r KJKJ

57OW^ f v*O

120012001£06512001200^J t V_* tl

w> / t't'

I2i30U /0Cl300

1200l£0067056059023001200

/i iPli'A*4 syltJ120©1200350•»<-,,-.-ji_ii-_D0

l£0Clfi~ni7f(n pi'ivi '-tTnTr1 £.WF

iiUIUtuIUiUiUIUIUlUIUiUIUiUlUiU1 JIUIUt Ji J1 JIUIU1 TJ *J

IUIU1 J1 J1 JLLJ j

f 1 • if] fw •»» •- iu

1

1111

11111111i1

lli11t1ilflit111

i n1I Uiii(1) - Cannot be separated from Di pheny lam me

FORM I SV-2 1/S7 Rev.

_ 1£ : EPA SScMIVQuATILE QRGWNICS ANALYSIS DATft "S^tET " ' " ____ _

i• t CAW62"

Name: VESSAR INC______________ Contract; 68-01-7471 i

Lmb Code: VERSAR Case No. : 1____36.3_ SAS No. : ______ SDG No. : CP.W50

Matrix: (soil/water) SOIL LaD Sampie ID. 95386

Sample wt/vols 30.0 <g/mL) G__ Lab File ID: V44£l

Level: (low/mea) LOW Date Received: igygB/a9

% Moimture: not aec. 23 dec. ___ Date Extracted: 12/.29Z59.

Extraction: <SepF/Cont/Sonc) SONC Date Analyzed: gH/S4/9E

GPC Cleanup: (Y/N) Y__ PH: 6.9 ., . Di lut ion/Factor:

CONCENTRATION UNITS:CflS N0- COMPOUND (ug/L or uq/Kg) UG/KG

,T**O1

o

""

i10e-95-£ ——————— Phenol • I 900111-44-4 ——— —95-57-fl —————541-73-1 ————1 06-46-7 —————100-51-6 —— ——Q«v— sr> -i _„_

95-4S-7 ——————39638-3£-9 ———

62 1 -64—7 —————67-72-1 —————98-95-3 ——————~7!~l .. "l ,..1 _--n,____

105-67-5 ———— "65-85-0 —————111-91-1 —————120-S3-£ —————1213-82-1 ————— -91-2S-3 ——————106-47-6- ————A"7_C H-. T— -r-»__-T-

59-5(3-7 ——————91-57-6 ——————77-47-4 ——————SS-06-2 ——————95-95-4 ——————91-58-7 ——————3S-74-4 ——————

, 131-11-3 ————£08-96-8 — ——606-20-2 —————

—— bis(£-Chloroethyl) Ether _____ 1—— 2-Ch 1 oropheno 1 ______________ , 1—— 1, 3— Dichlorobenzene 1—— 1, 4— Dichlorobenzene 1—— Benzyl Alcohol ' " l—— 1, 2— Dichlorobenzene i——— 2— Met hy 1 pheno 1 _______________ l—— bis (2— Chloroisopropyi ) Ether _ 1—— 4-fllethyl phenol i—— -N— Ni troso— Di-n— Propyla.nine __ t— —Hexach loroethane 1—— Nitrobenzene 1—— Isophorone i—— 2— Nitroohenol . 1— - "2, 4— Dimethylphenol '.. 1—— Benzoic Acid 1—— bis<£— Chl oroethoxy) Methane __ i——2, 4— Dichloropnenol 1—— 1, £f 4— Trichlorobenzene , I— —Naphthalene ________________ 1—— -4-Chloroani 1 ine 1—— Hexach 1 orobut ad i ene 1——— 4— Ch 1 oro-3-Met hy 1 pheno 1 . 1— *-£— Met h y 1 na ph t h a 1 ene _________ i— •— Hexachlorocyclopentadiene, ___ i—— £, 4, 6— Trichlorophenol 1——— £, 4, 5— Trichloroohenol f—— 2— Ch 1 orona ph t h a 1 ene 1—— 2— Nitroani 1 ine _____________ 1—— Dimethyl Phthalate 1—— Acenaphthy iene ______________ 1—-—2, 6— Dinitrotol uene __________ 1_ ^

900

900

9003009009)3(39130.500900

" "" '900,9i3i3900900900

9004400900

Si309013,500900900913090(3•5i30S004400-StfE"4400

SfPISb£00

1

'-*'. 'U

IUIUiu._iuiUIUiUi U1 U .""IU ...

" iUIUIUIU

.. iUIU 'IUIUlUJUiUIU;

IUiu_. .!UIUIU •

308 MS- -J U _ • . '

1U_.jl« » . y> r"t f31T&?!

1

<.

57FORM I SV-1 1/67 Rev.

1C :. " :. dp A SPfrfPLd NO".'SEMIVOLATILE"ORGANICS ANALYSIS.DATA SHEET _______________

i• - i CAW6£

Name: VERSAR INC...____. .. _. . . '. Contracts' 68-01-7471 l

Lab Code: VERSAR_. Case ..No. : 13383 SAS No. : ____' SDG No. : CP.W50

Matrix: (soil/water) SOIL , ... _LaD Sample ID: 93366

Sample wt/vol : 3i3. 0 <g/rnL) 6 Lab File ID: V4421

Level: (low/meet) LOW ..tv,,,= -. =......,.,....- ....-., ..-JJate Received: 15/20/8.9

% Moisture: not dec. £3 "dec. ____J " ~_Date Extracted: i£/£9/89

Extraction: (SepF/Cont/Sonc) SDNC Date Analyzed: 01/24/90

GPC Cleanup: (Y/N) Y__ pH: £. 9 Dilution Factor: 1.053

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg> UG/KG Q

•**«r * ^ -/

100-02-7 ————1 32-64-9 —— -121-14-2 ——— "

1 7005-72-3 ——DC. "7 ~ffOD / O /

100-10-6 —————534-52-1 ————Oo J1O u

87-66-5 —————

1 120-1 £-7 ————

£06-44-0 ————129-00-0 ———

56-55-3 — ———218-01-9 ————117-81-7 ————

WW / *+ W

!9l-£4-£ ———

( 1 ) - Cannot b

1- —— 3-N i t roan i 1 i ne i

Ml»LJrJ<_i^Ji)vJJl-rriLJ 1

— -— — S, 4— D i n i t ropheno 1 ___________ I——— 4-N i t ropheno 1 i— —— Dibenzofuran 1~ —— -2y ~D i n i t ro t o 1 uene - 1- —— Diethvlphthalate' " 1— : — - 4-Ch 1 orb phenyl— pheny let her __ i—'• —— FTuorene • j

•*v S-'Qi'^iir.'li1 _ . _^ _ __ _ _ _ _ _ t

——— 4, 6— Dinitro— £— Me't'hy 1 phenol __ 1——— N-Ni trosodi pheny 1 am ine ( 1 ) __ _ i—— — 4-Brorridphenyl — pheny let her ___ i———— Hexach lorobenzene l—— -Pent ach lorophenoi 1

— : —— Anthracene i— - — Di-n-Butyi phthalate 1——— Fl uoranthene t

r-Yri_TltJ - - 1

——— But y 1 oenzy 1 pht ha 1 at e 1——— 3, 3' — Dichlorobenzidine 1——— Benz o < a > Ant hracene 1

——— bis (£-Ethylhexyl) Phthalate __ 1— — Di-n-Octyl Phthalate 1-— -— Benso (bTFl uoranthene 1——— Benzo <k) Fl uoranthene 1

C*tJ ' * i *• v-' 'id/ " y r ur r i^j i

——— Indeno < 1 , 2", 3-cd) Pyrene ______ 1• — ^~ irf'-enz < a, h ) Anthracene I» ——— Benzo(q. h. i ) Per y Iene ________ 1

1e seoarat ed from D i pheny 1 am i ne

4400'30044004400900900

500• 00901344004400900900

90044009013900

900900908900

I8l3i3900900

90i3Oi^iTi

900900900

'300•4b8•300

1 1

!U iIU 1IU 1lU iIU 1IU iIU IIU iiU i)U <IU 1IU l1 U . 1IUIU llU 1IU 1IU 1IU iIU iIU 1iU 1IU tIU 1fU 1IU 1IU 1!U IIU 1

3.&!2b- ru- r' 1 „ — n~ "3110253

FORM I SV-2.,= -- 1/S7 Rev.

ID EPA SAMPLE NOPESTICIDE. QRGANICS ANALYSIS DATA SHEET

! CAW50b Names ___________ VERSAR- INC. ___ Contract :_6S-01 -7471 . " i ____ ____ .

Lab Code: VERSAR Case No. : 13383 SAS No.: SDG No.:

Matrix: (noil/water) WATER Lab Sample ID: __ 93373

Sample vt/vol: 1000 (g/ml) ML Lab File ID: ___

Level: (low/med) LOW Date Received: __ 12/20/69

% Moisture: not dec. _______ dec. _______ Date Extracted: __ 12/22/89

Extraction : (SepF/Cont/Sonc) ___ CONT Date Analyzed: __ 01/24/90

GPC Cleanup: <Y/N)N pH: ___ Dilution Factor: _ = 1.0

CONCENTRATION UNITS:CAS NO. - COMPOUND (ug/L or ug/Kg)_UG/L Q

76-44-8 ------309-00-2 ————1024-57-3 ———

60-57-1 ----- -•7:7-55 — Q- — —— — -

1031-07-8 ———f n -->Q "331-3 -c;? o72-43-5 —— — -53494-70-5 ——5103-71-9 ———S103-74-7----*-) j- *j j 'X ^

11104-23-2 ——11141-16-5 ——53469-21-9 ——

11097-69-1 ——

---alpha-BHC---beta-BHC—— delta-BHC—— -gamma-BHC ( Lindane J—— Heptachlor— -Aldrin- — Heptachlor Epoxide—— Endosulian I—— Dieldrin- — 4_ 4* -DDE—— Endrin-— Endasulian II

t ** — LJJJU—— Endoeulf an Sulfate- —— 4 4 ' -DDTJ. f i U LJ 1

- — Methoxychlor---Endrin Ketone- — alpha-Chlordane- — gamma- Chl ordane---Toxaphene---Aroclor-1016- — Aroclor-1221—— Aroclor-1232- — Aroclor-1242 !---Aroclor-1248- — Aroclor-1254---Aroclor-1260

0.050. 050.050.050.050.050.050. 050. 100. 100. 100. 100. 100. 100. 100.500. 100. 100. 10x . KJ

0.500. 500.500. 500.501 0J- » It/

1.0

UUUUUuuuuuuuuuuuuu •uuuuuuuu

400008FORM I PEST 1/87 Rev.

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

1 I1 CAW52 1

Lmb Name:__________VERSAR, INC.__ Contract:_68-Ol-7471 1_____________*

Code: VERSAR Case No. s13383 SAS No. : SDG No. :CAW5O

Matrix: (soil/water)SOIL Lab Sample IDs __93376

Sample wt/vols 3D <g/ml) G Lab File IDs ___

Level: Xlov/medJ LOW Date Receivedt __12/20/89

X Moisture t not dec. 18 dec. _______ Date Extracted t __12/29/89

Extractions (SepF/Cont/Sonc) ___SQHC Date Analyzed: __Q1/26/9O

GPC Cleanup: <Y/N>Y pHs___7.O Dilution Factors _ l.O

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L. or ug/Kg>_UG/KG O

3O9-OO-2 ——1Q24-57-3— —^ W^VA O t W

6O-57-1 ———72-55-9 ———72-20-8 ———

SO-29-3 ———72-43-5-———f -& JL J O

53494-7O-5-

g» . \*5 V* J* f51O3-74-2--8OO--35-2—

111O4-28-2-11141-16-5-j-*-j _*to oi aWw~%uZ7 d£-L J

12672-29-6-JLJtw3j UJ X. * rtQ_e OO tJp^U3Ovw^p w

———— elpha-BHC———— beta-BHC— —— delta-BHC———— gamma -BHC < Lindane)——— Heptachlor———— Aldrin———— Hept-achlor Epoxide _________———— Endosulfan I———— Dieidrin————— 4_4-_DDE———— Endrin———— Endoeulian II———— 4. 4 * -DDD ___________ _———— Endoeulian Sulfate————— 4 . 4 * -DDT _________ ; ___________—— — Methoxychlor———— Endrin Ketone

. -^ r*Ki — iQ W/IH uJJi JLuJr'ua Ji&—— - — gamma -Chlord ane———— Toxaphene— — !• - Ar oclor - 1 Ol 6 _____________ , __———— Aroclor-1221— — — Aroclor— 1232- - - — — Ar oc J. or - 1 242-- —— Arocloi — 1248

n± w.w uA ^ ^ JfA

——— -Aroclor-126O

. /

. /9.797* /9.79.7• *9.7191919191919199719191919O

9797*j fIS f

9719O190

UUUUUU

UUUUuuuuuuuuuuuuuuuu

AR300I22

FORM I PEST 1/87 Rev.

