certificate of analysis · 7.486% total thc at dry weight 5.485% total cbd w/12% moisture 6.587%...

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721 Cortaro Dr. Sun City Center, FL 33573 License No. 800025015 FL License # CMTL-0003 CLIA No. 10D1094068 Harlequin GDP-TruFlower- 3.5G Sample Matrix: CANNABIS (MMTC's) Flower & Plants (Inhalation - Heated) Certificate of Analysis Compliance Test Trulieve 6749 Ben Bostic Rd Quincy, FL 32351 Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12 Extracted From: N/A Sampling Method: MSP 7.3.1 Seed to Sale # FINP-FL-3.5G-H-20-PK-10 Lot ID: DUFL-H-20-PK-13 Cultivars: Harlequin GDP Test Reg State: Florida Cultivation Facility: Trulieve Cultivation Date: 2020-09-08 Production Facility: Trulieve Production Date: 2020-10-12 Order # TRU201012-110035 Order Date: 2020-10-12 Sample # AAAQ833 Sampling Date: 2020-10-13 Lab Batch Date: 2020-10-13 Completion Date: 2020-10-16 Initial Gross Weight: 380 g Product Image Potency Tested Terpenes Tested Heavy Metals Passed Mycotoxins Passed Pesticides Passed Residual Solvents Not Tested Moisture Passed Water Activity Passed Pathogenic Passed Microbiology (qPCR) Passed Filth and Foreign Passed Potency - 11 Specimen Weight: 202.530 mg Tested SOP13.001 (HPLC) Analyte Dilution (1:n) LOD (%) LOQ (%) Result (mg/g) (%) CBDA 150.000 0.00001 0.001 83.118 8.312 THCA-A 150.000 0.000032 0.001 58.558 5.856 Delta-9 THC 150.000 0.000013 0.001 3.496 0.350 CBGA 150.000 0.00008 0.001 3.394 0.339 CBD 150.000 0.000054 0.001 1.962 0.196 CBC 150.000 0.000018 0.001 <LOQ Delta-8 THC 150.000 0.000026 0.001 <LOQ CBN 150.000 0.000014 0.001 <LOQ CBG 150.000 0.000248 0.001 <LOQ CBDV 150.000 0.000065 0.001 <LOQ THCV 150.000 0.000007 0.001 <LOQ Sample Prepared By: 1024 Date: 2020-10-13 11:46:06 Sample Analyzed By: 1067 Date: 2020-10-13 11:46:09 Batch Reviewed By: 1050 Date: 2020-10-14 19:20:19 Lab Batch #: AAAQ833-14 Date: 2020-10-14 19:20:19 Detailed Terpene Analysis is on the following page Potency Summary Total CBD at Dry Weight 7.486% Total THC at Dry Weight 5.485% Total CBD w/12% Moisture 6.587% Total THC w/12% Moisture 4.827% Total CBG 0.298% Total CBN None Detected Other Cannabinoids None Detected Total Cannabinoids 13.269% Terpenes Summary Analyte Result (mg/ml) (%) Beta-Myrcene 5.170 0.517% Total Terpenes: 0.517% Lab Toxicologist Xueli Gao Ph.D., DABT Lab Director/Principal Scientist Aixia Sun D.H.Sc., M.Sc., B.Sc., MT (AAB) Definitions and Abbreviations used in this report: *Total CBD = CBD + (CBD-A * 0.877), *Total THC = THCA-A * 0.877 + Delta 9 THC, *CBG Total = (CBGA * 0.877) + CBG, *CBN Total = (CBNA * 0.877) + CBN, *Other Cannabinoids Total = CBC + CBDV + THCV + THCV-A, *Total Detected Cannabinoids = CBD Total + CBG Total + CBN Total + THC Total + CBC + CBDV + THCV + THCV-A, *Analyte Details above show the Dry Weight Concentrations unless specified as 12% moisture concentration. (mg/ml) = Milligrams per Milliliter, LOQ = Limit of Quantitation, LOD = Limit of Detection, Dilution = Dilution Factor (ppb) = Parts per Billion, (%) = Percent, (cfu/g) = Colony Forming Unit per Gram (cfu/g) = Colony Forming Unit per Gram, , LOD = Limit of Detection, (µg/g) = Microgram per Gram (ppm) = Parts per Million, (ppm) = (µg/g), (aw) = aw (area ratio) = Area Ratio, (mg/Kg) = Milligram per Kilogram This report shall not be reproduced, without written approval, from ACS Laboratory. The results of this report relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Accredited by a third-party accrediting body as a competent testing laboratory pursuant to ISO/IEC 17025 of the International Organization for Standardization. Phone Number: 866.762.8379 Email: [email protected] Form 40 Page 1 of 6

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  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Product Image

