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WIR SCHAFFEN WISSEN – HEUTE FÜR MORGEN EIGER: High frame rate pixel detector for synchrotron and electron microscopy applications Gemma Tinti:: SLS Detector Group :: Paul Scherrer Institut Vienna Conference on Instrumentation 2019

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Page 1: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

WIR SCHAFFEN WISSEN – HEUTE FÜR MORGEN

EIGER: High frame rate pixel detector for synchrotron and electron microscopy applications

Gemma Tinti:: SLS Detector Group :: Paul Scherrer Institut

Vienna Conference on Instrumentation 2019

Page 2: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

WIR SCHAFFEN WISSEN – HEUTE FÜR MORGEN

Detector development for Synchrotron and FEL applications

Erik Fröjdh M. Andrä, A. Bergamaschi, M. Brückner, S. Chiriotti Alvarez, R. Dinapoli, D. Greiffenberg, C. Lopez-Cuenca, A.

Mozzanica, M. Meyer, D. Mezza, S. Redford, C. Ruder, B. Schmitt, X. Shi, D. Thattil, G. Tinti, S. Vetter, J. Zhang

Vienna Conference on Instrumentation 2019

Page 3: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Paul Scherrer Institut

Neutron source

Muon source

Proton therapy

Proton accelerator

Nanotechnology

Radiochemistry

Radiopharmacy

Material sciences

Basel Zurich Germany Aarau/Bern

Hotlab

Particle physics

SwissFEL

Energy research

Biology

ESI Platform

Synchrotron Light Source

3

Staff: 2000

Users/year:

2300 people

5300 visits

Page 4: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

What do we do in the detector group?

Bump and wire bonding

Lithography

Users support

Chips Sensors Electronics Firmware SoftwareMechanics

Assembly Commissioning

4

Page 5: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

MYTHENII&III

EIGER GOTTHARDI & II

JUNGFRAU MÖNCH AGIPD

1D/2D Strip Pixel Strip Pixel Pixel Pixel

Working Mechanism

PhotonCounting

Photon Counting

Charge Integrating

Charge Integrating

Charge Integratin

g

Charge Integratin

g

Strip/Pixel size [µm]

50 75×75 25/50 75×75 25×25 200×200

Applications Powderdiffraction,

energy-dispersive

spectrometers, beam position.

Ptychography, coherentimaging,protein

crystallography.

@ FLASH,main energy-

dispersive detector for

EU-XFEL.

Spectroscopicapplications, high count

rateapplications at

XFELs & synchrotrons.

(Biological) imaging &

tomography, RIXS,

spectroscopy, Laue

diffraction.

Development for the EU-

XFEL.

Our detectors

5

Page 6: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• Single photon counting

1 global threshold

6 trimbits / pixel

• 75 x 75 μm2

• 256 x 256 pixels

• Noise 100-200* e- RMS

• Configurable: 4/8/12 bit counter depth

• Frame rate: 23/11/8 kHz

• Dead time free operation mode (3μs)

• Count rate dead time

EIGER: 200-600ns

Eiger

*Depending on gain setting

– fast frame rate, dead time free, photon counting

coun

ter

+1

E

I

Threshold VcmpAdj. Gain

6

Page 7: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• 2x4 chips

• Single 4x8 cm2 silicon sensor

• Sensor thickens 320 μm

• Dedicated read out system per half module

with 10Gb/s Ethernet for data output

Eiger: Module

Eiger module equipped with

ASICs but no sensor

2x pixel

4x pixel

7

Page 8: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• Modules can be tiled to large area detectors

• Due to the parallel design there is no penalty in performance when moving from a

single module to multi module systems

Eiger: Detector

8

Page 9: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

24 x 23 cm

3072 x 3072 pixels

9

Page 10: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• Charge integrating

• 75 x 75 um2 pixel

• 256 x 256 pixels

• Noise: 55e- (HG0 10us RT )

• Dynamic gain switching with 3 gain stages

Single photon sensitivity (from ~2 keV)

Dynamic range 104 12keV photons

• 1.1 kHz frame rate (2.4 kHz)

Jungfrau – dynamic gain switching, charge integrating

500k single module systemSame as Eiger

10

Page 11: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Automatic gain switching scan:

• White visible light illumination

• Requires removing of Al top layer

• Increasing integration time• plots in unit of 12keV

photons

Gain switchGain switch

Poisson

statistical limit

~20 ɣ ~700 ɣ~700 ɣ ~10800 ɣ

Noise across dynamic range

11A. Mozzanica (PSI)

Page 12: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• Charge integrating

• 25 x 25 μm2 pixel size

• 400 x 400 pixels

• Noise ~ 36e-/pixel

• Configurable but static gain

• Frame rate 3 kHz (6kHz)

