equipment and methods of metals and alloys chemical

Equipment and methods ofmetals and alloys chemical

analysis in various industries

These are the simplest methods, but not always accurate ones, as it isimpossible to determine the composition of the matter accurately based onone reaction.

- a solution colour change

- a precipitate resolution or formation

- the evolution of gas

Chemical analysis of the analyte is carried out using chemical, physical and physical-chemical methods, as well as biological methods.

Chemical methods are based on the use of chemical reactions, accompanied by easilyobserved physical effects such as:

Unlike with a chemical method, physical and physical-chemical methods are calledinstrumental, as analytical instrumentation and devices that record the physicalproperties of matters or changes in these properties used for the analysis.

A chemical reaction is not used while performing a physical analysis method, whereasphysical properties of matter are measured, which is a function of its composition.

For example, spectral analysis studies the frequency of the spectral emissions ofmatter. Their availability is determined by the existence of lines that typify theseelements in the spectrum while their quantitative content is determined by thebrightness of the lines.

Spectral analysis equipment

Optical emission spectrometers (OES)

X-ray fluorescent (XRF)analyzers

Laser-induced breakdownspectrometers (LIBS)

Optical emission spectrometers produced byG.N.R. s.r.l. - Analytical Instruments Group, Italy

Detectors CMOS

Optical System Paschen-Runge

Wavelength range from170 to 460 nanometers

Spark source Multi-frequency spark source. Excitation parameters controlled by computer

Extra features auto diagnosis, automatic standardization, network linking and remote control

Power Supply 110/220 V AC 16 A 1 KW

Dimensions W 50 x L 59 x H 31 cm

Weight 35 Kg

Detectors CMOS

Optical System Paschen-Runge

Wavelength range from 130 to 460 nanometers, if requested to 700 nanometers




Dimensions W 26 x D 73 x H 62 cm

Weight 50 Kg

S1 MiniLab 150

S3 MiniLab 300


Detectors CMOS

Optical System Paschen-Runge, vertical, Vacuum Pump System, with direct order of accuracy monitoring, without fiber optics

Wavelength range from 130 to 900 nm


Extra features auto diagnosis, automatic standardization, network linking and remote control, statistics tables.


Dimensions W90×D36×H621 см

Weight 100 Kg

Detectors CMOS

First Optical System vertical, Vacuum Pump System, Paschen-Runge, focal length 500 mm

Second Optical System aerial, , Paschen-Runge, focal interval 500 mm


Spark source Multi-frequency HEPS spark source. Excitation parameters fully controlled by computer, discharge frequency100−1000 Hz, voltage 100−500 W.


Power Supply 110/220 VAC 16A 2.5 KW


Weight 160 kg

S5 - Solaris CCD Plus (SCP)

S7 - Metal Lab Plus (MLP)


Detectors CMOS

First Optical System optical chamber sealed against light and dust, focal length 300 mm

Wavelength range from 165 to 610 нм

Spark source HEPS technic (High Energy Pre Spark) up to 500 Hz

Sonde ergonomical light pistol

Power Supply 220 single phase or batteries (optional)

Dimensions W 60 cm, D 29 cm, H 51 cm

Weight under 23 Kg

S9 Atlantis

E3 Esaport

Detectors CMOS

First Optical System vertical, Paschen-Runge, focal length 750 mm

Optical medium dry vacuum


Spark source Multi-frequency spark source, Excitation parameters controlled by computer, HEPS (High Energy Pre Spark) from 200 to 1000 Hz




Weight 320 Kg


Optical emission spectrometers produced byHitachi High-Tech Analytical Science, Germany

Determination of chemical elements, including C,S,P

Alloy measurements basedon

Fe, Al, Cu, Ni, Ti, Zn, Pb, Sn, Mg, Co

Wavelength rangefrom 172 nm to 671 nm

Weight 35 Kg

Measurement time 5-10 sec.

Technical specifications

- Paschen-Runge Optical System: Multi HighResolution CCD system

- Automatic line profiling for every measurement- Replaceable stands for individual matrices allow

you to quickly switch from one material to another- Optical emission spectrometer Foundry-Master

Smart UVR an excellent solution for incoming metalanalysis, foundry casting work analysis andproduct certification

SpecificationFOUNDRY-MASTER Smart

Wavelength range от 130 нм до 780 нм

Alloy measurements based on

Fe, Al, Cu, Ni, Ti, Zn, Pb, Sn, Co, Mg

Optical System Vacuum

Sample maximum weight under 20 Kg

Weight 70 кг

Dimensions 400x650x750 мм

Technical specifications FOUNDRY-MASTER XPR Specification

- Paschen-Runge Vacuum Optical System: Multi HighResolution CCD system of 4096 pixel

- Automatic line profiling during each measurementtakes into account the influence of temperaturefluctuations and mechanical stresses, excluding theuse of thermal stabilization of the optical system

- A vacuum optical system, unlike a gas-filled one,can significantly reduce gas (argon) consumption,as well as avoid contaminating impurity of theoptical system in case of low-quality gas supply.Consumption is about 3,000 measurements from astandard 40 litre cylinder



Basics possibleFe, Al, Cu, Ni, Ti, Zn, Pb, Sn, Co, Mg

Optical System based onCCD system Paschen-Runge

Wavelength range from 160 nm to 800 nm

Weight 70 Kg

Power Supply 220W, 50/60 Hz

- Paschen-Runge Optical System: Multi High ResolutionCCD system

- Small, virtually silent vacuum pump designed for everyday intensive work

- Ability to analyze thin rods, uneven surfaces, complex shapes thanks to the JetStream argon purge system

- The measuring table of the spectrometer allows you to measure large samples weighing up to 15 kg