    PotencyTested

    TerpenesTested

    Heavy MetalsPassed

    MycotoxinsPassed

    PesticidesPassed

    ResidualSolventsNotTested

    MoisturePassed

    Water ActivityPassed

    PathogenicPassed

    Microbiology(qPCR)Passed

    Filth and ForeignPassed

    Potency - 11 Specimen Weight: 202.530 mg

    TestedSOP13.001 (HPLC)

    Analyte Dilution

    (1:n) LOD(%)

    LOQ(%)

    Result(mg/g) (%)

    CBDA 150.000 0.00001 0.001 83.118 8.312 THCA-A 150.000 0.000032 0.001 58.558 5.856 Delta-9 THC 150.000 0.000013 0.001 3.496 0.350 CBGA 150.000 0.00008 0.001 3.394 0.339 CBD 150.000 0.000054 0.001 1.962 0.196 CBC 150.000 0.000018 0.001

  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Terpenes - FL Specimen Weight: 1.010 mg

    Dilution Factor: 1.000

    TestedSOP13.028 (GC-FID)

    Analyte Dilution(1:n) LOQ(%) Result(mg/g) (%) Analyte Dilution(1:n) LOQ(%) Result(mg/g) (%) Beta-Myrcene 1.000 0.02 5.170 0.517 (+)-Cedrol 1.000 0.02

  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Heavy Metals Specimen Weight: 248.570 mg

    Dilution Factor: 2.000

    PassedSOP13.009 (ICP-MS)

    Analyte Dilution(1:n) LOQ(ppb) Action Level(ppb) Result(ppb) Analyte Dilution(1:n) LOQ(ppb) Action Level(ppb) Result(ppb)Arsenic (As) 2.000 100 200

  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Pesticides FL V4 (Inhalable) Specimen Weight: 169.300 mg

    Dilution Factor: 8.860

    PassedSOP13.007 (LCMS/MS)

    Analyte Dilution(1:n) LOQ(ppb) Action Level(ppb) Result(ppb) Analyte Dilution(1:n) LOQ(ppb) Action Level(ppb) Result(ppb)Abamectin 8.860 28.23 100

  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Moisture Specimen Weight: N/A

    PassedSOP13.015 (Moisture Meter)

    Analyte Action Level(%) Result(%)Moisture 15 10.790

    Sample Prepared By: 1092 Date: 2020-10-13 11:21:25 Sample Analyzed By: 1092 Date: 2020-10-13 11:21:31

    Batch Reviewed By: 1092 Date: 2020-10-13 11:27:12 Lab Batch #: AAAQ833-10 Date: 2020-10-13 11:27:12

    Water Activity Specimen Weight: N/A

    PassedSOP13.016 (Water Activity Analyzer)

    Analyte Action Level(aw) Result(aw)Water Activity 0.65 0.536

    Sample Prepared By: 1092 Date: 2020-10-13 11:19:59 Sample Analyzed By: 1092 Date: 2020-10-13 11:20:09

    Batch Reviewed By: 1092 Date: 2020-10-13 11:20:12 Lab Batch #: AAAQ833-11 Date: 2020-10-13 11:20:12

    Pathogenic SAE (qPCR) Specimen Weight: 254.100 mg

    Dilution Factor: 1.000

    PassedSOP13.010 (qPCR)

    Analyte Action Level(cfu/g) Result(cfu/g) Analyte Action Level(cfu/g) Result(cfu/g)Aspergillus (Flavus, Fumigatus,Niger, Terreus) 1 Absence in 1g E.Coli 1 Absence in 1g

    Salmonella 1 Absence in 1gSample Prepared By: 1088 Date: 2020-10-14 13:09:17 Sample Analyzed By: 1088 Date: 2020-10-14 13:09:35

    Batch Reviewed By: 1088 Date: 2020-10-14 23:35:40 Lab Batch #: AAAQ833-25 Date: 2020-10-14 23:35:40

    Lab ToxicologistXueli Gao

    Ph.D., DABT

    Lab Director/PrincipalScientist

    Aixia Sun D.H.Sc., M.Sc.,B.Sc., MT (AAB)

    Definitions and Abbreviations used in this report: *Total CBD = CBD + (CBD-A * 0.877), *Total THC = THCA-A * 0.877 + Delta 9 THC, *CBG Total = (CBGA * 0.877) +CBG, *CBN Total = (CBNA * 0.877) + CBN, *Other Cannabinoids Total = CBC + CBDV + THCV + THCV-A, *Total Detected Cannabinoids = CBD Total + CBG Total +CBN Total + THC Total + CBC + CBDV + THCV + THCV-A, *Analyte Details above show the Dry Weight Concentrations unless specified as 12% moistureconcentration. (mg/ml) = Milligrams per Milliliter, LOQ = Limit of Quantitation, LOD = Limit of Detection, Dilution = Dilution Factor (ppb) = Parts per Billion, (%) =Percent, (cfu/g) = Colony Forming Unit per Gram (cfu/g) = Colony Forming Unit per Gram, , LOD = Limit of Detection, (µg/g) = Microgram per Gram (ppm) = Partsper Million, (ppm) = (µg/g), (aw) = aw (area ratio) = Area Ratio, (mg/Kg) = Milligram per Kilogram

    This report shall not be reproduced, without written approval, from ACS Laboratory. The results of this report relate only to the material or productanalyzed. Test results are confidential unless explicitly waived otherwise. Accredited by a third-party accrediting body as a competent testinglaboratory pursuant to ISO/IEC 17025 of the International Organization for Standardization.

