final addendum - los angeles

51-1-10052-021

APPENDIX H

CHEMICAL TESTING

51-1-10052-021 R1-AH/wp/ADY 51-1-10052-021

H-i

APPENDIX H

CHEMICAL TESTING

TABLE OF CONTENTS

ATTACHMENTS

AETL Report B-10 and B-11for Disposal (16 pages)

Disposal Manifest Form (3 pages)

Job Number Order Date Client 66662 08/23/2012 SH&W

Number of Pages 12 Date Received 08/23/2012 Date Reported 09/04/2012

Shannon & Wilson664 W. Broadway AvenueGlendale, CA 91204-1010

Project ID:Project Name:

51-1-10052-021White Point

Ordered By

Attention: Dean FrancuchTelephone: (818)539-8420

Enclosed please find results of analyses of 2 soil sampleswhich were analyzed as specified on the attached chain ofcustody. If there are any questions, please do not hesitate tocall.

Site: San Pedro, CA

2834 & 2908 North Naomi Street Burbank, CA 91504 • DOHS NO: 1541, LACSD NO: 10181Tel: (888) 288-AETL • (818) 845-8200 • Fax: (818) 845-8840 • www.aetlab.com

American Environmental Testing Laboratory Inc.

Cyrus Razmara, Ph.D.Laboratory Director

Approved By:Checked By:

Job Number Order Date Client

66662 08/23/2012 SH&W

Project ID: 51-1-10052-021

Date Received 08/23/2012

Date Reported 09/04/2012

Shannon & Wilson

664 W. Broadway Avenue

Glendale, CA 91204-1010

Ordered By

Attention: Dean FrancuchTelephone: (818)539-8420

Page: 1 A

AETL received 2 samples with the following specification on 08/23/2012.

CERTIFICATE OF ANALYSISCASE NARRATIVE



Lab ID Sample ID Sample Date Matrix QTY of Containers

66662.01 B-10 08/22/2012 Soil 166662.02 B-11 08/22/2012 Soil 1

The samples were analyzed as specified on the enclosed chain of custody.Analytical non-conformances have been noted on the report.

Cyrus Razmara, Ph.D.

Laboratory Director

Approved By:Checked By:

QC Batch No: 0824122A1

66662 08/23/2012 SH&W

AETL Job Number Submitted Client

San Pedro, CAShannon & Wilson664 W. Broadway AvenueGlendale, CA 91204-1010



2Page:

Ordered By

Attn: Dean Francuch

SiteANALYTICAL RESULTS

Telephone: (818)539-8420

Method: (8260B), Volatile Organic Compounds by GC/MS (SW846)



Date Sampled 08/22/201208/22/2012

Dilution Factor 1 1 1Units ug/Kg ug/Kg ug/KgMatrix Soil Soil SoilDate Analyzed 08/24/2012 08/24/2012 08/24/2012

Date Prepared 08/24/2012 08/24/2012 08/24/2012

B-10 B-11Client Sample I.D.