400016

ID EPA SAMPLE NOPESTICIDE QRGANICS ANALYSIS DATA SHEET

I CAW53Lab Names __________ VERSAR, INC. Contract: 68-O1-7471 I _

1 Code: VERSAR Case No. s!3383 SAS No. : SDG No. sCAWSO

Matrix: <moil/*ater)SOIL Lab Sample IDs __ 93377

Sample wt/vol: 3O (g/ml> G Lab File IDs ___

Levels < low/med) LOW Date Received: __ 12/2O/89

% Moictures not. dec. 32 dec. _______ pate Ext.rmct.edt __ 12/29/89

Extractions (SepF/Cont/Sonc) ___ SONC Date Analyzed s __ O1/26/9O

GPC Cleanups <Y/N)Y pHs ___ 7.O Dilution Factors _ l.O

CONCENTRATION UNITS:GAS NO. COMPOUND <ug/L or ug/Kg)_U(3/KG Q

II 319-84-6———————alpha-BHC.319-85-7———————be-ta-BHC_.319-86-8———————delta-BHC58-89-9———————^gamme-BHC (Lindane)76-44-S————————Heptachlor________,309-00-2———————Aldrin____________,1O24-57-3——————Heptachlor Epoxide.959-98-8———————Endoaul*an I____6O-57-1————————Dieldrin________72-5S-9—————————4, 4'-DDE™"_~_72-2O-8————————Endrin __33213-65-9—————Endoeul^an II.72-54-6—————————4, 4* -DDD_____.

121212121212i2

„ . 23232323232323120232323230120120120120120

________________ 23011O96-82-5—————Aroclor-126O________________I 23O

1O31-Q7-S——————Endosul^an Sulfate,5O-29-3—————————4, 4* -DDT__________'„72-43-5————————Methoxychlor.53494-7O-5—————Endrin Ketone.51Q3-71-9—————alpha-Chlordane.51O3-7-4-2——————gamma-Chl ordane,aoOl-35-2——————Toxaphene_____.12674-11-2—————Aroclor-1016.111O4-2S-2—————Aroclor-122l]11141-16-5—————Aroclor-1232.53469-21-9—————Aroclor-1242.12672-29-6—————Aroclor-1248.11097-69-1—————Aroclor-1254

UUUUUUUUUUUUUUUUUUUUUUuuuuu

FORM I PEST 1/87 Rev

n n

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ________________

I tt CAW54 i

Lab Names__________VERSAR, INC. __ Contract : 68-Ol -7471 I______________ t

IF code: VERSAR Case No. 113383 SAS No. s SDG No. sCAWSO

Matrixs <soil/water)SOIL Lab Sample ID: __93378

Sample wt/vols 3O <g/ml) G Lab File ID: ___

Level: (low/med) LOW Date Receiveds __12/2O/89

X Moistures not. dec. 19 dec._______ Date Extrsc-teds__12/29/89

Extractions iSepF/Cont/Sonc) ___SONG Date Analyzed: __O1/24/9O

GPC Cleanup: (Y/N)Y pHs___7.O Dilution Factors _ l.O

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg>_UG/KG O

76-44-8 ———3O9-OO-2 ——1O74-57-3--^ U J!> A ^t O

6O-57-1 ———

72-2O-8 ———^ *u u^ J

5O-29-3 ———n*^ A f+ P72-43-5----___„ .Q . ———— ___ „

tef M 1 —— Jl f U *|J

5103-74-2 —8OO1-35-2 —1 if ^9 Jt t t *^12674 -IJ. -2-111O4-28-2-11141-16-5-53469-21-9-12672-29-6-^«L%J*7' lj J ^11O96-82-5-

" — ' — — — B-LpnB-HHC

———— delta-BHC———— gamma -BHC (Lindane) ________———— Heptachlor———— Aldrin———— Heptachlor Epoxide—— — Endoaul-fan I———— Dieldrin———— 4. 4 - -DDE ____________ __———— Endrin_ _ ,_———— EndoEul-fan II———— 4,4'-DDD— ---Endosulian Sulfate _________———— 4r 4' -DOT- - — -Methoxychlor———— Endrin Ketone-• ——— alpha -Chlordane

———— Toxaphene— —— Ar ocl or - 1 0 1 6 _______________—— - — Aroclor-1221 ____ ___ _———— Aroclor l232——— -Aroclor-1242-- —— Aroclor-1248 _ _ _

— ——— Aroclor-126O

. D

* O

. O

. o

. o

. a

. O

. o2020202O202O2O37O

202O20200QO«pTCi

9898982OO2OO

UUUUU

UUUUUUUUUUuuuuuuuuuuu

^hFORM I PEST 1/87 Rev.

ID EPA SAMPLE NO.PESTICIDE QRGANICS ANALYSIS DATA SHEET _______________

I II CAW55 I

Lab Names__________VERSAR, INC. __ Contract :_68-01-7471 t ____________

L Code: VERSAR Case No.s!3383 SAS No.: SDG No.sCAWSO

Matrixs (moil/water)SOIL Lab Sample IDs __93379

Sample wt/vol: 3O (g/ml) G Lab File ID: ___

Levels <low/med> LOW Date Received: __12/2O/89

X Mo±«tures not dec. 24 dec._______ Date Extracted:__12/29/89

Extractions (SepF/Cont/Sonc) ___SONG Date Analyzed: __O1/26/9O•

GPC Cleanup: <Y/N)Y pHt___6.9 Dilution Factor: _ l.G

CONCENTRATION UNITS:GAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG Q

319-84-6———————alpha-BHC.319-85-7———————beta-BHC319-86-8———————delta-BBC_________,58-89-9————————gamma-BHC (Lindane),76-44-8———————Heptachior________.3O9-OO-2————————Aldrin1O24-57-3————-Heptachlor Epoxide_____959-98-8———————Endosulian I___________6O-57-1————————Dieldrin______________72-55-9—————————4, 4'-DDE________________72-2O-S————————Endrin________________33213-65-9—————Endosulfan II__________72-54-8—————————4,4'-DDD________________1O31-O7-8——————Endcsulian SulJate_____50-29-3—————————4,4*-DDT________________72-43-S————————Methoxychlor___________53494-7O-5—————Endrin Ketone___________51O3-71-9—————alpha-Chlordane________51O3-74-2——————^gmmma-Chlordane________SOQ1-35-2——————Toxaphene_____________12674-11-2—————Aroclor-lOlS__________111O4-28-2—————Aroclor-1221.11141-16-5—————Aroelor-1232.53469-21-9—————Aroclor-1242.12672-29-6——————Aroclor-1248.11O97-69-1——————Aroclor-1254.11O9S-82-5—————Aroclor-126O,

101010101010101021212121212114O1OO2121312101QO1OO1001001OO21021O

u

u..u,"u.

A H 3 O 2 5


ID EPA SAMPLE MO.PESTICIDE ORGAHICS ANALYSIS DATA SHEET __________________

i t" • • . ' • 1 CAW56 J

,ab Name:__________VERSAR, INC. _^_ Contracts_68-Ol-7471 I_____________ t

Code: VERSAR Case No. .13363 SAS No. : SDG No. :CAW5O

Ma-trix: (soil/water)SOIL Lab Sample ID: __933SO

Sample wt/vol: 3O <g/ml) G Lab File ID: ___

Level: (low/med) LOW D-rte Received: __12/2O/S9

X Moistures not dec. 25 dec._______ Date Extracted:__12/29/69

Extraction: (SepF/Cont/Sonc) ___SONG Date Analyzed: __O1/26/9O

GPC Cleanup: (Y/N)Y pHs___6.9 Dilution Factors _ l.O

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG Q

319-64-6————————alpha-BHC.319-85-7———————beta-BHC319-86-6———————del t a - BHC___________56-89-9————————gamma-BHC TLindane)_2..76-44-6————————Heptechlor_________~309-OO-2————————Aldrin1O24-57-3——————Heptachlor Epoxide.959-96-6———————Endosulfan I_____"m6O-57-1————————Dieldrin_ _ 22"72-55-9—————————4, 4' -DDE_2_22_22"72-20-8————————Endrin_______2_2_.33213-65-9—————Endoaulfan Il22_2]72-54-8—————————4,4'-DDD__________,1O31-07-8——————Endosulfan Sulfate"50-29-3—————————4,4'-DDT__________.72-43-5————————Me-thoxychlor___2_.S3494-7O-5—————Endrin Ketone____.51O3-71-9 — ———— alpha-Chlordane__.51O3-74-2——————gamma-Chlordane__.8OO1-35-2——————Toxaphene________,12674-11-2——————Aroclor-iO162___22]111O4-28-2—————Aroclor-1221____^11141-16-5—————Aroclor-1232_____.53469-21-9——————Aroclor-1242______12672-29-6—————Aroclor-1248_____.11O97-69-1—————Aroclor-1254_____.11O96-82-5—————Aroclor-126Q

UUUUUUUUuuuuuuu

uuuuuuuuuu

O

26FORM I PEST 1/87 Rev.

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _ ______

I I1 CAW57 I

Lab Names__________VERSAR, INC.__ Contract:_68-Oi-7471 1

L Code: VERSAR Case No.:13383 SAS No. s SDG No.:CAW5O

Matrlxs <«oil/water)SOIL Lab Sample ID: __93381

Sample wt/vols 3O (g/ml) G Lab File IDs ___

Levels (low/med) LOW Date Received: __12/2O/89

X Moim-ture: not. dec. 38 dec._______ Date Extraet.ed:__12/29/89

Extraction i <SepF/Cont/Sonc) ___SQNC Date Analyzed s __O1/26/9O

GPC Cleanups <Y/N)Y pH:___7.O Dilution Factors _ l.O

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG O

3QQ-QQ-7-— -— —^ <»' ^

6O-57-1 —————

J.UJ.1 — U/— o— — — —

S 4*3 -J

53494-7O-5 ——

11141-16-5 ——

"" TTl? ?? f

—— alpha-BHC

-— —delta -BHC— -gamiaa-BHC (Lindane)- — Heptechlor—— Aldrin— -Heptachlor Epoxide—— Endosulfan I—— Dieldrin