    Phone Number: 866.762.8379 Email: [email protected] Form 40 Page 5 of 6

  • 721 Cortaro Dr.Sun City Center, FL 33573

    License No. 800025015 FL License # CMTL-0003CLIA No. 10D1094068

    Harlequin GDP-TruFlower- 3.5GSample Matrix:

    CANNABIS (MMTC's)Flower & Plants

    (Inhalation - Heated)

    Certificate of AnalysisCompliance Test

    Trulieve6749 Ben Bostic RdQuincy, FL 32351

    Batch # FINP-FL-3.5G-H-20-PK-10 Batch Date: 2020-10-12Extracted From: N/ASampling Method: MSP 7.3.1

    Seed to Sale # FINP-FL-3.5G-H-20-PK-10Lot ID: DUFL-H-20-PK-13Cultivars: Harlequin GDPTest Reg State:Florida

    Cultivation Facility: TrulieveCultivation Date: 2020-09-08Production Facility: TrulieveProduction Date: 2020-10-12

    Order # TRU201012-110035Order Date: 2020-10-12Sample # AAAQ833

    Sampling Date: 2020-10-13Lab Batch Date: 2020-10-13Completion Date: 2020-10-16

    Initial Gross Weight: 380 g

    Total Yeast and Mold Specimen Weight: 10026.600 mg

    Dilution Factor: 1.000

    PassedSOP13.029 (qPCR)

    Analyte Action Level(cfu/g) ResultTotal Yeast/Mold 100000 Passed

    Sample Prepared By: 1142 Date: 2020-10-13 13:25:14 Sample Analyzed By: 1142 Date: 2020-10-13 13:25:36

    Batch Reviewed By: 1088 Date: 2020-10-13 13:25:39 Lab Batch #: AAAQ833-218 Date: 2020-10-13 13:25:39

    Filth and Foreign Material Specimen Weight: 1.000 mg

    Dilution Factor: 1.000

    PassedSOP13.020 (Electronic Balance)

    Analyte Action Level(%) Result(%) Analyte Action Level(mg/Kg) Result(mg/Kg)Covered Area 10 0.000 Feces 0.5 0.000Weight % 1 0.000

    Sample Prepared By: 1066 Date: 2020-10-13 12:36:15 Sample Analyzed By: 1066 Date: 2020-10-13 12:36:18

    Batch Reviewed By: 1092 Date: 2020-10-13 12:36:22 Lab Batch #: AAAQ833-17 Date: 2020-10-13 12:36:22

    Lab ToxicologistXueli Gao

    Ph.D., DABT

    Lab Director/PrincipalScientist

    Aixia Sun D.H.Sc., M.Sc.,B.Sc., MT (AAB)

    Definitions and Abbreviations used in this report: *Total CBD = CBD + (CBD-A * 0.877), *Total THC = THCA-A * 0.877 + Delta 9 THC, *CBG Total = (CBGA * 0.877) +CBG, *CBN Total = (CBNA * 0.877) + CBN, *Other Cannabinoids Total = CBC + CBDV + THCV + THCV-A, *Total Detected Cannabinoids = CBD Total + CBG Total +CBN Total + THC Total + CBC + CBDV + THCV + THCV-A, *Analyte Details above show the Dry Weight Concentrations unless specified as 12% moistureconcentration. (mg/ml) = Milligrams per Milliliter, LOQ = Limit of Quantitation, LOD = Limit of Detection, Dilution = Dilution Factor (ppb) = Parts per Billion, (%) =Percent, (cfu/g) = Colony Forming Unit per Gram (cfu/g) = Colony Forming Unit per Gram, , LOD = Limit of Detection, (µg/g) = Microgram per Gram (ppm) = Partsper Million, (ppm) = (µg/g), (aw) = aw (area ratio) = Area Ratio, (mg/Kg) = Milligram per Kilogram

    This report shall not be reproduced, without written approval, from ACS Laboratory. The results of this report relate only to the material or productanalyzed. Test results are confidential unless explicitly waived otherwise. Accredited by a third-party accrediting body as a competent testinglaboratory pursuant to ISO/IEC 17025 of the International Organization for Standardization.

    Phone Number: 866.762.8379 Email: [email protected] Form 40 Page 6 of 6

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351

    Certificate of AnalysisCompliance TestTrulieve6749 Ben Bostic RdQuincy, FL 32351