Analytes MDL Results Results ResultsPQL

Preparation Method 5030 5030 5030

Our Lab I.D. 66662.0266662.01Method Blank

50Acetone 25 ND ND ND

10.0Benzene 1.0 ND ND ND

10.0Bromobenzene (Phenyl bromide) 5.0 ND ND ND

10.0Bromochloromethane 5.0 ND ND ND

10.0Bromodichloromethane 5.0 ND ND ND

50Bromoform (Tribromomethane) 25 ND ND ND

30Bromomethane (Methyl bromide) 15 ND ND ND

502-Butanone (MEK) 25 ND ND ND

10.0n-Butylbenzene 5.0 ND ND ND

10.0sec-Butylbenzene 5.0 ND ND ND

10.0tert-Butylbenzene 5.0 ND ND ND

50Carbon Disulfide 25 ND ND ND

10.0Carbon tetrachloride 5.0 ND ND ND

10.0Chlorobenzene 5.0 ND ND ND

30Chloroethane 15 ND ND ND

502-Chloroethyl vinyl ether 50 ND ND ND

10.0Chloroform (Trichloromethane) 5.0 ND ND ND

30Chloromethane (Methyl chloride) 15 ND ND ND

10.02-Chlorotoluene 5.0 ND ND ND

10.04-Chlorotoluene 5.0 ND ND ND

501,2-Dibromo-3-chloropropane (DBCP) 25 ND ND ND

10.0Dibromochloromethane 5.0 ND ND ND

10.01,2-Dibromoethane (EDB) 5.0 ND ND ND

10.0Dibromomethane 5.0 ND ND ND

10.01,2-Dichlorobenzene 5.0 ND ND ND



30Dichlorodifluoromethane 15 ND ND ND


66662 08/23/2012 SH&W

AETL Job Number Submitted ClientProject ID:Project Name:


3Page:ANALYTICAL RESULTS




Date Sampled 08/22/201208/22/2012


Date Prepared 08/24/2012 08/24/2012 08/24/2012





10.01,1-Dichloroethane 5.0 ND ND ND

10.01,2-Dichloroethane (EDC) 5.0 ND ND ND

10.01,1-Dichloroethene 5.0 ND ND ND

10.0cis-1,2-Dichloroethene 5.0 ND ND ND

10.0trans-1,2-Dichloroethene 5.0 ND ND ND

10.01,2-Dichloropropane 5.0 ND ND ND



10.01,1-Dichloropropene 5.0 ND ND ND

10.0cis-1,3-Dichloropropene 5.0 ND ND ND

10.0trans-1,3-Dichloropropene 5.0 ND ND ND

10.0Ethylbenzene 1.0 ND ND ND

30Hexachlorobutadiene 15 ND ND ND

502-Hexanone 25 ND ND ND

10.0Iodomethane 5.0 ND ND ND

10.0Isopropylbenzene 5.0 ND ND ND

10.0p-Isopropyltoluene 5.0 ND ND ND

504-Methyl-2-pentanone (MIBK) 25 ND ND ND

10.0Methyl-tert-butyl ether (MTBE) 2.0 ND ND ND

50Methylene chloride (DCM) 25 ND ND ND

10.0Naphthalene 5.0 ND ND ND

10.0n-Propylbenzene 5.0 ND ND ND

10.0Styrene 5.0 ND ND ND

10.01,1,1,2-Tetrachloroethane 5.0 ND ND ND

10.01,1,2,2-Tetrachloroethane 5.0 ND ND ND

10.0Tetrachloroethene 5.0 ND ND ND

10.0Toluene (Methyl benzene) 1.0 ND ND ND

10.01,2,3-Trichlorobenzene 5.0 ND ND ND

10.01,2,4-Trichlorobenzene 5.0 ND ND ND

10.01,1,1-Trichloroethane 5.0 ND ND ND

10.01,1,2-Trichloroethane 5.0 ND ND ND

10.0Trichloroethene 5.0 ND ND ND

10.0Trichlorofluoromethane 5.0 ND ND ND

10.01,2,3-Trichloropropane 5.0 ND ND ND


66662 08/23/2012 SH&W



4Page:ANALYTICAL RESULTS




Date Sampled 08/22/201208/22/2012


Date Prepared 08/24/2012 08/24/2012 08/24/2012





10.01,2,4-Trimethylbenzene 5.0 ND ND ND

10.01,3,5-Trimethylbenzene 5.0 ND ND ND

50Vinyl Acetate 25 ND ND ND

30Vinyl chloride (Chloroethene) 15 ND ND ND

10.0o-Xylene 1.0 ND ND ND

20.0m,p-Xylenes 1.0 ND ND ND

Our Lab I.D. 66662.01 66662.02Method BlankSurrogates %Rec.Limit % Rec. % Rec. % Rec.