- — Endrin— -Endosulfan II

. . , r»p»r»4 . 4 Uw J

---EndoBulian Suliate—— 4^ 4 '-DOT—— Met.hoxychlor—— Endrin Ketone---mlphm-Chlordane—— gamma-Chlordane—— Toxaphene ____ _—— Aroclor-lO16—— Aroclor-1221—— Aroclor-1232—— Aroclor-1242—— Aroclor-1248

m uw-iku* A 4-fcj *—— Aroclor-126O

1313

13

1313

2626

262613O

2626

130

13O

13O

UUUUUUUUUUUUuuuuuuuuuuuuuuu

fc-V'/


ID , ,- EPA SAMPLE NQ_.PESTICIDE ORGAHICS ANALYSIS DATA SHEET __________________

t~ II CAW5S I

kab Names___________VERSAR, INC*___ Contracts_68-Ol-7471 I_______________1

Code: VERSAR Case No.:13383 SAS No.: SDG No.sCAWSO

Matrix: (aoll/water)SOIL Lab Sample IDs __93362


Levels (low/med) LOW Date Received s __12/2O/89

X Moistures not dec. 28 dec.________ Date Extracted:__12/29/89

Ex-traction s (SepF/Cont/Sonc) ___SONC Date Analyzed : __Ol /26/9O

GPC Cleanups <Y/N)Y pHs___6.9 Dilution Factors _ l.O

CONCENTRATION UNITS:CAS NO, COMPOUND (ug/L or ug/Kg)_UG/KG O

319-84-6————————alpha-BHC___________________319-85-7———————beta-BHC__________________319-86-6———————delta-BHC_______2222_22-2258-89-9— — ————garema-BHC (Lindane)________76-44-8————————Heptachlor________2222222223O9-OQ-2———————Aldrin____________________1O24-57-3—————Heptachlor Epoxide_________9S9-98-8———————Endosulfan I_____22-2_22_226O-57-1————————Dieldrin__________2_2_2~2272-55-9—————————4, 4 * -DDE_________________22-72-2O-8————————Endrin _ _33213-65-9——————Endoaul^an II______72-54-8—————————4,4'-DDD___________.1031-07-8——————Endosulfan iulifate.50-29-3—————————4>4'-DDT__________72-43-5————————Methoxychlor____;_.53494-7O-5—————Endrin Ketone____.51O3-71-9——————»alpha-Chlordane__]51O3-74-2——————gamma-Chlordane___8OO1-35-2—————-Toxaphene________12674-11-2 ———— -Aroclor-lO16-;____.11104-28-2—————Aroclor-1221_____11141-16-5—————Aroclor-1232_____.53469-21-9—————Aroclor-1242______.12672-29-6—————Aroclor-1248______11O97-69-1—————Aroclor-1254_____.11Q96-82-5—————Aroclor-126O

11111111111111112222222222222211O22222222O11011011Onono22022O

UUUuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

t t1 CAW59 I

Lab Names___________VERSAR, INC. ___ Contract s_68-Ol-7471 i_______________ I

L Code: VERSAR Case No. .13383 SAS No.: SDG No. sCAWSO

Matrixs (soil/water)SOIL Lab Sample ID: __93383

Sample wt/vols 3Q <g/ml) G Lab File ID: ___


X Moisture: not dec. 39 dec._______ Date Extracted:__12/29/89

Extraction* <SepF/Cont./Sonc) ___SONG Date Analyzed s __O1/26/9O

GPC Cleanups (Y/N)Y pHs___6.9 Dilution Factors _ l.O

CONCENTRATION UNITSsCAS NO. COMPOUND <ug/L or ug/Kg)_UG/KG O

5O-29— 3-- —— ——ww ~*& »j*T'9_^^_^______

O^W«3 f^~ — — — —

8QO1-35-2 ———* *>£SJA. 1 \ _O_

11141-16-5 ——

11Q96-S2-5 ——

—— alpha-BHCnet a one

— — — deJ.ta-oHC- — gamma-BHC ( Lindane >---Heptachlor • __________—— Aldrin— -Heptachlor Epoxide _________—— Endoaulian I—— Dieldrin

? LHJC* ______________—— Endrin—— Endoaulfan II

t *i. UUD __________

- — Endosul£an 5ul:f at.ef ft ULJ t _^ -.•.i.-—. _

—— Methoxy chlor—— Endrin Ketone— -mlpha-Chlordane—— gamma-Chlordane __ , _________- - -Tox aphene—— Aroclor-lO16 ________

. . . f+~—— — — Aroclor- 1242—— Aroclor-1248 ________ ——— Aroclor-1254_ ______— ——Aroclor -126O

1 3X<J13Jl -3

13 o1 3J. 1.1

nJU -313AWXtj

13oD

O

O

j O

JZQ

26xouoo

j£bDU

X >3 v

1 *^DJ. k3U

X iJU

X*3U

1 *^DJ, J

BU260

UUUU

UUUUUUUUuuuuuuuuuuuuu

FORM I PEST 1/87 Rev,

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _ ___

t II CAW6O t

Lab Names__________VE&SAIE, INC.__ Contract:_68-Ol-7471 I______________I

Codes VERSAR Case No.s13383 SAS No.s SDG No.sCAW5O

Matrix: <soil/water)SQIL Lab Sample IDs __93384

Sample wt/vols 3O (g/»l) G Lab File ID:


X Moisture: not dec. 32 dec.______. Dat-e Extracted:__12/29/89

Extractions (SepF/Cont/Sone) ___SONC Date Analyzed: __O1/26/9O

GPC Cleanups (Y/N)Y pHs___6.9 Dilution Factor: _ l.O

CONCENTRATION UNITS:GAS NO. COMPOUND <ug/L or ug/Kg)__UG/KG Q

1

319-66-8 ——

76-44-8 ———

*72-S5- — - — —f ff -JW ~*

OJ Jl J C3O ;3

72-54-6 ———1O31-07-8—

72-43 -S— — — —B? * A A <4 fff C.53494 -7O-5-510* -73 -o--oûw / *-f51Q3-74— *>— —«JJi-U.J t ** ...

8OO1-35-2 —12674-11-2-JLX JL w^ Ô ^

11141-16-5-53469-21-9-iÔ/A i3— O

11097-69-1-•i. J.U3O— O — 3"

—— — alpha-BHC

—— — delta-BHC— —— gamma-BHC (Lindane)———— Hep t a ch 1 or———— Aldrin———— Heptachlor Epoxide———— Endoeulf an I———— Dieldrin. _____————— 4 _ 4 - -DDE." ______ _22 ____ 22———— Endrin— —— Endosullan II ______________————— 4, 4J -DDD——— -Endoaulfan Sulfate _________———— 4. 4 * _DDT _________ 2222 ___ 22———— We-thoxychlor- ——— Endrin Ketone- —— -alpha -Chlord ane———— gamma -Chlord ane———— Toxaphene—— --Aroclor-lO16———— Aroclor-1221_. ___ . __________———— Aroclor-1232- ——— Aroclor-1242———— Aroclor- 1248 _______________——— -Aroclor-1254————— Aroclor- 126O

J.-C.

1212121212A *

124» »

1274"474j*i2424242474"412024242424012012012O12O12O240240

UUU

UUUUUUUUUUuuuuuuuuuuuuu

FORM I PEST

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: __ _VERSARf INC.. _ Contract: 66-O1-7471 I_

L Code: VERSAR Case No.:13383 SAS No. : SDG No. :CAW5O

Matrix: (aoil/water)SOIL Lab Sample ID: __93385


Level: (low/med) LOW Date Received: __12/2O/89

X Moimtures not. dec. 42 dec._______ Date Extracted:__12/29/89

Extractions (SepF/Cont/Sonc) ___SQNC Date Analyzed: __O1/26/9O

GPC Cleanup: (Y/N)Y pH:___6.9 Dilution Factor: _ l.O

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG Q

319-86-8 ————OS-03-9-——- ——76-44-8 ——————3Q9-QO-2 ————

959-98-8 ————6O-57-1 —————72-55-9 —————

72-54-8 —————1O31-07-8 ———

72-43-5 —————53494-70-5 ——51O3-71-9 ———5103-74-2 ———SOO1-35-2 ———12674-11-2 ——111O4-28-2 ——11141-16-5 ——

12672-29-6 ——11O97-69-1 ——11O96-82-5 ——

—— mlphm-BHC, . -our*i-I ^ L KV jU rf

—— delta-BHC—— gamma-BHC ( Lindane )—— Heptachlor—— Aldrin—— Heptachlor Epoxide—— Endosulian I—— Dieldrin—— 4,4*-DDE—— Endrin—— Endoaul-Can II—— 4, 4*-DDD—— Endoaul-tan Sulfate

44 * -DDTf UU M

—— Hethoxychlor—— Endrin Ketone—— alpha -Chl ordane- — -gamma -Chl ordane—— Toxaphene ______ __ _______- — Aroclor-1016

ft i • • T — ••• 1 ^ 1---Arocj.or-l22l_____ ____*.— -Aroclor-1232—— Aroclor-1242 ____ __ ^— — — Aroclor -1248—— Aroclor-1254 _ _—— Aroclor-126O .......

141414A

1414

14272727y27272727140272727

Jf f \J

14014014014014O27O270

UUUUUuuuuuuuuuuuuuuuuuuuuuu

RR300131FORM I PEST 1/67 Rev,

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

I CAW62 tb Name:__________VERSAR, INC. __ Contract s_68-Ol -7471 I _______________ 1

L.. . Codes VERSAR Came No. : 13383 SAS No. : SDG No. sCAWSO

Matrix: (soil/water)SOIL Lab Sample IDs __933S6

Sample wt/vols - 3O (g/rol) G Lab File IDs

Levels (low/med) LOW Date Receivers __12/2O/89

X Moisture: not dec. 23 dec._______ Date Extracted:__12/29/89

Extraction: (SepF/Cont/Sonc) ___SONG Date Analyzed: __O2/O2/9O

GPC Cleanup: (Y/N)Y pH:___6.9 Dilution Factor: _ l.O

CONCENTRATION UNITSsCAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG O

i31 9-84 -6 ——————— alpha - BHC _________________319-85-7 ——————— beta-BHC319-86-8 ——————— delta-BHC _________________58-63-9 ————————— gamma -BHC ( Lindane )76-44-8 ———————— Heotachlor309-OO-2 ———————— Aldrin1O24-57-3 —————— Heptachlor Epoxide959-98-8 ——————— Endosulian I „6O-57-1 ———————— Dieldrin72-55-9 ————————— 4, 4* -DDE72-2Q-8--- - — — Endrin_-,._p_. _ ._.. _._ ______ ,_„, .33213-65-9-- ——— Endosulfan II72-54-6 ————————— 4, 4 '-ODD ____ __ __ _ _1O31-O7-8- ——— — Endosul an Sul ate^ r* tf*i *•* A A f T T >*5Q-Z9-3 ———— ' —— - —— 4f 4 -DDT72-43-5-- — --- — Methoxychlor53494-7O-5 ————— Endrin Ketone51O3-71-9 —————— alpha-Chlordane51O3-74-2 —————— gamme-Chlordane ________ : ___8QO1-35-2 ——— —— 'Toxephene _ _ _ . _ . _12674-11-2 ————— Aroclor-lO16 _______111O4-28-2 ————— Aroclor-1221 __ 11141-16-5 ————— Aroclor-1232 __ _ __53469-21-9 ————— Aroclor-1242 ________________12672-29-6 ————— Aroclor-1248 _ _11O97-69-1 ———— -Aroclor-1254 __. . .11096-82-5 ————— Aroclor-1260 ______________

1O1O101O1O1O1O1O21762121< ^

21213SOWwJ^I

1002121212101OO1OO1OO1OO1OO210210

_ U __U

_ U __UUUU

_ U __U

UUUuuuu

_ u _ •uuuuuu

_ u _

BE300I32


ID EPA SAMPLE NO.PESTICIDE QRGANICS ANALYSIS DATA SHEET ________________

1 tt GPCBLANK I

Lab Names__________VERSAR, INC.__ Contract:_66-Ol-7471 I_____________I

I Code: VERSAR Case No.:13383 SAS No.: SDG Ho.:

Matrix: (aoil/water)SOIL Lab Sample ID: __GPCBLANK

Sample- wt/vols 3O (g/ml) G Lab File ID: ___


X Moistures not dec. O dec._______ Date Extracted:__12/29/89

Extraction: (SepF/Cont/Sonc) ___SONG Date Analyzed: __O1/26/9O

GPC Cleanups (Y/N)Y pHs___ Dilution Factors _ l.O

CONCENTRATION UNITSsGAS NO. COMPOUND (ug/L or ug/Kg)_UG/KG Q

319-e5-7 ——319-86-S ——

lllii_i_/ i_ii_i .*-1Q24-57-3 —333 3OO

60-57-1 ———72-55-9 ———72-2O-8 ———33213-65-9-72-54 -8 ———1O31-O7-S--

72-43-5 ———53494-7O-5-51O3-71-9—S1Q3-74-2--8O01-35-2—

11104-2S-2-11141-16-5-53469-21-9-12672-29-6-11097-69-1-11096-82-5-

- L _ ntrf*— — —-alpha-BBC———— beta-BHC _______ _____———— delta-BHC ___———— gamma-BHC (Lindane)———— Heptachlor ___ . __ ____ __———— Aldrin ___________ ________———— Heptachlor Epoxide _— —— Endosulf an I———— Dieldrin _______ _ _ _————— 4, 4 * -DDE ___ _ ____________— — —— Endrin— —— Endoaulf an II __ _———— 4, 4'-DDD———— Endosulfan Sul:fate _

———— Methoxychlor ___ _ . _———— Endrin Ketone ___ _______-----alpha-Chlordane———— gamma-Chlordane—————Toxaphene———— Aroclor-lO16———— Aroclor - 1 221 ___ _______———— Aroclor-1232————— Aroclor-1242 _____ _. ———— Aroclor-1248 ___ __. ———— Aroclor-1254 ___ __ .m ____- ———— Aroclor-126Q ___ . ________ ;_

8f\

a.oa.oa. o

» %./8n8.0

16161616161616ao16161 £

ISOAntabU

ao80aoao16O16O

uuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 1/67 Rev.