• Two side buttable

Mönch

Mönch 03

– small pixels, low noise, charge integrating

12

Page 13: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Bump bonding

Hit map from Ge Kα fluorescence

Yield better than 99.95%

Pilatus 172 μm Eiger75 μm

x5.3

Mönch25 μm

x47

• Standard process

• Performed in-house at PSI

• Indium balls of diameter ~ 15 μm

13

Page 14: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

High resolution imaging using interpolation

MÖNCH used as a photon counter (after clustering)

11 keV beam - Nanoscopium beamline, SOLEIL

No position interpolation

25 µm bins (pixels)

With position interpolation

1 µm bins

Measurement with: K. Medjoubi (SOLEI) Image processing: M. Ramilli (PSI)

Requires the primary track (ion, electron, photo electron) to be short

compared to pixel sizeFixed pattern due to that the charge sharing is position dependent

14

Page 15: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Page 15

Sensors characterization with Jungfrau

Silicon CdTe GaAs

Sensor production Hamamastsu Acrorad Tomsk State University

Type p-on-n Schottky Cr compensated, Ohmic

Bump bonding PSI Advacam PSI

Thickness 320 um 750 um 500 um

Pixel size 75 x 75 um2 75 x 75 um2 75 x 75 um2

Bias voltage 200 V -500 V -300 V

Leakage current < 1uA 1.5uA 35uA

Si GaAsCdTe

4cm

8 cm

Silicon

Page 16: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Microscopes

Philips CM12 20-100 keV Geant4 pixel simulation framework

A. Schubel et al. A Geant4 based framework for pixel detector simulation, JINST 9, 2014

Page 17: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Page 17

Page 18: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Page 18

Page 19: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Simulation of lateral spread

Page 19

Page 20: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Simulation of electron range

Page 20

Energy [keV]

Page 21: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Cluster size – Silicon sensor

Page 21Sensor thickness: 320 um

Page 22: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

MTF with single particle processing 100 keV

Page 22

Page 23: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Energy response

Page 23

GaAs 2us exposure time data with linearity correction applied

Silicon 10us no correction

CdTe 10us no correction

Page 24: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Energy response at 80 keV

Page 24

Page 25: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Measured efficiency of CdTe and GaAs

Page 25

Normalized using simulated Silicon efficiency, th 2.5keV

Page 26: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• SLS Detector group is developing strip and pixel detectors for photon science

applications

• Largest deployed detector system Jungfrau 16M Eiger 9M

• Working on larger area dynamic gain switching Mönch

• Electron detection with High Z sensors

• Thin entrance window sensor for low energy photon and electron detection

Summary

Page 26

Page 27: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

SLS Detector Group

Page 27

Page 28: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Subpixel interpolation

T/(T+B)

R/(R+L)

• The signal is fully contained in

a 2x2 pixels cluster

• We analyze the ratio between

neighbors

η𝑥=0∙𝐿𝑒𝑓𝑡+1∙𝑅𝑖𝑔ℎ𝑡

𝑅𝑖𝑔ℎ𝑡+𝐿𝑒𝑓𝑡

η𝑦=0∙𝐵𝑜𝑡𝑡𝑜𝑚+1∙𝑇𝑜𝑝

𝐵𝑜𝑡𝑡𝑜𝑚+𝑇𝑜𝑝

• Custom algorithms must be

developed to correct for non

linear charge sharing

28A. Bergamaschi (PSI)

Page 29: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

• The spatial resolution is higher in

the corner between pixels than in

the center of the pixels due to

limited charge sharing

• Energy dependent Higher energies, higher SNR

Lower energies, larger charge sharing

• Possible improvements Smaller pitch

Thicker sensors

Lower bias voltage

Spatial resolution

6 keVPencil beam scan

experiment

@ cSAXS beamline, SLS

29

25

0

Vertical resolution

0 25µm

3.3

1.4

µmµm

25

00 25µm

3.3

1.4

µmµm

Horizontal resolution

A. Bergamaschi (PSI)

Page 30: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Effect of removing top layer aluminum

Page 30

• Measured with Eiger at the SIM beamline at the Swiss Light Source

• Improves energy response and efficiency

• Still energy straggling in the entrance window

Page 31: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

MTF measurements with EIGER

Page 31

Page 32: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Energy response GaAs 100 keV

Page 32

Page 33: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Simulated efficiency - Silicon

Page 33

1.5 um Aluminum as entrance window – Matched

energy response at 20keV

Page 34: EIGER: High frame rate pixel detector for synchrotron and ... · •Largest deployed detector system Jungfrau 16M Eiger 9M •Working on larger area dynamic gain switching Mönch

Clustering

Page 34