Bromofluorobenzene 75-125 95.2 98.9 97.7

Dibromofluoromethane 75-125 97.3 106 96.6

Toluene-d8 75-125 107 103 107

QC Batch No: 082412OB2

66662 08/23/2012 SH&W





5Page:

Ordered By

Attn: Dean Francuch


Telephone: (818)539-8420

Method: (M8015G), TPH as Gasoline and Light Hydrocarbons Using GC/FID



Date Sampled 08/22/201208/22/2012

Dilution Factor 1 1 1Units mg/Kg mg/Kg mg/KgMatrix Soil Soil SoilDate Analyzed 08/24/2012 08/24/2012 08/24/2012

Date Prepared 08/24/2012 08/24/2012 08/24/2012





1.000TPH as Gasoline and Light HC. (C4-C12) 0.100 ND ND ND


Bromofluorobenzene 75-125 93.4 105 111

QC Batch No: 082412DB2

66662 08/23/2012 SH&W





6Page:

Ordered By

Attn: Dean Francuch


Telephone: (818)539-8420

Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GC/FID



Date Sampled 08/22/201208/22/2012


Date Prepared 08/24/2012 08/24/2012 08/24/2012



Preparation Method 3550B 3550B 3550B


5.0TPH as Diesel (C13-C22) 1.0 ND 22.1 ND

5.0TPH as Heavy Hydrocarbons (C23-C40) 1.0 ND 89.9 ND

5.0TPH Total as Diesel and Heavy HC.C13-C40 1.0 ND 112 ND


Chlorobenzene 75-125 93.8 100 97.7

QC Batch No: 0830122C1

66662 08/23/2012 SH&W





7Page:

Ordered By

Attn: Dean Francuch


Telephone: (818)539-8420

Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)



Date Sampled 08/22/201208/22/2012


Date Prepared 08/30/2012 08/30/2012 08/30/2012



Preparation Method 3050B 3050B 3050B


5.0Antimony 1.0 ND ND ND

5.0Arsenic 1.0 ND ND ND

5.0Barium 2.5 ND 52.1 21.3

2.5Beryllium 1.3 ND ND ND

2.5Cadmium 1.3 ND ND ND

5.0Chromium 2.5 ND 9.07 4.10J

5.0Cobalt 2.5 ND 2.80J ND

5.0Copper 2.5 ND 13.5 5.06

5.0Lead 2.5 ND ND ND

0.2Mercury (By EPA 7471) 0.1 ND ND ND

5.0Molybdenum 2.5 ND 4.06J ND

5.0Nickel 2.5 ND 14.4 5.13

5.0Selenium 1.0 ND ND ND

5.0Silver 2.5 ND ND ND

5.0Thallium 1.0 ND ND ND

5.0Vanadium 2.5 ND 19.2 7.18

5.0Zinc 2.5 ND 22.4 9.11

66662 08/23/2012 SH&W





8Page:

Ordered By

Attn: Dean Francuch

Site

Telephone: (818)539-8420




QUALITY CONTROL RESULTS

Analytes

Sample MSMS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD

Result RecovConcen % REC Concen Recov % REC % % Limit % Limit

QC Batch No: 0830122C1; Dup or Spiked Sample: 66703.01; LCS: Clean Sand; QC Prepared: 08/30/2012; QC Analyzed: 08/30/2012;