400012

Appendix D

Reviewed and CorrectedTentatively Identified Compounds

;.LriTXLC ORDAMTCS . ;-!i";LVo: S DATA SSKLE

I CAW50Man.* 5 VC^Sn^ IHC " Contvacbs GS-Ol--? ?!'" ! __ _, __ ; __ ,

Code: VERSAR Case No. s 13383 SAS Mo.: SDG Mo.: CftWSO

j ... A ; ; Ju± I..- w«. Uo f ) WM"! C>'< ;,.ab 3<-uviplvi I- j " "337-':

ulf wb/vol: " " "5.O (g/niL) I1L Lab File H) "= " JISS'-V.

.-- - 1 1 j*/,Tiu-iJ5 LCV; D^tu ReccJ-voiJ , 1 ,:/CO/ :C"

uac^uTs: .,ot dec. Date final/zisc' r . J

.bef TICs fwuftd s "0 <uy/L or uy/Kij)

CAS NUMBER I ^ COilPOUHD" >1flME V i "| RT ! '."lC-T. CGHC. ,!:

ftR300i35

i CAU51__ ______ __ _*b Names' VERSAR IWC --------- -•- Covi Irr^c t s Gt^-0i--7471 '

Codes VERSAR Case Ma. = 133S3" rshSTHo-s ' " SDG Mo.: CrtUSO

i«- (•.ioiI/waT.'iy-r)" " WAfE.1 "' . ' , '. - ,.. L^b Gum pis .rE". 'Ji 73;T" "

wb/vol!i . ' ~ ' ~ "- -S. 0 """Tcj/ftill) ""! il/' ! "..Lab ril

- -tiow/'-ned.) LOVJ .

urv/;; not Jec. :- " " " :"- - "- - " • At;.: .':. ;:,!,. *:i.:o -

PnCK " " ' v""r ™"""

^ AT i ON i;--n: T a „KH/ U(;/L"

> i ; . i: CnG N UMBER' ' "1 : COMPOUND " RA'flfe. ' " ' i'^RT " "l EST. COHC, : 3 ','\ : : = = = =:=: =•===.-:.=: 5= sirs.— — J = = ~:rs=: = = .— = =; — — insin: — — = =s_=: = ~=si:==-=:=:=i1 J s=sss = = === J =ss5ss::ssssss:s= = = s=s=ss | ss sssss: |

AR300I36

VDM-TU;

. . . .... ..i VEKSnr< INC . Cent-pacts &S-OJ. -747.1 '.

«;.* Cociiir: VERSAR Case Mo.; 133S3 SftS Wo. s ' SDG No. "s CAW50

s not dec. -i7

il^ ID

IC-j, foCtntJ s 0

1 . . .MU.'JCER ! CQI'iPOUHD NAME

uy/L or ug//,,,) "LC. 'I^

J

AR300I37

;;.!"" ':?f:-- .;c.

Jb Name: VERSAR INC "- ' " " " -"-' " Contract: &3~0i--7471 , ____ ___.

Lab Code: VERSAR Case No.:'13363 SAG No.: SDG No.: CAW50

: \3-o.il/water) (3OIL " " " ;^«b S^n.p3.tr 7!C: J ,-.. :-'i

wt/var:" "• "S. 0 " "-Tri/iiiL." "G " Lab rile II);: r<^7&r/

3d) L O W ' - - . . . . . . --_;"-.•

<p«fn::t/cA'p) PACK ". .. .__.._... "." " " Dilution i-'a

i i ;COMPOUND NAME' . I ... . RT 'i EST. CCMC- 1 C isrs: =2=: : =:=; — — = = — =rrt =r :===:=i. j ss=s=sss = = 2= =s j .KS :«ss5='sr.s:: =s.s-sr 35 ,?,•=; ~- j t-i: :.s BS -FL' :T. ]

. .1 1 i i

ftB300!38

i'von-fic - I/B? : ev.l •'-, •• .-^- u o Lr

•!•- . - . . . . . ; • :. „.- .:~". ..:: "••••??> 'i T):-:'L~;; U,?L-. T!TL^ uK.fi..Jij.cc .'..sriLvc c T.I"TH r.nir;.. S1 ' 1 * __.„1 _^_ " __ _Tc;"rrr.TXvcL'i ID:.:;-; ' " ~" ' : "'" ~ "~" ''~'"' _ ——..—.

J CAW34Lab MAIHIC-S VERSHR INC Con Ir Act: 6 Q '•• 0 .1 - 7 '< 7.1 i ______ _„„.

i_.ib Code: VERSAR"" Ca"se Mo.: 133S3 SAS Mo.: ! "SDG No. s CAW50

:! •-.,-' i ,» j -. o* t/wci wu'i .' liiJlL uuij iij it.:.' It? ! V' j '.' -vJ 'j.f

L-^ftiiiJ..; w-O/'vois 5. 0 Cg/mL) G Lab "File" IDs "-;;.i-i;.3

"-- <•--'->• - .

i.ui.ilx.?! TIC:j foui-u: 0"" (uy/L OT utj/!<t|. UO/i'L .. .

: i ' I . I . .. - i! CflS NUMBER "T "" COMPOUND Nfl!1L " {" " ' tff i" E2T. CORC. "T

-Ttc•*•*-* W v '

Iab Names VtRSAR 'INC'" " Cou trac ca "63- 01-7471

Codes VERSAR" """C&se -i-Jo/a" 133S"3 "~: SAS";-;o."s G0G Mo.:

is wt/vol: 5.0 -Cy/inL) G .. . . Lab File ID:;

j \.iow/med; . .LOW .. . Dale Recelvmj - i^/ao/^"

••!,.:..:::Ju;rc_ not ie.'C-i ~ ---CS "'' : "" " '• " - Pate' : na.!.;< ;.cd , :LJ/i2i/r^

' jJ.LHi.i- <Dt.ck/uap) PACK "J - - ;. liut-uO.! ."'aC ';.. _.. 0 --

_ _ . . .r TZCsi founds 0 - - - - U.g/L o i1 ug/K_. >

__ ... ._,__,- - .....^.-CAS" NUMBER J " ""CO^PQUNO WAME "~_~ T" " RT t 1ZST. COr-IC. ', C: :: : = = = =sr=j := =.=sj== j =assss.-=ss=ss = :ssss::a:i=ssssssss=:=cs==;s=sssss==::,-s;:= ( s: = = = 3SS:s=5= ] =::=r.iC=-:.K::=ss===sa :=:i3ss } E:: ss ss = -s; ..

.__ ________ ____] __. ___ . ______ . ________ ; ______ _____ I _________ I ________________ 1 _ ___ _ \

ABSOOUO

VOfi-T.TC - -, •1 "- ' •' ,7"O. O O O U i.

J _j 1 I i 1 * * 1 ' l"L 1 I " ' '*' *l f ' h •' 'l*"1 "• •***" - i • ' i • ••• > I»**L_-*«- i n n*- „, , _, . •i..*,' *.•-*.\_t.* • * j' \_j L,« j 4. A ..'

VCRSA'R IMC — Contract: S&--01--747V ;__;„__„,..__

i_AD Code: VERSftR Case !4o. : 13383 SAS Mo. : SDG No- : CAU50

^** HIM XL.- wfc/voli " --S.O v_i/,uL;: "G " :•"-• Lab J^ilo X D s " R3700 "'

-. = --*-•-' tiuw/med) LOW Date i':'i-''Cu..A :J : ' c-/lT\>.-'B'3

• w^ ^-srv:: r;•:*.; ••er, JEG Da tt-j An,\.; > ;.t-.d E "./I'Z.'E'v

-' ' ' I I - ^ T " - J"^ /^~ *-" * " . .M, • i I - F ————"

CONCEHTO-iTIGW u.i;iTStr " --ilutinjwr TICs found: 1"" (uo/L OT- uy/Au) .J::/Ku ~"

1 I i . ;! GAS MUNBER 1 "" COMPOUND NAME " !" ' RT i llS1."- CO>IC. :; L- . ..

I -1- 1UHKWOWM ! 3.08 ! L - 31 J

«:

.

CTti'>-.:.••• * • • • ' - ' ' ." '! "* P—— '--•-— ' • T- -' --- v'. - - '. . -

_---.-.-, j.-- ._...-_-,- . -rf. A * -.-,.. ,., r .„=..,,._,• Ui^/o1

Names VERSAR Tl-IU"" " " " ' f "-"-"""- """ ion^ac ts &T--01-747.L " 1 __I™1

Codes VERSAR C*se No. s 13363" "'SAS No. = SDG Ho. s

•ixt ( oj.;/w,; ev). saiu • .:... - ' :.""; :.j, ^ ..L ir,_ :•;„,

>ie wt/voi: .......I. , ..-I. .o-"' TtJ/mL) G "!"""" ""Lab r'ue'lDs K^7

• -~ - - < i c w /• iii e a 3" "" !_O W

ck, cup; PACK "' ' Diiu L...UI, /..luLo, . ,- j

..............umber "irCl.- founij": 1 <u^/L or ujj/K,,;) LJG/i-:C

.COiiROUNDMIE; iROUND^M/^IE _.. , .__ I _ Rf. ..i LSI... CQMC. .

- "

• • • • > - - --•-•

:. * xj o c

FIL£ ORGftNIQG .'iN.-tLYSKS frftTTT ^T.GiIT1

.~..j Hunt..-: VZR n'R 7NC" ' Cent cac 1. -. v.3 \>i- /^71 i ___________^Mk!

.aU Code: VERSAR Case Ho.: 133S3 SA'S" Mb. :" " "~" "~ "~SDG~~No.": CAUSO

:. » - . A r .^Oj-^/WriLor) SOIL . . Lab .Guti.p L D.":. OJ^r^fv" _^

.u.iHiJ.ti wL/volr . 5.0 <y/mL) G Lab File ID: R37V^

> LOW

l; dec. IL7

PfTCK

c; o H c L: M T F? A T i o i-i u : •: i T 3 <uy/L or ug/Kg. ":JC/:\Q

CnS

i.

!.-iUM.BL::': " -T " "" "COHPLJUND NAME

1 UNKNOWN1

1 RT

2. 3

] 1

i '"' llST.~"CdMC- T"

a l'~ 3.S! «j !

uKTATllVZV: ^DUNTircrS" COMPOUNDS '

Lab Name: VERSAR THC"- ~ ' ' ConUvac't, Cii-

ab Code: VERS'RR'~ ' Castr^o.V f 33&3 . "IsAS Tio.' =

.''al-rixs i:^bil/wab^f:y""saiL ::": . " '" .. _^;_,

I* wt/vol: -"5,0. "lg7»L)"""o " 7~ ^~~ Lab File ID,

~ -• -£ioto/nied> LQUl.._. ..... ..... . D_:I ,__..