- Dimensions: 368x635x889 mm

Specification

Wavelength range from 130 nm to 780 nm

Alloy measurements based on


Optical System Vacuum

Sample maximum weight under 15 Kg

Weight with power supply unit PR — 70 Kg

LAB — 160 Kg

Main unit dimensions

XPR — 400x650x750 mmLAB — 1130x840x720 mm

Technical specifications Specification

- Vacuum optical system according to the Paschen-Runge scheme using 16 CCD (CCD) high resolution of4096 pixels

- The vacuum optical system is located at an angle sothat it is possible to analyze the spectrum in the deepultraviolet region, which allows for high-precisionanalysis of nitrogen, carbon, sulfur, phosphorus

FOUNDRY-MASTER UVR

FOUNDRY-MASTER LAB



Basics possibleFe, Al, Cu, Ni, Ti, Zn, Pb, Sn, Co, Mg

Optical System

based on CCD system according to the Paschen-Runge scheme

Wavelength range170-420 nm (under 671 nm for Cu, Na, Li)

Weight 28 Kg

Battery life 8 hours

- There are three options for removable power supplies: a power supply unit, a battery pack for fieldwork, a cart with a built-in high-capacity battery for use in the workshop

- Built-in grade guide for foreign brands and GOST- The ultra-compact optical system in the UV-PRO

sensor for low C, S and P analysis- Dimensions: 355x290x500 mm

Specification

Wavelength range170-420 nm (under 671 nm for Cu, Na, Li)

Alloy measurements basedon


Sample maximum weightunder 15 Kg

Weight

analyzer — 12 Kg, with battery — 15 Kg, sensor — 1.1 Kg, UVTouch sensor — 2 Kg

Main unit dimensions 410x425x235 mm

Technical specifications Specification

- The PMI-MASTER SMART portable optical emissionspectrometer is a high-precision analyzer of thechemical composition of metals for working in thefield and any inaccessible places: workshops, onracks, construction sites, on pipeline elements

- The JetStream argon flow around the electrodeprovides the ability to measure uneven samples, thinrods, and wire without selecting and using adapters

- There are two touch displays - one on the device, andthe other on the UVTouch sensor.

PMI-MASTER UVR

PMI-MASTER SMART


X-ray fluorescence analyzer produced byHitachi High-Tech Analytical Science, Germany

X-ray fluorescence analyzer produced byHitachi High-Tech Analytical Science, Germany

Скорость анализа 2-5 секунд

Диапазон обнаружения элементов от 0% до 100%

Анализ всех металлов, включая легкие Mg, Al, Si, P и S

Перенос данных с помощью USB–порта (без внешних устройств и настройки ПО)

Время работы от аккумулятора 10-12 часов, 16 часов в режиме ожидания

Вес прибора с аккумулятором 1,5 кг

Reliability and industrial design:• IP54 (NEMA 3) dust and moisture

protection certificate;• Large modern color Blanview LCD

display, 57x98mm;• Return to operating mode 20 seconds

after switching on;• Battery life: 10-12 hours, 16 hours

standby time;• High level of radiation safety;

Measurement time 2-5 sec.

Element Detection Range From 0 per cent up to 100per cent

Analysis of all metals, including light ones Mg, Al, Si, P and S

Data transfer via USB port(without external devices and software settings)

Battery life 10-12 hours, 16 hours on standby

Weight with battery 1,5 Kg

Technical specifications:

Laser-induced breakdown spectrometers produced byHitachi High-Tech Analytical Science, Germany

Measurement time 1 sec.

Element Detection Range(depending on the element and the basis)

0,02 – 0,2 per cent

Analysis of all metals, including light ones Be, Al, Si, Mg

Temperature range from 0 °C to 40 °C

Battery life 8-10 hours

Weight with battery 1,5 Kg

Technical parameters:

Convenient and simple operation:• Large modern color display 57x98 mm• Large display of the brand according to GOST, AISI, DIN• Data transfer via USB connector without connecting to a computer

Analytical capabilities:• Empirical calibrations with auto-selection of the program for the main types of alloys• All kinds of steels, aluminum, titanium, cobalt, copper, tin, magnesium, lead, nickel alloys• A function of recalibration at one point• Typical detection limits are 0.02 – 0.2% depending on the element and base

Reliability and industrial design:IP54 dust and moisture protection certificate

MIL-810 g certificate-vibration and drop protection

Laser-induced breakdown spectrometers produced byHitachi High-Tech Analytical Science, Germany

Laser spark emission spectrometer produced by Laser-Export, Russia

Advantages of laser analyzer ELANIK:• Analysis of alloying elements, including C (carbon) without the use of inert gases.• Built-in camera-convenient for analyzing a specific location on the sample.• The ability to measure small samples: the scope of analysis is less than 0.3 mm.• Automatic recognition of the alloy without user intervention.• Built-in stamp-automatic determination of the alloy grade based on the analysis results.• High accuracy of the results is achieved by averaging over several points.• Automatic storage of measurement data in the built-in memory of the device up to 100 000 measurements.• High reliability: does not contain elements requiring replacement or maintenance.• Power supply: 220V or rechargeable Li-ion batteries.

The calculation of the carbon equivalent (CE):


Main technical characteristics

The display shows:• alloy type • alloy grade (3 closest to the measured chemical• composition) • equivalent carbon content • chemical composition of the sample• the absolute RSD for the measured points (if the

measurement was taken at several points) • camera view of the burning spot • measurement number (the result is automatically

saved and stored in the instrument memory)


Laser analyzer ELANIK is included in the register of measuring instruments of Russia, Belarus and Kazakhstan


equipment and methods of metals and alloys chemical

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