Units: mg/Kg

Antimony 75-125 <15 0.00 50.0 34.0 M 68.0 50.0 34.9 M 69.8 2.61

Arsenic 75-125 <15 2.89 50.0 46.2 86.6 50.0 46.7 87.6 1.15

Barium 75-125 <15127 50.0 169 84.0 50.0 176 98.0 15.4

Beryllium 75-125 <15 0.00 50.0 46.8 93.6 50.0 47.7 95.4 1.90

Cadmium 75-125 <15 0.00 50.0 42.8 85.6 50.0 44.8 89.6 4.57

Chromium 75-125 <15 11.9 50.0 53.4 83.0 50.0 56.0 88.2 6.07

Cobalt 75-125 <15 3.87 50.0 44.3 80.9 50.0 45.2 82.7 2.20

Copper 75-125 <15 14.2 50.0 56.2 84.0 50.0 58.4 88.4 5.10

Lead 75-125 <15 20.1 50.0 59.2 78.2 50.0 61.1 82.0 4.74

Mercury (By EPA 7471) 75-125 <15 0.00 0.500 0.555 111 0.500 0.555 111 <1

Molybdenum 75-125 <15 0.00 50.0 41.7 83.4 50.0 43.1 86.2 3.30

Nickel 75-125 <15 14.7 50.0 54.8 80.2 50.0 57.1 84.8 5.58

Selenium 75-125 <15 0.00 50.0 43.1 86.2 50.0 43.4 86.8 <1

Silver 75-125 <15 0.00 50.0 43.5 87.0 50.0 45.4 90.8 4.27

Thallium 75-125 <15 0.00 50.0 34.6 M 69.2 50.0 35.6 M 71.2 2.85

Vanadium 75-125 <15 18.9 50.0 62.4 87.0 50.0 65.6 93.4 7.10

Zinc 75-125 <15 63.8 50.0 101 M 74.4 50.0 105 82.4 10.2

Analytes

LCS LCSLCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD

Concen % RECRecov Concen Recov % REC % REC % Limit % Limit


Units: mg/Kg

Antimony <15 50.0 44.7 89.4 50.0 44.6 89.2 <1 75-125

Arsenic <15 50.0 45.3 90.6 50.0 45.1 90.2 <1 75-125

Barium <15 50.0 46.2 92.4 50.0 46.6 93.2 <1 75-125

Beryllium <15 50.0 48.1 96.2 50.0 48.1 96.2 <1 75-125

Cadmium <15 50.0 45.5 91.0 50.0 45.9 91.8 <1 75-125

Chromium <15 50.0 45.7 91.4 50.0 46.0 92.0 <1 75-125

Cobalt <15 50.0 45.4 90.8 50.0 45.6 91.2 <1 75-125

Copper <15 50.0 45.0 90.0 50.0 45.2 90.4 <1 75-125

Lead <15 50.0 44.8 89.6 50.0 44.8 89.6 <1 75-125

66662 08/23/2012 SH&W



9Page:





Analytes




Units: mg/Kg

Mercury (By EPA 7471) <15 0.500 0.545 109 0.500 0.545 109 <1 75-125

Molybdenum <15 50.0 45.6 91.2 50.0 45.9 91.8 <1 75-125

Nickel <15 50.0 45.2 90.4 50.0 45.5 91.0 <1 75-125

Selenium <15 50.0 44.9 89.8 50.0 45.1 90.2 <1 75-125

Silver <15 50.0 45.1 90.2 50.0 45.4 90.8 <1 75-125

Thallium <15 50.0 44.8 89.6 50.0 44.7 89.4 <1 75-125

Vanadium <15 50.0 46.4 92.8 50.0 46.8 93.6 <1 75-125

Zinc <15 50.0 45.2 90.4 50.0 45.4 90.8 <1 75-125

66662 08/23/2012 SH&W





10Page:

Ordered By

Attn: Dean Francuch

Site

Telephone: (818)539-8420





Analytes



QC Batch No: 0824122A1; Dup or Spiked Sample: 66645.06; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012;

Units: ug/Kg

Benzene 75-125 <20 1.49 50.0 48.6 94.2 50.0 47.0 91.0 3.46

Chlorobenzene 75-125 <20 0.00 50.0 52.0 104 50.0 48.6 97.2 6.76

1,1-Dichloroethene 75-125 <20 0.00 50.0 55.0 110 50.0 54.0 108 1.83

Methyl-tert-butyl ether (MTBE) 75-125 <20 0.00 50.0 44.7 89.4 50.0 45.6 91.2 1.99