<pack/cap> PACK . . . . - Dilute.-. T

. lumbt*-. TICs found: 0 "' - • <ug/L or -.tj/Kij:- L.li/*-;i

; : ' ' _ . . . ] . i :: ens NUMBER : COMPOUND ..NAME._..;_ i 'L -,. ' ' - CLI'MC. ; c; .] 2B=ss==s = a=.=rs=sjsss=-s3KSsi=-}' -l:-i== = =^ = r=- . ========K :=r:ssr==::=='==.- 2:Si==.=r. j ==ss:=:=s »as= | =:. Lr-.;:::.; 55 ssprs-. 5=sr.-:j= j :=..:--:=sss j

i _______.._______.1 __________________________.] _______ ! ____________ i _____ i

683001

F"OSJ'! "I VDi" • TIC -,- - r.x w . <• XT.; Rev.* ' ; •i. U o .1. J-

i£ • •"• " -" - LPfi 03FIPLE HO.VOLATILE aKtirU-ilCU A.-IftLYCilS EATft EKETT* * " ' - — — - - • - • - ~ ' _

Laiy Manuss VERSAR INC Contract: Sa-Ql-7471 J_________,

««b Code: VERSAR Case No.: 13333 SAB Mo.: SDG No. : CAW30

•:*-UTI*= (soil/water) SOIL Lab Sample" ID: 93395A

:,,u:ipj.t w.t/vol: 5.0 vy/niL. G Lab rile IDs

Level: (lo^/ined) LOW Date Received -

"f- ^r^Eture: not dec. 3E Date Anal/zee!: 1&/2S7Q9

Col Limri < pack/cap) PACK D i 1 u Lion F a c U or j 1 * b ';:&?&-

CONCEWTRATIOH UNITS:" "" fVlumber TICs found: O (ug/L or urj/Ky) UG/KG ".f:;

] i l l !1 CAS NUMBER I COMPOUND NAME I RT 1 ESI- CONC. I Q i

i________________I__________ I I ' - I !

FORM 1 VOA--TIC . • "-. l/G? Re( "\ ....— 'i ^y* u u j. o

-' • . . .- . LTn SfKPLC MC.VOLATILE ORGA!.;iU& hALY21'S | DAT.A

"

• •• - Co-n fcTac L s & ti ••-•.} 1--7 47.1, i __ ____

b Codes VERSAR Case No. .» 13363 ., 'SAS Ho. : SDG Ho. M CAWKO

Matrix^ -v^ol I/water) "SOIL ' -" L^b Sample .21). 333?Cf, '

Sample wt/vols " -5.0 ','tj/mL> CT ' -------- ^,.

LOW " '. n^L--

" : n o t dec. ^ 1 - - - - - - - •»«.!•&-Analysed.

Coiunm (pack/cap) PACK " " ' ' D il u L .u, n r',; c b o

....._._.. ..._ .._, _. CONCENTRATION U.LC^- found: 1 "" ' "" <uy/L or

1 . - .... ...-CrtS NUMBER"""! COMPOUND NAM£ ~

1. 1169-93-1 -TT!^ISILaXSHEr;'T,Y."3.3,i5,5-HEX

.

27. a?

! 1ESr. COI-iC. i G :

2. 71 J 11 1

AR300U6

I VOA-TIC 1/ii?JL. o

.:•<>'

1 L _ - - - - _ _ - " " " "

VULi'tTILL CRuHrl ICL: I'.HfiLVSZS BiTT," "rriHTCTT . :". . ' ~"~~t.r ' '" _ JT_ __ ._„.».'£.%i;-iTXViILY '*. JLHTm^iJ C^T'CU^DXi ; . . " . . ._; " .^. „;. :

i r. ''iW&HLiAL* elates y£RSP.R IHC _ Contracts S8--01-74"71 j/ . . .Lab Codes UERSAR Case No. ; 133S3 SAS No.: SDG. >4o^ s CAU50

:*!*Lii:«= <-».oi:/ivaior> SOIL Lab "^ampici 1!i">u 9j377fi

;;.Aniple wt/voi „• IS. 0 " Cjj/n.L) G " Lttb F7ile ID.-: R3SJ.O

WUJ.UIRH <pacK/cap> PACK Dilation !•' actoi j -- o

TIGM UNI'.Ss " " ~" " "Humbcv TICs fount!: O .ut|TL OT ui'g/Ky) ' "JG/KG

: ; ; ; .! CAS NUMBER I COMPOUND NAME ... I RT ! EGT. CONC. \ Q

ftR300ll»7

FOR]'! 1 VOA-TIC ! / - --' -. ' 1/07 T?ev

B IF Epp) SAMPLE NO.SEMIVOLATILE ORGANlECS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS ] ~" ~ J.......... I CAU50 I

Lab Name: VERSAR INC Contract: 68-01-7471 !_____________]

b Code: VERSAR" Case No.: 13383 -SAS No.: SDG No.: CAU50

Matrix: (soil/water) WATER - Lab SajRple IDs g33ga

Sample wt/vols 1000 <g/mL> ML Lab File IDs T1368

Level: <low/roed. LOU ' " " ' '" ^ ' J)ate Received5 ia/20/89

% Moisture: not dec. • ''~~ dec. Date Extracted: 12/HS/89

Extraction: CSepF/Cont/Sonc) SEPF Date Analyzed: 01/24/90

GPC Cleanup: CY/N) N ———- - pH_ Dilution Factor: 1.0

__ . ., , . ._, CONCENTRATION UNITS:Number TICs fouriffV f "~ "". -- <ug/L or ug/Kg) UG/L

CAS NUMBER

1.. . ....... ..-~

!1 COMPOUND NAME

IDIOCTYL ADIPATE ISOMER,.I ..- ......... ., .. - -• - — -*--

. .. 1 I1 RT 1

1 30.51 1,- - 1 1

1EST. CONC. 1 Q

DC 1 J

!

FORM I SV-TIC

IF •: : - - .-:• £Pfl SAMPLE NU.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET " _______________

TENTATIVELY IDENTIFIED COMPOUNDS _ If CAW52

Name: VERSAR INC______________ Contract: 66-01-7471 I _

i_ab Coae: vERSAR Case" No. : 13383 SAS No. : ______ SDG No. : CAW50

: (soil/water) SQXw Lab Sample ID: 93376____

Sarnplfj wt/vol: 30. 1 <g/mL) g___ _ . Lab File ID: V44S9.

.low/med) LOW _ Date Received: l£/£0/e9

* Moisture: not dec. 17 dec. ___ Date Extracted: l£/£3/&9

Extraction: CSepF/Cont/Sonc) SDNC Date Analyzed: 01/£4/90

GPC Cleanup: (Y/N) Y__ oH: 6.3 _ Dilution Fact or s_ l. 053

CONCENTRATION UNITS:TICs four.d: __£0 iug"/l_ or ug/Kg. UG/KG

t 1I CAS NUMBER 1

t 1 ttvli/Mm.iK

——— 5, —————————————— ] UNKNOWN'i,,' /i. ————————— i UNKNOWN1 5. [UNKNOWN

1 1COMPOUND NAME 1 RT 1 EST. CONC.

HEXEN-1-DL ———————————— I ——— 5. *5- I ——————— 4C!O... ..,-- -, 1 S.'SS 1 - 16120-

1 7. 57I 8.79

1 6. 1UNK. ORGANIC ACID 1 £3.641 7. i UNKNOWN! S. [UNKNOWNI 9. [UNKNOWNi Id. [UNKNOWNi l l . i UNKNOWN1 li. . ,.i UNKNOWN1 13. -[UNKNOWN1 14. [UNKNOWNt IS. 1 UNKNOWN) IS. [UNKNOWN[ 17. 1 UNKNOWNI 18. 1 UNKNOWN1 13. i UNKNOWN

1 £3. 841 31.741 3£. 561 3£. S£1 33. 1 1! 33. 791 34.011 35. 66

HYDROCARBON 1 36. 45! 37.091 39. £6

HYDROCARBON f 40. 361 40. 76

——————— 33CUZI£900S50£504£064

- 13001400££0059034013004£0340590340

1 £0. i SUBSTITUTED NAPHTHALENE i 4U ££ 1 " 5101 l 1 1

1 t1 Q 1

- t-SJ ——— \

1 J1 J1 J1 J1 J1 J1 J1 J1 J[ J1 J1 J 11 J 11 J 11 Ji J

_ t _____

FORM I SV-TIC

IF" EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANTALYSIS' DATA SHEET ________________

TENTATIVELY IDENTIFIED COMPOUNDS l_ I CAW53

3 Name: vERSAR I' C ".' " ContTract:"^6-01-7471 1_,____________

Lao Code; vglxSAR Case No. : i3363 "SAS No. : SDG No. : CAW50

Matrix: (soil/water) SOIL ...... .. _._..._ - ....Lad Sample ID: 93377

Sample wt/vol: 30.0 .g/rnL) G___ _Lab File ID: T137£

L_evei: Ciow/mea) LOW ^ .__'. _'.' Date Received: l£/£0/89

% Moisture: not dec. 3_1._.._._ dec. ___ Date Extracted: l£/£9/89

Extraction: .SepF/Cont/Sonc) SDNC .Da_te Analysed: i3l/£4/90

GPC Cieanub: (Y/N) Y" /...""_... JpH: __ 6/9 Dilution Factor: 1.053

CONCENTRATION UNITS:Number TICs found : "__lj&""._".!'.""" _/JL"'". " '".''."._J"".!i"—=--"lIlU"ija/L"" ar ug/Kg > UG/KJ3

CAS NUMBER

1. £0019-64-1 .

i -" :"."._;.=i":~I J-r,.. 4.5. 57—10-35.7.a.9.10.

11.

1£. - - - -- - - - - - -

13. - —14.15.16.

COMPOUND NAME~~ ~~ — ~"

£<5H)"-FURANONE, 5, 5-D I METHYLUNKNOWN"UNKNOWNUNK. POLYCYCLIC AROMATICHEXADECANOIC ACIDUNK. POLYCYCLIC AROMATICUNKNOWNUNK. POLYCYCLIC AROMATICUNKNOWNUNKNOWNUNKNOWNUNKNOWNUNKNOWNUNKNOWNUNKNOWNUNKNOWN

i 11 RT 11 ~S£ ————— ___ f —

1 7.77 l1 6. 70 11 9. 97 11 £4. 97 11 £5. 19 11 24. £4 11 £5. 9£ 1i £9. 06 11 30. 7£ 11 31.07 I1 31.36 if 33. ££ 11 33. 69 11 34.61 11 40. £1 I1 4£. 13 i1 1

EST. CONC.

££00£3001100

18001500

3101£00

9£01100l£i3010003£016001£001900£300

Q

JJJJJJJJJJJJJJ.JJ

48300150

N-J

U"

FORP1 I SV-TIC l/»7 Rev,

IF EPA SAMPLE NO.SEMIVOLATILE ORGAN tCS ANALYSIS DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS ' . ' - i II CAW54

Nam^s VER5AR INQ ____ : _________ Contract ; 66-01-7471 I

Lab Code: ^/ERSAR Came_No. : 133S3 _ SAS NO. ; STJG~~No. : CAWSgi

Matrix : («oi I/water) SOIL uao Sample ID: 93378 ___

Sample wt/vol: 30. H <g/roL> G.__ ~ TTab'TiTe ID:. V4430

L_ev@l: .low/med) LOW _ Date Received: l£/£0/89

"A Moisture: not aec. 19 dec. ____ . _._Date E_xtracte0: i£/£9/89

Extraction: ^SepF/Cont/Sonc) SDNC .. _ ... D_ate Analyzed: 01/84/90

GPC Cleanup: <Y/N) Y__ pH: 7. a .Dilution Factor: 1.053

CONCENTRATION UNITS:[Mumper i ICs f ouno: £6 <ug/L or ua/Kg) UG/KG

c

ii1111lttt1111ilil[J1111

CftS NUMBER

1 — •

_"_j.6.7.8.9.10.

11. £43— 4£— 5l£.13.14.IS.16. 84-15-117. S£-05-316.19.£0. 8£-d5-3£1.££.£3.£4.£5.£6.