Toluene (Methyl benzene) 75-125 <20 2.25 50.0 50.8 97.1 50.0 48.5 92.5 4.85

Trichloroethene 75-125 <20 0.00 50.0 55.5 111 50.0 53.0 106 4.61

Surrogates

Bromofluorobenzene 75-125 <20 0.00 50.0 46.4 92.7 50.0 47.3 94.5 1.94

Dibromofluoromethane 75-125 <20 0.00 50.0 46.8 93.6 50.0 47.4 94.7 1.18

Toluene-d8 75-125 <20 0.00 50.0 50.5 101 50.0 50.5 101 <1

Analytes



QC Batch No: 0824122A1; Dup or Spiked Sample: 66645.06; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012;

Units: ug/Kg

Benzene <20 50.0 50.5 101 50.0 51.5 103 1.96 75-125

Chlorobenzene <20 50.0 55.8 112 50.0 56.8 114 1.77 75-125

1,1-Dichloroethene <20 50.0 56.3 113 50.0 57.8 116 2.62 75-125

Methyl-tert-butyl ether (MTBE) <20 50.0 45.1 90.2 50.0 47.2 94.0 4.13 75-125

Toluene (Methyl benzene) <20 50.0 54.0 108 50.0 54.0 108 <1 75-125

Trichloroethene <20 50.0 58.5 117 50.0 58.5 117 <1 75-125

LCS

Chloroform (Trichloromethane) <20 50.0 47.7 95.4 50.0 49.7 99.0 3.70 75-125

Ethylbenzene <20 50.0 55.1 110 50.0 55.5 111 <1 75-125

1,1,1-Trichloroethane <20 50.0 55.7 111 50.0 56.1 112 <1 75-125

o-Xylene <20 50.0 54.3 109 50.0 54.6 109 <1 75-125

m,p-Xylenes <20100 114 114 100 114 114 <1 75-125

Surrogates

Bromofluorobenzene <20 50.0 45.9 91.9 50.0 46.0 91.9 <1 75-125

Dibromofluoromethane <20 50.0 46.9 93.7 50.0 46.6 93.1 <1 75-125

Toluene-d8 <20 50.0 50.5 101 50.0 50.0 100 <1 75-125

66662 08/23/2012 SH&W





11Page:

Ordered By

Attn: Dean Francuch

Site

Telephone: (818)539-8420

Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GC/FID




Analytes



QC Batch No: 082412DB2; Dup or Spiked Sample: 66661.01; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012;

Units: mg/Kg

TPH as Diesel (C13-C22) 75-125 <20 0.00 500 398 79.6 500 478 95.6 18.3

Surrogates

Chlorobenzene 75-125 <20 0.00 100 76.2 76.2 100 89.1 89.1 15.6

Analytes

LCS LCSLCS LCS/LCSD

Concen % RECRecov % Limit

QC Batch No: 082412DB2; Dup or Spiked Sample: 66661.01; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012;

Units: mg/Kg

TPH as Diesel (C13-C22) 500 466 93.2 75-125

Surrogates

Chlorobenzene 100 91.8 91.8 75-125

66662 08/23/2012 SH&W





12Page:

Ordered By

Attn: Dean Francuch

Site

Telephone: (818)539-8420

Method: (M8015G), TPH as Gasoline and Light Hydrocarbons Using GC/FID




Analytes



QC Batch No: 082412OB2; Dup or Spiked Sample: 66647.01A; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/25/2012;

Units: mg/Kg

TPH as Gasoline and Light HC.(C4-C12)

75-125 <20 0.00 1.00 0.840 84.3 1.00 0.870 86.5 2.58

Surrogates

Bromofluorobenzene 75-125 <20 0.00 0.0500 0.0472 94.4 0.0500 0.0481 96.2 1.91

Analytes



QC Batch No: 082412OB2; Dup or Spiked Sample: 66647.01A; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/25/2012;

Units: mg/Kg

TPH as Gasoline and Light HC.(C4-C12)

<20 1.00 0.850 84.5 1.00 0.830 83.1 1.67 75-125

Surrogates

Bromofluorobenzene <20 0.0500 0.0445 89.0 0.0500 0.0459 91.8 3.10 75-125

final addendum - los angeles

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