1 1i COMPOUND NAME 1

— iG CVCLDI1CXCN 1 OL ———— ; ——————— *— j UNKNOWN —————————————————————— [— ia-CVCLDHEXEN-1-ONC —————— ——-4—— 1 UNKNOWN ——— ———— ——————————————— j—— i UNKNOWN —————————————————————— I

i UNKNOWNiUNK. POLYCYCLIC AROMATIC1 UNKNOWNiUNK. ORGANIC ACIDIS. 10-PHENANTHR£NEDIONt£i BENZO CEO NAPHTHO C£, 3-D 3 FURANlONK. POLYCYCLIC AROMATICIUNK. POLYCYCLIC AROMATICIUNK. POLYCYCLIC AROMATICIUNK. POLYCYCLIC AROMATIC11,1' s£', 1' '-TERPHENYL1 7H-BENZ CDE3 ANTHRACEN-7-ONEIUNK. POLYCYCLIC AROMATICi UNK. POLYCYCLIC AROMATICi 7H-BENZ CDE3 A.NTHRACEN-7-ONEIUNK. POLYCYCLIC AROMATICtUNK. PQLYCYCLIC AROMATIC1 UNKNOWNIUNK. POLYCYCLIC AROMATICIUNK. POLYCYCLIC AROMATICIUNK. POLYCYCLIC AROMATIC1

1RT \

W. -TW >

GJ. 1-Jk. 1

ff y. I"* i

——— a; G5 — Hr • o t i8.79 1

£3. 4£ t£3. 54 I£3. 65 1

" £4. 35 i£6.71 1£7.09 1£7. 4£ 1£7. 6£ 1£7. 74 1£6.81 1£9. 06 1£9.41 1£9.51 1£9.71 i31.37 131.49 131.81 )33.71 134. 3£ 134.81 1

1

EST. CONC.

-A"l

——————— HjflB ————— : —— r—— —— Sfl gl ———

C9O1 SOtl£4006007708606i3043d430

1 1003405203406906006005£07705£05£0190061003500

1i Q

ffef ——E_T

IBJ -IDJ1 Ji Ji J1 Ji JJ

1 JJ

1 J1 J.1 JIJ1 J1 J1 J1 J[J1 Ji J1 JIJ1

11

13JT

J 0

T1 -Iu/1 31 3"1 JIZJ1 /Jl/Jlal"i/Jlai~3jjo

FORM I SV-TIL

IF tPft SAMPLH NO."SEMIVOLATILE" QRGANICS ANALYSis~DATA SHEET ____ __ ___'_

TENTATIVELY IDENTIFIED COMPOUNDS " I ~ "" |1 CAW55 1

Name: VERSAR INC_____________ Qontract: 66-01 "7473. I______________ I

i-ab Code: vERSAR „,Case No...: 13563" ;SAS No.: ______ SDG No.: CAW50

Matrix: (soil/water) ^ni> - -

Sample wt/vol: JM^ ., <g/rr.L> G___ " " Lab File ID: V44££

Level; Uow/inea) .-Oul .... . ........ ... . . .... Date Received: l£/£0/89

% Moisture: not dec. __£3 ...: aed. ____ "7 Date Extracted : l£/£9/69

Extraction: - (S¥pF/Cont/Soncr SONG; " . Date Analyzed : 01/£4/90

GPC Cleanup: - -(Y/N>~^_ . ;;___pHs 6. 9 „„ /Dilution Factor: 1.053

. ..CONCENTRATION UNITS:Numoer TICs rounds __7 ._ .. ....... (ug/L or ug/Kg) UG/KG

1i CAS

l 3^ ——1 ,£, ——»-3.

- 4.I 5.l 6.1 7.1

iNUMBER 1 COMPOUND NAME

——————————— i UNKNOWN ———————— ; ———— — ——————————— — —— 1 UNKNOWN —— - ———— — —— • — —— ; ———

_ ""("UNKNOWN"1 UNKNOWN[UNKNOWN1 UNKNOWN HYDROCARBONiUNKNOW'N HYDROCARBON)

! . .....1 RT't .. __..o« oc;

———— t —— •••.— • "? ——— F*J-f... . 1

1 S. 79_- 1 3£. 6£... 1 33. 1 1

l__ 33.791 36. 441

EST. CONC.

.oii———————— l-S0tfi —

1500450640640540

Q_=

BJIBJ •JJJJJ

TTJ7TJ

FORM I' SV-TIC

IF = EPA "SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______

TENTATIVELY IDENTIFIED COMPOUNDS 1I CAW5&

t D Name: VERSAR INC " Contract: 68-01-7471 1

Lao Code: VERSAR _ Case No. : 13383 SAS No. : ______ SDG No. : CAW50

matrix: (soil/water) SOIL Lab Sample IDs 93380____

Sample wt/vol: 30. 1 (g/rnL) G___ Lab_File IDs V44£7

uevsls <low/med) wOW Date Received! l£/£0/89

% Moisture: not dec. £5 dec. ___ Date Extracted: l£/£9/89

Extraction: <SepF/Cont/Sonc) SQNC Date Analyzed: 01/£4/9gi

GPC Cleanuo: (Y/N) Y__ pH: 6. 9 Dilution Fact'or: 1. ft S3

CONCENTRATION UNITS:TICs found: 14 < ug/L or uo/Ko > UG/XG

lCAS NUMBER

-H — oiIiG:— 67-5 —•eS ————————————

r — =K — 93&-6S-7 —Vw.. •**? ——————————

6.7.8.9.1®.1 1.l£.13.14.

11 ..._. COMPOUND NAME -

—— 1 UNKNOWN ———————————————————————— 1-2 CYCLOICXCN 1 ONE ———————————— 1 UNKNOWN ———————————————————————— 1 UNKNOWN ———————————————————————

1 UNKNOWNIUNK. ORGANIC ACIDl UNKNOWNi UNKNOWN HYDROCARBON! UNKNOWN! UNKNOWNI UNKNOWN1 UNKNOWN HYDROCARBONI UNKNOWN HYDROCARBONI

RT

- , --.-,. AwD. -i»#

1 ——— 61 48 •D. Di_r. *-i f8.79£3. 6431. 0£31.743£."6633. 1 i33. 7736.4640. 3£

EST. CONC.

1 ——————— 378 —i ————— nac1 ———————— £80

752*

3500560370370l£00

1300£600£700930

i1 Q

n T1 D*J

-4-BJ ——— I

1BJ11 JIJ1 J1 J1 J1 J[ J1 J1 J1

FORM 1 SV-TIC - — - . 1/87 Rev.

IF EPfl SflPJPLE NO.SEMIVOLATILE ORGAN 1CS ANAl-YSlS DATA SHEET ______________.

TENTATIVELY IDENTIFIED COMPOUNDS i— - —----- - - - - - - - - - - - - j CAW57

3 Name: VERSrtR INC_______________ Contract.: 68-01-7471 f

Lab Code: vERSAR "~~gase"'fijbri "13383 T ~"SAS No. : ______ SDG No.: CAW50

Matrix: (soil/water) SOIL ^, - _ - , . . - - , . . . ....-.-- . ..J_ab Sample ID: 93351____

Sample wt/v'oi: " 30. 0 Cn/r/iL) S__' Lab File ID: V44£3

Level: (low/mea) LOW _ _. . . __ , ,. ,;. .. -Date Received: l£/£0/89

% Moisture: not dec. 38 „ .dec. ___. _ Date Extracted: l£/£9/89

Extraction: (SepF/Cont/Sonc) 5QNC Date Analysed: 0l/£4/90

GPC Cleanup: CY/N) Y" . 77" pH: ~ 2=A ~ Di lution Factor: 1.053

CONCENTRATION UNITS:Number i ICs found: £6 ". ~ ".: - ." ' ; (ug/L or ug/Kg) UG/KG

11 CftS NUMBER

»• 5. ———————————_ 4 . - - - - - - - - -

1 5.1 6. £09l-£9-4t 7. -—..-.1 S.1 9.1 10.1 1 1 . - ----- -

1 l£« : . . . - - ------

[13. ~" — --"1 14.1 15.1 16.t 17.t 16. "1 19. "" ""•" ; ""I 20.( 21.1 ££.t 23.1 £4.1 £5.t 26.1

1 .. , , 1r COMPOUND NAME' i RTi UNKNOWN —————————————— : ——————— t ——— fe.3£ "ll UNKNOWN '" "" "'"" " ""' . ": ——— '• ——— H ——— G. G7 1i UNKNOWN —————————————————————— 1 ——— 7. 57 1(UNKNOWN _ S. 801 UNK. ORGAN 1C AC I D £3. 6719-HEXADECENOIC ACID £5.96J UNKNOWN 30.94[UNKNOWN " ~ 31.27i UNKNOWN 31. 54(UNKNOWN 31.94i UNKNOWN 32. 07[UNKNOWN 32, £1TDNKNOWN " r . . . . - . . - - - - - - 3£^ 4g1 UNKNOWN . 1 3 £ . 8 9i UNKNOWN ~'= 33* 1 6rONKNOWN" "" " " " 33.31('UNKNOWN HYDROCARBON 33.77iURKNOWN 34. 02TDNKROWN - r ' -" r 34. 171 UNKNOWN " ~" 34. 311 UNKNOWN j 34.47[UNKNOWN " 35. 19[UNKNOWN " .----•----• •- - - - - - - - - | - 25^ 3£1 UNKNOWN HYDROCARBON 1 36.51(UNKNOWN 1 37. 19(UNKNOWN 1 38.71( i

EST. CDNC.

— —— — —— 1900

' - --ctn*r* tm4000

3100338091014001000

11001000910__£7001900£700££005900330034003600£3003100

£6006500£6003400

11 Q I

1 !IDJ 1

H-B F — 11 J Ii J 11 J »1 J1 J[ J1 J1 JUJ J] J1 Ji JIJ1 J1 J1 J1 J] Ji J1 J! J1 J1

T

FORM 1 5V-TIC

IF - • -••• - -- ££A "SAMPLE MO.SEf*JlvOi_ATILE ORGANICS ANALYSIS DATA SHEET ' " —— '"" '_ ________ ~ ___ _._

TENTATIVELY IDENTIFIED COMPOUNDS -- - ii CAW

1 5 Name: VERSAR INC _______________ Contract : 66-0 1-7471 i

Lab Code: vERSAR Case No. : 13383 SAS No. : • — - -.. — -_gD£ NCu .

Matrix: (soil/water) SOIL Lab Sample ID: 933B£"

Sample wt/voli 30. £ (g/rnL) G__ Lab File ID: V44S5

Level E C low/med) U.Q.W__ Date Received: l

% Moistures not dec. &7 dec. ___ Date Extracted: J.2/S9/69.

Extraction: <SepF/Cont/Sonc) SQNC Date Analyzed: 0l/£4/90

GPC Cleanup: <Y/N> Y__ pH: 6.9 Dilution_Factor: 1.053

CONCENTRATION UNITS:Number TICs found: 17 (ug/L or ug/Kg> UG/KG ;

1 11 CAS NUMBER 1

i — i . aan-67-3 —— i-1 W. ]

i-.— 5i ———————— i-\..",* f. ,1 5. 116. ~ \1 7. 746S5-36-£ I] 6. 1i 9. i1 10. [

1 1 1 . 1l l£. - - - - -1I 13. i1 14. 11 15. 11 16. -11 17, (1 1

COMPOUND NAME

•P— CYCLrQHgyB^h"-t--^t ————————————— 1UNKNOWN ———————————————————————UNKNOWN ———————————————————————UNKNOWN ———————————————————————UNKNOWNUNKNOWNOXACYCLOTETRADECANE-£, 11-DIOUNK. ORGANIC ACIDUNKNOWNUNKNOWNUNKNOWNUNKNOWN ALDEHYDE ~~ :.._:UNKNOWNUNKNOWNUNKNOWN HYDROCARBONUNKNOWNUNKNOWN HYDROCARBON

1RT 1 EST. CORC;

i —— s. 47 i ———— - eoci1 ——— 6. 3£ "i ——————— 11001 ——— G. 07 — 1 — — ——— ' — 07B- - , , * _ _ , .. -. , i. ,-1

8. 57 l £906. 80 t 3400

•£2.--54 l" "'" ~ 330:£3". 65 l .: : l£0W£5. 92 1 : " ' 67031". 74 ) 5703£. 6£ f" 1£0»

I. ..33. 12 i £1V»3i 33. 7S i 3000l 35. 66 l "" ~ 6701 36.46 1 £6001 39. £6 1 4801 40. 36 1 860t 1

li " Q

tBJ----—— t-fej ——IDJIDJi Ji JVJ1 Ji Ji J1 Ji Ji Ji Ji Jl Ji JI

ii

i1<iiiiliIiiiil11

T

i "

.\ ..ii';, ...o .FORM I 3V-TIC : — . -l/a7 Rev.

SEM I VDLflT !,_£_: ORSfiNICS fiNflLYSIS ' DflTR- SHEET ' ^ 3flr1PLE N°'VtNTSTTVti-Y "IDENTIFIED COMPOUNDS' '' ' i ~ ————————————

Name •• 'EESRR..INC - . . con . ract : 58-01-7471 I _ _ _ _ _ _ _ _ .

Lab Code: .ERSflR . * No. 13383 SflS No: ______ SDG No.: CftW50

Matrix: (soil/H.ter) SOU.__, ,;,, , . , i ,_ ;= •__;; LaD : Sample ID: 93385

Sample wt/vol: .. .. 30. 1 <jg/rnL) S__ Lad File ID: V44£6

Level: (low/med) UOU .;;..,. , . . . . ...Date Received: l£/£0/d9

* Moisture: not dec. .39 - , dec. _______ . ..Date Extracted: i£/£3/89

Extraction: (SepF/Cont/Sonc) SQNC . .Date Analyzed: 0l/

SPC Cleanup: (Y/N) Y__ . PH: 6.9 Dilution Factor: 1.053

CONCENTRATION UNITS:TICs found: "££"". ;.;." :.."V ..-'".: .._ -iTug/L^oi^ .. ig"/Kg) UG/KU

1f CAS NUMBER

i a, -- - - -- ——L*TV TS ———— _ _______________r 'L./4.

D»6; £091-89-47.6.9.10. 57-11-411. ~12.13.14.IS. £490-43-416.17.IS.19.£0.21.c!c?.£3.£4.£5.£6. "" ^ ""

11 COMPOUND NAME

1 UNKNOWN ————— ——— — ————————1 UNKNOWN ————— - — - ————— ; ——————I UNKNOWN —— : ——— — — .. —— ——[UNKNOWN '1 UNKNOWN1 9-H"&ADt_TC--_NO I C AC I D 'IUNK". ORGANIC ACID ._., ~. . "IUNK. ORGANIC ACIDi UNK. oRGAN ic ACIDIOCTAD£CANOIC ACID(UNKNOWN" HYDROCARBON(UNKNOWN HYDROCARBnN , __["UNKNOWN1 UNKNOWN . . . . . . . .T£-METHYL-I-HEXADE"CANOLI UNKNOWN[UNKNOWN ALDEHYDE . .. . .1 UNKNOWN1 UNKNOWN[UNKNOWN HYDROCARBON( UNKNOWN[UNKNOWN1 UNKNOWN ALDEHYDE : , . .1 UNKNOWN[UNKNOWN . . . . . .i UNKNOWN "1

1 11 RT

=SS ) ==S=SE31==±=S

1 L>. -->i_ I—— \ ——— 6. G7 1-,,. _— 1 ______ "7— = "7 .. 1_. j A'.— C! f

_..._..( . .S. 57.."i. . a. 79

i . £3. 44......I £3. 54

_..(_. £3. 651 £5. 961 £6. 14

. f. £7. 74.. .( --£9. 87. l _ 30. 5£

1 31.01J 31.74l . 3£. SIi 33. 1 11 33. 791 35. 66J 36.44t ..37.121 .37. S71 39. £71 40.07

-i 40.791 41. £6i

EST. CONC.

————— t -ena ——————— sea ————————— 4 H&« ——

57049003005701S00

69069069059057069013001100

£5004500570££00690300570300S£0320- _

lJ Q

-ttEtf--t-BJ--J-B6-

l Jt Jl Ji JIJ>Ji Ji JUi Ji J

•l Jl J1"J1 JU1 J1 J1 JI J1 J1 j1 JJ ___

l1

i1f1Ii»1ii!i1i1i*!11i\\

__

FORM I SV-TfC

ii7 - , . Es-'A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET " ________:__.____

TENTATIVELY IDENTIFIED COMPOUNDS ; . i - -.«. ~- . ' CAW60( '3 Name: VERSAR XNC "__________ Contract: 66-01-7471 i________

Lab Code: VERSAR Case NO.: 1338.3 SAS No.: ______ SDG No.: CAW50

Matrix: (soil/water) SQI.L Lab Sample ID: 93384____

Sample wt/vol: __30.0 (g/rnL) G___ Lab File IDs V44£4

Level: <low/r.iea> LOW Date Received: l£/£0/89

% Moisture: not dec. 3g dec. ___ _. Date Extracted; l£/I=:9/a9

Extraction: (SepF/Cont/Sonc) SQNC Date Analysed: 01/S4/90

GPC Cleanup: (Y/N) Y__ pH: 6. 9 Dilution Factor: l,0

CONCENTRATION UNITS:TICs found: IS _ (un/L or ug/Kn/ y

CAS

lr— €.

k~-3i ——W *r. ——

5. *6.7.6.9.10.1 1.12.13.14.15.16.

1 i 1NUMBER 1 COMPOUND NAME ) RT 1 EST. CONC.

idC! -G7 3 ——— 1C CYCLDMCXEN--1 Ob —————————— i —— • 5. 45 1 ———————— 'lift——————————— . UNKNOWN —————————————————————— i ——— 0,30 1 ————————— 7C.3——————————— j UNKNOWN ———————————————— : —————— t ——— 6. 6S 1 ———————— 730

l urJi\rJUWi4 1 i . vJ / i L--W-.'t UNKNOWN 1 8. 79 4500IUNK. ORGANIC ACID 1 £3.64 ' 7£0[UNKNOWN 1 £5.96 l 310[UNKNOWN 1 3£."09 310[UNKNOWN 1 35.51 330[UNKNOWN 1 3£. 6£ S.S0(UNKNOWN ALDEHYDE ' " — 1 33.11 3£0"01 UNKNOWN 1 33. 79 : 4700[UNKNOWN 1 35.64 5£01UNKNOWN HYDROCARBON 1 36.47 14001 UNKNOWN | 40.77 5£8I UNKNOWN 1 41. £4 i 6£01 t 1

li Q

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FORM I SV-TIC . 1/87 Rev,

ii- """" ' " o'A SAMPLE NO.ORGANICS ANALYSIS iSATO"""SHEET ____.__________

TENTATIVELY IDENTIFIED.COMPOUNDS .. . . - - . - j CAW61

;• 3 Name: VERSAR INC_____________.Contract: 66-01-7471 t______________

Lab Code: VERSAR Case No.:, j .3.3.8 3- , SAS No. : __ SDG No.:

matrix: (soil/water) SOIL , ... , , Lab Sample ID: 93385

Sample wt/vol: 30. 1 <o/rnD _G Lab File ID: V44£S

Level: ' (low/med) LOW .. ... ._ ... ._,, .... -Date Received: l£/£'0/89

% Moisture: not dec. 41 dec. ___ Date Extracted: 12/29/69

Extraction: CSepF/Cont/Sonc) SONC .Date Analyzed: 01/£4/9O

GPC Cleanup: (Y/N) Y pH: 6. 9 Dilution Factor: 1.053

CONCENTRATION UNITS:Numoer TICs found: 25 (ug/L or ug/Kg) UG/KG

11 CAS NUMBERj — . .. ..__

i - 1-, oca- G7 3 ——. S. 93O-66-7 ———

™- ^i.i -j»l 6.1 7.I S. £09l-£9-4! 9.1 10.

l 11.l 1£. 57-11-4l 13.1 14.1 15.1 16.i 17.1 IS.119.1 £0.[ £1.1 £2.1 £3.1 £4.1 £5.1

11 COMPOUND NAME 1

IE CYCLQHrXETN • 1 - (~H1 UNKNOWN ——————————————————————— 1I£-CYCLOHEVEN 1 ONEI UNKNOWN ———— — —— : —— _ ..1. . . _. ._...__..._ 1[UNKNOWN —— — ——— : —————————————— i1 UNKNOWN1 UNKNOWN[ 9-HEXA0ECENO I C AC I DIUNK- ORGANIC ACIDIUNK. ORGANIC ACID1 UNKNOWN(OCTHDECANOIC ACID1 UNKNOWN1 UNKNOWN __. _ .__ .../UNKNOWN ALDEHYDE .1 UNKNOWNf UNKNOWN(UNKNOWN HYDROCARBON1 UNKNOWN1 UNKNOWN[UNKNOWN ALDEHYDE . - • - - . . . "1 UNKNOWN[UNKNOWN HYDROCARBON1 UNKNOWN1 UNKNOWNi

RT 1

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-• •* "" ww.__. / '.' D /• '•8.558.79£3. 4££3. 52£3.64£5.94£6. 1431. 7£3£. 61

_33. 0933. 7735.6436. 4437. 1137. 8639. £440. 0640. 3240. 7€»41. £4

EST. CONC.

= tiT'f.T,

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3U0172FORM I SV-TIC 1/87 Rev.

IF | - -~ ... .EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ' ——- ;______________._

TENTATIVELY IDENTIFIED COMPOUNDS - i ..l CAW&£

I . Name: VERSAR INC ___________ Contract: £5-01-7471 i __________.

Lab Code: VERSAR Case No. : 13383_. SAS No. : ______ SDG No. : CAW50 ..._

Matrixs <soil/water) SUIu Lad Sample ID: 33386_____

Sample wt/vol: 50.0 (g/rnL) G___ Lab File ID: V44£ 1

Level: (low/med) L.DW Date Received: i£/j£ia/59

% Moisture: not dec. £3 dec. ___ Date Extracted: l£/£3/69

Extraction: (SepF/Cont/Sonc) SONG Date Analysed: 0l/£4/9@

GPC Cleanup: (Y/N) Y__ pH: 6. 9 Dilution Factor: 1.053

CONCENTRATION UNITS:Number TICs founds _5 <ug/L or ug/Kg) UG/KG

CAS

4-- —

T-* 3.

5.

1NUMBER J COMPOUND NAME

——————————— 1 UNKNOWN —————————————————————— i—————————— 1 UNKNOWN ——————————————————————

1 UNKNOWN1 UNKNOWN1 UNKNOWN HYDROCARBON1

RT

&. 30I ——— 7,55-

8.7733. 7635. 4£

EST. CONC.

I ———————— &4#—

l&Cifc460360

1 I1 Q 1

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l T

300259FORM I SV-TIC 1/87 Rev,

Appendix E

DPO Report

RegionORGANIC REGIONAL DATA ASSESSMENT

CASE NO. J 33.S3____________ SITELABORATORY _VfrS OJT

" - " . " ' "-" "-"---'

sow* t ./ S7

DPO: ACTION ' FYT

NO. OF-SAMPLES/ 1 w'-lkT -MATRIX '..... 11 5oi [ _REVIEWER (IF 'NOT ESD Si 1~M ft ILLREVIEWERS NAME^"-^n C-Urp^irfVcr, ' "

COMPLETION DATE 3/ 2 fe|? 0

DATA ASSESSMENT SUMMARY • - * , -

1. HOLDING TIMES

2. GC/MS TUNE/INSTR. PERFORM.

3. CALIBRATIONS

4. BLANKS

5. SURROGATES

6. MATRIX SPIKE/DUP

7. OTHER QC

8. INTERNAL STANDARDS

9. COMPOUND IDENTIFICATION

10. SYSTEM PERFORMANCE

1 1 . OVERALL ASSESSMENT

O « Data had no problems/or qualified dueQ * Data qualified due to major problems.U » Data unacceptable.X * Problems, but do not affect data.

ACTION ITEMS:

VOA BNA PEST - OTHER "

0 q 0 KAo o oX K riA ,0 P .___0

0 0 0

X X X

o o oO 'O ' Q

o o OG O O

o o oto minor problems.

-

AREAS OF CONCERN:' 5(\veft?J icr uer*. hard fa rtzd <) d *nrtn more.cli-ff>i':J/r

xi1«*.-m)

NOTABLE PERFORMANCE: ft DOAf. * C 1

APPENDIX FSUPPORT DOCUMENTATION

62

Calibration Outliers for Volatile Analysis

Compound Sample %Diff DateMatrix

2-Butanone Soil -32.5 12/22/89Total Xylenes Soil -28.3 12/22/89Bromoform Soil -27.2 12/22/89Acetone Soil 27.2 12/28/89Total Xylenes Soil -27.3 12/28/89Bromomethane Water -36.8 12/28/89Carbon Disulfide Water -33.8 12/28/891,1-Dichloroethane Water -37 12/28/891,2-Dichloroethene Water -28.8 12/28/89Chloroform Water -41.8 12/28/891,2-Dichloroethane Water -58.3 12/28/892-Butanone Water -32 12/28/891,1,1-Trichloroethane Water -38.9 12/28/89Bromodichloromethane Water -34.8 12/28/89cis-l,3-Dichloropropene Water 31.4 12/28/891,1,2-Trichloroethane . Water -33 12/28/89trans-l,3-Dichloropropene Water -42.6 12/28/89.4-Methyl-2-Pentanone Water -41.4 12/28/892-Hexanone Water -51.5 12/28/891,1,2,2-Tetrachloroethane Water -40.1 12/28/89Toluene Water -25.3 12/28/89

tom -

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; I

Lab Name: VERSAR IMC Contracts 63-01-7471 I

i-ab Code: VERSAR Case No.s 13383 SAS Mo-: DDG No. s CAW50

.**fixs <iiOil/waUer> SOIL Lal* G^mpls 12= V£LK£

Sample wt/vols D.O <g/mL> G Lab File'lDs R3709_._._*-,• •

Level: (low/med) LOW Da be Received; -r,

?S Moistures not dec* - ** -cJ- iS/eS/03

• - ~ •- . , . •uolumn: (pack/cap) PACK ,' Dilution Factors

' ' CONCENTRATION UNITS sCS3 NO. COI1PQUHD

74— S7-3 ———————— Chlo'rome thane74-Q3-9 ———————— B'romomethane _75-01-4 ———————— Vinyl Chloride75-00-3 ———————— Chloroethane75-09-a ———————— llethylene Chlorde67-64-i ———————— Acetone75-iS-O ——————— —Carbon Disulfide _75-35— 4 —— • ——— : — 1, l-0ichloroe't"hene/S-35-3 ——— '• ———— i, 1 -Pich 1 or oe thane ______540-S9-0 ——————— -l,2-Dichloroethene"Ttotal)&7— 6£-3 ——————— —Chloroform107-OG-2 — --" —— - 1,2-Di chl oroeth ane

___I, i, i-Trichloroeth^nco ~ . - - 5 - —————— Carbon Tetracnlor ide __100 "OS-4 ————— — Vin/175n"S7-4 ———————— Bromod i chl or O\A& thane7Q-S7-5 ——————— -*l, 2-Di chl oro p100S10-1-5 ————— cis-1,3— Dichl or opropene79-0 1~€» ———————— T'ricJiloroefchene

l 79-34-5————————1,1,2,2-Tetrachloroethane1 ioa-oa-3———;———Toluene ;i • •• -I 103-30-7——————

! 1330-20-7———--Total

<uy/L or ug/Kgi UG/KG ' ft'G

_________ • _ , _ i124-48-1 —— -r ——— Dibromoch lorome thane ___ -•_ ____7S-OO-5 ——— '—'• ——— i,l,H-Tri chl oroeth ane _______71-43-2 ———————— Benzene _________ [ ___ IIIII10OS1 -02-6 ————— trans-1, 3-Dichloropropene75-25-H ——— 'f" —— -Bromoform ___ lr_t~i:±10S-10-1 ——————— 4-Methyl-i-Pentanone

VQLATILE ORBAHICS flNrtLYCI.i DflTft SHEITT, reHTATiVe_Y IDENTIFIED "COMPOUNDS ;

i VBLKB9Lab Name: VERSAR INC Contract: &S-01-7471 I_________.

lab Code: VERSAR "Case No. = 133S3 SAS No.: SDG f-!o. s CAW50

.-.ab.fixs <_iuil^wa-Eer> SOIL" . Lab Sample ID. VBLK3S

3 AM pie wt/vols -5.0 : (g/ml.) G : Lab rile ID: 337&3

Level: (low/med) LOW ' Dafee Raceivoiij

* ttoii.tures-T.ot;" dec. "" """" " :" " ' Date finalized: i2/S2/OS

Column (pack/cap)" PflCK """ "" - - - — — - _ ,. Bilution Factova i.o-'

• •"""

'___'_ CONCENTRATION UNITS:<ua/L ov ug/Kg) L!D/KG

I! CflS NUMBERr "

i i.i 2. 1E4-3S-91 3.1 —————————————

11 COMPOUND NfiME•

(UNKNOWNICfiRBQN DIOXIDE <ACM)I UNKNOWN

—J — _ : _______________ _;

I E i ;1 RT 1 EST. CONC. 1 Q i

1 1.03 1 540 ! J i. . 1 1.33 1 .13"- IJ 1

i, a.i7 ; .'.a- oij ;x__z_i !'•_ ___ :_; _ i _____ ±£?3&' k\-_____ (

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,

scSEMIVQLATILE INTERNAL STANDARD AREA SUMMARY

: VERSAR INC - Contract: 6B-O1-7471

Lab Code: VERSAR Case No. : 13383 SAS No. : SDG No. : CAU50

_ab File ID (Standard): V4419 Date Analyzed: 01/24/90

Instrument ID: V Time Analyzed: 1138

[1I 12 HOUR STD

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 WO.

01 1CAU52OSICAU54031CAU5504 1 CflUISSosicnus?G61CAU58071CAU59OSICAU6009ICAU61101CAUSH11 ICAU54MS1EICAU54MSD13ISBLK47

1

IS4<PHN)AREA H

S14OO

162800

40700

106OOO113OOO3730010SOOO1070001020009S70011200010500082400119000

1 1110001 645OO1

RT

21.70

sssss=

21.7021.7021.7021.7021. 7O21.7221.7021.7021.6921.6921.7221.7021.69

IS5<CRY)AREA **

==========63400

1 126800

1 31700

11

1 737001 981001 64600t 757001 112OOQ1 608OO1 692001 71OOO1 70900! 61100! 981001 972001 327001

1RT 1

30.171

1

1

1I

30.17130.19!30.17130.17130. 19130.17130.17130. 17!30.1613O. 16130.21130.19130. 1&!

1

IS6<PRY)AREA tt

29400

58800

14700

38900492003400038900

F 62700 *32000.39500354003650032100510005040015100

1RT 1

34.66!____________ |

1ni HI n i i i i j

I

11

34.67134.71134.67134.66134.74134.67134.66134.67134.66134.64134.71134.69134.641

I

IS4 (PHN) = Phenanthrene-dlO UPPER LIMIT = + 100%ISS (CRY) * Chrysene-dl2 of internal standard area.IS6 <PRY) - Perylene-dl2 LOWER LIMIT = - 50*

of internal standard area.

tt Column used to flag internal standard area values with an asterisk

r,1 of 1

FORM VIII SV-2 1/87 Rev.300277

b Code: VeKartS"'" ""Case.. No. s i33B.i SAS Ho. _ b:_>£_,

Instrument ID: 0' ^ " ' :"V --Calibration "j>atV<s7s ILVSLVfi'J

,0.

Flcl X %ti'JJ ': or 1;:.,_' fv: ) "i " t.J"0. .' '->

COMPOUND " 'IRKK20 iKtfFbC ! RHFiOO I KRFlÔ j *Kr _:0o i ^Ki- I KUU :. _. -__ __ . _ .i__. , , [ • ;""ftj-" j K~T -~"-*r - -• J.Ll -'_ -'- = -' "'i 1 • --=-:—- - r-- " ' -"- - -

J «rB a« M±= «i ii»ii -SCsfes=« ^ d£1|1j.-...i=:.s.=iS( asa:jaAJB.ii } T-rtsssss rt j_ •-•'~-s -•-::::..; -~ -: r .v : e . *.-. •;- ---.,. .-

. ..rhloroft 'K S'. _____±_:__™____ ..p.. !. . .__000_)_p._.i63i..p- /4ai. 0. f^>JI 0. :i.?.1 v-;. O.JBromorif,i.Mirtane__^___^___^^ /_j;3! 0- &£z i O-.b' G f v, J/.- ^, '- .li ;;:. v"."•Vin/l L'iKiaricm_____.^..___._______«_ ..O-J/OiJ i p.ij&iij y.biil w- A'-j.'i • /) '-: -• . , - • • • • -•y-1>4.1.1. <-'».J>v^ : 0.3. •; v. i./,;..; !-..._:

———————————___._„,_..._,• . . .s.w..'™'-.-. -- w < -.- i y . JlS6 ; O- ^ i J . 0-_-;_.»- C-_ -jiXL. . ._-._... .;2 .iMethylene Uiiio'ride_________J _i.. 23 J .1.7H3I 1.H33I 1. Ofld 1 l. Oflli i 1, 3 a 3 ! -H^î! ricetone——_________._____ i 0,6571 0. 39S'l 0. a'S4 I""o.agg! 0.3S9I 0. 377 ' f TH .I Carbon bisulfide_________«.^.^:l-7^' A-61U...J,.,.- 7S ! 1. 710 i_. I.S96! 1.686! V. 3 !' 1,., J.- Dio*'i j.o'roefchtMtpi •••'•• "' i-.s'--• ••< <*•*' • ""• -• -•• •!• [-T.-i,,hir <—».i-' —————— -----'^ y. 70-ti i.w/jj v.vi/i i-o,;.o; _.-.o; ;.>; ,-,->-j., i -Jionj.c,rot-thane .... . u i. /OP i -t S,M i -i v4-,'ti •, ^--* »" • , .. .-, ,. , . ——————————^TT... ••*."-' -'.fe.l J-- ~<Ui_ ] 1- / 'J| J. .b/? .-. „ !;•,.'»;-' : • .:..-., r -. .'Jl: :r ;::r Ktne"e-!t j . :; !4 L- -i;.±, > ,.,.;: :::•:;,: :.:,;'

_-^._-_«i4^: -.-" ^ O-.- ^ r. C ^ .r.; .•^-"CH9! 0.023 I .0. OH'iiJ v. 0^4 i O.Oc'Ci- o./jl j. 'jll.. - .

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i<r£-.'„. ,>_-.!»,'.,-/.. j. _.y- * ._:,.M O-i_.5(.:-, C'~ •••' : " .:..:::.i. i. .o7iii .i,isa: "A-0-^; 111 ;. ~:: : ;- "T. -,- -. i ^ .i.. ^ , ^ ^ ^ ^ ^ ^ _______ .. . _li_,|

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IF • = - - EPfl SftMPLE NO,SEMIVOLATILE ORGftNICS ftNflLYSIS DflTfl SHEET - ______________.

TENTATIVELY IDENTIFIED COMPOUNDS . "Ii SBLK47

. 3 Names VERSflR INC______________ Contracts 56-01-7471 I .

Lab Code: VERSQR Case No. : 13383 SAS No.: ___ SDG No.: CAW50

Matrix: (soil/water) SOIL Lab Sample IDs RB634-7

Sample wt/vois 30, g <g/mL) g___ Lab File IDs V4420

Levels (low/med) LOW Date Receivers l£/gg/8S

*A Moimtures not dec. ___ dec. ___ Date Extracted s l£/£9/B9

Extraction: (SepF/Cont/Sonc) SQNC Date Analyzed: 01/24/90

GPC Cleanups <Y/N) Y__ pH: ____ Dilution Factor: 1.063

CONCENTftflTIPN UNITS:Number TICm founo : _6. (ug/L or ug/Kg) UG/KG

CftS NUMBER

1 . S££-G7-32.

_v 4.1 5.1 6.1

11 COMPOUND NAME

1 S-C YCLOHE X EN- 1 -OLI UNKNOWNI £-CYCLOH£XEN-l-ONE(UNKNOWN KETONE1 UNKNOWN1 UNKNOWN1

RT

5. 556. 33S. 476.727.60S. 97

EST. CONC.

14070140£10140£10

11 Q

IJ1 J1 J1 J1 J1 J1

C300427

FORM I 5V-TIC 1/67 Rev

case no: : 13383 · the samples collected on december 19, 1989, were designated as case 13383. case...

Documents